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Home My WebLink AboutAnalytical Data Report for Southold Landfill 1992 t • TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT nyte senvironmentalinc. box 1518 o 60 seaview blvd., port washington, ny 11050❑ (516) 625-5500 c fax (516) 625-1274 _d _ TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT r nes environmental August 24, 1992 RECEIVED � AUG 2 55 1992 Town of Southold P.O. Box 1179 53095 Main Rd. ' I Southold, NY 11791 i Attn: Judith Terry ri j Nytest is pleased to submit our Project No. 9219242 Log in No. .13412,13425 on your sample (s) received: 7/23.,24/92 ' ? `rest sample (s) associated with this project will be retained for a period of thirty (30) days, unless Otherwise instruct- ed. - 4- My I staff is available to answer any questions concerning our report and we look forward to serving your future analytical needs. i Very truly yours, I Nytest vironLental Inc. i Remo Gigante Exec. VP rRG: Enc. Inorganic w/disk J SHIPPED VIA : Fiver Report to: Dvirka & Bartilucci 6800 Jericho Turnpike I Syosset, NY 11791 i Attn: Robbin Petrella r t 1 i R box 1518 ❑ 60 seaview blvd., port washington, ny 11050 ❑ (516) 625-5500 fax (516) 625-1274 TOTAL ANALYTICAL SERVICES FORA SAFE ENVIRONMENT r nftest environmental inc.- Project No.: 9219242 Log in No. 13412, 13425 P.O. No. Pending Date August 24, 1992 ANALYTICAL DATA REPORT PACKAGE FOR Town of Southold P.O. Box 1179 53095 Main Rd. Southhold, NY 11791 ATTN: Judith Terry REF: Southhold LandfiLL,Proj#1027 LABORATORY SAMPLE TYPE OF NUMBER IDENTIFICATION SAMPLE rSEE NEXT PAGE r NYS Lab ID #10195 WE CERTIFY THAT THIS REPORT IS A NJ Cert. #73469 TRUE REPORT OF RESULTS OBTAINED tj FROM OUR TESTS OF THIS MATERIAL. Report to: Dvirka and Bartilucci G� ' 6800 Jericho Turnpike Syosset, NY 11791 RESPECTFULLY SUBMITTED, Attn: Robbin Petrelta NYTEST ENVIRONMENTAL INC. Report on sample(s) furnished by client applies to sample(s). Report on sample(s) obtained by us applies only to lot sampled. Information contained herein is not to be used for reproduction except by special permission.Sample(s)will be retained for thirty days maximum after date of report unless specifically requested otherwise by client. In the event that there are portions or parts•of sample(s) remaining after Nytest has completed the required tests.Nytest shall have the option of returning such sample(s)to the client at the client's expense. box 1518 ❑60 seaview blvd., port washington, ny 11050 o (5161625-5500 tU.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 SOW No. : 12/91 EPA Sample No. Lab Sample ID. FB0724 342510 MWIDGW 341203 MWISGW 341201 MW2SGW 342501 MW3SGW 342502 MW6DGW 342504 MW6DGWD 342505D MW6DGWS 342506S MW6SGW 342503 MW7DGW 341204 MW7SGW 341202 PW-001 342507 PW-002 342508 PW-003 342509 Were ICP interelement corrections applied? Yes/No YES Were ICP background corrections applied? Yes/No YES If yes-were raw data generated before application of background corrections? Yes/No NO Comments: II certify that this data package is in compliance with the terms, and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer-readable data submitted on diskette has been authorized by the Laboratory Manager or the Manager's designee, as ver�fied by t e following signature. A Signature: , � ? Name: REw Gigante 1 Date: 1 ! I� Title: Executive VP COVER PAGE - IN 0 0 0 0 0 0 1 ;3/90 ' NON-CONFORMANCE SUMMARY (Case Narrative) Login No. : 13425 The sample was analyzed according to the required protocols. No problems were encountered. NOTE: Calcium, sodium, magnesium, and zinc were found to have levels greater than the CRDL. 1 1 0000002 TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT ny test environmental CHAIN OF CUSTODY RECORD Page / of� SHIP TO: Nytest Environmental Inc. REPORT TO: Client Name 60 Seaview Blvd. Address ('A5(n-n `J� 10 1 R! K Port Washington, NY 11050 (516) 625-5500 Phone Atm. 1Kc SlneG_ kx) / A) Attn Project o Pr 'ect Name Date Shipped Carrier — , OV7 -0cb Ljud /l 22L,g,ci Sampler- 'Signature, Analytical Protocol Air Bill No. Cooler No. t Sample Date/Time Sample No. Of 1.D. Sampled Description Coneys ANALYSIS REQUESTED Ity _ 75_6d�� WIT lc&)4�u , A-Pdpo-4-no Pal /��-/L-6cJ Flu Idl 5 �'ov�iv�E,�czsel hP 1�'�l��Z��S T-1 R uisn by IStgnature) Cate I Time Recd By (Signature) Date / Time Prtryc Name ��1 Pant Name Relinquished by (Signature) Date I Time Re_d by (SignatureDate / Time i Print Name Pant Name Relinquished by (Signature! Date Time 1 Recery fob a rator y !S. at r Date / Time l 7 Print Name Pr." "e � rr �� "" Special Instructions/Comments l�`ll �,[� I;r I/VI )-' / —� Ll� �/�t1./t C7l 7-123/s2 a - M w- --5-C Lj ' l� 6x 7-/a3)5�Z ak 0 Ci M 0000003 Client Retains Yellow Copy Only TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT ny test environmental inc CHAIN OF CUSTODY RECORD Page4—of _ SHIP TO: Nytest Environmental Inc. REPORT TO: Client Name —D—\; —t4 r r-t-- 60 Seaview Blvd. Address Port Washington, NY 11050 yP4- (516) 625-5500 Phone 3�0 — Z Attn. M,kQAttn. Project No. Project Na a / Date Shipped Carrier A i� TIL (S�na Con- -re) Analytical Protocol Air Bill No. Cooler No. ample Date(Time Sample No. ANALYSIS REQUESTED I.D. Sampled Description tainers ZV 1 1 1 1 fished y :Signature' Date I Time Re-o By IS,gnaturel Date Time P Name /57/ / `jQ 1 Print Name - Relmqu,shed by(Signature! Dat / Time 1 Recd by(Signature) i Date /• Time Print Name I I Pant Name Relinquished by (Signature) Date Time Recewed fo abdr y b (Sign ure) I r Time Print Name j Pr.nr Na / ✓ I / �)/' I` 7/LCA rJ`7�—t�J I`(p Special Instructions/Comments T mek.ls +c.Lkr 1 411 1n e l 4- 1 �clr �S n � 2 55&L/C 4's' �2e�� ala. �. &S 0000004 1 Client Retains Yellow Copy Only TOTAL ANALYTICAL SERVICES FOR A SAFE ENVIRONMENT ' n test environmental al ,,,c CHAIN OF CUSTODY RECORD Page_-'�_of�_ SHIP TO: Nytest Environmental Inc. REPORT TO: Client Name 60 Seaview Blvd. Address -" Port Washington, NY 11050 P' (516) 625-5500 Phone Attn._ Attn. Project No. Project Name Date hipped C rrier C/7 � Y er: Analytical Protocol Air Bill No. Cooler No. ample D to/Time Sample No, Of I.D. I Sampled Description tamers ANALYSIS REQUESTED 0`ll, c� h107— oil shed by(S,g Date Time 1 Recd By (Signature) Date / Time Print Name -""��' 9 / / Print Name Relinquished by(Signature! Date / Time j Recd by (Ssgnaturei Date / Time Print Name i Print Name Relinquished by (Signature Date ! Time 1 Rec d fo bor ory'b %IS. n ,ure) DateI% Time Print Name I PnXame 7y V 1� .4I� Special Instructions/Comments 0000005. Client Retains Yellow Coov Oniv I NYTEST ENVIRONMENTAL INC . INTERNAL CHAIN OF CUSTODY boratory Person Breaking Field meal on:: '.Sample Shuffle&A ResponsbBity for Sample NAME: /�- S ! TPTLE: Clie t:. Military Time Seal Broken: /4 W4 O SO o Date Broken 7! 2- 9/2- Login.# /3 41 Z Analytical Parameter/Fraction 3 O S E L��/t' SAMPLE NO. ALIQUOVEXTRACT NO. SAMPLE NO. ALIQUOT/EXTRACT NO. hi W -/S-6w /3 ,q/2- o � vi I 1 uATE I TI ME RELINQUISHED BY RECIEVED BY ! PURPOSE OF CHANGE OF CUSTODY 1171 i n0 'PR D Y /Q / !PRINTED SAME �C' A)cl &Q/CI^l cO/GTS�� V � SZGNATUSZGNATU PRINTE �PRINTED V �p+O SIGNATURE? !SIGNATURE 'PRINTED NAME 'PRINTED SAME, c c-VL. ;SIGNATURE !SIGNATURE 'PRINTED NAME jPRI S re + ' { � jSIGNATURE SIG � ,SrO 444 6-C PRINTED N (PRINTED NAME i SIGNATURE SIGNATURE PAINTED NAME PRINTED NAME I (SIGNATURE ISIGNATURE (PRINTED NAME (PRINTED NAME SIGNATURE SIGNATURE ( { PRINTED NAME PRINTED NAME 0000006 SIGNATURE ISIGNATURE NYTEST ENVIRONMENTAL INC. INTERNAL CHAIN OF CUSTODY boratory Person Brea]ong Field . Deal an Sample ShiiWe&Accepting Rao&mibc`lity for Sample NA.&M TITLE: Client:_ Military Time Seal Broken: i Date Broken �L Lo in 11.# ' v? Anal cal ParameterlFraction: SAMPLE NO. ALIQUOT/EXTRACT NO. SAMPLE NO. ALIQUOTMKTRACT NO. h I S GZI) DATE j TAME RFAINQUISUED BY i RECIEVED BY PURPOSE OF CHANGE OF CUSTODY PRINTE PRINTED NAME �Dt ( � ISIGNATUR V V v jSIGNATURE I I PRINT E / /�_� L I PRINTED N jSIGNATURE SIGNATd� ' PRINTED NAME PRINTED NAM iSIGN7ITURE I SIGNATURE PRINTED PRINTED D I � SIGNATUREL v jSIGNATURE PRINTED NAME �jJ - PRINTED N SIGNATURE y L SIGNATURfi I PRINTED NAME ; iPRI OfOJAG I Sao SIGNATURE C ISZGNA S ry I PRINTED N PRINTED NAME i �II SIGNATURfi ISIGNATIIRE I ;j PRINTED NAME PRINTED NANH 0000007 ` SIGNATURE SIGNATURE U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET FB0724 Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Lab Sample ID: 342510 Level (low/med) : LOW Date Received: 07/24/92 % Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 32 . 6 U P 7440-36-0 Antimony 55.2 U P ' 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 31.4 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4 .8 U P 7440-70-2 Calcium 26400 P 7440-47-3 Chromium 6. 5 U P 7440-48-4 Cobalt 7.3 U P 7440-50-8 Copper 6.4 U P 7439-89-6 Iron 10.8 U P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 8400 P 7439-96-5 Manganese 8.7 B P 7439-97-6 Mercury 0.20 U CV 7440-02-0 Nickel 16.8 U P 7440-09-7 Potassium 1610 U P 7782-49-2 Selenium 5. 0 U W F 7440-22-4 Silver 9.3 U P 7440-23-5 Sodium 10800 P 7440-28-0 Thallium 5. 0 U W F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 91. 1 P Cyanide 10. 0 U AS 101or Before: COLORLESS Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: C1000008FORM I - IN 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MWIDGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Lab Sample ID: 341203 Level (low/med) : LOW Date Received: 07/23/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 822 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 30. 1 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4.8 U P 7440-70-2 Calcium 15900 IP 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7.3 U P 7440508 Copper 11.8 B P 7439-89-6 Iron 1610 P 7439-92-1 Lead 8 .1 N F 7439-95-4 Magnesium 6910 P 7439-96-5 Manganese 224 P 7439-97-6 Mercury 0.25 CV 7440-02-0 Nickel 16.8 U P 7440-09-7 Potassium 1610 U P 7782-49-2 Selenium 5 .0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 14600 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6.0 U P 7440-66-6 Zinc 35. 3 P Cyanide 10.0 U AS tlor Before: COLORLESS Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: FORM I - IN 0000005 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MWISGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Lab Sample ID: 341201 Level (low/med) : LOW Date Received: 07/23/92 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 1190 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 51.9 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4.8 U P 7440-70-2 Calcium 6810 P 7440-47-3 Chromium 11.7 P 7440-48-4 Cobalt 7 .3 U P 7440-50-8 Copper 10.8 B P- 7439-89-6 Iron 2830 P 7439-92-1 Lead 3 .2 N F 7439-95-4 Magnesium 5260 P 7439-96-5 Manganese 327 P 7439-97-6 Mercury 0. 20 U CV 7440-02-0 Nickel 33 .4 B P 7440-09-7 Potassium 1960 B P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 22900 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 33 .8 P Cyanide 10. 0 U AS tlor Before: YELLOW Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: ' FORM I - IN 00000i0 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MW2SGW fLab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Lab Sample ID: 342501 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 173 B P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 180 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4 .8 U P 7440-70-2 Calcium 153000 P 7440-47-3 Chromium 8.5 B P 7440-48-4 Cobalt 13 .6 B P 7440-50-8 Copper 13 . 6 B P 7439-89-6 Iron 3610 P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 23300 P 7439-96-5 Manganese 5930 P 7439-97-6 Mercury 0. 33 CV 7440-02-0 Nickel 18 .0 B P 7440-09-7 Potassium 80000 P 7782-49-2 Selenium 5. 0 U W F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 74300 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 17440-66-6 Zinc 14 .8 B P Cyanide 10.0 U AS tlor Before: YELLOW Clarity Before: CLEAR Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: FORM I - IN 0000011 . 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MW3SGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Lab Sample ID: 342502 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 348 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5.0 U F 7440-39-3 Barium 210 P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4 .8 U P 7440-70-2 Calcium 121000 P 7440-47-3 Chromium 8. 5 B P 7440-48-4 Cobalt 11.9 B P 7440-50-8 Copper 11.8 B P 7439-89-6 Iron 2110 P 7439-92-1 Lead 3 .0 U N F 7439-95-4 Magnesium 27100 P 7439-96-5 Manganese 20600 P 7439-97-6 Mercury 0.40 CV 7440-02-0 Nickel 23 .9 B P 7440-09-7 Potassium 47700 P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 86800 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 14 .4 B P Cyanide 30. 0 AS tlor Before: YELLOW Clarity Before: CLEAR Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: FORM I - IN 3/90 U.S. EPA - CLP EPA SAMPLE NO. ' 1 INORGANIC ANALYSIS DATA SHEET MW6DGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Matrix (soil/water) : WATER Lab Sample ID: 342504 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 56.9 B P 7440-36-0 Antimony 55.2 U P- 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 101 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4 .8 U P 7440-70-2 Calcium 78000 P 7440-47-3 Chromium 7 . 6 B P 7440-48-4 Cobalt 13 . 6 B P ' 7440-50-8 Copper 6.4 U P 7439-89-6 Iron 18400 P 7439-92-1 Lead 3 . 0 U NW F 7439-95-4 Magnesium 38000 P 7439-96-5 Manganese 14200 P 7439-97-6 Mercury 0.20 U CV 7440-02-0 Nickel 32 .9 B P 7440-09-7 Potassium 38100 P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 99100 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 23 . 6 P Cyanide 10. 0 AS tlor Before: ORANGE Clarity Before: CLEAR Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: 0000013 FORM I - IN 3/90 r U.S. EPA - CLP EPA SAMPLE NO. ' 1 INORGANIC ANALYSIS DATA SHEET MW6SGW fLab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 'Matrix (soil/water) : WATER Lab Sample ID: 342503 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 255 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5.0 U W F 7440-39-3 Barium 123 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4.8 U P 7440-70-2 Calcium 61200 P 7440-47-3 Chromium 14. 2 P 7440-48-4 Cobalt 14.0 B P 1 7440-50-8 Copper 10. 0 B P 7439-89-6 Iron 15000 P 7439-92-1 Lead 3 .0 U N F 7439-95-4 Magnesium 15400 P 7439-96-5 Manganese 3070 P 7439-97-6 Mercury 0. 69 CV 7440-02-0 Nickel 35. 0 B P 7440-09-7 Potassium 37000 P 7782-49-2 Selenium 5.0 U W F 7440-22-4 Silver 9.3 U P 7440-23-5 Sodium 85200 P 7440-28-0 Thallium 5.0 U F 7440-62-2 Vanadium 9. 2 B P 7440-66-6 Zinc 21.2 P Cyanide 10. 0 U AS �lor Before: ORANGE Clarity Before: CLOUDY Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: 1 ' FORM I - IN 00000100000143/90 r U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MW7DGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Matrix (soil/water) : WATER Lab Sample ID: 341204 Level (low/med) : LOW Date Received: 07/23/92 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) : UG/L i CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 258 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 38. 3 B P 7440-41-7 Beryllium 1.0 U P 7440-43-9 Cadmium 6.3 P 7440-70-2 Calcium 9320 P 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7 . 3 U P 7440-50-8 Copper 6.4 U P 7439-89-6 Iron 535 P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 4680 B P 7439-96-5 Manganese 34 . 1 P 7439-97-6 Mercury 0. 34 CV 7440-02-0 Nickel 16. 8 U P 7440-09-7 Potassium 1610 U P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 70500 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 33 .4 P Cyanide 10. 0 U AS 101or Before: COLORLESS Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: ' FORM I 7 IN 0000015 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET MW7SGW Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Matrix (soil/water) : WATER Lab Sample ID: 341202 Level (low/med) : LOW Date Received: 07/23/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 238 P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F 7440-39-3 Barium 51.9 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4 .8 U P 7440-70-2 Calcium 14300 P 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7. 3 U P 1 7440-50-8 Copper 6.4 U P 7439-89-6 Iron 496 P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 3090 B P 7439-96-5 Manganese 136 P 7439-97-6 Mercury 0.20 U CV 7440-02-0 Nickel 16.8 U P 7440-09-7 Potassium 2800 B P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 14200 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6.0 U P 7440-66-6 Zinc 19. 2 B P Cyanide 10. 0 U AS glor Before: COLORLESS Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: ' FORM I - IN �i000d1 6 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET PW-001 Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 'Matrix (soil/water) : WATER Lab Sample ID: 342507 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M ' 7429-90-5 Aluminum 63. 0 B P 7440-36-0 Antimony 55.2 U P 7440-38-2 Arsenic 5. 0 U F ' 7440-39-3 Barium 20.5 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4.8 U P 7440-70-2 Calcium 5270 P 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7.3 U P ' 7440-50-8 Copper 107 P 7439-89-6 Iron 8210 P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 5320 P ' 7439-96-5 Manganese 203 P 7439-97-6 Mercury 0.39 CV 7440-02-0 Nickel 16.8 U P ' 7440-09-7 Potassium 4080 B P 7782-49-2 Selenium 5. 0 U F 7440-22-4 Silver 9. 3 U P 7440-23-5 Sodium 9870 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 10. 1 B P 7440-66-6 Zinc 35. 3 P Cyanide 10.0 U AS tlor Before: COLORLESS Clarity Before: CLEAR Texture: olor After: COLORLESS Clarity After: CLEAR Artifacts: mments: ' FORM I - IN 0000017 3/90 1 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET PW-002 Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Matrix (soil/water) : WATER Lab Sample ID: 342508 Level (low/med) : LOW Date Received: 07/24/92 iSolids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 32 . 6 U P 7440-36-0 Antimony 55.2 U P- 7440-38-2 Arsenic 5.0 U W F 7440-39-3 Barium 43 .7 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 4.8 U P 7440-70-2 Calcium 58900 P 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7. 3 U P ' 7440-50-8 Copper 268 P 7439-89-6 Iron 10.8 U P 7439-92-1 Lead 3 . 0 U N F 7439-95-4 Magnesium 15100 P ' 7439-96-5 Manganese 7 . 0 B P 7439-97-6 Mercury 0.36 CV 7440-02-0 Nickel 17. 0 B P ' 7440-09-7 Potassium 7460 P 7782-49-2 Selenium 5. 0 U W F 7440-22-4 Silver 9. 3 U P ' 7440-23-5 Sodium 11900 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6.2 B P 7440-66-6 Zinc 50.2 P Cyanide 10. 0 U AS tlor Before: COLORLESS Clarity Before: CLEAR Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: G000018 FORM I - IN 3/90 U.S. EPA - CLP EPA SAMPLE NO. 1 INORGANIC ANALYSIS DATA SHEET Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 PW-003 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Matrix (soil/water) : WATER Lab Sample ID: 342509 Level (low/med) : LOW Date Received: 07/24/92 Solids: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L CAS No. Analyte Concentration C Q M i7429-90-5 Aluminum 32 . 6 U P 7440-36-0 Antimony 55.2 U P 7440-38-T Arsenic 5. 0 U W F 7440-39-3 Barium 51.9 B P 7440-41-7 Beryllium 1. 0 U P 7440-43-9 Cadmium 5. 0 P 7440-70-2 Calcium 37000 P 7440-47-3 Chromium 6.5 U P 7440-48-4 Cobalt 7.3 U P ' 7440-50-8 Copper 83 .2 p 7439-89-6 Iron 10.8 U P 7439-92-1 Lead 3. 0 U N F ' 7439-95-4 Magnesium 11300 P 7439-96-5 Manganese 7.2 B p 7439-97-6 Mercury 0.24 CV 7440-02-0 Nickel 16.8 U P 7440-09-7 Potassium 4320 B P 7782-49-2 Selenium 5.0 U W F 7440-22-4 Silver 9.3 U P 7440-23-5 Sodium 8860 P 7440-28-0 Thallium 5. 0 U F 7440-62-2 Vanadium 6. 0 U P 7440-66-6 Zinc 32 . 1 P Cyanide 10. 0 U AS tlor Before: COLORLESS Clarity Before: CLEAR Texture: for After: COLORLESS Clarity After: CLEAR Artifacts: mments: ' 0000019 FORM I - IN 3/90 TOC ANALYSIS FORM Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SDG No. : 676 SOW No. : 3/90 ' DEC SAMPLE NO. LAB SAMPLE NO. TOC IN mg/L MW2SGW 342501 55. 6 MW3SGW 342502 36. 5 ' MW6SGW 342503 20.4 MW6DGW 342504 9. 9 MW6DGW DUPLICATE 342504D 9 .5 MW6DGW SPIKE 342504S 207 PW-001 342507 <1. 0 ' PW-002 342508 <1. 0 PW-003 342509 <1. 0 ' FB0724 342510 <1. 0 RPD : 4 . 12 o Spike Added : 200 mg/L ' Percent Recovery : 98. 6 00000 (_ 0 U.S. EPA - CLP ' 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 IlLab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Initial Calibration Source: SPEX IND. Continuing Calibration Source: SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration ' Analyte True Found %R(1) True Found %R(1) Found %R(1) M Aluminum 1000. 0 969.76 97.0 3000. 0 3072 . 07 102 .4 2991.47 99.7 P Antimony 1000. 0 1046.76 104.7 5000.0 4996.20 99.9 5025. 03 100.5 P ' Arsenic 90. 0 89.90 99 .9 50.0 52 .20 104 .4 50. 20 100.4 F Barium 1000. 0 1035.25 103 .5 3000. 0 3000. 00 100. 0 2997. 26 99 .9 P Beryllium 1000.0 1032 . 60 103 . 3 1000. 0 999. 50 100. 0 1001. 00 100. 1 P ' Cadmium 1000.0 1018.01 101.8 3000. 0 2996.83 99 .9 2964 .75 98 .8 P Calcium 26000. 0 24744 . 12 95. 2 25000. 0 24932 . 63 99 . 7 25124 . 30 100.5 P Chromium 1000. 0 1026.24 102 . 6 3000. 0 2991.88 99 .7 2989 . 10 99. 6 P Cobalt 1000. 0 1032. 14 103 . 2 3000. 0 2973 . 10 99 . 1 2926. 68 97. 6 P ' Copper 1000. 0 1012 . 13 101.2 3000. 0 3015.44 100. 5 3028. 41 100.9 P Iron 1000. 0 974. 50 97.4 12500. 0 12441. 34 99. 5 12373 .20 99 . 0 P Lead 90. 0 87.40 97 . 1 50. 0 51. 20 102 . 4 50. 10 100. 2 F ' Magnesium 1000. 0 946. 05 94. 6 7500. 0 7555. 63 100. 7 7498 .51 100. 0 P Manganese 1000. 0 1030.43 103 . 0 2000. 0 1984. 29 99 .2 1987 . 34 99.4 P Mercury 7.5 6.54 87.2 5. 0 4. 68 93 . 6 5. 00 100. 0 CV Nickel 1000. 0 1043.42 104 . 3 3000. 0 2972. 16 99 . 1 3025. 03 100.8 P Potassium 30000. 0 31519.84 105. 1 20000. 0 20187 . 00 100.9 20344 . 00 101.7 P Selenium 90. 0 86.20 95.8 50. 0 47 . 00 94 . 0 45.40 90.8 F Silver 1000. 0 1076.84 107.7 3000. 0 2999.97 100. 0 2910.82 97. 0 P ' Sodium 11000. 0 10916.24 99. 2 27500. 0 27610. 35 100.4 27290.78 99 . 2 P Thallium 90. 0 91. 10 101. 2 50. 0 50. 30 100. 6 48.70 97.4 F Vanadium 1000. 0 1003 .99 100.4 3000. 0 3005. 30 100.2 2997.76 99 . 9 P ' Zinc 1000. 0 1028.52 102.9 3000.0 2998. 05 99.9 3007 . 65 100.3 P Cyanide 500. 0 518. 00 103 . 6 100. 0 101. 00 101. 0 93 . 60 93 . 6 AS (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 ' FORM II (PART 1) - IN 0000021 3/90 U.S. EPA - CLP ' 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Initial Calibration Source: SPEX IND. Continuing Calibration Source: SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M Aluminum 3000. 0 2726. 30 90.9 3042 .46 101.4 P Antimony 5000. 0 4992 . 62 99 .9 5086.40 101.7 P ' Arsenic 50. 0 54.60 109 .2 54 . 00 108. 0 F Barium 3000. 0 3054. 26 101.8 3071. 07 102 .4 P Beryllium 1000. 0 1042 . 16 104 .2 1006. 65 100.7 P ' Cadmium 3000.0 3018.99 100. 6 3047.50 101. 6 P Calcium 25000.0 25106.71 100.4 25643 . 63 102 . 6 P Chromium 3000. 0 3089.76 103 . 0 3045. 83 101. 5 P Cobalt 3000. 0 2995.71 99.9 3028. 39 100.9 P ' Copper 3000. 0 3096. 17 103 .2 3078. 10 102 .6 P Iron 12500. 0 12216. 01 97 .7 12675.85 101.4 P Lead 50. 0 51. 00 102. 0 48. 60 97.2 F Magnesium 7500. 0 7266.55 96.9 8089. 73 107 .9 P Manganese 2000. 0 2033 . 30 101.7 2011. 16 100. 6 P Mercury 5. 0 4 .70 94. 0 CV Nickel 3000. 0 3154.28 105. 1 3078. 37 102 . 6 P Potassium 20000. 0 20681. 00 103 . 4 20408. 00 102 .0 P Selenium 50. 0 48.70 97. 4 50. 30 100. 6 F Silver 3000. 0 3117. 58 103 .9 2991. 12 99 .7 P Sodium 27500. 0 25739.62 93 . 6 28226. 88 102 . 6 P Thallium 50. 0 49.90 99.8 50. 20 100.4 F Vanadium 3000. 0 2986.88 99. 6 3064. 16 102 . 1 P Zinc 3000. 0 3077.82 102 . 6 3057. 34 101.9 P Cyanide 100. 0 96. 20 96.2 97. 40 97.4 AS (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN 0000022 3/90 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ' Initial Calibration Source: SPEX IND. Continuing Calibration Source. SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M Aluminum 3000. 0 2915.44 97 .2 3092 . 03 103 . 1 P Antimony 5000. 0 4931.23 98 . 6 5041.20 100.8 P ' Arsenic 90. 0 96.90 107.7 50. 0 50.90 101.8 49. 60 99.2 F Barium 3000.0 2971.29 99. 0 3021.86 100.7 P Beryllium 1000. 0 973.25 97. 3 988.54 98.9 P Cadmium 3000. 0 2964 .25 98. 8 2990.95 99.7 P Calcium 25000. 0 24609. 61 98.4 25071.20 100.3 P Chromium 3000.0 2915.95 97. 2 2976. 16 99.2 P Cobalt 3000.0 2906.96 96.9 2965.83 98.9 P ' Copper 3000.0 2976.76 99 .2 3037. 