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HomeMy WebLinkAboutAppendix 11 May 2014 Site Investigation Lab Report American Analytical Laboratories,LLC AMERICAN 56 Toledo Street �NALYTICALL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 Website www American-Analytical com May 12, 2014 Walter Berninger Berninger Environmental, Inc. 90 Knickerbocker Avenue,Unit B Bohemia,NY 11716 TEL: (631) 589-6521 FAX (631) 589-6528 RE: Rt. 48 Southold, 54540 Rt. 48 (Sound Ave), Order No.: 1405040 Dear Walter Berninger: American Analytical Laboratories, LLC. received 8 sample(s) on 5/7/2014 for the analyses presented in the following report. Samples were analyzed in accordance with the test procedures documented on the chain of custody and detailed throughout the text of this report. The results reported herein relate only to the items tested or to the samples as received by the laboratory. This report may not be reproduced, except in full, without the approval of American Analytical Laboratories, LLC and is not considered complete without a cover page and chain of custody documentation. The limits (LOQ)provided in the data package are analytical reporting limits and not Federal or Local mandated values to which the sample results should be compared. There were no problems with the analyses and all data for associated QC met laboratory specifications. If there are any exceptions a Case Narrative is provided in the report or the data is qualified either on the sample results or in the QC section of the report. This package has been reviewed by American Analytical Laboratories' QA Department/Laboratory Director to comply with NELAC standards prior to report submittal. If you have any questions regarding these tests results, please do not hesitate to call (631)454- 6100 or email me directly at lbeyer@american-analytical.com. Sincerely, y"u• it 4 Lori Beyer Lab Director American Analytical Laboratories, LLC. Original Page 1 of 105 AMERICAN American Analytical Laboratories,LLC. Workorder `/T 56 Toledo Street ®NALT t ICAL Farmingdale,New York 11735 Sample Summary LABOR-TORIES TEL•(631)454-6100 FAX.(631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 CLIENT: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Lab SampleID Client Sample ID Tag No Date Collected Date Received Matrix 1405040-OOIA B-1 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-OOIB B-1 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-002A B-2 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-002B B-2 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-003A B-3 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-003B B-3 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-004A GW-2 5/6/2014 5/7/2014 2:15:00 PM Liquid 1405040-004B GW-2 5/6/2014 5/7/2014 2:15:00 PM Liquid 1405040-005A GW-3 5/6/2014 5/7/2014 2:15:00 PM Liquid 1405040-005B GW-3 5/6/2014 5/7/2014 2:15:00 PM Liquid 1405040-006A Drain Pool 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-006B Drain Pool 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-007A Susp. Sepctic @ 10-12.5' 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-007B Susp. Sepctic @ 10-12.5' 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-008A SD-Rear 5/6/2014 5/7/2014 2:15:00 PM Soil 1405040-008B SD-Rear 5/6/2014 5/7/2014 2:15:00 PM Soil Page 2 of 105 Ei�AIVIERICAN CHAIN OF CUSTODY CERTIFICATIONS ANALYTICAL 56 Toledo Street,Farmingdale NY 11735 NY ELAP-11418 PA DEP-68-00573 I.�BOR�TORIES (1)631-454-6100 (F)631-454-8027 NJ DEP-NY050 CT DOH-PH-0205 www.american-analVbGal com . Client Information Project Information _ Analytical Information Company Name ` �� e Project Name l" Address CZ) _ �. Streat �Y, crty state Zln City -State .ap Project Contact I Project# Phone# r \ SamplePs Name!Compa l�J (U E-mail SamplePs Signature LAB Sample Information Sample Co Ion Sample Containers SAMPLE# Number of Each Preserved Bottle (LAB USE ONLY) Client Sample ID STypee Matrix Code Date Time Glasscl Total# z = z = _ o bottles D -ria 1 - 1 - ocj -2— Z Cb3 AD -3 -z- I L X Turnaround Time(Business Days) SAMPLE TYPE MATRIX CODES Comments I Remarks Standard (,� k3-125 7-10 Business Days F---713,Day RUSH G=Grab L=Liquid PC=Paint Chip r 5 Day RUSH �2 Day RUSH C=Composite S=Soil SL=Sludge 4 Day RUSH D1 Day RUSH B=Blank O=Oil SD=Solid W=Wipe M=Miscellaneous Cooler Temp: Sample custody-,must be documented below,each time.samples change possession,with a signature,date,and time. RELIN BY(SIGNATURE) DATE PRINTED NAME RECE) D BY (SIGNATURE) TIME f TIME R IN ISHED BY(SIGNATURE) DATE PRINTED NAME RECEIVED BY LAB(SIGNATURE) DATE PRINTED NAME TIME TIME AMERICAN American Analytical Laboratories,LLC 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX (631)454-8027 Sample Log-In Check List Website www American-Analytical com Client Name Benninger Work Order Number 1405040 RcptNo 1 Logged by- Cate Ferrara 5/7/2014 2:15:00 PM C Vj— Completed By Cate Ferrara 5/7/2014 lC Oii tv-01— Reviewed By* Lori Beyer 5/8/201410:28:05 AM l6K.t Chain of Custody 1. Is Chain of Custody complete? Yes W No ❑ Not Present ❑ 2. How was the sample delivered? Clien Log In 3. Coolers are present? Yes W No ❑ NA ❑ 4. Shipping container/cooler in good condition? Yes ❑d No ❑ Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present ❑d No. Seal Date: Signed By: 5. Was an attempt made to cool the samples? Yes W No ❑ NA ❑ 6. Were all samples received at a temperature of >0°C to 6.0°C Yes ❑d No ❑ NA ❑ 7. Sample(s)in proper container(s)? Yes ❑ No ❑d 8, Sufficient sample volume for indicated test(s)? Yes ❑�/ No ❑ g, Are samples(except VOA and ONG)properly preserved? Yes ❑d No ❑ 10.Was preservative added to bottles? Yes ❑ No ❑d NA ❑ 11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm? Yes ❑d No ❑ No VOA Vials ❑ 12.Were any sample containers received broken? Yes ❑ No ❑� 13. Does paperwork match bottle labels? Yes No ❑ (Note discrepancies on chain of custody) 14.Are matrices correctly identified on Chain of Custody? Yes ❑d No ❑ 15. Is it clear what analyses were requested? Yes ❑./ No ❑ 16.Were all holding times able to be met? Yes No ❑ (If no,notify customer for authorization) Special Handling(if applicable) 17.Was client notified of all discrepancies with this order? Yes ❑ No ❑ NA ❑d Person Notified Date By Whom. Via ❑ eMad ❑ Phone•❑ Fax ❑ In Person Regarding. Client Instructions 18.Additional remarks. Samples were not collected according to Method 5035A. Cooler Information Cooler No I Tem- °C I Condition I Seal Intact I Seal'No I Seal Date I Signed B Page 3 of 105 —AMERICAN .4 merican Analytical Laboratories,LLC Case Narrative 56 W-NALi I ICAL Farmingdale,New YoTolero Street k 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com Date: 5/12/2014 CLIENT: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Samples were analyzed using the methods outlined in the following references: Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, SW846 and additional methods as detailed throughout the text of the report. All method blanks, laboratory spikes, and/or matrix spikes met quality assurance objectives with exceptions notated in this Narrative discussion and/or in the QC Summary Section of the lab report with appropriate qualifiers. Additional quality control information such as surrogate recovery values for organic testing is provided as part of the analytical results. Soil sample results analyzed for Volatile Organics via preparation method SW846 Method 5035A via the Low Level procedures potentially may be estimated, "J" (biased low) since the samples for this test were not collected according to the 5035A Method. Volatile LCS are analyzed with preservatives- HCL/NaHSO4/Methanol depending on level of analysis (high/low)similar to sample analysis. Outliers can be attributed to the presence of chemical preservatives. 2-Chloroethyl vinyl ether readily breaks down under acidic conditions. Samples that are acid preserved, including standards will exhibit breakdown. The data user should take note. SD-Rear SVOA analysis resulted in matrix interferences. As a result of complicated matrix,reporting limits have been elevated(diluted analysis). This sample was selected for MS/MSD analysis and several spike recoveries are outside range. Acceptable LCS was analyzed. The following parameters (if included in this report) are not offered by NY ELAP: VOA 8260 Soil; 1,2,4,5-Tetramethylbenzene, Chlorodifluoromethane, Diisopropyl ether, Ethanol,Freon-114,p- Diethylbenzene,p-Ethyltoluene, Isopropyl Acetate, n-Amyl Acetate, n-Butyl Acetate, n-Propyl Acetate. VOA 8260 Liquid; 1,2,4,5-Tetramethylbenzene, Chlorodifluoromethane, Freon-114,p-Diethylbenzene, p-Ethyltoluene, Isopropyl Acetate, n-Amyl acetate, n-Butyl Acetate,n-Propyl Acetate. Pesticides 8081 Soil; DBCP. Herbicides 8151 Soil; 3,5-Dichlorobenzoic Acid, 4-Nitrophenol, Acifluorfen,Bentazon, Chloramben,DCPA,Picloram .Lachat 10-107-6-1B Ammonia in Soil, SM 2540G Total Volatile Solids, Soil TKN, Soil Organic Nitrogen, Percent Moisture, SM 4500-SO3 B Sulfite in Liquid, Total Sulfur in Soil, Acid Soluble Chloride by ASTMC1152, Water Soluble Chloride by ASTMC1218, Chlorine Demand by SM 2350 B, Total Residual Chlorine in Liquid The test results meet the requirements of the NYSDOH and NELAC standards, except where noted. The information contained in this analytical report is the sole property of American Analytical Laboratories, LLC. Or the client for which this report was issued. The results contained in this report Original Page 4 of 105 AMERICAN American Analytical Laboratories,LLC. Case Narrative 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 WO#: 1405040 LABORATORIES TEL (631)454-6100 FAX.(631)454-8027 Website:www American Analytical com Date: 5/12/2014 CLIENT: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou are only representative of the samples received. The sample receipt checklist is included as part of this lab report. Conditions can vary at different times and at different sampling conditions. American Analytical is not responsible for the use or interpretation of the data included herein. Original Page 5 of 105 AMERICAN American Analytical Laboratories,GLC. Definition Only 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 WO#: 1405040 L�BOR�TORIES TEL (631)454-6100 FAX (631)454-8027 Website.www American-Analytical com Date: 5/12/2014 Definitions: Sample Result and QC Summary Qualifiers-Level I and Level II Reports ND -Not detected at the reporting limit/Limit of Quantitation B -The analyte was detected in the associated method blank. For volatiles, methylene chloride and acetone are common lab contaminants. Data users should consier anything<10x the blank value as artifact. E -The value is above the quantitation range D -Analyte concentration was obtained from diluted analysis or from analysis using reduced sample volume. J -The analyte was detected below the limit of quantitation but greater than the established Limit of Detection(LOD). There is greater uncertainty associated with these results and data should be considered as estimated. U -The compound was analyzed for but not detected. H -Holding time for preparation or analysis has been exceeded. S - Spike recovery is outside accepted recovery limits. R-RPD is outside accepted recovery range. P - Secondary column exceeds 40%difference for GC test. * -Calibration exceeds method requirement. Due to the large number of analytes for organic testing, the method allows 10%of analytes to have%RSD and/or%D to be>20%. LOD-Limit of Detection; the lowest level the analyte can be determined to be statistically different from a blank. LOQ- Limit of Quantitation; the lowest amount of analyte in a sample that can be quantitatively determined with suitable precision and accurary. M-Analyte was manually integrated for GUMS. +- Concentration exceeds regulatory level for TCLP Original Page 6 of 105 American Analytical Laboratories, LLC. Date: 12-Kray-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-1 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-OOIA Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5036A Analyst: LA 1,1,1,2-Tetrachloroethane ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2 40 00 PM 1,1,1-Tnchloroethane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 1,1,2,2-Tetrachloroethane ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2 40 00 PM 1,1,2-Tnchloro-1,2,2-trifluoroethani ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2:40:00 PM 1,1,2-Trichloroethane ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2 4000 PM 1,1-Dichloroethane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2:40.00 PM 1,1-Dichloroethene ND 101 5.0 U Ng/Kg-dry 1 5/8/2014 24000 PM 1,1-Dichloropropene ND 1.01 5.0 U Ng/Kg-dry 1 5/8/2014 2:40:00 PM 1,2,3-Tnchlorobenzene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2 40 00 PM 1,2,3-Tnchloropropane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 1,2,4,5-Tetramethylbenzene ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2 4000 PM 1,2,4-Tnchlorobenzene ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 1,2,4-Tnmethylbenzene ND 1.01 5.0 U ug/Kg-dry 1 5/8/2014 2.40.00 PM 1,2-Dibromo-3-chloropropane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM 1,2-Dibromoethane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM 1,2-Dichlorobenzene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 1,2-Dichloroethane ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2:40:00 PM 1,2-Dichloropropane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40 00 PM 1,3,5-Tnmethylbenzene ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2 40:00 PM 1,3-Dichlorobenzene ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2 40:00 PM 1,3-dichloropropane ND 1 01 50 U pg/Kg-dry 1 5/8/2014 2:40.00 PM 1,4-Dichlorobenzene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 1,4-Dioxane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40:00 PM 2,2-Dichloropropane ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 240:00 PM 2-Butanone ND 5.03 10 U pg/Kg-dry 1 5/8/2014 2:40:00 PM 2-Chloroethyl vinyl ether ND 101 5.0 U' pg/Kg-dry 1 5/8/2014 2 40.00 PM 2-Chlorotoluene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2:40:00 PM 2-Hexanone ND 5.03 10 U pg/Kg-dry 1 5/8/2014 2:40 00 PM 2-Propanol ND 1.01 5 0 U pg/Kg-dry 1 5/8/2014 2:40.00 PM 4-Chlorotoluene ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2:4000 PM 4-Isopropyltoluene ND 1.01 5 0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM 4-Methyl-2-pentanone ND 5.03 10 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Acetone 3.7 1.26 10 BJ' pg/Kg-dry 1 5/8/2014 2 4000 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com e Page 7 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-1 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-OOIA Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA Benzene ND 101 50 U pg/Kg-dry 1 5/8/2014 2 40.00 PM Bromobenzene ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM Bromochloromethane ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2 4000 PM Bromodichloromethane ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2:40 00 PM Bromoform ND 101 5 0 U pg/Kg-dry 1 5/8/2014 240.00 PM Bromomethane ND 101 5.0 U* pg/Kg-dry 1 5/8/2014 2 40 00 PM Carbon disulfide ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM Carbon tetrachloride ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2.40 00 PM Chlorobenzene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2:4000 PM Chlorodifluoromethane ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2:4000 PM Chloroethane ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2.40:00 PM Chloroform ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2:40.00 PM Chloromethane ND 1 01 5.0 U* pg/Kg-dry 1 5/8/2014 2 4000 PM as-1,2-Dichloroethene ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2 4000 PM cis-1,3-Dichloropropene ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2 40:00 PM Cyclohexane ND 2.01 5 0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM Dibromochloromethane ND 1 01 5 0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Dibromomethane ND 1 01 5 0 U pg/Kg-dry 1 5/8/2014 2:40.00 PM Dichlorodifluorometharie ND 101 5.0 U* pg/Kg-dry 1 5/8/2014 2.40 00 PM D isopropyl ether ND 1 01 5 0 U pg/Kg-dry 1 5/8/2014 2:4000 PM Ethanol ND 101 20 U pg/Kg-dry 1 5/8/2014 2.40 00 PM Ethylbenzene ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Freon-114 ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2.40 00 PM Hexachlorobutadiene ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2.40 00 PM Isopropylbenzene ND 1.01 5 0 U pg/Kg-dry 1 5/8/2014 2 40:00 PM m,p-Xylene ND 2.01 10 U pg/Kg-dry 1 5/8/2014 2 40:00 PM Methyl Acetate ND 1 01 50 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Methyl tert-butyl ether ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2:40:00 PM Methylene chloride 6 5 1 01 5 0 B* pg/Kg-dry 1 5/8/2014 2.40.00 PM n-Butylbenzene ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2 40.00 PM n-Propylbenzene ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Naphthalene ND 101 5 0 U pg/Kg-dry 1 5/8/2014 2*40,00 PM o-Xylene ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2.40.00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical com ` e Page 8 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-1 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-OOIA Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW6035A Analyst: LA p-Diethylbenzene ND 101 50 U pg/Kg-dry 1 5/8/2014 2 40 00 PM p-Ethyltoluene ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2 4000 PM sec-Butylbenzene ND 101 50 U pg/Kg-dry 1• 5/8/2014 2:40.00 PM Styrene ND 101 50 U pg/Kg-dry 1 5/8/2014 2.4000 PM t-Butyl alcohol ND 251 50 U* pg/Kg-dry 1 5/8/2014 2 4000 PM tert-Butylbenzene ND 101 50 U pg/Kg-dry 1 5/8/2014 2.40.00 PM Tetrachloroethene ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2 4000 PM Toluene ND 1.01 50 U pg/Kg-dry 1 5/8/2014 2 40 00 PM trans-1,2-Dichloroethene ND 1 01 5.0 U pg/Kg-dry 1 5/8/2014 2 40.00 PM trans-1,3-Dichloropropene ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2 40:00 PM Trichloroethene ND 1.01 5.0 U pg/Kg-dry 1 5/8/2014 2 40 00 PM Trichlorofluoromethane ND 101 50 U pg/Kg-dry 1 5/8/2014 2:40 00 PM Vinyl acetate ND 101 5.0 U* pg/Kg-dry 1 5/8/2014 2 40 00 PM Vinyl chloride ND 101 5.0 U pg/Kg-dry 1 5/8/2014 2:40 00 PM Surr.4-Bromofluorobenzene 100 0 56-133 %REC 1 5/8/2014 2 40 00 PM Surr:Dibromofluorom ethane 104 0 60-132 %REC 1 5/8/2014 2 40 00 PM Surr Toluene-d8 997 0 69-125 %REC 1 5/8/2014 2:4000 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical com ` a Page 9 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-1 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-001 B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 41 1 10 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Tnchlorobenzene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32.00 PM 1,2-Dichlorobenzene ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32 00 PM 1,3-Dichlorobenzene ND 251 250 U pg/Kg-dry 1 5/9/2014 232:00 PM 1,4-Dichlorobenzene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32 00 PM 2,4-Dinitrotoluene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32 00 PM 2,6-Dmitrotoluene ND 503 250 U pg/Kg-dry 1 5/9/2014 2:32.00 PM 2-Chloronaphthalene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32:00 PM 2-Methylnaphthalene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 3200 PM 2-Nitroandme ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32:00 PM 3,3'-Dichlorobenzidine ND 251 250 U pg/Kg-dry 1 5/9/2014 2.3200 PM 3-Nitroantline ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM 4-Bromophenyl phenyl ether ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2.32.00 PM 4-Chloroamline ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM 4-Chlorophenyl phenyl ether ND 251 250 U pg/Kg-dry 1 5/9/2014 232:00 PM 4-Nitroaniline ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Acenaphthene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32.00 PM Acenaphthylene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Aniline ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2.32:00 PM Anthracene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Azobenzene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Benzidine ND 50.3 500 U pg/Kg-dry 1 5/9/2014 2 32:00 PM Benzo(a)anthracene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32.00 PM Benzo(a)pyrene ND 251 150 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Benzo(b)fluoranthene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32.00 PM Benzo(g,h,i)perylene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 3200 PM Benzo(k)fluoranthene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32:00 PM Benzyl alcohol ND 251 250 U pg/Kg-dry 1 5/9/2014 2 3200 PM Bis(2-chloroethoxy)methane ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Bis(2-chloroethyl)ether ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Bis(2-chloroisopropyl)ether ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32 00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.amencan-analytical com Page 10 of 105 a American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-1 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-001B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D • SW3546 Analyst: MH Bis(2-ethylhexyl)phthalate ND 25.1 250 U* pg/Kg-dry 1 5/9/2014 2 32 00 PM Butyl benzyl phthalate ND 25.1 250 U* pg/Kg-dry 1 5/9/2014 2 32 00 PM Carbazole ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Chrysene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2:32.00 PM Dibenzo(a,h)anthracene ND 25.1 150 U pg/Kg-dry 1 5/9/2014 2 3200 PM Dibenzofuran ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2 3200 PM Diethyl phthalate ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2:32:00 PM Dimethyl phthalate ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2.32.00 PM Di-n-butyl phthalate ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32:00 PM Di-n-octyl phthalate ND 50.3 500 U* pg/Kg-dry 1 5/9/2014 2.32.00 PM Fluoranthene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2.32.00 PM Fluorene ND 251 250 U pg/Kg-dry 1 5/9/2014 232.00 PM Hexachlorobenzene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2 32:00 PM Hexachlorobutadiene ND 251 250 U pg/Kg-dry 1 5/9/2014 2.3200 PM Hexachlorocyclopentadiene ND 503 250 U* pg/Kg-dry 1 5/9/2014 2:3200 PM Hexachloroethane ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32:00 PM Indeno(1,2,3-c,d)pyrene ND 251 250 U pg/Kg-dry 1 5/9/2014 2:3200 PM Isophorone ND 251 250 U pg/Kg-dry 1 5/9/2014 2:32 00 PM Naphthalene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2,32 00 PM Nitrobenzene ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32 00 PM N-Nitrosodimethylamine ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM N-N itrosod i-n-propyla mine ND 251 150 U pg/Kg-dry 1 5/9/2014 2 32 00 PM N-Nitrosodiphenylamine ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32.00 PM Phenanthrene ND 25.1 250 U pg/Kg-dry 1 5/9/2014 2.32 00 PM Pyrene ND 251 250 U pg/Kg-dry 1 5/9/2014 2 32 00 PM Pyridine ND 251 250 U pg/Kg-dry 1 5/9/2014 2.32.00 PM Surr.2-Fluorobiphenyl 694 0 21-143 %REC 1 5/9/2014 2 32 00 PM Surr 4-Terphenyl-d14 741 0 15-137 %REC 1 5/9/2014 2 32 00 PM Surr:Nitrobenzene-d5 722 0 17-136 %REC 1 5/9/2014 2 32 00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com = e 4' Page 11 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Benninger Environmental,Inc. Client Sample ID: B-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-002A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA 1,1,1,2-Tetrachloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,1,1-Trichloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08.00 PM 1,1,2,2-Tetrachloroethane ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3.08.00 PM 1,1,2-Tnchloro-1,2,2-tnfluoroethani ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 1,1,2-Trichloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08 00 PM 1,1-Dichloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 1,1-Dichloroethene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 1,1-Dichloropropene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08.00 PM 1,2,3-Trichlorobenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,2,3-Trichloropropane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08 00 PM 1,2,4,5-Tetramethylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08:00 PM 1,2,4-Tnchlorobenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 1,2,4-Tnmethylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08.00 PM 1,2-Dibromo-3-chloropropane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,2-Dibromoethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,2-Dichlorobenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,2-Dichloroethane ND 104 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 1,2-Dichloropropane ND 104 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,3,5-Tnmethylbenzene ND 104 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,3-Dichlorobenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,3-dichloropropane ND 104 52 U pg/Kg-dry 1 5/8/2014 3:08.00 PM 1,4-Dichlorobenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 1,4-Dioxane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3:0800 PM 2,2-Dichloropropane ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3.08 00 PM 2-Butanone ND 518 10 U pg/Kg-dry 1 5/8/2014 3.08 00 PM 2-Chloroethyl vinyl ether ND 104 52 U' pg/Kg-dry 1 5/8/2014 3 0800 PM 2-Chlorotoluene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 0800 PM 2-Hexanone ND 518 10 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 2-Propanol ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08 00 PM 4-Chlorotoluene ND 1 04 5 2 U pg/Kg-dry 1 5/8/2014 3:08 00 PM 4-Isopropyltoluene ND 1 04 5 2 U pg/Kg-dry 1 5/8/2014 3 08 00 PM 4-Methyl-2-pentanone ND 518 10 U pg/Kg-dry 1 5/8/2014 3 08.00 PM Acetone 4 5 129 10 BJ' pg/Kg-dry 1 5/8/2014 3 08 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale, New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com ` e Page 12 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-002A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA Benzene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Bromobenzene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 3 08:00 PM Bromochloromethane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Bromodichloromethane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Bromoform ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Bromomethane ND 1 04 52 U* pg/Kg-dry 1 5/8/2014 3 08 00 PM Carbon disulfide ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08.00 PM Carbon tetrachloride ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Chlorobenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Chlorodifluoromethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Chloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08 00 PM Chloroform ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Chloromethane ND 104 52 U* pg/Kg-dry 1 5/8/2014 3 08 00 PM cis-1,2-Dichloroethene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 308:00 PM cis-1,3-Dichloropropene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 3.08.00 PM Cyclohexane ND 207 5.2 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Dibromochloromethane ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 3 08.00 PM Dibromomethane ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Dichlorodifluoromethane ND 1.04 5.2 U* pg/Kg-dry 1 5/8/2014 3:08:00 PM Dusopropyl ether ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3 08 00 PM Ethanol ND 104 21 U pg/Kg-dry 1 5/8/2014 3:08 00 PM Ethylbenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Freon-114 ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3.08.00 PM Hexachlorobutadiene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3.08 00 PM Isopropylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3,08,00 PM m,p-Xylene ND 207 10 U pg/Kg-dry 1 5/8/2014 3:08:00 PM Methyl Acetate ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08:00 PM Methyl tert-butyl ether ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 308:00 PM Methylene chloride 6.6 1.04 5 2 B* pg/Kg-dry 1 5/8/2014 3:08 00 PM n-Butylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08:00 PM n-Propylbenzene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 308.00 PM Naphthalene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 0800 PM o-Xylene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3.08.00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com e Page 13 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-002A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA p-Diethylbenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 3.08:00 PM p-Ethyltoluene ND 104 52 U pg/Kg-dry 1 5/8/2014 3 08 00 PM sec-Butylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM Styrene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 3:0800 PM t-Butyl alcohol ND 259 52 U" pg/Kg-dry 1 5/8/2014 3:08 00 PM tert-Butylbenzene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08.00 PM Tetrachloroethene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3:08 00 PM Toluene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 308.00 PM trans-1,2-Dichloroethene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3 08.00 PM trans-1,3-Dichloropropene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Trichloroethene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 3.08.00 PM Trichlorofluoromethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 3.08:00 PM Vinyl acetate ND 1 04 52 U' pg/Kg-dry 1 5/8/2014 3 0800 PM Vinyl chloride ND 104 52 U pg/Kg-dry 1 5/8/2014 3 0800 PM Surr:4-Bromofluorobenzene 101 0 56-133 %REC 1 5/8/2014 3 0800 PM Surr:Di bromofluorom ethane 104 0 60-132 %REC 1 5/8/2014 3.08.00 PM Surr Toluene-d8 100 0 69-125 %REC 1 5/8/2014 3 08.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com ' Page 14 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-002B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 4.0 1 1.0 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Trichlorobenzene ND 255 250 U pg/Kg-dry 1 5/9/2014 2.57 00 PM 1,2-Dichlorobenzene ND 25.5 250 U pg/Kg-dry 1 5/9/20142.57.00PM 1,3-Dichlorobenzene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57.00 PM 1,4-Dichlorobenzene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57.00 PM 2,4-Dinitrotoluene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57.00 PM 2,6-Dmitrotoluene ND 509 250 U pg/Kg-dry 1 5/9/2014 2:57.00 PM 2-Chloronaphthalene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM 2-Methylnaphthalene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM 2-Nitroaniline ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:5700 PM 3,3 Dichlorobenzidine ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57:00 PM 3-Nitroaniline ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2-57*00 PM 4-Bromophenyl phenyl ether ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57:00 PM 4-Chloroaniline ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57 00 PM 4-Chlorophenyl phenyl ether ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57:00 PM 4-Nitroaniline ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:57:00 PM Acenaphthene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Acenaphthylene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Aniline ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:57:00 PM Anthracene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM Azobenzene ND 255 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Benzidine ND 50.9 510 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Benzo(a)anthracene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 257:00 PM Benzo(a)pyrene ND 255 150 U pg/Kg-dry 1 5/9/2014 2.57.00 PM Benzo(b)fluoranthene ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57:00 PM Benzo(g,h,i)perylene ND 255 250 U pg/Kg-dry 1 5/9/2014 2:5700 PM Benzo(k)fluoranthene ND 255 250 U pg/Kg-dry 1 5/9/2014 2:5700 PM Benzyl alcohol ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:57.00 PM Bis(2-ch loroethoxy)m ethane ND 255 250 U pg/Kg-dry 1 5/9/2014 257.00 PM Bis(2-chloroethyl)ether ND 25.5 250 U pg/Kg-dry- 1 5/9/2014 2.57 00 PM Bis(2-chloroisopropyl)ether ND 255 250 U pg/Kg-dry 1 5/9/2014 2.57.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 , Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com Page 15 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-002B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Bis(2-ethylhexyl)phthalate ND 25.5 250 U' pg/Kg-dry 1 5/9/2014 2 57 00 PM Butyl benzyl phthalate ND 25.5 250 U` pg/Kg-dry 1 5/9/2014 2.57 00 PM Carbazole ND 255 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Chrysene ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57 00 PM Dibenzo(a,h)anthracene ND 255 150 U pg/Kg-dry 1 5/9/2014 2:57.00 PM Dibenzofuran ND 255 250 U pg/Kg-dry 1 5/9/2014 2:5700 PM Diethyl phthalate ND 255 250 U pg/Kg-dry 1 5/9/2014 257:00 PM Dimethyl phthalate ND 255 250 U pg/Kg-dry 1 5/9/2014 2 5700 PM Di-n-butyl phthalate ND 255 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM Di-n-octyl phthalate ND 509 510 U' pg/Kg-dry 1 5/9/2014 2 57 00 PM Fluoranthene ND 255 250 U pg/Kg-dry 1 5/9/2014 2 5700 PM Fluorene ND 255 250 U pg/Kg-dry 1 5/9/2014 2 57 00 PM Hexachlorobenzene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:57.00 PM Hexachlorobutadiene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2:57 00 PM Hexachlorocyclopentadiene ND 50.9 250 U' pg/Kg-dry 1 5/9/2014 2*57*00 PM Hexachloroethane ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57.00 PM Indeno(1,2,3-c,d)pyrene ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57 00 PM Isophorone ND 255 250 U pg/Kg-dry 1 5/9/2014 2:5700 PM Naphthalene ND 255 250 U pg/Kg-dry 1 5/9/2014 2*57,00 PM Nitrobenzene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.57 00 PM N-Nitrosodimethylamine ND 255 250 U pg/Kg-dry 1 5/9/2014 2:57.00 PM N-Nitrosodi-n-propylamme ND 255 150 U pg/Kg-dry 1 5/9/2014 2.57 00 PM N-Nitrosodiphenylamine ND 255 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM Phenanthrene ND 25.5 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM Pyrene ND 255 250 U pg/Kg-dry 1 5/9/2014 2.5700 PM Pyndme ND 255 250 U pg/Kg-dry 1 5/9/2014 2 5700 PM Surr.2-Fluorobiphenyl 71.2 0 21-143 %REC 1 5/9/2014 2 5700 PM Surr:4-Terphenyl-d14 74.4 0 15-137 %REC 1 5/9/2014 2 57.00 PM Surr:Nitrobenzene-d5 324 0 17-136 %REC 1 5/9/2014 2 57 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com vp Page 16 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-003A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA 1,1,1,2-Tetrachloroethane ND 103 51 U pg/Kg-dry 1 5/8/2014 3:36.00 PM 1,1,1-Trichloroethane ND 103 5.1 U pg/Kg-dry 1 5/8/2014 3.36:00 PM 1,1,2,2-Tetrachloroethane ND 103 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,1,2-Tnchloro-1,2,2-tnfluoroethani ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,1,2-Trichloroethane ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM 1,1-Dichloroethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,1-Dichloroethene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3.36.00 PM 1,1-Dichloropropene ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 336.00 PM 1,2,3-Trichlorobenzene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,2,3-Tnchloropropane ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM 1,2,4,5-Tetramethylbenzene ND 103 51 U pg/Kg-dry 1 5/8/2014 3.36 00 PM 1,2,4-Trichlorobenzene ND 103 5.1 U pg/Kg-dry 1 5/8/2014 3.36 00 PM 1,2,4-Tnmethylbenzene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,2-Dibromo-3-chloropropane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3*36 00 PM 1,2-Dibromoethane ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,2-Dichlorobenzene ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3:36:00 PM 1,2-Dichloroethane ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 1,2-Dichloropropane ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3:36:00 PM 1,3,5-Tnmethylbenzene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM 1,3-Dichlorobenzene ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3.36:00 PM 1,3-dichloropropane ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3:36:00 PM 1,4-Dichlorobenzene ND 103 5.1 U pg/Kg-dry 1 5/8/2014 3 36.00 PM 1,4-Dioxane ND 103 5.1 U pg/Kg-dry 1 5/8/2014 3:36:00 PM 2,2-Dichloropropane ND 103 5.1 U pg/Kg-dry 1 5/8/2014 3:36:00 PM 2-Butanone ND 5.15 10 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 2-Chloroethyl vinyl ether ND 103 51 U' pg/Kg-dry 1 5/8/2014 3 36.00 PM 2-Chlorotoluene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3,36,00 PM 2-Hexanone ND 5.15 10 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 2-Propanol ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM 4-Chlorotoluene ND 103 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM 4-Isopropyltoluene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 336:00 PM 4-Methyl-2-pentanone ND 5.15 10 U pg/Kg-dry 1 5/8/2014 3:36.00 PM Acetone 4.0 1.29 10 BJ' pg/Kg-dry 1 5/8/2014 3.36.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 QP Tel-(631)454-6100 Fax-(631)454-8027 wwwamerican-analytical.com Page 17 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-003A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW6035A Analyst: LA Benzene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM Bromobenzene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 336.00 PM Bromochloromethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM Bromodichloromethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36 00 PM Bromoform ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36 00 PM Bromomethane ND 103 51 U* pg/Kg-dry 1 5/8/2014 3 36:00 PM Carbon disulfide ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36.00 PM Carbon tetrachloride ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36:00 PM Chlorobenzene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36 00 PM Chlorodifluorom ethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36.00 PM Chloroethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3.3600 PM Chloroform ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3,36*00 PM Chloromethane ND 1.03 51 U* pg/Kg-dry 1 5/8/2014 3.36 00 PM cis-1,2-Dichloroethene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 336.00 PM cis-1,3-Dichloropropene ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3.36.00 PM Cyclohexane ND 206 51 U pg/Kg-dry 1 5/8/2014 3.36 00 PM Dibromochloromethane ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3:36.00 PM Dibromomethane ND 103 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM Dichlorodifluoromethane ND 1 03 51 U* pg/Kg-dry 1 5/8/2014 336:00 PM Diisopropyl ether ND 1 03 51 U pg/Kg-dry 1 5/8/2014 336:00 PM Ethanol ND 10.3 21 U pg/Kg-dry 1 5/8/2014 3 36:00 PM Ethylbenzene ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3.36.00 PM Freon-114 ND 103 51 U pg/Kg-dry 1 5/8/2014 3.36 00 PM Hexachlorobutadiene ND 103 51 U pg/Kg-dry 1 5/8/2014 3,36*00 PM Isopropylbenzene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM m,p-Xylene ND 206 10 U pg/Kg-dry 1 5/8/2014 3.36.00 PM Methyl Acetate ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3:36.00 PM Methyl tert-butyl ether ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM Methylene chloride 6 7 1 03 51 B* pg/Kg-dry 1 5/8/2014 3.3600 PM n-Butylbenzene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 3600 PM n-Propylbenzene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM Naphthalene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3:36 00 PM o-Xylene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3.36.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.amencan-analytical com Page 18 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Benninger Environmental,Inc. Client Sample ID: B-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-003A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA p-Diethylbenzene ND 1.03 5.1 U pg/Kg-dry 1 5/8/2014 3.36.00 PM p-Ethyltoluene ND 103 51 U pg/Kg-dry 1 5/8/2014 3.36.00 PM sec-Butylbenzene ND 103 51 U pg/Kg-dry 1 5/8/2014 3.36 00 PM Styrene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3.36.00 PM t-Butyl alcohol ND 257 51 U* pg/Kg-dry 1 5/8/2014 3:36:00 PM tert-Butylbenzene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3.3600 PM Tetrachloroethene ND 1 03 51 U pg/Kg-dry 1 5/8/2014 3.36:00 PM Toluene ND 1.03 5.1 U pg/Kg-dry 1 5/8/2014 3 3600 PM trans-1,2-Dichloroethene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM trans-1,3-Dichloropropene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM Trichloroethene ND 1.03 51 U pg/Kg-dry 1 5/8/2014 3 36 00 PM Trichlorofluoromethane ND 1 03 5.1 U pg/Kg-dry 1 5/8/2014 3 36:00 PM Vinyl acetate ND 103 5.1 U* pg/Kg-dry 1 5/8/2014 3 36 00 PM Vinyl chloride ND 103 51 U pg/Kg-dry 1 5/8/2014 3.36:00 PM Surr 4-Bromofluorobenzene 98.8 0 56-133 %REC 1 5/8/2014 3:36 00 PM Surr Dibromofluoromethane 103 0 60-132 %REC 1 5/8/2014 3:3600 PM Surr Toluene-d8 99.2 0 69-125 %REC 1 5/8/2014 3 3600 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com e Page 19 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-003B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 35 1 1 0 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Tnchlorobenzene ND 254 250 U pg/Kg-dry 1 5/9/2014 3*21,00 PM 1,2-Dichlorobenzene ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21:00 PM 1,3-Dichlorobenzene ND 254 250 U pg/Kg-dry 1 5/9/2014 321:00 PM 1,4-Dichlorobenzene ND 254 250 U pg/Kg-dry 1 5/9/2014321.00 PM 2,4-Dinitrotoluene ND 254 250 U pg/Kg-dry 1 5/9/2014 3.2100 PM 2,6-Dinitrotoluene ND 50.8 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM 2-Chloronaphthalene ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21.00 PM 2-Methylnaphthalene ND 254 250 U pg/Kg-dry 1 5/9/2014 3:2100 PM 2-Nitroaniline ND 254 250 U pg/Kg-dry 1 5/9/2014 321.00 PM 3,3'-Dichlorobenzidine ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM 3-Nitroamline ND 254 250 U pg/Kg-dry 1 5/9/2014 3 2100 PM 4-Bromophenyl phenyl ether ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM 4-Chloroarnline ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM 4-Chlorophenyl phenyl ether ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21:00 PM 4-Nitroamime ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Acenaphthene ND 254 250 U pg/Kg-dry 1 5/9/2014 3:21.00 PM Acenaphthylene ND 254 250 U pg/Kg-dry 1 5/9/2014 3:21.00 PM Aniline ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Anthracene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM Azobenzene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3:21.00 PM Benzidine ND 508 510 U pg/Kg-dry 1 5/9/2014 3.21.00 PM Benzo(a)anthracene ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21.00 PM Benzo(a)pyrene ND 25.4 150 U pg/Kg-dry 1 5/9/2014 3,21,00 PM Benzo(b)fluoranthene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 2100 PM Benzo(g,h,i)perylene ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM Benzo(k)fluoranthene ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21.00 PM Benzyl alcohol ND 25 4 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM Bis(2-chloroethoxy)methane ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21.00 PM Bis(2-chloroethyl)ether ND 25.4 250 U pg/Kg-dry 1 5/9/2014 321:00 PM Bis(2-chloroisopropyl)ether ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3-2100 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical coin e �n Page 20 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: B-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-003B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst. MH Bis(2-ethylhexyl)phthalate ND 254 250 U* pg/Kg-dry 1 5/9/2014 3.21.00 PM Butyl benzyl phthalate ND 254 250 U* pg/Kg-dry 1 5/9/2014 3.21 00 PM Carbazole ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21:00 PM Chrysene ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21.00 PM Dibenzo(a,h)anthracene ND 25.4 150 U pg/Kg-dry 1 5/9/2014 3 21.00 PM Dibenzofuran ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Diethyl phthalate ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Dimethyl phthalate ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21 00 PM Di-n-butyl phthalate ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3.21.00 PM Di-n-octyl phthalate ND 50.8 510 U* pg/Kg-dry 1 5/9/2014 3 21 00 PM Fluoranthene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Fluorene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Hexachlorobenzene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3,21,00 PM Hexachlorobutadiene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Hexachlorocyclopentadiene ND 50.8 250 U* pg/Kg-dry 1 5/9/2014 3 21 00 PM Hexachloroethane ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM Indeno(1,2,3-c,d)pyrene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3.21.00 PM Isophorone ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3.21:00 PM Naphthalene ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21-00 PM Nitrobenzene ND 254 250 U pg/Kg-dry 1 5/9/2014 3 21 00 PM N-Nitrosodimethylamine ND 254 250 U pg/Kg-dry 1 5/9/2014 3-21-00 PM N-Nitrosodi-n-propylamine ND 254 150 U pg/Kg-dry 1 5/9/2014 321:00 PM N-Nitrosodiphenylamine ND 254 250 U pg/Kg-dry 1 5/9/2014 3.21:00 PM Phenanthrene ND 25.4 250 U pg/Kg-dry 1 5/9/2014 3:21:00 PM Pyrene ND 254 250 U pg/Kg-dry 1 5/9/2014 3:21 00 PM Pyridine ND 254 250 U pg/Kg-dry 1 5/9/2014 3:21:00 PM Surr.2-Fluorobiphenyl 71 3 0 21-143 %REC 1 5/9/2014 3:21:00 PM Surr 4-Terphenyl-d14 789 0 15-137 %REC 1 5/9/2014 3:21.00 PM Surr:Nitrobenzene-d5 729 0 17-136 %REC 1 5/9/2014 3:21:00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale, New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com ` e Page 21 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-004A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst: LA 1,1,1,2-Tetrachloroethane ND 05 20 U pg/L 1 5/8/2014 9.39 00 PM 1,1,1-Trichloroethane ND 05 2.0 U pg/L 1 5/8/2014 939:00 PM 1,1,2,2-Tetrachloroethane ND 0.5 20 U pg/L 1 5/8/2014 9.39.00 PM 1,1,2-Trichloro-1,2,2-tnfluoroethani ND 0.5 20 U pg/L 1 5/8/2014 9:3900 PM 1,1,2-Trichloroethane ND 05 20 U pg/L 1 5/8/2014 9 39:00 PM 1,1-Dichloroethane ND 05 2.0 U pg/L 1 5/8/2014 9 3900 PM 1,1-Dichloroethene ND 05 2.0 U pg/L 1 5/8/2014 9 3900 PM 1,1-Dichloropropene ND 05 20 U pg/L 1 5/8/2014 9.39.00 PM 1,2,3-Trichlorobenzene ND 05 20 U pg/L 1 5/8/2014 9:39 00 PM 1,2,3-Tnchloropropane ND 05 20 U pg/L 1 5/8/2014 9:39 00 PM 1,2,4,5-Tetramethylbenzene ND 0.5 20 U pg/L 1 5/8/2014 9:39:00 PM 1,2,4-Trichlorobenzene ND 0.5 20 U pg/L 1 5/8/2014 9:39.00 PM 1,2,4-Tnmethylbenzene ND 0.5 20 U pg/L 1 5/8/2014 9:39.00 PM 1,2-Dibromo-3-chloropropane ND 05 20 U pg/L 1 5/8/2014 9:39 00 PM 1,2-Dibromoethane ND 05 20 U pg/L 1 5/8/2014 9:39:00 PM 1,2-Dichlorobenzene ND 0.5 20 U pg/L 1 5/8/2014 9:39.00 PM 1,2-Dichloroethane ND 05 20 U pg/L 1 5/8/2014 9 3900 PM 1,2-Dichloropropane ND 05 2.0 U pg/L 1 5/8/2014 9.39:00 PM 1,3,5-Tnmethyl benzene ND 05 2.0 U pg/L 1 5/8/2014 9:39 00 PM 1,3-Dichlorobenzene ND 05 20 U pg/L 1 5/8/2014 9 3900 PM 1,3-dichloropropane ND 05 2.0 U pg/L 1 5/8/2014 9.39:00 PM 1,4-Dichlorobenzene ND 0.5 20 U pg/L 1 5/8/2014 9 39.00 PM 1,4-Dioxane ND 05 20 U pg/L 1 5/8/2014 9 3900 PM 2,2-Dichloropropane ND 0.5 20 U pg/L 1 5/8/2014 9:39 00 PM 2-Butanone ND 1.25 50 U pg/L 1 5/8/2014 9 39 00 PM 2-Chloroethyl vinyl ether ND 1 40 U pg/L 1 5/8/2014 9:39 00 PM 2-Chlorotoluene ND 05 20 U pg/L 1 5/8/2014 9 39.00 PM 2-Hexanone ND 1 25 5 0 U pg/L 1 5/8/2014 939:00 PM 2-Propanol ND 0 5 2 0 U pg/L 1 5/8/2014 9,39,00 PM 4-Chlorotoluene ND 0 5 2 0 U pg/L 1 5/8/2014 9:39 00 PM 4-Isopropyltoluene ND 0.5 2 0 U pg/L 1 5/8/2014 9:39:00 PM 4-Methyl-2-pentanone ND 1.25 5 0 U pg/L 1 5/8/2014 9 39:00 PM Acetone 2 1 125 5.0 BJ` pg/L 1 5/8/2014 9 39.