38 101.2 P Iron 12500.0 12211.89 97.7 12444.70 99.6 P Lead 50. 0 48.80 97 . 6 49. 20 98.4 F ' Magnesium 7500. 0 7231. 12 96.4 7459. 36 99.5 P Manganese 2000. 0 1942 .74 97 . 1 1974. 19 98 .7 P Mercury 7. 5 6. 33 84.4 5. 0 4.96 99. 2 4 .79 95.8 CV ' Nickel 3000. 0 2921.82 97 . 4 2947 .30 98.2 P Potassium 20000. 0 19543 . 00 97 .7 19929. 00 99. 6 P Selenium 50. 0 46.40 92 . 8 F Silver 3000. 0 2946.45 98 .2 3020.90 100.7 P Sodium 27500. 0 27536.96 100. 1 27730. 14 100. 8 P Thallium 50. 0 50. 60 101.2 50. 10 100.2 F Vanadium 3000. 0 2938 . 60 98. 0 2984 .84 99. 5 P Zinc 3000. 0 2955. 06 98.5 3023 .98 100.8 P Cyanide ' - (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 ' FORM II (PART 1) - IN C 0 G 0 Q j 3/90 U.S. EPA - CLP ' 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Initial Calibration Source: SPEX IND. Continuing Calibration Source: SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration ' Analyte True Found %R(1) True Found %R(1) Found %R(1) M Aluminum _ Antimony _ ' Arsenic 50. 0 48 .50 97. 0 F Barium _ Beryllium ' Cadmium — Calcium Chromium _ Cobalt _ Copper Iron _ Lead 50.0 51. 40 102 .8 F ' Magnesium Manganese _ Mercury 5. 0 4 .71 94. 2 4 . 95 99. 0 CV ' Nickel — Potassium Selenium Silver Sodium _ Thallium 50.0 50. 30 100. 6 51. 20 102 .4 F Vanadium ' Zinc Cyanide ' (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 ' FORM II (PART 1) - IN 0000024 3/90 U.S. EPA - CLP ' 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION fLab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 'Initial Calibration Source: SPEX IND. Continuing Calibration Source: SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration ' Analyte True Found %R(1) True Found %R(l) Found %R(1) M Aluminum _ Antimony Arsenic — Barium _ Beryllium Cadmium Calcium _ Chromium ' Cobalt — Copper Iron _ Lead ' Magnesium Manganese _ Mercury 5. 0 4 .72 94.4 4 .78 95. 6 CV Nickel Potassium _ Selenium Silver — Sodium Thallium 50. 0 54 .20 108 .4 52 .90 105.8 F Vanadium ' Zinc Cyanide (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (PART 1) - IN 0 0 0 0 0 '4-1-' 5 3/90 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 'Initial Calibration Source: SPEX IND. Continuing Calibration Source: SPEX / I.V. Concentration Units: ug/L Initial Calibration Continuing Calibration ' Analyte True Found %R(1) True Found %R(1) Found %R(1) M Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium ' Cobalt = Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium Silver = Sodium Thallium 50. 0 51.80 103 . 6 F Vanadium ' Zinc Cyanide (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 ' FORM II (PART 1) - IN �• � 3/90 aoaao � � U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 AA CRDL Standard Source: SPEX IND. ICP CRDL Standard Source: SPEX IND. Concentration Units: ug/L CRDL Standard for AA CRDL Standard for ICP ' Initial Final Analyte True Found %R True Found %R Found %R Aluminum Antimony 120.0 168.09 140. 1 117 .75 98. 1 Arsenic 10. 0 8.80 88. 0 Barium ' Beryllium 10. 0 10. 68 106.8 10.82 108.2 Cadmium 10. 0 11. 15 111.5 8.59 85. 9 Calcium Chromium 20. 0 17.32 86. 6 20.49 102.4 Cobalt 100. 0 101. 39 101.4 102 .90 102.9 Copper 50. 0 51.79 103 . 6 54.28 108. 6 Iron ' Lead 3 . 0 3 . 10 103 .3 Magnesium Manganese 30. 0 30.49 101. 6 29.28 97 . 6 Mercury Nickel 80. 0 90. 06 112 . 6 83 .84 104 .8 Potassium Selenium 5. 0 5. 10 102 . 0 ' Silver 20. 0 21. 52 107 . 6 17 .86 89. 3 Sodium Thallium 10. 0 9.70 97. 0 ' Vanadium 100. 0 105. 03 105. 0 102 . 57 102 . 6 Zinc 40.0 38 .83 97 . 1 42 . 37 105. 9 1 00000271FORM II (PART 2) - IN 3/90 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 AA CRDL Standard Source: SPEX IND. ICP CRDL Standard Source: SPEX IND. Concentration Units: ug/L CRDL Standard for AA CRDL Standard for ICP ' Initial Final Analyte True Found %R True Found %R Found %R Aluminum Antimony Arsenic 10.0 8.70 87. 0 Barium ' Beryllium Cadmium Calcium Chromium ' Cobalt Copper Iron Lead Magnesium Manganese Mercury Nickel Potassium Selenium ' Silver Sodium Thallium ' vanadium Zinc 0000028 FORM II (PART 2) - IN 3/90 U.S. EPA - CLP ' 3 BLANKS Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L ' Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration ' Analyte (ug/L) C 1 C 2 C 3 C Blank C M Aluminum 32 . 6 U 32 . 6 U_ 32 . 6 U 32 . 6 U_ 45.4 B P Antimony 55. 2 U 55.2 U_ 55.2 U_ 55.2 U_ 55. 2 U_ P Arsenic 5. 0 U_ 5. 0 U 5. 0 U_ 5. 0 U 5. 0 U F Barium 14 . 6 U 14. 6 U 14.6 U_ 14 . 6 U_ 14 . 6 U P Beryllium 1. 0 U 1. 0 U_ 1.0 U_ 1. 0 U_ 1. 0 U P Cadmium 4 .8 U 4.8 U 4.8 U_ 4 .8 U_ 4 .8 U P Calcium 1013 .4 U 1013 .4 U 1013 .4 U_ 1013 .4 U 1013 .4 U_ P Chromium 6.5 U_ 6. 5 U_ 6.5 U 6.5 U 6. 5 U_ P Cobalt 7. 3 U 7.3 U 7 . 3 U 7. 3 U 7 . 3' U_ P Copper 6.4 U_ 6.4 U 6.4 U -7.5 B 6.4 U_ P Iron 10. 8 U_ 10.8 U 10.8 U_ 10.8 U 10. 8 U_ P Lead 3 . 0 U_ 3 .0 U_ 3 . 0 U 3 . 0 U_ 3 . 0 U F Magnesium 1003 .4 U_ 1003.4 U_ 1003 .4 U 1003 . 4 U 1003 .4 U P Manganese 1. 2 U 1. 2 B 1.7 B 2 . 9 B 1.2 U P Mercury 0.2 U 0.2 U_ 0.2 U_ 0.2 U_ 0. 2 U CV ' Nickel 16. 8 U 16.8 U_ 16.8 U_ 16.8 U 16.8 U_ P Potassium 1610.4 U 1610.4 U 1610.4 U 61 _ 1610.4 U 10.4 U P Selenium 5. 0 U 5. 0 U 5. 0 U_ 5. 0 U 5. 0 U F Silver 9 . 3 U 9. 3 U 9.3 U_ 9. 3 U 9 . 3' U_ P Sodium 990.2 U 990. 2 U 990.2 U_ 990. 2 U 990. 2 U P Thallium 5. 0 U_ 5. 0 U 5. 0 U 5. 0 U_ 5. 0 U_ F Vanadium 6. 0 U 6. 0 U 6. 0 U_ -6. 1 B 6. 0 U P Zinc 4 . 3 U_ 4. 3 U_ 4 . 3 U 4 . 3 U_ 4. 3 U_ P Cyanide 10. 0 U 10. 0 U 10. 0 U 10. 0 U 10. 0 U AS FORM III - IN 0000029 3/90 U.S. EPA - CLP 3 BLANKS Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) . UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Aluminum _ 32 . 6 U 32.6 U 60. 0 B _ P Antimony _ 55.2 U 55.2 U 55.2 U_ _ P Arsenic _ 50.4 U_ 50.4 U _ _ P Barium _ 14. 6 U_ 14.6 U 14 . 6 U _ P Beryllium _ 1.0 U_ 1. 0 U_ 1. 0 U _ P Cadmium - 4. 8 U_ 4 .8 U_ 4. 8 U = P Calcium 1013 .4 U 1013 .4 U 1013 .4 U P Chromium _ 6.5 U 6.5 U 6.5 U_ _ P Cobalt _ 7. 3 U 7. 3 U 7. 3 U_ _ P Copper _ 6.4 U 6.4 U_ 6.4 U _ P Iron _ 10.8 U 10.8 U 24 . 3 B _ P Lead _ 3 . 0 U_ 3 .0 U 3 . 0 U_ _ F Magnesium _ 1003 .4 U_ 1003 .4 U_ 1003 .4 U _ P Manganese _ 1.7 B 1.9 B 1.2 U _ P Mercury 0. 2 U_ 0.2 U_ 0.2 U_ 0. 2 U _ CV Nickel _ 16.8 U_ 16.8 U 16.8 U _ P Potassium _ 1610.4 U 1610.4 U 1610.4 U _ P Selenium _ 5. 0 U_ 5. 0 U_ _ _ F Silver _ 9. 3 U 9.3 U 9.3 U _ P ' Sodium _ 990. 2 U 990.2 U_ 990.2 U _ P Thallium _ 5.0 U 5. 0 U 5. 0 U_ _ F Vanadium 6. 0 U 6.0 U 6. 0 U P Zinc = 4 . 3 U 4.3 U 4.3 U = P Cyanide 10. 0 U AS FORM III - IN3/90 0000030 U.S. EPA - CLP 3 BLANKS Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L i Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Aluminum Antimony Arsenic 5. 0 U_ 5.0 U_ 5.0 U_ 5.0 U_ _ F Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead _ 3 .0 U_ _ _ _ F Magnesium Manganese Mercury _ 0.2 U_ 0.2 U_ 0.2 U _ CV Nickel Potassium Selenium Silver Sodium _ Thallium _ 5. 0 U_ 5. 0 U_ 5. 0 U_ _ F Vanadium Zinc Cyanide FORM III - ING0000 3/90 U.S. EPA - CLP 3 BLANKS Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Preparation Blank Matrix (soil/water) : WATER Preparation Blank Concentration Units (ug/L or mg/kg) : UG/L ' Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M Aluminum Antimony Arsenic Barium Beryllium Cadmium - - - - - — Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Mercury _ 0.2 U_ _ CV Nickel Potassium Selenium Silver Sodium Thallium _ 5. 0 U 5.0 U _ _ F Vanadium — Zinc Cyanide FORM III - IN G0000i2 3/90 U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Vab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: 61 ICS Source: SPEX IND. Concentration Units: ug/L True Initial Found Final Found Sol. Sol. Sol. Sol. Sol. Sol. Analyte A AB A AB %R A AB %R Aluminum 540055 536472 544211 514618.5 95.9 531406 503602 .9 93 .9 Antimony 154 164.6 134 105. 6 Arsenic Barium 502 7 489.5 97.5 8 492 . 0 98. 0 Beryllium 480 0 473 . 1 98 . 6 0 465. 6 97. 0 Cadmium 907 -16 903 .9 99 .7 -11 901.7 99.4 Calcium 494040 512228 471365 444142 .9 86.7 468588 445133 .9 86.9 Chromium 529 9 498. 0 94. 1 14 498.7 94 .3 Cobalt 477 3 446.4 93 . 6 10 443 .7 93 . 0 Copper 543 -39 458.8 84. 5 -33 458.7 84.5 Iron 206236 199845 187761 177519.2 88.8 187113 177641.2 88.9 Lead Magnesium 531358 527530 498999 467197.4 88. 6 497535 472051.9 89.5 Manganese 496 28 484.0 97. 6 29 482. 3 97.2 Mercury Nickel 940 10 877.7 93 .4 11 861. 8 91.7 Potassium -655 -679.4 -338 -1497.4 Selenium Silver 960 -11 965.7 100. 6 -16 945.4 98 .5 Sodium 1588 1486. 5 1543 1435. 0 Thallium Vanadium 509 6 490. 0 96. 3 8 486. 0 95.5 Zinc 1208 207 1191. 1 98 . 6 214 1203 . 0 99. 6 ' FORM IV - IN 3/90 GO000 �3� � U.S. EPA - CLP 5A EPA SAMPLE NO. SPIKE SAMPLE RECOVERY MW6DGWS i Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 �J Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Level (low/med) : LOW % Solids for Sample: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Aluminum 75-125 2463 .9700 _ 56. 9200 B 2000. 00 120.4 _ P Antimony 75-125 623 .7700 _ 55.2000 U_ 500. 00 124. 8 _ P Arsenic 75-125 31.7000 _ 5.0000 U_ 40. 00 79.2 _ F Barium 75-125 2420.5000 _ 101. 1300 B 2000. 00 116. 0 _ P Beryllium 75-125 58.3400 _ 1.0000 U_ 50.00 116.7 _ P Cadmium 75-125 51. 1400 _ 4 .8000 U_ 50. 00 102 . 3 _ P Calcium _ _ _ NR Chromium 75-125 235.4800 _ 7. 5600 B 200. 00 114 . 0 _ P Cobalt 75-125 582 .8700 _ 13 .5800 B 500. 00 113 .9 _ P Copper 75-125 287 .7200 - 6.4000 U_ 250. 00 115. 1 _ P Iron 21111.4200 18426.5100 1000. 00 268.5 _ P Lead 75-125 26. 3000 _ 3 . 0000 U 20. 00 131.5 N F Magnesium _ _ _ NR Manganese 16531. 1300 _ 14222 .9400 _ 500. 00 461. 6 _ P Mercury 75-125 1.0500 _ 0.2000 U_ 1. 00 105. 0 _ CV Nickel 75-125 610. 2600 _ 32 .9000 B 500. 00 115.5 _ P Potassium _ _ _ NR Selenium 75-125 7.9000 _ 5. 0000 U 10. 00 79. 0 _ F Silver 75-125 46. 1500 _ 9. 3000 U_ 50. 00 92 . 3 _ P Sodium _ _ _ NR Thallium 75-125 46. 2000 _ 5. 0000 U_ 50. 00 92 .4 _ F Vanadium 75-125 576.2300 _ 6. 0000 U_ 500. 00 115.2 _ P Zinc 75-125 611.2200 _ 23 . 6200 _ 500.00 117.5 _ P Cyanide 75-125 78 . 0000 _ 10. 0000 U 100. 00 78 . 0 _ AS tmments: FORM V (PART 1) - IN 3/90 0000034 U.S. EPA - CLP 5B EPA SAMPLE NO. POST DIGEST SPIKE SAMPLE RECOVERY MW6DGWA Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Level (low/med) : LOW Concentration Units: ug/L Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Aluminum _ _ _ NR Antimony NR Arsenic — — — NR Barium NR Beryllium _ _ _ NR Cadmium _ _ _ NR Calcium _ _ _ NR Chromium _ _ _ NR Cobalt _ _ _ NR Copper _ _ _ NR Iron _ _ _ NR Lead _ _ NR Magnesium — _ — NR Manganese NR Mercury _ _ _ NR Nickel _ _ _ NR Potassium _ _ _ NR Selenium _ _ _ NR Silver _ _ _ NR Sodium _ _ _ NR Thallium _ _ _ NR Vanadium _ NR Zinc — — = NR Cyanide NR tmments: FORM V (PART 2) - IN 3/90 00000 : 5 U.S. EPA - CLP 6 EPA SAMPLE NO. DUPLICATES MW6DGWD Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Level (low/med) : LOW % Solids for Sample: 0. 0 Solids for Duplicate: 0. 0 Concentration Units (ug/L or mg/kg dry weight) : UG/L Control Analyte Limit Sample (S) C Duplicate (D) C RPD Q M Aluminum 56.9200 B 81.4300 B 35.4 _ P Antimony 55. 2000 U_ 55.2000 U _ P Arsenic 5.0000 U_ 5. 0000 U _ F Barium 101. 1300 B 98.4000 B Beryllium 1.0000 U_ 1. 0000 U _ P 1 Cadmium 4.8000 U 4 .8000 U = P Calcium 77958.9000 _ 77117. 6900 _ 1. 1 P Chromium 10. 0 7. 5600 B 11. 3400 _ 40. 0 _ P Cobalt 13 . 5800 B 14 .4000 B 5.9 _ P Copper 6.4000 U 6.4000 U _ P Iron 18426. 5100 _ 16721.7900 _ 9 .7 _ P Lead 3 . 0 3 . 0000 U 3 .2000 _ 200. 0 _ F Magnesium 38014. 1200 _ 37394. 6200 _ 1. 6 _ P Manganese 14222 . 9400 _ 14047. 6900 _ 1.2 _ P Mercury 0. 2000 U 0.2000 U CV Nickel 32 .9000 B 31. 3000 B 5. 0 = P Potassium 38061.9700 _ 38086. 1200 0. 1 P Selenium 5. 0000 U 5. 0000 U _ F Silver 9 . 3000 U 9 . 3000 U _ P Sodium 99058 .5600 _ 97740.8200 _ 1. 3 _ P Thallium 5. 0000 U_ 5. 0000 U _ F Vanadium 6. 0000 U_ 6. 0000 U_ _ P Zinc 20. 0 23 . 6200 _ 31.4100 _ 28. 3 _ P Cyanide 10. 0000 U 10. 0000 U AS tFORM VI - IN G 0 0 0 0 j 3/90 U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE ab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 olid LCS Source: EPA 212 Aqueous LCS Source: SPEX IND. Aqueous (ug/L) Solid (mg/kg) Analyte True Found %R True Found C Limits %R Aluminum 10000.0 10283 . 12 102.8 ;Antimony1000. 0 1044.01 104.4 Arsenic 90.0 96. 00 106.7 Barium 1000. 0 999.54 100. 0 Beryllium 1000.0 982.25 98.2 Cadmium 1000.0 1006.98 100.7 Calcium 51000.0 48537. 01 95.2 Chromium 1000.0 989 .75 99 .0 Cobalt 1000. 0 972 .22 97.2 Copper 1000. 0 975.85 97. 6 Iron 11000.0 9650.99 87 .7 Lead 90.0 86.40 96. 0 Magnesium 21000.0 20620.90 98.2 Manganese 1000. 0 1002 . 15 100.2 Mercury Nickel 1000. 0 959.58 96. 0 Potassium 20000. 0 20841.78 104 . 2 Selenium 90.0 83 .40 92 .7 Silver 1000. 0 856.48 85. 6 Sodium 10000. 0 10057.82 100. 6 Thallium 90. 0 87.40 97. 1 Vanadium 1000.0 983 .05 98 .3 Zinc 1000. 0 1000.85 100. 1 Cyanide FORM VII - IN 000OO 37 3/90 U.S. EPA - CLP 9 EPA SAMPLE NO. ICP SERIAL DILUTIONS MW6DGWL Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Matrix (soil/water) : WATER Level (low/med) : LOW Concentration Units: ug/L ' Serial Initial Sample Dilution Differ- Analyte Result (I) C Result (S) C ence Q M Aluminum 56.92 B 310. 05 B 444 .7 _ P Antimony 55.20 U_ 276. 00 U _ P Arsenic _ _ _ F Barium 101. 13 B 109. 30 B 8 . 1 _ P Beryllium 1. 00 U_ 5. 00 U _ P Cadmium 4 .80 U 24. 00 U _ P Calcium 77958.90 _ 80202 . 00 _ 2 .9 _ P Chromium 7.56 B 34. 65 B 358. 3 _ P Cobalt 13 .58 B 36. 50 U_ 100. 0 _ P Copper 6.40 U_ 32 . 00 U = P Iron 18426.51 18736. 20 _ 1.7 P Lead _ _ _ F Magnesium 38014 . 12 _ 41010. 15 _ 7 .9 _ P Manganese 14222 .94 _ 14461. 10 _ 1. 7 _ P Mercury _ _ _ CV Nickel 32 .90 B 103 .45 B 214 .4 _ P ' Potassium 38061.97 _ 41298 . 20 _ 8. 5 _ P Selenium _ _ _ F Silver 9.30 U 46. 50 U _ P ' Sodium 99058. 56 = 100647. 65 = 1. 6 - P Thallium F Vanadium 6. 00 U 30. 00 U_ _ P Zinc 23 . 62 _ 53 .55 B 126. 7 _ P r FORM IX - IN 0000038 3/90 j U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: 61 Date: 07/01/92 Flame AA ID Number: Furnace AA ID Number: ' Wave- length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Aluminum 308 .21 200. 0 32 . 6 P Antimony 206.83 60. 0 55. 2 P Arsenic 20. 0 50.4 P Barium 493 .40 200.0 14 . 6 P Beryllium 313 . 04 5. 0 1. 0 f:,- Cadmium Cadmium 222 .80 5. 0 4. 8 P Calcium 317.95 5000. 0 1013 .4 P Chromium 267.71 10. 0 6.5 P Cobalt 228. 61 50. 0 7. 3 P Copper 324 .75 25. 0 6.4 P Iron 259.94 100.0 10.8 P Lead 220. 35 3 . 0 48. 1 P 1 Magnesium 279. 08 5000. 0 1003 . 4 P Manganese 257 . 61 15. 0 1. 2 P Mercury 0. 2 _ Nickel 588 .99 40. 0 16. 8 P Potassium 766. 50 5000. 0 1610.4 P Selenium 196. 00 5. 0 79 .8 P Silver 328. 06 10. 0 9 . 3 P Sodium 588.99 5000. 0 990.2 P Thallium 10. 0 81. 2 P Vanadium 292 .40 50. 0 6. 0 P Zinc 213 .85 20. 0 4. 3 P Comments: 00000 : 9 FORM X - IN 3/90 U.S. EPA - CLP ' 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: Date: 07/01/92 Flame AA ID Number: Furnace AA ID Number: 3030 Wave- length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Aluminum 200. 0 _ Antimony 60. 0 _ Arsenic 197.20 BZ 10. 0 Barium 200. 0 _ Beryllium 5. 0 _ Cadmium 5. 0 _ Calcium 5000.0 Chromium 10. 0 _ Cobalt 50.0 _ 1 Copper 25. 0 _ Iron 100. 0 _ Lead 220. 00 BZ 3 . 0 3 . 0 F Magnesium 5000. 0 _ Manganese 15. 0 _ Mercury 0.2 _ Nickel 40. 0 _ Potassium 5000. 0 _ Selenium 196. 00 BZ 5. 0 5. 0 F Silver 10. 0 _ Sodium 5000. 0 Thallium 276.80 BZ 10. 0 5. 0 F Vanadium 50. 0 _ Zinc 20.0 _ Comments: 4 0 FORM X - IN 3/90 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: Date: 07/01/92 ' Flame AA ID Number: Furnace AA ID Number: Wave- length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Aluminum 200. 0 _ Antimony 60. 0 _ Arsenic 10. 0 = Barium 200. 0 Beryllium 5. 0 _ Cadmium 5. 0 _ Calcium 5000. 0 — Chromium 10. 0 _ Cobalt 50. 0 _ Copper 25. 0 — Iron 100.0 _ Lead 3.0 _ Magnesium 5000. 0 _ Manganese 15. 0 — Mercury 253 .70 0.2 0. 2 CV Nickel 40. 0 _ ' Potassium 5000. 0 — Selenium 5.0 _ Silver 10. 0 _ Sodium 5000. 0 = Thallium 10.0 Vanadium 50.0 _ Zinc 20. 0 _ Comments: 00000 -11 FORM X - IN 3/90 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (QUARTERLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: Date: 07/01/92 Flame AA ID Number: Furnace AA ID Number: 3030#2 Wave- length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Aluminum 200. 0 _ Antimony 60. 0 _ Arsenic 193.70 BZ 10.0 Barium 200.0 _ Beryllium 5. 0 _ Cadmium 5. 0 _ Calcium 5000. 0 _ Chromium 10. 0 _ Cobalt 50. 0 _ Copper 25. 0 Iron 100. 0 _ Lead 220. 35 BZ 3 . 0 1. 0 F Magnesium 5000. 0 — Manganese 15. 0 Mercury 0. 2 _ Nickel 40. 0 _ Potassium 5000. 0 Selenium 196.00 BZ 5. 0 3 . 0 F Silver 10. 0 _ Sodium 5000. 0 Thallium 190. 86 BZ 10. 0 5. 0 F Vanadium 50. 0 ' Zinc 20. 0 — Comments: 0000042 FORM X - IN 3/90 U.S . EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: 61 Date: 06/01/92 Wave- Interelement Correction Factors for: length Analyte (nm) Al Ca Fe Mg NI Aluminum 308.21 -0. 0002800 Antimony 206.83 0. 0003440 Arsenic 193 .70 0.0054380 0.0009350 0.0009350 Barium 493 .40 Beryllium 313.04 Cadmium 222 .80 -0. 0000700 -0. 0008600 Calcium 317 .95 Chromium 267.71 Cobalt 228. 61 0.0000460 0. 0001910 Copper 324.75 -0. 0002100 Iron 259.94 -0. 0004300 Lead 220. 35 0. 0007800 0. 0001050 0. 0005090 Magnesium 279.08 Manganese 257.61 -0. 0000500 Mercury Nickel 588.99 Potassium 766.50 Selenium 196. 03 -0. 0021700 Silver 328.06 -0.0005000 Sodium 588.99 Thallium 190.86 0. 0026620 -0. 0004200 Vanadium 292 .40 Zinc 213 .85 0.0005000 0. 0035220 Comment: 000004 FORM XI (PART 1) - IN 3/90 U.S. EPA - CLP 12 ICP LINEAR RANGE (QUARTERLY) Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 ICP ID Number: 61 Date: 07/01/92 Integ. Time Concentration Analyte (Sec. ) (ug/L) M Aluminum 5. 00 500000.0 P Antimony 5. 00 100000. 0 P Arsenic _ Barium 5. 00 50000.0 P Beryllium 5. 00 40000. 0 P Cadmium 5. 00 60000. 0 P Calcium 5.00 450000.0 P Chromium 5. 00 150000. 0 P Cobalt 5. 00 100000. 0 P Copper 5. 00 200000. 0 P Iron 5.00 200000.0 P Lead 5. 00 400000. 0 P Magnesium 5. 00 400000. 0 P Manganese 5. 00 60000. 0 P ' Mercury Nickel 5. 00 50000. 0 P Potassium 5. 00 300000. 0 P Selenium _ Silver 5. 00 50000. 0 P Sodium 5. 00 400000. 0 P Thallium _ ' Vanadium 5. 00 60000. 0 P Zinc 5. 00 100000. 0 P Comment: 0000044 FORM XII - IN 3/90 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Method: P EPA Sample Preparation Weight Volume No. Date (gram) (ml) 1 FB0724 08/05/92 loa LCSW 08/05/92 MWIDGW 08/05/92 MWISGW 08/05/92 MW2SGW 08/05/92 MW3SGW 08/05/92 MW6DGW 08/05/92 MW6DGWD 08/05/92 MW6DGWS 08/05/92 100 MW6SGW 08/05/92 MW7DGW 08/05/92 MW7SGW 08/05/92 PBW 08/05/92 PW-001 08/05/92 1 PW-002 08/05/92 PW-003 08/05/92 FORM XIII - IN 3/90 Gaaaa45 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Method: F EPA SampleSample Preparation Weight Volume No. Date (gram) (ml) FB0724 08/05/92 100 LCSW 08/05/92 MWIDGW 08/05/92 MWISGW 08/05/92 MW2SGW 08/05/92 MW3SGW 08/05/92 MW6DGW 08/05/92 MW6DGWD 08/05/92 MW6DGWS 08/05/92 MW6SGW 08/05/92 MW7DGW 08/05/92 MW7SGW 08/05/92 PBW 08/05/92 PW-001 08/05/92 PW-002 08/05/92 PW-003 08/05/92 FORM XIII - IN 3/90 U.S. EPA - CLP 13 PREPARATION LOG Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 ' Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Method: CV EPA Sample Preparation Weight Volume No. Date (gram) (ml) FB0724 08/12/92 100 MWIDGW 08/12/92 MWISGW 08/12/92 MW2SGW 08/12/92 MW3SGW 08/12/92 MW6DGW 08/12/92 MW6DGWD 08/12/92 MW6DGWS 08/12/92 MW6SGW 08/12/92 MW7DGW 08/12/92 MW7SGW 08/12/92 PBW 08/12/92 PW-001 08/12/92 PW-002 08/12/92 PW-003 08/12/92 1 1 1 i FORM XIII - IN 3/90 000007" U.S. EPA - CLP 13 PREPARATION LOG Lab Name: NYTEST ENVIRONMENTAL INC. Contract: 9219242 Lab Code: 10195 Case No. : 13425 SAS No. : SDG No. : SDG676 Method: AS 1 EPA Sample Preparation Weight Volume No. Date (gram) (ml) FB0724 08/03/92 MWIDGW 08/03/92 MWISGW 08/03/92 MW2SGW 08/03/92 MW3SGW 08/03/92 MW6DGW 08/03/92 MW6DGWD 08/03/92 MW6DGWS 08/03/92 MW6SGW 08/03/92 MW7DGW 08/03/92 MW7SGW 08/03/92 PBW 08/03/92 ' PW-001 08/03/92 PW-002 08/03/92 PW-003 08/03/92 1 FORM XIII - IN 3/90 0000048 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 61 Method: P Start Date: 08/11/92 End Date: 08/11/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 08:09 x X 1XIX X X X X X X X xjxj Ix X 1XIX x x ' STD 1 1 X X X X I Ix STD 2 1 X STD 3 1 1 X X X Ix X X X XIX X1 X X1 1XIX X STD 4 1 X X I X X X XIX X X X XIX X1 X X1 1XIX x x ICV 19 1 x I XIX xXxxxXIX x x I 1 11 xx ICV 7 1 X 1xi I I I I I X X X X ICB 1 X X X X X X X X X X xlxlxl X X X x X X CCV1 1 08:41 XX xXXXXXxxx x X1 IxX XX x CCB1 1 Ixx XxxxxXIX xx x X1 x XX XX CRII 1 Ix X1 X X X X XXX X X X X1 X X X X1 X x ICSAI 1 X I I X I x X I X ICSABI 1 X X X X X X X X X X X X X x X X ICSAI 5 ICSABI 5 PBW 1 X X x X x X X XIX x I x X XIX I X x x ' LCSW 1 X X X X X X X XIX X I X X XIX I X X X ZZZZZZ ZZZZZZ ZZZZZZ CCV2 1 09:39 X X x XIX X X X X X 1XIX X X1 Ix X 1XI CCB2 1 x X XIX X x X X X x jxjxj X X1 ix X 1XI ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV3 1 10:53 x XIX xxxXXX IxX x X1 XX X CCB3 1 X X x X X X X X x X Ix xi X X1 xjxj X MW2SGW 1 X X XIX X XXX X x X X1 x X1 XIX X MW3SGW 1 X X X x X x X X X x X X xjxj XIX X MW6SGW 1 ix X X XXX X X X X X X xjxj XIX x MW6DGW 1X X X X XIX X XIX X1 X X X X X X X 0 FORM XIV - IN 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 61 Method: P Start Date: 08/11/92 End Date: 08/11/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N MW6DGWD 1 XX 1XIXxxxxxxxxx x X1 IxX XX MW6DGWS 1 X X x X x X X X X x x x X x X Ix X X X MW6DGWL 5 X X x x x x x x x x x x x X x Ix X X X MW6DGWP 1 x X X X x x X x X x xlxlxl X X 1XIX X X PW-001 1 x x x x x xlxlxl x x xjxj X I X Ix x x x PW-002 1 x xxxxxXIX xxxx XX IxX IxX CCV4 1 11:44 x 1XIXxxxXIX xxxx XX IxX IxX CCB4 1 IxX xxxxxXIX xxxx XX IxX IxX PW-003 1 x X1 1XIXxxxXIX xxxx XIX Ixx x FB0724 1 x X1 1XIXxxxXIX xxxx XX 1XIX XX FB0724 1 x X1 jxjxjxxxXIX xxxx x 1XIX x MWISGW 1 X X1 1XIX X X XXX X x X x x X 1XIX X X MW7SGW 1 x X1 1XIXxxxXIX xxxx x X1 1XIX XX MWIDGW 1 X X 1XIX x x x XIX X X X x X X X X X X MWIDGW 1 XX 1XIXxxxxxxxxx XX x x CCV5 1 12:27 x xXIX xxxxxxxx x x x CCB5 1 X X X XIX x x X X X x xjxj X X x x 1XIX CRIF 1 1 Ix xlxlxl 1XIX X ICSAF 1 X I X I Ix X1 I ' ICSABF 1 X X X X XIX X X xjxj X I X ICSAF 5 ICSABF 5 CCV6 1 12:50 x X1 XIX X XIX XIX X xlxlxl X X XIX x x CCB6 1 x x x x x x x x x xlxlxl x XIX x FORM XIV - IN 0000050 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/10/92 End Date: 08/10/92 ANALYTES EPA D/F Time %R Sample A S A B BC C C C C F P M M H N R S A N T V Z C L B S A E D A R O U E B G N G I E G A L N N STD 0 1 08:15 x STD 1 1 X STD 2 1 X STD 3 1 x STD 4 1 x ICV 1 X ICB 1 X CRA 1 X CCV 1 1 09:00 X CCB1 1 X PBW 1 X PBWA 1 104.0 1XI LCSW 2 1XI LCSWA 2 96.0 1XI MW2SGW 1 X MW2SGWA 1 88.0 X MW3SGW 1 X MW3SGWA 1 86.0 X MW6SGW 1 X MW6SGWA 1 83.0 X CCV2 1 09:50 X CCB2 1 x ' MW6DGW 1 X MW6DGWA 1 85.0 X MW6DGWD 1 X MW6DGWD 1 87.0 X MW6DGWS 1 X PW-001 1 X PW-001A 1 89.0 X PW-002 1 X PW-002A 1 1 84.0 X CCV3 1 1 10:45 x FORM XIV - IN 0000051 3/90 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/10/92 End Date: 08/10/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N CCB3 1 x PW-003 1 x PW-003A 1 82.0 x FB0724 1 x FB0724A 1 95.0 x CCV4 1 11:30 x CCB4 1 X r i t 0000052 FORM XIV - IN 3/90 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/12/92 End Date: 08/12/92 ANALYTES EPA D/F Time %R ' Sample A S A B BC C C C C F P M M H N K S A N T V Z C L B S A E D A R O U IIEIB G N G I E G A L N N STD 0 1 08:00 x ' STD 1 1 X STD 2 1 X STD 3 1 X STD 4 1 X ICV 1 X ICB 1 X CRA 1 X CCV 1 1 08:30 X CCB1 1 X ' PBW 1 X PBWA 1 103.0 X LCSW 2 X LCSWA 2 105.0 X MWISGW 1 X MWISGWA 1 101.01 X ' MW7SGW 1 x MW7SGWA 1 96.0 x MWIDGW 1 X ' MWIDGWA 1 97.0 1xi CCV2 1 09:20 X CCB2 1 x MW7DGW 1 X MW7DGWA 1 90.0 X CCV3 1 10;20 X CCB3 1 X FORM XIV- IN 0000053 3/90 U.S. EPA - CLP 14 ■ ANALYSIS RUN LOG ■ Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/11/92 End Date: 08/11/92 ' ANALYTES EPA D/F Time %R ' Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 03:15 X STD 1 1 X STD 2 1 X STD 3 1 X 1 STD 4 1 X STD 5 1 X ICV 1 X ICB 1 X CRA 1 X CCV 1 1 04:00 X CCB1 1 X ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV2 1 05:00 X CCB2 1 I X1 I ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ' CCV3 1 05:45 X CCB3 1 X FORM XIV - IN 0000054 3/90 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 ' Instrument ID Number: 3030 Method: F Start Date: 08/11/92 End Date: 08/11/92 ' ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N PBW 1 x PBWA 1 100.0 x LCSW 2 X LCSWA 2 93.0 X MWISGW 1 x MWISGWA 1 104.0 X MWISGW 1 x MW7SGWA 1 110.0 X MWIDGW 1 x MWIDGWA 1 100.0 X CCV4 1 06:30 1 X CCB4 1 X MW7DGW 1 X MW7DGWA 1 113.0 X MW2SGW 1 X MW2SGWA 1 110.0 1 X ' MW3SGW 1 X MW3SGWA 1 110.0 X MW6SGW 1 X MW6SGWA 1 112.0 X MW6DGW 1 X ' MW6DGWA 1 117.0 Ix CCV5 1 07:15 X CCB5 1 X ' MW6DGWD 1 x MW6DGWD 1 103.01 x MW6DGWS 1 x PW-001 1 X PW-001A 1 106.0 X PW-002 1 X ' PW-002A 1 115.0 X PW-003 1 X FORM XIV - IN 0000055 3/90 U.S. EPA - CLP 14 ' ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/11/92 End Date: 08/11/92 ' ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N PW-003A 1 107.0 1 X ' CCV6 1 08:00 1 X1 I CCB6 1 X FB0724 1 X FB0724A 1 108.0 X ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ CCV7 1 08:45 X ' CCB7 1 x ' NPW-003A 107 CCV6 08:00 FORM XIV - IN 0 0 0 0 0 5 E 3/90 U.S. EPA - CLP 14 ' ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/11/92 End Date: 08/11/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 04:00 x ' STD 1 1 x STD 2 1 X STD 3 1 X STD 4 1 X STD 5 1 x ICV 1 1XI 1 ICB 1 X CRA 1 X CC V 1 1 05:00 x ' CCB1 1 x PBW 1 X PBWA 1 _ 90.0 X LCSW 2 j x LCSWA 2 83.0 X MWISGW 1 X ' MWISGWA 1 99.0 x MW7SGW 1 x MW7SGWA 1 101.0 X ' MWIDGW 1 X MWIDGWA 1 1 86.0 1 1 X CCV2 1 05:45 1 1 X ' CCB2 1 x MWIDGW 1 x MW7DGWA 1 104.0 X ' MW2SGW 1 x MW2SGWA 1 56.0 x MW3SGW 1 X MW3SGWA 1 93.0 x MW6SGW 1 x MW6SGWA 1 83.0 x ' MW6DGW 1 X FORM XIV - IN , 000057 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 ' Instrument ID Number: 3030 Method: F Start Date: 08/11/92 End Date: 08/11/92 ' ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N ' MW6DGWA 1 84.0 1 1XI CCV3 1 06:30 1 X CCB3 1 x MW6DGWD 1 X MW6DGWD 1 82.0 x ZZZZZZ 1 X ' MW6DGWS 1 1XI PW-001 1 1XI PW-001A 1 90.0 1XI ' PW-002 1 1XI PW-002A 1 76.0 1XI PW-003 1 x t PW-003A 1 78.0 x CCV4 1 07:15 X CCB4 1 X ' FB0724 1 x FBO724A 1 69.0 x ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ' CCV5 1 08:00 1XI CCB5 1 x 0000058 FORM XIV - IN 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 ' Instrument ID Number: 3030 Method: F ' Start Date: 08/12/92 End Date: 08/12/92 ANALYTES ' EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N ' STD 0 1 05:00 X STD 1 1 X STD 2 1 X ' STD 3 1 X STD 4 1 X ICV 1 1XI ' ICB 1 1 x CRA 1 x CCV 1 1 06:00 X CCB1 1 x ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV2 1 06:45 X ' CCB2 1 X ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ CCV3 1 07:30 X CCB3 1 X ZZZZZZ FORM XIV -IN 0000059 3/90 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 ' Instrument ID Number: 3030 Method: F Start Date: 08/12/92 End Date: 08/12/92 ' ANALYTES EPA D/F Time %R ' Sample AS A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ' zzzzz ZZZC1 08:15 1 1 1 X ' CCB4 1 IX ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ CCV5 1 09:00 x ' CCB5 1 X ZZZZZZ ZZZZZZ ' ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ FORM XIV - IN 0000060 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 ' Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 ' Instrument ID Number: 3030 Method: F Start Date: 08/12/92 End Date: 08/12/92 ANALYTES EPA DIF Time 11R Sample A S A B B C C CC C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N II ' CCV6 1 09:45 X CCB6 1 X ZZZZZZ ZZZZZZ ZZZZZZ CCV7 1 10:15 1 1 X1 I CCB7 1 X1 I PBW 1 X PBWA 1 90.0 X LCSW 2 ix LCSWA 2 50.0 x MWISGW 1 X ' MWISGWA 1 104.0 x x MW7SGW 1 MWISGWA 1 110.0 X MWIDGW 1 x MWIDGWA 1 104.0 X CCV8 1 11:00 X CCB8 1 X MW7DGW 1 x MWIDGWA 1 100.0 X ' MW2SGW 1 X MW2SGWA 1 100.0 x MW3SGW 1 X MW3SGWA 1 100.0 x MW6SGW 1 X1 I MW6SGWA 1 104.0 X1 I ' MW6DGW 1 I I x MW6DGWA 1 99.0 X CCV9 1 11:45 x CCB9 1 x MW6DGWDj 1 x 0000061 FORM XIV - IN 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 3030 Method: F Start Date: 08/12/92 End Date: 08/12/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N MW6DGWD 1 98.0 x MW6DGWS 1 x PW-001 1 x PW-001A 1 106.0 x PW-002 1 x PW-002A 1 111.0 X PW-003 1 x PW-003A 1 109.0 x CCV10 1 12:30 x CCB 10 1 X FB0724 1 x FB0724A 1 116.0 x CCV11 1 01:15 x CCBII 1 x 0000062 FORM XIV - IN 3/90 U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 100 Method: CV Start Date: 08/13/92 End Date: 08/13/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 08:38 x STD 1 1 X STD 2 1 X STD 3 1 X STD 4 1 X STD 5 1 X ICV 1 X ICB 1 X CCV 1 1 08:43 X CCB1 1 x ZZZZZZ ZZZZZZ PBW 1 X ZZZZZZ MW2SGW 1 X 1 MW3SGW 1 X MW6DGW 1 X MW6DGWD 1 X MW6DGWS 1 x CCV2 1 09:12 x CCB2 1 1 1 1XI PW-001 1 1 1XI PW-002 1 I 1XI PW-003 1 I 1XI FB0724 1 I 1XI MWISGW 1 I 1XI MW7SGW 1 I 1XI MW7DGW 1 I 1XI ZZZZZZ ZZZZZZ CCV3 1 09:39 x CCB3 1 # I I 9XI FORM XIV -IN 0000063' 3/90 U.S. EPA - CLP 14 1 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 100 Method: CV Start Date: 08/13/92 End Date: 08/13/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 12:17 x STD 1 1 X STD 2 1 X STD 3 1 X STD 4 1 x STD 5 1 X ICV 1 X ICB 1 x CCV 1 1 12:22 X CCB1 1 X ZZZZZZ ZZZZZZ CCV2 1 12:34 x CCB2 1 x ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ 1 CCV3 1 13:01 X CCB3 1 I X ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ PP�w i x FORM XIV - IN 0000064 3/90 U.S. EPA - CLP 14 I ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 100 Method: CV Start Date: 08/13/92 End Date: 08/13/92 ANALYTES EPA D/F Time 11R Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I IE G A L N N ZZZZZZ ZZZZZZ ZZZZZZ zC ZZ 1 13:33 x zzz1 x ZZZZZZ ZZZZZZ ZZZZZZ zC ZZ 1 13:51 x zzz1 x ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ FB0724 1 x ZZZZZZ ZZZZZZ CCV6 1 14:14 x CCB6 1 x r FORM XIV - IN 0000065 3/90 U.S.. EPA - CLP 14 ' ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 200 Method: AS Start Date: 08/05/92 End Date: 08/05/92 ANALYTES EPA D/F Time 116 Sample A S A B B C C C C C F P M M H N K S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N STD 0 1 11:00 X STD 1 1 X STD 2 1 X STD 3 1 X STD 4 1 X STD 5 1 x 1 ICV 1 X ICB I X CCV1 1 11:24 x CCB1 1 X ZZZZZZ ZZZZZZ ZZZZZZ ZZZZZZ PBW 1 X MWISGW 1 X MWISGW 1 x MWIDGW 1 X MW7DGW 1 X CCV2 1 11:57 X CCB2 1 X ZZZZZZ MW2SGW 1 x MW3SGW 1 X MW6SGW 1 X MW6DGW 1 X MW6DGWD 1 X MW6DGWS 1 x ZZZZZZ PW-001 1 X CCV3 1 12:33 x CCB3 1 x FORM XIV - IN 000006G 3/90 i U.S. EPA - CLP 14 ANALYSIS RUN LOG Lab Name: Nytest Environmental Inc. Contract: 9219242 Lab Code: 10195 Case No.: 13412 SAS No.: SDG No.: 676 Instrument ID Number: 200 Method: AS Start Date: 08/05/92 End Date: 08/05/92 ANALYTES EPA D/F Time %R Sample A S A B B C C C C C F P M M H N R S A N T V Z C L B S A E D A R 0 U E B G N G I E G A L N N ZZZZZZ PW-002 1 X PW-003 1 X FB0724 1 X ZZZZZZ ZZZZZZ i Z ZZZZZZZZZZZ ZZZZZZ CCV4 1 01:09 X CCB4 1XI t FORM XIV - IN 0000067 3/90 27 Profile 'im : Cu 3£i:?54 Peak Pars-ition : -.246132 Peak Intericsibi: 2-7,01`5 i Peak Width 9.59265 New Spec, SM14,, at fi, i -3i 3 RpectFim 'hifter Position 0000068 ' Tue 08-11-92 08:09:57 AM page 2 Mth«d: CLFB Ste:Jdard: IVBLK E 3 em FL SES AS BF: BE CI; CA c,.ge .0074 -.C"'Or is -.001--e :lfAl J .ortiJ i .0C)OC i ,00,6H Siev .0014 .000.3 . /1003 WOO! .ri00 :011 .ijr)C)�' %RSi7 19. ii 2i i 142 u 7.443 jc)rjri =r}, r,r]r1iJ #1 :00 at` -.0004 _.0040 of).r)ijd6 -tlJ{ rj .UL?.00-66#2 0064 ,0000C;0 i ij3,08 Lir'+%1S OC170 E 1 e:r) CR CO CU FE F'S Mr M P. ge i-�> ^ t`) .Oi'1s_ `S GDev 00,04 f)tif:-7 .00,03 .C) ,,Osj0iA- 01000 %F;SD 3 C2.6L, CSC. . 22..= 1--.63 vC cl.� 1411 _.4 ,;iit pr, #1 io I=_ .C�il'.!C .f)t)t,�j' .i j:i�� ,i lid C1� .00 2 .fl%t-I C. "i.:3.) ' 1oryi� is - 5E r[ P3.i TL - ..,�y_ 00'.)6 .:.�. ... .001 0 S Ie•: .00114:i 114 ,G ).32 ,C-x 42 r.O 13 1 ;;RSD 2351.'/ 141 .4 7.928 4 '.92 #i -.10016 .-)196 .00,6 C} .C-002 f)f)!�f .�)+j22 I .000") #C ��t)l?4 .e11 Jai E2em tY B2496 Pvge >Ct 9 .C)15? S'Dev .0010 . :0r)1 %R*SB 52.1 r) #1 -i1Ci26 .r)15S #2 C-0I E .0156 --------------------------------------------------------------------------- Method: C;-PB Standard: IV4 E i est) AL CA FE MLS NA - ti`Jge .5401 17.44 �.S •.x.r).o1 .85 �.603 SBev .001-3 .1:i .043 .051 .()06 /RSr .2357 .5645 .4421 .5948 .2173 #1 .5392 17.37 9.790 .2524 2.597 #2 .54I0 17.51 rI -.J- .5596 2.607 ----------------------------------------------- "Method: CLPB Standard: IV2 Elem SB Hvge .51 r)i Siev .-)l i7 %RSB .1356 #1 .5106 - -------- - 0,9 -------------------------------------------------------- 0000069 : Method: CLPB Standard: IV3 Eleni At S' BA BE CD CR CO cu Avse 2.633 .4312 .8i65 1.31E i.849 1.460 6436 SDe. . 03 .0014 sx 214 .0024 .009 .0i 1 .009 .0023 '.:RS-D .10,78 _3`IS0 _?q44 _6546 .58:2 .35 16 #1 2.835 .4302 .814E 1.3:2 1.612 1.4.=i4 .6420 #2 2.8 1 .4JG2 .eL 1 .32Y 1 .4C6 .645-0 E1e1* P2 MN r�}: k.� T! Ave 1 .4Q6 2.714 1.,}'/5 1 .620 .774l .3 SBev ,009 ,i:I L: .009 L?CF6 .I% 7^ .00 35 a .t1x:9 %..:;:SD .6240 .5002 .es 1., _3�cr j4. 1.nnc; .9.15 .E yto7 4i 1.489 _.7x;5 1.068 1.616 .7686 .3$54 ; .116 #2 1 .502 2.724 24 .77?6 .3gC;t . .122 Elem V ZN Av:;e 2.151 2-4," sDev .010 O t e RSD .4667 #i 2. 11-4 2.391 -'ri.2 2 159 2.41 Me hod.- CLPR Standard! IVj E l esr: B_2496 Avue 49-70 %RSD . 1 i 38 #1 .496, #2 .4974 -------------------------------------------------------------------------- Method: CLPE �r- Element Wavelen Nigh std Low std Slope Y-ir: ero= ta-d -ed Date jt�:�d , i_ AL 3.13.215 IV4 IBL---' 11.2634 -.i0iE3 434? C}8:`i 1:92 rI 16:22 s 206.838 I V2 I VBLK 19.J�t63 .00 1919 06,111192 Cie:16:22 A5 17-3.` 6 6 I V3 I VFit K 1.D5,t61 ;f i26. .3 I 1/Y2 08:16:22 BA 493.4.=9 IV3 I VBJ_K 13.914? 00ij , 00 08/1:/92 08:16:22 BE _13.x:,42 IVs I VELE" 2.4515E -.00-1716 nq/11/92 x32:16:22 CD 228.8'02 IV3 IVE?LK 4.55270 C!()0 000 08,111/92 08:16:22 CA 317.933 i V4 I VERU*; 2.86858 -.019506 09/11/92 2. 16:2c CR 267.716 IV3 IVELK 3.24658 -.004221 08/11/92 08:16:22 CO 22$.616 IV3 IVBLK 4, 11072 -,001233 3/1 L 2 rte.:16:^22 f'i-, t '4� f'Q � CU 324.752+ I V3 I i1BLK 9.33707 -.009337 081' 1/QP 04:16:22 FE 259.940 IV4 IVBLK 2.54710 -.x,14773 r;aj11/92 OP: RB 220.353 IV3 I VELK 13.387£ -.025437 Oe/11/92 09:16:22 MG 279,079 IV4 I ilRL : 17.5561 ..124573 i.E/i 1/e- . C1E:1b:22 MN 257.610 tir l V 3 I VBLr: 1.47372 i;i s:ii 00 Oe/11/92 t►d:16:22 iiI 231.604 Jim IVBL : 5.579$4 ,003?/,S e/I1j92 Cf8: 16:21= 0000070 - Element Wavelen High star Low =td Slope Y-intercept Date Standardized K 766.491 IV3 IVrLK 249.553 -4.31744 06/11/92 08:16:22 SE 196.026 1 ;3 IVOLK 12.9685 -.038905 (8/11/92 08:16:22 AG 328.068 IV3 IVBLK 15.4719 -.001547 08/11/92 08:16:22 NA 524.975 T_V4 IVBLK 21.5864 -1.19373 08/11/92 08:16:22 TL 190.864 IV3 I:?FLS: 17.9163 -.102123 08/11/92 08:16:22 V 292.402 IV3 IVBLK 2.79044 .003628 08/11/92 08:16:22 213.855 I Vim' IVBLL-: -.0047746 2.49313 .Cts i4 7 46 6/11/92 06:16:22 8-2496 249.678 IV1 IVt!_K 20.7771 -.226200 06/11/92 08:16:22 -------------------------------------------------------------------- Methcar: CLPB Sar: le Name: Ii V I Operator:: TC-'MF P Run Time: ;8/11:92 08: 19.,55 Comment: ICS: _ C;C-7 ?`lade: CONC Corr. Factor. 1 n E1ei% ".L .�.� A Pt E,E,E CD CY } tc �rna•r n r m U�� Pr rr r. .: pp pp. pp1*, pp, .c?69e .013' 2 ev so _>Civ !;;"r t:i %R6211-2;SID . 1�' .=4 34.9? s u;; i,; 0 0 424 .36--514 #i .9641 .rJr�.1`-. .C}I?? 1 .+135 .0002 -.CU'8 .i i t 7 42 ,975=+ .027E .01 i 7 i .035 ,r s,;r}2 .0-0-06 .1113 E.rC='-S �'C �'a�= fi`:`v��?fil rI NOCHECK' s s NO-CHECK SCC! Eck: N'Oc�E:CK Va-Iue 1.00) 1.000 Range 10.00 101 Of) E`e:m >,:.�R C0 Cu FE P8 ME MN }r!3 LS rtm �;.j 'r.m T. r{ m n rr-r Pr ` P rr° FF PP- FF rF ! lq .00ye r;i3 :jiifJ .f 13 EDev .t?r:i:} ,r;_" .�j+.-5.3 .Q,--� .0133 .fuj7i. .r�r:;rj2 %RSL, 42.43 565. 7 282.8 4.569 22,01 424.3 15.71 #1 .f}0420 }Ci . i:jia ,r�lt.v� -.r}�5� .��3� .��+ 1 -•-�Y -.:.) i - •t +cam - -.rte 1a #2 ,00.23 X.12 .(W 6 .0068 070 .00_2 Errors P OC!-ECK NOCHECK NOCHECK NOCHECK' NOCHECK SNOCHECK NOCHEL- Val::e Range E1e:,;r NI K SE FG3 NA TL V Units FPm PF? ppm ppm Fpm ppm ppm Avge .00117 31.52 t=363 077 10.92 .0753 .001.1 SDev .Q i I IS .42 02194 Oili .09 .01431 .0004 %.RSD 707.1 1.344 e().B6 1.1}16 .783+ 57.21 35.36 #1 -.;}1, _} 1�1; _ri155 1 .069 10.58 .0449 -.{iC}14 #2 .'_}0167 31.82 7 0570 1.085 10}.86 .1058 -.0 }��1 j Errors NOCHECW OC Pass NOCHECK CC Pass CSC Pass NOCHECK NOCHECK Value 30.0:} 1.0010 10 11.1:::: Range 10.00 10.00 Elem ZN B2496 L' is PPm ppm Avge .j�065 .9121 0000071 : SLIev .CO i 1 .01166 %RSD 16.31 1.23+3 #1 .00172 .4`'i 4 #2 .0057 .9038 Error=- NCCHECK NGCHECk; Valate Range Method: C!PE Sample Name: I'VI Operator: TCS' Run T isle: IS!11192 08:22:41 C�:rment: IC:- Cv.-`9 Mode: CONC Corr. FaCto:: 1 E1em AC SB AS B-A B_ C LA {.illi +Fc nr �; r "" r.-.� m PFI Fr F rr° rt- Fp pF`•"' Avge -.0220 i,0222} 1.1047 1 083 .`ui28 1.- 33 1 Csi8 24.74 4 ..,4 SDev. 0111 . 1 r}t: ;r.'-1r;r; ;�;;: cFr}c r %RSL 50.71 .1 -�+1 1.176 .369' .2530 . .091 1 =:(}CR : . "�7 ? .V9 -CS 1 .it�i 1.ij2.i ly. titZ .69 #L 0141 1 .047 1.074 .002,3 1.0'35 1.0116 24 131 C 2,s N u r 1. �- s � Errors NOD4ECl�� opas= L Fd_ 1 � � 1' tr F'�cs CC. C.': G.. as- �� Pass �� Pass v".rl i .(ffii: i .G�'�' 1.00f, 26.::: Range 10:.:11? ii ..% 1ri.rIf3 16.of-I 1(,.1;11 E l em C; CU FE P8 Mc MN Cl-1,t s pm rpm pp"--l ppm 01;1 FF' pYT Avge 1.0216 1,032 X32 1.:12 .9745 .9566 .9461 1.0361 T1o.l .:.212.21 ,00170i 1'� t17: .007',6 ..}!12_5 ,ij61� %RSD .4474 6155 .2609 .c?a; .7678 .2624 A(A5 #1 1 .023 1 .027 i.01;.1 .9730 .;1?19 =9475 1 .02-1 #2 1.:129 1.0 37 1.(--114 .976:% .98-12 94-43 1.033 Er:ars CC Pass OC Pass CC- Pass CC Pass CC Pass CC Pass CC Pass Value 1 .0010 1.iv n 1.000 i.000 1.C:i 0i 1.0010 1.{iy, Range 1x'.00 10.00 Iila.00 10.00 10.0ii 1i,--I Elem Ni K: 5E A3 NA -C v Units FpT -�; �m Pp1'� PnIn p ppm m Fp- FP Avg e 1.043 -.0250 .9230 -.0093 .i 112,0 I . 186 i.004 SDev .013 .3529 .011715 .f:Oc_ .0061 .056 .r 01, %RSD 1 .210 1414. 7.276 23.57 12.31 5.133 .3537 41 1"035 -.27=:5 .9324 =:OCC 7 � 1:047 1 .rj;j 1 #2 1.05 1 2 .2246 1.034 �= t}8 04`x6 611 125 1.007 Errors CC Pass NOCHECK CC Pass NOCHECK NOCHECK OC Pass OC Fuss Value I.rs00 i.000 I_01063 i .0063 F°a:-)ge 121.00 iC;,i�i} i w�.,1�> 10.C)Cl Eiem -2N B_2496 UT-1itppm ppm 0000072 I .029 _C)0 SDev .001 01 _0059 %RSD .1375 6.656 1 1 .026 .01?25 #2 1 .030 .0842 E: ro-s CC Pass NOCHEC K Value 1..+00 Range IJ1 ,-)O Method: CLPB Sample Name: IC61 Ctce a.t4i : TC" Run T:me: 08/11/92 03:26:06 Comment: (-ICS Mode: CONC CDrr. Fac tc F: 1 E I em YLgr: as F'f% B.- A Units s Of'. ppe, PPIT, nnfr; Pr•f* Lp it ^.vge ;csc 6, 0 Cj)e.; .'-J'E!' .<'= <} .r)1'."1 .iT;li�i� .tiilCiv .'JL)1 .vr�� 'r.RSD 23.5.6 330.Ci 353.6 .00-00 ti .71 7 E).68 14,14 41 .;i02.. 196 - 0:142 ;j 0; - -riq #2 -.01090 .X}72 .00!Q9 .C11010 .ii(ir)7 .0027 .021Ci7 Errors LC Pas_ LC Pass NOCHFCK LC Pass LC Pass LC Pass LC Pass Low -.2000 -.CIA i)G -.20'0 EIe:T: CR CC. C1 FE �' u MINA +;ni.� ppr ppm rim pp:r. Ypi1 F=�'; PYm fav e -.0-}26 .0016 --On.1:f% :CiC'+ii} -.i r _ 0 6,i T1'3 1.17 .ii 34 .0.,09 =_I)A V .:} «� `li li};± �}{�26 .� C i.^R_C^t4 .J 1:x'� i:fii: UnitesF-m �m r Fr P.vge .00ci ) .G145 SDev .0ryr i3 .0054 Y.RSD 304e6 401 36 ' i .Q C,0.3 :0187 #2 0003 f,1 C}4 ' Error=_ LC Pass CrCCHEC.. Luft -.C)ct)C ------ ----- ---------------------- Method: CLF'SSa:a;:le Nair-'e: CL;IjC e}-9}G ----- TCM Run Time: e/11!42 08:41 :09 Comment: CCV Made: CONC C_+r)-. Facto-: 1 E1eal: AL SB AS BY BE CD L r f-vge 3.C:7 2 4.496 I0.GO 3.n c, .?c`a.`s 0. X4.4� SUev .022 .r i 1 .01 .r p 12 " _ %GSD .73223 3?,? 1,58; 4 324 .44 4792 1 3.056 4.^23 .4rr7i .47 c4.85 #2 3.C:29 5.011 i0.010 3.014 1.002 3.C}j7 255.02 Err_.-s GC Pass CC Pass QC F'a=-a 4C Pass zC Pass Cr Pass Or Pass tie 1 tte 3.rtC;r. 5.r:r;r) 10,Q0 3.OfU0 1"000 v 25. Fartge 1'3.t1:1 IC ,riri 1C).(":;_t 10.rtr i;a.t;ri V .C,�, 1C}.r, E' CF. s^C, CU PE F3 11413 FiC Units Fpmpp^ P, FFm Fpr. FFA Fpm Av-e 2.492 2.97-3 3 0151c.44 9.412 ?.556 1.484 SO?ev .013 .rtt2 .01 ' .rJ7 6 .037 .rJ11 :=.t=:SD .6 105 .4193 .5540 .58 17 .0562 _4f?7c .5433 #1 2.474 2.9wL 3.0,04 1c.39 4'.416 53�i 1.4". J..t 005; ` c.A? 3,027 j-,40 Q 4C,4 C. . ,58 2 1 .442 Errors QC Pas CC Pas=_ for pass oar. pass - 'aim F'�-- '�cc .. L F,..._ CC Pass CC F_._.. Value 3.000 ,C72.00 , Range 10.00 1r;,ri0 10. 0 10 t: 1v.r;(} E?em M1 K SE y8 NA TL 'v Units FFm Fp:r. Fpm - Fpm FFm FFm Pvge 2.?72 t 1.4 5 037 3,f-WIC) 27.6': 10.46 3..iU{ --' � SDev .036 1 .6 .25 0,11 C,. %RSD 1.221 .8654 .4962' .3624 1.065 .4707 .8413 ?i,1-1.6 5.014 .pcC= 2 7.40 1n.L. a.GS7 42 2.448 2C:3.1 5.054 3.008 27.82 1 C).5C. 3.023 Errors_ CC Pass CC Pass CC Pass CC Foss Cr Pass_ CC PassF Fa s= r ss Value 3.c.O0 200.0 C)()E} 3.004-1 -27 50 10.00 v.r..0c Range 10.00 1'ri.CV) j;,.0t, 'tC,.t)cl 10,00 1!=.00 1'0.:1x1 0000074 1 Err+ ZN 3 2496 U,-I FPM PFM Avge 2.99e 4.977 SDev n. 1 0,1- %RSD _3778 .2643 #1 2.990 4.g6o #2 3.r?�J6 4.996 Errors QC Pass NICCHBCV Value 3.;0.0 Range 1i: .(?0 --------------------------------------------------•----------------------- Method: CLP6 Sample Name: CCB-1 Operate•:-: TCN :urs Time: 0611-1/92 %'e:--:23 Comment: CCTB ?ode: „ut Co 1 Eley' AL S$ AS EA Units F?fq F0M FFM tpm PF"' rpm Y f >J "000 .;3188 ST}Cv .01 2 E 5 .i'1L1 192 j014 00 00 .00138 %RSD 166.9 130e.98 7?.42 47.14 .%f0o.) 424.1 2S.19 1 ##i .tJ:==9L -. =Ji i` :010Is .0Q i :v'�}C)2 �0l• 6 ,{?2 23 #2 .0*24 r�424 0376 .C:+C?c7 0002 _iy<,,L �t.D1 . Errc:re LC Vass LC Pass i'aOCHECK LC Pass LC Pass LC Pass LC Vass High _2`w J, �v600 .2c,00, .CiCY5�3 Low .2000 .i`:6ftfi .C;I;iEJ E 1 ear cp CJs CU FE L; MG Unite PFm FP" PP:r: Fpr': PPm FFFFT Avge ,0005 .003 -.0021 .0052 -.041,0 .tjiO3 .0012 L3eV .003s .C"Cj3L (jilyii") ijiJ1C .0019 jt�13? fji)Cly '%RSD 618.1 95.09 _.J0.00 35.28 16.78 .2 i.9 000-01 #1 -,0017 ,0012 -.rQ21 .r,t3v5 -.UC,17 C.i-' CJJic #2 .0.027 .01G!6Cs -.s,s=21 .uu3Z9 -.,j123 .022)1 .0 0 , + 12 Errors s LC Pass LC Pass LC Paas L PC-.=-E LL Pass LC Pass LC F'asc- if'yh �Cl.iCIO �i;�: C; = i �i=+f. �0000 b5: Low Y . J G 0 ?f4S3 -_ `l( -.015 Elem .J NI E SE AS NA TL v Units PPM PFm PPM PFrr Fpr" PPS' FPM Avge .0055 -.7265 .0161 -.nrj1� .Cj7C2 .111f36 -.0014 SDev ,CJCrg3 .4118 ,C1412 .CIO 67 .0671 .0221 .+0i 0 /,R'S D 1 7.5 56.67 227.4 5b2.2 85.$! b05.9JJ-0 #1 -.0010 -1.sf1S .0473 .CDC)4.6 .0,307 .019S -.0014 1#2 .0121 -.4354 -.0i1Ci -.0077 .1256 -.0 2r. - E"C+14 Errors LC Pass LC Pass NOCHECK LC Pass LC Pass NOCHEC ; LC Pass High .C9400 5.00 .0100 5.0-DO .0500 Law -.0400 -5.000 -.0i00, -5.000 -.G5 0;1-1 0000075 i EIem 2N B-2496 Uni is Fpm pprr. Avge .00;,18 .02-10 SLQv .CIO IOl .0000 %RSD 123.8 .01513 #1 .00"16 . X21 0 #2 . 1001 .0210 Errors LC Pass NOC!-ECi_ High r ! Low Cw -----------t--- --- -------------------------------------------------------- NatiQ CLPF S.?mrliz Name. LRT7Operator TCM Faun Time: 1'0/11!'=2 08:45'49 mode: CONC Corr. Fac rc.r: 1 r E1nT: AL `.L! AS S Fid CD CA pp p0 -r pp F• r}- r Avc e .C40-98 . 168-1 .02 %3 CIC 127 - -.0-42R 0107 .0112 01 4 28 `ria;. 011[1 0-,+03 .'.eOIQ 2n,Q ,01016 ".RISD 326.0 11 38 i 98.C1 7[0.71 3.143 16.96 12.86 #I -.0331 . 1SIc -.0485 -.Of-.41 .01;34 .i)c1gq -.0139 #f2 .{ I35 .054625 -,0116 Errors LC F3ss LC Pass NOCHECV LC F_ass LC Pass LC Pass LC Pass 5i:,00 Low -.`i`3iIP} -.:16---0 -.2l:ilam} -.005(} Elem CR co C;! FE P8 i'l8 MN Chit s ppm ppf" ppm p p r. pp:"p ppm ppn ' A./ a :iEi?3 '1L'U14 000-:1 S -.0052 -i 271 -:n149 .(.305 SD'evf ;`.007 �1� Lt0 0013 :!(_119/ i l�l00 ri iQ, i jOi`O r.RSD 5.143 3.11=. 2.4$1 35.61-1 .0026 123.7 .0000 1 r 016 7 .09SC ,0'=;n9' -.OCi65 .1271 -.0271 .03051 #2 .i1I8t: .1(42 .23527 -.0039 . 1271 -.C1;t_9 .C%3C15 Errors LC Pass LC Pass LC Pa LC Pass LC Pass 1 Pass LC Pass H i g 1 00 200-i2C0.0 400.C 41[ .j 6Cs Low -.0100 -. %500 -.0250C; -5.;:Dnr1 -.`1I ilI Elem NI 1, SE A8 NIA TL U Units ppm pp,=: pp,- pp,r. pp� pp, ppir Avge .C 401 .50:095 .0241 .0215 -.05,Q7 .0502 .1050 I C 88 3� j! 43SDev _C .00,32 .O.0.8 .00-0 7 /.RSC, L1.1-4 168.4 172.6 20.20 5.43^ 19.E55 .0004) #1 :0?72 -:rl ?I -.0063 .0135 =-1-610 .ti- . 1050 -2 0 1 [1 830 116 . 545 .02-46 0565 .0433 .1[15{.3 ErroTs LC Pas=_ LC Pass NOCHECK LC Pass LC Pass NOCHECE: LC Pass 00000 '76 Low -.0 400 -5.000 -.J 1()ra -5.000 -.0500 Elem ZN 8_2496 Units Pott: PPM P.vge .+0338 -.+"0r" 0 Sne.: .0017 .0��Or i %RS9L` 4.=;I S 2K.7 #1 .0;3?6 -00001, #2 .0400 0000 ; ' Errors LC Fuss NQCHECK High 100.0 Low -.:7200 --------------------------------------------------------- P!ethed: CL PE Sa 0r1L Name-: ICS4r QL_-a}oTCM Run Time: Oe/11i92' 03:5:6:34 Co rp.mei t t: EPA; F:c= MATERIA_ PaRT M.Ae: CONC Corr Facto:.- 1 E l eim A. SB AS 2 $c CD Ci Ur:i is PP,� PP ppmPPPFP,�O Opal PPM r,vt�e 5LY.2 . 15 7 2.6:05 .r;C,6P_ 0002 .0.i16 L71 .4 EDev ! .0 .027S .033 .iloi.o ._'C0t'3 1 './.RSD .1344 17.7C,, 1.285 .fuvr 0%: 1-41.4 20.20 .Ic13 #1 5j.. .9. 154` C: X81 .�i0i r.ri ,� -.iJ'7� L71 .9 #2 543.5 .17300 2.623 .0;68 .7t0,CI -.0134 1.7.0.9 Error_ LC- Fas s COCHECK NOC:,EZ",: 1`!C}...:._ sC..•:-EEK' CC Pass Value 540.1 4914.1', Range 20.00 ari.0r; Elem CR CC. Cu FE FF MG M=•! ' Unit=_ FF:r PPT PFT PF,lo PPT PF" PPM Avge o0rgI 0032 0,291 187.8 .4744 497.0 .0233 SOJer,:053 .0000 .0064 .4 .<<168 .:S '/>RJiO 58.52 t 1 v6 16.44 .2299 3.401 .1593 .7179 #- .'�i 2•: .0030 -.:i; - 18-9. 1 Q-25 ..,N 02,85 �, 2 , ; 5 �: .. .r;i.s.4 ,�:iO3c -.�0-'..b f�?.., ._:•f¢,•? 49 .4 .t0282 Errors NQCHEC k: NQCNECK NOCHECK GIC F•as=_ NQC':HEC' CC Pass NQCHECK ala 1 j 2+-16.2 531.4 Ran..ge 2rI -.r trj 2r,_f;r s Elem P;I K SE Fs8 t-A TL v Uni }= m PPM -. m m r tr nm nrn PF=•• r FP rP rP Fr rr+ Avge .009e .6551 2971- -.()toe 1.5915 .2382 .006=-: S7ev .0093 .7e92 .0227 .t0022, .0089 .rJr328 %RSD 94.23 120.5 7.643 20.20 5,633 65.11 43.CA #1 .:1164 -.0971 -.2830 23 1.651 .3478 .r0•:gc. #2 .00133 -1.213 -.3131 -.0 092 1.525 .1285 .U 045 Error=_ NOCHECt: NQCHECK NCOCHECK MOCHECK NQCHECK NQCHECh: NQCHECK j 0000077 . i value F-an Eleni ?1,14 B2496 Uni is PPjr 11 Avgc ;?016-8 .r�114 SDev ��:,455 00015 %RSD. 2.158 4.42' #i .2099 .0 i I'-D #2 .2036 .0liS Errors NOCHECK INOC iECi<: Value F;ange -------------------------------------------------------------------------- ?iat`,cd: .LPA Saap?z fl-m.re: lCSaHT CPe-ator: TCM Run T i me: 02/11/921 00-010,-01 �� Comment: (EPA (;REF MATERIAL F-ILPT a 1-A.R S Mode: CONC Curr. F-.rtsr: i E l e AL SF! GS D{; 8E CD CA.. Units PpT Ppm, ppf' PPT PP'Tl P11 r=pT Avge 514.6 .1646- 2.551 .43%5 .4731 .9031y 444. : SDev - . 4.0 .'0305 .01? .OriSS ;0030 :C)n- 3.3 %R'S;1 7717 16.50 4548 1.185 6'386 4159 75 Of 6 #1 511 .o : 1431 2.543 :a 8 5 4 .4;09 :50 441 .S #2 517.E 1861 2.560; 4936 .4752 .966-1 446-.5 Ewe=rs C- O ss NOC! C E . CC CC Pass - �= E E: id�J1:.H��.�!�° Pa=_ CC Pass CC Pass ' Value 536.5 .5ii2:,1 .4800 .9070 512.2 Rarge pri r`-? 2J.C;r; 20.00 20,in 20_00 E 1 elm CR CF's CU FE PB Me MIN Unit=_ Ppm RPT PPT pp"' PPT PPT PPT Avge .4920 .446-4 .4589 177.5 4.971 467.2 .484:4 SDev 0027 iirll 1 0039 - 1 .5 r,a8 - 4.3 i UY39 %PSD 5367 2537 6401 8535 1 ?65 91r '%985 #1 .496-1 .4456- .456-1 176-.4 x.902 464.2 .48.12 #2 .4999 .4472 .4616- 178.6 5.040 47;7.2- .4868 Errors CC Pass CC Pass CC Pass CC Pa=s CC Pass_ CC Pass CC P2=5 Value .5290 .4770 .54317 199.8 4.724 527.5 .4960 Range E0.00 20 00 20-00 20.00 20.00 20).'00 2i r"r, E 1 em WE k: SE A<3 NA T! V Units Perr pPIT. pR'T Pp+" Ppm PPT PP's Avge .8777 .6794 .2924 .9657 1.487 .1645 .49001 SDev .1,11216 .1373 0=;-:,C) .)ne-, .329 .�-!762 %RSD 2.463 20.2i- 19.47 .9008 1.934 46.301 1.451 #1 .8624 -.7764 -.3333 .95?5 1.466 . 1105 .465r.D #2 .£930 -.5823 -_2526 .4718 1 .5~17 .21,84 .49501 0000078 i Error=_ CC Pass NOCHECK NOCHECKCCPass NOCHECK NOCHECK CC Pass 1 Value `9400 .9600 .519:s Range rry ()0 20.00 -00.00 ' E 1 eve 7,1 R_2496 u=nits PF°"? PPm Avge 1. 191 .0220 1 %PSD .8357 20.21 #1 1 . 184 .0189 #2 1 . 148 .Aa5r -. ;-rigs CC Pass NOCHE�Ct•. Value 1 .206 Range `yi itil -------------------------------------------------------------------------- MEthoC: CLF,B 5a:r.Ple Name: ICSLI CPe:ata:-: TCS? Run Time: 0.8/11;92 C19:r:�4:13 Co:,wrient: 1 :5 DIL Mode. CONC Corr. Factor. 1 E?em AL S8 AS 2n BE Cr CA rd'si is PPM PP's PPm FF`" FP^ FPm FPM =vge 117. 1 .�`6 � .5458 -.':C;14 .0000 -.04),18 107. . SDev l.c .C�i1U ,04;-- ,OOC-10 ,mix. .00,63 %RSD 1 .r,12 16.88 5.894 .`JC?:ji F ,i?C:C►r; 353.6 .6760 #1 116.3 5716 -. ;ri1[ 1 nA 7 #2 11e i� ,ii731 .5259 -.0014 L-.rJC6^c ' Errors LC Pass LC Pass NOCHECK' LC F'ass LC Pass LC F'_ss LC F-ass High _3.iti i0C",.r? 5;0.00 4.0%.GO 60.00 450.10 Low -.i'_?0 -.O600 -.0-000 -.0051? -.DO50 -5.,000 Eleni CR CC C1! FE PE ?18 110IN Lin it s Pm PP^ PFM PPM PPM PPm PPM Avge -..:0 y3 -.0032 -.0072 42 6;ti .ry9 v15 10?8.5!ti. .0076 SDev 0('162 (1`169 .0077 77 f 1 t 12 r:r 3,0,^ :dRSB 1980. 212. i106.1 .t?c i 8 12.45 .572$ 2.668 ' #1 ,ri,yil .Crri16 -_0011 4`.324 .f:�3:a 1 �3.n .�?07S #2 -.Cu&47 -.COeO -.0127 42,86 .0)825 10E.9 ,i: Errors LC Pass LC Pass LC Pass LC Pass LCPss LC Pass LC F a=_= High 151?.0 100.0 &X).0 200, ry 4r,-O.0 400.0 60.00 Low -.011-ICI -.0500 -.opy, -. 