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical com P y° e Page 22 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-004A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst: LA Benzene ND 0 5 2.0 U pg/L 1 5/8/2014 9:39:00 PM Bromobenzene ND 05 2 0 U pg/L 1 5/8/2014 9:39:00 PM Bromochloromethane ND 05 2 0 U pg/L 1 5/8/2014 9,39*00 PM Bromodichloromethane ND 05 2 0 U pg/L 1 5/8/2014 9 39 00 PM Bromoform ND 05 2 0 U pg/L 1 5/8/2014 9 39 00 PM Bromomethane ND 1 4 0 U* pg/L 1 5/8/2014 9.39.00 PM Carbon disulfide ND 0.5 2.0 U pg/L 1 5/8/2014 9.39 00 PM Carbon tetrachloride ND 05 2.0 U pg/L 1 5/8/2014 9 39 00 PM Chlorobenzene ND 05 2 0 U pg/L 1 5/8/2014 9 39.00 PM Chlorodifluoromethane ND 05 2 0 U* pg/L 1 5/8/2014 9 39.00 PM Chloroethane ND 05 2 0 U pg/L 1 5/8/2014 9 39 00 PM Chloroform ND 0.5 2 0 U pg/L 1 5/8/2014 9.39.00 PM Chloromethane ND 05 2.0 U pg/L 1 5/8/2014 9:39:00 PM cis-1,2-Dichloroethene ND 0.5 2.0 U pg/L 1 5/8/2014 9.39:00 PM cis-1,3-Dichloropropene ND 0.5 2.0 U pg/L 1 5/8/2014 9:39:00 PM Cyclohexane ND 0.5 2.0 U pg/L 1 5/8/2014 9:39:00 PM Dibromochloromethane ND 0 5 2 0 U pg/L 1 5/8/2014 9:39:00 PM Dibromomethane ND 05 2 0 U pg/L 1 5/8/2014 9 39 00 PM Dichlorodifluoromethane ND 05 2.0 U pg/L 1 5/8/2014 9,39 00 PM Dusopropyl ether ND 05 2 0 U pg/L 1 5/8/2014 9:39.00 PM Ethanol ND 25 10 U pg/L 1 5/8/2014 9.39:00 PM Ethylbenzene ND 05 2.0 U pg/L 1 5/8/2014 9.39:00 PM Freon-114 ND 0.5 2.0 U pg/L 1 5/8/2014 9.39:00 PM Hexachlorobutadiene ND 0.5 2.0 U pg/L 1 5/8/2014 9:39:00 PM Isopropylbenzene ND 0.5 2.0 U pg/L 1 5/8/2014 9:3900 PM m,p-Xylene ND 1 4.0 U pg/L 1 5/8/2014 9 39 00 PM Methyl Acetate ND 0 5 2 0 U pg/L 1 5/8/2014 9 39 00 PM Methyl tert-butyl ether ND 05 2 0 U pg/L 1 5/8/2014 9.39.00 PM Methylene chloride 2 5 05 2.0 B* pg/L 1 5/8/2014 9 39 00 PM n-Butylbenzene ND 0 5 2 0 U pg/L 1 5/8/2014 9 39:00 PM n-Propylbenzene ND 05 2 0 U pg/L 1 5/8/2014 9:39:00 PM Naphthalene ND 0.5 2.0 U pg/L 1 5/8/2014 9:39.00 PM o-Xylene ND 05 2.0 U pg/L 1 5/8/2014 9.39 00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.amencan-analytical com Page 23 of 105 i American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Benninger Environmental,Inc. Client Sample ID: GW-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-004A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst. LA p-Diethyl benzene ND 05 20 U pg/L 1 5/8/2014 9 39:00 PM p-Ethyltoluene ND 05 20 U pg/L 1 5/8/2014 939:00 PM sec-Butyl benzene ND 05 20 U pg/L 1 5/8/2014 9.39 00 PM Styrene ND 0.5 20 U pg/L 1 5/8/2014 9:39 00 PM t-Butyl alcohol ND 25 10 U pg/L 1 5/8/2014 9:39.00 PM tert-Butylbenzene ND 05 2.0 U pg/L 1 5/8/2014 9:39.00 PM Tetrachloroethene ND 05 20 U pg/L 1 5/8/2014 939:00 PM Toluene 098 05 20 J pg/L 1 5/8/2014 9.39.00 PM trans-1,2-Dichloroethene ND 0.5 20 U pg/L 1 5/8/2014 9.39:00 PM trans-1,3-Dichloropropene ND 05 20 U pg/L 1 5/8/2014 9:39:00 PM Trichloroethene ND 0.5 20 U pg/L 1 5/8/2014 9:39:00 PM Tnchlorofluoromethane ND 0.5 20 U pg/L 1 5/8/2014 9 3900 PM Vinyl acetate ND 05 20 U' pg/L 1 5/8/2014 9.39:00 PM Vinyl chloride ND 05 2.0 U pg/L 1 5/8/2014 9 3900 PM Surr.4-Bromofluorobenzene 101 0 70-128 %REC 1 5/8/2014 9.39,00 PM Surr.Dibromofluorom ethane 99.7 0 75-129 %REC 1 5/8/2014 9,39*00 PM Surr Toluene-d8 101 0 70-124 %REC 1 5/8/2014 9 39.00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com = ' Page 24 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-004B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270(BN) SW8270D SW3510C Analyst: MH 1,2,4-Tnchlorobenzene ND 05 50 U pg/L 1 5/9/2014 11:2000 AM 1,2-Dichlorobenzene ND 05 50 U pg/L 1 5/9/2014 11.20.00 AM 1,3-Dichlorobenzene ND 0.5 50 U pg/L 1 5/9/2014 11 20 00 AM 1,4-Dichlorobenzene ND 05 50 U pg/L 1 5/9/2014 11*20*00 AM 2,4-Dimtrotoluene ND 05 50 U pg/L 1 5/9/2014 11.20.00 AM 2,6-Dinitrotoluene ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM 2-Chloronaphthalene ND 0.5 50 U pg/L 1 5/9/2014 11.20.00 AM 2-Methylnaphthalene ND 05 50 U pg/L 1 5/9/2014 11:2000 AM 2-Nitroaniline ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM 3,3'-Dichlorobenzidine ND 0.5 5.0 U pg/L 1 5/9/2014 11 20.00 AM 3-Nitroamlme ND 0.5 50 U pg/L 1 5/9/2014 11 20.00 AM 4-Bromophenyl phenyl ether ND 0.5 5.0 U pg/L 1 5/9/2014 11 20 00 AM 4-Chloroamline ND 05 50 U pg/L 1 5/9/2014 11.20 00 AM 4-Chlorophenyl phenyl ether ND 0.5 5.0 U pg/L 1 5/9/2014 11 20 00 AM 4-Nitroarnline ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM Acenaphthene ND 0.5 5.0 U pg/L 1 5/9/2014 11 20 00 AM Acenaphthylene ND 05 5.0 U pg/L 1 5/9/2014 11 2000 AM Aniline ND 05 50 U pg/L 1 5/9/2014 11:20:00 AM Anthracene ND 0.5 50 U pg/L 1 5/9/2014 11.20 00 AM Azobenzene ND 0 5 5.0 U pg/L 1 5/9/2014 11 20 00 AM Benzidine ND 1 10 U pg/L 1 5/9/2014 1120:00 AM Benzo(a)anthracene ND 05 5 0 U pg/L 1 5/9/2014 11,20:00 AM Benzo(a)pyrene ND 0 5 5 0 U pg/L 1 5/9/2014 11:20:00 AM Benzo(b)fluoranthene ND 05 5 0 U pg/L 1 5/9/2014 11:20.00 AM Benzo(g,h,i)perylene ND 0 5 5.0 U pg/L 1 5/9/2014 11.20 00 AM Benzo(k)fluoranthene ND 0 5 5.0 U pg/L 1 5/9/2014 11.20 00 AM Benzyl alcohol ND 0 5 5.0 U pg/L 1 5/9/201411 20 00 AM Bis(2-chloroethoxy)methane ND 0 5 5.0 U pg/L 1 5/9/201411 20 00 AM Bis(2-chloroethyl)ether ND 0 5 5.0 U pg/L 1 5/9/201411 20 00 AM Bis(2-chloroisopropyl)ether ND 0 5 5.0 U pg/L 1 5/9/201411 20.00 AM Bis(2-ethylhexyl)phthalate 0 61 0 5 5.0 J pg/L 1 5/9/201411 2000 AM Butyl benzyl phthalate ND 0.5 5.0 U pg/L 1 5/9/201411 20:00 AM Carbazole ND 0.5 5.0 U pg/L 1 5/9/2014 11:20 00 AM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com . e Page 25 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-2 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-004B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270(BN) SW8270D SW3510C Analyst: MH Chrysene ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM Dibenzo(a,h)anthracene ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM Dibenzofuran ND 05 50 U pg/L 1 5/9/2014 11:20 00 AM Diethyl phthalate ND 05 50 U pg/L 1 5/9/2014 11 20 00 AM Dimethyl phthalate ND 05 50 U pg/L 1 5/9/2014 11.20 00 AM Di-n-butyl phthalate ND 05 50 U pg/L 1 5/9/2014 11-20:00 AM Di-n-octyl phthalate ND 05 5.0 U pg/L 1 5/9/201411 20:00 AM Fluoranthene ND 05 50 U pg/L 1 5/9/201411 2000 AM Fluorene ND 0.5 50 U pg/L 1 5/9/2014 11 20 00 AM Hexachlorobenzene ND 0.5 50 U pg/L 1 5/9/2014 11 20 00 AM Hexachlorobutadiene ND 0.5 50 U pg/L 1 5/9/2014 11 20 00 AM Hexachlorocyclopentadiene ND 1 10 U pg/L 1 5/9/2014 11 20.00 AM Hexachloroethane ND 05 50 U pg/L 1 5/9/2014 11.20 00 AM Indeno(1,2,3-c,d)pyrene ND 06 5.0 U pg/L 1 5/9/2014 11.20.00 AM Isophorone ND 05 5.0 U pg/L 1 5/9/2014 11.20:00 AM Naphthalene ND 05 50 U pg/L 1 5/9/2014 11:20 00 AM Nitrobenzene ND 05 50 U pg/L 1 5/9/2014 11.20 00 AM N-Nitrosodimethylamme ND 05 50 U pg/L 1 5/9/2014 11:20.00 AM N-Nitrosodi-n-propylamine ND 05 50 U pg/L 1 5/9/2014 11:20.00 AM N-Nitrosodiphenylamine ND 05 50 U pg/L 1 5/9/2014 11:20 00 AM Phenanthrene ND 0.5 50 U pg/L 1 5/9/2014 11.20 00 AM Pyrene ND 05 50 U pg/L 1 5/9/2014 11 20.00 AM Pyndme ND 0.5 5.0 U pg/L 1 5/9/2014 11:20.00 AM Surr.2-Fluorobiphenyl 810 0 22-134 %REC 1 5/9/2014 11 20:00 AM Sum 4-Terphenyl-d14 829 0 20-144 %REC 1 5/9/2014 11 2000 AM Surr.Nitrobenzene-d5 779 0 21-146 %REC 1 5/9/2014 11:20 00 AM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com a _ e Page 26 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-005A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst. LA 1,1,1,2-Tetrachloroethane ND 05 20 U pg/L 1 5/8/2014 1007 00 PM 1,1,1-Trichloroethane ND 05 20 U pg/L 1 5/8/2014 10 07.00 PM 1,1,2,2-Tetrachloroethane ND 05 20 U pg/L 1 5/8/2014 10:07.00 PM 1,1,2-Trichloro-1,2,2-tnfluoroethan ND 0.5 2.0 U pg/L 1 5/8/2014 10 07 00 PM 1,1,2-Trichloroethane ND 05 20 U pg/L 1 5/8/2014 10.07.00 PM 1,1-Dichloroethane ND 05 20 U pg/L 1 5/8/2014 10 07 00 PM 1,1-Dichloroethene ND 0.5 2.0 U pg/L 1 5/8/2014 10.07.00 PM 1,1-Dichloropropene ND 0.5 2.0 U pg/L 1 5/8/2014 10 07 00 PM 1,2,3-Tnchlorobenzene ND 0.5 20 U pg/L 1 5/8/2014 10:07:00 PM 1,2,3-Tnchloropropane ND 0.5 20 U pg/L 1 5/8/2014 10.07.00 PM 1,2,4,5-Tetramethylbenzene ND 0.5 20 U pg/L 1 5/8/2014 10:07:00 PM 1,2,4-Tnchlorobenzene ND 05 20 U pg/L 1 5/8/2014 10.07:00 PM 1,2,4-Tnmethylbenzene ND 0.5 2.0 U pg/L 1 5/8/2014 10:07:00 PM 1,2-Dibromo-3-chloropropane ND 05 20 U pg/L 1 5/8/2014 10 07.00 PM 1,2-Dibromoethane ND 0.5 20 U pg/L 1 5/8/2014 10.07 00 PM - 1,2-Dichlorobenzene ND 0.5 2.0 U pg/L 1 5/8/2014 1007 00 PM 1,2-Dichloroethane ND 0.5 20 U pg/L 1 5/8/2014 10 07 00 PM 1,2-Dichloropropane ND 05 2.0 U pg/L 1 5/8/2014 10,07*00 PM 1,3,5-Tnmethylbenzene ND 05 20 U pg/L 1 5/8/2014 10:07:00 PM 1,3-Dichlorobenzene ND 05 20 U pg/L 1 5/8/2014 10 07 00 PM 1,3-dichloropropane ND 05 20 U pg/L 1 5/8/2014 10 07 00 PM 1,4-Dichlorobenzene ND 0.5 2.0 U pg/L 1 5/8/2014 10,07,00 PM 1,4-Dioxane ND 0.5 2.0 U pg/L 1 5/8/2014 10.07.00 PM 2,2-Dichloropropane ND 0.5 2.0 U pg/L 1 5/8/2014 10.07.00 PM 2-Butanone ND 125 50 U pg/L 1 5/8/2014 10.07.00 PM 2-Chloroethyl vinyl ether ND 1 40 U pg/L 1 5/8/2014 10.07:00 PM 2-Chlorotoluene ND 05 20 U pg/L 1 5/8/2014 10 07 00 PM 2-Hexanone ND 1.25 5.0 U pg/L 1 5/8/2014 10 0700 PM 2-Propanol ND 0.5 2 0 U pg/L 1 5/8/2014 10.07 00 PM 4-Chlorotoluene ND 0.5 2.0 U pg/L 1 5/8/2014 10 07 00 PM 4-Isopropyltoluene ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM 4-Methyl-2-pentanone ND 1.25 5 0 U pg/L 1 5/8/2014 10.07.00 PM Acetone 2.6 1.25 5 0 BJ' pg/L 1 5/8/2014 10 07:00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical com +e I Page 27 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-005A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst: LA Benzene ND 0 5 2 0 U pg/L 1 5/8/2014 10.07:00 PM Bromobenzene ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Bromochloromethane ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Bromodichloromethane ND 0 5 2 0 U pg/L 1 5/8/2014 10:07 00 PM Bromoform ND 05 2 0 U pg/L 1 5/8/2014 10:07 00 PM Bromomethane ND 1 4 0 U* pg/L 1 5/8/2014 10 07 00 PM Carbon disulfide ND 0.5 2 0 U pg/L 1 5/8/2014 10 07.00 PM Carbon tetrachloride ND 0 5 2 0 U pg/L 1 5/8/2014 10:0700 PM Chlorobenzene ND 0 5 2 0 U pg/L 1 5/8/2014 10.07 00 PM Chlorodifluoromethane ND 0 5 2 0 U* pg/L 1 5/8/2014 10 07 00 PM Chloroethane ND 0.5 2 0 U pg/L 1 5/8/2014 10.07.00 PM Chloroform ND 0 5 2 0 U pg/L 1 5/8/2014 10 0700 PM Chloromethane ND 0 5 2 0 U pg/L 1 5/8/2014 10.07.00 PM cis-1,2-Dichloroethene ND 0.5 2 0 U pg/L 1 5/8/2014 10 07 00 PM cis-1,3-Dichloropropene ND 0 5 2.0 U pg/L 1 5/8/2014 10.07.00 PM Cyclohexane ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Dibromochloromethane ND 0.5 2.0 U pg/L 1 5/8/2014 10.07.00 PM Dibromomethane ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Dichlorodifluoromethane ND 0 5 2 0 U pg/L 1 5/8/2014 1007 00 PM Dusopropyl ether ND 0.5 2 0 U pg/L 1 5/8/2014 1007 00 PM Ethanol ND 2.5 10 U pg/L 1 5/8/2014 1007.00 PM Ethylbenzene ND 0.5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Freon-114 ND 0 5 2.0 U pg/L 1 5/8/2014 10:07:00 PM Hexachlorobutadiene ND 0 5 2.0 U pg/L 1 5/8/2014 10 07:00 PM I sopropyl benzene ND 0 5 2.0 U pg/L 1 5/8/2014 10 07:00 PM m,p-Xylene ND 1 4.0 U pg/L 1 5/8/2014 10 07 00 PM Methyl Acetate ND 0 5 2 0 U pg/L 1 5/8/2014 10 07.00 PM Methyl tert-butyl ether ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM Methylene chloride 2 9 0.5 2 0 B* pg/L 1 5/8/2014 10 0700 PM n-Butylbenzene ND 0 5 2 0 U pg/L 1 5/8/2014 10 07 00 PM n-Propylbenzene ND 0 5 2 0 U pg/L 1 5/8/2014 10:07.00 PM Naphthalene ND 0 5 2 0 U pg/L 1 5/8/2014 10 0700 PM o-Xylene ND 0 5 2.0 U pg/L 1 5/8/2014 10 07 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com Page 28 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-005A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5030C Analyst: LA p-Diethylbenzene ND 05 20 U pg/L 1 5/8/2014 10 07 00 PM p-Ethyltoluene ND 0.5 2.0 U pg/L 1 5/8/2014 10.07.00 PM sec-Butylbenzene ND 0.5 20 U pg/L 1 5/8/2014 10 07:00 PM Styrene ND 0.5 2.0 U pg/L 1 5/8/2014 10:07:00 PM t-Butyl alcohol ND 2.5 10 U pg/L 1 5/8/2014 10:07:00 PM tert-Butylbenzene ND 05 20 U pg/L 1 5/8/2014 10:07 00 PM Tetrachloroethene ND 05 20 U pg/L 1 5/8/2014 1007:00 PM Toluene ND 05 2.0 U pg/L 1 5/8/2014 10:07:00 PM trans-1,2-Dichloroethene ND 05 20 U ug/L 1 5/8/2014 10.07.00 PM trans-1,3-Dichloropropene ND 05 2.0 U Ng/L 1 5/8/201410.07:00 PM Trichloroethene ND 05 20 U Ng/L 1 5/8/2014 10.07 00 PM Trichlorofluoromethane ND 0.5 20 U Ng/L 1 5/8/2014 1007.00 PM Vinyl acetate ND 05 20 U' pg/L 1 5/8/2014 10 07 00 PM Vinyl chloride ND 0.5 2.0 U pg/L 1 5/8/2014 10 07 00 PM Surr:4-Bromofluorobenzene 102 0 70-128 %REC 1 5/8/2014 10 07 00 PM Surr.Di bromofluorom ethane 101 0 75-129 %REC 1 5/8/2014 10 07 00 PM Surr Toluene-d8 102 0 70-124 %REC 1 5/8/2014 10 07 00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical com e Page 29 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-005B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270(BN) SW8270D SW3510C Analyst: MH 1,2,4-Tnchlorobenzene ND 059 59 U pg/L 1 5/9/2014 11 4400 AM 1,2-Dichlorobenzene ND 059 59 U pg/L 1 5/9/2014 11 4400 AM 1,3-Dichlorobenzene ND 059 59 U pg/L 1 5/9/2014 1144.00 AM 1,4-Dichlorobenzene ND 059 59 U pg/L 1 5/9/2014 11 44 00 AM 2,4-Dinitrotoluene ND 059 59 U pg/L 1 5/9/2014 11 44 00 AM 2,6-Dinitrotoluene ND 059 59 U pg/L 1 5/9/2014 11.44.00 AM 2-Chloronaphthalene ND 059 59 U pg/L 1 5/9/2014 11:44 00 AM 2-Methylnaphthalene ND 059 59 U pg/L 1 5/9/2014 1144,00 AM 2-Nitroamlme ND 059 59 U pg/L 1 5/9/2014 1144 00 AM 3,3"-Dichlorobenzidine ND 059 59 U pg/L 1 5/9/2014 11:44:00 AM 3-Nitroamlme ND 059 59 U pg/L 1 5/9/2014 1144 00 AM 4-Bromophenyl phenyl ether ND 059 59 U pg/L 1 5/9/2014 11:44.00 AM 4-Chloroandme ND 059 59 U pg/L 1 5/9/2014 1144:00 AM 4-Chlorophenyl phenyl ether ND 059 59 U pg/L 1 5/9/2014 1144-00 AM 4-Nitroamline ND 059 59 U pg/L 1 5/9/2014 1144 00 AM Acenaphthene ND 059 5.9 U pg/L 1 5/9/2014 11.44 00 AM Acenaphthylene ND 059 59 U pg/L 1 5/9/2014 1144-00 AM Aniline ND 059 59 U pg/L 1 5/9/2014 11 44.00 AM Anthracene ND 059 59 U pg/L 1 5/9/2014 1144-00 AM Azobenzene ND 059 59 U pg/L 1 5/9/2014 1144:00 AM Benzidine ND 1 18 12 U pg/L 1 5/9/2014 11.44.00 AM Benzo(a)anthracene ND 059 5 9 U pg/L 1 5/9/2014 11,44:00 AM Benzo(a)pyrene ND 0.59 5 9 U pg/L 1 5/9/2014 11.44.00 AM Benzo(b)fluoranthene ND 059 5 9 U pg/L 1 5/9/2014 11 44 00 AM Benzo(g,h,i)perylene ND 059 5 9 U pg/L 1 5/9/2014 11 44.00 AM Benzo(k)fluoranthene ND 059 5 9 U pg/L 1 5/9/2014 11.44 00 AM Benzyl alcohol ND 059 5.9 U pg/L 1 5/9/2014 1144-00 AM Bis(2-chloroethoxy)methane ND 0.59 59 U pg/L 1 5/9/2014 11.44 00 AM Bis(2-chloroethyl)ether ND 0 59 59 U pg/L 1 5/9/2014 11 44 00 AM Bis(2-chloroisopropyl)ether ND 059 5 9 U pg/L 1 5/9/2014 1144:00 AM Bis(2-ethylhexyl)phthalate 1.4 0.59 59 J pg/L 1 5/9/2014 11 44 00 AM Butyl benzyl phthalate ND 0.59 59 U pg/L 1 5/9/2014 11.44 00 AM Carbazole ND 0 59 59 U pg/L 1 5/9/2014 11.44 00 AM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.amencan-analytical com Page 30 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: GW-3 Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: LIQUID Lab ID: 1405040-005B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270(BN) SW8270D SW3510C Analyst: MH Chrysene ND 059 59 U pg/L 1 5/9/2014 11:44:00 AM Dibenzo(a,h)anthracene ND 059 59 U pg/L 1 5/9/2014 11.44.00 AM Dibenzofuran ND 0.59 5.9 U pg/L 1 5/9/2014 1144 00 AM Diethyl phthalate ND 0.59 59 U pg/L 1 5/9/2014 1144 00 AM Dimethyl phthalate ND 0.59 59 U pg/L 1 5/9/2014 11:44.00 AM Di-n-butyl phthalate ND 0.59 59 U pg/L 1 5/9/2014 1144:00 AM Di-n-octyl phthalate 073 059 59 J pg/L 1 5/9/2014 11.44:00 AM Fluoranthene ND 0.59 5.9 U pg/L 1 5/9/2014 11.44:00 AM Fluorene ND 059 59 U pg/L 1 5/9/2014 11:44:00 AM Hexachlorobenzene ND 059 59 U pg/L 1 5/9/2014 11:44:00 AM Hexachlorobutadiene ND 059 5.9 U pg/L 1 5/9/2014 11:44:00 AM Hexachlorocyclopentadiene ND 1.18 12 U pg/L 1 5/9/2014 11:44:00 AM Hexachloroethane ND 059 5.9 U pg/L 1 5/9/2014 11:44:00 AM Indeno(1,2,3-c,d)pyrene ND 059 5.9 U pg/L 1 5/9/2014 11:44.00 AM Isophorone ND 059 59 U pg/L 1 5/9/2014 11:44:00 AM Naphthalene ND 059 59 U pg/L 1 5/9/2014 11 44 00 AM Nitrobenzene ND 0.59 59 U pg/L 1 5/9/2014 11:44.00 AM N-Nitrosodimethylamine ND 0.59 59 U pg/L 1 5/9/2014 1144 00 AM N-Nitrosodi-n-propylamine ND 0.59 5.9 U pg/L 1 5/9/2014 1144 00 AM N-Nitrosodiphenylamine ND 059 59 U pg/L 1 5/9/2014 1144-00 AM Phenanthrene ND 059 59 U pg/L 1 5/9/2014 11.44:00 AM Pyrene ND 059 5.9 U pg/L 1 5/9/2014 11.44:00 AM Pyridine ND 059 5.9 U pg/L 1 5/9/2014 11:44:00 AM Sura 2-Fluorobiphenyl 775 0 22-134 %REC 1 5/9/2014 11:44.00 AM Surr 4-Terphenyl-d14 792 0 20-144 %REC 1 5/9/2014 11:4400 AM Surr Nitrobenzene-d5 71.5 0 21-146 %REC 1 5/9/2014 11:44.00 AM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical com e Page 31 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW6035A Analyst: LA 1,1,1,2-Tetrachloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM 1,1,1-Trichloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM 1,1,2,2-Tetrachloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,1,2-Trichloro-1,2,2-tnfluoroethani ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 1,1,2-Trichloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04 00 PM 1,1-Dichloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 404:00 PM 1,1-Dichloroethene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04:00 PM 1,1-Dichloropropene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,2,3-Tnchlorobenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,2,3-Tnchloropropane ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,2,4,5-Tetramethylbenzene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 1,2,4-Trichlorobenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,2,4-Trimethylbenzene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 1,2-Dibromo-3-chloropropane ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04.00 PM 1,2-Dibromoethane ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4:04,00 PM 1,2-Dichlorobenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 1,2-Dichloroethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 1,2-Dichloropropane ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 1,3,5-Trimethylbenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04:00 PM 1,3-Dichlorobenzene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04:00 PM 1,3-dichloropropane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04:00 PM 1,4-Dichlorobenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM 1,4-Dioxane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM 2,2-Dichloropropane ND 1.12 5.6 U pg/Kg-dry 1 5/8/2014 4.04.00 PM 2-Butanone ND 56 11 U pg/Kg-dry 1 5/8/2014 4:04.00 PM 2-Chloroethyl vinyl ether ND 1.12 56 U' pg/Kg-dry 1 5/8/2014 4 04.00 PM 2-Chlorotoluene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04 00 PM 2-Hexanone ND 56 11 U pg/Kg-dry 1 5/8/2014 4:04.00 PM 2-Propanol ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 0400 PM 4-Chlorotoluene ND 1 12 5 6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM 4-Isopropyltoluene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04 00 PM 4-Methyl-2-pentanone ND 5 6 11 U pg/Kg-dry 1 5/8/2014 4 04:00 PM Acetone 3.0 1 4 11 BJ' pg/Kg-dry 1 5/8/2014 4.04 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com ` e • Page 32 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5036A Analyst: LA Benzene ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4:04.00 PM Bromobenzene ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4 04.00 PM Bromochloromethane ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM Bromodichloromethane ND 112 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Bromoform ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Bromomethane ND 1.12 5.6 U* pg/Kg-dry 1 5/8/2014 4:04:00 PM Carbon disulfide ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Carbon tetrachloride ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04.00 PM Chlorobenzene ND 112 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM Chlorodifluoromethane ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM Chloroethane ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM Chloroform ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4:04.00 PM Chloromethane ND 112 56 U* pg/Kg-dry 1 5/8/2014 4:0400 PM cis-1,2-Dichloroethene ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4:04 00 PM cis-1,3-Dichloropropene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM Cyclohexane ND 224 5 6 U pg/Kg-dry 1 5/8/2014 4.04 00 PM Dibromochloromethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 404.00 PM Dibromomethane ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04:00 PM Dichlorodifluoromethane ND 1 12 5.6 U* pg/Kg-dry 1 5/8/2014 4:04:00 PM Dusopropyl ether ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 0400 PM Ethanol ND 11.2 22 U pg/Kg-dry 1 5/8/2014 4 04 00 PM Ethylbenzene ND 1 12 5 6 U pg/Kg-dry 1 5/8/2014 4.04.00 PM Freon-114 ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Hexachlorobutadiene ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4.04.00 PM Isopropylbenzene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04.00 PM m,p-Xylene ND 224 11 U pg/Kg-dry 1 5/8/2014 4 04 00 PM Methyl Acetate ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04 00 PM Methyl tert-butyl ether ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04.00 PM Methylene chloride 7.7 1 12 5.6 B* pg/Kg-dry 1 5/8/2014 4.04.00 PM n-Butylbenzene ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM n-Propylbenzene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04:00 PM Naphthalene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4:04.00 PM o-Xylene ND 1 12 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com e Page 33 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA p-Diethylbenzene ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4 04 00 PM p-Ethyltoluene ND 112 5.6 U pg/Kg-dry 1 5/8/2014 4.04.00 PM sec-Butylbenzene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4.04 00 PM Styrene ND 112 56 U pg/Kg-dry 1 5/8/2014 4:0400 PM t-Butyl alcohol ND 28 56 U' pg/Kg-dry 1 5/8/2014 4 04 00 PM tert-Butylbenzene ND 112 56 U pg/Kg-dry 1 5/8/2014 4 04.00 PM Tetrachloroethene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4 04 00 PM Toluene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04.00 PM trans-1,2-Dichloroethene ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4.04 00 PM trans-1,3-Dichloropropene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4 04.00 PM Trichloroethene ND 1.12 56 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Trichlorofluoromethane ND 1 12 56 U pg/Kg-dry 1 5/8/2014 4 04:00 PM Vinyl acetate ND 112 5.6 U" pg/Kg-dry 1 5/8/2014 404:00 PM Vinyl chloride ND 1.12 5.6 U pg/Kg-dry 1 5/8/2014 4:04:00 PM Surr 4-Bromofluorobenzene 99.5 0 56-133 %REC 1 5/8/2014 4:04.00 PM Surr Dibromofluorom ethane 105 0 60-132 %REC 1 5/8/2014 4.04.00 PM Surr:Toluene-d8 98.3 0 69-125 %REC 1 5/8/2014 4 04 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com Q. P— Page 34 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 11 1 1 0 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Trichlorobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM 1,2,4-Trichlorobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4,10 00 PM 1,2-Dichlorobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/20144.10.00 PM 1,2-Dichlorobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM 1,3-Dichlorobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 1,3-Dichlorobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 1,4-Dichlorobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 1,4-Dichlorobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM 2,4-Dinitrotoluene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM 2,4-Dinitrotoluene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 2,6-Dlmtrotoluene ND 55.6 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 2,6-Dindrotoluene ND 55.6 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 2-Chloronaphthalene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 2-Chloronaphthalene ND 278 280 U pg/Kg-dry 1 5/9/2014 410.00 PM 2-Methylnaphthalene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 2-Methylnaphthalene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 2-Nitroaniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4.1000 PM 2-Nitroaniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10:00 PM 3,3 Dichlorobenzidine ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 3-Nitroaniline ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 3-Nitroaniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 4-Bromophenyl phenyl ether ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 4-Bromophenyl phenyl ether ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 4-Chloroaniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM 4-Chloroamline ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM 4-Chlorophenyl phenyl ether ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM 4-Chlorophenyl phenyl ether ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 4-Nitroaniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM 4-Nitroaniline ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM Acenaphthene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.1000 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com = e Page 35 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006B Certificate of Results Analyses Sample Result LOD LOQ Qua[ Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Acenaphthene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Acenaphthylene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10 00 PM Acenaphthylene ND 278 280 U pg/Kg-dry 1 5/9/2014 4,10*00 PM Aniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4 1000 PM Aniline ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10:00 PM Anthracene ND 278 280 Um pg/Kg-dry 1 5/9/2014 410.00 PM Anthracene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Azobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Azobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10.00 PM Benzidine ND 55 6 560 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Benzo(a)anthracene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Benzo(a)anthracene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Benzo(a)pyrene ND 278 170 U pg/Kg-dry 1 5/9/2014 4 1000 PM Benzo(a)pyrene 41 27.8 170 J pg/Kg-dry 1 5/9/2014 4 10:00 PM Benzo(b)fluoranthene 60 27.8 280 Jm pg/Kg-dry 1 5/9/2014 4:10.00 PM Benzo(b)fluoranthene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Benzo(g,h,i)perylene 100 278 280 J pg/Kg-dry 1 5/9/2014 4.10 00 PM Benzo(g,h,i)perylene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 1000 PM Benzo(k)fluoranthene ND 278 280 U pg/Kg-dry 1 5/9/2014 410.00 PM Benzo(k)fluoranthene 32 278 280 Jm pg/Kg-dry 1 5/9/2014 4 10.00 PM Benzyl alcohol ND 278 280 U pg/Kg-dry 1 5/9/2014 4 1000 PM Benzyl alcohol ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Bis(2-chloroethoxy)methane ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Bls(2-chloroethoxy)methane ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Bis(2-chloroethyl)ether ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM Bis(2-chloroethyl)ether ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Bis(2-chloroisopropyl)ether ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4 1000 PM Bls(2-chlorolsopropyl)ether ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Bis(2-ethylhexyl)phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Bis(2-ethylhexyl)phthalate 320 278 280 * pg/Kg-dry 1 5/9/2014 4.10.00 PM Butyl benzyl phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Butyl benzyl phthalate ND 27.8 280 U* pg/Kg-dry 1 5/9/2014 4 10 00 PM Carbazole ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.amerlcan-analytical com e-- Page 36 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ED : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Carbazole ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Chrysene 44 278 280 J pg/Kg-dry 1 5/9/2014 4.10 00 PM Chrysene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Dibenzo(a,h)anthracene ND 278 170 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Dibenzo(a,h)anthracene ND 278 170 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Dibenzofuran ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Dibenzofuran ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM Diethyl phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM Diethyl phthalate ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10:00 PM Dimethyl phthalate ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Dimethyl phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 410:00 PM Di-n-butyl phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Di-n-butyl phthalate ND 278 280 U pg/Kg-dry 1 5/9/2014 4:1000 PM Di-n-octyl phthalate ND 556 560 U* pg/Kg-dry 1 5/9/2014 4.10.00 PM Di-n-octyl phthalate ND 55.6 560 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Fluoranthene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Fluoranthene 33 278 280 J pg/Kg-dry 1 5/9/2014 4 10.00 PM Fluorene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Fluorene ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM Hexachlorobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4*10*00 PM Hexachlorobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Hexachlorobutadiene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM Hexachlorobutadiene ND 278 280 U pg/Kg-dry 1 5/9/2014 4:10.00 PM Hexachlorocyclopentadiene ND 556 280 U pg/Kg-dry 1 5/9/2014 4 1000 PM Hexachlorocyclopentadiene ND 55.6 280 U' pg/Kg-dry 1 5/9/2014 4.10:00 PM Hexachloroethane ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Hexachloroethane ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10:00 PM Indeno(1,2,3-c,d)pyrene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10:00 PM Indeno(1,2,3-c,d)pyrene 89 27.8 280 J pg/Kg-dry 1 5/9/2014 4.10 00 PM Isophorone ND 278 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM Isophorone ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10.00 PM Naphthalene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10:00 PM Naphthalene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com e Page 37 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Drain Pool Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-006B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Nitrobenzene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Nitrobenzene ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10:00 PM N-Nitrosodimethylamine ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10:00 PM N-Nitrosodimethylamine ND 278 280 U pg/Kg-dry 1 5/9/2014 4.1000 PM N-Nitrosodi-n-propylamme ND 278 170 U pg/Kg-dry 1 5/9/2014 4 10 00 PM N-Nitrosodi-n-propylamine ND 278 170 U pg/Kg-dry 1 5/9/2014 4 1000 PM N-Nitrosodiphenylamme ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10.00 PM N-Nitrosodiphenylamme ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Phenanthrene ND 278 280 Um pg/Kg-dry 1 5/9/2014 4:10.00 PM Phenanthrene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10.00 PM Pyrene ND 278 280 U pg/Kg-dry 1 5/9/2014 4 10 00 PM Pyrene 43 27.8 280 J pg/Kg-dry 1 5/9/2014 4.10 00 PM Pyndine ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4.10 00 PM Pyndine ND 27.8 280 U pg/Kg-dry 1 5/9/2014 4:10 00 PM Surr:2-Fluorobiphenyl 590 0 21-143 %REC 1 5/9/2014 4 10.00 PM Surr 2-Fluorobiphenyl 688 0 21-143 %REC 1 5/9/2014 410:00 PM Surr.4-Terphenyl-d14 594 0 15-137 %REC 1 5/9/2014 4 10.00 PM Surr.4-Terphenyl-d14 614 0 15-137 %REC 1 5/9/2014 4 1000 PM Surr Nitrobenzene-d5 624 0 17-136 %REC 1 5/9/2014 4:10.00 PM Surr:Nitrobenzene-d5 596 0 17-136 %REC 1 5/9/2014 4 10 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com e Page 38 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Susp. Sepctic @ 10-12.5' Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-007A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW6035A Analyst: LA 1,1,1,2-Tetrachloroethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,1,1-Trichloroethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,1,2,2-Tetrachloroethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4 31 00 PM 1,1,2-Trichloro-1,2,2-trifluoroethani ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4 31.00 PM 1,1,2-Trichloroethane ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM 1,1-Dichloroethane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,1-Dichloroethene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,1-Dichloropropene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,2,3-Trichlorobenzene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,2,3-Tnchloropropane ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4:31:00 PM 1,2,4,5-Tetramethylbenzene ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31:00 PM 1,2,4-Trichlorobenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 1,2,4-Tnmethylbenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4 31 00 PM 1,2-Dibromo-3-chloropropane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4-31-00 PM 1,2-Dibromoethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4 31 00 PM 1,2-Dichlorobenzene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4:31:00 PM 1,2-Dichloroethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4.3100 PM 1,2-Dichloropropane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4:31:00 PM 1,3,5-Tnmethylbenzene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4.31.00 PM 1,3-Dichlorobenzene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM 1,3-dichloropropane ND 104 5.2 U pg/Kg-dry 1 5/8/2014 4:31.00 PM 1,4-Dichlorobenzene ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31.00 PM 1,4-Dioxane ND 104 52 U pg/Kg-dry 1 5/8/2014 4-31-00 PM 2,2-Dichloropropane ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4.31.00 PM 2-Butanone ND 5.22 10 U pg/Kg-dry 1 5/8/2014 4.31.00 PM 2-Chloroethyl vinyl ether ND 1.04 5.2 U* pg/Kg-dry 1 5/8/2014 4.31.00 PM 2-Chlorotoluene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 4:31.00 PM 2-Hexanone ND 5.22 10 U pg/Kg-dry 1 5/8/2014 4.31:00 PM 2-Propanol ND 104 52 U pg/Kg-dry 1 5/8/2014 4-31-00 PM 4-Chlorotoluene ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31 00 PM 4-Isopmpyltoluene ND 1.04 5 2 U pg/Kg-dry 1 5/8/2014 4:31.00 PM 4-Methyl-2-pentanone ND 522 10 U pg/Kg-dry 1 5/8/2014 4 31 00 PM Acetone 4.3 1.31 10 BJ* pg/Kg-dry 1 5/8/2014 4 31.00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com = { e Page 39 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Susp. Sepctic @ 10-12.5' Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-007A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA Benzene ND 104 5 2 U pg/Kg-dry 1 5/8/2014 431.00 PM Bromobenzene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM Bromochloromethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4 31*00 PM Bromodichloromethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4:31*00 PM Bromoform ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31 00 PM Bromomethane ND 104 52 U* pg/Kg-dry 1 5/8/2014 4:31:00 PM Carbon disulfide ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4:31:00 PM Carbon tetrachloride ND 1 04 5 2 U pg/Kg-dry 1 5/8/2014 4.31.00 PM Chlorobenzene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4:31 00 PM Chlorodifluoromethane ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4.31 00 PM Chloroethane ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4:31 00 PM Chloroform ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4:31.00 PM Chloromethane ND 1.04 52 U* pg/Kg-dry 1 5/8/2014 4 31*00 PM cis-1,2-Dichloroethene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 4.31:00 PM cis-1,3-Dichloropropene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4 31:00 PM Cyclohexane ND 209 52 U pg/Kg-dry 1 5/8/2014 4:3100 PM Dibromochloromethane ND 104 5 2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM Dibromomethane ND 104 52 U pg/Kg-dry 1 5/8/2014 4 31:00 PM Dichlorodifluoromethane ND 104 52 U* pg/Kg-dry 1 5/8/2014 4:31.00 PM Dnsopropyl ether ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31 00 PM Ethanol ND 104 21 U pg/Kg-dry 1 5/8/2014 4:31 00 PM Ethylbenzene ND 104 52 U pg/Kg-dry 1 5/8/2014 4*31 00 PM Freon-114 ND 1.04 5 2 U pg/Kg-dry 1 5/8/2014 4.31-00 PM Hexachlorobutadiene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4 31.00 PM I sopropyl benzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4 31.00 PM m,p-Xylene ND 209 10 U pg/Kg-dry 1 5/8/2014 4.31 00 PM Methyl Acetate ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4.31 00 PM Methyl tert-butyl ether ND 1 04 5 2 U pg/Kg-dry 1 5/8/2014 4 3100 PM Methylene chloride 6 4 1 04 5.2 B* pg/Kg-dry 1 5/8/2014 4 31 00 PM n-Butylbenzene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4 3100 PM n-Propylbenzene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 431.00 PM Naphthalene ND 1 04 52 U pg/Kg-dry 1 5/8/2014 4 31.00 PM o-Xylene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4.3100 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale, New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com ? iK e Page 40 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Susp. Sepctic @ 10-12.5' Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-007A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA p-Diethylbenzene ND 104 52 U pg/Kg-dry 1 5/8/2014 4 31 00 PM p-Ethyltoluene ND 104 52 U pg/Kg-dry 1 5/8/2014 431:00 PM sec-Butylbenzene ND 104 5.2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM Styrene ND 104 52 U pg/Kg-dry 1 5/8/2014 4.31.00 PM t-Butyl alcohol ND 2.61 5.2 U' pg/Kg-dry 1 5/8/2014 4.31:00 PM tert-Butylbenzene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4:31:00 PM Tetrachloroethene ND 104 52 U pg/Kg-dry 1 5/8/2014 4:31*00 PM Toluene ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 4 31 00 PM trans-1,2-Dichloroethene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 4 31 00 PM trans-1,3-Dichloropropene ND 1.04 52 U pg/Kg-dry 1 5/8/2014 431:00 PM Trichloroethene ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4.31 00 PM Trichlorofluoromethane ND 1 04 5.2 U pg/Kg-dry 1 5/8/2014 4.31.00 PM Vinyl acetate ND 104 5.2 U' pg/Kg-dry 1 5/8/2014 4:31:00 PM Vinyl chloride ND 1.04 5.2 U pg/Kg-dry 1 5/8/2014 431:00 PM Surr.4-Bromofluorobenzene 100 0 56-133 %REC 1 5/8/2014 4:31:00 PM Surr Dibromofluorom ethane 103 0 60-132 %REC 1 5/8/2014 4:31 00 PM Surr Toluene-d8 100 0 69-125 %REC 1 5/8/2014 4 31.00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com = Page 41 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ED : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: Susp. Sepctic @ 10-12.5' Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-007B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 39 1 1 0 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Tnchlorobenzene ND 256 260 U pg/Kg-dry 1 5/9/2014 346.00 PM 1,2-Dichlorobenzene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3 46.00 PM 1,3-Dichlorobenzene ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46 00 PM 1,4-Dichlorobenzene ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46:00 PM 2,4-Dinitrotoluene ND 256 260 U pg/Kg-dry 1 5/9/2014 3.46:00 PM 2,6-Dimtrotoluene ND 512 260 U pg/Kg-dry 1 5/9/2014 346.00 PM 2-Chloronaphthalene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:4600 PM 2-Methylnaphthalene ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46.00 PM 2-Nitroaniline ND 256 260 U pg/Kg-dry 1 5/9/2014 3,46.00 PM 3,3'-Dichlorobenzidine ND 256 260 U pg/Kg-dry 1 5/9/2014 3 4600 PM 3-Nitroaniline ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM 4-Bromophenyl phenyl ether ND 256 260 U pg/Kg-dry 1 5/9/2014 3.46 00 PM 4-Chloroamlme ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46.00 PM 4-Chlorophenyl phenyl ether ND 256 260 U pg/Kg-dry 1 5/9/2014 3.46.00 PM 4-Nitroamline ND 25.6 260 U pg/Kg-dry 1 5/9/2014 346.00 PM Acenaphthene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3.46:00 PM Acenaphthylene ND 256 260 U pg/Kg-dry 1 5/9/2014 3 4600 PM Aniline ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46:00 PM Anthracene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 346.00 PM Azobenzene ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46 00 PM Benzidine ND 51 2 510 U pg/Kg-dry 1 5/9/2014 3:46 00 PM Benzo(a)anthracene ND 256 260 U pg/Kg-dry 1 5/9/2014 3.46.00 PM Benzo(a)pyrene ND 25 6 150 U pg/Kg-dry 1 5/9/2014 3,46.00 PM Benzo(b)fluoranthene ND 25.6 260 Um pg/Kg-dry 1 5/9/2014 3:46 00 PM Benzo(g,h,i)perylene ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46:00 PM Benzo(k)fluoranthene ND 256 260 Um pg/Kg-dry 1 5/9/2014 3 46 00 PM Benzyl alcohol ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Bis(2-chloroethoxy)methane ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3 46:00 PM Bis(2-chloroethyl)ether ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Bis(2-chloroisopropyl)ether ND 256 260 U pg/Kg-dry 1 5/9/2014 3.46 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical com Nt ; Page 42 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Benninger Environmental,Inc. Client Sample ID: Susp. Sepctic @ 10-12.5' Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-007B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Bis(2-ethylhexyl)phthalate ND 256 260 U* pg/Kg-dry 1 5/9/2014 3.46.00 PM Butyl benzyl phthalate ND 256 260 U* pg/Kg-dry 1 5/9/2014 3.46.00 PM Carbazole ND 256 260 U pg/Kg-dry 1 5/9/2014 346:00 PM Chrysene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:4600 PM Dibenzo(a,h)anthracene ND 25.6 150 U pg/Kg-dry 1 5/9/2014 3.46.00 PM Dibenzofuran ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Diethyl phthalate ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:46:00 PM Dimethyl phthalate ND 256 260 U pg/Kg-dry 1 5/9/2014 3:4600 PM Di-n-butyl phthalate ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:46:00 PM Di-n-octyl phthalate ND 51.2 510 U* pg/Kg-dry 1 5/9/2014 3 46 00 PM Fluoranthene 37 256 260 J pg/Kg-dry 1 5/9/2014 3 46 00 PM Fluorene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3.46 00 PM Hexachlorobenzene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:46:00 PM Hexachlorobutadiene ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3:4600 PM Hexachlorocyclopentadiene ND 512 260 U* pg/Kg-dry 1 5/9/2014 3 46.00 PM Hexachloroethane ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Indeno(1,2,3-c,d)pyrene ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Isophorone ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46 00 PM Naphthalene ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46:00 PM Nitrobenzene ND 256 260 U pg/Kg-dry 1 5/9/2014 3:46:00 PM N-Nitrosodimethylamine ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM N-Nitrosodi-n-propylamine ND 256 150 U pg/Kg-dry 1 5/9/2014 3 46.00 PM N-Nitrosodiphenylamme ND 25.6 260 U pg/Kg-dry 1 5/9/2014 3.46:00 PM Phenanthrene 34 256 260 J pg/Kg-dry 1 5/9/2014 3:46:00 PM Pyrene 32 256 260 J pg/Kg-dry 1 5/9/2014 3:4600 PM Pyndine ND 256 260 U pg/Kg-dry 1 5/9/2014 3 46 00 PM Surr.2-Fluorobiphenyl 775 0 21-143 %REC 1 5/9/2014 3:46.00 PM Surr 4-Terphenyl-d14 828 0 15-137 %REC 1 5/9/2014 3.4600 PM Surr:Nitrobenzene-d5 796 0 17-136 %REC 1 5/9/2014 3:46:00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com r` Page 43 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: SD-Rear Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-008A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA 1,1,1,2-Tetrachloroethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59.00 PM 1,1,1-Trichloroethane ND 11 5.5 U pg/Kg-dry 1 5/8/2014 4:59-00 PM 1,1,2,2-Tetrachloroethane ND 11 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 1,1,2-Trichloro-1,2,2-trifluoroethan ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM 1,1,2-Trichloroethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 459.00 PM 1,1-Dichloroethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM 1,1-Dichloroethene ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 1,1-Dichloropropene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM 1,2,3-Trichlorobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM 1,2,3-Trichloropropane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM 1,2,4,5-Tetramethylbenzene ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4:59 00 PM 1,2,4-Trichlorobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 5900 PM 1,2,4-Tnmethylbenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 1,2-Dibromo-3-chloropropane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 1,2-Dibromoethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM 1,2-Dichlorobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM 1,2-Dichloroethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59.00 PM 1,2-Dichloropropane ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4:59.00 PM 1,3,5-Tnmethyl benzene ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM 1,3-Dichlorobenzene ND 1.1 5.5 U pg/Kg-dry 1 5/8/2014 4:59 00 PM 1,3-dichloropropane ND 1 1 65 U pg/Kg-dry 1 5/8/2014 4 59 00 PM 1,4-Dichlorobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 1,4-Dioxane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 2,2-Dichloropropane ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4.59.00 PM 2-Butanone ND 55 11 U pg/Kg-dry 1 5/8/2014 4 59 00 PM 2-Chloroethyl vinyl ether ND 1 1 55 U' pg/Kg-dry 1 5/8/2014 4:59.00 PM 2-Chlorotoluene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM 2-Hexanone ND 55 11 U pg/Kg-dry 1 5/8/2014 4 5900 PM 2-Propanol ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM 4-Chlorotoluene ND 1 1 5 5 U pg/Kg-dry 1 5/8/2014 4.59 00 PM 4-Isopropyltoluene ND 1 1 5 5 U pg/Kg-dry 1 5/8/2014 4 59:00 PM 4-Methyl-2-pentanone ND 55 11 U pg/Kg-dry 1 5/8/2014 4.59.00 PM Acetone 2 4 1 37 11 BJ" pg/Kg-dry 1 5/8/2014 4 59 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www.american-analytical.com a Page 44 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: SD-Rear Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-008A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW5035A Analyst: LA Benzene ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4,59 00 PM Bromobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM Bromochloromethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM Bromodichloromethane ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4 59:00 PM Bromoform ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59:00 PM Bromomethane ND 1 1 55 U* pg/Kg-dry 1 5/8/2014 4:59.00 PM Carbon disulfide ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59.00 PM Carbon tetrachloride ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59:00 PM Chlorobenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:5900 PM Chlorodifluoromethane ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4.59 00 PM Chloroethane ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Chloroform ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Chloromethane ND 1.1 55 U* pg/Kg-dry 1 5/8/2014 4 59 00 PM cis-1,2-Dichloroethene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM cis-1,3-Dichloropropene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Cyclohexane ND 22 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Dibromochloromethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 459:00 PM Dibromomethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM Dichlorodifluoromethane ND 1 1 55 U* pg/Kg-dry 1 5/8/2014 4.5900 PM Dusopropyl ether ND 1.1 55 U pg/Kg-dry 1 5/8/2014 459:00 PM Ethanol ND 11 22 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Ethylbenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4,59,00 PM Freon-114 ND 1 t 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM Hexachlorobutadiene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59.00 PM Isopropyl benzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM m,p-Xylene ND 2.2 11 U pg/Kg-dry 1 5/8/2014 4 59.00 PM Methyl Acetate ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4 59:00 PM Methyl tert-butyl ether ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4.59:00 PM Methylene chloride 73 1.1 5.5 B* pg/Kg-dry 1 5/8/2014 4.59.00 PM n-Butylbenzene ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4:59 00 PM n-Propylbenzene ND 1 1 5 5 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Naphthalene ND 1 1 5 5 U pg/Kg-dry 1 5/8/2014 4 59:00 PM o-Xylene ND 1.1 5.5 U pg/Kg-dry 1 5/8/2014 4.5900 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www american-analytical.com = ' Page 45 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: SD-Rear Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-008A Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed VOLATILE SW-846 METHOD 8260 SW8260C SW6035A Analyst: LA p-Diethylbenzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM p-Ethyltoluene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59.00 PM sec-Butyl benzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 5900 PM Styrene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.5900 PM t-Butyl alcohol ND 275 55 U* pg/Kg-dry 1 5/8/2014 4*59 00 PM tert-Butyl benzene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 59:00 PM Tetrachloroethene ND 1.1 55 U pg/Kg-dry 1 5/8/2014 4 59 00 PM Toluene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4.59 00 PM trans-1,2-Dichloroethene ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4.59 00 PM trans-1,3-Dichloropropene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59:00 PM Trichloroethene ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4:59.00 PM Trichlorofluoromethane ND 1 1 55 U pg/Kg-dry 1 5/8/2014 4 5900 PM Vinyl acetate ND 1 1 55 U* pg/Kg-dry 1 5/8/2014 4:59.00 PM Vinyl chloride ND 1 1 5.5 U pg/Kg-dry 1 5/8/2014 4:59 00 PM Surr 4-Bromofluorobenzene 981 0 56-133 %REC 1 5/8/2014 4.59:00 PM Surr.Dibromofluoromethane 105 0 60-132 %REC 1 5/8/2014 4.59 00 PM Surr:Toluene-d8 990 0 69-125 %REC 1 5/8/2014 4 59:00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale,New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com '" e Page 46 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Berninger Environmental,Inc. Client Sample ID: SD-Rear Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-008B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed PERCENT MOISTURE D2216 Analyst: CF Percent Moisture 11 1 1 0 wt% 1 5/8/2014 SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH 1,2,4-Tnchlorobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35:00 PM 1,2-Dichlorobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35:00 PM 1,3-Dichlorobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:3500 PM 1,4-Dichlorobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/20144:35:00 PM 2,4-Dmitrotoluene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35:00 PM 2,6-Dinitrotoluene ND 1098 5500 DU pg/Kg-dry 10 5/9/2014 4.35:00 PM 2-Chloronaphthalene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.3500 PM 2-Methylnaphthalene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.3500 PM 2-Nitroamline ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35.00 PM 3,3'-Dichlorobenzidine ND 549 5500 DU pg/Kg-dry 10 5/9/2014 435.00 PM 3-Nitroandme ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35.00 PM 4-Bromophenyl phenyl ether ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35:00 PM 4-Chloroamline ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM 4-Chlorophenyl phenyl ether ND 549 5500 DU pg/Kg-dry 10 5/9/2014 435.00 PM 4-Nitroamlme ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM Acenaphthene 1100 549 5500 DJ pg/Kg-dry 10 5/9/2014 4 35.00 PM Acenaphthylene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35 00 PM Aniline ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35.00 PM Anthracene 1600 549 5500 DJm pg/Kg-dry 10 5/9/2014 435.00 PM Azobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM Benzidine ND 1098 11000 DU pg/Kg-dry 10 5/9/2014 4.35:00 PM Benzo(a)anthracene 10000 549 5500 Dm pg/Kg-dry 10 5/9/2014 4:3500 PM Benzo(a)pyrene 10000 549 3300 D pg/Kg-dry 10 5/9/2014 4.35:00 PM Benzo(b)fluoranthene 13000 549 5500 D pg/Kg-dry 10 5/9/2014 4:35:00 PM Benzo(g,h,i)perylene 7000 549 5500 D pg/Kg-dry 10 5/9/2014 435:00 PM Benzo(k)fluoranthene 11000 549 5500 Dm pg/Kg-dry 10 5/9/2014 4.35:00 PM Benzyl alcohol ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4:35.00 PM Bis(2-chloroethoxy)methane ND 549 5500 DU pg/Kg-dry 10 5/9/2014 435:00 PM Bis(2-chloroethyl)ether ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35 00 PM Bis(2-chloroisopropyl)ether ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35.00 PM American Analytical Laboratories,LLC.,56 Toledo Street,Farmingdale,New York,Zip-11735 r Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com e Page 47 of 105 American Analytical Laboratories, LLC. Date: 12-May-14 ELAP ID : 11418 CLIENT: Benninger Environmental,Inc. Client Sample ID: SD-Rear Lab Order: 1405040 Collection Date: 5/6/2014 Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou Matrix: SOIL Lab ID: 1405040-008B Certificate of Results Analyses Sample Result LOD LOQ Qual Units DF Date/Time Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3546 Analyst: MH Bis(2-ethylhexyl)phthalate 1200 549 5500 DJ* pg/Kg-dry 10 5/9/2014 4.35.00 PM Butyl benzyl phthalate ND 549 5500 DU* pg/Kg-dry 10 5/9/2014 4.3500 PM Carbazole 2800 549 5500 DJ pg/Kg-dry 10 5/9/2014 4.35.00 PM Chrysene 15000 549 5500 D pg/Kg-dry 10 5/9/2014 4 35 00 PM Dibenzo(a,h)anthracene 1700 549 3300 DJ pg/Kg-dry 10 5/9/2014 4.35 00 PM Dibenzofuran 630 549 5500 DJ pg/Kg-dry 10 5/9/2014 4.35.00 PM Diethyl phthalate ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35:00 PM Dimethyl phthalate ND 549 5500 DU pg/Kg-dry 10 5/9/2014 435.00 PM Di-n-butyl phthalate ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM Di-n-octyl phthalate ND 1098 11000 DU* pg/Kg-dry 10 5/9/2014 4.35:00 PM Fluoranthene 28000 549 5500 D pg/Kg-dry 10 5/9/2014 4.35:00 PM Fluorene 1200 549 5500 DJ pg/Kg-dry 10 5/9/2014 435:00 PM Hexachlorobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.3500 PM Hexachlorobutadiene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35:00 PM Hexachlorocyclopentadiene ND 1098 5500 DU* pg/Kg-dry 10 5/9/2014 4 35.00 PM Hexachloroethane ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35.00 PM Indeno(1,2,3-c,d)pyrene 8700 549 5500 D pg/Kg-dry 10 5/9/2014 4 3500 PM Isophorone ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 3500 PM Naphthalene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35.00 PM Nitrobenzene ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4.35 00 PM N-Nitrosodimethylamme ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM N-Nitrosodi-n-propylamme ND 549 3300 DU pg/Kg-dry 10 5/9/2014 4 35.00 PM N-Nitrosodiphenylamine ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35 00 PM Phenanthrene 20000 549 5500 D pg/Kg-dry 10 5/9/2014 4 3500 PM Pyrene 25000 549 5500 D pg/Kg-dry 10 5/9/2014 4.35:00 PM Pyridine ND 549 5500 DU pg/Kg-dry 10 5/9/2014 4 35.00 PM Surr.2-Fluorobiphenyl 675 0 21-143 D %REC 10 5/9/2014 4.35.00 PM Surr:4-Terphenyl-d14 831 0 15-137 D %REC 10 5/9/2014 4 3500 PM Surr:Nitrobenzene-d5 837 0 17-136 D %REC 10 5/9/2014 4 35 00 PM American Analytical Laboratories,LLC,56 Toledo Street,Farmingdale, New York,Zip-11735 Tel-(631)454-6100 Fax-(631)454-8027 www amencan-analytical com Aww Page 48 of 105 -�MERIC-N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTI CAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website•www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID LCS-1123 SampType: LCS TestCode: 8260_S Units: pg/Kg Prep Date, 5/8/2014 RunNo: 1813 Client ID. LCSS Batch ID 1123 TestNo SW8260C SW5035A Analysis Date. 5/8/2014 SegNo: 31604 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ 1,1,1-Trichloroethane 43 5.0 5000 0 863 40 125 1,1,2,2-Tetrachloroethane 41 5.0 50.00 0 823 35 139 1,1,2-Trichloroethane 42 5.0 5000 0 837 40 124 1,1-Dich[oroethane 44 5.0 50.00 0 87.1 33 134 1,1-Dich[oroethene 43 5.0 50.00 0 86.2 30 141 1,2-Dichlorobenzene 38 5.0 50.00 0 75.2 33 126 1,2-Dichloroethane 40 5.0 50.00 0 80.5 36 131 1,2-Dichloropropane 43 50 5000 0 85.1 38 131 1,3-Dichlorobenzene 39 50 5000 0 785 31 130 1,4-Dichlorobenzene 38 5.0 5000 0 75.9 33 121 2-Ch[oroethyl vinyl ether 20 5.0 5000 0 40.1 36 138 Benzene 44 5.0 50.00 0 88.3 36 126 Bromodichloromethane 42 5.0 50.00 0 830 38 125 Bromoform 41 5.0 50.00 0 82.2 36 131 Bromomethane 19 5.0 50.00 0 37.2 23 135 Carbon tetrachloride 44 5.0 50.00 0 877 37 130 Chlorobenzene 39 5 0 50.00 0 78.3 41 123 Chloroethane 67 50 50.00 0 134 20 128 S Chloroform 42 50 50.00 0 84.6 39 125 Chloromethane 47 5.0 50.00 0 94.7 33 143 cis-1,3-Dichloropropene 42 5.0 50.00 0 84.9 34 125 Dibromochloromethane 43 5.0 5000 0 86.4 36 125 Ethylbenzene 44 5.0 50.00 0 875 42 124 Methylene chloride 19 5.0 5000 0 37.0 33 135 B* Tetrachloroethene 36 5.0 50.00 0 72.1 30 121 Toluene 45 5.0 50.00 0 89.1 43 121 Qualifiers: R RPD outside accepted recovery lututs S Spike Recovery outside accepted recovery bruits Original Page 49 of 105 AMERICAN American Analytical Laboratories,LLC. QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 WWebsite www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID LCS-1123 SampType. LCS TestCode 8260_S Units: pg/Kg Prep Date. 5/8/2014 RunNo. 1813 Client ID- LCSS Batch ID. 1123 TestNo SW8260C SW5035A Analysis Date. 5/8/2014 SegNo. 31604 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit HighL]mit RPD Ref Val %RPD RPDLimit Qua] trans-1,2-Dichloroethene 42 5.0 50.00 0 837 32 124 trans-1,3-Dichloropropene 43 5.0 50.00 0 861 33 120 Trichloroethene 41 5.0 50.00 0 81.7 40 124 Trichlorofluoromethane 60 50 5000 0 120 35 140 Vinyl chloride 56 50 50.00 0 111 40 146 Surr 4-Bromofluorobenzene 51 5000 102 56 133 Surr Dlbromofluoromethane 55 5000 109 60 132 Surr Toluene-d8 51 5000 102 69 125 Sample ID MB-1123 SampType MBLK TestCode. 8260_S Units. Ng/Kg Prep Date: 5/8/2014 RunNo 1813 Client ID PBS Batch ID. 1123 TestNo: SW8260C SW5035A Analysis Date 5/8/2014 SegNo 31608 Analyte Result PQL SPK value SPK Ref Val %REC LowLimlt HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1,1,2-Tetrachloroethane ND 5.0 U 1,1,1-Trichloroethane ND 5.0 U 1,1,2,2-Tetrachloroethane ND 5.0 U 1,1,2-Trlchloro-1,2,2-trifluoroethane ND 50 U 1,1,2-Trichloroethane ND 50 U 1,1-Dichloroethane ND 50 U 1,1-Dichloroethene ND 50 U 1,1-Dichloropropene ND 50 U 1,2,3-Trichlorobenzene ND 50 U 1,2,3-Trlchloropropane ND 50 U 1,2,4,5-Tetramethylbenzene ND 50 U 1,2,4-Trichlorobenzene ND 5.0 U Quatiflers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limas Original Page 50 of 105 � ERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT Street Al^M'ALYTICAL Farmingdale,New Yoe k 11735 LABORATORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website.www.Amerrcan-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType: MBLK TestCode: 8260_S Units: Ng/Kg Prep Date, 5/8/2014 RunNo• 1813 Client ID- PBS Batch ID, 1123 TestNo: SW8260C SW5035A Analysis Date 5/8/2014 SegNo 31608 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit Hlghi-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trimethylbenzene ND 5.0 U 1,2-Dlbromo-3-chloropropane ND 5.0 U 1,2-Dibromoethane ND 5.0 U 1,2-Dichlorobenzene ND 5.0 U 1,2-Dichloroethane ND 5.0 U 1,2-Dlchloropropane ND 5.0 U 1,3,5-Trimethylbenzene ND 5.0 U 1,3-Dichlorobenzene ND 5.0 U 1,3-dichloropropane ND 5.0 U 1,4-Dichlorobenzene ND 5.0 U 1,4-Dioxane ND 5.0 U 2,2-Dichloropropane ND 5.0 U 2-Butanone ND 10 U 2-Chloroethyl vinyl ether ND 5.0 U. 2-Chlorotoluene ND 5.0 U 2-Hexanone ND 10 U 2-Propanol ND 5.0 U 4-Chlorotoluene ND 5.0 U 4-Isopropyltoluene ND 5.0 U 4-Methyl-2-pentanone ND 10 U Acetone 4 7 10 ,1* Benzene ND 50 U Bromobenzene ND 5.0 U Bromochloromethane ND 5.0 U Bromodichloromethane ND 5.0 U Bromoform ND 5.0 U Qualifiers: R RPD outside accepted recovery hunts S Spike Recovery outside accepted recovery limits Original Page 51 of 105 _ AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street AILEANALWICAL Farmingdale,New York 11735 L®BORATORIES TEL•(631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www.Amertcan-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType. MBLK TestCode 8260_S Units- pg/Kg Prep Date: 5/8/2014 RunNo. 1813 Client ID- PBS Batch ID, 1123 TestNo SW8260C SW5035A Analysis Date: 5/8/2014 SegNo. 31608 Analyte Result PQL SPK value SPK Ref Val %REC LowLimlt HlghLlmlt RPD Ref Val %RPD RPDLImit Qual Bromomethane ND 50 U. Carbon disulfide ND 50 U Carbon tetrachloride ND 5.0 U Chlorobenzene ND 50 U Chlorodifluoromethane ND 50 U Chloroethane ND 50 U Chloroform ND 5.0 U Chloromethane ND 5.0 U. cls-1,2-Dlchloroethene ND 5.0 U cls-1,3-Dichloropropene ND 5.0 U Cyclohexane ND 5.0 U Dlbromochloromethane ND 5.0 U Dlbromomethane ND 50 U Dichlorodifluoromethane ND 5.0 U. Dusopropyl ether ND 50 U Ethanol ND 20 U Ethylbenzene ND 50 U Freon-114 ND 50 U Hexachlorobutadlene ND 50 U Isopropylbenzene ND 50 U m,p-Xylene ND 10 U Methyl Acetate ND 5.0 U Methyl tert-butyl ether ND 5.0 U Methylene chloride 6.5 5.0 n-Butylbenzene ND 5.0 U n-Propylbenzene ND 5.0 U Qualifiers: R RPD outside accepted recovery/amts S Spike Recovery outside accepted recovery hunts Original Page 52 of 105 EEW�AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABOR®TORIES TEL (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Webs to www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType: MBLK TestCode• 8260_S Units: pg/Kg Prep Date: 5/8/2014 RunNo. 1813 Client ID: PBS Batch ID: 1123 TestNo SW8260C SW5035A Analysis Date- 5/8/2014 SegNo 31608 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua] Naphthalene ND 5.0 U o-Xylene ND 5.0 U p-Diethylbenzene ND 5.0 U p-Ethyltoluene ND 5.0 U sec-Butylbenzene ND 5.0 U Styrene ND 5.0 U t-Butyl alcohol ND 50 U. tert-Butylbenzene ND 5.0 U Tetrachloroethene ND 5.0 U Toluene ND 50 U trans-1,2-Dichloroethene ND 50 U trans-1,3-Dichloropropene ND 50 U Trichloroethene ND 50 U Trichlorofluoromethane ND 50 U Vinyl acetate ND 50 U Vinyl chloride ND 50 U Surr 4-Bromofluorobenzene 50 5000 99.1 56 133 Surr Dibromofluoromethane 51 5000 103 60 132 Surr Toluene-d8 50 5000 100 69 125 Qualifiers: R RPD outside accepted recovery lints S Spike Recovery outside accepted recovery hmas Original Page 53 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 o Street ANALYTICAL- Farmingdale,New York 11735 LABORATORIES TEL•(631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchlD: 1123 Sample ID LCS-1123 SampType LCS TestCode• 8260_S Units: pg/Kg Prep Date: 5/8/2014 RunNo. 1796 Client ID: LCSS Batch ID 1123 TestNo• SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31286 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 43 50 5000 0 863 40 125 1,1,2,2-Tetrachloroethane 41 50 5000 0 823 35 139 1,1,2-Trichloroethane 42 50 5000 0 83.7 40 124 1,1-Dichloroethane 44 50 5000 0 87.1 33 134 1,1-Dichloroethene 43 50 5000 0 86.2 30 141 1,2-Dichlorobenzene 38 5.0 50.00 0 75.2 33 126 1,2-Dichloroethane 40 5.0 5000 0 80.5 36 131 1,2-Dichloropropane 43 5.0 50.00 0 85.1 38 131 1,3-Dichlorobenzene 39 50 50.00 0 78.5 31 130 1,4-Dichlorobenzene 38 5.0 50.00 0 75.9 33 121 2-Chloroethyl vinyl ether 20 50 50.00 0 40.1 36 138 Benzene 44 5 0 50.00 0 88.3 36 126 Bromodichlorom ethane 42 5 0 50.00 0 830 38 125 Bromoform 41 5 0 50.00 0 822 36 131 Bromomethane 19 5.0 50 00 0 37.2 23 135 Carbon tetrachloride 44 5 0 5000 0 87.7 37 130 Chlorobenzene 39 5 0 5000 0 78.3 41 123 Chloroethane 67 5 0 5000 0 134 20 128 S Chloroform 42 5.0 5000 0 846 39 125 Chloromethane 47 5.0 50.00 0 947 33 143 cis-1,3-Dichloropropene 42 5.0 50.00 0 84.9 34 125 Dibromochloromethane 43 5.0 50.00 0 86.4 36 125 Ethylbenzene 44 50 50.00 0 87.5 42 124 Methylene chloride 19 5 0 50.00 0 370 33 135 B* Tetrachloroethene 36 5 0 50 00 0 721 30 121 Toluene 45 5.0 50 00 0 89.1 43 121 Qualiflers: R RPD outside accepted recovery tunics S Spike Recovery outside accepted recovery limits Original Page 54 of 105 �MERAmerican Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street ANAL`I�C--N i 1 ICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchED: 1123 Sample ID LCS4123 SampType: LCS TestCode: 8260_S Units. pg/Kg Prep Date. 5/8/2014 RunNo• 1796 Client ID LCSS Batch ID: 1123 TestNo: SW8260C SW5035A Analysis Date* 5/8/2014 SegNo. 31286 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ trans-1,2-Dich[oroethene 42 50 50.00 0 83.7 32 124 trans-1,3-Dich[oropropene 43 50 50.00 0 86.1 33 120 Trichloroethene 41 5.0 50.00 0 81.7 40 124 Trichlorofluoromethane 60 5.0 50.00 0 120 35 140 Vinyl chloride 56 5.0 5000 0 111 40 146 Surr 4-Bromofluorobenzene 51 5000 102 56 133 Surr Dibromofluoromethane 55 5000 109 60 132 Surr Toluene-d8 51 50.00 102 69 125 Sample ID MB-1123 SampType: MBLK TestCode: 8260_S Units pg/Kg Prep Date, 5/8/2014 RunNo: 1796 Client ID, PBS Batch ID* 1123 TestNo: SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31287 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ 1,1,1,2-Tetrachloroethane ND 5.0 U 1,1,1-Trichloroethane ND 50 U 1,1,2,2-Tetrachloroethane ND 50 U 1,1,2-Trichloro-1,2,2-trifluoroethane ND 50 U 1,1,2-Trichloroethane ND 5.0 U 1,1-Dichloroethane ND 5.0 U 1,1-Dichloroethene ND 5.0 U 1,1-Dichloropropene ND 50 U 1,2,3-Trichlorobenzene ND 5.0 U 1,2,3-Trichloropropane ND 5.0 U 1,2,4,5-Tetramethylbenzene ND 5.0 U 1,2,4-Trichlorobenzene ND 5.0 U Qualifiers: R RPD outside accepted recovery hnuts S Spike Recovery outside accepted recovery lunns Original Page 55 of 105 AI V IERICAN American Analytical Laboratories,LLC o Street QC SUMMARY REPORT A NALYTI CAL Farmingdale,New Yo56 rk 11735 L�BOR�TORIES TEL (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType• MBLK TestCode. 8260_S Units Ng/Kg Prep Date, 5/8/2014 RunNo: 1796 Client ID PBS Batch ID, 1123 TestNo SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31287 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghLlmlt RPD Ref Val %RPD RPDLImit Qual 1,2,4-Trnmethyl benzene ND 50 U 1,2-Dibromo-3-chloropropane ND 50 U 1,2-Dibromoethane ND 50 U 1,2-Dichlorobenzene ND 50 U 1,2-Dlchloroethane ND 50 U 1,2-Dlchloropropane ND 5.0 U 1,3,5-Tnmethyl benzene ND 5.0 U 1,3-Dichlorobenzene ND 5.0 U 1,3-dichloropropane ND 5.0 U 1,4-Dichlorobenzene ND 5.0 U 1,4-Dioxane ND 5.0 U 2,2-Dlchloropropane ND 5.0 U 2-Butanone ND 10 U 2-Chloroethyl vinyl ether ND 50 U. 2-Chlorotoluene ND 50 U 2-Hexanone ND 10 U 2-Propanol ND 5 0 U 4-Chlorotoluene ND 5 0 U 4-Isopropyltoluene ND 5 0 U 4-Methyl-2-pentanone ND 10 U Acetone 4.7 10 J. Benzene ND 5.0 U Bromobenzene ND 5.0 U Bromochloromethane ND 5.0 U Bromodlchloromethane ND 5.0 U Bromoform ND 5.0 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 56 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT ANALYTICAL Farmingdale,New YorkStreet56 Toledo 11735 L�BOR�TORIES WO#: 1405040 TEL. (631)454-6100 FAX (631)454-8027 Website www American-Analytical com 12-May-14 Client: Benninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType: MBLK TestCode. 