10001 -.rl4rylii -S, �ij -,fyyS:i E1e,m 1d1 K BE AC-: NA TL V v Lnit= PPM FPM PPm PPm FPS' PPm PC.. e - '.i i - rii;i; - i rY - r ? 5 .1 95 .C Arg_ .U.;1 .:� . . 3-�3 ."?.iIS 61� 4 �r?ri SL�ev OIOE 2.rJ5IS8 ?597 .i}i?22 0799 0190 '.6R5D 989.9 1727e645.78 141.4 22.10 12.73 347.1 #i .0066 1.456 _. 1881 -.003i .4179 .1629 .0106 ##2 .o ►87 -1.45,6 .1725 .i�r QO _30150 .1360 .0045 ' 0000079 Errors LC Pass LO Pass NOOHECk; LC Pass LC Pass NOCHECK LC Pass S 3 t► Low cr , - - High ...iCJry C?+�.C1 50.00 4ri),r;� bt.J.{ij3 .0400 Elem ZN S_2496 Unit=_ rrm rpm Avge .0572 .0009 SDev 10003 .J! 21 %RSD .6000, 376.0 f#1 575 -.;lii.'. #2 .0570 .0028 Errors LC pass NOCHECK* High 100.0 Lew ri200 `1ethod: -CLFS Sample dame: ICSZHI Operas,;-: -rCM Run Tli'-.e: 08/11/92 09:A7:'36 Comment: 1 :': DIL Horde. CONC Corr. Factor. 1 rlen AL g3 A3 Sr BE CD CA ' Unito rr,npr r]m Ppm �' m m Avge 114.v 0632 5686 0998 =33 .1922 SDev . . 00e3 .0146 .001:0 .0003 !iRSD .5959 13.1. 2.56: .0 it30 .3251 .93 t 63 t 1 � �r- 114. 1 %.�. .�/C"� .moi n.• i� tJ .1 ir.� 104.- #2 .0690 .5582 _C==8 .:_{3,7 .1936 1��5.7 Errors LC Pass LC Pass_ NGCHECK LC Gass LC Pass LC Pass LC Pass High 500.0 100.0 50.Or' 1.0.00 60.00 L•5i.5.J 1 Low -.20,00 -.060ti1 -.2�i00 -.'lr)�tJ -.x050 -F.,'oo Elem CR CG Cl! FE FF ,MG MN Units rpm ppm ppm C. pm, FF'� rpm Avge .1071 .0990 .0972 41 .21 1 .107 107.3 1051 SDev .0031 .064r) ,r10 i 3 .32 .026 ,3 ,0101 %RSD 2.912 4.00e 1.322 .7015 2.333 .7603 .9673 ' #1 .10193 .rj963 41 .5Q 1 .059 1r>6.5 .1044 #2 .1049 .1018 .0981 42.04 1 .126 107.9 .10,79 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pas=_ LC Pa=_=_ High 150.0 1 CIO.0 200 200.0 400.0 400.0 60-00 Low -.()1rirJ -.050'0 -,02-50 -,1000 -.0400, -rj*000 -.01,70 Elem NI �l, SE AG NA TL v Units rrm Ppm ppll. ppm ppm Ppm Frm ' Avge .2036 .9463 -.0.177 .2076 .296x) :1122 .1027 SDev x`065 .3r�88 .0485 0065 .(X 64 r 247 .002r-, XRSD 4.171 32.64 276.2 3.143 2.159 21.72 I.Gis #1 .1976 .7 79 ,titb9 .3op .2914 .01:�5£? .1101 0000080 ##2 .209E 1 . 165 -_0522 .2122 .3005 .1306 .1073 Errurs LC Pass LC Fans NOCHECK LC Pass LC Pass NOCHECK LC Pass High 50.C:o 304D.0 50.00 400.0 60.Oe) Loa: -,0400 -5,000 -.0100 -5.000 -.050.E E1em Zf! B2496 }Unit=_ Ppm ppm 1 Avge -2626. .0063 SOev 0J24 .0029 %RSD .9150 45.92 #i .26-,)9 .00'4p #2 .2643 .0093 Errors LC Fass NOCHECK: High 1001.01.0 Low -.0200 ----------------`------------- ------------------------ -------------------------------------------Me:had. CLPE Samp i e Name: N1342-'5- •2 WATER Operator: TCS? Run Time: r 8i11/92 09:15:54 ^ Comment: TOWN OF SGl1TNL t�lL' 921%2=�� n7 ra4?Ez 46�J Mode: CON--- Cc' r. Factor: 1 E 1 em AL S2: AS 3A $E Cu CY U.-Ii is PPIT Ppm ppm PPm Fr, Ppm pem Avge .0654 .0425 -.60379 -.-)'027 ,orlotj .0013- .0009 1 4 7.e,: .0104 ,ri164 .0230) .0019 :r 1rJf .0'.,-1.6 .0004 14 PS% 22 91 32.56 60.69 70.71 2':1 '•? 47.1L #1 .036-0 ,030c -,0542 -.0.041 :r}000 ,r 036 ,00-1 2 ##2 .r' 27 .0541 216 0'.?14 001,0 0 .0027 ,0006 Errors LC Pass LC Pass NOCHECK LC Pass LC Pass LC Pas=_ LC Pass !••i i g h .2000;i: �060- .200-10 ()40-150 �i};jE-0 5.04)0 Law 2f000 C)4,CjjD 2000 ,V'}„0 -15,000 Elem CP CO Cl! FE Pte+ M3 MN Uni t ppm ppm ppm Pr^m PPm PPm ppm 7-t�/'�}e 00,16 -.E.4:la(1 -.!!3 3G. .(►f 199 -.611;4- -.040%i9 -00019 0009 .O(-31 i .'.lii2C .i�(177 0263 l;,,i i4' %RSL- 56.57 28.26 70.71 1 t!{..2 257.0 1414. 47.14 #1 -.v:}c2 -.C,r}48 -.�}x!55 .0}ib9 -.�J4f;}6 .0162 -.il006 #E' -.0(')-_9 -.0032 -.0018 .00-29 .011 S -.'32015 -.0101R Errors LC Pas_ LC Pass LC Pass LC Pass LC Pass LC Pa LC Pas= !-High _0 1 Go _05.00 _0250 _too() ,'0481 5.000 .0150 Low rr 100 0-Sor) -.0250 i c-0 .04$1 -5.cwIr l .J 1E-0 E 1 em N11 K SE A,G NA TL V Q'`==s PPm PPm Pp1r1 PPm PP , -- PPm Avge .0s?22 .3639 .Oo76 ,001 C5 1175 0034 .0017 SLev .0216 .1741-6 2448 .002-2 022 .r 1160 .0 :a ?!�?4 %RSL? 989.9 47.14 583.0 141.4 13.60 2505. 141.4 0000081 i #! -.0175 .4553 . 1241 -.0031 .1 r=62 .o73 J!]G #2 .Il131 .2426 -.0393 .CK►:30 .1268 -.0641 .0034 Errors LC Pass LC Pass NOCHE'CK LC Pass LC Pass NOCHECK LC Pass High "0400 15,000 .0100 5.000 .05011 Low -.0400 -5.000 -.010(1 -5.000 Elem ltd B24966' ' Uniis ppm ppm Avge .0005 . 1051 SDev .0010 .0099 099 ' '/,NSP' 212.0 9.440 41 .01012 .09?1 #2 -.01002 .1422 ' Errt-:-s LC Pas_ N 0,'--HEC1K Nigh - ----------'af- ----- ------------------------------------------------------- Melhod: CLP5 Sample Name: f4l3425-LCS WATER Operator: TCM Run T i r.:e: '08111/92 09.21 :28 ,_;7 i 24,x;., LCSW Commrn t: TOWN OF SGU s:�L2•�tD 9'219242 Mode: CONN Corr. Factor: 1 E i em P.! SL3 3ti t±EElf 7�1� -n t^: nits pPm ppf" ppt? pp ^ prtT r n P^sOtT. P vgY 10,28 1 .2-:44 1 G 7 4 .0995 9132 1:r•'-] 16 .RSD .2190 1 .32-}8 1 .781 .7738 I8 .3432 .3282 ' #1 -111.27 1 .2-154 1 .']e 7 .9(i41 Q7-39 I.00,15 4L.42 #2 10.30 1.034 1 .060 .98,-:6 1.009 48.65 ' Errors LC Pass LC Pa=ss NOCFiEC;e: LC Pass LCPass LC Pass LC Pass N i g 5r'0.0 i 01-1.0 501 CIO 4 i:.,00 60-00 452-1.0 L ,w -.`rujr] -.0600 ' Ele:n C.R CO CU PE P2 Mi m Units PPp' PPm PPm PPm PPm PPm PPT: 4arge .9139B .9722 .9759 9.6-51 91105 20.62 1 .002 5L'av .ca- t .CFry23 .0020 .' 3z .02-i 1} .02 .00-1 % :SD .3151 .2333 .2634 3921 2.C;7 e .-1021 .38`:7 #1 .9e75 .97-S .9714C! 9.624 :9661 20.61 .9'794 #2 .99243 .973e .9777 9.67E 9949 20.64 1.r tc,5 ' Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 150.0 101:1.0 200.0 200.0 4;1:,.0 400.0 6f) ; LOW -.2-1100 -.rJ�CiO� -.rJ25':J -.1000", -.0400 -S.00rJ E 1 ern N i K SE Q3 MA TL v Units ppm ppm ppm ppm ppm ppm FPm Avge .5595 20.84 1 .017 .e565 ICu.06 i.-MO ,9231 ' SDev .2-'24 7 I.61 .011 .0239 ,r,a .019 :C-10S %RSL1 2.574 7.738 1.052 2.793 8577 i.930 843 000008 ? 01 .977, 21.96 i_,0 0 .E396 1 ;.12 1.024 .977c #2 .9421 19.70 1 .025 .B,34 9.997 .9960 .9629 Errors LC Pass LC Pass NOCHECK LC Pass LC pass NOCHECK LC Pass High -;0.fuy 300.0 510F.('iii 400. 60.;00 Leri 0400 -5.0,;)D -.0100 -5.OfUO .r15,yr j Elem ZN B-2446 Lill t ppm ppm Avge 1.001 1.002 SDev .0x14 .013 %RSDS .3771 1.316 #1 .4952 .7926 #2 1 .004 1.01.1 Errors LC pass NOCHEC t:: Hi g+`'• 101.0 Low Method: CLPB Sample N_zme: N13425-1 Operator: TCS! Purr Tim-_: 08/11/92 09:26:20 Comment: TGv'h 1 4F SOUTHLAN'D, 9219242 OW24/92 (rW-2S-G :) 6a'A T Ems: Mode: CONC Carr. Factor: 1 Elan AL S!:� AS BA B= CD CA ' Cni t=_ ppir ppJT ppm ppm ppm ppm �. ppm Avge 1 .259? .0143 .0272 .01179 cj,i n .004_2 7.1c4 SDev .066 .0246 .076 J01t?(1 ..'?13 %RSD 5.271 171.9 23.038 i.021 . 000 70.64 .S i 4s #1 1.297 .03f: -.C?326 .0?5::?6 .�;Cr!:� .i�/t,'? . 122 #2 1.203 -.003-11' -.0216 .X1451 .0000 _)027 7.20 Errors LC Pass LC Pass NOCHECK LC Pass LC pass LC Pass LC PassHigh 500.0 1(110.C. 5.0.01,1 40.00 601.00 450.0 ' L Caw. -,2000 -,0600 -.c 010 -.0050/ -.OC)50 -5.t '10 Elen CR CC CU FE PB MG W, tJr,its Pp'n Fpm ppm PPM pr ppm FYm ' Av-e .01 29 .10#132 0136�. 2 .010 952 -.(3r 70 x.881 .343? SDe .0036 0123 00 1 3 0 i 0 ir��i 1 1 063 0026 %RSD 27.59 701.74 9.422 .3475 1159.3 1.074 .76eg #1 .'1104 .0144 .C31?7 2.945 -.0344 5.936 .3=;21 #2 .0154 .Of)16 .0145 2.954 .C?t 109 5.925 .3458 Errors LC Pass LC Pass LC Pass Li Passe LC Pass LC Pass LC Pass High i 50.0 100.0 200.0 200.0 400.0 400-0. 60.00 l Low -.0100 -.00;A ; -.0250 -. I,-,cC? 0400 -5.C'ijC' -.6150 ' E3em- NI K SE AG NA TL v iUnits ppm ppm pp�r, ppm ppm ppm ppm Avge .0382 1.626 -.019' :0692 23.34 .0+573 .003 Dre Sv .�093 ,240 .0054 0326 12 .0098 0012 0000083 " %RSL1 24.24 14.78 27.41 47.14 .5201 17.20 22.33 1 .0443 1.456 -.0155 .[0923 23.26 .0642 .Q061 #2 .0317 1.795 -.0231 _0461 23.43 .0503 _0045 ' Errors LC Pass LC Pass NGCHECK LC Pass LC Pass NCCHECK LC Pass High 50.0=3 300.0 50.00 400.0 60.00 Low -.04Q0 -5-000 -.0134; -._1.0 0Q -.0500 ' EIein ZIN B_2496 Units Rpm opm Avge 0366 0876 SOev CiCQ7033 ::RSD 1.874 3.748 #1 137 i Cle52 42 0336,2 C,8 yP Errors LC Pass N?CHECK High 1CO.C) ' Method: C} t-8 Sample Name: td1342;�-2 ----Operator: TCM ----- r Run Time: 081111 Q2 09:: :52 ' Comment: TOWN OF SOUTHLAND 9219242 07124192 (M 3c GW) WATER Mode: !GNC Lc,rr. Factor: 1 1 Elam AL SS AS 8A P. CJ CF: yRnm nrnrr Rnm rnnr . frrUllic RRTrot fiR•r C -169 .0492 WwiiQ vi.4 e. C : ; �i P:11�: �I1�}`if} 0013 v� SDe .0 �:4 ..�.�' .RSO 1.676 81.58 =:�i.53 3.923 .€iia } 141.5 _1585 'tf: .0156 -.0053 .!x50600-Do -,001q_ 14.44 #2 .2044 .:58 i -.0,456 .O=+79 . iO:� v;C;{} i 4.46 Errors LC Pass LC Pass NCCHECK LC Pass LC Pa= LC Pass LC Pass High 541C3.C" 1101}.C: 50.00 /pn, 60 450.0 . I -. •i') LG73l:i•3i_) t i.�{�f ii�1i;f) Cl ti`lei/ Jt�rl E 3 e:Tr CR CO Cit FE MG_ MN \ Cnits Rpm RRm RRm RRm Rpm I—R1AvCe ui13 .tit.:�c'0 .43EJi3 .5�+17 3.='C)8 .1394 SDe`. .0i.}1 'lilt}- .0[026 .t0f+C)7 .0}16 �i�r0r06'i.RSL% 1Ca. 1 2�c. i 141.4 .i4?+2 .4775 .43?8 #1 -.r�}Qt i:3 -.Ctr i160036 .5011 42 -_ -.0022 -.0024 .0000 .5022/ -.43!314 3.319-- .1398 Er:oa � LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 150.0 100.0 no.C) 201}f-0 4.0.C; 4 0.0 60.{0 Lce� 0!01C, - }t, -._=5t:1 -. t;J00 -._}4'00 -5.00 -.r115i 1 E l em TY 1K �`� v NA T L 1% ' units Rrm RRm RRi" %RRm Rpm Rom pR:r, Av-e .010105 4.147 0058 .0031 14.3? .0295 C, 06 i• 0000084 SDev .0100 .377 .t305 .00-100 -04 .0*41 .0004 ' %RSD 41838. 8.999 528.3 .000 0, .26-615 15==.9 47.1 + #i -.0066 4.464 ,01 5,Q .0031 14.36 -.C?59 -.00e?6 #2 .007'0 Ji,7o 3.931 -.ti273 .t1ii31 14.42 .0027 -.tt 11 Errorss LC Pass LC Pass NOCHECK LC Pass LC Pass P OCHEZ,. LCF'as- s 6 0 Ut3 Low -.0400 -5.000 -.0100 -_5 00 G, EIem N E2446 UA nits ppm ppm vge .0141 .11:,-9 3ev .0111103 . JifC' %RSE. 2.441 O-)52 #2 .01'43 1 i 159 Errors LC Pass F GCHEr:, Hirs7 h 1'410.0 Low -.r32tirl Method: C:LPB Sample Name: N13425-3 npe-atctr: T-M ' Run Time: 08/11/92 A-P:37:3'; ` Com:fsent: TUii¢d OF Su•_;THLAN 9219242 0;7/24/92 -'MW-6S-GW, Mode: CONC Corr. Fac t:r. 1 E i em AL 58 AS 2A. SE Ci CY U-1-lits Pc'" PPM rPT P'r'n PPm r^p=n pr . A`Jge .845+ .060-3 -.00,32 .0301. .rjnn, , .0,1)41� 16.Cr= SDev .O 12 j .0)465 .01 1: .0007 l,RSi} _ .435 77.02 332.9 6.426 4141.4 424.1 .7119 ' #1 S. :C;93'c =.040 :t1cL7 ;�%�ti4 10.11 8 #2 . ,64 41;275 0043r>3iL r,t:rt; 054 15.95 Errors � -a=s _ Pass NOCHECK: LC Fav_ LC Pass LC =ass LC -Pass High 15-0.0 Ic rt 5 0 40.00 60.i1f1 Low -.c-J -.G6✓'-_ -.2CDC -.tVj- -.��ti�ti ' E 1 em- CR coCU FE PB 2116 MN Unites pP": pr;, ppm ppr ppm ppm pp;;: A`Jge .0095 .01020 .0,1191 41.610 .rl115 7.083 .2276 SDev .vt►t?4 .00016 .00Sc 014 .02-q6 .079 :Ou-,12 %RSD 4.714 29.28 20. 0 .8673 256.? 1.115 53157 #I .nt?91 c4 :ri`t8 I .620 -.09u 7.139 :C23�i #2 .0093 .0016 r 116s: i.6f,-10- 0322 7.0 $ 2270 Errors LC Pass LC Pass LC Piss LC Fass LC. Pass LC Pass LC Pass ' High 151?.0 1:10.1/ 200.0 200.0 441N:.t1 4?0,t? Lowr 100 ,015`X) 00 1ru`1;] rl4iylii 5_!,r?� .ri �i� 1 � ' Elem NI K 5E AL NA TL v Units PPM PPM PPM. Ppm PPM PPr PPM. 0000085 I Avg e 0098 2.356 -.0035 .0031 14.40 .C-072 _0075 SDev .0062 .309 .0358 :!00-D .22 .017i .O O i 2 %9;'SD 62.85 13.69 1021. .�y Jt�i� 1 .553 233.4 15.71 #1 .0142 2.475 .01121S .0031 14.56 .0193 .O 167 I #g2 .1JJ55 2.038 -_El222 _0031 14.24 -.E+049 .Ok)84 Er:-ors LC Pass LC Pass NOC:HECK LC Fres LC Pass !OCHECK LC PZSS High 5':.Elis 20 _02 150.0*", 4001.05 60.Ov Low !14 tt, `no i)10 0 -5.0 0 .050 0 Eleni 27N E.-2476 Units PP{R PP e: Avge 023 7 i .o712 SDev i�si s i Ji ,Of ii! %%ISD 3.693 .F 1432 #1 .029i ' C .j?SC 's<0 ' • i Errors LC Pass N0CHEC"k-: HIgis 100,0 Low ---- `-` )�� ----- --------------------------------------------------------- IMethod: CL PE vancie Name: CCUP {Operat:'r: TQM Run Time OS/411192 {,:=:39.4C> Comment: V IMode: C^�C Corr. -actor. = / E 1 en AL S �? F'rs 32 CD i A U-1 itS F:t,n FR{'� FPm _ _Fr{?: F>ir pPm PP{' �\ ' Avge E.991 5 .F25 9.279 2:497 1 001 2.965 �J.1? SDev .0!9 025 J;. 12SU .63386 .4897 .6017 .4516 .3689 .3192 .567; #1 3.005 5.nns. 2.98-q .4984 2.458 42 2.9.7$ 5.0542 9.921 3.007 1.o z, 2.971 25.23 ' E:-:-c+r=_ C!: PaSs CC Pass CC '=ass GC F'a_.s CC Pass Gr- Vass GC Pass Value 3.t ,-)A S.0 ;0 tej.GO 3.0-00 1.000 3.0 ':t 25.441 Ra-,nye 10.00 jri.or)) 10.Of-) 10.00 i .00 n.iE�1 Elem CF: CC CU FE FBMr MN Units PF7 RP{" RR`s PF{r. rpm RRr rtPm A,>ge 2.439 2.927 3.022 12.37 9.829 7.•499 i.987 SDev .016 W)g �ti14 .05- .083 ;y1e .Oi 1 %RSD- ..55365 .2no5 .4667 .4C007 .8482 .2453 .5323 ' #1 2.978 2.921 ... y18 12.34 9.77? #2 3.000 2.933 . .Ey33 12_41 4.858 7.512 1 .995 ' Errors_ CC Pass {3C Fass GC Pass CC Pass CC Pass CC Pass LC Pass va, l ue 3.000 3.04iJ 3 01-10 i 2.-o i i t.00 7.50:50 2. 000 Range 1_1.00 1n_n)-, 1;.00 10.00 10_4'i 10.0E. I0_-DQ ' EIL^ IN k: F:8 ter' TL v 0000086 1 Uni t- ppm PPrr. PPm PPm PPm PPM pp,r. Av7e 3.1:!25 203.4 x.090 2.911 27.29 It}_05 2.9� Rr=3D .3573 1 .130 1.0513 1.718 . 1756 .5384 .2766' 1 S.=017 201_34.i2e 2.97: ?7.2E 111.01 205-1 P. 2 i}3y .052 2.946 27.32 10.0 t 3.Q;r14 ' Er ars LC Pass CC sass QC Pass QC ?-'ass GC F'ass Qc Pass QC Fass Va l'ue .3 0(u,} 20i 0 5.000 3.000 2?.5« 10.00 00 3.000 iJ Rangy 10.00 1 !.0 ir0,0.! 10_00 10 GO 1n_0_ ' Elea. ??y B2496- Units PPT PPT Avge 3.0 !a 4.447 %T�ESD _3423 .134': !fl .2 J� 3a f S 15 ' Errors OC Pas_ 1`0CHE�F. t:a1 3.C!00 Range ic_ .0cl ' I?ethod: ..Li-Li ..GR'.��c s:!�?�� ^� l�.'::C: Wil.tJ S-. xrM----------- - Time. 081/1i092 09:4-5 ;54 v Comment: CCB _. I"-3de: CCO C Corr. Fact_ + ' E em AL Sri AS L ~- - - }. B;`. uE Cn Cts Units ppm PPm Ppm Ppm pYm pp�r. ppm A`ge .004y _01 5 .{:21': .0041 _.'10 .32 0C.)13 .0249 SDev .r}r!6? .0 i(-,9 .'�000 .0019 .i000 l .�>" )6 .0x021 9:RSr 141.:, 54.75 _0256 47.14 .0!010:} 47.14 8.241 #1 .r }GS -.iJ1`1,. __Ccl .01027 .0002 .�!'Jie .f 164 #2 00 000214!214 .f1 1�� .�!iJ'>2 .(!ljii4 =23� Errors LC Pass L.. Pass NOCHECK LC Pass C Pass LC Pas_ LC Fass High .2CYD010,600 .2=}.}0 _t's,i�r0 .00510 5.00i) E 1 am CR co CU FE F'B Me Mi f Unit`- PPm PPM PPT PPir PPM PPM PPT A:•g¢ 0036 .0012 .0057 .0091 .0nng .0015 x 017 Kiev .006.: .CIC.57 .L`}rJ5ji ,0000 ,04$2 .012i 1 .;Tr;riy %RSD 173.7 4e4.0 90.13 .0323 6317. 1414. 23.257 41 .c OOG .00512! -.0021 1 .C�3=�$ ..!i64 .0014 #2 -.OfCpl ! -.0023 -.0'?3 .009i .0333 -.0134 .0020 Errors LC Pass LC Pass LC Pass LC Pass LCPass LC Pass LC Pass Low -.0100 025-! -.1000 -.04$1 -5.000 -,0155x0 0000087._ i E l esrr NI K SE AG NIA TL v ' Uni is PPM PPrn PPm PP'" PPm PPrn PPm Avge .0066 -1.163 E?207 .0000 .130i .0193 0008 SDev .0046 1 .510 .06173 0022 .0256 .0000-1 ,�}r i5Z %RSD 69.93 129.9 425.2 22360. 19.64 .1541 663.2 ' .09P -.!1Q.: .0028 .0015 .148-2 ,rtf47 ,0071 #2 .00133 -2.23; -.041` -.01015, .1121 .0193 -.0047 ' Errors LC Pass LC Pass NOCHECK LC Pass LC Pass NOCHECK LC Pass H i g .0400 5.c!00 .U 1 O ? 1.0 00 .01500 Low -.04��rt -`.Elt3�i -.r�lrif, -S.Jv$0 ' EIem Zni E 249' ` Units pom PPm Avoe 0t:' 4 02 34 t�; SZ'eV On r" 1,..�L 686.2 4p.v 1 #1 ,i�tl`ii ,fliia ##2 -,ryEi13 ,r116u ' E rors LC Pass NOCHEC V High .0200 Lc,w -.020,0 ------------------------------------------------------------------------ Methac: CLFB Sample N_am,et N134c5- . S?pera� . . ICM Gu. TiMe: 02/141192) 09:4Q:5Q ` r'om cent TOWN LF SCts#THt r yi qr i 92Gr i 7: i 2 // ii'�,TE ri: V [�",t-J4-LTi`.S 1 Yd!'7 1 ter✓ Mod_, CONN C:.:rr. F 4-c, 1 Eiern AL SP AS 2i E= CL CA Units t, tIr- prm Porn ppr<r / cc-n ppm Av-e .2412 .01156 -.0239 .0369 ._,coo 9.613 SDe-v .0399 .01 .0f72 ,OrInc, .rinf f:; ,CtE?5'; .rrY1 '.;i=:'-D 16.53 70.Oe 72.02 .O00 .fjcE O:" 159.1 .3190 ' #1 .?130 .010`9 --011 7 :0.- .! riV L-,()x;76 ?.611 #2 .2694 .02;3 0301 036 :c,0 i ,Oi;rJ4 9 655 Errc,r=_ LC Fa- LC Pass N;0CHECK L/Fass LC F_ass LC Pass LC Pas=_ ' High 500).0 10.0 50.00 60. 10 45:7.0 Lc'til .C�t'Jt1 `6VLj `ji15131 ,0 ,50 -=.i riij Eleni CF: co C: Fu t�GUnits ppm PPm pp:^. oPpm PPr" PPnAvge .0.029 _.r�5= .OC 73 . .0224 4.8090348 �Ce! .l)'1�.��! i1j�1 i 1%�.'1 ,0 1 6" .11t t3 .�1i li�):.a \\ :!F:SLi 15.72 32.63 71:j . /S . .09�: 74.58 .0_547 1.169 #1 .0025 -.0064 rtrz5'347 -.0341 4.Si17 ._5345 #2 .i1i�32 -.r;;j1.:; .01r430 -.0106 4.81,► .03_51 Erro s LC Pass LC Pas=_ LC C Pass LC Pass LC Pass LC Pass ' High 1`0.0, 1 CIO.'; 20m, 200.0 400-0 4i u t.0 60.iJ:= Low 01001rJ_5Uf1 .02 5!3 .1000 0400 000 .rJ 150 0000088 1 Elem Ni K S; F6 NA TL- v - Units FFfn ppm FFn pp-InFFA" FFM FFm t;��3e -. ; C. .5823 -.01312 .�e�uJ�= 70.53 -.04-94 -.tv036 SDev .0062 1 .30;4 .1{)9'3* .0022 .33 . 539 .:)i�43 ' 'ARSB 2652c-6 223.9 85 .a .t'000 .4666 1vR. 1 119.7 #i -.00144 -.3397 -.10615 -.01115 1.30 -.013CIO,67 ' i� .L3f344 i.5j>4 .;1461 .iJ;r15 70.77 .tE�7-s -.J�t%b Errors LC Pass LC Pass NOCHECK LC Pass LC Pass NOCHECK LL Pass _ 1 14igl-; 5r;.00 300. � �s�'.tJc 4111 60.00 Low -.ii:�4��..� _5."DOO -.t>1tlU -5.000 E:e,q 7i# B2496 l units FFir, Frm �S Gyro 03 11 i f;1:51 �. %P3r ...637 7.317 #i .02Q9 .0422 ` Ii 1 vi =71-Ors LC Pass NOCHECK T:.� High 1:.�...�� C L 0000089. ' Tie $-ii-92 10:02;13 AM pare i Method: CLPE Sample Name: N13425-5 Operator. TCM Run Time: i1e/11/92 10:t !;15 Comment: Ti1W ! OF SCUT-LAND 9214242 07!24!92 s TD# Ml-!-60-C-WMS? WATF; Mode: CONC Cor:-. Facto:-: 1 ' E I eti: AL SB AS BA BE CD CA Unit Pp!rl FF}M FFm FFm ppm FFT pFpt. ' Avge .05,&2 -.01354 .`i336 .1002 .00 2 of+i9 78.f!7 r i 1 7� f f f �ti' ry yii 1! `1i (Y f �Je ..7 ,G JCS. �0.t> .�!2b %RSD 32.25 152.9 65.23 .0000 _r•i irk: 262.7 .4370 ' #i .041 9 - ?t3i.4 .,.j .i_loc" .r 1v_C -,i.ir ,��r 83 #2 .06-66 .0113 .01212 .i 0,02 0002 .0027 72 31 Errors LC Pass LC Pass NOCHECK" LC Pass LC- Pass LC-Pass L1. Pas=_ H 5rii).(1 C! I O v F1 li �" 0C, L:� fisi 6i� {lli 1}=-ijli�. Lit .2 110C' -.06010! -.2';1 o -. �J5l? -.i 'J5{J - .rirjri � 19 (� M� Clem L-: L1 CU r� F MG. M Ur.=ts FFm ppT ppm PPM ppm ppm FPt?; Avge .&('6a .`1129 -,0019 16.61 -.020 37.36 34.70, ' SDev :f)7r• 0 .0000 .00103 .135 .00?5, .Ori -,34 . %F. i. r J %F.SD !%tikJC"+ t3t36-r CJ'>iH .2950 0 40.88 1.0e3 293 #1 .0062 .i3i12 =.ru!1q 16.58 =:i�15� g7.0S #2 0362 .1J 1 r4, AJC!i s 0.b s 14.73 ' Errora LC Pass LC Pass LC Pass LL Pa,ss LC FZss f i Pass LC Pass f� Hi-hi l�Yi f) 1fit; (> Lf1:J.�! 2yi.-I C! 4tjfj !; , ft ijii �( Lew -.i 115i�1 1 ' Eler, �tii i c2 AG N,-A TL `J l::iits FFm FFA PPr PFT FFm FFm FrP(r, �J Avg-2 .,212 38. 1 i -.0076 .0.046 92 '2Ci .1091 -.0-102 SDev .0142 .14 .0036 :00:1C �.31 .x035 III.F.SD 66.99 .3705z 47f.51 121410 32.19 22.3? #1 .0-112 38,01 -,0101 . 046 91.98 .0 G43 - - 0,--) ^ n2 0312 38.21 5J v'46 92.42 . t33r .i1j 130 Er':ors LC PassLC Pass P-OC!(ECt: LC ass LC Pass tOC!?ECR: LC Fc=_s Low ill if") -5 f]i irl `/i r.r! rl:irl 0500 E l em ZN B-2496 U:fIts r^^FT FFm Avge .0335 .37o0 SDev .0011 .i3r!9 ' %RSD 3.168 2.592 #1 .032. .391 ' #2 .0342 .38x9 Er :-s LC F- s NOCHECk" High z 001 {1 Lc a i32'.J:? ------------------------------------------------------------------------fro 0 0 0 C, 0 ' Tue 08-11-93 10:07:06 AM page C ' Method: CLPE . Sample Name: N13425-6 Operator; TCM Faun Time: Oe/11/9? 10:04:13 Comment: TOWN OF SOUTFL AND 9 i9?42 07/24/92 tID# MW-60-SWMSD?WATR Mod_: COdC Corr. f=actor: 1 ' tlem AL SR AS Fr BE LD CA Units Fpsn Fpm FFm ppin ppip pp,r, r ppm ' Av-e 2.175 -5950 .i.?352 2.�YL?? .0613 .t;Jl 64.90 SDev 022 0361 4181 .028 .0010 00` .917 %RSD 1 .019 6.063 =_.361<147 1.7 .01615 : .124 ' #1 2.160 .5697 ,0284 2.382 .0 96x_5:0 84 .3 C #F2 2.191 .6207 .i148?? 2.421 .{ 610Y/.' LC .f131Cs L5.58 ' (Er ror= LC Fa=_s LC Pass NOCHEk"' LC Pass LC Pa - t ss LC Pas= }41g^ �rYti.i1 1r->L1.if �(?,fYe; ,.'!S f:r' 6:i f::: L�Ct r =rI Y(1 - A 6i it; -1 - n, ElesY CF, CO. Ci' FE F •� "`f Lam.t= prm FFYT pp'r Fplm T pem petr. Avge .2316-0 .5693 .2?57 2�?.1t? .53=9 40;.70 16. ? ' SDev .0046 .0.023 :!3,C 00 .mac .U3`$ .03 6 V . i' ♦' CT . '. /.rte. y ^. %RED 778 s .40992 r_=,::,0 1.L?"'9 7. .19 2 .96.32 73 . �c .Lt D. .5 5-4 L i�Y 6� 16 35 fer 2347 .5709 .29�" 2t?_ / �`Y-77 ,.;..75 16.6: Errors LC Pass LC Pass LC Pas=_ LG/a=_= L� LC Pas= LC F'a=s High 15;).0 100.0 2 0 0. 2G�0.0 L10,0.0 ? 6 -.0i06 -.L?5TH'i ti NTL' Units tT. ^ " T. ^ rt pr �tTi pfr FP rp' pp rP Fs ni Fr pr Avge .615J 42. 15 -.050 .04=-9 101::1.6 .6339 _557Q, SDev .0 2_2 9 .r?r] ?i C .0044 0028 1c �.7c3 a .1? • ^.28_ . g6c%RrD 3.7:8 .0.00 - #1 .539," -, .. 4 .15 -- .�?L fir'.' .i.141� ��7� .��ES "i.I J'� #2 .62-16 42. 15 .0412 .�1.,4?ii !r?i _6ty57 SSS; Errors LC Pas= LC Pa=_, 1r0CHECc_ LC Pass LC F'a _ NOCuECK"' LC Pa_s High, �t?.00 300.0 50.4 C,v ii _i;c, Low 040C -5.v');_' .1310;1 �.oi"Yl ,,1��IJ ' E1em Z E-2496 Units ppm pp,;, Avge .6153 1.011 SDev .,07 i .r?-::'J %RSD 1.142- 1 .945 #1 .6102 .9967 #2 _6203 1.024 E: rocs LC Pass N_ViECt<. Nig` i111.0.0 Loi .0200 ----------------------------------------------------------------------Oy 0 0 0 0 9.1 1 Tue 8-11-92 1-':20:46- AM page 3 1 Method: CLP + Sample Name: N13425-4L Operator: TCM Run Time: Oe/11/92 10:12:1e Comment: TOWN OF SOUTHLA4D z0219242 07/24/92 :ID## MW-61-Cid? WATER Mode: COiNC Corr. Factor: 1 1 E I ears AL SE AS BA BE CD � Cr; Uiii is ppm ppt� pp" pp T- ppm pFmt ppt'•• 1 Avge .f x• Oi 292 -.0156 -.0077 O111 .C}'. 0 2 10009'}i•J:J? 1.951 SDev 014i _ l ;31 q ti�i+tliJ .0000 [:rit7 ijlrl %RSD 65.41 70'.67 168.P- .040100 .C 00,,0 141.4 .5197 1 ##1 .047 _.'J j?� -.168 .0iii 0002 1 .tiu[a #2 .;%15? -.0235 .0015 .:rii1 .0102 .:oie 1-9`9 Errors LC Pass LC Vass N0C #ECS: LC PassC Pass LC Pass LC Fuss 100.0 50. it1 4 , vt(y 6 C',; \- La•,q -.200t) -.13600 1 Ele•T. Cit CL CU FEr'$ MG ^''Y units om n jT n 1 t p� rp rp•n ppT prm prtjr AVge -.CIO 16 -,0016 '.0023 .714 1 SLey .f ii7f:a .0029 .0013 01069 .f i 1 1 i} �ii_i•1,•G l li!i`}Li %RSD 56.57 176.8 47.14 5.$35 49 >S c: _S5 .e9 i .i� 4 ., 1 #i -.0023 -.0 013 7 =.0037 1 i2.1 .1126^. -.030S #x2 i''r.'J1 i .t it:}4 .0.0 .6147 9232 .6109 ; 1 Errors LC Pass LC Pass LC Pass LC Pass - LC Pass LC Pass LC bass High 150.0 i CPO, 0 `i I}.t; 3i}i}.i t L:ss t ?) C_}r,..i j 6,J. _if, 1 E1em NI SE AE NA TL 11 Un=t= pp, peri ppn p'pz pFm prr: ppm Avge .i..i06 -.`t4?2 .li02 .0 000 13-192 .Li15 -,i;iul 1 SDev 01C,!71 _L 1?6 .0,_55'J .•Jt;C2 - .05 .0481 .r 5 15.7 7 .71 538.9 .rJoi-10 g�3u 1.�c52.6: 66 5 , 1 .01i2 /-.6738 -.0287 -.:U.5 13.74 -.r025 -.2246 .OIL91 .0015 13.36 .ti6'55 -.002 Erro s LC Fa=s LC Pass NOCHECA: LC Vass LC F'ascNOCHECK r Pz = High 501.Oili 300.0 50 r': 4 i u�.0 -�- •U- 60.0�1 Lor .ilea o -5.000 00 0i' E1eft ZN K-2496 Units pYm ppm Avge .0125 -018 1 SDe`: .000*3 .0033 %RSD 2.931 1 S.C;, 60 1 #2 .0122 .C,2 4 Errors LC Pass N'G,_-H,E 1 Nigh IX1.0 Low 0200 ------------------------1----------------------------------------------0000092 1 ' Tue CT8-11-93 iJ:S_:151 AM pare 4 Method: CLPB Sample Mame: CCV3 CYerator: TCM ' Run Time: 08/11/92 10:53:13 Comment: TGWN OF SOUTHLAND 9219242 07/24/92 WATER Made: CCMC Corr. Factor: i E}em AL SB AS BA EE C0 C>1 Uni is ppm PPM pPm ppa'tl Ppm pp:r. pp"P rAvge 2.726 4.993 10.33: 3.0`4 1 .042 3.319 GL'ey .017 .006 .010, .010 ei)A r tC '.%RSI .6416 . 1113 .0390 .3221 .51988 .0640 .3442 #i 2.739 4,797 10.34 3.061 1 .047 3.t%�C) c5, 17 #2 2.714' 4.98? 10.33 3.047 1 .03 3.012 25. 15 Erro. Ci. Paz= GC Pass t4,C Pass CL. Vass Oe pass 88 Pass LL. Pas= Value 311.C�t;C; . r)ijrj } ). te rt, C', t ijr it R 1G.CIO 1 Oc f ,nn +i' 0 - r , MG i"•ti E 1 e+^ CF: G, �; Fc r B Ur" ppm ppt^ ,pn i�p." p_r: ppn PP;7: Av e 3.09;._1 2.--9c 3.096 12.22 .26 %R'SD .1466 .5239 17/06 .4070 1 4 .75-51 7.2 �Q C 4c #2 3.0 87 2.9351 3.092 12.18 9.c,•a 7.305 r t25 Errors QC Pass QC Pass CC Pass CC Pa=_=_ GC. Vass CC Vass DcPz=_ Value 3.000 3.01-}0 3.00.0 12.50 1=_% i;"} 7.�':rt Ranue iC).00 1ri,r}i 1;),i}r� jr�,�;r} iri.00 jU.cv, E'1 emt r I K S !�E AG A TL v uni t= pp:.r• PPM p P M ppn PPT pp-In ppm, Avge 3.154 206.2 51.238 :3. 1 i8 251.7 : 10.511 2.987 S1?ev .029 .9 .O i 5 .0,22 .03 .iii ,1-117 r %RSig .92516 .4437 .278e .7C}18 .10}67 .9:351 -51 8i #1 i7J 207.5 �.S4S 3.iw3 2`i.7L^ 1�t.44 C:.Q1�: ' #2 3.134 206.2 5.227 3.102 25.7? Err,!rs CC Pass QC Pass C:. Pass Cor Pass CC Pa=_s or- Pass CSC Vm-1 Lie :,ruin 20.01.0 `1:.0:10:} 3.0001 27.50 10.CIA t Rar,ge 10.00 10.O(i 1 j ,1r" 10.00 1 iirt j:-t fWl r:rt r Elem Z_N! B-2495 units 0pm PPT Avg-2 3.07e}7e 4.968 SOey .0.0'7 A07 _PSIS .2411 . 1326 #1 3.0e3 4.97_3 #2 3.073}73 .964 Errors GC Pass NOCHECK Value 3.!i O -P3}1ge i;i,,;yr} 11 O O ((��U 0 9 .� r Tue 09-11-02 10:58:11 AA page 5 Method: CLFB Sample Mame: CCB- G-orator: TCM Run Time: 08,111/92 i0:55:52 Comment: CCB Mode: CONN- Corr. Facto-: 1 E 1 em ALSB AS BA EE CD CA LMi is PP r ppm ppT PFT ppT Pi=m ppm AVge -.0j117 -,i)094 -.01-=7 .i;rp{)i) .0009 .0041 .0. 56 SDJe`S .01000, .002E-024 .1-1010 .r}000 00 03 .01006 .0026 026 %RES' .0076 29.27 8.997 .0.00 32.17 15.72 9.459 #1 it -_. r,rt74 =:si1r."iri _rvrjri0j tt()i)L .;_1;} � .()2e'3 ;f2 0ii #? fb1 i 0 14 .iCAIU14i 00 i S .0'45 .0,239 Errors LC Fass LC Pass itf:� �i %' L� ��+= LL C` F' N _ .� "- _C F Fars a=_=_ L! Pass High .