8260_S Units: pg/Kg Prep Date: 5/8/2014 RunNo* 1796 Client ID: PBS Batch ID 1123 TestNo: SW8260C SW5035A Analysis Date: 5/8/2014 SegNo. 31287 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLtmit RPD Ref Val %RPD RPDLimit Qual Bromomethane ND 5.0 U. Carbon disulfide ND 50 U Carbon tetrachloride ND 5.0 U Chlorobenzene ND 5.0 U Chlorodifluoromethane ND 5.0 U Chloroethane ND 5.0 U Chloroform ND 5.0 U Chloromethane ND 5.0 U. cis-1,2-Dtchloroethene ND 5.0 U cis-1,3-Dichloropropene ND 5.0 U Cyclohexane ND 50 U Dibromochloromethane ND 50 U Dibromomethane ND 50 U Dichlorodifluoromethane ND 50 U. Dusopropyl ether ND 5.0 U Ethanol ND 20 U Ethylbenzene ND 5.0 U Freon-114 ND 50 U Hexachlorobutadiene ND 50 U Isopropylbenzene ND 50 U m,p-Xylene ND 10 U Methyl Acetate ND 50 U Methyl tert-butyl ether ND 5.0 U Methylene chloride 6.5 5.0 " n-Butylbenzene ND 5.0 U n-Propylbenzene ND 50 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 57 of 105 SAM' ER`I/C��I V American Analytical Laboratories,LLC. QC SUMMARY REPORT 56 Toleo Street AN. AMA 1 ICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID MB-1123 SampType. MBLK TestCode: 8260_S Units. Ng/Kg Prep Date 5/8/2014 RunNo• 1796 Client ID PBS Batch ID 1123 TestNo SW8260C SW5035A Analysis Date, 518/2014 SegNo• 31287 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ Naphthalene ND 50 U o-Xylene ND 50 U p-Diethylbenzene ND 50 U p-Ethyltoluene ND 50 U sec-Butylbenzene ND 50 U Styrene ND 50 U t-Butyl alcohol ND 50 U. tert-B utyl benzene ND 5.0 U Tetrachloroethene ND 5.0 U Toluene ND 5.0 U trans-1,2-Dich[oroethene ND 5.0 U trans-1,3-Dich[oropropene ND 5.0 U Trichloroethene ND 50 U Trichlorofluoromethane ND 50 U Vinyl acetate ND 50 U. Vinyl chloride ND 50 U Surr 4-Bromofluorobenzene 50 5000 991 56 133 Surr-Dibromofluoromethane 51 5000 103 60 132 Surr Toluene-d8 50 5000 100 69 125 Sample ID 1405040-008AMS SampType MS TestCode 8260_S Units, pg/Kg-dry Prep Date. 5/8/2014 RunNo 1796 Client ID SD-Rear Batch ID. 1123 TestNo SW8260C SW5035A Analysis Date 5/8/2014 SegNo: 31294 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 38 5.6 5564 0 675 26 108 Qualifiers: R RPD outside accepted recovery lams S Spike Recovery outside accepted recovery hmits Original Page 58 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 o Street ANALYTI CAL Farmingdale,New York 11735 LOBO- ATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID 1405040-008AMS SampType. MS TestCode: 8260_S Units- pg/Kg-dry Prep Date: 5/8/2014 RunNo: 1796 Client ID: SD-Rear Batch ID. 1123 TestNo: SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31294 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,2,2-Tetrachloroethane 40 56 55.64 0 71.1 18 109 1,1,2-Trichloroethane 34 56 55.64 0 616 21 105 1,1-Dichloroethane 41 5.6 55.64 0 732 28 108 1,1-Dichloroethene 41 5.6 55.64 0 732 24 110 1,2-Dichlorobenzene 22 5.6 55.64 0 40.1 18 108 1,2-Dichloroethane 36 5.6 55.64 0 644 21 105 1,2-Dichloropropane 38 56 55.64 0 67.6 29 107 1,3-Dichlorobenzene 25 5.6 55.64 0 45.4 20 115 1,4-Dichlorobenzene 25 5.6 55.64 0 44.8 21 117 2-Chloroethyl vinyl ether 6.0 56 55.64 0 108 18 113 S. Benzene 38 56 55.64 0 67.8 30 103 Bromodichloromethane 33 5.6 55.64 0 60.1 22 106 Bromoform 38 5.6 5564 0 67.5 20 113 Bromomethane 6.2 5.6 55.64 0 111 20 130 S. Carbon tetrachloride 36 56 55.64 0 65.3 23 111 Chlorobenzene 30 56 55.64 0 54.3 27 117 Chloroethane 61 56 5564 0 110 30 130 Chloroform 38 5.6 55.64 0 680 24 112 Chloromethane 33 5.6 55.64 0 593 21 130 cis-1,3-Dichloropropene 22 5.6 55.64 0 39.4 20 104 Dibromochloromethane 31 5.6 5564 0 56.4 22 104 Ethylbenzene 33 56 55.64 0 59.5 30 115 Methylene chloride 19 5.6 55.64 7 281 20.9 22 104 BS* Tetrachloroethene 26 5.6 55.64 0 474 20 103 Toluene 34 56 55.64 0 61 1 20 115 trans-1,2-Dichloroethene 39 5.6 55.64 0 693 23 107 Qualifiers R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 59 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABOR®TORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website:www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID 1405040-008AMS SampType MS TestCode• 8260_S Units: pg/Kg-dry Prep Date- 5/8/2014 RunNo: 1796 Client ID- SD-Rear Batch ID: 1123 TestNo SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31294 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit HlghLlmit RPD Ref Val %RPD RPDLimit Qual trans-1,3-Dichloropropene 24 56 5564 0 426 20 105 Trichloroethene 33 56 5564 0 602 22 138 Trichlorofluoromethane 58 56 5564 0 104 22 131 Vinyl chloride 52 56 5564 0 92.7 30 130 Surr.4-Bromofluorobenzene 51 5564 91.2 56 133 Surr Dibromofluoromethane 59 5564 105 60 132 Surr-Toluene-d8 54 5564 97.2 69 125 Sample ID 1405040-008AMSD SampType MSD TestCode• 8260_S Units pg/Kg-dry Prep Date 5/8/2014 RunNo: 1796 Client ID: SD-Rear Batch ID- 1123 TestNo. SW8260C SW5035A Analysis Date. 5/8/2014 SegNo: 31295 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 35 57 5654 0 61.3 26 108 37.55 807 20 1,1,2,2-Tetrachloroethane 36 5.7 56.54 0 629 18 109 39.58 10.7 20 1,1,2-Trichloroethane 33 57 5654 0 576 21 105 3428 519 20 1,1-Dichloroethane 40 57 5654 0 70.6 28 108 40.75 205 20 1,1-Dichloroethene 39 57 5654 0 68.8 24 110 4073 460 20 1,2-Dichlorobenzene 19 5.7 56.54 0 337 18 108 2233 15.7 20 1,2-Dichloroethane 36 5.7 56.54 0 631 21 105 3584 0.442 20 1,2-Dlchloropropane 35 57 5654 0 628 29 107 37.64 5.86 20 1,3-Dichlorobenzene 22 57 5654 0 38.1 20 115 25.27 159 20 1,4-Dichlorobenzene 21 57 5654 0 37.4 21 117 24.91 164 20 2-Chloroethyl vinyl ether 5.4 57 5654 0 950 18 113 6.020 114 20 JS` Benzene 36 5 7 5654 0 642 30 103 3775 3.86 20 Bromodichloromethane 31 5 7 56.54 0 554 22 106 3343 6.55 20 Qualifiers: R RPD outside accepted recovery bouts S Spike Recovery outside accepted recovery lints Original Page 60 of 105 �M ERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1123 Sample ID 1405040-008AMSD SampType. MSD TestCode: 8260_S Units pg/Kg-dry Prep Date: 518/2014 RunNo: 1796 Client ID: SD-Rear Batch ID: 1123 TestNo: SW8260C SW5035A Analysis Date: 5/8/2014 SegNo: 31295 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imlt RPD Ref Val %RPD RPDLimit Qual Bromoform 35 5.7 56.54 0 61.6 20 113 37.56 7.51 20 Bromomethane 11 5.7 56.54 0 19.1 20 130 6.176 54.4 20 RS* Carbon tetrachloride 33 5.7 56.54 0 575 23 111 3631 11.0 20 Chlorobenzene 27 5.7 56.54 0 470 27 117 3024 13.0 20 Chloroethane 62 57 5654 0 110 30 130 61 16 1.49 20 Chloroform 37 57 5654 0 64.7 24 112 37.83 3.41 20 Chloromethane 39 57 5654 0 68.7 21 130 32.97 163 20 cis-1,3-Dichloropropene 22 5.7 5654 0 38.9 20 104 21.95 0 115 20 Dibromochloromethane 29 57 5654 0 50.9 22 104 31.40 8.81 20 Ethylbenzene 28 57 56.54 0 50.2 30 115 33.08 15.3 20 Methylene chloride 19 5.7 56.54 7.281 210 22 104 1892 1.36 20 BS* Tetrachloroethene 22 5.7 56.54 0 389 20 103 2639 18.2 20 Toluene 31 5.7 56.54 0 54.0 20 115 33.98 10.6 20 trans-1,2-Dichloroethene 38 5.7 56.54 0 66.7 23 107 38.55 2.20 20 trans-1,3-Dichloropropene 23 5.7 5654 0 41.1 20 105 2373 1.98 20 Trichloroethene 30 57 5654 0 536 22 138 3347 9.90 20 Trichlorofluoromethane 53 57 5654 0 941 22 131 57.70 8.13 20 Vinyl chloride 53 57 5654 0 93.0 30 130 51.59 1.94 20 Surr:4-Bromofluorobenzene 52 5654 91 5 56 133 0 0 Surr:Dlbromofluoromethane 60 56.54 107 60 132 0 0 Surr-Toluene-d8 56 56.54 98.2 69 125 0 0 Qualifiers: R RPD outside accepted recovery binds S Spike Recovery outside accepted recovery lards Original Page 61 of 105 _ �MERAmerican Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street �NAL`I�C-�N r I ICA - Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website-www.Amertcan-AnalytrcaLcom 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType LCS TestCode: 8260_W Units: pg/L Prep Date: 5/8/2014 RunNo. 1819 Client ID: LCSW Batch ID. 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31654 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 36 2.0 50.00 0 71.5 35 131 1,1,2,2-Tetrachloroethane 37 20 50.00 0 74.4 33 152 1,1,2-Trichloroethane 41 2.0 50.00 0 82.0 38 121 1,1-Dichloroethane 33 20 50.00 0 66.9 31 132 1,1-Dichloroethene 30 2.0 5000 0 597 22 131 1,2-Dichlorobenzene 38 2.0 50.00 0 75.3 44 123 1,2-Dichloroethane 42 20 50.00 0 83.2 43 127 1,2-Dichloropropane 42 20 5000 0 836 42 126 1,3-Dichlorobenzene 38 20 5000 0 75.1 45 127 1,4-Dichlorobenzene 37 20 5000 0 73.7 43 126 2-Chloroethyl vinyl ether ND 40 50.00 0 0 20 133 SU Benzene 42 2 0 50.00 0 834 30 137 Bromodichloromethane 42 2 0 50.00 0 83.0 38 122 Bromoform 36 2 0 50.00 0 727 46 128 Bromomethane 29 4.0 50.00 0 580 27 146 Carbon tetrachloride 37 2.0 5000 0 734 35 134 Chlorobenzene 39 2.0 5000 0 770 47 120 Chloroethane 46 2 0 5000 0 92.3 38 130 Chloroform 35 2 0 50.00 0 703 35 138 Chloromethane 52 2.0 50.00 0 104 20 155 cis-1,3-Dichloropropene 41 2 0 50.00 0 81 8 33 120 Dibromochloromethane 41 2 0 50.00 0 82.2 42 128 Ethylbenzene 39 2 0 50.00 0 77.8 46 134 Methylene chloride 6.3 2.0 50.00 0 126 27 137 BS* Tetrachloroethene 36 2.0 50.00 0 72 2 30 125 Toluene 41 2.0 5000 0 823 32 126 Quatitlers: R RPD outside accepted recovery huuts S Spike Recovery outside accepted recovery hmds Original Page 62 of 105 - ERIC�I V American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street AlAM'ALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website•www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType LCS TestCode. 8260_W Units. pg/L Prep Date 5/8/2014 RunNo. 1819 Client ID. LCSW Batch ID: 1128 TestNo• SW8260C SW5030C Analysis Date: 5/812014 SegNo• 31654 1 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual trans-1,2-Dlchloroethene 29 20 5000 0 587 24 130 trans-1,3-Dlchloropropene 42 20 50.00 0 84.3 30 120 Trichloroethene 39 2.0 50.00 0 785 41 125 Trichlorofluoromethane 50 2.0 5000 0 100 38 149 Vinyl chloride 56 2.0 50.00 0 113 24 152 Surr.4-Bromofluorobenzene 48 50.00 95.8 70 128 Surr:Dibromofluoromethane 47 50.00 931 75 129 Surr Toluene-d8 52 50.00 104 70 124 Sample ID MB-1128 SampType. MBLK TestCode: 8260_W Units: pg/L Prep Date. 5/8/2014 RunNo: 1819 Client ID: PBW Batch ID 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31655 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1,1,2-Tetrachloroethane ND 2.0 U 1,1,1-Trichloroethane ND 2.0 U 1,1,2,2-Tetrachloroethane ND 20 U 1,1,2-Trichloro-1,2,2-trifluoroethane ND 20 U 1,1,2-Trichloroethane ND 20 U 1,1-Dichloroethane ND 2.0 U 1,1-Dichloroethene ND 2.0 U 1,1-Dichloropropene ND 20 U 1,2,3-Trichlorobenzene ND 2.0 U 1,2,3-Trichloropropane ND 2.0 U 1,2,4,5-Tetramethylbenzene ND 2.0 U 1,2,4-Trichlorobenzene ND 2.0 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 63 of 105 4 i AM ERICAN American Analytical Laboratories,GLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WOM 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode 8260_W Units pg/L Prep Date 5/8/2014 RunNo• 1819 Client ID- PBW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date. 5/8/2014 SegNo 31655 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trimethylbenzene ND 2.0 U 1,2-Dibromo-3-chloropropane ND 2.0 U 1,2-Dibromoethane ND 2.0 U 1,2-Dichlorobenzene ND 20 U 1,2-Dichloroethane ND 20 U 1,2-Dichloropropane ND 20 U 1,3,5-Trimethylbenzene ND 2.0 U 1,3-Dichlorobenzene ND 20 U 1,3-dichloropropane ND 20 U 1,4-Dichlorobenzene ND 20 U 1,4-Dioxane ND 2.0 U 2,2-Dichloropropane ND 2.0 U 2-Butanone ND 5.0 U 2-Chloroethyl vinyl ether ND 4.0 U 2-Chlorotoluene ND 2.0 U 2-Hexanone ND 5.0 U 2-Propanol ND 2.0 U 4-Chlorotoluene ND 2.0 U 4-Isopropyltoluene ND 2 0 U 4-Methyl-2-pentanone ND 5 0 U Acetone 2.4 5.0 J. Benzene ND 2.0 U Bromobenzene ND 2.0 U Bromochloromethane ND 2.0 U Bromodichloromethane ND 2.0 U Bromoform ND 2.0 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 64 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 AW L�BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType. MBLK TestCode: 8260_W Units. pg/L Prep Date. 5/8/2014 RunNo: 1819 Client ID: PBW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date. 5/8/2014 SegNo- 31655 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Bromomethane ND 40 U Carbon disulfide ND 2.0 U Carbon tetrachloride ND 2.0 U Chlorobenzene ND 2.0 U Chlorodifluoromethane ND 2.0 U. Chloroethane ND 20 U Chloroform ND 20 U Chloromethane ND 20 U cis-1,2-Dichloroethene ND 20 U cis-1,3-Dichloropropene ND 2.0 U Cyclohexane ND 2.0 U Dibromochloromethane ND 2.0 U Dibromomethane ND 2.0 U Dichlorodifluoromethane ND 2.0 U Diisopropyl ether ND 20 U Ethanol ND 10 U Ethylbenzene ND 2.0 U Freon-114 ND 2.0 U Hexachlorobutadiene ND 2.0 U Isopropylbenzene ND 2.0 U m,p-Xylene ND 4.0 U Methyl Acetate ND 2.0 U Methyl tert-butyl ether ND 20 U Methylene chloride 25 2.0 n-Butylbenzene ND 2.0 U n-Propylbenzene ND 2.0 U Qualifiers: R RPD outside accepted recovery lututs S Spike Recovery outside accepted recovery lands Original Page 65 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street -NALYTI CAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website-www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode: 8260_W Units: pg/L Prep Date. 5/8/2014 RunNo. 1819 Client ID: PBW Batch ID 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo. 31655 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual Naphthalene ND 20 U o-Xylene ND 2.0 U p-Dlethylbenzene ND 2.0 U p-Ethyltoluene ND 2.0 U sec-Butyl benzene ND 2.0 U Styrene ND 20 U t-Butyl alcohol ND 10 U tert-Butyl benzene ND 20 U Tetrachloroethene ND 20 U Toluene ND 20 U trans-1,2-Dichloroethene ND 2.0 U trans-1,3-Dlchloropropene ND 2.0 U Trichloroethene ND 2.0 U Trichlorofluoromethane ND 2.0 U Vinyl acetate ND 2.0 U. Vinyl chloride ND 2.0 U Surr 4-Bromofluorobenzene 48 5000 958 70 128 Surr Dibromofluoromethane 54 50.00 108 75 129 Surr Toluene-d8 52 50.00 103 70 124 Qualiflers' R RPD outside accepted recovery lariats S Spike Recovery outside accepted recovery lints Original Page 66 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www.Amertcan-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType: LCS TestCode: 8260_W Units: pg/L Prep Date: 5/8/2014 RunNo: 1814 Client ID: LCSW Batch ID* 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31622 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 36 20 50.00 0 715 35 131 1,1,2,2-Tetrachloroethane 37 2.0 50.00 0 744 33 152 1,1,2-Trichloroethane 41 20 50.00 0 820 38 121 1,1-Dichloroethane 33 2.0 50.00 0 669 31 132 1,1-Dichloroethene 30 20 50.00 0 59.7 22 131 1,2-Dichlorobenzene 38 20 50.00 0 75.3 44 123 1,2-Dichloroethane 42 20 50.00 0 83.2 43 127 1,2-Dlchloropropane 42 2.0 50.00 0 836 42 126 1,3-Dichlorobenzene 38 20 50.00 0 75.1 45 127 1,4-Dichlorobenzene 37 20 50.00 0 73.7 43 126 Benzene 42 2 0 50.00 0 83.4 30 137 Bromodichloromethane 42 2 0 50.00 0 83.0 38 122 Bromoform 36 2 0 50.00 0 727 46 128 Bromomethane 29 4.0 50.00 0 58 0 27 146 Carbon tetrachloride 37 2.0 50.00 0 73.4 35 134 Chlorobenzene 39 2.0 50.00 0 77.0 47 120 Chloroethane 46 2 0 50.00 0 92.3 38 130 Chloroform 35 2 0 50.00 0 703 35 138 Chloromethane 52 2 0 50.00 0 104 20 155 cis-1,3-Dichloropropene 41 2.0 50.00 0 818 33 120 Dlbromochloromethane 41 2.0 50.00 0 82.2 42 128 Ethylbenzene 39 2 0 50.00 0 77.8 46 134 Methylene chloride 6.3 2 0 50.00 0 126 27 137 BS Tetrachloroethene 36 2.0 50.00 0 72.2 30 125 Toluene 41 2 0 50.00 0 823 32 126 trans-1,2-Dichloroethene 29 2 0 50.00 0 587 24 130 Quatiflers: R RPD outside accepted recovery lumts S Spike Recovery outside accepted recovery hunts Original Page 67 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735!& LABOR®TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType LCS TestCode• 8260_W Units. pg/L Prep Date: 5/8/2014 RunNo. 1814 Client ID LCSW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date, 5/812014 SegNo 31622 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HlghLlmlt RPD Ref Val %RPD RPDLimit Qual trans-1,3-Dichloropropene 42 2.0 50.00 0 84.3 30 120 Trichloroethene 39 20 50.00 0 78.5 41 125 Trichlorofluoromethane 50 20 5000 0 100 38 149 Vinyl chloride 56 20 5000 0 113 24 152 Surr•4-Bromofluorobenzene 48 5000 958 70 128 Surr. Dibromofluoromethane 47 5000 93.1 75 129 Surr•Toluene-d8 52 5000 104 70 124 Sample ID MB-1128 SampType: MBLK TestCode 8260_W Units: Ng/L Prep Date: 5/8/2014 RunNo: 1814 Client ID. PBW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo: 31623 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HighLlmlt RPD Ref Val %RPD RPDLimit Qual 1,1,1,2-Tetrachloroethane ND 20 U 1,1,1-Trichloroethane ND 20 U 1,1,2,2-Tetrachloroethane ND 20 U 1,1,2-Trlchloro-1,2,2-trifluomethane ND 20 U 1,1,2-Trichloroethane ND 20 U 1,1-Dichloroethane ND 2.0 U 1,1-Dichloroethene ND 2.0 U 1,1-Dichloropropene ND 2.0 U 1,2,3-Trlchlorobenzene ND 2.0 U 1,2,3-Trichloropropane ND 20 U 1,2,4,5-Tetramethyl benzene ND 20 U 1,2,4-Trichlorobenzene ND 2.0 U 1,2,4-Trimethylbenzene ND 2.0 U Qualifiers- R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 68 of 105 �MERIC-N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L®BOR-TORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType MBLK TestCode. 8260_W Units pg/L Prep Date* 5/8/2014 RunNo• 1814 Client ID: PBW Batch ID: 1128 TestNo• SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31623 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,2-Dibromo-3-chloropropane ND 20 U 1,2-Dibromoethane ND 20 U 1,2-Dichlorobenzene ND 20 U 1,2-Dichloroethane ND 20 U 1,2-Dichloropropane ND 2.0 U 1,3,5-Trimethylbenzene ND 2.0 U 1,3-Dichlorobenzene ND 2.0 U 1,3-dichloropropane ND 2.0 U 1,4-Dichlorobenzene ND 2.0 U 1,4-Dioxane ND 2.0 U 2,2-Dichloropropane ND 20 U 2-Butanone ND 50 U 2-Chloroethyl vinyl ether ND 40 U 2-Chlorotoluene ND 20 U 2-Hexanone ND 5.0 U 2-Propanol ND 2.0 U 4-Chlorotoluene ND 2.0 U 4-Isopropyltoluene ND 2.0 U 4-Methyl-2-pentanone ND 5.0 U Acetone 2.4 50 J Benzene ND 2.0 U Bromobenzene ND 2 0 U Bromochloromethane ND 2 0 U Bromodichloromethane ND 2.0 U Bromoform ND 2.0 U Bromomethane ND 4.0 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 69 of 105 AMERICAN American Analytical Laboratories,LLC. QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchED: 1128 Sample ID MB-1128 SampType: MBLK TestCode• 8260_W Units pg/L Prep Date 5/8/2014 RunNo: 1814 Client ID. PBW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo: 31623 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Hlghl-imit RPD Ref Val %RPD RPDLimit Qua[ Carbon disulfide ND 20 U Carbon tetrachloride ND 20 U Chlorobenzene ND 20 U Chlorodifluoromethane ND 20 U Chloroethane ND 20 U Chloroform ND 2.0 U Chloromethane ND 20 U cis-1,2-Dlchloroethene ND 2.0 U cls-1,3-Dichloropropene ND 2.0 U Cyclohexane ND 2.0 U Dibromochloromethane ND 2.0 U Dibromomethane ND 2.0 U Dichlorodifluoromethane ND 20 U Diisopropyl ether ND 20 U Ethanol ND 10 U Ethylbenzene ND 20 U Freon-114 ND 20 U Hexachlorobutadiene ND 20 U Isopropylbenzene ND 20 U m,p-Xylene ND 40 U Methyl Acetate ND 2.0 U Methyl tert-butyl ether ND 2.0 U Methylene chloride 2.5 2.0 n-Butylbenzene ND 2.0 U n-Propylbenzene ND 2.0 U Naphthalene ND 2.0 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 70 of 105 -n flCnl�-n' American Analytical Laboratories,LLC QC SUMMARY REPORT V'E G 'V 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX (631)454-8027 WO#. 1405040 Website.www.American-Analytical com 12-May-14 Client: Berninger Environmental,=Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode: 8260_W Units pg/L Prep Date* 5/8/2014 RunNo: 1814 Client ID- PBW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date- 5/8/2014 SegNo• 31623 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual o-Xylene ND 2.0 U p-Diethylbenzene ND 20 U p-Ethyltoluene ND 20 U sec-Butylbenzene ND 2.0 U Styrene ND 2.0 U t-Butyl alcohol ND 10 U tent-Butylbenzene ND 2.0 U Tetrachloroethene ND 2.0 U Toluene ND 2.0 U trans-1,2-Dichloroethene ND 2.0 U trans-1,3-Dichloropropene ND 20 U Trichloroethene ND 2.0 U Trichlorofluoromethane ND 20 U Vinyl acetate ND 2.0 U Vinyl chloride ND 2.0 U Surr.4-Bromofluorobenzene 48 50.00 958 70 128 Surr Dibromofluoromethane 54 5000 108 75 129 Surr-Toluene-d8 52 5000 103 70 124 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 71 of 105 AM ERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALLY 1 ICAL Farmingdale,New York 11735 LABOR-TORIES TEL-(631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www.Amertcan-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType LCS TestCode. 8260_W Units: pg/L Prep Date: 5/8/2014 RunNo: 1788 Client ID LCSW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date, 5/8/2014 SegNo• 31036 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,1,1-Trichloroethane 36 2.0 5000 0 71 5 35 131 1,1,2,2-Tetrachloroethane 37 2.0 5000 0 744 33 152 1,1,2-Trichloroethane 41 2.0 50.00 0 820 38 121 1,1-Dichloroethane 33 2.0 50.00 0 66.9 31 132 1,1-Dichloroethene 30 2.0 50.00 0 597 22 131 1,2-Dichlorobenzene 38 20 5000 0 753 44 123 1,2-Dichloroethane 42 20 5000 0 83.2 43 127 1,2-Dichloropropane 42 20 5000 0 83.6 42 126 1,3-Dichlorobenzene 38 2.0 50.00 0 751 45 127 1,4-Dichlorobenzene 37 2.0 50.00 0 737 43 126 Benzene 42 2.0 50.00 0 834 30 137 Bromodichloromethane 42 2.0 50.00 0 830 38 122 Bromoform 36 2.0 50.00 0 72.7 46 128 Bromomethane 29 4 0 50.00 0 58.0 27 146 Carbon tetrachloride 37 2 0 5000 0 734 35 134 Chlorobenzene 39 2.0 5000 0 770 47 120 Chloroethane 46 2 0 5000 0 92 3 38 130 Chloroform 35 2 0 5000 0 70.3 35 138 Chloromethane 52 2 0 50 00 0 104 20 155 cis-1,3-Dichloropropene 41 2.0 50.00 0 81.8 33 120 Dibromochloromethane 41 2.0 50.00 0 82.2 42 128 Ethylbenzene 39 2.0 50.00 0 778 46 134 Methylene chloride 6.3 2.0 50.00 0 12.6 27 137 BS Tetrachloroethene 36 2.0 50.00 0 72.2 30 125 Toluene 41 2 0 50.00 0 82.3 32 126 trans-1,2-Dichloroethene 29 2 0 50.00 0 58.7 24 130 Qualifiers: R RPD outside accepted recovery lints S Spike Recovery outside accepted recovery limits Original Page 72 of 105 AMERICAV American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street NAL`I/C1T�I CAL Farmingdale,New York 11735 LABORATORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType LCS TestCode 8260_W Units. pg/L Prep Date. 5/8/2014 RunNo. 1788 Client ID- LCSW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date 5/8/2014 SegNo 31036 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual trans-1,3-Dichloropropene 42 20 5000 0 843 30 120 Trichloroethene 39 20 50.00 0 78.5 41 125 Trichlorofluoromethane 50 2.0 50.00 0 100 38 149 Vinyl chloride 56 20 50.00 0 113 24 152 Surr-4-Bromofluorobenzene 48 50.00 968 70 128 Surr:Dibromofluoromethane 47 50.00 93.1 75 129 Surr:Toluene-d8 52 5000 104 70 124 Sample ID MB-1128 SampType: MBLK TestCode: 8260_W Units: pg/L Prep Date: 5/8/2014 RunNo: 1788 Client ID: PBW Batch ID. 1128 TestNo: SW8260C SW5030C Analysis Date, 5/8/2014 SegNo• 31037 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] 1,1,1,2-Tetrachloroethane ND 2.0 U 1,1,1-Trichloroethane ND 2.0 U 1,1,2,2-Tetrachloroethane ND 2.0 U 1,1,2-Trichloro-1,2,2-trifluoroethane ND 2.0 U 1,1,2-Trichloroethane ND 2.0 U 1,1-Dich]oroethane ND 2.0 U 1,1-Dichloroethene ND 2.0 U 1,1-Dichloropropene ND 2.0 U 1,2,3-Trichlorobenzene ND 2.0 U 1,2,3-Trichloropropane ND 2.0 U 1,2,4,5-Tetramethylbenzene ND 20 U 1,2,4-Trichlorobenzene ND 2.0 U 1,2,4-Trimethylbenzene ND 2.0 U Quatiflers: R RPD outside accepted recovery Imuts S Spike Recovery outside accepted recovery limits Original Page 73 of 105 AMERICAN American Analytical Laboratories,LLC. QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L®BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode 8260_W Units: pg/L Prep Date: 5/8/2014 RunNo. 