>✓' .0600 ',rye., 0k1.:0 J.iJ+lU Low -.2t '.!vi -.060ri El em CR CO Cii FE F,Fj MC M'l un;to PP ppf' pF"t PrT pFm pp". pYm Avge -.0052 -.'10112 -.x175 _()=4)2 -.01224 -.x:226 .r !2 SL)e`r .,I-4;w .tj::)i rt .:1026 .v)15 51 .'1128 .0000 SB 77.66 .02:95 34.00 14.40 66.545=-.27 .000(1 #i =.::i ii 0 = 1")0•.)10_ (i019 3 r.i S 1� I S'��5 03 i s :0'1.1`9 ''t'.2 -.0023 i2.r1r iy{157 it0"72 x)1211 D137 0,eD2? Error LC Pass LC Pass LC Pass LC F•asa LC PZss LC Pass LC Fl`as 'rJi g}+ =E}1 (J {'i` ii) �)250 ii;rii1 .04;St �.(ytif. ,:;ic.`i .tJ.'{til �)CJ'-_! 1(iOrlaC': =lesr. NI K SE AG Pic Ti L++:-tits pp:'t pp,T pp:m FFT pp^ ppt" ppm Fvge -.0078 -1.17? -.0055 -.0015 .1539 .Q1?0 EL'e`S Oi)6•y .4 7 .00513 .0042 .i X455 %RSD 86.6-4 4 0.6?1 96.02 272.2 29.52 38.74 45 11 #1 -.n126 -1 .5Ii -.ft(?92 -.0,045 . 1C17 .0071 -.iar�:rrt #2 -.OID30 -.43-7 -.ri413 .0014 .4361 03,019 -.0 Yom_ Errors LC Pass LC Pass NOCHECK LC Pass LC Fass NOCNECR LC Fps=_ Lc'rJ r`itr0s;1, c ryrrlOc tr)ri -�- . J i -.s. .. 05 )i i Elem B_2496 Lit3i ts ppm ppm Avge -.0-001 .028r.j SI?ev '00 .0 99 %R'SD 236.4 35.37 #1 0004 .0-35--, #2 000 .021 ry Errors LC Pass Nigh .0012{X) Lose -.02,00 --------------------------------- -- ------------0 0 0 0 0 9 4 Tue 08-11-92 11:02:38 AM Rage b Method: CLPB Sample Name: x#;3425-1 Operator: Trig Run Time: 08%11192 11:00:41 . Caim"Tent: TOWN OF SOUTHLAND 9219242 07/24/92 (?D# Mild-28-B?4; WATEF: T ue 08-11-92 11 :05:2-33, AM page . Method: CLPB Sample Name: N13425-2 Operator: TCM Pun Time: 08/1:198 11:03:25 Comment: TOWN OF SOUTHLAND 9219242 07124/92 :ILk# MW-3^-Lir-'? WATER Mode: CONC Corr. Factor: 1 Eletn AL Sit f:S BA LfE CD CA GiZit= pt- pp Z rptf pp. ppi ppiT prm :vge .348.. .0)1 t4 s -C'192 .2105 -.rs H! -.tai}23 12L"s-rr clev fy 1 7 .�) t53 f)�?39 CF+`��tf� r if;^Q 7 �� %RS-B I.5115 5.!x19 1-237, , 00 169.6 .2152 #1 :3448 -.iiij` :t`1gg - , - - - - �=} _. '_?i C> )!?7 ?rim 1=f t c 185 213 =ii};'? -_00,150 12 °.7 E-rorsL ` amass N;�HEicv LC. Pass ) f ): Pass C Pass L 2= .. )-High �s:;i t) its ),fi `:� 00 4:s fpti 6G'.t ^f EIe:r ti :ti CU FE fr M- U,1 li t s -L:1its ppm ppfip pprf PPM ppm �r,.r r�r .(11 i9 .f%11_ 2.11 .013? i7.13 20).55 SDev .;jj 4E3 .E?C164 ,Q_}- .C)1-1 to .i fi< RS^ 20 95 4?.89 `4.39 . 13-796 115.3 .iL 16 i#i .005-18 `?156 0 16 ?_CSL _j, 1 �s 70 `7 #c . C-073 0082 C'1072 7` 2. 1-02 :3C)at:} 1.16 2 c Errors . as `'acs Lam- Pass C P-mss LC ass LC F,aSS ��. F s= LC F' L � L ,�. __ High } 2i,):i Fj 20t} f} 60, i': rt y ;�(ifl - •�l L_ - fC�i - 1 rsf_)c} s4:_ -c;.ci QCs 15C; 2Iem. h3I i_' = r+7 NA TL ll L`it,ts pPfl! pR i✓rm f"fl ppr�: ppm ppm Avije .0239 47.7213-.026_ , _75 .0265 003 Si?ay .0150 ,68 ,2._^. .f;Ci73 ,Jrt4fi '!.r'8L b?.05 1 .431 Csf;cvs .2527 ?7.47 f#1 f.;.345 4 ..=1 1'?1cs7 ,002- t?•6.J cti fj3 17 c J .` :ifJc. 0133 47.24 ��63L ^:,ac 80.91 :i2I4 rjis`'i Error= LC Pass Lt, Pass NOCHECK L! Pass L_ Pass N*0 H2ri.. • r'�_S - Hich 5 .00 300.i? S:l Fst ise tJ Et i?.; f:`�i�i .�)�"':) E1em 7N B-2406 Un..its pnm ppm AvBe .,�-s144 .6923 %RSD .,'c:=-:5 .4763 f#1 .::144 .6900 i#2 .0144 .6946- Errors 6946Errors LC Pass N0,--HED--. High 1010.0 Low -.0200 - -------------------------------- ---G 0 0 0 0 9 0 r Tue 08-11-92 11:09:08 AM page 3 Method: CLPS Sample Nar.:z: !113425-3 Operator: TCM Run. Time: 08!11192 11:07:11 Comment: TOWN OF SOUTHLr"•.,ti)L 9219242 07/24/92 (In# K,4---'S-GW) WATER Mode: CONC Co-r. Fac tc•r: 1 Eleni a. SP AS p+= EE CD CA Units FPM PFt'l ppM ppm. ppM Ppm PPM Avge .2-555 .0373 .0417 .12301 -.01-107 -.211123 51.20 SDev .0279 .00)56 .10309 .003 .0)000 .�;ft26 .32 %RSDS 10.53 14.92 74.15 3.143 .-1002) 113.2 .5300 ' =.0 7 =. . 6;3. #1 .2357 .i- . 1198 .12{33 1.: {}fv41 9' #2 2752 0412 .0636` .1257 .0,'-!)7 .01c,_,5 61.43 E :-o;= LC Pa=_s LC Pass MOCHEC$: LC F3=_s LC• Pass LC- Pass LC Pas= H h �C10) r. 10)>��.{: 5r� i; i: r:`i r L 55:. Q, Low `1)111} - `)6 .0.050 Eleni Ct'. ~IG Units FPM PPT FPj"• FPm PPT FFM oo'• Avge .0142 .{_140 .",1U0, 15,01 .!'171 15.4;1 SDc=v .0037 .0013 „ice ,ti- , i3 .0.. %RSD 18.85 .;05-5 1^c.8 .3537 66.44 .7820 .3535 #1 .0123 :011-0 .0i09 14.97 :CD2 7 6 15.31 3:0.66 3#2 1)161 f}i i1 ,Lfs9r'! 15.`)5 006415.43 3 0)81 � E1:-ors LC Pass LC P-zss LC- Pass_ LC Pass LC Pass LC Vass LC Pass l-43yh 1.2.'91.13 100.ft -V- - 200.0 4:.:fi 0 4f:i.:-0 Q:. C, Lcr -�ftirM, -.t)Jl�'_t -.r}nCC U -.101315 -.;_Glil) -5.000 -.fSf�v1 ie- ).!nits FF,r. pP:� ppm FFm PPM FFfl; PFM Avge .()350. 36.98- .0187 .0060 85. 1-7056,. -0 .o92 SDel -t .65 1a 1 .29 0_048 %RSE) 413.71 1.755 9.747 .012x_0 .3-y-.,q 51.76 5;1.4 3 #1 .,--)249 36.52 :C)200 :{3 0)621 85.38 :0355 #2 0145 i 37.43 0)174 0)0601 G'- .97 0765 .U 12c Erre:-=_ LC Pass Lss NOCHECI LC PaSS LC Pa==_ P!GCHcCh: LC F'as High 5{3.0)0) 300. 50.00 40-0.0 60.00 LDV/ 114/10) -51.000 010-.) Eleni 7M 8_2496 Uni is PFM PFST5 Avge .1,3212 .2521 Sue .000-7 .0032 %RSD 3.254 1.263 #1 .0230 7 .2498 #2 .0217 .2544 Errors LC Pass NOCHECK High 100_0 L:,w -�01c+J0 -------- ---- ----------------------------------------------G0 0 0 0 9 7 TL:e 08-11-92 11:15:25 AM p. ge 9 Method: CLPB Sample Mame: N13425-4 Operator: TCM RL-n Time: 06/11/92 11:13:25 2Gmfnent: TOWN OF SOUTHLAND 9219242 07/24/92 (ID4 MW-60-GW) CATER !Mode: CONC Corr. Factor: 1 Elem AL S6 AS LCL`. EE LL' CA Units 0P.m pp:n api" ppm pa(B aaram Avge .i X56'? .0166 .0311 _toil - 000", --.0077 77.96 SDev .00513 r}ii27 r}r}35 r:fpJrj C;rjii:j 002637 16.54' 12 ''�'- 9.317 .c:5 :1000 .0t.tt-0 ?3.26 .472s #1 .060" `ry 166 :0333 35 10111 --i 007 L-.0055 7 7.7:0 #2 }532 0114 7 0264 10)11 0007 L-.0059 78.22 Er:-�r a LC Pas= iIP LC Pass LC Low, LC Pas= fiiC,: 5_C . v , L.C! 40.eirs bC;.t)(.� 45,�..L= L ow -.nAatr) - �i`}i)`i -.r-H'50 - 0CIO5:J� -5.r,.N) i em CR CG CU c PEi'3 MN U: i t=_ ppm apm pp'" pp'T p'=" A'V9e X 76 . 1136 .004 :2.43 -.00P-6} 3e,01 14.1 JLic;: t ti iii i;741 .:'`)i 3r, .i}c84 .rte'7 .f 7 . 3.R5ID 693 3i` .!J 1 26 28 552 i 5 .i rrs 19 5203, J #1 :r1'? '' :'F? 74 ?v.S� -V-14 ::r fe 2 C>=173 C}rv�`a16 S.50rJ26 i 3B.C: i 4 2g Err 0 S LIC Pa LC Pas= LC Pas= LC Pass LC-Pa_s LC Pa== LC Fass 'D High 1�`).r 0 ❑ijr: r; 2,0)0.Cs 4Jir.0 4U.Q.0 s`;.0-0 Lo -.010'; 0="')C' .iJa "U -. 1 ?fi .r:url!' -5. )-'r� -.°}15 ! E 1 eT, s; KSE AG NA. TL v Un.t� ppm ppm pPm ppi?) apFn apm PPM Av-e .iT-3219 38. 1C -,i) 69 -.t:cj'r} 79.('^ .Cr2C)3 .0025 SDe':' 01:F6/ - .41 (1ri3a ,. c .ni�ILL . . . }=.)`;j4 `rSt21c3 . .tr7: 1-.40 y141 .4 .4399 G #2 .0231 3e.35 'J245 10000 99.37 0122 0025 2 LC Pass LC Vass ?,!U'CHECi: LC Fass LC Fass t1GC ;ECK LC Pass Hi,,i. 50.001 300'.0 50.,')0 4f,0.i; -0.00 .� Elem.J ZN 5_2496 Un;t= ppm pp--q AivYe .0236 .325- 2r;ev .C,nfu _r�rj.65 3.p:S2, 5.630 2. )3 #1 .0226 .321 f) 42 .x.1246 . 3r s2. Errors LC Pass 4+lOCHECK" Low -.02010) - -----------------------------------------------------------------R 0 0 0 9 8 Tue 09-11-92 11 .19:301 AM page 101 Method: CLPE Sample Name: N11-3425-5 uperator: TCM Ru-.,) Time: 06111/92 i1:17:33 Comment: TOWN GR SOUTHLAND 9219242 07/24/92 (IIS# MW-6,0-51;MS) WATER Mode: CC:NC Corr. Factor: 1 tElem t4L S2 A FsM BE CD CA Units PP's PPM PPM PPrr, Ppm Purr PP+� Avge i 0-1299 .0411 .0994 -itilir-%7 -00415 77.:2 SDe�: .0140 -0055 .0077 f r}:}r) g-)0 0 0006 .26 %RAE, 17.21 12.51 13.73' .0000 .0000 1=x.14 .3363 # .139 s3 0313e 046-6 0YG 114 .3:}"" .0050 76.93 #2 .0,-71 0726!. :0357 .0984 'Yrs<<7 .uL 1 77.30 Error= 0 LC` P_s=_ Lt Faec ��C+C! ESE. LC Faes LC- Pass= LC Pa=_s r.cYPacs . H 5, igh .o i 3f .} Lei rit; LGrJ 2t,-100 -,0..6rict -.010,153'0 E I em CR: co Cu FE PE NG �"y Unity ppm part FPm'r PPM PFr'm C.p m PPM A" 7.+_}i 1, .0144 ..0-63 16.72 .Lmt 22 37. �"" 14.!C Soea .0,:t"t31 .moi�!Sd .��i1J .!!`ct .0296 .2.' %RSL' 27. )0 12.12 2:,.200 .3284 1-096. .676-2r 23�6 #i .01-46 .013E .C)i, 72 16,.::5 .0196 37..s 3'7 �. 1-e 02 #2 0:91 0156 0054 16.76 -;2 3 .221 14.07 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC 'ra=_s LC Pass High 1 .t7100.t' 2V0.0 200.0 L4•)O.0 40, .0 60 00 2 i em N! K SE A. NIA TL v U ni ts PPM ppm. Ppr?I PPM FirM Prrn pp�: Avge .0-013 36.o=' -.0332 .00Z-5 47.74 .r'-0691 .0u,56 S Ley ,001 r 1 .4rI .00is .0-!63 .4i .040 %rSD 4 7Y4 3.677 55.506 140 .4226 5,3.54- 49.=.i; #1 :-3 2 4 39.06 ="0316 --00SR 97.45 ; 6 ¥fa f�.=!�2 37.10 .r.-3�.5 r}f}F10 QS f�!3 00405 1:(1�^ E ro s LC Pass LC Pass N0CHECF: LC Pass LC "-'ass NOCHEC:-: LC Fa=-s High 50.00 300.00.re0 4'!!i,() }sj LGM i ,!400 -5.000 r i 00 -�,rjnn Clem Lf`1 B. 2496 Unit= PPM PP11 Avge .0214 .3456 Sne-v .0011 .L .i Oi iO %RSD :4.32.5.0 .00022 #1 .,m 324 .3456 #2 .030!4 .3456 Errors LC Vass NGCHECF: nigh 100.0 Low --020c! _ GOOG099 Tue 08-11-42 11:23: 11 AM page 11 MethDd: CLPH Sample tame: N13425-6- Operator: TCM Run Time: 08/11/92 11:21:1.: Ccmmer,t: TOWN OF SOUTHLAND 9219242 07124/92 (ZD#i t W-60-GWMSD) WATEP Mode: CONC Corr. Factor: 1 Elem. AL S8 AS BF. BE CD C* U•r:its PPE, ppm ppf., PpIp Ppm ppIII ppfII Avge 2.464 .6238+ .0625 2.421 ;_+=83 .0511 87.87 •3Dev 017 021a .042 0(.36 Cj0 0 S .00,38 .29 %RED .^f j87 6.228 78.71 .2396 .:r7i►2 7.507 .3296 #i 2.4776 .5.36- 1`?4 C.l!16 .0586 .0434 Ee.0S C; c 7 n2) -c^a -cam �+ # .4_.2 .6-i 11277 2.42_. fi5e, .:j g 87.6: Errors LC Pass LC Pas NOCHECK LC Pass LC Pass LC Pass LC Fuss High `00.0 1ijf: r5 50.`'0 4 j. 0 60.00 L:<'v! -.`r_iiyii -.rjvil 1 -.i }'J�_ -.'itJ r' -.,115511 s.) Elefst CR co CL, FE F i v NAA Un.ts ppin rpm p0fn ppm PPS pp. pPm Avge 2355 5829 .2877 22 . 11 .5'758 45.36 16.53 S D e v .00 1 B 01(j G 1 (j Jili1 . 16 .r1�! Y.h:SPi .757 1.31008 �j.1C1Ci .111E .ij a 7 .3558 .22i"t"7 #� .2I6! :Jt40� :X8'7 27:13 :.'(S8 .iJ.:Ft 16. 6 #2 .234,-2 5771 2877 21 09 5758 4`s.25 16.5-1 - r` Pas Pa P- r Lr s s Error L LC LC 'asp LC a=_s LC Pas=_ L_ Pass Fa_� !-i.tjr 0 20.".0 200.0 4.00. i 4x00.0 6C+.iXli Lois 4. C'-.C'25rf -.Ii�;jr5 -,r,4r:r; EIefr, Ni K �t AL IN TI 5r U:'-is Pp=' pPfn r, t1t, r'p"f pptt: pp:r Avge .61013 42.02 -.Ei26? .3462 110.7 :5275 .5762 SDev .006 7 .2)7 .0228 .Of- .2 .i E31 .006'' %RSD 1Ci7 .6502 84.68 13.69 17014 19-61 1 .169 #41 ,btiSJ ? ,t~ -.0431 .050 5 11 G.$ .54015 .521 is 1 #2 .bi5 42).22 -.r:;i to .0417 111.5 .7145 .5715 Errcrs LC Pass LC Pass NOCHECK LC Fass LC Pass NOCHECK LC Pass Lc'w OLnn i 5 000 0 1 i.1'.J c f j0; E efi Z 8-2476 Units Ppm ppm Avge .6112 1 .023 SDev .001 .013 %RSD .1641 1.298 #1 .6105 1.013 #2 .6120 1 .032 Errors LC Pass NOCHECK High 10.: .0 �Iw 020 , 0000100 Tue 08-11-92 11:30:46 AM page 12 method: CLF°B Sample name: NI3425-4L Operator: TCM Run Time: 08/11/92 11:28:44 Comment: TOWN OF SOUTHLAND 9214242 07/24/92 { i-)tF Mei-60-6'v;) -WATER Mode: CONC Corr. Factor. 1 E 1 em. AL SLS AS BA B2 CD CA liiiito ppm, PP+n PPIr ppm pP)r PPm PP+" A>>ge }62ti .O5C}C> `s 1143 .0>219 -.0}�. -0032 16.04 SDev .01015 .0056 :12130, 0Gc}0 rlC:;jrj Ct)13 14 =SDD 16.89 1 i .0S 14'4.9 .0000 .Cx,Y 3 40.43 .1337 a 4 #1 .0546 }S 0 .`.1 41 .X12 1 -.0007 -.0023 15.94 #= .0694 .C)�:6:i -.;)i�%c .[1214 -.0.-07 -.001- 16.s- E.rur s LC Pass LIC r'as il0C Et: LC. Pass LC Pass LC Pass LC Pass 14; y, C? J ru.t} }.. 60.0.0 4150.-0 rrf rpnyrrr Pp rI Fr A vg 006u )"1 5; 33,747 7 .L!116 C.202 .0'91 83 - •- .'De. 00 13 D05-874 J 7'.; i 2, ',RSD 19.28 1:}1.C) 28.28 .4122 146.3 .65 �9 .9215 1 .Ciil'0 (7[}:'a 33.7 35 =.,}zyic�:� S. 1 bf+ G:�` 3.760 0:237 6.240 Error=- LI: Pass LC Pas_ LC Vass LC Pass LC Pas=_ LC 'e. LC Higi: 150.C) 2{ i: i} =c}0_Ov C} 4t;i) �{ 6') ` .. ,0 5. Ea , t:il i_ SE AL NA TL u Units ppm ppm Ypr. pp: ppm pp:r. pp:r. pvge _6,207 8.260 .0134 .0074 2:7.12 .0a=`3 - )5 1 S?ev .C)1PC} .92C) .056+J !7�1 . .27 .(1.43 .t) 1� %F.3D 58.02 4.424 419.4 28.29 1.341 49 07 29.77 #1 .L7232 v 637 - ..0i 60 .94 t)J�7 .0064 i_lP .01[2 7.68+{J .rJ��1,) {i1.' :'� 2�). 0256 0,042 Errors LC F`ass C Pass=_ NOCHECK LC ra=s Lr Pass NOCHt°=f'. LC F'a=_s LOP: .C74C}{} -�,O(I`) EIem ZN $_2496 Units Ppm PPm Arifle .0107 .05=;7 SDe%: .0624 _011_)66 %RSD 22.50 s 2 •:Zv #1 .c,124 .C:5-3 #2 .Cw-,.9_) Errors LC Pass Lr.rw -.02 `' 0000101 Tue 08-11-92 11 :35:44 AM page 13 Method: CLPB Sample Name: N13425-4P Operator: TCM Pun Time: 08/11!'='2 11 :33:43 Ct3,3anert: TOWN GP S?3UTHLND 92192=+2 07.24/92 4 Tom# M41-60-ObI? -WATER Mode: CONC Ca:-r. Pact3r: 1 E i em AL SB AS EA BE CB CA U-ni to pp,m FpfT FF"� ppm ppm ppm pp,n 4vge 1.035 .021-23 .0287 .0429 .00 10",2 -.ON-5 73.42 SDev 072 .01.47 0000 .0045 .46 XFSr 7.085 74: .97 90.28 .0111,1100 .CfOr,`i 99.02 .6234 #1 .=;s=c :01(D5 .0450 :r;q2^y :r0002 L=:0077 "3. ri } 0 3` 12 4 092q r l 2 001 73.75 Errc:rs LC Pass LC Pass POC ECi: LC Pas' LC Fa_c LLC Pass LC Fa=_e High 5".A01.0 1fi.: ii 5li._YD 4G.0,0 60.00 4 5101.,r Ltw -.2000 -.0600 0- '.:}!) 135l -,flrt�r} _r, fo CR O}ii ts, ppm ocm ppRr ppm pp:r. ppr,; pp; A•r02 ,% ge .05 . ..1.2 .O<}81 17.47 34 38.5.3 15.19 SDeV .0036 .v"}!Ci .i� 0039- 'c`9 -LL %R'SD =>i .9i � 53.03 47 14 .7176 f 1<i... .7575 9i1 #1 .0110 .`082 :0054 17..38 :O008 32.35 13.14 006? iti 81 L'i1F}'� 1 7 56 0f 561 36.76 1� 2=: LC Fa=_s LC teals LC Pass LC Ea__ LIZ F'a=_s LC. Pass L Cs '= s i�SOii 150.:} 1011-1.�} 2C= }.i} `t;i}.�} 4.0i),C: = E:e3, N1 K SE Av st s L Lr,it= PFrn ^rprn FF'Tr ppfr'i pP": pug; pnm f"vge .01244 30..;9 _rlrii,L. -,iii.i� 91 .9%i .10ii f",03'i SDev ,00c?9 51 .0019 .0021 .54 .0168 .0,00,y %RSD 39.97 1.45%. 437.5 141.4 5239 1-6.60 .000z i ?11 .0175 34.7= .CN018 -.r}iJ3r} 91 .52 . iI30 .0C%?I #2 .0313 35.45 -.Ai;6r, -.IDIC160 `.'E.23 .fipgp .0031 E rars LC Pass LC Pates N!7C'r:'ED,"' LC Pa=_=_ LC Pass NOC* C^: Lf, ' High: 5C).00 300.0 5.0.CC) 400.Q 60.CIL L o rV -5. tom,�} ice}1 E1e,n Zfi`i B_24yR6 } -lits FFM Fem P.vge .0265 .9406 SZtev .0021 .o,f13i %RSO 7.786 .3:339 #1 .025: .9383? #2 .0280*, .9422 Errors LC Pass NOCHECK High i00.0 Low -.0200 ---------------------------------------------------------------------L_0 0 010 2 1 TUe 06-11-92 11:40:55 AM page 14 Method: CLPB Sample Maine: NIZ-42:-7 Operator: TCM Run Time: Oei 11!92 11-:38:52 Cominent: TOWN OF SOUTHLf-t`ND 9219242 .0,7124;92 4 j1-,# PW-I , -W':TER Mode: CGNC Ccrr. Factor: 1 E 3 em AL SS ;S BA BE CD CA Urii t pPm prig PPil'• PPrr RPM PPM ppm Ayge 0631_ ,Ct139 ,01372 ..?205 --0007 JOO} ` .• .P69 J SDev 029 }361 (03 33 .00Iq .N J, 3 012 '.:RSC, -7.11 258.9 90.68 9.428 .of)vi? 292.5 .2223 #1 .:1420 -.[ 1 16 .061 1 .0191 -. 007 -.00ray 5.=7 #2 .0El41 .:!'3911- .t?1 .0?219 .0007 .0}1-11-12 5.2b1 Errors r: LC P-=.=-=- LC "Pass PIF3CHECt: LC Pass LCF'a= L� Pas=_ LC Pass=_ P4 lg i 50.,.0 ?00.0 150. ?0 l0,•r �; 6(0.00 4y,0; C-600 _ _rlt":' - _J�f�t -.�itl�rj -17I-W)c E 1 em CR co Z".,}..6 PB Me M!•'': 11^•-}� PPS t-m pt- pprn Ppm Prm ppf, A-e .0050 .1_1070 ,1 1069 8.206 .f i i? `.324 .21-1-3 SDev .'..}l)2C _rte 01 41 .i�f Si�'.1 .�ii")c3 ..:fj1`�' ..�V .000 F.S t 41..19 :'e.24 clor'.f, .1 1�4 1 .9�' r'•2 i f o 42 ' Y 1 CIO---5 �.i(;9c; �1 CIA L74 P E IC) �10,098 y `q�L` #2 0062 0i::�}1 i�►::8 8.213 1112, -5.30,66 a :•a2 Errc..-s LC Pass LC Pass=_ LC Pass LC Pass Lr Pass LC Pass LC. Pass High i=f1- 1 `j.ft �,Jtc).0 -f.O.O 10101.1•' ::00.C, 60 Srr Loo -.flt �} -.OJ V; -.n2c;O -. 11-1-1-11; - f)Lf):�i -J.LLf.' - Eje^s 1-:j k: SE f?v NA TL v Units ppm PPMPPM PPM PP'n ppff, PP^• v7e .f,31i3 4.002 -.001-5 .I} ?15 9.273 .051e .U144 SDev ftr}LS ,6LQ f}L jv .i}l}']i 1=3 .0 }73 ,0020 S %R*SB 31 .-43 15.90 2648 141.4 3C:1 14. 11, 1x:.64 #1 00310,:017:' 3.6?3 .0P::% - f;rlffi 9.967 :01466 .0115 #P f!1?1 4.54f t r�2{3t 3 . 9.77E C}=59 .01-167 E}- s LC Pas= LC Pass_ N-OCHECI!: LC Pass LC Pass NCCHE K LC F'as=_ High; 5:1--;:cj 300. 50.00 0.01) Eiem qhs B2496 /L,n i tS PPM PPM Av-e .035-3 .0965 SDev Xr'-SD 9.7 4 211? #1 .03-,7 .0,58- #2 .(1320° ,I%P42 Er ors LC Pass NGCHECK High 11-,0.e LOW ----------------- ---------0000103 Tue 8-11-'?2 12 :44:34 AM pane 15 Melbod: CLGE 22mple Mame: W13425-e Operator: TCM Rt!yj Tame: 06 11!9 1=:42:36 Comment: TOWN f3E SOUTHLAND 9219242 07124192 (lD# PW-3) -MATER Mode: C13NC Cvrr. f=acto:': I E l eT #;L S A2 3c Bc CD CA Lnits ppir. ppr. Fpm #I rpm ppm A,ge .lWs99 .00.9 .'x'`}96 .0437 -.0- 7 .0rj0- .95 SLe+: .01%5 .0313 3 .rjiJ� .rir:rj;j ,ririr:;j .001 .41 %RSD 176.6 339.5 111 .3 .000r, .iW100 Iy2.0 .695 rl : :rjy3? =.r}L;;i^ _,rivri� •9.c4 #2 0223 .0334 :s17: 043'7 f3 Ci }7 53.bb Er cr= LC ra_= LC. F'ac= NOCHE-1: L=C. Ea=_a L- F'`_= LC. rass LC High 500.!} it1r' :i .S!. ,uj 4�} 6�} 00 Lei�`.•.) Lc,w -.2 i;ari -.060C.t -.2 0 El CST CR ro cu U'.i is FmTt in pp �n�' rr�'T r :J. rr -r' pr C Avge .L}i:3g .{X5512 ....672 -.01K; -.0013 155. 13 cj]ey ,ijC;t 3 r1r1r,34 :iji�::'j!i .!i!]I` .Ci 3`.36 47. 15 000:+ 10.23 _}1 �i-.� Oo _ 15. 1t #fie (X747 000*12 2676 vi 4b '+_•��- tJ.r?3 !�'�1 '7 ,- ,;-e C Pa=c CO.'as= r a F'as LC Pass LC r G C Fa a=_c L'_ L t' LC N2 . 1 2. 2..}. .i, ::r Ci.s, 40'--' 6;. L�;•1 -7.ai0 LL-..=�W" -.0=-CC -. 1�' C' -.r,:�;arJ -�.fr1trJ } - E l C;Z NI 14- Ti t% u. is ppa pptT: ppi-I pptl ppn prm pPtT Avyes17rJ 7.463 .! .j�s7 -_iirjrvG 12.E .C:!j3i j62 'r �4. 1 0-', .02 /s3D 30.97cb � c;7. 8= Ott 02rt7 7iC �.j423 -.'"30 , � «'00-3� #2 O i 3zl 7.' 23 03Ci'7 i i`;�,: 41 .67 a,13`,i 07 E:-,-c• s LC Pass LC Pas= NOD-ECK LC, Pass LC F'aa LC F'a=: High 50.OC, 3r}i-._C. <?.rt r i ' :,i i liar LQr} r i Elea y 2_2496 Lh.i is pp-M ppt.n Avge .05112 .1035 SDsv 00 10 16 5j :'fRSD 2.060 155.49 #2 .0494 Errors LC Pa_s NOCHECK 1 H i 9 100 0 Lo as -.0200. ------------------------------------------------------ -------------O-9 0 010 4 Tue 03-11-9- 11:46:44 AM Page IS Method: CLP3 Sample Name: CC(14 Operator: T.,,CM Run Time: GO/1114E 11:44:44 Comment: TOWN OF SOUTHLAND 9219242 (171-'24l4E WATER Mode; CONC Corr. Fao for: 1 Eler PL S5 n5 3A Ec LD CA Units PPmPPm PPm PPIT' PPm PP'T ppm ' A%,ge3.046 _,.�+35 1=J:13 3.07: 1.00 3.i 142 =�.6=f SDev 01' .CICS is =+37 .GI? T---9 .25 %';.SD . 1469 .4916 1.429 1.i sS 1 ._9(a 1.281 .98-8+61 #1 3.0315 `. 1 r4 10.26 3.CYF 7 1 .015 q.0l.C..' 5.067- iO.03 , .i:,5 3.020 25.46 Er:-ors SOC F'a=s C Fas_ QC Fas=_ CC Pa_c rr pass CC Pass Q'-- F a.s 17 Fance 1r%_._l.0t<".of,-) _or) 1r;_(_(i Elegy± CR Cu CU FE P3 !!O KN units Ppm PP,n IT., Pp,r. YPm PP" PP.; Fuge ?.046 . .068 '3,0 2 1E.Sa 1r, 1, 8.09 t 2,n., I Si?ev .(icS .01L .03c") . Zi .04 .rj54 ,r.1� V /.RSD .6636 .5958 1 .161- .ca97 .41 Ci 7 .8550 .8766 ' #1 3.C�S4 .(;4 3 3- 1 3- 16.76 10.17 S.139 ?::"}?4 #? 3.027 3.016 3 053 12.60 10.11 $.`K 1 i .999 Errors CC Pass CC Pas_ CC' Pass CC� Pass CC Pas= CC Pass CC Pa_� a1Lte ='.Oc)(t 3 f%�%y ^ ni1(} '•2.`C 10.0 17ti� =.�yY;J ^:an0� 1:i,r0 i( .rfill Icl.Oi nt i (; C} ir'. %'v 10J(+: 10.no, E1 em FSI K S: am NA ,L ( j +-= T I': rnm rrk :( PP,, r'Jir fir.. Ppm PP,r PFm r Avge 3.0-16 204. 1 ...081 2.491 125.23 10.15 3.064 SDe: �7? 2.6 . .tiOE .019 .04. . .is .`J31 %R-SD 2.340 i .272. L%376 .6335 0,461 1 72.4 1 i 3i j9 #1 8.169 P'?5.9 5.0 t .-.Clt` 28.24 i f1.29 3 .GG6. #2 3.027 E02.2 5.082 2.478 26 2-2 10.03 2.10-42 E, =rs CC P-=_s 0C Pass 6!C pass CC CC Pz.s QC Pass CC Pas=_ 1 :'aIi(e 3.10E i 2i)Ct.0 5.0"80 3.G010 27.5:ri11i.(ul d.'ifii Range 1r.')_(](� 1ri rin 10.(.10 iJ.(�C% 1;�%_Oful 1w r;ci 16;.00, 6I er. ?Pi g-2496. Lin its pm m PPm Avge 3.057 5.0u5 SrDe''V .0116 .023 %F-ISD . . 510 4t�6 4' #1 3.(}61' 5.Q11.61 #2 3.0=15 5.029 Errors CC Pass NOCHEC : Range 10.0t% 0000105 Tue 08-11-92 11:49:55 AM page 17 Method: CLFE Sample dame: CCH4 Operator: TCM Run Time: 08111/92 11:46.-55 Comment: CCH Mode: CONC Cc:rr. Factor: 1 E i e: AL SH AS BA ERE CLQ CA Gaits ppf� PPTt Ppm pP!'} ppm PP;tr. ppm AV-e .0113 .%}119 .0173 .0000 .r.00-P -.0027 .04r_ SDzv .C}1 57 .C.11 1 .0 135 ijf}r}n .0000 .C?f11'.-�. .Ct?61 ..RS:.' 133.2 =4.31 73.20 .00001 .!-,;000 47.1 : 14..26. #rt :0007i39 .C} 68 :rJrir,";f! : -.f"OIG .0468 #8 r;226 0196 .0077 C}t;; ,r i2 of n36 .0382 Errors LC F'ass LC F'ass NOCHECK L` pa=s LC Pass LC Pass LC Pass Lo,.i -.PC)Or} -.4)600) -.=f}r.' i -.r}i �il _ ftfl�:j -` 00 1 c 1 L-f•:! CR CPCL'' FE Pi W.G MN is ff., 0Ptr. PF,tr: Ppr.: rpm Pe T! ppm Av9c 9 0 t",'3377 -.00:13 ('4161 -.'124:1 .413{4 .0007 ST:_;; .002P ..1C}C` .rx126 ,r�i' '� .0206 .07154 `01'04 :: 0}RSr, 126. 62.83 ES15.0 36.25 e6.40 46.02 a3 s7 }'?!2 :u 54 -.O 2i t_f:^6 =:C}'35Q ..1443 OICIP1 rsf #2 0033 0021 . -1 C5 ��:4� 0 94 .0225 i}01._ -:-Fors LC Pass LC Fa_s Lr Pa LC Fags LC LC Pass LC Pass }- sigh. O::v;; f.it:J 025 :{ii;l: it. �. C}CiC1 i IJ� Lobi .010 , 1500 0250 .1OrI.f,! E 1e!.!J t i S c AL ?A TT v Gni t` PP' pnf" Ppfm ppm rpm. Pptn ppm Avgt .LtC1C 1 .4162 .f 18 i -.L1Cu f .1631 .:}42$ .ClOptj SDev .GO2P .27132 .0175 .f 021 .O'S46 0458 .0002 1RSD 27.x'1 65 .C6 96.95 3610 55 4 16 r ii C}:�S5 .22x25 i�305 .r:'t 15 .10,33 .t�i 04 001 #2 0 4 f) :j .6!174 r i/5:7j l 014 .2227 .3752 025 Errors LC Pass LC Fass NDCHECK' LC Pas= LC Pa=_ NOCHED:, LC Fass High _i:iii:lj =.1:' l})4`} }I(1Cj _ f.150t- Lobs f (t of-.,;! .fJ li lfi � 0C, jft E1e�:J ZN B_2-:?6 G tit- Ppc: ppm =:vge -.Oi2fti .1130-4 SOev .00-17 .01322 %R:Si D 1441. 43.52 #I .i�C111 ,r}:q7 #2 -.CIO .0121.0, Errors LC Pass NGCH'E&'I High .02,"-10 ----------------------- 0 010 f Tue 06-11-42 11 :53:02 Aid Pace 16 Method,-, CLF'E: SaffiP1J Mame: M13425-9 Operator: TCM Run Time: 08!11192 11 :51:05 Comment: TGWN OF SOLTHLAND 4217242 07/24!92 !I?# PW-37 -WATER Male: CONC Carr. Factor: 1 Ell eff. AL SS ;Ag BA 2E CD CA limit= PPT) pp'B pm PP'" PPTI ppm PPm Av-e .1223 -.l}255 .i'0 .0519 .s: '(v Ci .:+J<i) ^6.904 EE-:, 052f .00,6 . .! '.}117 f_)`}i�;_Y .'JZ+�'.:b .G S XRSD 23.57 32.64 1_39.4 .0100 .0000, 12.87 .5581 n1 .'2`0 _?-iI 0000 0 10.l L? #2 .01 fly !!146 .C3C?P7 x.:519 ,Cie)(�:l ,0054 E-ror= LC Pas= LC 's=_= NGIC^E;CK' LC• F"a=-s LC rase LC Pas= Lr Pas= Low 2 0 - i).600 - `(,(_Q" E e ;-R, C: CLi FE F4 M3 wp Units pper p01 ppl71 PP'; PP3T PPI pP'TY Av g_ -.0032 -.01" 52 .0832 -.0125 040? 11 .24 .s 72 �.D is .0 ii :1ST1 � �i 0 00 .r7 ��RSI'l :t2.43 2(.: 3 v ", 00 1 :� s 031-96 .6, 56 r. c': JO. .41 -.0022 =.0"J 6 :0832 U?3� 00:,70.10 12.23 i"i is #2 .0;341 .0< r4 18?2 _075 Er:-o s LC Pass LC F'a=_= LC -`ass ''_. C F'e.=_= LC Pass LC -ss LC F'�___ High 'SG.;: 3rJ0; "? 2 ?r1.(> �'0)"?,( 4J.��."i 400.0 6(1. 0 Lori -.010CY E1e 5? fd1 C_ AG NA ;_ it L�nits PPm ppY�? Petr. PP:;) PP)n PPT PP" A,rge -.0):341;) 4.323 -.!.0070: -.0 030 e.S.56 -.0065 -.0025 S1 )135 S - ."?0401 .(1(5� - ^�� ev �;� .�4� .,Cf .016 :?1 (J:?"?u s�RS%' 149.7 15 071 189.t< 7;3.71 1830 293.1 15.71 rl JC?1oC 4.7x2 =,1}173 =:�Y�iS 6.845 _.!7?(?1 =.(1 }22 #2 1 Y(01S 3.13 64 i ei 022) (iIY:.•- 8.662 .,C:7i�j 002S i. EEr-1-01-5o:-= LC F'a=_a LC .-=.ss }`•iC�...�-?ECF: Lr_ Pass LC Pass b1�:"t,!-!`r i:` i n�.. Pass High .. -I - , VC. rix` -;f- r> - Low (", fYr'a j0i i)'• r'i (if�r'; .1}51(0(? E?em -2A1 5-2496 U-lits P.nm PPM Avge .01321 .1iC9 SDev ,rY"?03 CRF-: %RSD 1.070 6.072 #1 .0324 .1559 1 #2 .0319 1319 .1699 Errors LC Pass NOCHECik: Low 0200 0000107 ------------------------------------------------------------------------ Tue 08-11-92 11:7:29 AM nzn= lg Method: CLPB Sample Name: N1342'5-10 Operator: TCM +=un Time: 08111/92 11 :55:32 C-omment: TOWN OF SOUTHLAND 921?242 07/24/92 !I0# FIELD R'_ANr- )-iFATER Mode: CONC Corr. Factor: 1 Eleris AL 58 AS BA ec Cs! CA unity ppM ppgj FPm FFM FFm Pt, PPM A,.f e ,0099 -,0157 -.0157 .!,314 .r:r00', _00109 26.33 SLev .-:052 .0167 .O l S3 .CIO 1, .0001", ,CIO l0 .r_ %RSD S 3.06 1 C06.1 1 1 7.0 t 6.1'19 .0000 .0627 .1196.L #1 :rj1S.G =:0035 --JrE-7 :r 32E :r t�00 :Cri ae 26.32 #2 0062 `)275 0266 r�1�=1 r.,;00 10009 26.4r. • High E�r ror=_ LC Pas_ LC pa=ss P:LC�?FCR: LC Pass_ LCF'a=_= LLC Pa=s C":S S`' ..i�;�i () 1(j;i !) 4i01 0, 60.0 Lcv.; -.201tr, -,r)600 -.2 :jr`: -.!,)C�;� E1em. CR C-L" Cu FE FP M3 MJJ z it op: FFjT PFM FFM roar. FFM poM :-V"e -. i057 -.ru)1=+ _,0rt12 .0107 -.i-'' 6.r 9.396 .002.7 '=jY1C ._ 0004 ,001 7 ,0"00ri ,r_}rrlQ ,r:rl7V "D 7.857 1-41 .4 .0000 17 113.1 .89S6 4.714 #i =:r)r;6r =.0GVE�i =:r�0i :1vf2'.y --r)I;zf `.L1a ,;yrs :ri #2 :;i:`s4 .00;A 0012 (K)94 rIn13 $.272 .00-84 E rr or s LC Pass LC Pass LC Pass Lj.. Pass _C Pass LC Pa_s ' C P=ss �'lyh i5r�,rt lrrf,r) 2i: '.Ci 2r 0. 4r.rs,r 4r;r.,i} 6.r],ri.; L�+�! .!)1�ifi fy�f;tyri ,StJi:jrt lturlr: tj:�rj (y1� ; E: ^.1 t--i Units ts pPil! PPjT FPM FFT FF" FFM in Avge -0064 1.111 -.0174 .00010 1u.pr- -.0504 oilX28 .cSLev ,r)r lr 1p .068 ,Oc2I rt :OOr=1 ,07 .0436 .,04-l',24 XRSL 11 .79 6.149 121.1 00100 .6623 86 1 i 8= 8� #1 .0052 1 ,063 0025 .0015 10,75 -.0197 -,001-1 #2 .0069 1.159 -."322 -.oc,15 10.8 -.02410 -.r GU 5 Errors LC Pass LC Pass NOCHECK LC Fa_s LC Pass NOCHECK LC Pass 4!;-h <<.,lirlv 3C-0.0 50.00 4fr:.t 60 nn -5.0it i C l r`U 5.ry;ltri Oy :Or, 7tJ Ee.-2Lgb units FFM FPM Avge .0911 .0:1741 %RSL .37311 ,1412 #1 .0913 .0071 #2 .0900 .0071 Er ror s LC Pass NOCHECK, ' Nigh 02 G000108 Low -.412. :. ---------- j------"r} ------------------- - Tu•e 08-11-72 12:02:21 FM rage 20 Method: CLPB Sample Name: N13425-10 Operator: TCM Run Time: oe/1}/72 12-00:2i- Comment: 2:00:airCGmment: TUWIN' OF SOUTHLAND 9219242 i 37/24 i 42 (F D# I=i L=LD BLAINK)-WATER Mode: CONC Corr. Factor: I \ E I em Al- S8AS B-A B CD CA 1 Unite r^P.n FP^ FPT FP'n PFT PrT npfn Avge -.L!r:4G ,i!r�rlo -.01e4 ,x:3:25: ,r:�rp�o .0041 26.54 ;Dev ,C1?2 .CIQ5, .002q ?000 :x:30(00 .0019 .13 ;:F;SD 194.4 47111 0. 