1788 Client ID: PBW Batch ID 1128 TestNo. SW8260C SW5030C Analysis Date: 5/8/2014 SegNo 31037 Analyte Result PQL SPK value SPK Ref Val %REC LowLimlt HighLimit RPD Ref Val %RPD RPDLimit Qua[ 1,2-Dibromo-3-chloropropane ND 2.0 U 1,2-Dibromoethane ND 2.0 U 1,2-Dichlorobenzene ND 20 U 1,2-Dichloroethane ND 20 U 1,2-Dichloropropane ND 20 U 1,3,5-Trlmethylbenzene ND 20 U 1,3-Dichlorobenzene ND 2.0 U 1,3-dichloropropane ND 2.0 U 1,4-Dichlorobenzene ND 2.0 U 1,4-Dioxane ND 2.0 U 2,2-Dichloropropane ND 20 U 2-Butanone ND 50 U 2-Chloroethyl vinyl ether ND 40 U 2-Chlorotoluene ND 20 U 2-Hexanone ND 5.0 U 2-Propanol ND 2.0 U 4-Chlorotoluene ND 2.0 U 4-Isopropyltoluene ND 2.0 U 4-Methyl-2-pentanone ND 5.0 U Acetone 2.4 5.0 J Benzene ND 2 0 U Bromobenzene ND 2 0 U Bromochloromethane ND 2 0 U Bromodichloromethane ND 2.0 U Bromoform ND 2.0 U Bromomethane ND 4.0 U Qualltlers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 74 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT o Street ANALYTICAL Farmingdale,New Yo56 rk 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode 8260_W Units Ng/L Prep Date: 5/8/2014 RunNo: 1788 Client ID- PBW Batch ID: 1128 TestNo• SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31037 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit HighLimit RPD Ref Val %RPD RPDLimit Qua[ Carbon disulfide ND 20 U Carbon tetrachloride ND 2.0 U Chlorobenzene ND 2.0 U Chlorodifluoromethane ND 20 U Chloroethane ND 20 U Chloroform ND 20 U Chloromethane ND 2.0 U cis-1,2-Dichloroethene ND 2.0 U cis-1,3-Dichloropropene ND 20 U Cyclohexane ND 20 U Dibromochloromethane ND 2.0 U Dibromomethane ND 2.0 U Dichlorodifluoromethane ND 2.0 U Dnsopropyl ether ND 20 U Ethanol ND 10 U Ethylbenzene ND 20 U Freon-114 ND 2.0 U Hexachlorobutadiene ND 20 U Isopropylbenzene ND 2.0 U m,p-Xylene ND 40 U Methyl Acetate ND 20 U Methyl tert-butyl ether ND 20 U Methylene chloride 25 20 n-Butylbenzene ND 2.0 U n-Propy[benzene ND 20 U Naphthalene ND 2.0 U Qualifiers: R RPD outside accepted recovery Itauts S Spike Recovery outside accepted recovery hmrts Original Page 75 of 105 American Analytical Laboratories LLC. AMERICAN y 56 Toledo Street QC SUMMARY REPORT ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Webstte•www,American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType MBLK TestCode: 8260_W Units Ng/L Prep Date: 5/8/2014 RunNo 1788 Client ID: PBW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31037 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual o-Xylene ND 2.0 U p-Diethyl benzene ND 20 U p-Ethyltoluene ND 20 U sec-Butylbenzene ND 20 U Styrene ND 2.0 U t-Butyl alcohol ND 10 U tert-Butylbenzene ND 20 U Tetrachloroethene ND 2.0 U Toluene ND 20 U trans-1,2-Dichloroethene ND 20 U trans-1,3-Dichloropropene ND 20 U Trichloroethene ND 20 U Trichlorofluoromethane ND 20 U Vinyl acetate ND 2.0 U Vinyl chloride ND 2.0 U Surr-4-Bromofluorobenzene 48 50.00 95.8 70 128 Surr:Dibromofluoromethane 54 50.00 108 75 129 Surr Toluene-d8 52 50.00 103 70 124 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 76 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT Toledo Street ANALYTICAL Farmingdale,New York 11735 56 JUELABORATORIES TEL•(631)454-6100 FAX (631)454-8027 WO#: 1405040 Website.www American-Analytical cam 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType: LCS TestCode 8260_W Units. pg/L Prep Date: 5/8/2014 RunNo 1787 Client ID: LCSW Batch ID 1128 TestNo. SW8260C SW5030C Analysis Date. 5/8/2014 SegNo• 31643 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 1,1,1-Trichloroethane 36 2.0 5000 0 71.5 35 131 1,1,2,2-Tetrachloroethane 37 2.0 5000 0 744 33 152 1,1,2-Trichloroethane 41 2.0 5000 0 820 38 121 1,1-Dichloroethane 33 2.0 5000 0 669 31 132 1,1-Dich[oroethene 30 2.0 50.00 0 597 22 131 1,2-Dichlorobenzene 38 2.0 50.00 0 753 44 123 1,2-Dichloroethane 42 2.0 50.00 0 832 43 127 1,2-Dich[oropropane 42 2.0 50.00 0 83.6 42 126 1,3-Dichlorobenzene 38 20 50.00 0 75.1 45 127 1,4-Dichlorobenzene 37 2.0 50.00 0 73.7 43 126 Benzene 42 2 0 50.00 0 83.4 30 137 Bromodichloromethane 42 2.0 50.00 0 830 38 122 Bromoform 36 2 0 50.00 0 727 46 128 Bromomethane 29 4 0 50.00 0 580 27 146 Carbon tetrachloride 37 2.0 5000 0 73.4 35 134 Chlorobenzene 39 2.0 5000 0 77.0 47 120 Chloroethane 46 2.0 5000 0 92.3 38 130 Chloroform 35 2 0 5000 0 70.3 35 138 Chloromethane 52 2.0 5000 0 104 20 155 cis-1,3-Dich[oropropene 41 2.0 50.00 0 81.8 33 120 Dibromochloromethane 41 2.0 50.00 0 822 42 128 Ethylbenzene 39 2.0 5000 0 77.8 46 134 Methylene chloride 6.3 2.0 50.00 0 126 27 137 BS Tetrachloroethene 36 2.0 50.00 0 72.2 30 125 Toluene 41 2.0 50.00 0 82.3 32 126 trans-1,2-Dich[oroethene 29 2.0 50.00 0 587 24 130 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 77 of 105 AK ERIIAmerican Analytical Laboratories,LLC 56 Toleo Street QC SUMMARY REPORT ANALi/CAN 1 ICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website. www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchED: 1128 Sample ID LCS-1128 SampType LCS TestCode 8260_W Units pg/L Prep Date. 5/8/2014 RunNo. 1787 Client ID- LCSW Batch ID. 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31643 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual trans-1,3-Dichloropropene 42 2.0 50.00 0 843 30 120 Trichloroethene 39 20 5000 0 785 41 125 Trichlorofluoromethane 50 20 50.00 0 100 38 149 Vinyl chloride 56 20 5000 0 113 24 152 Surr 4-Bromofluorobenzene 48 5000 95.8 70 128 Surr.Dibromofluoromethane 47 5000 931 75 129 Surr Toluene-d8 52 5000 104 70 124 Sample ID MB-1128 SampType MBLK TestCode 8260_W Units. pg/L Prep Date- 5/8/2014 RunNo 1787 Client ID PBW Batch ID 1128 TestNo• SW8260C SW5030C Analysis Date: 5/8/2014 SegNo 31644 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1,1,2-Tetrachloroethane ND 20 U 1,1,1-Trichloroethane ND 20 U 1,1,2,2-Tetrachloroethane ND 20 U 1,1,2-Trichloro-1,2,24rifluoroethane ND 20 U 1,1,2-Trichloroethane ND 20 U 1,1-Dichloroethane ND 20 U 1,1-Dichloroethene ND 2.0 U 1,1-Dichloropropene ND 2.0 U 1,2,3-Trichlorobenzene ND 20 U 1,2,3-Trichloropropane ND 2.0 U 1,2,4,5-Tetramethylbenzene ND 20 U 1,2,4-Trichlorobenzene ND 20 U 1,2,4-Tri methyl benzene ND 2.0 U Qualifiers: R RPD outside accepted recovery!mots S Spike Recovery outside accepted recovery hmds Original Page 78 of 105 -OMER`IAmerican Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street ANALYTICAL ICTAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www,American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode 8260_W Units: Ng/L Prep Date: 5/8/2014 RunNo• 1787 Client ID PBW Batch ID: 1128 TestNo SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31644 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hlghl-imit RPD Ref Val %RPD RPDLimit Qual 1,2-Dibromo-3-chloropropane ND 2.0 U 1,2-Dibromoethane ND 20 U 1,2-Dichlorobenzene ND 20 U 1,2-Dlchloroethane ND 2.0 U 1,2-Dichloropropane ND 2.0 U 1,3,5-Trlmethylbenzene ND 2.0 U 1,3-Dichlorobenzene ND 2.0 U 1,3-dichloropropane ND 2.0 U 1,4-Dichlorobenzene ND 2.0 U 1,4-Dioxane ND 2.0 U 2,2-Dichloropropane ND 20 U 2-Butanone ND 50 U 2-Chloroethyl vinyl ether ND 40 U 2-Chlorotoluene ND 20 U 2-Hexanone ND 5.0 U 2-Propanol ND 2.0 U 4-Chlorotoluene ND 2.0 U 4-Isopropyltoluene ND 2.0 U 4-Methyl-2-pentanone ND 5.0 U Acetone 24 50 J Benzene ND 2.0 U Bromobenzene ND 20 U Bromochloromethane ND 2.0 U Bromodlchloromethane ND 20 U Bromoform ND 2.0 U Bromomethane ND 4.0 U Qualifiers: R RPD outside accepted recovery linuts S Spike Recovery outside accepted recovery hmrts Original Page 79 of 105 AM ERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT ANYI�-� 56 Toledo Street - TT II Farmingdale,New York 11735 LABORATORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType MBLK TestCode 8260_W Units: pg/L Prep Date 5/8/2014 RunNo. 1787 Client ID PBW Batch ID, 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31644 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Carbon disulfide ND 20 U Carbon tetrachloride ND 20 U Chlorobenzene ND 2.0 U Chlorodifluoromethane ND 20 U Chloroethane ND 20 U Chloroform ND 20 U Chloromethane ND 2.0 U cis-1,2-Dichloroethene ND 2.0 U cis-1,3-Dichloropropene ND 2.0 U Cyclohexane ND 2.0 U Dlbromochloromethane ND 2.0 U Dibromomethane ND 2.0 U Dichlorodifluoromethane ND 2.0 U Diisopropyl ether ND 20 U Ethanol ND 10 U Ethylbenzene ND 2.0 U Freon-114 ND 20 U Hexachlorobutadiene ND 20 U Isopropylbenzene ND 20 U m,p-Xylene ND 40 U Methyl Acetate ND 20 U Methyl tert-butyl ether ND 20 U Methylene chloride 2.5 2.0 n-Butylbenzene ND 2.0 U n-Propylbenzene ND 2.0 U Naphthalene ND 20 U Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 80 of 105 -MERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType: MBLK TestCode: 8260_W Units: pg/L Prep Date. 5/812014 RunNo 1787 Client ID. PBW Batch ID 1128 TestNo: SW8260C SW5030C Analysis Date, 5/8/2014 SegNo. 31644 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual o-Xylene ND 2.0 U p-Diethyl benzene ND 2.0 U p-Ethyltoluene ND 2.0 U sec-Butylbenzene ND 20 U Styrene ND 20 U t-Butyl alcohol ND 10 U tert-Butylbenzene ND 2.0 U Tetrachloroethene ND 2.0 U Toluene ND 2.0 U trans-1,2-Dichloroethene ND 2.0 U trans-1,3-Dichloropropene ND 20 U Trichloroethene ND 2.0 U Trichlorofluoromethane ND 2.0 U Vinyl acetate ND 2.0 U Vinyl chloride ND 2.0 U Surr:4-Bromofluorobenzene 48 5000 95.8 70 128 Surr.Dlbromofluoromethane 54 50.00 108 75 129 Surr Toluene-d8 52 50.00 103 70 124 Qualifiers: R RPD outside accepted recovery hnuts S Spike Recovery outside accepted recovery hinds Original Page 81 of 105 AMERICAN American Analytical Laboratories,LLC o Street QC SUMMARY REPORT -NAMICALL Farmingdale,New Yo56 rk 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www.Amerrcan-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType: LCS TestCode 8260_W Units: pg/L Prep Date 5/8/2014 RunNo. 1769 Client ID: LCSW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date- 5/8/2014 SegNo 31632 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit HighLlmit RPD Ref Val %RPD RPDLImit Qual 1,1,1-Trichloroethane 36 20 5000 0 71.5 35 131 1,1,2,2-Tetrachloroethane 37 2.0 5000 0 744 33 152 1,1,2-Trichloroethane 41 2.0 50.00 0 820 38 121 1,1-Dichloroethane 33 2.0 50.00 0 669 31 132 1,1-Dichloroethene 30 2.0 5000 0 597 22 131 1,2-Dichlorobenzene 38 2.0 5000 0 75.3 44 123 1,2-Dichloroethane 42 20 5000 0 83.2 43 127 1,2-Dlchloropropane 42 2.0 5000 0 836 42 126 1,3-Dichlorobenzene 38 20 5000 0 75.1 45 127 1,4-Dichlorobenzene 37 20 5000 0 737 43 126 Benzene 42 2 0 5000 0 83.4 30 137 Bromodichloromethane 42 2.0 50.00 0 830 38 122 Bromoform 36 2 0 50.00 0 727 46 128 Bromomethane 29 4.0 50.00 0 580 27 146 Carbon tetrachloride 37 2.0 5000 0 73.4 35 134 Chlorobenzene 39 2.0 50.00 0 77.0 47 120 Chloroethane 46 2 0 50.00 0 92.3 38 130 Chloroform 35 2 0 5000 0 703 35 138 Chloromethane 52 2 0 5000 0 104 20 155 cis-1,3-Dlchloropropene 41 2 0 5000 0 81.8 33 120 Dibromochloromethane 41 2.0 5000 0 82.2 42 128 Ethylbenzene 39 2.0 50.00 0 778 46 134 Methylene chloride 6.3 2.0 50.00 0 126 27 137 BS Tetrachloroethene 36 2.0 5000 0 72.2 30 125 Toluene 41 2.0 5000 0 82.3 32 126 trans-1,2-Dichloroethene 29 2.0 5000 0 58.7 24 130 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 82 of 105 �M ERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT � 56 Toledo Street ANALYTICAL ICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website•www.Amerrcan-Analytical com 12-May-14 Client: Benninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID LCS-1128 SampType. LCS TestCode: 8260_W Units: pg/L Prep Date: 5/812014 RunNo: 1769 Client ID: LCSW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo. 31632 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] trans-1,3-Dichloropropene 42 2.0 50.00 0 843 30 120 Trichloroethene 39 2.0 50.00 0 785 41 125 Trichlorofluoromethane 50 2.0 50.00 0 100 38 149 Vinyl chloride 56 2.0 50.00 0 113 24 152 Surr•4-Bromofluorobenzene 48 5000 95.8 70 128 Surr•Dlbromofluoromethane 47 5000 93.1 75 129 Surr.Toluene-d8 52 50.00 104 70 124 Sample ID MB-1128 SampType. MBLK TestCode: 8260_W Units: pg/L Prep Date. 5/8/2014 RunNo: 1769 Client ID: PBW Batch ID: 1128 TestNo: SW8260C SW5030C Analysis Date: 5/8/2014 SegNo: 31633 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,1,1,2-Tetrachloroethane ND 20 U 1,1,1-Trichloroethane ND 2.0 U 1,1,2,2-Tetrachloroethane ND 2.0 U 1,1,2-Trichloro-1,2,2-trifluoroethane ND 2.0 U 1,1,2-Trichloroethane ND 20 U 1,1-Dichloroethane ND 20 U 1,1-Dichloroethene ND 20 U 1,1-Dichloropropene ND 20 U 1,2,3-Trichlorobenzene ND 2.0 U 1,2,3-Tnchloropropane ND 20 U 1,2,4,5-Tetramethylbenzene ND 20 U 1,2,4-Trichlorobenzene ND 20 U 1,2,4-Trimethylbenzene ND 2.0 U Qualifiers: R RPD outside accepted recovery hints S Spike Recovery outside accepted recovery limits Original Page 83 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www,American-Analytical com 12-May-14 Client: Benninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType MBLK TestCode 8260_W Units. Ng/L Prep Date* 5/8/2014 RunNo 1769 Client ID- PBW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date, 5/8/2014 SegNo. 31633 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimlt Qual 1,2-Dibromo-3-chloropropane ND 20 U 1,2-Dibromoethane ND 20 U 1,2-Dichlorobenzene ND 20 U 1,2-Dichloroethane ND 20 U 1,2-Dichloropropane ND 2.0 U 1,3,5-Trimethylbenzene ND 20 U 1,3-Dichlorobenzene ND 20 U 1,3-dichloropropane ND 20 U 1,4-Dichlorobenzene ND 2.0 U 1,4-Dioxane ND 20 U 2,2-Dichloropropane ND 2.0 U 2-Butanone ND 5.0 U 2-Chloroethyl vinyl ether ND 4.0 U 2-Chlorotoluene ND 2.0 U 2-Hexanone ND 5.0 U 2-Propanol ND 2.0 U 4-Chlorotoluene ND 2.0 U 4-Isopropyltoluene ND 2.0 U 4-Methyl-2-pentanone ND 5.0 U Acetone 2.4 50 1 Benzene ND 2 0 U Bromobenzene ND 2 0 U Bromoch lorom ethane ND 2 0 U Bromodichloromethane ND 2 0 U Bromoform ND 2 0 U Bromomethane ND 4.0 U Quatitlers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 84 of 105 AMERICANAmerican Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York]]735 LABORATORIES TEL:(631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType. MBLK TestCode 8260_W Units: pg/L Prep Date. 5/8/2014 RunNo 1769 Client ID. PBW Batch ID: 1128 TestNo. SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31633 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Carbon disulfide ND 20 U Carbon tetrachloride ND 20 U Chlorobenzene ND 20 U Chlorodifluoromethane ND 20 U Chloroethane ND 2.0 U Chloroform ND 2.0 U Chloromethane ND 20 U as-1,2-Dichloroethene ND 2.0 U cis-1,3-Dichloropropene ND 2.0 U Cyclohexane ND 20 U Dibromochloromethane ND 2.0 U Dibromomethane ND 2.0 U Dichlorodifluoromethane ND 2.0 U Dusopropyl ether ND 2.0 U Ethanol ND 10 U Ethylbenzene ND 20 U Freon-114 ND 2.0 U Hexachlorobutadiene ND 2.0 U Isopropylbenzene ND 2.0 U m,p-Xylene ND 4.0 U Methyl Acetate ND 2.0 U Methyl tert-butyl ether ND 2.0 U Methylene chloride 25 20 n-Butylbenzene ND 20 U n-Propylbenzene ND 20 U Naphthalene ND 2.0 U Qualifiers: R RPD outside accepted recovery[mots S Spike Recovery outside accepted recovery hours Original Page 85 of 105 EEW�AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1128 Sample ID MB-1128 SampType MBLK TestCode 8260_W Units: pg/L Prep Date 5/8/2014 RunNo. 1769 Client ID, PBW Batch ID 1128 TestNo SW8260C SW5030C Analysis Date 5/8/2014 SegNo. 31633 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qua] o-Xylene ND 20 U p-Diethylbenzene ND 2.0 U p-Ethylto]uene ND 2.0 U sec-Butylbenzene ND 2.0 U Styrene ND 2.0 U t-Butyl alcohol ND 10 U tert-Butylbenzene ND 20 U Tetrachloroethene ND 2.0 U Toluene ND 20 U trans-1,2-Dichloroethene ND 20 U trans-1,3-Dichloropropene ND 20 U Trichloroethene ND 20 U Trichlorofluoromethane ND 20 U Vinyl acetate ND 20 U Vinyl chloride ND 20 U Surr 4-Bromofluorobenzene 48 50.00 958 70 128 Surr Dib romofluoromethane 54 50.00 108 75 129 Surr-Toluene-d8 52 50.00 103 70 124 Qualifiers: R RPD outside accepted recovery hits S Spike Recovery outside accepted recovery hmds Original Page 86 of 105 AMERICAN Enl^-n 1 American Analytical Laboratories,LLC QC SUMMARY REPORT =W= 56 Toledo Street -fJWANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID MB-1132 SampType: MBLK TestCode: 8270_S Units: pg/Kg Prep Date* 5/8/2014 RunNo. 1833 Client ID- PBS Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date: 5/9/2014 SegNo 31896 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimlt Qua] 3,3'-Dichlorobenzidine ND 250 U Benzidine ND 500 U Sample ID LCS-1132 SampType LCS TestCode 8270S Units. pg/Kg Prep Date: 5/8/2014 RunNo: 1833 Client ID LCSS Batch ID. 1132 TestNo- SW8270D SW3546 Analysis Date 5/9/2014 SegNo: 31897 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimlt Qual 3,3'-Dich]orobenzidine 1600 250 1982 0 78.6 10 105 Benzidine 820 500 1982 0 41.6 2 112 Sample ID 1405040-008BMS SampType MS TestCode 8270_S Units: pg/Kg-dry Prep Date: 5/8/2014 RunNo- 1833 Client ID: SD-Rear Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date. 5/9/2014 SegNo 31904 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimlt Qua] 3,3'-Dichlorobenzidlne 1200 5500 2200 0 535 5 129 DJ Benzidine 2700 11000 2200 0 124 1 106 DJS Sample ID 1405040-008BMSD SampType- MSD TestCode: 8270_S Units: pg/Kg-dry Prep Date. 5/8/2014 RunNo- 1833 Client ID. SD-Rear Batch ID: 1132 TestNo SW8270D SW3546 Analysis Date: 5/9/2014 SegNo. 31905 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimlt Qual 3,3'-Dichlorobenzidine 940 5500 2182 0 43.2 5 129 0 200 20 DJR Qualifiers: R RPD outside accepted recovery lariats S Spike Recovery outside accepted recovery kinds Original Page 87 of 105 AMER`I/CAN American Analytical Laboratories,LLC. QC SUMMARY REPORT ANALYTICICL 56 Toledo Street Farmingdale,New York]]735 L�BOR�TORIES TEL•(631)454-6100 FAX (631)454-8027 WO#: 1405040 -K Website www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchlD: 1132 Sample ID 1405040-008BMSD SampType MSD TestCode: 8270_S Units pg/Kg-dry Prep Date 5/8/2014 RunNo: 1833 Client ID SD-Rear Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date. 5/9/2014 SegNo: 31905 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Hight-imit RPD Ref Val %RPD RPDLimit Qual Benzidine 2700 11000 2182 0 124 1 106 0 200 20 DJRS Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 88 of 105 �MERICvN American Analytical Laboratories,LLC QC SUMMARY REPORT EEWEE56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABOR®TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID MB-1132 SampType, MBLK TestCode. 8270_S Units. tig/Kg Prep Date* 5/8/2014 RunNo: 1830 Client ID* PBS Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date. 5/9/2014 SegNo• 31860 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ 1,2,4-Trichlorobenzene ND 250 U 1,2-Dichlorobenzene ND 250 U 1,3-Dichlorobenzene ND 250 U 1,4-Dichlorobenzene ND 250 U 2,4-Dimtroto[uene ND 250 U 2,6-Dimtrotoluene ND 250 U 2-Chloronaphthalene ND 250 U 2-Methylnaphthalene ND 250 U 2-Nitroamline ND 250 U 3-Nitroamline ND 250 U 4-Bromophenyl phenyl ether ND 250 U 4-Ch[oroandine ND 250 U 4-Chlorophenyl phenyl ether ND 250 U 4-Nitroaniline ND 250 U Acenaphthene ND 250 U Acenaphthylene ND 250 U Aniline ND 250 U Anthracene ND 250 U Azobenzene ND 250 U Benzo(a)anthracene ND 250 U Benzo(a)pyrene ND 150 U Benzo(b)fluoranthene ND 250 U Benzo(g,h,i)perylene ND 250 U Benzo(k)fluoranthene ND 250 U Benzyl alcohol ND 250 U Bis(2-chloroethoxy)methane ND 250 U Qualifiers: R RPD outside accepted recovery hunts S Spike Recovery outside accepted recovery hmrts Original Page 89 of 105 American Analytical Laboratories LLC. AMERICAN y QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website. www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID MB-1132 SampType MBLK TestCode. 8270_S Units pg/Kg Prep Date: 5/8/2014 RunNo. 1830 Client ID, PBS Batch ID: 1132 TestNo SW8270D SW3546 Analysis Date: 5/9/2014 SegNo. 31860 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghLlmlt RPD Ref Val %RPD RPDLImIt Qua] Bls(2-chloroethyl)ether ND 250 U Bls(2-chloroisopropyl)ether ND 250 U Bls(2-ethylhexyl)phthalate ND 250 U. Butyl benzyl phthalate ND 250 U" Carbazole ND 250 U Chrysene ND 250 U Dl-n-butyl phthalate ND 250 U Dl-n-octyl phthalate ND 500 U. Dibenzo(a,h)anthracene ND 150 U Dibenzofuran ND 250 U Diethyl phthalate ND 250 U Dimethyl phthalate ND 250 U Fluoranthene ND 250 U Fluorene ND 250 U Hexachlorobenzene ND 250 U Hexachlorobutadiene ND 250 U Hexachlorocyclopentadlene ND 250 U* Hexachloroethane ND 250 U Indeno(1,2,3-c,d)pyrene ND 250 U Isophorone ND 250 U N-Nltrosodl-n-propylamine ND 150 U N-Nltrosodlmethylamine ND 250 U N-Nltrosodlphenylamine ND 250 U Naphthalene ND 250 U Nitrobenzene ND 250 U Phenanthrene ND 250 U Qualifiers: R RPD outside accepted recovery Imuts S Spike Recovery outside accepted recovery hmds Original Page 90 of 105 ®MERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID MB-1132 SampType: MBLK TestCode* 8270_S Units: pg/Kg Prep Date: 5/8/2014 RunNo: 1830 Client ID: PBS Batch ID 1132 TestNo. SW8270D SW3546 Analysis Date: 5/9/2014 SegNo: 31860 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimlt RPD Ref Val %RPD RPDLimit Qual Pyrene ND 250 U Pyndine ND 250 U Surr-2,4,6-Tribromophenol 1500 1984 74.9 11 135 Surr-2-Fluorobiphenyl 760 9921 76.4 21 143 Surr-2-Fluorophenol 1900 1984 95.7 14 122 Surr.4-Terphenyl-d14 850 9921 85.3 15 137 Surr:Nitrobenzene-d5 820 992.1 82.2 17 136 Surr:Phenol-d6 2000 1984 98.3 10 116 Sample ID LCS-1132 SampType: LCS TestCode. 8270_S Units: pg/Kg Prep Date: 5/8/2014 RunNo 1830 Client ID- LCSS Batch ID 1132 TestNo. SW8270D SW3546 Analysis Date 5/9/2014 SegNo. 