15.ei3 ,;jr3rir: i.r,":Cu-"� [:7.15 .4477 #1 .03 -rJr339 =,1!16=+ -1-1328 .rJr,:0 .f1r)2? 0225; ?6.64 #a <tC'34 .0205 032ei;r.:,:� .00f4 26 45 Er1-or LC Pas_ LC Pass NOCHCCK LC Pass LC Pass LC. Pace !'C F'ae !-IiC:r _(,i: }r,. ter, ;sib �i'� vii! :fr r:4r '-�r1,r� -.rs-rirj -.C;�trlr.' -.r3i_��,.' -.r.v`i! -�,r)QQ E 1 e:, CL C; c P CF: E--. ;.r. � tt,;its PPS oP� Pr` FF^ PFT Prm Pfi"i -.Ci:.i}e .00S2 11090 Kievf:iifl� a 0006L - .'3 1± 1f.--' iDO / !SLs 21.74 9 i.. i,ru�i: 14.21 1? -b ? -53 4.562 #i ,0047 =,r!,!; S =..C!C!18 "jr! •i =:ri,,94 v.2 0 r!Ciq: E!0 5 .00255 -.wie 0047 :?2rJ ti.0755 -0)rj87 Err ore LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 15--.0 100.0 201 .0 2.0,0.0` 4==�a.'.? 400.0 Ar..r.�r L�. ,1 iia,_! i:moi"Sr3 rj``{} 1000 ,04;":C. rjr,i rit�C: EI err 'MI b. 5c ,8G "m p- :,_ v .,i �. nnm nri Pm nm nnm 11-. - P},.n PPm rr F. P Fr rr Avge -:0032 }.352 .C!186 -.006,0 1r. .eq -.0194 ' $del' .0066 42 ,re^. -r1r v .2097 `, r .i r ; ,00 S .3 22e !-E: C!S %--SD 212. : �`5. 122.6 35.3; 2,9/ 297 7 70 71 41 -.r7rv1S`! i .-574 .C,0 2 -,0,1074 10,91 -.C!6!,4 -.0G,1, #2 .'?v1: I . 1}145 irs.8c .0211 -.i,.,i E:rors LC Pass LC Pas= NOCHECK LC Pass LC Pass N0CPECi:; LC Pass Hi g` ..50.03 40 !,0 61.rJ:- EI em_ 7ij 8_2476 U-i FPT Fr Tr A/ge .ogie .!.165 SDev .0014 ,0?01--) ' :SRSD 1 .54!,: .1 32 #1 .C!9?B ,i?1b5 #2 .C!90,e .0165 E rors LC Pass MOCHECK High 1(,c1.0 L -.02rlo 0000200 Tue 8-11-9E 12:11:36 FM page 21 Method: CLPE Sample Mamo- NI3412-1 Ogre-:.tar= TCM Run Tice: 08!11%92 12:09:39 Comment: TOWN OE SGOTHL AN'D 931924-0 07/24/92 ID# MW-1S $L'1 WATER Made: CONC COrr. Factor: 1 Elem AL Sp E+ E'E r� C^ hili t=_ ppm ppr ppm. FI" . Fr- FFA FFA" A,.ge i.19:j .012 .4yi!32 .O7 i 9 .+ tr.,;, .0045 6.802 SDcV .0012 ,fu)ryrj ,0,14� .x,000 .0000 .00-100 .010 7.r SL+ .1461 .0274 4=A.r! ,00(",Ja 000 .Ov,77 .14$3 #1 i 1. .0125 -.r!(DI - :05i9 Ok011-)� .004-56.815 #_ 1 , 1r�8 (J 125 .Gri'34 :)�i9 iv�:�i .0045 6.2�s1 E:rags LC Free LC Pass NOCHC-r-` L:: F'a_ LC Pass LC Pass LC F•a_ v: 1 F ` High .Ir: ) :r�, f! y t j 4i).(_0 .�,50. ! 1 efi CF. CO Cu =E PB 1�3 Mt: tlrS: "pfn pG;Ti Df" nr.n nn)" nr.�n -�nr rr+ p rr rr rr i�r Al:ge .0117 .0132` .0100 2.831 .+�r) 4 c'64: 27=) 1 De ,Ov 18 �(y03 ;Of-,0 ! ...:!1 c - .0246 .046 %RSD 15.29 i4; � i)ir?'t �4��9 `98;' .E?6r} .b249 #1 :r)s;j4 •ry000 :0iOR 2.2420170. v:`3i . 3�•-•5 o 'tEE U 129 ,0049 !)Jncy 2.$2i) !17S � a�7 3=56 EF-ors LC Pass LC Pass LC Fass LC Pass LC F`ass LC F'ass LC. Pass_ Nigh 15Cy.fy iLtr! sl ?;<<3}.i `!C!.(1 40 .:') �:Ut!.C) Lrj �)s; L K -.01:!'-' -.til.:) >! -.025:! -. 1n!)7) - fii�f)i) -5.f.)l}!! - r)15r! El em, NI K Sc F$ NA TL it Units PPM pp"" pPr" Fp n FF'" Ppm ppm Avye .C)334 1.9 6 .0399 ) A1C 22.9 ( �:4 SOe> .O1Cj5 . :1i .0086- ,r 00t) ,15 .0i I? .00:: r) %RSI 31 .43 36.66 22-03 000c) .6667 1$; 6 47 114 #1 :02.60 1.440; -,0461 -. CfC+15 '3 2 .03 -. 0146 :r ;}?, #-2 €?4E;; 2 46 3 .0337 ji 1 C7 `3 Ai 00E Error= LC F'a=-_ LC Pass NOCHECK LC Pass LC Pa=_s NOCHECK LC Pass N-1: X0.00, 3rvr!.G 5r:.0 400.0 TJ.vr, L t•! Ei4r, , �.rJL ) .01 clu -5.000 r)�t!CJ Eleni 2� E_2496 Ul; t� ppfrI pp- Avg� .0336 .0662 SDe•: .0014 .0,+J 6.6 %RSE) r:6� 9.$92 1 .c)342 .0621 #2 .0,329 .0711: Erre:-=- LC Pass NOCHECK ' High 10.0.C. Low -.0200 --------------------------------------------------------------- ------- 0000110 ' -1c 08-11-92 12:16:15 PM pope 22 Method: CLP3 Sample Narne: ?,13412-E Operator: TCM Run. Time: 06/11/92 12: 14:18 Comment: TGUIN OF SOUTHLAND 4219242 07/24/92 1 ID# M.W-75-GW) -WATER Mule: CONC Corr. Factor: 1 E l e^? YL =B AS E+A uE Cr- CA :+�:-,its pp` pprn pprn ppm ppf: FFm Fprn Avge '2382 -.1,W4!1 -.: 898 .051 :(';;AL? .0018 14.28 041 (100")SDev .025rJ .r�SL (100") CROWr,rj 13 OL %R3D 17.61 60.81 0013.1 ,z:000 ,r_000 70.74- .2986 1 #i :2!?8b .0009 'j,7J=,i 5(}27 14=25 2679 �{- =234 03 19 .OC;�? 9 1 2 1 Er =rc LC F'asc LC Pass wICCHEC : LC. Pass LC Pas LC Pass LC ;:a=_ HiC` r?`�f,�i,(r 1 ur �!? r':r._i laai.(.? 60.00 45; .D Love -.C;(JSJ E1e CR C1 CL- FE FE? Mf; MT Urate ppM FFM rp:r. ppm ,p:r. pp+': pF:n P.vge -.t?;t-'9 -.00K -_f;000 .4?555 -.'�f1'75 3.C•S8 .13`5 SD-zv .0.036 .0070 .0(177 ,rt`?G` ,Ai=f .r'CS .rif?iQ %RED 377.1 212. 1 1649e.c 1.Sb3' 8-6.63 9124 1 .361 #1 ?016 = ?�?16 -0(15 ! .4-890 -. 0066 3.(169 1334_ #2 .")8.35 .C?08,2 f IJ s? .5:121 t X222 3.i 6 13 2 LC Pass LC Pz== LC Pas= LC Pas_ LC Pass LC Pass LL F'= High 150.0 1i,O.0 20,0:.0 200.0 40-i.0 400. 6(?.0. L �t r,1 rv.r, .05(^�� .il`5t J . 100 i ,i 1400 -5.Q!OO .r)l 5rl Eleni NI r SE iii NA TL v U:ii t= pp pp FFM pFM pp:" ppM ppM P.vge -_(i,i3? 2.8,1? -.0207 .0103<1 14.24 ?; 00213 1.503 .(?ra`Sr .006 .02 .01:41 .0,04(' %RSD 70':.71 5-3-44 32.25 212.1 -1 1270 1711.5 11 .4 #1 -.CDC)4c 3.864 -.C12 ?5 -.0?r.?15 ? 12 .Cir r2 -.0016 1.739 -.0321 .00!74 14.23 .0029 -.0056 Errors LC Pass LC Pass NOCHECK LC Pa=-_ LC Pas=_ NJC;HEC�' LC Pass H=Sh SCi.C;,'r 3riri.r' 50i.7Jt? 4-30.0 6/x.00? L01.1i ilir"if1 -� r ii jt? -.0100 r;t1(} _:�5r}j E l e:r. B-2494-- Units _2496Units Pp-TI ppm r:vge .0192 ,0993 %RSD 29.38 9.996 1 .0p4c .1063 #2 .0139 .0923 Errors LC Pass NOCHECK High 100.() Low -.0200 ________0000111 Tue Cj6-i1-92 12:21:02 FM page 23- Method: 3Method: CLPB Sample Name- N13412-3 Operator: TCM Run Time: 08/11/92 12:19:05 Comment: TOWN OF SOUTH AN92'9242 1)7/24/92 ! Tut 08-11-92 12:27:00 PM page 24 Method: ELPE•t Sa;Tsple Pdatne: N13412-4 Operator: TCM Run Time: C}8.11 i 42 12:25:02 Comment: TOWN OF EWTHLAND 4214242 O 24I92 (I D# MW-7D-GW) -6P,TER !`code: CONC Corr. F_mctor: 1 E,em AL SB AS PA E` CD CA Units Frm Pira fl. Fpm pptn pp;n Fpm Avge .252-0 -.0136 -.:�1�2 .L'3E3 .i; rii: .��Ci63 9.323 S1e.; .0140 .0194 -022c .nr;.i r; ,1-1,3,00 .13:00 . -1 7..^SD 5.42;) 142'.9 146.2 .GOOD} i r00 i .oc .1170 r 2481 :6`J 1 -.0309 .0323 :C}Lit„�} :0063 ?.3 i b ` #2 _679 1;273 O :-15 i�';Cui 0Cv3 9.331 E.rocs LC Pas=- LC pass ;10CHEC : Lr` Pass L C Pass La C Pss LC Pass !)ich 5010.f) r7?j.fl �:` 7}n1it't 00 6_}.00 45; Low -.Co7!i.i - i,l :tf1(i - t f)`C, -. =0 -c.fes',!(_' ' EIem CR_- co CU = P3 MG ^;;e Lhil ._ ppm Pt`m FPm pP n ��:r. m pD rP;n rp Av-e .(}032 -.00GE .0063 .5354 .Ct334. 4.67` .034-1 1 SD,ev .0013oCiS_ .0 13 :1`RD,15 .U! 14 .r10:54 .CIOC)6 %RSD 35.3 136 6 7 .8 20.20 276_5 34: 1'13 1.151 ' #1 .0047 003 .01072 :5344 :04144.6= ..1.7 r;33C 0:05 . 4 5365 2;54 4.7'3 03L5 Lrror= LC Pass LC P=E= LC Pass LC Past LC Pass LC Pass LC Pas_ HJ.9i5:0.0 100.(! 2C-40.0, 200.0 i-0 i:+ 400.C. 60.00 E 1 err, NI E= PC- NA Units Ppm PPtn ppfl', ppm r".pr". pPt: Avge .0069 1 .328 -.0379 .0`0,00 70.53 -.0059 .C3ix-6 ' SDev .006:) .034 .rt1V: Tue 08-11-92 13.39:37 PM page 25 Method: CLF'N Sample Name: CCV'5 Operato • TCS ' Fut: Time: Oe 11!92 12:27:26 Comment: Mode: CONC Corr. Factor: 1 ale+^ cL 5B AS `1 8E CD CA Units pp;n pp;n PPm PI'l Prm PPm PPT Avg e 2-95 4.931 9.832 2.971 .4733 2.964 24.61 EDe-.; 000 .000 J55 ji 9i .0010 . 7jn .06 XFSD .0006 .1,87 .`-�4C .6 05 .1026 2590 .2360 1 #1 2.915 4.937 9.79Y2.955 .9725 2.9 7C, 2-4.57 }`? 2.915 =i.925 9.8+.71 2.92- ,^y740 24.65 ' E-rare C~ Pa_s CC Pas=- CC Fa=_=_ CC" Pass CC Pass Q F3aa CC Pas= l:aj: o 3.000? tirtif 1Cy, 1{ C!CFO I ii�:r: ?.t CiG 25.UC: F:=:'g1J.00 i0.0C! lit.''r.'� irjrjCi Iij.00 i0.i1t1 ' El� ,�, CF Co C1-► F PP MG tot! U::its P.- PP'n Pim Pr�T PPm Prm Prm Avge 2.916 2.907 2.97:' 12.21 9.731 7.231 1.94.: SDev .:)ilLt iJ2 .iJJ3 .7!3 .053 ,061 ,ili`1i� %FSD .1376 .08Ct1 .i e60 .23354 .5447 .6srj2- .021 1 =:913 c.9C?9 2.975 12.1'? 9.758 7.`"38 1.942 '-#'2 2.919 2.91?=. 2 2?9 12.23 9.6 i=-: 7.P'7:z ; .9i_3 Errors CC F'ass CC Pass CC Pass CC Pass CC Pas= QC F°ass +CC Pas= i V u- 3,rif`i CP,-1 �,iir iii : , Irl.C?!} 7 5611 ` ii F?iige iil,i'iij I'l 01+ 1-0,1 i0.00 1+J.rii1 10 .00 l�J.r;i7 Ulnits PP'n PPm PPS" PP+T PPR Pr+� PPm A:g2.922 195.4 4.9 4 2.946 27.54 9.925 2.939 'lraSi: :•8g i .52433 .6727 142? .2126 1.030 31;j2 41 2,913 194.7 4.-77 2,949 P7,F8 10,06 2.93 #2 2.932 ?95.2 4.93.1 2.9 3 27.50 9.912 2.945 E:r or s CC Pass GC Pass CIC F'a=_s CC Paca GC pass CC Pass CC Pas_ Value 3.;:(1Cti 2Cici.: -.Cif!:! 3.C.-j- 27.50 11;,1;1_ v.r�C? Fatiye Il 0. iC? 110 1j?.rjii 1;:, rjfi Iri,:'}r! 1,_.00 tri cif; �t e= D. B2496 Units ppm PP's Avge 2.955 4.696 aGov .Ci_a .ri2.- %RSD . 1166 .5391 1 2.953 4.87'' }#2 2.958 4.911 -Tors QC Pass NOCHEICk. Value 3.000 Range 10'.00 0000114 Tale 0 -I1-9c 1-0:31:39 Pat page Lc Method: CLPB Sample Name: CCE�5 Operator: TCM Run Time: 08111!92 #2:24:3? Comment• CCB Made: CON!C Corr. Factor: 1 G_ Se AS BA B> CD t!zi is PPIR ppm Ppm pp'n pp ppm pp' Avge .009-i 0039 .0166 .0027 -0-D02 :Of,)1=-: r�2:3 SDev .L!2-'5 0000 0048 .000,,,--) 01000 C1032 rlrjLr'? .0163 229.33 .(iVU .Li:i-1)0 '2'35.6 1-1..733 AA � I !f I -.0092 .+_ii?3 f i�: )r _: -27#S 02Cr Lv C .2 .0036 f302 ' Cr o = LC Pass LC ='as N+CCHECt= L C Pas= LC Pas LC Pass LC Pas ti c .200f, .06ri0 (JLi,`} f r;c' f'`5s fJ'. LOW -.Eel'.-i -.r IE11= Cit C C+3 Ft P-ID MN Un i is pprn ppin ppm _ pp-In P .nPp a-;T A-vge0002 .00)2�.i SDev .0 ;5 ,r>012 r,-110 g O)O;:tit r:lith fi+1 .6.1`7 , _ . . L-c `'ARSD 138'? 40.41 127.1 . 4-2741 %rj iB 37.`:i .88 1 i �s Sc =r:1_� 61 ?20 #-2 .OOD2 i 0037 0003 10,082 Frs LC Pas= LC Pa== LC Pas= LC Pas= LC Pasa LC F'a�_a Lr Fa_= � .0-101 .L-.s ii2`t .1ci_r r o_ � r��: .rJiJ=; LC+i�! .C}1(�+: .0500 ,ft;�Jrl . 1 5 )rl .043 5.00-11) .:?1WA Elem NI K, SC Ti- v t:t=``- p PP-!M Pp:r ppii pptn Pr^"' pprn Avge .X067 .5 6= .0213 }Lri=} .179'2 .0291 )'?J S'De- .0i 05 1 . 127, .0-578 i`)I�Ti�2 v 061 %RED 121 .4 2-019.9 2-5.4 294.4 #t)7.6 96.Be #, .0161 -.2601 -.0191 -.001 ' K s u,)12 1.33 4 .0627 .:%i:=i- .i 355 .r i5 i C .007 Er r o r s LC Fa=_=_ LC S=ass' "iOCHECI: LC Pass LIZ Pav= NOCECK ? �� p°== �i�c. _ Hig`; O'LO 5.::)fk% -�10C-1 5.0➢� tr -fSJiJ Low x!400 -5.i?tic! _fJ1':iL ,Ci?ii!0 J... ' EIem �„ B_219cs L;zi is pprrl pp;r. fi}vge -.III-)i3 .0163 SDev _r fa07 .0066 `_.RSB 51 .48 4-:1.42 #I -.C+:I+3 .0210! #2 -.00019 .0117 Errors LC Pass N01C�±E+�� High .0200 Lc'`Y -0-00`? 0 0 0 0115 Tue 08-11-9c 12:33:58 FM page 27 ' Method: CL P`$ Sample Name: CRIF Operator: TCM Run Time: C?8111192 12:36:52 Comment: CRDL X2 Mode: CONN Corr. Faztor: i Eleni AL S3 nS 2=. 2E CD C U n i is PPm pp;:: ppm pp,• Ppm ppm rPrr. ' vye -.C:i61 ,- .0129 .000?U ., i02 .00e6 -.0251 ��ev .O3v .�j 111 .f]iiuu r:0)C}U .('}!11(0!1 t}t�37 .-316 1sF+SC 228.5 8 342.7 .u,010 0 .0000 L.4.6s 6.426 #E -.0420, .104313 .0443 ;c i f i .o l r)6 .0113 -.0263-5 }t2 fUY? .1256 .Li i 84 .{JU'?' .0108 i�:i f52 f-24fj Er' ors LC Pass LC Pass NOCHE K aLC.F'a L C PassLC Pass 5:0 High 0.0 l 00 0sri"}, 0 4± 0060.40c; C% .%. L ovs -.2000 -,i_}6r}fj -.2 }t t!_1 '.1)10 :sem -.0050 051) E CR co CC F- „� e,,`y Units rPT PPsn Prm. PPT PFT FPm P=`" A,:•7e .02':)5 1029 .0543 -.!?1,37 . 1C .C)2_99 .C?r9a SDe'i ,r�r}2` ',C}s j3 .L?,J64 _OL)1 1 .L?ri."�.,3 .'1 �1 .0002 lF:Si1 1=x.88 394 11.79 It .44 2.e!,-',3 �i.8` .7iis,_}1 #: :C?22I :1ri�4 :05L8 _.0?T 1J : 137^ 3 --02 3 C ., 271 0 53 2 0294 C: or �a - Pass G : cc r Pass L C Pa �ro. LCF �, a_� LC Fess LC a=s L F`a__ L.. �=s �� Hick, 15:).0 1:.J}.! Pilo.L' -00.0 L'f C, l±ijU.L? 6<<. }U c-.- c c- L uV) -.01 0 -.,!500 J2 -.li,, "r -.LSaiIU -J.rli -.r_!1 ' _IeT tai? %: SE tic NA TL v U:-:i t s ppm Purr. rp:r: PPm PPr" PQ,m. Ppm .0?`836 -.0242 -.C)i36 .0179 -.1 -57 .�r:}85 ._026 v1 •fS`! c .47/823 %'} ,r}f}ilii . rv.3c .�:C..3.Q :1020 Le`! 1101J.. C.. .0 `L ;:RSO 12.53 198,-'i. 25.73 .O(:iLj0 2:3.97 33=+ 7 #1 .0913 .3140 -.0161 .0179 -.11-7 . I040 ' # .0764 -.36:3 -.!J?ii fi179 -. 1587 -.0419 .1:)12 Errors LC Pass LC Pass NOCHECss Pass !' L iJh, 50.00 300.0 5'-l.,iU u_}L?.Q 6L;,00 Lo vi .04,',1) Eleni D4 B2496 Uri iis pp:n ppr.: PYge .0424 ,0023 SDev .0130?7 .r 033 ' %RSD 1.624 140.6 #1 .0419 .01 fu4^ ' #2 .0,4p? .000o Er r c r s LC Pass t'OCHEC K 'nigh 100.0 L_w, -0-PO,L) 000011G Tue 08-11-92 12:43:38 PM page 28 ' Method: CLF'B Sample hare: ICSAF Operator: TCM Faun Time: 06/11/92 12:41:25 Comment: Mode: CONC Ccrr.. Eac l,-3r: i E?e+: AL 5B «..S BA 2:E Cry CA Uni is pps': pp:r. ppfft pp:n pprr. ppm PPIM Ave 531.4 .1336 2.775 .0082►82 .cls s p _,sit 13 46a.6 SDe:, t 5.0086 .t Xcit jCj 74 , 0 ,r i;03 .0013 i q %RSB .3492 6.39.3 2.674 .iK"00 141.4 11.32 .40a7 ' #1 53s0. 1 . 12_76 2c.827 ;082 r C'0 -.iJ15 4.4.7.;3 #2 5 2.7 .13.. x.722 .:1 :�2 .s 0.00 -.�i1u4 464.7 ' `Efa' lr_oers QC F. 'a� r 0 C htv: PG IL-.ECk. ft!n E CtI�CHE k, Ln Pass I- 4- s=I- 494.f*. El ez.- C^: CL 4`RL MIN I 1 r n nn in r.Tm nnm Ln s pps� FF PPT, _ Pr rr!° P ° rr :Avco .2;142 . 1sv2f" "?7. :8i. t .-?tea 4?7.. .��27' ' SDev .CIO 13 .00 i 4 ,001 3 .6 .0541 2.2 .00i-1:z SE, 9.428 16.96 3.923 .-42('11 7.646 .4382 1 .407 #1 0 i C5 O'.iq i -.0335 156.5 5 2 56 49.6.J 020-2 ii2 .."P132 s.�11` i �i '87.1 4717 499.4 `-294 hOCHED,' N 0 C -C +C = N HE C -•- H� F: [ F'ae•- .SGC. 0.. tee- :•l3CHEC�: Val .�2 2'�16.2 531.4 1 E1er h: K, SE As hi. TL lin=+= Ppm PP!r PpPPm prm prm ppr I.. ,• v{ ,. C1.� } � r.v-e s106 -.3364 -.3-235 -,:>164' ..�� 6 .1371 .C�+181 SDev .0150) .4440 `3 .Ct2= : 11; C '8.. rJ J-l•j t�.i..lam :SSB 141 4 131 3 ry a� =:'.8=� 7 Je: 336.:6 9 753 #i 01")001 -�652 -�2C3J - '.11 79 1 .L•11 I - f I., .0076- n #2 r)01 2 t}2 384' 0149 1 .626 1036 rJ 76 Errors hOCILECF:: NOCHECK 1113Ci ECKi•10CH'-:r-k: N13CHECK NOCHECE: hOCHEC F_ Value F:anee- E l efv; Zh B_2496 units pp+a pprr: Avge .2136 .C,_•16 ' SLzV ,2x135 .0011 %RS'? 1.77+4 S.qPf", #1 .2i09 ' 42 .2162 .022 e Er s NOCHED.- hCCHECF.: va 1 L;e Rance 0000117 T.:e C13-i1-Q2 12:45:4:5 PM pane E- Method: .CLP8 Sample Name: ?C'3AHP CRe:-atc:r: TCM ' Run Time: 08/11/92 12:43:4:5 Comment: Made. CD-NC Carr. Facts:-. 1 Elen A5 B= BE C01 CA RR1 PR rF� Rr Ram ' QV £ 503.6 .14�^ ^ It rte(! �u ri: 44� r� 2.61-9 .4y_ 6c: .9 _7 �.1 SDev 2.2 .x=1442 .011 .003? .0017 00-38 1 .6 :AEA .4303 41.83 .4102�2 78�? #1 505.1 t17:1 ai 2.615 7 `!. .9 .46674u.�J.^, ##2 502.1 . L'361? 2.6.41 .=18 Q3 .4644 .8 x'90 ' Errors CC Fuse N01C14ECI NOCHEC"' CC Pies {CSC Fas s CC Pass v QC Pass fla1ue 50ErJ uAr:rlGr•71:+ X12.? !^:a'.-q-e -20.00 `t?-`il ,. }rJ sI).Ci', 30. trl E I em CR r;n. CU FE PB ?u MIN Un pRm p�{T r.n�+ rr-:T"?` �.r:3: . pr:r, Avge .49'37 .=-:437 .4537 177.6 5.r,29 472.1 ."' e23 SL1ev .0045 .00,?3 :0026 v .6 .026 .Cir i21 `.6,r't`�D 3939 2.`_``+79 5579 3 32 .221 r .4416 4 - #i .5;1i a :4�r3 : =:,Ar 173, .448 472.5 .48'37 #2 . 4?56 4371 4569 177. -0 1 471.6- .4808 ' Errors LC Pas= CC F'a5-= i��C Fas CC Fa=_s C Pass OC Pass C;. Pass Value 5290 477x., .s4 3c} i 99'.E 4.724 `27.` 4?60 F:aiige 20.0ll PCI.r:? cD.;�0 20,.00 2G.r}C1 20.00 24.1171C ' Ele.m N3_ k: St 11A TL v Ur.z isRRm RR'i P--fnRRm RRm RR:T pp! F?rg_ -6618 -_ .497 -.3.1,44 .4454 1 .=35 .1960 ,4264 ' SDev 1.567 4 3`• 1.=64 + .r}3i 17 :0 }6L` .�1L3 .0{ .7 .. 1 r. 7}f}Cau %RSr1 • .567 e4.40 I C}.C7 6681 1 .Sd6 9.C 44 6 r71 ' 41 :3522 -,6036 -.3261 .?49, i.45 ,g:1 #3 37 i.^-• 3?1 2327 .4 4 1 r01 1 419 =r3$5 4829 E:-.-o s LC Pa hi0 Ct: NOCH C�: CC F`a NC%C! ECS: tdCCHECk; 0; Pass Value -9-104--1 96 0ua Range 14.ru01 .: .Sr,r• 4� _•,3-;it ' Elern N B_2496 Units pptr. Rom. avge ' SDev .414 .04i:�6 :.^Su 1 145 ? q?^ #1 1 .213 .r.^r ' #2 1.193 .02i1 Errors OC Pass NOCHEC K' VaIue : .206 M-ngle `r} CM-1 0000118 T+ue 08-11-92 12:48:27 PM pace tri ' Method: CLFE Sample Name: ICSAF Operator: TCM Run Time: 08/11/92 12:46:2= C:rr!'rent: 1 .5 BI_ Mode: CONC Carr. Factclr. 1 AL Sp. f`c DA 14.;: CD i� _.. G IT iT r� iP, ^r ^T: !nit ppi=: prs7: p. pF rp Pr-'++ pri pv e i ice.i i2 .� 69 ,601? - 0027 :1;11;:1 -.0:i1B 1C1- SDev ,17 1; T:le :18-11-92 12:50:48 F i page 31 ,�. fJay� Method: CLFB Sample Name: ICSABF operator: TCM i Run Time: 06/11/9? i2:48:4q Comment: 1 :5 n rL Mode: C<<NC Corr. Factor: 1 ' E i em AL Sp AS BA 2E Cis co- Un i AUni is ppn ^rpm pptr pF•'1 ppm pprF pprf SP,ev 1 Q (13:z;03 -11 Q7 i000 f'l ) ii In; 1 :SRSI; 1. 179 :6.46 3.557 008 2.357 1 .071 #1 f 1(J:5 .03579 �t9813 .1366 i 02.S Y2 1 f 2 .01'19 47 .19?2 14.1 ' Error_ LC PE._s LC Fa=-s N0C±4ECrk:: LC Pass LC Pass LC F's._s LC Pass Hi 50-,--1. FL F`r. N;� Lh i i- ppTt pr Apr pp:T l FCIT! r n t3� _ Cw7Q .. , - - .. ill :7 .3-,-• _n ;fie, )0!^ CIO1 r,"rrv� L:� 1104 ! .4 %R'SD _.297 1 .2 1 E. .0C-1C)0 1 .C-89 3=3 1 c7(i . 1013 .��.ii. 42 104:' ( ?63 i f;.�.8 ' Error=_ LC Pass LC Fass LC Pass LC Pass LC Pass LC Pass00LCPr - Hi 1501.!1 S41' ,e: �`7f1 !!' 00 4,'0 6 4 . . 60.00 Lc-,,j -,.iirl(j -,ri5(�r; -.:'2�iJ - (,r}r,, - r: •('ti(? _c E1em NI K SE CC Air^ i - TL _nits pp,l pt, pp'' pp' pets ppin pp,r Aw-e .1948 -1.25- -.0995 .1951-- .?c77 .01718 .1u��1 SDe: .0218 .512 .c%129 .C)r?2i .ri12J ,r14S9 %sRJD '11 .117 40.79 1"'�' G�J 080 5.714 Li f' `• 6 -•7 r(I(`•i 1 ' #1 .1794 =1.61$ _:X1904- . 1330 :c369 .1:119 .too #2 .21:11 .8936 iC86 .1965 21 L5 .+i408 . f r LC Pass LC Pa==_ NOC-iED"' LC F•ass LC Pass NOCH.cCK LC Pass Hi : c. .C� rJ: rL:. ,s.`jiJ;5 6-;. 1, 1rJ,i1 L ` i`I ' Elet?1 Lf•i P :2496 Units pp'-49 pp:Tt Fvge .260'-L. .0Q177 SDe- 00-28 0073 "Rcz- ii. -V #i .2566 ,rijGa #2 .2625 E1 r c:rs LC Pass NOCHECK ' High 1 X11.0 Low 0200 00001L 0 T zs C)8-1 i-Q2 12:52:59 FM rage 32 Method: CLF'8 Sample Name: CCV6 aper *or: TCM ' Run Time: +68/11/92 12:50:52 Coms?ell t Mr-:de: CONC CCr. . F"---tor: 1 Elegyt AL SB AS ECD CA Unit psr'T pp" T r nn Fps.. pps.. r�sT. pp t pp:r. Avge 3.0'2 5.041 9.92'8 3.022 2.991 2`.07 ' SDev . .004 .025 ,c 05 ,f 06 .r)060 ,022 V .cis :;RSDi 1135 .4956 485 .1919 .6058 .7%273 .3 }29 �y J .tEl.. O1C -.443 -2.9,76 i5.r}2 #2 S.01-F-0 5.05r-2 7.934 3.-02-6 492S 3.006 ?C. 12 Errors CC Pas_ OC ! a== Cc Pass OC F'a=_e ..+CPass or pass t?L- F'a= Val vie 3f:j .tam 95 f i00 i f.f �� ^" .: -i�} i ,�'�ily i:• (70C. `�; 2'fg� ljt.4`_' i0.."!0 i!.-�'.fJ 11 i0.fli_ { CC i U nt-i t s pprrPp*s p'nn !'p';., Yps ppt-' [p,, u.. C76 C-6� ge- -• - -.0331 12.--' . .9r6 7.4c-::; 1,974 %PSE; 3146 .3337 4213 . 174-17 .3=•.32 .3 i91 .2`77 ' #1 7.2.r970 2,g-;:;g-;:; .028 jpa3 9.903 -7.v.7v !j #2 E .!S3 2.973- 3.[}L-:. •2.Lc6 C.92-5lent 1.977 Err�� C� Pass %;- Pass CC Pass L� Pass �C CC Pass Lr;. -- va l ue 3.f'if ji'i 3.000 3.000 10.CL! j 0.rw�f 7.54-10 2.GOO pant e 10.;n In.i r1r, 1 ,0 0 Eiem Ni K Sc A6 `A TL v tlni is ppm ppmppm ppm pp^ pp T, ppm. Avge 2.947 19?.3 4.991 3.!}c1 x/.73 1�'.;is 2.925 02" .6 .0j J .0i5 .06 10 .013 t��.C.� 16l 2-� Sf L'Lt-t`lv CYct � C: ,,:;,,L 9 .3 :� .2 j{-3 1 .i:13 382 #1 2,928 198.2 4.98: 3.0I1 2?_69 4',?37 0^ ' ##2 2.96.6 197.8 4.x.+98 3.031 2"7.7; 10.0L7. 2.9=4 Errors QC Pass CC Fas= CC Pass QC Pass LC Pass CC F'as=_ GC FEE=- V a'ue S.0 }i} `t_ta;-,l j .FWc) .006 t `" -r,r f f}.0- r F: 3 3}fji a-11ge 1:} ;0 1,} :;C} jrt,�j:) fti.f30 ' E l em Z-Ae $_2496 Units p :n ppm Avge 3.024 5. }13 SDev x,108 .f?13 .2576 .2634 5. 1:)3 ' #2 3.027 E rocs 00 Pass NQCHEC;,: Value 3,000 Range 10.00 0000121 TiUe rie-11- +3 1 :56:ri3 FM page 33 Method: CLFB Sample Mame: CCB6 Operater: TCri Run Time: 08/11/92 12:53:08 Comment: CCB Mode: CIONC Corr. Fac tDr: - E}e; AL SE! AS B;; .E Cn CA units ppfr. pprr, pprT PPn Ppm PP" PPfq g= .1J6C?ri ,CrLi3c' .0::12 .01%27 n4-AE .0023 .ii553 cDer .' = . " .()137 :J r.? 4'J 135, i?1 ?b .r�rj3�Y ?�lDO ,I045 r ,sr'.�L: -3.31 9tj? 4if �f+! 198.C. 24.82 25.7? i 4 t .`F �'"'` 0314 rt Ej7 -0-- :x002 ,i,00,? .1J455 ' Errors LC Pass LC Pass NOCHEC!": LC Fa=_=_ LC Pass LC Pas `r Pass High 20jL?ii 0600 : i r c. L"'! -.fi6i30 _.2000 -.+.r'Oci� ' E 1 er: .R Cr CL a: FE F'3 + i Iii! PP;T7 pr.m. Lp'r pr(T P(-('? PPT, pp"ll Y'. �f ge -.0011 .G�. .] -.rf:+1 .t.1c43 .moi.l;.if Kiev G 041-11 RE i.l ff_:r) .)O-Z70010E 'I.F:S:B 53.47 i l i_.01i i5. 1 i 65 21:7.5 E� 2B r?rjr?i: r,ii?G '.2 !1017 0057 -.0217 E r�54 .t11 1� f)`Sri I Erre-•rs LC Pass LC Fa__ LC Pass LC Pass LC a=a LC Fess LC Pass_ {i5tiC-1i?; 5,i.;jir Lam:•: .Cij�ji .'j`(0,? -.�? r3 -. irj ?r,' -. :u l -5..?r.'O _.r5��ri ' E 1 em N I K SE c iWA TL 4 l!n:t s ppm pp:llpprip pplrPRM pp!r ppm Avge .OID26 -.592-2 -.02;4 -.0045 ,J--n SD-2v SD-2 00677 .2732- .0173 !.'ir_rL2 .Ll22E N-10C, fr;J11) 239.7 45.62 Sd.C1 '3.; '6•?.- ['c'ivi'l ' #1 0076 7` 14 -,0067 =: j�7 ?te.-j .. % , #m 0�2' 4 j�"j i34C �; +� :j 4�� itB7 � .%3=: Errors LC Pas_ LC Pass NOCHEC.. LC Pass LC Paas NOCHECK LSC Pa=s -1i �i17 crl arf - �-1 �tUJ ��ivtl(; Hier .4: .r. Ci ro riri r rin �- + r`;i.r -5l+`j L`J Y. +y�i�i t)!:J ii lir) c ��j un,i t ppm pprr. Avge -.0-00116 .06,93 SDev .r ir);13 .0099 ' Y..F:SD 56.21 :1:,4.1 Er:-ors LC Fass NGCHECK H+y}i .020 j Low 1)P.". 0000122 1 NYTEST ENVIRONMENTAL INC. FURNACE ANALYSIS RUN LOG AN?.LYST: Y FYI II:7iE,T1' �S 4T I01 1"2 ��I yr n 3o3a — ' DATE: CALIBRAT-LON DATE: g//0 l/ 92 LOG LN, R's: 3 � y START TIME: �' 1 - END Ill,E: IN i cGRA11ON TIME: �• Y ' .. - ` 7r.RDS �• Snex S,AN-DARD SOURCE: S T ANN ARD LOT T . 2 A5 ST,,`+-DARD PREP.yRAT1ON D.=.T_. 9 /10192 STANT ARD F.kPI^�ATiO\ DATE: �30 !93 I ' ST.-\DARD PREFAB-.TiO\ LOCBGOK PAGE =: CLQ �wll) t L E vA�i= ACCE �\1Cr LIvtITS I CO�IttE\'TS :.QC SA: IPL I • jcv ' ICB I < H-) CRQL I { CCV - I - 90 CCB ( < (+!-) CRQL ' LCS ) SO-120 or E?A Ll-,11-1 S I { PREPARATION BLANK I <(=H CRW I { DUPLIC.-\ - SPI,—E. REVIEWED BY: 0000123 1 A"9r 1o, 1992 VIY�� b. PrtR T�r�t 1 As ' AA ZAA DC PEAK HEIGHT (ADSOPPANCE) 0. 027 0. 028 0. 01" PEAK AREA (ADS-SECONDS) 0. 017 0. 007 0 . 010 READ: 0 . 001 C �A" ppp) ------------- -------------------------------------------------------- -------- - - AA ZAA DC ' PEAK HEIGHT (ABSORBANCE) 0. 034 0. 025 0 . 016 PEAK AREA (ADS-SECONDS) 0. 014 0. 00.9 0. 011 READ: -0. 004 --- MEAN-=--------0-. 00^--`-----S--TD--. --DEV--. ------- y G . GO�=+ COEF. VAR. - 9- .99 ---------- -- ---- --- 0. 000 0. 000 AUTOZEPO AA ZZAA E,5 PEAK HEIGHT (ADSOREANCE) 0. 074 0. 065 0 . 02_, PEAK AREA (ADS-SECONDS) 0. 067 0. 054 0. 014 READ: 0. 048 10 ------------------------------------ - ------------------------ --- - --------- -- -- -- AA ZAA Dr-. PEA}:: HEIGHT (ABSORBANCE) 0. 07° 0. 066 0 , 020 ' F'EAt: AREA (ADS-SECONDS) 0. 06; 0. 0521 0 . 01 REAL-: 0. 04-17 ' ---- ----- ----- ` ----- --- ------ - -- MEAN= 0. 040STD. DEV. - O. 001 CGEF. VAR. = 2. 1.3 10. 0 STANDARD 1 A S AA ZAA BG ' PEAK HEIGHT (ADSORBANCE) 0. 145 0. 141 0 . 015 PEAK AREA (ABS-SECONDS) 0. 138 0. 124 0. 014 READ: 25. 0 ss ' - ---------------------------------------Aa------------ZAA------------E'C --------- PEAK HEIGHT (ABSORBANCE) 0. 168 0. 158 0 . 023 ' PEAK AREA (ADS-SECONDS) 0. 142 0. 127 0 . 016 READ: 25. 5 0000124 --------------------------------------------------------------------- ------- ---- MEAN= 225.'2' STD,DEV, = 0. 4 COEF, VAR. = 1 . 41 A IS (CONTINUED) ' 25,2 E-50: READING GREATEP. THAN HIGHEST STAPJDAF.D 25. 0 STANDARD 2 A S AA ZAA BG ' PEAK HEIGHT (ABSORBANCE) 0.305 0.280 0, 0331 PEAK AREA (ABS-SECONDS) 0.280 0.251 0. 030 READ: 50. 1 SQ m ZAA PEAT; HEIGHT (ABSORBANCE) 0.323 0, 296 0. 032 PEAK AREA (ABS-SECONDS) 0, 292 0,268 0. 025 READ: 53. 4 ---------------------------------------- ----------------------------------- - ---- MEAN= 51 .7 STD. DEV. = 2.3 COEF.VAR. = 4. 25 7. 51 . 7 ' E-50: READING GREATER THAN HIGHEST STANDARD 50. 0 STANDARD 3 A� AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 538 0.468 0 . 044 PEAK AREA (ABS-SECONDS) 0. 524 0,484 0. 041 READ: 87. 3 IDD ----- ---- -------- --- - --------------------------------------------------- -------- ' AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.548 0.511 01046 PEAK AREA (ABS-SECONDS) 0. 525 0. 41B5 0. 041 ' READ----- -------- -- --- - - -- --- -------- ------ ------ ------------ ---- ----- --- - -- - - - - MEAN= 87. 4 STD, DEV, = 0. 1 COEF, VAR. = 0. 11 'X.. *jFi*?!-iF�F]FSE?4jr?f-*�jFdEjEiF�F�jFiEjE'.FBF*?F'lFjFjF�#4iF�#�FdF�('iF�F��?F*�FjE�F�FiE�('�EiF#jF?FiFaFiEiF��1F#iF#?FiEjFiFIF�E#44iEE-1F�4 87. 4 E-50: READING GREATER THAN HIGHEST STANDARD 99. 8 STANDARD 4 o. qqg 0000125. ' As OGOE AA ZAA FG PEAK HEIGHT (AFSORFANCE) 0. 532 0.492 0 . 047 PEAS:: AREA (AFS-SECONDS) 0. 480 0.439 0, 041 READ- 89, 8 Cil :: 100•/1 ------------------- - -- ---- AA ZAA PC PEAY; HEIGHT (AFSORFANCE) 0.556 0.504 0 . 0522 PEAK AREA (AFS-SECONDS) 0. 482 0,440 0. 042 READ: 90 . 0 ---------------- ----- ------------------------------------------ MEAN= 89.9 STD, DEV. = 0.2 COEF.VAR, = 0. 19 'k. AS; Oo4 AA ZAA FG PEAK HEIGHT (ABSORBANCE) 0. 024 0. 023 0 . 020 PEAK AREA (ABS-SECONDS) 0. 017 0. 007 0. 009 READ-------- -0, 4---------------- -- --------------------------------- --------- - --- AA ZAA P PEAK HEIGHT (ABSORBANCE) 0. 026 0. 024 0, 017 PEAK AREA (AFS-SECONDS) 0, 014 0. 006 0. 002, READ: 0. 1 MEAN= -------O, J- ----STD, DEV. =------- 2 G . -----COEF, VAR, = 82. 08-4�------ ------- - --- A S O 0 � o qq ZAA BG PEAK HEIGHT (AE,SORDANCE) 0. 081 G. 0' 0. 01 21, PEAK AREA (AFS-SECONDS) 0. 064 0. 051 0 , 01 ' FEAD: 8. 9CRA --------- --------- --- ------------- --------------- - ---------- ------- - -- -- - --- - -- AA ZAA PC, 1 PEAK HEIGHT (ADSORIANCE) 0. 074 0. 063 0. 022 PEAK AREA (ABS-SECONDS) 0. 065 0. 050 G, 016 ' READ: 8.7 --------- ------- - ------- - MEAN= 8. 8 STD, DEV. = 0 .2 COEF.VAR. = 2. 00 . t AS 0OQS9 AA ZAA E:G PEAK HEIGHT (ADSORBANCE) 0.324 0.:304 0. 029 PEAK AREA (ABS-SECONDS) 0.2PS3 0. 261 0. 022 READ: 51 . 5 ccYl' l0q�/.-------- -�-�M ------ ------------------------------- ---- ----- - - - - -- -- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0,335 0, 309 01029 PEAK AREA (AFS-SECONDS) 0. 294 0.268 0. 02E READ-. 52. 9 MEAN= 52, 2 STD.DEV, = 1 . 0 COEF.VAR. = 2. 00 % 0000126 AE3 0030 AA ZAA BG PEAK HEIGHT (ABSORPANCE) 0. 017 0. 022 0. 017 PEAK AREA (ABS-SECONDS) 0. 011 0. 002 0. 009 READ: -0. 6 cc� --------- -------- ------------------------ --- ------------------ ------------------ AA ZAA FG PEAK HEIGHT (ABSORBANCE) 0. 022 0. 018 0, 01; PEAK AREA (ABS-SECONDS) 0. 008, -0. 001 0. 009 READ: - 1 . 1 - ------------------------------------------------------------------------ - -- ---- MEAN= -0.9 STD. DEV. = 0. 4 COEF.VAR. = 59. 91 - A S 0 1 3 AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0. 018 0. 021 0. 01E, ' PEAK AREA (ABS-SECONDS) 0. 008 -0. 001 01009 READ- - 1 .2 13425-rt3W AA ZAA Fila PEAK HEIGHT (ABSORDANCE) 0 . 020 0. 019 0 , 015 PEAT; AREA (ABS-SECONDS) 0. 008 -0. 004 0, 012 FEAD: - 1 . 7 - -------- ------------------=------------- ------------------------ ------- - ---- --- MEAN= - 1 . 4 STD. DF-/. = 0. 4 COEF. VAR. = 25,90 AS 001 AA 'ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 155 0. 140 0. 02=• PEAK AREA (ABS-SECONDS) 0. 126 0, 111 0, 015 READ: 20. 8 P13WA /0411/1 AA SAA BG PEAK HEIGHT (ABSORBANCE) 0, 157 0, 131 0 , 02el PEAT: AREA (ABS-SECONDS) 0. 127 G. 112 0. 015 READ: 21 , 0 ----------------- ----- ------=f------------ ---- --------------- ------- - -- --- ---- -- MEAN= 20. 9 STD. DEV./ 0. 1 COEF. VAR. = 0. 45 K A S 0 0 1 Ec AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 521 0.297 0, 028 PEAK AREA (ABS-SECONDS) 0. 2�A_ 0.242 0. 02 READ- 47. E ------------------------------------- '----------------------- ---- --- --- ---- - --- - AA 2AA EG PEAK HEIGHT (ABSORBANCE) 0.519 0,295 0. 052 PEAK AREA (AES-SECONDS) 0. 2-70 0,246 0 , 025 READ: 48. 4 0000127 0 ----------------------------------------------------------------- ------ -------- nmfnni- A0 n -_ - __ cTn_-nry-- _ ---- --/�-r' -- - rnpp. vap. IILn1V� _r60v �Jla/I LJLr • - �. v vv�.• • •..•.• . . v- n A S 0 0 1 ,4 AA ZAA DG PEAS: HEIGHT (ABSORBANCE) 0. 416 0.388 0. 041 PEAK AREA (ADS-SECONDS) 0.358 0, 330 0. 028 READ: 66. 1 LGSW A 06%) ----------------- ------------------------ -------------------------------- ------- _ AA ZAA DG PEAK:: HEIGHT (ABSORBANCE) 0.425 0.399 0. 032 PEAK: AREA (ABS-SECONDS) 0. 365 0.2141 0 . 024 READ66.5 -------- ------- MEAN= 67.3 STD. DEV. = 1 .5 COEF, VAR. = 2.6%B AS; 0015 AA ZAA DG PEAK; HEIGHT (ADSOP.BANCE) 0, 070 0. 029 0. 0617 PEAK: AREA (ADS-SECONDS) 0. 040 0. 008 0 , 031 READ, 0. 6 13425 -01 NSW2SGv�( --------------------- -------------------- -------------------------- - ----- - --- -- - AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0. 0;18 0. 029 0. 064 PEAK; AREA (ADS-SECONDS) 01045 0. 011 0 . 023, READ- 1 . 2 ----------------------------------------------------------------- --- ----- ------- MEAN= 0,9 STD. DEV, = 0. 4 COEF,VAR, = 45,65 %. 1FiE1E?FiEdF#�E1FiE�FiF�FiE�F3EjFjF*jE?E?ESE*iF***9FiF*9E4ir�F�FiF�EiF�iFiFlFjEjE�E**�E�FIE�#�E�E�#iE�E�F�EiF�iF*�**f�F*#**�F��FiE�E* AE3 0 0 1 E AA ZAA Do PEAK. HEIGHT (ADSORDANCE) 0 . 181 0. 121 0 . 06' PEAK: AREA (ADS-SECONDS) 0. 1136 0. 095 0. 040 READ: 17. 7 of A gg/ --------- --------- -- ----------------------- -- ---------------------- -- ------ -- --- AA ZAA EG PEAK: HEIGHT (ABSORBANCE) 0 . 1?5 0 . 122 0 . 066 PEAK: AREA (ABS-SECONDS) 0. 137 0. 095 0. 042 READ; 1;. 6 MEAN= 7 STU, DEV, = 0. 1 COEF,VAR. =--O. -'S % - ----- A!E3 00177- . AA ZAA DG PEAK: HEIGHT (ADSORDANCE) 0. 041 01018 0. 034 PEAK AREA (ABS-SECONDS) 0. 030 0. 002 0 . 028 0oo012-1s READ- -0. 6 13/425-02 MW3SGW -------------------- --------------------------- -------------------------- ------- AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0, 043 0. 022 0, 041 PEAK AREA (ADS-SECONDS) 0. 030 0, 003 0. 027 READ: -0. 4 ------------------------------------------------------- MEAN= -0.5 STD, DEV. - 0.2 COEF.VAR. = 3_1.50 %. A8 O O 1 a AA ZAA DG FEAK HEIGHT (ADSORBANCE) 0 . 140 0. 111 0. 039 FEAK AREA (ADS-SECONDS) 0. 1.90 0. 096 0. 09:9 READ- 17.13 A ---------------------------------– -----------—% -------- -- ----- -- ---- AA ZAA BG FEAK HEIGHT (ADSORBANCE) 0. 13E 04104 0. 04:3, FEAK AREA (ADS-SECONDS) 0. 120 0. 009 0. 031 1 P.EA-------------------------------------------------------------------------- - -- MEAN= 17.2 STD. DEV. = 0.9 COEF.VAR. = 5. 47 firE3 00 1 %3 AA ZAA B_ FEAK HEIGHT (ADSORBANCE) 0. 049 0. 021 0. 042' FEAK AREA (ABS-SECONDS) 0. 035 0. 005 "__. 031 READ- -0. 1 13425_03 N\VN (-SG\t --------- ---------------------------- ---------------------------- -------- - -- - --- AA ZAA BG FEAK HEIGHT (ADSORDANCE) 0. 048 0. 020 0, 04 FEAK AREA (ADS-SECONDS) 0. 035 0. 00:9 ' READ; -0,4 ------------------------------------------------------------------------- ----- -- MEAN= -0.3 STD. DEV. = 0.2 COEF. VAR. = 92. 0° 7. AS 000 AA ZAA DG FEAK HEIGHT (ABSORDANCE) 0. 111 0. 039 0. 040 PEAK AREA (ADS-SECONDS) 0. 115 0. 089 0. 026 READ; 16, 5 03A g3% AA ZAA BG FEAK HEIGHT (ABSORBANCE) 0. 121 0. 092 FEAK AREA (ADS-SECONDS) 0. 121 0. 091 0 . 0:91 READ; 16. ° ------------------------------------------------------------------ - -- - - -- - - - -- -- MEAN= 16.E STD, DEV, = 0.2 COEF, VAR. = 1 ,21 x. E3 a o 1 00001 AA ZAA i FEAK HEIGHT (ADSORBANCE) 0. 306 0.2;3 0. 0:91 FEAK AREA (ABS-SECONDS) 0. 276 0, 24' 0 , 020 z too READ ------------------- ---------------------------J-------- --------�9--- - – - -- DD ^OD RC: PEAK HEIGHT tABSORDANCE) 0. 315 0 , 292 0. 054 PEAS: AREA (AFS-SECONDS) 0,256 0.2261 0. 024 READ; 51 . 6 MEAN= 50. 2 STD, DEV, = 2. 1 CGEF, VAR. = 4. 15 K- 1 AA ZAA DG PEAK HEIGHT (ADSORDANCE) 0. 018 0. 018 0. 01=, PEAK AREA (ADS-SECONDS) 0. 008 0. 000 0. 008 READ1 + 1 --------- ----- --- ------ ----------------------------------- -------- - -- ---- AA ZAA DG PEAK HEIGHT (ADSORDANCE) 0. 020 0. 016 0. 012 PEAK AREA (ADS-SECONDS) 0. 012 0, 005 0. 00; READ: 0. 0 MEAN= -0.5 STD, DEV. = 8 COEF, VAR, = 913+139 % A 00at AA 7AA DG PEAK HEIGHT (ABSORBANCE) 0. 071 0, 029 0 . 056 PEAK AREA (ADS-SECONDS) 0. 050 0. 010 0+ 041 READ: 0, 9 13425-04 MW(OO(IYq --------- ------------ --- ------ --------------------------- ------------ ----- --- --- _ AA ZAA DoPEAK. HEIGHT (AESORDANCE) 0. 072 0. 0213 01062 PEAS: AREA (ADS-SECONDS) 0, 052 0. 011 0 . 041 READ; 1 , 2 - ----- -- ----- -------- --- -- ------------------------ ----------- ------- ----- -- -- - -- MEAN= 1 . 0 STD+ DEV. = 0. 2 COEF. VAR. = 18. 58 % AS 00 ^-4 AA Z_AA DG PEAK HEIGHT (ADSORDANCE) 0. 129 0. 095 0. 054 PEAK AREA (ABS-SECONDS) 0. 136 0, 093 0. 043 READ: 1;.:? 04A g�1 ----------------- ----- ---- --------------------------------------- --- ----- --- ---- i AA ZAA DG PEAK. HEIGHT (ADSORDANCE) 0. 129 0 , 099 0. 064 PEAT: AREA (ADS-SECONDS) 0. 143 0. 092 0. 051 READ: 1:. 0 --------- - --- ---- ---- --------------------------------- ------------------- -- ----- MEAN= 17. 1 STD. DEV, = 0. 2 COEF.VAR. = 1 . 07 % AE; 00 ^s 0000130 AA ZAA BG ' PEAK HEIGHT (ADSORDANCE) 0. 070 0. 028 0. 056 PEAT: AREA (ABS-SECONDS) 0. 051 0. 006 0, 046 READ: 0. 1 13 5 ds Cave of cv) AA ZAA PC PEAK HEIGHT (ABSOP..DANCE) 0. 066 0. 030 0. 057 PEAS: AREA (ARS-SECONDS) 0. 055 0. 009 0. 046 READ: 0.9 MW(cDGW D --------- ------------------------------------------------------------------- ---- MEAN= 0.5 STD. DEV. = 0.5 COEF. VAR. = 99.99 % 1 AS 00 6 AA ZAA DG PEAS: HEIGHT (ABSORBANCE) 0. 128 0. 097 0. 058 PEAK: AREA (ADS-SECONDS) 0. 138 0. 09.9 0, 044 READ: 17.3 D5 coup A 91'/o --------- -------------------------------AA------------`AA------------PC--- ------ PEAK HEIGHT (ABSORBANCE) 0. 129 0. 101 0, 058 PEAK AREA (ADS-SECONDS) 0. 137 0. 094 0. 04= READ: 17.4 -- ---------------------------- ------------- ---------------------- --- - -- -- -- - - --- MEAN= 17. 4 STD.DEV. = 0. 0 COEF.VAR. = 0.26 AS O Of- AA ZAA DG PEAK HEIGHT (ABSORPANCE) 0 . 195 0. 162 0612 PEAK AREA (ADS-SECONDS) 0. 215 0. 166 0, 049 04) READ---------;`------- -----------------------------------—----------- --- -- ---- AA ZAA DG PEAK: HEIGHT (ABSORBANCE) 0. 138 0, 148 0. 063 PEAT: AREA (ABS-SECONDS) 0,216 0. 164 0. 057 READ: 31 .5 MW(ppVW MEAN= 31 .7 STD. DEV. = 0. 4_____COEF. VAR. = 1 . 11 °k ***9E jF�F iF��F jE�F 3F jF 1F�iF iE iF�E�E jF�F 1E�iE�F if dE iF 9E 1F�F jF it�F�E�E iE jE�E dE dF�E�E jE�F 9E�E iF iE iF'.E*iE�E jE�F jF�3F jF jF iE jF iF iF iF 4 iF�F�E#iF dF iF# iF iE iF AE3 OO �a AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 031 0, 016 0. 021 PEAK: AREA (ABS-SECONDS) 0, 018 0. 005 0, 014 READ: -0. 1 13429-07 PW-0 3\ -- -------------------- ----------- -------------------------------- ------ --- -- - --- AA ZAA BG PEAK: HEIGHT (ABSOP..DANCE) 0, 028 0. 016 01018 PEAT; AREA (ADS-SECONDS) 0. 01.3 -0. 002 0. 015 P.EAB--------- 1 . 4------------------------------------------------C OR O 1-3 1------- MEAN= -0.8 STD.DEV, = 0.9 COEF.VAR. = 99.99 % AE3 0017's on 7L1A Rr PEAK HEIGHT (ABSORDANCE) 0. 127 0. 110 01026 PEAK AREA (ADS-SECONDS) 0. 116 0. 094 0. 021 READ; 17. 5 074 % AA ZAA DG PEAK HEIGHT (ADSORDANCE) 0. 12; 0. 113 0. 026 PEAK AREA (AES-SECONDS) 0. 117 0. 098 0. 019 READ; 18.2 ------------------------------------------------------------------------------- MEAN= 17.9 STD. DEV. = 0.5 COEF. VAR. = 2.89 % AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 037 0, 027 0. 0281 PEAK AREA (ADS-SECONDS) 0, 024 0. 003 0. 021 READ-. -0,5 13425 -09 P W - oo-�_ AA SAA EG PEAK HEIGHT (ABSORBANCE) 0 . 0.34 0. 020 110. 029 PEAK AREA (ADS-SECONDS) 0. 025 0. 004 0. 021 ' READ; -0. 3 ------ --- ----------- -------- ------------------ ------------------------------ - - -- MEAN= -0. 4 STD. DEV. = 0. 1 COEF.VAR, = 91 . 81 % R E3 O O :-c 1 - AA ZAA DG PEAK HEIGHT (ARSORDANCE) 0. 128 0. 100 0. 037 PEAK AREA (AFS SECONDS) 0. 121 A0. 089 0. 032 READ: 16. 5 09 A u o" 1 --------- -------- ----- - --- ------------- -- ------------------------ -- AA ZAA DG ' PEAK HEIGHT (ABSOP.DANCE) 0. 121 0. 101 0 . 028 PEAK AREA (ADS-SECONDS) 0 . 118 0, 092 0. 02G READ-. 17. 1 MEAN= 16, 8 STD. DEV. = 0.5 COEF.VAR, = 2.8.3 °/<• GOOOI32 AS O O :D AA LAA EG PEAK HEIGHT (AESOP.FANCE) 0.345 0.320 01029 PEAK AREA (AFS-SECONDS) 0.301 0. 273 0 , 023 READ-. 54. 0 cV 3'loq�v ` to ,4s Am --------- ------------ ----------------------------------------------------------- AA LAA FG PEAK HEIGHT (ABSORBANCE) 0.341 0.317 0. 032 PEAK AREA (AFS-SECONDS) 0.300 0,278 0 . 022 1 READ: 55. 1 --------------------------------- ------------------------- -------------- - - --- --- MEAN= 54.E STD. DEV, = 0.8 COEF.VAR. = 1 .41 . AS O O _D:Ec AA LAA BG PEAK HEIGHT (AFSOREANCE) 0. 018 0. 018 0. 013, PEAK AREA (AFS-SECONDS) 0. 009 0. 004 0, 005 READ-z -0. 2 CC{3 ---------------------------------------------------------------------------- -- -- AA LAA EG PEAK HEIGHT (ABSORBANCE) 0. 015' 0. 017 0 , 01E PEAK AREA (AES-SECONDS) 0, 008 0. 001 0 . 007 iREAD- -0. 8 --------- ----------------- ------------------------------- -------------- -- - -- - - -- MEAN= -0, 5 STD, DEV, = 0. 4 COEF. VAR. = 7=9. 04 . AA LAA FG PEAT; HEIGHT (AFSOP.FANCE) 0, 028 0. 019 0 . 022 PEAK AREA (ADS-SECONDS) 0, 021 0. 005 0. 01E READ: 0. 0 13425- Oq c - ------------ ------- ----------------------------------------- ------------ - - -- - -- as LAA F, PEAK HEIGHT (ABSORBANCE) 0. 028 0. 019 0, 022 PEAK AREA (AFS-SECONDS) 0. 019 0. 003 0. 01E READ; -0. 5 -- ---- --------------------------------------------------- ------------ - - --- -- - -- - MEAN= -0.3 STD, DEV. = 0,3 COEF,VAR, = 99,99 °X. A S 0 O :B!5 AA LAA BG PEA}; HEIGHT (AESOP,FANCE) 0. 12? 0. 106 0. 023= PEAK: AREA (APS-SECONDS) 0. 114 0. 092 0. 022 READ: 17. 1 OqA 82 c ---------------------------------------- AA------------LAA-------- EG------ --- PEAK. HEIGHT (ABSORBANCE) 0. 1 12 0. 100 00001. 33' 0. 029 PEAK AREA (ADS-SECONDS) 0. 108 0, 085 0 , 023 ornn. �S o 11L r'1L• 1 v. V MEAN= 16, 4 STD, DEV, - 1 , 0 COEF,VAR, = 5.51 %. AS 00 -D6 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 025 0. 020 0, 015 PEAK AREA (ABS-SECONDS) 0. 012 01002 0. 010 READ: -016 13 25 -DSD �80l2-4 ---- ---------------------------------------------------------------------------- AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 022 0 . 024 0. 01; PEAT; AREA (ABS-SECONDS) 0. 011 0. 000 0. 011 READ: - 1 . 0 ----- ---- ----------------- -- --------01 -)----------- MEAN= -0. 8 STD, DEV. = COEF.VAR. = 34.63 % I AS 00 -Hc:- AA ZAA BG PEAK HEIGHT (ABSORDANCE) 0, 107 0, 102 0 . 0,211 PEAS; AREA (ABS-SECONDS) 0. 115 0, 100 Q 0. 013 READ-. 18.6 010,A q��u -------------------------- -------- -------- -------------- ------------------------ AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 114 0. 101 0. 021 PEAK AREA (ABS-SECONDS) 0. 122 0. 104 0. 01; READ19 . 5 -------- ------ -- ------------------------- ------------ ------- - --- ---- - --- MEAN= 19, 1 STD, DEV. = 0.6 COEF.VAR. = 3.24 %. AE3 00 -c AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 854 0.339 0. 0,.jO ' PEAK AREA (ABS-SECONDS) 0. 295 0. 275 0. 020 READ-. 54. 4 CGS/ -109 (11'30 A-M ---- ----------------- ------------------------- ' AA ZAA EIG PEAK HEIGHT (ADSOP.DANCE) 0.371 0, 349 0. 031 PEAK AREA (ABS-SECONDS) 0. 296 0.271 0. 02E READ53. 5 -- ------ - ---- ---------------------------------------- -------- -- --- --- --- MEAN= 54. 0 STD. DEV. = 0 .7 COEF.VAR. = 1 .25 %. AS 00 -D AA ZAA BG 1 PEAS: HEIGHT (ABSORBANCE) 0. 018 0. 014 0 . 014 PEAK AREA (ABS-SECONDS) 0. 009 01000 01008 READ: -0.9 CC43 G O 00 1 '�4 AA ZAA BG 17F�k' t IC T( GIT r cu�ncaTJnnir� n. n?n 0. 014 NYTEST ENVIRONMENTAL INC. FURNACE ANALYSIS RUN LOG ANALYST: Yi�i D, r m .m SIS DATE: I� 19�Z r�� -err D . 3030 CALIaR.-kT1O,r D;i S: I� START TIME: 14M ' rl onI END TI,i=: X3202 '� 5 SrrCs a f tit GpEX ST \�DA.RD SOL-RCE: c7A\7AR.D LOT # . 2-5�1 —AS Si. -DARD PREPARATION D.-.T=. g 1 �'9Z \ ON DATE: 1 r 30 193 ` ,RD F.XPIRAT; 1 sT.:NDARD PRE?AR=.TION LOGEOOK PAGE =. � Cru' �IOOf t J S LIPLE N.L�iE I CCi-?T NCE Llyti t S CO `` Ni INIEN T I QC SA. .ICV I 9x-110 I 4 ICB I < (-!-) CRQL CCV I 90-110 ::...: I I CCB I < (+/-) CRQL LCS ( SO-120 or E?A LIMITS I � PREPARATION BL.avR I <(=!-) CRQL I I DUPLICATE I SPI"U. I REVIEWED BY: 0000135 : i �uf uST' 1-21 1992 VIVI 1 P, C'!1'IZTAIN AS ~ Pro -- - - - - - - - - - - - - - - -- - - - - -- - - - - - - -- - --- - --'- -- ----- ----------- '-- - --- ------- - - - --- - --- A F.E A.L ^E r0lVi°= � fi , + 1 � �_; f,r-,:; F E 4#'+t('##T�++t�t#t+ :�t,sz :.��t+++*#+#t#t####�'#t�' t###+#'E+4#++-tx++tt###++-t#=►3+-+ i#iF+t FEr':?': HEiG*HT f A;=='r'FF 'NCE r , c__ , ' - PEhli?: r..P.EH l iyD'= r;Er-'_r!Ni':1 r;= F 7- to -- - -- - - - --'- ♦ `� - - -- -- - -- -- -- - - -- - - - - - -- ----— - ---- -- --- - --- ---- ---- --- - - - - - - _•H i .,-,i'y. N V 7 ID PLnL. t" -.r- '_'�eD='i 1' . �'r.� C' > C• �_ a i` - ----- --- - --- -- - - - --- ----- -- -- - ------ - ------ --- - ---------- --- - ------- -- - - - -- - - -- iF!h4iF?4�et?F4t��4'�F#�' ##+?f;+;t###�.tE�-•.1x-�#+iE###4X## 'x4#4t#'!F#ttiE#t+?c}�E+F#4E+=ryt;f�.4#+fEifi# 1 v. =TADART , � rr FEAK. HE 1 L^t T r. l . t h =L'PSD�=- �9 E �; i,. ; _ . , = 25 1 - --- ----- -- - - - -- - - -- - - -- - - ----- - - --- - ----- ----- ----- --_------ - -- -- -- - --- - -- - --- - F;r, F E A HE TC:HT i r~.PSC"RP.ANCE' FLAK AREA (ABS-SE NDS. 1 READ ; C, 0001 .> 6 MEAN= 24. 0 STD, DEV, = C0. 4 COEF. VAR. = 1 . 64 titiF#EiEst:E#++i4?E?FfF###�•}irtt?E?E#}#?FiFiE•!tt##+E?FirjFiE•:etiE�t-fEjF•!E4rjF?F?F�i��F#�F##�Fie'4?F•)FiF?FkiE#4tEE#aF}iF '4. 0 I Z-50 : READING GREATER THAN HIGHEST STANDARD 25. 0 STANDARD ##}Ott}}}}*�}}}*•��•*�xt�}##}##r�*t}t�#*•��t��fi��}r}#•�•�#��# �#•��•�}�}�x}#��#�}}}++ PEAK HEIGHT (ABSORBANCE) 0. 371 0. 354 G. Uc PEAL. AREA (ABS-SECONDS) O. Sio O. E1.{ 0. 027 RLf'IL • 55. 6 - -------- --- - - --- --- - ---- --- --- - --- ---------------.------------------- -- -- - -- - -- (CNTINED: nn ::nn r. n Zn:1 B-1_ rtr,k HEIGHT r,r^,_F:BnNCc� 0. 362 0. 331 G; G-._ PEA: AREA (ABS-SECONDS) �.1 . :306 0 .27*3 02.5 RSA- . 54. 5 MEAT,=- - - - - -�_ . _ - - - - -^Tip, DE',.�. _----- -- =�L--- --C"EF. vA�=:, =--i -�---;-- -- ----- -- - - - - - ?Ftt #ta}t#isiF+�:tt+�•j##}}tti4t#��t}� .+{#r.t##+?F3 sf{ tsiaFEe+#•ice#�4#. ��}{iF?4 #t��-ctt� i 55, C' 0: READING GREATER THAN HIGHEST STAiDA - }}7->} }}++}}}fi;!}}#}}}}}+*ti�}}}+}}fi}fi}t}�}�}}}•Y}}}}}}*}}tt*}}t+l}+jf-}#i }}+}}fit-}}}+}}. 50 . 0 TANDARD •!•)(•#kf.}}y}}t}}�}+�f: }•�•}��ia7:}i�}3Fti}•�}�r#�1:}�E•#}:1`3.-jt#}•Y•} ?(.�.its.a .ii#�.it+�}}}}}}+ytt}�+}}+a ANEs AA ZAn r:_ ' PEAK HEIGHT 1 AESO BANCE. 0012 0. 58'f 0. 054 AK PEAREA (ABS-SECONDS) v, .0151i 0. 04E REAL. SEAR - -- -- - - - - -- - - --- - --- - - - - --- -- - - - - ----------- --n A Ipo- ----- -- --------- ---- ------ - - -- - AZAA. PEAK HEIGHT (AE_O R ANC E) 0. 6310) 0 . 503 0 . 050 FEAT. AREA (A00-S:ECONDS. 0. 5_5 0.S: _ 0 . 04Z 1 READ . 20 . 0 ---- - ---- -- - - - - - - - --- --- ---- ----- ------ -- -- ----- ---- ----------- --- --------- - - - - MEAN= 89 . S '=TD. DE`J. = c COEF,1 AF. = 0 . 17 % ?ftt#t#�FiF+E=.c##'f-�E#il �t?Ft#aF##iEe}++E#'k?Ftf 4s.iF'4riF##+E-i#3tt## t�l•i#i•#�r##�E# #a+4 ti(•+###�F##'E itic±Fee' OJiu E-50 : READING GREATER THAN HIGHEST STANDARD }}}*rr. #*t##}t. t}�.s####•�r}}#f}x}}#a};:Yrt-kit#r.###sr. x#i�*�xtiF�E}}x�F•�s}�riFs#}+�•+;}}}..}•r}f- 95, G STANDARD 4 G. 999 }t'•)c#•iF#•l}}}�E}}#}#t}t�-#}i }}r.i >**}}t#t#}}fi}t.fix}+#}r.}f •F#}� ir#tt. }}r}t#+#t. ts. }}+}t}f#t*- 0000137 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 666 0.610 0 . 055 FEAR. AREA (A3S-SECONDS) 0 . 544: 0, 501 0. 043 READ: 97. 4 lcy- (oZ - ---- - -- ---- - - --- --- ---- ---- - --- - - ---- --- ------------------------- ----- ---- - -- ---- - - --- --- ---- ---- - --- - - ---- --- ------------------------- ------- ------- AAA BG PEAK HEIGHT (ALS ORBANCE) 0.634 0, 591 0 . 054 PEAK AREA (ABS-SECONDS) 0. 50, 0, 49' 0 . 03S READ: _C: . S - -- - - - --- - - - - - ------- - --- --- - --- - - --- - --------- -------------- -------- ----- -- -- - - MEAN= SE ' s STD, L'E . = 07! C'. E . VAR. = 0.71 ###�t4##�•�it+se##<#�F+�t+?•##z#iE#+4#a##•#;E#�•##i[#•'.E•###?F:!-•rY4#te3#?4#t:##-##+?F#####t4�t3-#l•##1E3af•+ t� r.; A. ._Ari W-7 F'EAK "EIGHT 1AE=:'CR:BNf'.!_Ei 0. 01E 0. 0=4 0 . 002 FEA`. AREA ABS—SECONDS) —0. 002 0 . 001, —0 . X10 FE AL . : -4 IPP - - - --- -- - - - - - -- - - ----- - - - - - - - - - -- - - --n^ --- ---------`.._- ------- -- --F--- - - - -- - - i'G H I••. H L 1'=iii ;. •L:S t!R B r NC i=) 0, 021 0 . 029 ''1 , i Wti PEA" A E.A th;$: SE_,JNTrSi 0 . 010 - 0. 006 0. 004 READ: . _ -- - ---- -- - - - - - -- - - - --- - - - - -- - - -- - - - - - - - -- -- - - -------- -- -- -- --- - -- - - --- -- - - -- - - - -- ricAN- G. E STD, D-V: . . ._ C"-F. vn,,. - t_:: , : aE*t34#*t+} + Y4#i�'4'#?4',k'#1•t?4}?ra•iF+#•4t' it'k:lt# 4}iF?(•jf•Vit'.#=#�F4•:'[•�F +��?#s:t{aF�.f*fes#;�+�#4+Ert+�} � f--t Es A A. 2 AA :,r PEAK HEi=•Hi (AES_kihN'=EG , G" 0 . 064 C' , ' FEAT. AREA :, BS—S;_ ONDS ) 0. 064 0. 04 2- 010iff READ-- -- - -- - -" - --- - - - --- --- - - - -- ------'----- AA. ZArAi FLAK HEIGHT (ABSORBANCE) 0. 073 0. 07: 0 , OE6 PEAK AREA (ABS-SECONDS) O . 064 0. 051 t , r; 1 G FEAD: 1 ' MEAN=- - --- --"/ STD . DE`.�, C', 4 CHEF,VA:F'. ` - - - - =- - - - - - - ----- =-- +fl--- -- . - - ----- -- - - ---- - ttttttttt�FttiE4t#ttt�#t*?Ft�Ettt#t#4#ttt�•tttt ##•flei#•(•ir:e'i+t#tt#iF�►?e•4e#�•iF+:►+E#•!E?#t+t4xir4{ L AA EAAL'=: FEA��: HEIGHT (A�SOFBANCZ) 0 . 359 OWE 0 , 042 PEAK AREA (ABS-SECONDS) v. _.i_i 0 ,272 Q 0 , 032 AA REAL': 50 . Cry-102 7r (8 . 3o �M) - -- - --- ---- - - - - --- --- ---- ------- - --- - - -- - ----------------- - - -- -- --- - - ----- -- - -- - AA SAA af_ FEAR HEIGHT (ABSORBANCE) 0 . .6TS 0 .30= 0 , 04j FEAT, AREA CABS-SECONDS) 0 1 1 0 , 2o._ 0 . 02Ec, READ:1 . -- --- ---- - - - ---- -- -- - ---- --- - -- - ----------- ------- -- --------- - - - - -- MEAN= 50 . 9 STD. DEV. = 017 COEF.VAR. = 1 . 46 i•`: 00001138 iF•iti�t�iF�F�Y.#�F#tt•iEl#Y•#�F?F'�iE•1F3(•##�t•aFBF+#f#4iE#*•)Fit#iF�iE••3E�jl•iF�(•#�(•�(•�k#.4+## 44aEiE#fxif•iFiF#4s•1F+Fx�F?FiF#•4t#(•�F i �S 0Ci1d AA A� BG PEAK. HEIGHT (ADSORDANCE) 0. 0'?6 0 , 21 el 0 . 01 E. PEAK' AREA (ADS-SECONDS) 0 . 015 0 . 005 0 . 010 READ: 0. F COP --- ------ -- - - -- - --- ---------- --------------- --------- ---- -------------- --- - - - - - 1 AA �, SAA �. PEP-7-' HEIGHT (AiSORDANCE) 0 . 0 4 0. G IL 0 . 0211 F'EA1': AREA (ADS-SECONDZE) 0 . 008 -0. 005 -A- - --- - --- -- --- ---- ---------- -- - - -- ------------------------------------ - -- - -- - MEA(J= G. 0 STD, DEV, _ : . C C!CEF,VAR. _ SS. 99 I; ' ?E?F?F'.###iFitEt�tt•4#EiF?4�.iFiEt.t'4.IF?F3i•#iE�t4iF4}:4�e�:6#?E:►#-i(.s-?F?F##�•i;#.t�i•#iEiF+F#4}tt4ac3F�F•iF?E#?FE#saE•4�# r1 Es d d 1 1 AA SAA DG PEAK HE I CHT (r, 0RDA:J E0 . 02�, G , C, PEAK A—t-A 0. 'V 12 -0 . C,r)1 .'- 1: FEAD: 1 13412-FfW - -- - - - - - - -- - -- - - - --- - -- - - - ----- - - - - - ---- -�-- -------- --`- - ------ -- --- - -F1'_- - --- - - Eftit. HE CH^ i.ASS-°!_:SLP A1',i'_t.' .3. 0,'-.; G, !_'_'G PEAK. AREA AB'=-SE :C�'JL'' ! , G1� 'C . 0C'_ 010, READ: ''J . 1 ' M- ---- -- - --- - - - - - - --- - --- - -- - --- - - -- - ------------- ---------- -- ------- ------ --- -- - 1v C eTD, DE's, = t:, COEF.VAF:, tiFf +. #t'17E-4t#ttx++f:t�#++##{ESE#E�•+ Et+4 4?E#7.?4�'.E�Fsr+{#aEiEti4E�?F?F4t+4�Ft•1.4�FaE4.�F+Y�F#E#�'kiltF�- X--, „ A - nn PEAK HEIGHT iADSORDAN--E0 . 1r,G c PErk; AREA (r,L,--.-^E'CJrJDS't ti;. i?0 � , 01 REAL : 2e . PPWA I03% -- - - --- - - - -- - -- - --- -- - - ----- -- - - - - - - - - - - ---- - - ------ -- --- -- - ---- ---- - -_- - - -- - - -- r:• E 7o cp ,� ,�.. HET,-HT AL'M ,R .mrJr��) G. 1. ;, . 1.� , o PEAS; AREA (F E'= ::E;ONDS:' 0. 13C5 G . 1 1 C,r READ; ^^-0 . 6 --- - ---- - - - - - - --- -- - - -- - - ------ - ---- ----- ---- -- ----- -- ---------- - -- - - - -- - -- - - - -- - MEAN= 71r- , -, STD. DEV. = 0. 1 COEF, VAR, = 0. 69 % iE#t•4?�+#�{ tiF jF E'.4?F 1E tt�F:k #t'.Ef.#iF:kkt+a4�F�f?F'�iF�iE#�l•iF'3F�•�iF•ie#�•?�iF?EaF�#?!•a4+..iF*iE�F?4#iF{{4{�{?¢.1E?F'tt#t•?F� AA SAA DG PEAI HEI--HT (ADSOr?DANE) 0 . =;i? . . E � rPEAF AREA (AD S _NS 25 0-1 READ: t 5 13 12 "Lcsw �x 6t(,, 1 - -- -- -- - --- -- --- .--- - - -- --- - ---- - - -- - - ---a(--:--- - ------- ---SAA----- ------ -EC-- - - - -- - - - PEAK HEIGHT (ABSORDANCE) 0, SE' 0 . 1G6 0. 035 PEA!-.:: AREA (APS-SECONDS) G. E';, 1 0. DQE. C� 0 0 0 1 -, 911 . 02t, ' MEAN= ------4: , :J- --- -STD. DEV, =--- - -- ' 1 . 21-----COEF.VAR. _--21, 63- -'y------------ ----- iEjF�('•?EiE*#aE•iE?t#?Foie'�:#4'hiF?F*�-k•1EjtE?('#?E�['}#-1E�('#',E?EBF-1EiEY#*��.iF'1l'iE?F?�?F?FdFiE$#iF�!':'�9F?EifiF*aF?F!''1FiF+.F#iEY'iE##�tt#iF A S 0 0 1 _- AA 7AA BG PEAT: HEIGHT (ABSORBANCE) 0, 4.x!6 0. 40E 0. 03E PEAK AREA (ALS-SECONDS) 0. 364 0,352 0 . 0.6E 09 W A (10911.) READ---------- -!---- - - - - -------- - --- - ---------` -- ------ ------ -- ------------ - --- AA ZAA BG PEAK HEIGHT (ABSORBANC-E) 0.449 0, 414 0. 046 PEAK AREA (ABS-SECONDS'.- 0 . :9'9 0, 344 C. , 0.35 ' READ. ------- - - --- - -- -- ---- - -- ------- -- - --- -- ------ ------- ----- - --- -------- --- - - -- - . �. — _ C V MEAN E�. I STc!. LE'v. - 1 , ��,k, - OC' ,'... �Ft?F?E?F+E?Ff�•<?tt++#�f#�?4�t;:�{#�!f?4�}?F�F�t?Ft«f��r:?F'F��!•:��#let'�#t?��t?F�iFX+'�•�iFiF#: ��#?��Ef#-flEt#a ' A.s 00 1 AA -A.A BG FEi-�r.. HE I GHT (r.BSGRr r,NCE i 0. C' r Ct ; .:9 ' PEAK AREA (t=B -=ECOf�DS) C!, 0�4 0, ;0021 READ: 0 . 5 '3gfz,�� P'�WISC,v�I -------- - - --- - -- -- -- -- ----- ---------- ---- ---- ----- -- ---- -- ---------- -------- - - --- AAA=; EG PEA,' REICH T (A B SSO F B A M C 0. O 3 O 0 . 0 2.'9 FEAK AREA (ABS-SECONDS) 0 . 0^-5 0. 00 ' RcA-- --- --- - - -- ----- ----- - -- ----- - - ------- -- - ---------------- - - --- -------- - --- MEAN= 1 . 0 S TLS. DEV. = D. E C,--,EF. VAR. _ E+, 55 +ESE}-iFt+#il-*t#aca�# �xs.!:.��.;t•:r#+?k#iF##:r#?��F'.F4�#!#�#?� K�#�•�tiF�##t•�E�iF+#t?F±F444+#4Fr. ?F##t4+FxiF} 1 AS - �.101c - AA SAA E,G FEAK HEIGHT , ABSORDANCE' 0 , 16' 0. 14: 0 . 0=. FEAD: 211 . 0 0IA -- ---------- - - -- - -- - -- --- -- - --- -- - - - --- - - -- - --- - ---- -- ----------- -- - - -- ---- - - - -- AA PEAK HEIGHT (ABSORBANCE) 0. 1?7 0. 14E 0 . 