31861 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Tnchlorobenzene 1600 250 1982 0 82.0 30 125 1,2-Dichlorobenzene 1700 250 1982 0 852 24 122 1,3-Dichlorobenzene 1600 250 1982 0 81.8 25 125 1,4-Dichlorobenzene 1700 250 1982 0 85.2 23 121 2,4-Dmitrotoluene 1700 250 1982 0 85.2 30 134 2,6-Dinitrotoluene 1700 250 1982 0 842 24 130 2-Chloronaphthalene 1600 250 1982 0 822 30 130 2-Methylnaphthalene 1500 250 1982 0 756 22 128 m 2-Nitroamline 1800 250 1982 0 915 25 125 3-Nitroarnline 1500 250 1982 0 773 20 120 4-Bromophenyl phenyl ether 1800 250 1982 0 887 35 135 4-Chloroanlllne 1300 250 1982 0 637 11 121 Quatiflers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 91 of 105 EEWEEAMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 o Street ANALYTICAL— Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website•www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID LCS-1132 SampType LCS TestCode: 8270_S Units: pg/Kg Prep Date: 5/8/2014 RunNo• 1830 Client ID LCSS Batch ID, 1132 TestNo- SW8270D SW3546 Analysis Date. 5/9/2014 SegNo 31861 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 4-Chlorophenyl phenyl ether 1700 250 1982 0 84.4 30 128 4-Nitroanillne 1700 250 1982 0 875 20 120 Acenaphthene 1600 250 1982 0 800 25 137 Acenaphthylene 1700 250 1982 0 834 23 136 Aniline ND 250 0 0 1 105 U Anthracene 1800 250 1982 0 885 23 150 Azobenzene 1800 250 1982 0 93.2 20 130 Benzo(a)anthracene 1800 250 1982 0 89.1 31 140 Benzo(a)pyrene 1700 150 1982 0 873 36 136 Benzo(b)fluoranthene 1700 250 1982 0 861 30 140 Benzo(g,h,l)perylene 1600 250 1982 0 815 21 143 Benzo(k)fluoranthene 1700 250 1982 0 836 30 140 Benzyl alcohol ND 250 0 0 20 125 U Bis(2-chloroethoxy)methane 1600 250 1982 0 81.9 18 110 Bls(2-chloroethyl)ether 1700 250 1982 0 85.0 30 131 Bis(2-chloroisopropyl)ether 1500 250 1982 0 734 34 124 Bis(2-ethylhexyl)phthalate 2200 250 1982 0 109 35 137 Butyl benzyl phthalate 2100 250 1982 0 105 34 140 Carbazole 1700 250 1982 0 856 20 130 Chrysene 1600 250 1982 0 81.6 31 133 Di-n-butyl phthalate 1900 250 1982 0 96.8 35 131 Dl-n-octyl phthalate 2100 500 1982 0 106 37 143 Dlbenzo(a,h)anthracene 1700 150 1982 0 87.7 24 145 Dibenzofuran 1600 250 1982 0 81 7 23 130 Diethyl phthalate 1700 250 1982 0 849 35 130 Dimethyl phthalate 1600 250 1982 0 826 32 130 Qualifiers: R RPD outside accepted recovery lunds S Spike Recovery outside accepted recovery hinds Original Page 92 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 o Street -NOLYTI CSL Farmingdale,New York 11735 L�BOR�TORIES TEL (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website x,ww.Amertcan-Analytical com 12-May-14 Client: Beminger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID LCS-1132 SampType: LCS TestCode. 8270_S Units, pg/Kg Prep Date* 5/8/2014 RunNo. 1830 Client ID. LCSS Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date: 5/9/2014 SegNo: 31861 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit Highl-imit RPD Ref Val %RPD RPDLimit Qual Fluoranthene 1600 250 1982 0 82.4 21 139 Fluorene 1600 250 1982 0 827 30 130 Hexachlorobenzene 1700 250 1982 0 843 30 130 Hexachlorobutadiene 1600 250 1982 0 82.0 30 125 Hexachlorocyclopentadiene 1500 250 1982 0 76.1 12 126 Hexachloroethane 1700 250 1982 0 86.6 30 125 Indeno(1,2,3-c,d)pyrene 1900 250 1982 0 97.5 28 141 Isophorone 1700 250 1982 0 87.4 30 125 N-Nitrosodi-n-propylamine 1800 150 1982 0 912 39 125 N-Nitrosodimethylamine 1500 250 1982 0 753 10 123 N-Nitrosodiphenylamine 770 250 1982 0 39.0 15 110 Naphthalene 1600 250 1982 0 81.9 27 131 Nitrobenzene 1700 250 1982 0 83.9 35 125 Phenanthrene 1600 250 1982 0 78.7 35 130 Pyrene 1700 250 1982 0 85.4 30 152 Pyridine ND 250 0 0 1 101 U Surr 2,4,6-Tribromophenol 1500 1982 757 11 135 Surr 2-Fluorobiphenyl 740 991.1 74.9 21 143 Surr 2-Fluorophenol 1600 1982 79.0 14 122 Surr 4-Terphenyl-d14 780 991.1 79.2 15 137 Surr:Nitrobenzene-d5 800 991.1 80.4 17 136 Surr:Phenol-d6 1500 1982 782 10 116 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery[units Original Page 93 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LrBOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website www.American-Analytical corn 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID 1405040-008BMS SampType MS TestCode 8270_S Units pg/Kg-dry Prep Date. 5/8/2014 RunNo: 1830 Client ID SD-Rear Batch ID• 1132 TestNo SW8270D SW3546 Analysis Date. 5/9/2014 SegNo. 31870 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit HighLimit RPD Ref Val %RPD RPDLimit Qual Biphenyl 2100 5500 2200 0 97.6 30 130 DJ 1,2,4-Trichlorobenzene 2000 5500 2200 0 908 21 128 DJ 1,2-Dichlorobenzene 2600 5500 2200 0 117 20 129 DJ 1,3-Dichlorobenzene 2300 5500 2200 0 104 19 122 DJ 1,4-Dichlorobenzene 2500 5500 2200 0 112 22 127 DJ 2,4,5-Trichlorophenol 2300 5500 2200 0 107 23 129 DJ 2,4,6-Trichlorophenol 2200 5500 2200 0 100 20 126 DJ 2,4-Dichlorophenol 2200 5500 2200 0 99.0 18 125 DJ 2,4-Dimethylphenol 2200 5500 2200 0 99.6 22 130 DJ 2,4-Dinitrotoluene 1600 5500 2200 0 71.8 21 124 DJ 2,6-Dinitrotoluene 1700 5500 2200 0 770 20 127 DJ 2-Chloronaphthalene 2100 5500 2200 0 935 18 145 DJ 2-Chlorophenol 2700 5500 2200 0 122 18 117 DJS 2-Methylnaphthalene 2100 5500 2200 0 934 20 120 DJm 2-Methylphenol 2600 5500 2200 0 120 20 120 DJS 2-Nitroaniline 2100 5500 2200 0 975 20 120 DJ 2-Nitrophenol 1700 5500 2200 0 790 15 121 DJ 3+4-Methylphenol 3000 5500 4399 0 68.3 25 137 DJ 3,3'-Dichlorobenzidine ND 5500 2200 0 0 5 129 DSU 4,6-Dinitro-2-methylphenol 8000 11000 2200 0 366 12 128 DJS 4-Bromophenyl phenyl ether 2200 5500 2200 0 995 27 135 DJ 4-Chloro-3-methylphenol 2100 5500 2200 0 971 20 130 DJ 4-Chloroanilme 1200 5500 2200 0 561 11 121 DJ 4-Chlorophenyl phenyl ether 2100 5500 2200 0 94.8 35 125 DJ 4-Nitroaniline 1800 5500 2200 0 829 20 120 DJ 4-Nitrophenol 2000 11000 2200 0 899 22 141 DJ Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery hinds Original Page 94 of 105 � ERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toleo Street AnM,ALYTICAL Farmingdale,New York 11735 LABOR®TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website, www American-Analytical com 12-May-14 Client: Benninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchED: 1132 Sample ID 1405040-008BMS SampType, MS TestCode• 8270_S Units: pg/Kg-dry Prep Date: 5/8/2014 RunNo. 1830 Client ID: SD-Rear Batch ID, 1132 TestNo. SW8270D SW3546 Analysis Date. 5/9/2014 SegNo• 31870 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Acenaphthene 3700 5500 2200 0 170 24 132 DJS Acenaphthylene 2100 5500 2200 0 94.5 22 134 DJ Acetophenone 2800 5500 2200 0 127 20 120 DJS Aniline ND 5500 2200 0 0 1 105 DSU Anthracene 4800 5500 2200 0 219 23 139 DJSm Atrazine ND 5500 2200 0 0 30 130 DSU Azobenzene 2300 5500 2200 0 103 5 110 DJ Benzaldehyde ND 11000 2200 0 0 30 130 DSU Benzidine ND 11000 2200 0 0 1 106 DSU Benzo(a)anthracene 16000 5500 2200 12120 156 24 134 DSm Benzo(a)pyrene 16000 3300 2200 13740 814 23 136 D Benzo(b)fluoranthene 18000 5500 2200 15740 94.5 24 132 D Benzo(g,h,i)perylene 11000 5500 2200 9118 74.3 27 131 D Benzo(k)fluoranthene 14000 5500 2200 11840 79.8 25 135 Dm Benzoic acid 18000 11000 2200 0 830 5 131 DS Benzyl alcohol ND 5500 2200 0 0 20 130 DSU Bis(2-chloroethoxy)methane 2000 5500 2200 0 922 23 133 DJ Bis(2-chloroethyl)ether 2600 5500 2200 0 117 20 120 DJ Bis(2-chloroisopropyl)ether 2200 5500 2200 0 101 32 120 DJ Bis(2-ethylhexyl)phthalate 4200 5500 2200 0 190 28 144 DJS" Butyl benzyl phthalate 2900 5500 2200 0 133 28 142 DJ" Caprolactam ND 5500 2200 0 0 20 130 DSU Carbazole 6000 5500 2200 0 273 20 130 DS Chrysene 20000 5500 2200 17860 113 24 136 D Di-n-butyl phthalate 2300 5500 2200 0 106 25 133 DJ Di-n-octyl phthalate 7600 11000 2200 0 347 23 142 DJS' Qualifiers: R RPD outside accepted recovery luntts S Spike Recovery outside accepted recovery limits Original Page 95 of 105 EEWEFAMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL ICAL Farmingdale,New York 11735 L�BOR�TORIES TEL:(631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website:www American-Analytrcal.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchED: 1132 Sample ID 1405040-008BMS SampType MS TestCode 8270_S Units: pg/Kg-dry Prep Date: 5/812014 RunNo: 1830 Client ID- SD-Rear Batch ID: 1132 TestNo SW8270D SW3546 Analysis Date. 5/9/2014 SegNo• 31870 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HighLlmlt RPD Ref Val %RPD RPDLimit Qual Dibenzo(a,h)anthracene 4200 3300 2200 0 190 24 134 DS Dlbenzofuran 3100 5500 2200 0 141 20 130 DJS Diethyl phthalate 2200 5500 2200 0 983 24 130 DJ Dimethyl phthalate 2200 5500 2200 0 991 24 131 DJ Fluoranthene 39000 5500 2200 38400 44.2 22 122 D Fluorene 4100 5500 2200 0 187 22 124 DJS Hexachlorobenzene 2200 5500 2200 0 101 25 132 DJ Hexachlorobutadlene 2200 5500 2200 0 984 23 123 DJ Hexachlorocyclopentadiene 13000 5500 2200 0 580 1 124 DS* Hexachloroethane 880 5500 2200 0 398 3 111 DJ Indeno(1,2,3-c,d)pyrene 13000 5500 2200 10880 119 26 140 D Isophorone 2200 5500 2200 0 101 23 127 DJ N-Nitrosodl-n-propylamine 2700 3300 2200 0 123 24 126 DJ N-Nltrosodlmethylamine 2100 5500 2200 0 94.0 5 110 DJ N-Nitrosodiphenylamine 1000 5500 2200 0 471 15 110 DJ Naphthalene 2200 5500 2200 0 997 20 120 DJ Nitrobenzene 2100 5500 2200 0 93.4 17 117 DJ Parathion ND 11000 2200 0 0 30 140 DSU* Pentachlorophenol 15000 11000 2200 0 678 17 116 DS Phenanthrene 29000 5500 2200 26320 143 18 126 DS Phenol 2200 5500 2200 0 986 11 106 DJ Pyrene 35000 5500 2200 30570 191 20 137 DS Pyndine ND 5500 2200 0 0 10 120 DSU Surr 2,4,6-Tribromophenol 2100 2200 97.5 11 135 D Surr.2-Fluoroblphenyl 930 1100 84.8 21 143 D Surr 2-Fluorophenol 2400 2200 111 14 122 D Qualifiers: R RPD outside accepted recovery IuMs S Spike Recovery outside accepted recovery/units Original Page 96 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL (631)454-6100 FAX. (631)454-8017 WO#: 1405040 Website•www.Amertcan-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID 1405040-008BMS SampType: MS TestCode: 8270_S Units: pg/Kg-dry Prep Date* 5/812014 RunNo: 1830 Client ID. SD-Rear Batch ID 1132 TestNo. SW8270D SW3546 Analysis Date: 5/9/2014 SegNo: 31870 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HlghLlmit RPD Ref Val %RPD RPDLImit Qual Surr:4-Terphenyl-d 14 1200 1100 105 15 137 D Surr.Nitrobenzene-d5 1000 1100 93.9 17 136 D Surr.Phenol-d6 2200 2200 101 10 116 D Sample ID 1405040-008BMSD SampType: MSD TestCode: 8270_S Units: pg/Kg-dry Prep Date: 518/2014 RunNo: 1830 Client ID. SD-Rear Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date: 519/2014 SegNo: 31871 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmlt HighLlmit RPD Ref Val %RPD RPDLImit Qual 1,2,4-Trichlorobenzene 2100 5500 2182 0 94.9 21 128 1997 3.62 20 DJ 1,2-Dichlorobenzene 2400 5500 2182 0 109 20 129 2567 7.97 20 DJ 1,3-Dichlorobenzene 2400 5500 2182 0 111 19 122 2284 5.80 20 DJ 1,4-Dichlorobenzene 2400 5500 2182 0 108 22 127 2463 4.35 20 DJ 2,4-Dinitrotoluene 1600 5500 2182 0 73.0 21 124 1578 0.983 20 DJ 2,6-Dinitrotoluene 1700 5500 2182 0 78.3 20 127 1694 0 895 20 DJ 2-Chloronaphthalene 2200 5500 2182 0 99.7 18 145 2058 5.60 20 DJ 2-Methylnaphthalene 2700 5500 2182 0 126 20 120 2053 28.8 20 DJRSm 2-Nitroanlllne 2000 5500 2182 0 91.8 20 120 2145 6.78 20 DJ 3,3'-Dichlorobenzldlne ND 5500 2182 0 0 5 129 0 0 20 DSU 4-Bromophenyl phenyl ether 2300 5500 2182 0 105 27 135 2189 4.93 20 DJ 4-Chloroaniline 1400 5500 2182 0 63.5 11 121 1235 11.6 20 DJ 4-Chlorophenyl phenyl ether 2100 5500 2182 0 964 35 125 2086 0.850 20 DJ 4-Nitroaniline 1800 5500 2182 0 82.8 20 120 1823 0 823 20 DJ Acenaphthene 8900 5500 2182 0 409 24 132 3735 B2.0 20 DRS Acenaphthylene 2200 5500 2182 0 103 22 134 2080 7.40 20 DJ Aniline ND 5500 2182 0 0 1 105 0 0 20 DSU Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 97 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX. (631)454-8027 WO#: 1405040 Website•www American-Analytical coin 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID 1405040-008BMSD SampType: MSD TestCode• 8270_S Units. Ng/Kg-dry Prep Date: 5/8/2014 RunNo: 1830 Client ID SD-Rear Batch ID. 1132 TestNo SW8270D SW3546 Analysis Date: 5/9/2014 SegNo: 31871 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Anthracene 9700 5500 2182 0 443 23 139 4817 66.9 20 DRSm Azobenzene 2200 5500 2182 0 103 5 110 2257 0.324 20 DJ Benzidine ND 11000 2182 0 0 1 106 0 0 20 DSU Benzo(a)anthracene 29000 5500 2182 12120 769 24 134 15560 600 20 DRSm Benzo(a)pyrene 27000 3300 2182 13740 595 23 136 15530 53.0 20 DRS Benzo(b)fluoranthene 30000 5500 2182 15740 639 24 132 17820 50.0 20 DRS Benzo(g,h,i)perylene 17000 5500 2182 9118 360 27 131 10750 44.9 20 DRS Benzo(k)fluoranthene 24000 5500 2182 11840 551 25 135 13590 54.9 20 DRSm Benzyl alcohol ND 5500 2182 0 0 20 130 0 0 20 DSU Bis(2-chloroethoxy)methane 2100 5500 2182 0 951 23 133 2028 2 38 20 DJ Bis(2-chloroethyl)ether 2500 5500 2182 0 115 20 120 2578 248 20 DJ Bis(2-chlorolsopropyl)ether 2100 5500 2182 0 97.0 32 120 2229 511 20 DJ Bis(2-ethylhexyl)phthalate 4500 5500 2182 0 208 28 144 4188 8.27 20 DJS* Butyl benzyl phthalate 2900 5500 2182 0 134 28 142 2923 0.409 20 DJ* Carbazole 8800 5500 2182 0 402 20 130 6003 37.6 20 DRS Chrysene 36000 5500 2182 17860 811 24 136 20340 545 20 DRS Di-n-butyl phthalate 2400 5500 2182 0 109 25 133 2325 2.46 20 DJ Di-n-octyl phthalate 7300 11000 2182 0 335 23 142 7626 4.11 20 DJS* Dibenzo(a,h)anthracene 6000 3300 2182 0 275 24 134 4175 36.1 20 DRS Dibenzofuran 6000 5500 2182 0 277 20 130 3103 64.2 20 DRS Diethyl phthalate 2100 5500 2182 0 97.2 24 130 2161 1.83 20 DJ Dimethyl phthalate 2100 5500 2182 0 97.2 24 131 2181 270 20 DJ Fluoranthene 75000 5500 2182 38400 1680 22 122 39370 62.4 20 DRS Fluorene 8900 5500 2182 0 407 22 124 4115 734 20 DRS Hexachlorobenzene 2100 5500 2182 0 970 25 132 2223 4.88 20 DJ Hexachlorobutadiene 2000 5500 2182 0 93.7 23 123 2165 5.73 20 DJ Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 98 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT A' 56 Toledo Street AI ALYTICA Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX (631)454-8027 WO#: 1405040 Website:www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1132 Sample ID 1405040-008BMSD SampType: MSD TestCode: 8270_S Units- pg/Kg-dry Prep Date, 5/8/2014 RunNo: 1830 Client ID: SD-Rear Batch ID: 1132 TestNo: SW8270D SW3546 Analysis Date: 5/9/2014 SegNo: 31871 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qua] Hexachlorocyclopentadiene 13000 5500 2182 0 580 1 124 12760 0.833 20 DS' Hexachloroethane 1200 5500 2182 0 541 3 111 875.7 29.7 20 DJR Indeno(1,2,3-c,d)pyrene 22000 5500 2182 10880 509 26 140 13500 47.9 20 DRS Isophorone 2100 5500 2182 0 96.3 23 127 2225 574 20 DJ N-Nitrosodi-n-propylamme 2700 3300 2182 0 124 24 126 2711 0.297 20 DJ N-Nitrosodimethylamme 2200 5500 2182 0 103 5 110 2068 8.26 20 DJ N-Nitrosodtphenylamme 1400 5500 2182 0 63.4 15 110 1035 28.9 20 DJR Naphthalene 2700 5500 2182 0 123 20 120 2194 203 20 DJRS Nitrobenzene 2100 5500 2182 0 97.0 17 117 2054 2.96 20 DJ Phenanthrene 64000 5500 2182 26320 1750 18 126 29470 74.5 20 DRS Pyrene 64000 5500 2182 30570 1540 20 137 34770 59.5 20 DRS Pyndine ND 5500 2182 0 0 10 120 0 0 20 DSU Surr:2,4,6-Tnbromophenol 2200 2182 103 11 135 0 0 D Surr.2-Fluorobiphenyl 930 1091 85.2 21 143 0 0 D Surr 2-Fluorophenol 2500 2182 114 14 122 0 0 D Surr 4-Terphenyl-dl4 1000 1091 95.7 15 137 0 0 D Sum Nitrobenzene-d5 1000 1091 92.7 17 136 0 0 D Surr Phenol-d6 2500 2182 114 10 116 0 0 D Qualifiers: R RPD outside accepted recovery Wmts S Spike Recovery outside accepted recovery hunts Original Page 99 of 105 American Analytical Laboratories LLC AMERICAN Amey Laboratories, Street QC SUMMARY REPORT ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX.-(631)454-8027 WO#: 1405040 Website:www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1134 Sample ID MB-1134 SampType: MBLK TestCode• 8270BN_W Units: pg/L Prep Date: 5/9/2014 RunNo: 1821 Client ID PBW Batch ID 1134 TestNo SW8270D SW3510C Analysis Date: 5/9/2014 SegNo. 31675 Analyte Result PQL SPK value SPK Ref Val %REC Lowi-imit HighLimit RPD Ref Val %RPD RPDLimit Qua[ 3,3'-Dich[orobenzidine ND 50 U Benzidine ND 10 U Sample ID LCS-1134 SampType LCS TestCode 8270BN_W Units: pg/L Prep Date. 5/9/2014 RunNo. 1821 Client ID- LCSW Batch ID 1134 TestNo• SW8270D SW3510C Analysis Date* 5/9/2014 SegNo 31676 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 3,3'-Dich[orobenzidine 32 5.0 40.00 0 811 37 115 Benzidine 9.4 10 40.00 0 236 1 101 Qualifiers' R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 100 of 105 �MERICeN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL•(631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website•wwwAmerican-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1134 Sample ID MB-1134 SampType. MBLK TestCode• 8270BN_W Units: pg/L Prep Date: 5/9/2014 RunNo. 1793 Client ID: PBW Batch ID: 1134 TestNo• SW8270D SW3510C Analysis Date: 5/9/2014 SegNo- 31185 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene ND 5.0 U 1,2-Dichlorobenzene ND 5.0 U 1,3-Dichlorobenzene ND 5.0 U 1,4-Dichlorobenzene ND 5.0 U 2,4-Dinitrotoluene ND 5.0 U 2,6-Dinitrotoluene ND 5.0 U 2-Chloronaphthalene ND 5.0 U 2-Methylnaphthalene ND 5.0 U 2-Nitroamline ND 5.0 U 3-N[troan[line ND 5.0 U 4-Bromophenyl phenyl ether ND 5.0 U 4-Chloroamline ND 5.0 U 4-Chlorophenyl phenyl ether ND 5.0 U 4-N[troan[I[ne ND 5.0 U Acenaphthene ND 5.0 U Acenaphthylene ND 5.0 U Aniline ND 50 U Anthracene ND 50 U Azobenzene ND 5.0 U Benzo(a)anthracene ND 5.0 U Benzo(a)pyrene ND 5.0 U Benzo(b)fluoranthene ND 5.0 U Benzo(g,h,i)perylene ND 5.0 U Benzo(k)fluoranthene ND 5.0 U Benzyl alcohol ND 5.0 U Bis(2-chloroethoxy)methane ND 5 0 U Qualifiers: R RPD outside accepted recovery[amts S Spike Recovery outside accepted recovery hmits Original Page 101 of 105 �MERIC�N American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALLYTIC-L Farmingdale,New York 11735 LABORALTORIES TEL.(631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website•www American-Analytical.com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1134 Sample ID MB-1134 SampType• MBLK TestCode• 8270BN W Units: pg/L Prep Date, 5/9/2014 RunNo. 1793 Client ID. PBW Batch ID 1134 TestNo: SW8270D SW3510C Analysis Date 5/9/2014 SegNo. 31185 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Bis(2-chloroethyl)ether ND 5.0 U Bis(2-chloroisopropyl)ether ND 5.0 U Bis(2-ethylhexyl)phthalate ND 50 U Butyl benzyl phthalate ND 50 U Carbazole ND 50 U Chrysene ND 50 U Dl-n-butyl phthalate ND 5.0 U Dl-n-octyl phthalate ND 5.0 U Dibenzo(a,h)anthracene ND 50 U Dibenzofuran ND 5.0 U Diethyl phthalate ND 5.0 U Dimethyl phthalate ND 5.0 U Fluoranthene ND 5.0 U Fluorene ND 5.0 U Hexachlorobenzene ND 5.0 U Hexachlorobutadiene ND 5.0 U Hexachlorocyclopentadiene ND 10 U Hexachloroethane ND 5.0 U Indeno(1,2,3-c,d)pyrene ND 50 U Isophorone ND 50 U N-Nitrosodi-n-propylamine ND 50 U N-Nitrosodimethylamine ND 50 U N-Nitrosodiphenylamine ND 50 U Naphthalene ND 5.0 U Nitrobenzene ND 5.0 U Phenanthrene ND 5.0 U Qualifiers: R RPD outside accepted recovery lumts S Spike Recovery outside accepted recovery 6mds Original Page 102 of 105 AMERICAN American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES WO#: 1405040 TEL•(631)454-6100 FAX (631)454-8027 Website•www American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1134 Sample ID MB-1134 SampType. MBLK TestCode: 8270BN_W Units: pg/L Prep Date. 5/912014 RunNo 1793 Client ID* PBW Batch ID: 1134 TestNo: SW8270D SW3510C Analysis Date: 5/9/2014 SegNo• 31185 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual Pyrene ND 50 U Pyridine ND 5.0 U Surr.2-Fluorobiphenyl 15 20.00 72.8 22 134 Surr:4-Terphenyl-d14 16 20.00 79.5 20 144 Surr•Nitrobenzene-d5 14 20.00 724 21 146 Sample ID LCS-1134 SampType: LCS TestCode: 8270BN W Units: pg/L Prep Date: 5/9/2014 RunNo: 1793 Client ID. LCSW Batch ID 1134 TestNo. SW8270D SW3510C Analysis Date 5/9/2014 SegNo 31186 Analyte Result PQL SPK value SPK Ref Val %REC Lowl-imit Highl-imit RPD Ref Val %RPD RPDLimit Qual 1,2,4-Trichlorobenzene 33 50 4000 0 829 26 140 1,2-Dichlorobenzene 33 5.0 40.00 0 83.5 50 117 1,3-Dichlorobenzene 34 5.0 40.00 0 85.4 42 120 1,4-Dichlorobenzene 34 5.0 40.00 0 84.8 45 120 2,4-Dinitrotoluene 35 5.0 4000 0 88.1 46 135 2,6-Dinitrotoluene 35 5.0 40.00 0 864 55 133 2-Chloronaphthalene 34 5.0 40.00 0 84.8 62 120 2-Methylnaphthalene 32 50 4000 0 80.3 47 125 2-Nitroaniline 36 5.0 40.00 0 90.2 42 124 3-Nitroaniline 32 50 40.00 0 80.9 50 124 4-Bromophenyl phenyl ether 35 5.0 40.00 0 88.4 33 145 4-Chloroanillne 30 5.0 40.00 0 73.8 20 120 4-Chlorophenyl phenyl ether 36 5.0 40.00 0 89.1 35 137 4-Nitroandine 36 5.0 40.00 0 89.6 20 140 Acenaphthene 34 5.0 40.00 0 84.9 34 138 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 103 of 105 -AMERICAN American Analytical Laboratories,LLC. QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 LABORATORIES TEL-(631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website.www.American-Analyttcal.com 12-May-14 Client: Benninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchUD: 1134 Sample ID LCS-1134 SampType: LCS TestCode 8270BN_W Units pg/L Prep Date: 51912014 RunNo: 1793 Client ID. LCSW Batch ID, 1134 TestNo SW8270D SW3510C Analysis Date: 5/9/2014 SegNo: 31186 Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HlghLlmit RPD Ref Val %RPD RPDLImit Qual Acenaphthylene 35 5.0 40.00 0 867 45 133 Aniline ND 5.0 0 0 5 105 U Anthracene 36 5.0 40.00 0 901 55 137 Azobenzene 37 5.0 40.00 0 93.0 45 120 m Benzo(a)anthracene 36 5.0 40.00 0 90.4 57 133 Benzo(a)pyrene 36 5 0 40.00 0 89.8 51 128 Benzo(b)fluoranthene 33 5 0 40.00 0 832 54 132 Benzo(g,h,l)perylene 36 5.0 4000 0 90.2 38 143 Benzo(k)fluoranthene 38 5 0 4000 0 94.4 58 124 Benzyl alcohol ND 5 0 0 0 20 120 U Bis(2-chloroethoxy)methane 34 5 0 4000 0 84.3 41 120 Bis(2-chloroethyl)ether 33 5.0 40.00 0 83.4 24 142 Bls(2-chloroisopropyl)ether 29 5.0 4000 0 73.0 45 129 Bls(2-ethylhexyl)phthalate 38 5 0 4000 0 94.6 49 140 Butyl benzyl phthalate 39 5 0 4000 0 964 52 136 Carbazole 36 5 0 4000 0 909 40 142 Chrysene 36 5 0 4000 0 88.8 50 134 Di-n-butyl phthalate 38 5 0 4000 0 94.3 39 131 Dl-n-octyl phthalate 37 5.0 40.00 0 91 7 45 145 Dlbenzo(a,h)anthracene 36 5.0 4000 0 907 19 145 Dibenzofuran 35 5.0 40.00 0 88.3 45 120 Diethyl phthalate 36 5.0 40.00 0 91 2 50 136 Dimethyl phthalate 36 5.0 40.00 0 891 59 129 Fluoranthene 36 5.0 40.00 0 89.3 54 134 Fluorene 35 5.0 40.00 0 87.7 52 130 Hexachlorobenzene 36 5.0 40.00 0 89 7 55 141 Qualifiers: R RPD outside accepted recovery hams S Spike Recovery outside accepted recovery limits Original Page 104 of 105 �M ERIC�I V American Analytical Laboratories,LLC QC SUMMARY REPORT 56 Toledo Street ANALYTICAL Farmingdale,New York 11735 L�BOR�TORIES TEL. (631)454-6100 FAX-(631)454-8027 WO#: 1405040 Website-www.American-Analytical com 12-May-14 Client: Berninger Environmental,Inc. Project: Rt.48 Southold,54540 Rt.48(Sound Ave),Sou BatchID: 1134 Sample ID LCS-1134 SampType: LCS TestCode: 8270BN_W Units* pg/L Prep Date: 5/9/2014 RunNo: 1793 Client ID* LCSW Batch ID: 1134 TestNo: SW8270D SW3510C Analysis Date: 5/9/2014 SegNo: 31186 Analyte Result PQL SPK value SPK Ref Val %REC LowLlmit Highl-imit RPD Ref Val %RPD RPDLimit Qua[ Hexachlorobutadiene 33 5.0 40.00 0 82.2 43 123 Hexachlorocyclopentadiene 28 10 4000 0 69.8 5 125 Hexachloroethane 35 5.0 4000 0 86.6 50 120 Indeno(1,2,3-c,d)pyrene 37 5.0 40.00 0 91.5 53 145 Isophorone 35 5.0 40.00 0 87.4 61 120 N-Nitrosodi-n-propylamine 35 5.0 40.00 0 88.0 56 122 N-Nitrosodimethylamine 17 5.0 40.00 0 432 14 109 N-Nitrosodiphenylamine 17 5.0 40.00 0 41.8 20 140 Naphthalene 34 5.0 40.00 0 84.5 18 136 Nitrobenzene 34 5.0 40.00 0 84.7 60 120 Phenanthrene 34 5.0 40.00 0 856 57 133 Pyrene 35 5.0 4000 0 872 28 141 Pyridine ND 50 0 0 10 110 U Sum 2-Fluorobiphenyl 16 20.00 78.0 22 134 Surr.4-Terphenyl-d14 16 20.00 80.1 20 144 Surr.Nitrobenzene-d5 15 20.00 775 21 146 Qualifiers: R RPD outside accepted recovery limits S Spike Recovery outside accepted recovery limits Original Page 105 of 105