0_:99 PEAK AREA (ADE-SECONDS) 0 . 145 0. 1 1 U . C,3.;- READ :j:ry REA--- ----- - - --- - - - - - - - - - - -- - - - -- - - -- -- --- -- - --- ------ -------- --- ----- ----- - ----- MEAN= = STD, DEV. = 1 . 1 COEF, VAR. = 5. 46 �F�E*#��•*## kk#E#s. ttiF�F###iF#art?F?�i�r.t4x*tY41F:r�FF#+#4�FiE}#?FBF+FBF+�'4f## tY•'rEt'�iF+tiF4�F�F•i!•j�Eir�4# - AA SAA F,0 PEAK HEI"HT (ABSORBANCE) 0. 03E. 0. 0216 0 . 021.E PEAS:: AREA (ABS-SECONDS) 01013 01001 01 READ: 0. 4 /;Y/2--C)2 ri:=<^ . (1^t 1) . 07,9 PEAL. AREA (AEE-SECONDS) 0 . 018 0 , 000 0 . 019 FEAD: 0 . ? -------- ------------ ---- ------- - ------------------------------------------------ ' MEAN= G. := STD. DEV. = 0.2 COEF.VAP. = 60 . 66 % lE iE iE iF iE�t iF iE?F#�F 4 i•�?F•K�aF iF-i. It?F#�E?E :#iF�f aF fF?F iF�jF iF�F iE?E i#�k iF iF i#�F jf 1F if�?F?#�E f;!iE?#iF#.:!jE iF iF?F iF iF�F��?F jF?!•if aF ii it lE•ll•�! AA 4An EG PEA;: HEIGHT (ABSORBANCE) G, i 85 0 , 161 0 . C:G4 PEAK AREA (AIS-SECONDS? 0, 140 10, 114 G . G36 READ_-- ---- -1-'---------------- ---- - --------------- ---- ------------------------ - A n -7�A�n h� B'. PEAK HEIGHT (AESOR$ANCL 5E 13 . 0=x+4 PEAK AREA (ABS-SECONDS) 0. 140 0 . 109 0, RcAD - -- - ---------- ---- - - - --- - -- -_---- --- ------------------- . -------- ----- -- - --- MEAN= 1 : :� E;TD. DEV. - G. 6 C0EF,VAF: = -, 1� 'A {i-;tlt�a•4�EiF�t�•+##?`�+#3!•t##if•4 k+i(..k+#� 'jF?f•'• fiF#$ti tt jFit �iF+.•s. 4'kiE iFe�•++tf•iF�FiF#t�#�•#iF�+ttt+iEit�rjf A E;PEAK - 0 v 1 - AAA�=; E G He H� (n _ 1�.br,.J�:_I=: u, ,,.�`: , .�.�;. G. 01�� PEAT: AREA (A2"=-SEC_0ND . 0100- t G . 02 1 ' READ_ ------------ - - - - -- - - ---- --- ---- ----- ----- -- ------------ --- ----------- -- ------ --- ' AA Z A A E:c PEf"iK HEIGHT (ABSORBANCE) 0. 04C, 0. G 2 3 G . 0 PEAK AREA (AES-SECOi": S: : G, .012= G . 0 0 0 . OC READ: ------------- - - -- - - - --- -'---_- - ----- ----- --- --_- -- _--- -_------- - -- - - f- -- - - - MEAN= 1 . 1 STD. LEV . r. t• CCtF.VR. 1 . 5 7A; AA^ I=AA PEAK HEIGHT (ABSORBANCE) 0. 16,, 0. 140 G . G= PEAK AREA (AL= SECONDS) 0. 1.3-9 0 . 1 13 0 , 0.3'6 READ: 1a , c, 03A 97� ------ - --- --- - -- - - -- --- ------ --- - --- --------- --- - -------- ------------ --- ----- - -- - BG ' - AA SAA PEAK HE I HEIGHT (;;�:SGR;:�ANCE) 0 0. 14� , 1�5 0 . 0 FEAk: AREA (AES-SECONDS) 0 . 1 Jy 0, 111 G , 0 218 READ- -- - ---- - - -- - -- - ----- --- -- ------ - --- ------------- --- --- -------- - - ----- -- - - -- MEAN= 19 . 4 STD. DE'J. = 0 , 5' COEF.VAR: = 1 , 1C, A. 00001 41 1 iE7.•iF?kiF�iF�iF?F�?F�l�:►+Ff�?Eit•1FiF�#�fl�t## i##4-k:t��F�f•�7ki!•iF#ii'#1�iF4iFiF•f!• #�F��F�FiFiEit�FE?4?EiFiFit�F4-if3taF4ittiEt�+aFjl• AE3 O 0 117, 1 AA ZAA BG PEAK HEIGHT (ABSCDREANCE) 0. 318 G, X38. O. 034 PEAT. AREA (ABS-SECONDS) 0. 286 0. 2)64 G , 0 '3 ocnn, a, c -------- ------ - -------- -- --- - ----- - -'-- ----- -'-'------- - ---------- -- ------ -- AA AA BG --- -- PEAK HEIGHT (ABSORBANCE) 01333 0. 31'2 0 . 0-3 2) PEAS. AREA (ADS-SECONDS) 0. 3017 0.284 0. 0212 READ. 51 . 6 CCV2; �f , C9:70 ?tm ----- ------ - -- ---- ------------------ -------------------------------- ----------- - MEAN= 45 , 6 6TD, DEV, = =', 0 COEF.VAR, = 6, 0' k. AS X00 _^_ AaAa BG PEAT; HEIGHT (ABSORBANCE) 0 . C15 0. 016 0. C,`:_ PEAK AREA. (ADS-SECONDS) 0. 011 0. 001 0 . 010 REAL: 0, 3 r"N --- - --- ------- -- ---- ----- ----------- ------------------ ----------------- --- --- AA Aa PEA'',.: HEIGHT (aBSORDANCE) 0. 0312 0. ?E= 0 . 020 PEAU. AREA (ABS-SECONDS) . 01E 0 . 004 C . 00 READ; 0. 8 --- -- ------- - - - - - --- --- - --- -- -- - - -- - - -- - -- - - --------- ----------- -- -- - ------ - - - - - MEAN= Cl . G. S l it. LtV . = ). 4 0 VA)':. = n C C�EF, 6i . � %; 'r#'�##+}#t��4a#;Fi#iE#:#xiF?F##�F'!t+iFie#F#i+}$#ir'iFkiF?E�FiFiER?F�E?F##iF�#iF�E •it#it?Fe##-iF:i�rE#+iEiF4#t?f�#+ AE 00C,= AA An B's PEAY'. HEIGHT (ABSOFDANC:E) 0. 0=,5 C . 012) C.. C2 PEAK AREA (AE-RS-SECONDS) 0. 0?,, C. 000_ 0 . 021 FEAD 0 . 021 E=;D -- - - - - ---- - - -- -- - - - -- - --- ----'32 — 0 -- ---- ----- - - DGYlI71 - - AA BC PEA.k: HEIGHT (ABSORBANCE) 0. 0 3,G 0, 0121= 0 , 1")30 PEAS: AREA (ADS-SECONDS) 0 . 0125 0, 00 0, C,21 C, FEaD- 1 , 8 --- --------- --s-- ---STD, E --_------ - - ---- --- -----til--- ---D---- -'r - ---- --- ---- - - -- - MEAiJ= : , STD, LE'v. - 0. 4 COEF, ,AP... _ 1 AS 00 _-4- as ZAA BG PEAI', HEIGHT (ABSORBANCE) C , 164 Cl. 13171 0 . C, =5 PEAK AREA (ABS-SECONDS) 0. 1315 0. 104 0 . 031 READ- 18. 1 OqA 17070 --- - -- - - - - -- -- -- --- - ---- --- - - ------ - ------------------ - --- --- --- -- -- - AA "AA B:_ PEAK HEiCHT '.ABSORBANCE) 0 . 148 0. 12'74 0 1 PEAK. AREA (ADS-SECONDS", C , 1:S 1 G , 104 0 . C?' READ- 1;. 13 ---- ---- ------- ---- ----- -- -- ----- -- - ----- -- - -------------------- - --- --------- MEAN= 1 U. 0 STD. DEV, = 0. 1 COEF.VAP... = 0,54 % 0000EEEEQ Q Q 014 2 EEEiFEE##iFEEEEEE�( tEEEEE#EEiFEE#+EEEEiFEE#EEExEEEEE*EEE4EEEEEE#EEE?!EE #E#E AS 00 ^5 AA ZAA BCJ r,?71 -- (`;. 1)?A . r Ci ,1A MEAN= 19. �3 STD. DEV. = 0, 5 COEF.VAR, = •�±��••�**�*;�**��•�•�•�•f��•*##•��•x•�?��•*�•�*� x•:�•**-�-�-��•�##�r��•+�#ifs#��#�•*##?�*�•�•�t�*��•= A S O O S S AA SAA EG PEAK HEIGHT (ABSOREANCE) G . C3_ 0, G 0 . 035 PEAK AREA (AES-SECONDS) 0 .284 0,?622 0. 023 READ; 4:, ' CGV3= 97% (16 "20 Alh) --- -- -- - --�--- - - - - - - -- - - - ------- - -------- ---- ----- ----------- ----- --- ------------ AA -ZAA PEAK HEIGHT (ADSORBANCE) 0 , 340 J. 15 C' , 036 FEAT: AREA (ABS-SECONDS) 0 . 2'?`? 0.'?;E 0 . G24 ' READ- ----------- - -- - ---- - ---- ----- -- ---- ---- ---- ---- -------- - ------ - --- -- ------ MEAN= 4S, 5 STD, DEV. = 2 0 CC'EF.VM'R, = 4, 1 ' - ' ��'*#�'��•��•X'��-1f�•�•��•�•X•i� ,��•'��+:IF �'?F?h�3F 'iF iF iF!!•�h i4.1F?L'$��jt#iFYt�saG:k?Fi('?i?F!'iF+:l�'1f'•�#��'�'.f�#��*44*- A S O O -4 AA r-iA Z'� n �C r ` C' 4 c ;� PEAT; HEIGHT {r1E��JRE�-�PJCE) U. � G . •- . _ G , G�1 FEAT: AREA (Ai 'SEt OND S) 01. 'J 1 1 '0. 0C i 11 . 0 1 READ; 0 , co ZAA B( PE: k:: HEIGHT (ABSORBANCE) , ODS 0. ro FEAT. AREA (AES-SECOND':,) 0. 010 0 . 0G3 0. 0!x; READ: 0. ----- -- ----- -- - - --- - - - -- --- - -- --- - - - - --- - --- ---- ---- ---- --- - - -- - - --- - --- - -- - - -- - ' MEAN= 0 . 4 STD. DEV. = 014 CCEF, b'At= , _ ? . E' >; >iE�tt�e#�•?E+k*+#iE+�?F#•ftp(-f�f#:!••lf �}�FiF#aE#�4:►#fit#?F# �#�t� k�e?E+iF•�+tiF•R#die#+4E#�•4iFi�{4+tiF4a+�4t��.a AA -ZAA Do PEAT: HEIGHT (ADS?RBANCE) 0 12E•17' 0,2,3= 0 . C'=Ell PEAT' AREA (ABS-SECONDS) 0, 0:i 0 , 1;3 0. 030 READ: 30 . 47' D' SPI1� - ------- - -- - - - -- -- - - --- -- -- - ---- - -- - ---- n- - - - -- - -- - --- ----- - ---- -----_ -tt --- - - --- _AfM PEAK HEIGHT (ABSORBANCE) 0. X54 J. _ 3'J „ PEAK AREr (ABE-SECONDS) 0 . 1211 0 , 193 6 . 018, REND: :34. 1 ' - ---- --- - --- -- ----- -- -- ----- - -------- --- --- -- ---- - --- - - --- --- -- ---- - --MEAN= ES STD. D v. = . COEF.VAR. = S.cD SAA F.G ' PEAK HEIGHT (ABSORBANCE ) . 062 G, 024 0 . 056 PEAK AREA (AFS-SECONDS) 0, 045 0. 001 0. 044 READ: 0 . 4 'WS7 -02 0 0 0 O l 4.3 -- ------- --- - - -- --- ---- - ---- - - - - --- ------ -- ------------------------- ----- - - - --- AA SAA F:% NYTEST ENVIRONMENTAL INC. ' F�JRNACE ANALYSIS RUN LOG ' ANALYST: A P/��•VMF.IP 'IEi�Tl` DATE. -DZT?.I.k-?r ID Q CALIBRE1 SON DATE: P J11 142 i LOGLN, 's: START TiNtE: ' END T1NIE. IN ZGIT.10`Ti:1:: 6.Q Sa S IAN 11./.7 SOURCE: ..l..�L..R S PC x ST A`'DARD LOT " 5 A-N-D ARD PRE?.yR.�.T!ON DATE: S �` i5XPIR�TiO : DATE:r ` 7iT ' ST A`DARD PRE?AR s.TiON LOGBOOi: PAGE =: L PP'REVIF—WED LE NA-Ml. 4CCE2T-\'CE L?�SIiS C0N1`:St\'TS I 1 90< (-!-) CRQL 90-110 - I < (+/-) CRQL I SO-120 or E?A LIMITSBLA`+K I < (=!-) CRQLi✓Y: 000014 .4 Q AA 7AA BG PEA,; HEIGHT (ABSORBANCE) 01007 0. 0071 0. 002 PEAK AREA (ABS-SECONDS) 0. 001 0, 002 -0. 001 READOOL -- --- --- ------ ---- -- -- --- ----------- -rr --------------- ---- --------- ------ ' AA SAA B� PEAk:: HEIGHT (ABSORBANCE) 0. 00; 0. 006 0. 002 PEAK AREA (AES-SECONDS) -0 , 001 0. 00=, -O . G04 ' READ; 0. 000 --- -- - - -- -- - --- - --- - -- -- --- ---- ---- -------- - ------- ----- - - --- -- - -- - --- MEAN= 0 , 00Cl. STD. DEV. = GG00 COEF, Vha , = 01 COG AUTO-ZERO AA -'^^ FG PEAK HEIGHT (ABSORE:ANCE) 1 . 085 0,841 0 ,_•45 ' PEAK AREA (ABS-SECOtdDS) 0. 610 0, 431 J, 129 READ: 0 . 47WO n - -------------------------- - ----- - - - --- - --- - - -- - ---- ---- - --- - -- -- ---- -- - - ----�. A^ ::. r1r, AA E,ti• PEAK HEIGHT (ABSORBANCE) 1 . 075 0 , 329 0 . —...— PEAK AR EA (ABS-SECONDS) 0. E.01 0.47- G, 12S ' READ: 0. 472 ----- - --- ---- - -------- --------------------------- ------- -- -- MEAN= 0, 475 STD. DEV. = 0 , 004 COEF.VAR. = 0. 92 7. 100 . 0 STANDARD 1 -j7_. AA ?AA p0 PEAF: HEIGHT (ABSORBANCE) 0. E17 0. 494 G. 124 PEAKAREA (ABS-SECONDS) 0, 24 0, 'EO G . 064 READ: 54. 2 --- - -- -- - - --- -- --- ------- ---- -- -- - --- --$ ------------------- -- ---- --- -- --- - --- AA ZAA Bc PEAK HEIGHT (ABSORDANCE) 0. 615 0. 49= 0, 124 PEAF: A1=:EA (AES-SECONDS) G, •J5 0,26 READ; 54, 3 ---- --- ---- - -- ----- ---- ------------ ------ -- - -- - -- - -- -- - - -- MEAN= 54. 5 STD. DEV. = 0. 4 COEF. VAR. = 0.70 % iFiF#1F#*�iE�aE��jFiE�F?F�FjF�EiEjF1F�F1F*1E�r�iFlE•IF*4iF�E4aF-1FiF�F#?FiFjF�FJE��jtiF#?EjF9Fi��Fi�F�EFtf}-kiF�F?Fit�F44#?4iFiF�44#3 5G . G STANDARD �E#*+*{�E#�E��{iF#iF�kjF,EiF -3tiFi� iF#�F�F1+FE�EiFaF?F��9E�F�E#�F�EiE�FIF*#�4iFiF�F�F�iF*iF�F�F�F�#tF�EIl1EJ�A�F49��FtiFifkt# AA 7AA BG PEAK HEIGHT (ABSOREANCE) 0. 3:B7 0.269 0 . 063 PEAK AREA (ABS-SECONDS) 0, 167 0. 1.9+6 0. 0E+1 READ: 24.6 --- - - -- - - - -- ---- --- ------------- ---------- -- ----- - - ---- (CONTINUED) AA SAA DG PEAK HEIGHT (ADSORDANCE) 0 . 33 0. 71 0 . 06;, ' PEAK AREA (ADS-SECONDS) 0. 170 0. 138 0 . 032 READ: 25. 1 ---- - ----- -------- --- - ----- -- - -- - ---- - --- --- ------------------------------- ----- ' MEAN= , S STD. Dt`Y'. = 0. COEF. VAR. = 1 . 27 X. '12,4, a STANDAP'D aFiFiFiFieiFiFt�taF##�t?F?F?##t##tyEtr��E4#+:� lF•k#ti+{•4ie�#?F#iF#.#'r.iF�FiF#+�Fz�F�#irtiF##ii4iF�E�FiE#?E itiF4?4#iF4iF• 1p E. AA Z A A DG ' PEAK HEIGHT (AESORE,ANCE) 0, 146 0. 1211 0 . 026 PEAK AREA (ADS-SECONDS) 0. 071 0 . 060 0 . 011 READ----- --- 1G .:3- - -- - ---- - ---- ---- --- --�Q- - ------------------------ ----- -------- ' AA SAA DG PEAK HEIGHT (ABSORBANCE ) x. 144 0. 118 0 . 026 PEAS: AREA (ADS-SECONDS) G, 0;.` 0 . 060 G. G1E' ' READ: 10 . 4 ----- - -- -------- - - -- --- - - - --- -- - - - -- - ---- -- -- --- -- ------- - ------- --- - ----- - ----- MEAN= 10 .3 STD, DEV. = 0, 0 COEF. VAR. = 0 .20 1E�iE9F#1F•lEk3E�E)E•kiE3F�(•-lE#3f?F?[iE�FaF#�F�##iF*t*iFiE'kjF*}iE?Ft?F��#*##�F�E?f9E#FiE*#?F*±F jt at#iFJh�iE#?FE?F jtiFiF?Fir-k�iEiE 10.5 STANDARD 4 �F•iFiF*�E�+�FiFt•]F�EjtiF##iFjF�FjF�F•!FIF�(-ifaF4ifiF�aF#iFlf�ir-1��FiF4?FjF�##��F�4iEiE3hiFi[•iEiiiF#��E�F��FiEiF#�jFiEiF#?4iEiFiE�#iFiE'. AA SAA DG PEAK HEIGHT (ADSORDANCE) 0. 075 0. 062 0 , 014 ' PEAK AREA (ABS-SECONDS) 0. 030. 0 . 0:61 0 . 0GO READ: 5. 0 5 AA SAA EG PEAK HEIGHT (ADSOREANCE ) . 0;'1 0. 053 0 . 014 PEAT; AREA (AES-SECONDS) 0 . 03= 0. 025 0 , 004 ' READ: 4, -------- - ----------- ---- -------- - - ---------- ------ ---------------- -- - --- - ---- --- ' MEAN= 4. 9 STD, DE"/. = 0 . 2 COEF, VAR, = 3. 21 % ?EiF�i•1(•iEiE#�F#4Yt?FiF#�(•'kiF4'd•i(•* Fir#iF�iE?4#�F��EiE4iEiF}t?E?FiE?FjFiFiE1F�#i!•4fiFlFi(•ihlF4iE�FiE�#lE1F?F�•IF1E?F�F�E?EjFt�(•#iF? 4.9 STANDARD aaa 0lgia i 1 1 �5 (CONTINUED) AA SAA SG PEAK HEIGHT (ABSORBANCE) 0.338 0.271 0 . 067 PEAK AREA (ADS-SECONDS) 0. 170 0 . 138 0 . 032 k-, � EAD., „��. 1 ' --- - -- ---- - ------- ----- --�------ -- --------- MEAN= �'�:. y STD. DE'�'. = 0' =; COEF. VAF:, = 1 . 2; 24. 9 STANDARD - AA ZAA D 1 PEAK HEIGHT (ABSORBANCE) 0. 14E 0. 121 0. 06 PEAK AREA (ADS-SECONDS) 0. 071 0 . 060 0 : .011 READ: 10.3 PEAK HEIGHT (ABSORBANCE) 0. 144 0. 1 13 0. 02E PEAK AREA (ADS-SECONDS) 0. 072 0. 060 0. 012 READ: 10. 4 ------ --- ---------- ------ -------- -------- ---- ------------ ---- ------- - ------- - --- ' MEAN= 10. 0 STD. DEV. = 0. 1 COEF. VAR. = 0.20 N. iO.S STANDARD 4 IE: AA SAA SG PEAK HEIGHT (ABSORBANCE) 0. 075 0. 062 0. 014 PEAS: AREA (ABS-SECONDS) 0. 0311-1 01031 01000 READ: 5. 0 :5 AA zAA EG PEAK HEIGHT (ABSORBANCE) 0, 071 0. 053 0. 014 PEAT: AREA (ADS-SECONDS) 0. 03:0 0. 02: 0 . 004 ' READ; 4.7 - ----- -- - ------------------------ ----------- -- -------------------- -- ------------ MEAN= 4.9 STD. DEV. = 0. 2 COEF. VAR. = 3. 21 f.. 4. '? STANDARD 5 000014,7 AA -ZAA FG PEAK HEIGHT t AFSORFANCE) 0, 994 0.776 0.220 ' PEAK AREA (AFS-SECONDS) 0.5.33 0, 427 01111 READ, - ---- ---Q7_. 4----- ---- - ---- ---- -- -LCX----- - --- -----jf•------- ---------- --- -- A A ----- ---------- --- --AA 2AA FG PEAT'.: HEIGHT (AE:SORDANCE) 0.95'3 0, 4:9 0 . ?I 0, 5?9 0. 426 G . 112 PEAT: AREA (AFS-c,SECONDS) i READ,. 87 , 4 ---- ----- ---- - ------ --------- ---- ---- ---- MEAN= 87. 4 STD. DEV. = 0 . 0 COEF,VAR. = 0. 02 'k ' dF#-iF#FSE?E�EiE.!E1E�r�Fx�taF�E#�*ir�F�F####?4#?(�iF?E-iEt#. #*�#jF#'�#�*f'�4#��**4�'jFir#1F+�FiEiEiEiFtyEieiriF�F�##�Fx# i 1 is ^ '.'G_ AA �� E r� ,� PEAT: HEIGHT (AFSORFANCE) � 4� 0. 005 G . G0 PEAK AREA (AFS-SECONDS) 0. 000 0. 001 -0 . 001 READ: -0,_ - -- - - - - --- - - ----- - ---- - - - - ----- - -- - ---- — ————————— — — ——— ————————— — — —— — ——— — — ———— r.r. i tiff E'l: ' PEAR; HEIGHT (AFSORFANCE) 0. 005 0. 006 0 . 002 PEAR: AREA (AES-SECONDS) -01001 0. 002 -0 . 004 ' READ; 0 . 0 MEAN= -------0. i -----STD, DEV, =--- ----0 .2' C:.,EF.VAF. = 99,99 '. AA 2NA BC, PEAR'. HEIGHT (AFSOPEANCE) G. 045 0. 03v 0. 006) ' PEAT: AREA (ADS-SECONDS) 0. 019 0 . 419 0 . 0010 READ; 'S* C' AA ZAA FG PEAK HEIGHT (ABSORBANCE) 0. 047 0. 041 01002. PEAT: AREA (ADS-SECONDS) 0. 021 0. 020 0 . 001 - READ: 3. ' ---- --- - -- --S --- -- MEAN= 3. 1TD. DEV. = 0. 1 COEF. VAR. = 3. 75 '% F: AA SAA FG ' PEAT' HEIGHT (AFSOPRANCE) 0. 600 0. 47'5 0. 126 PEAR; AREA (ABS-SECONDS) 0. 331 0. 21660. 01-55 0000148 0 0 O 15 8 READ: 51 , 0 0 11_ ---------------�Q�f- --------- - -- -- ' A------ --- -- - -- ------ I ; � -- -- - �--- / ^ 4- E;G _HEIGHT_ (AFSORFANCE) 0.610 0 . 456 0 . 126 - - - - - --- -- r .,r-rl - n_ nAA READ; 51 . 5 ------ --- ------------------------ ------------------------------------- ----------- MEAN= 51 .2 STD. DEV. = 0.5 COEF.VAR. 0, 54 % 2-3 I: AA SAA FC PEAK HEIGHT (ABSORBANCE` 0 . 005 0. 004 0. 002 ' PEAK AREA (ABS-SECONDS) -0. 001 0. 001 -01002 READ, 0' 2 - ---- ---- - ------- - ----- --------- ------------- --------------- -- --- --- AA Z_AA BG PEAK HEIGHT (ABSORBANCE) 0, 00.5 0, 005 0 . 001 PEAR AREA (ABS-SECONDS) -0. 002 0, 002 -0 . 004 ' READ: 0 . 0 - ---- ---- ------- --------- ------- - --- ---------------------- -------- -- - - --- - - - - --- MEAN= -0. 1 STD, DE'J, = 0. 1 C0EF. VAR. = 9S,9y ' 1riE!E+4tE+�#•lEt##�tiF?F#ifiE�'kaF?i+##�'.��t+�E�F}?F•!F#?F#�k3FiEw1FE3�#?4x}4it?FSE#:4t#�E�Fie'E#.�F4�t?Fj(-iF?F?t3�F?k t�F�#i F,E: O G 1 AA AA BG PEAK HEIGHT (ABSOREAPd�E` 0. 00x. 0. 00 0 . 001 PEAT: AREA (ABS-SECONDZ= o 0. 001 -0 . 005 READ- - --- - ----G. -- --- - ml_---- ---- - ------- -------- --- -- -- - - - - ' 2AA. BC PEAK HEIGHT (ABSORBAN0 . 004 ' PEAK AREA (ABS-SECOND0. 001 PEAL:; ' MEAN= -0 , E' S DEV COEF. VAR. = 10.79 -- --- - -- - - -- Y:E: O 0 1 :D AA SAA PO PEAK HEIGHT (ABSORBANCE) 0, 262' 0.2i2 0 . 051 PEAK AREA (ABS-SECONDS) 0Z= O 157 0. 114 0. 024 ' READ-- --- ---- - --f- - -- - - - ----- --------- - --- - - -- - - - - ' . . _10,� �6_A SAA BC:PEAF': HEiCHT i AESORBAP�1a�PEAK AREA (AES-SECONDS158 0. 1 1? 0 . c,^�READ: _ ___ __MEAN= 20. STCOEF. `v'AR. = 0 . 11 1 �'��7t3F1F?ElF�/- y��F#�#'k JE iE iE iF*-%"If�•�+�jF iE aE lF iF jttE�F•1FiEf'It�iE��({#i!#;F iE 1F il-iF�?F#1F iF�F#iF!!9E?F aF'� lFfi#��}?F{#+jF R�: O O 1 _4 L r AA SPC HA PEAK HEIGHT (ABSORBANCE) 0. 51 0, 409 0 . 105 PEAK AREA (ABS-SECONDS) 0. 86 0, 252 0 . 054 READ-- --- --- --- - 3 - --- - -ap--- ---j - ` -- SSG ----------------------- -- - - - - -- - -- ' AA PEAK HEIGHT (ABSORBANCE) 0.515 0 . 415 0 . 10E PEAK AREA (APS-SECONDS) 0. 255 0. 229 0. 055 READ: 4.3, .E 000019 ----- - --- ---- ---- --- -- ---- -- ------ ------------------------ ---------- ---- -- -- - --- ME'Ahl— no a eTr, r,r�� = n . rnrc . vcr. 11LPIIY� moi'1 v ..,!1 L • LL Y • - V .l YyVvy y�y y FIE* O O 1 AA ZAA D1:; PEAK HEIGHT (ADSOFDANCE) 0. 6912 0.550 0 . 145 PEAK: AREA (ADS-SECONDS) Z= 0, 0.31212 0 . 07 FEAR; 63.2 ' ---- ------------ - ------- -A--------------96--- ------ - - -- A' SAA BG PEAK HEIGHT (ABSORDANCE) 0,551 0. 150 PEAK AREA (AES-SECONDS) 0.319 0 . 077 ' READ; 612. 4 MEAN= 62.8 STD, EF• VAR. = 0,92 �F�E�t#iFiFiF�F�E#�FiEEiE�F#"1EiF1F#*�iF+E#�F�i� 1F*aF•�x}}*•��•�*iFiEjF"]E�tiF?EiF"iEiF fF4�Eit#iFiEiF#�t�F�?F?F?E�E�EiF�F�aF4?F#��F43 F-,F_: O O 1 6 AA SAA t'v PEA:-:: HEIGHT (ABSORBANCE) 0. 014 O. OGS 0 , 0012 PEA1". AREA (ABS-SECONDS) -0 .01 0, 001 -C , 002 ' FEAD; - --- - - -- - --- - --- ----- -- - - -- ---- --I- -39= -pis--------------- ---- - - - - ------ - -- - - AA SAA BG PEAK HEIGHT iABSORBAPJCE) 0. 01'?{ 0 , 004 0 . 002 PEAK ATEA (ABS-SECONDS) -0. 0012 0. 002 -0 . 004 ' READ-. 0, 0 - --- - MEAN= -0. 1 STD. DEV. = 0. 1 COEF.VAR. = 99. 99 ?E��Eir?Fk"iFt?F###1llE"1F#ktx?E"aE"YY#�f""!F'iFt4#f.itiF"k?4if"4iF"lF##jF��F?la4aEjF#iE#iF'E#"iF�F#�F�F?F��E#'k#*�E#iEaFiFye�E�?F3#i!+!- :E. 0 0 1 7' AA Z7AA DG ' PEAK HEIGHT (ABSORBANCE) 0. 1267 01.1215 0 . 05=' PEAK AREA :ADS-SECONDS) 0. 140 0, 115 0 . 025 FEAD— 20 . 6 - S Q A - - --- -- - - - - - - --- - - --- ------- - ------- - ---- ---- - -- --- - - ---- ------------1-3 , AA SAA E,��: PEAK: HEIGHT (ABSORBANCE) 0.269 0. 217 0 . 05:' PEAK ATEA (ABS-SECONDS) 0. 138 0. 115 0,221 READ; 1210 . 6 --- -- ---- - -- ------ - --- -- - f--- -- -- -- - - ----- - --- --- -- --- --- MEAN= 120 , E STD. DEV. = 0. 0 COEF.`"iAF. = 0 . 24 1. �F�FiF�iF�F?FjFjEjE��FiEif?F?4�l"'FiFiF�EiEil�FiFiEaF#iFiF�EiF#1FaE4�F#�FiF?E�EiF�t�F?Fri#iF1E#1FiE"Y.*iF+EiFiFi(iE*#jFiFiF�##'k'1E"1E "lF��iF�? ll: O 0 1 ' AA 2AA DG PEAK: HEIGHT (ABSORBANCE) 0. 399 0 .319 0 . 087 PEAR': AREA (AD'S-SECONDS) 0.222 0. 17 6 0 , 04c, ' FEAD- ---- ---?2' S--- -- -J13,33.9__1.__ s_ .2------------- -- --- - - - AA SAA B1Z PEAK: HEIGHT (ABSORBANCE) 01390 0, 310 0. 630 ' PEAK AREA (ABS-SECONDS) 0,220 0. 175 0. 045 READ: Ste. MEAN= 322. 4 STD. DEV, = 70.3COEF,VAN. = 0. 7;' % AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 589 0.466 0. 1214 PEAK AREA (AFS-SECONDS) 0.3228 0. 261 0. OC, READ: 49. 9 # ------ ------- - ------- ---Las-- - - --- -- - - 1 3 _� --,less-.212 --- ---- --- --94 . ' A ZAA DO, PEAK HEIGHT (ABSORDANCE ) 0 . 466 0 . 12 ' PEAS' AREA (ALS-SECONDS) 0, 'jar' 0, 2513 O. 06°• ' READ: 49 , 4 j-- - - - - -- - - -- ---- -- ----- ------ -- S --------- --- - -- -^-- - - -- --- - --- - --- - DIEMEAN= 49 . 7 STD 0 . 4 COEF. VAR. = C . 81 r. F,3 E: 0 0 :2 0 ' AA ZAA PC PEAK HEIGHT (ABSORDANC E) 0 . 4?._ 0 , 374 0. 100 PEAK AREA (AFS-SECONDS) 0. �8a 0. �?4 0, 064 ' READ- ----- --4i♦ -- ---- - - - - - --- - - -- - 3 3 _7_01 ---------- -------- ---- -------- --- AA AA DCS PEAK HEIGHT (ADSORDANCE) 0. 466 0, :i-: p 0, 097 PEAK AREA (ADS-SECONDS) 0. �8' 0 , 065 1 . 8 READ- ---- ---- --------- ---- --- - ------- ----- --- ---------------- -------- ---------- - MEAN= 422. 0 STD. DEV. = 0.3 COEF.VAR. = O . e? % ' Fl El 0 O 7 1 AA ZAA BG PEAK HEIGHT (ADSORBANCE) X= co) 0.511 0 . 198 ' FEAK AREA (ADS-SECONDS) . 307 0 . 0'90 READ--- - ----- - -- ----- - --- - - - - -- ---- ------- - ---------�------ - - - - -- ' ' ZAA ' DC PEAK HEIGHT (APSORDANCE) 0. 51:' 0 . 140 PEAK AREA (ADS-SECONDS) 0.: 08 p , p o o READ: 60, 0 MEAN= 59, 9 STD, D. OEF. VAR, = 0 . 11 �E#�?F?F-1E9E�E]E4jE�tiFiF4#�EiE #�FiF��E�*�*�*.j��EaE fF�F�#�E�#�F 7F-1FaE�F:�#?F*#-IE�iFiFit�jF?FiFjF�tiEiF#ifiFaF�F1F1F�EiF##444iF#+ 1p F' 0 0 AA SAA D ' PEAK HEIGHT (ABSORBANCE) 01508 0. 482 0. 1,26 PEAK AREA (ABS-SECONDS) 0, :9 .9 0. -41612, 0. 061 READ: 50 . 10 0 0 01. 51 ' - -------- - ---- ------- ---- `--P --- --L; ------------- ---- --- 100 -- ------ - -- - PEAK. HEIGHT (ABSORBANCE) 0. 612' 0.438 0 . 12'6 PEAT; AREA (AES-SECONDS) 0. 32'6 0.2'62' 0 . 064 ' READ-. 50 . 0 ----- ------------ ---- --------------- -------- -- ------ ----------------- --- -------- MEAN= 50. 1 STD. DEV, = 0. 1 COEF, VAR, = 0 . 15 % i2'4i2'iFiEiE?F4iF?F4iFiEiF44iFiE k444iE�?ti2'4444444iF12'#444�ir44�##iFiF:4iFiEi2'iFi2'4iEiEi2'j2'44E4iF4444444444444i2'4? AA ZAA BG PEAT; HEIGHT (ABSORBANCE) 0, 0013 01004 0 . 002' ' PEAK. AREA (ARS-SECONDS) -0. 001 0. 001 -0 . 002' 13 READ---------0------- --- ----- -------- ------------------------- ---- -------- ' A ZAA BG PEAK HEIGHT (ADSOPBANCE) 0 . 006 0. 006 0, 002 ' PEAK. AREA (ADS-SECONDS) -0 . 002' 0, 002' -O. CC14 ' READ0 . 1 --------- --------- ---- ---- - ----- ----------- - ----------- ---- - --- -- -- ------- MEAN= -0. 2 STD. DEV. = 0. 1 COEF. VAR. = 50. 63 K. ' #iFii?E�iEiF-IF?FiF?E?e!FiEiF+#iFE#iF?EiEt?F?E#�ir?F1Fe##*#?F?FIEiEEiE'iF�##1F'rEIF?E#i2'?t?Ft###iF�it?2'4#?E*?F4#4�'.� 1Fs?E�4aE�+ ' Pte: 0 O AA nA BMJ PEAL: HEIGHT (ABSORDANCE) O . 3. 4 0.2'63 G , 060 PEAK: AREA (ADS-SECONDS) 0, 164 0, 135 0. 0:90 READ- 24. 4 3 - -------- ---- -------- ---49)(-- ----- -�33-�-0'` --------------- ---- - - - --- ----- - - -- ' AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 3.37' 0. 2'63 0, 069 PEAK AREA (ABS-SECONDS) 0 . 167 0. 135 0. 0:92' ' READ: �4, ------ --- -- - '- -+----- ------------------- ------------------------- -- - --- - -- - - - - -- MEAN= 2'24. 4 STD, DEV. = 0. 0 COEF,VAR, = 0. 15 'K i�F-iyF i2'iF iF iF i2'if'i2''IF 1r?E'iF iF iF'!�i2''':t 1F iF'12''iF iF t i('i2'ih it?F iF iF iF iF iF?F t#i2'iF�F 4 iF iF if ?�!F i2'iF iF iF i2'iF*'12'iF if i!'iF iF i2'iF iF iF iF iF iF iF;f#�#it iF iF Y*?E iF ih i. AA ZAA BG ' PEAK HEIGHT (ABSORBANCE) 0. 566 0.446 0. 1:'0 PEAK: AREA (RBS-SECONDS) 0. 2''36 0.29 0 . 057 READ-- --- --------------- ----- - - -- ---- Q' ---- - ------------7-� ---- -- --- -- ---- ' AA LAA DG PEAK: HEIGHT (ABSORBANCE) 0.57.3 0, 452' 0. 12'1 PEAK AREA (ABS-SECONDS-) 0. 2'37 0.2237 0 , 059 READ- 42'. 9 ----- -------- - -- --------- - --- - --- - --------------------------- ---- --- - -- - -- -- ---- MEAN= 43. 0 STD. DEV, = 0.2 COEF. VAR. = 0 . 51 % f YD F: 0 O 2!Cl AA ZAA DG PEAK HEIGHT (ADSORDANCE) 0, 267' 0. 2'1'3 0 . 054 PEAK AREA (ADS-SECONDS) 0, 1:90 0, 105 0, 02'5 123 ' READ -------- 18, i-- ---------- ---- - - ------- ---- ----- -- Z ----- ---- ----- -- ZAA DG PEAK HEIGHT (ABSORBANCE) . 263 0. 211 0. 052 PEAK AREA (ADS-SECONDS) 0. 127 0. 105 0. 02 READ: 131E ---- ----- ---- - ---- ------ ------ --- --- ---------------------------------------- -- - MEAN= 18. E STD. DE'J, - 0. 1 COEF.`JAR. = 0.3 }�E: 4 O AA 2AA DG PEAK HEIGHT (ABSORDANCE) 0. 4136 0.3138 0. 100 PEAK AREA (AES-SECONDS) 0, 247 012'00G. 047 READ-. 37, 2 - -------- ---- -- - ---- -- ---- --- ---- - -- -- -- --- ---- ---- --------- I--E_ ---- - - - - - -"" 'n inn ;�_ PEAK HEIGHT (ADSORBANCE' 0. 437 0, 399 010`?8 PEAK ARE^, (ADS-SECONDS) G, ��'..' G. 2G7' C . G46 READ- 3716 -- --- ---- -- -- --- - -------- -----/' -- ------------- -- - - -- -- - - - MEAN= ^, 4 STD, DE'V. =/ - ---0. ��-- -- -COEF. VAR. = G.,�2 �['iEit�F#?EBF+:'�FiF}!#�F'1F'1F###�'1F��F:l�F4 '}.'*#?E?EiEiF#aFP('#+'iEjF9F##iF#-k�['iF-1FaE+!'*�('��FiF'lE'iR'iFjF*iE�('?F#iF�'#iF?F3E�F�aFiF4iFiFjt �: 0 0 =O AA SAA BG PEAK HEIGHT (ADSORBANCE) 0. 280 0 , 228 C' , 05c PEAK AREA (ADS-SECONDS) 01133 0. 113 0 , 025 READ-- --- --- -------- - - ----- ----- -- ------- --- - - - -- A A E n Lf1iti G PEAK HEIGHT (rBSOR�ANCE 0.2$0 0, 221 0 , 061 PEAK AREA (AES-SECONDS) 0. 140 0, 112 G . 012S READ- 20 . 0 -- -- - - --- ---- -- - -- --- - -- - --- - --- - --- - --- ------ ------------------ ------ - - --- - --- MEAN= 20 , 1 STD. D7-V. = C / COEF, VAR, = 1 . 11 !. 41F�FiEiF'�F?riE#�FiE#�E�F�#iFiF4iF��F�F#�E?4�F�F#iE##�F?E#�FiFitiFir#tt. '.4�E# lr#. #iFiFiEiFiFjE�t��FiF�F*�FiE�E�iFiFjFiFiFiEiEjE3(# 1F��E##iF �]E AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 03- 0. 031 0. 007 PEAK AREA (ADS-SECONDS) 0 . 01t, 0 , 015 01000 DEAD: 2. 2 J3339r l02 -- ---- --- --- - --- - -- - - - --- - --- - -- ---- ------- -- - --------------- ---- --- - --- - -- - - - - - . AA 2AA B'- PEAK HEIGHT (ABSORDANCE) /= C,. , 041 0. 034 0. 00 PEAT: AREA (A3S-SECONDS) . 019 0. C17 0 . 002 ' READ----- ---- , 6-- - ------ - ---------------------- ------- - -- - ---- -- -- MEAN= 2, 4 STD, DE COEF. VAR. = 12, 07 7, 00001513' 4*�E*iF�F�F?E#iE�F�FiE�E1F�iE#�FiE�F##iF�iFiEiF�FiE#;f*-1EiF*aFiEaE9F*iEiEiFjFiFiF�EjFiF�jFEiEib1FIFiE��iFiF-IF�F?F3F�if�3FiF�*�*�FiEiE�EiF PEAK HEIGHT (ADSORDANCE) 0, 289 0.228 0 . Oc2 PEAS: AREA (ADS-SECONDS) 0, 162 0. 128 0 . 031:_ READ-= ----- --- --------------------- � _339_= -------------------- 11��-- ---- ---- A SAA DG PEAK HEIGHT (ABSORBANCE) .277' 0.219 0, 058 PEAS: AREA (ADS-SECONDS) 0. 160 0. 12' 0 . 032 READ: 22. 9 MEAN= 23, 0 STD. DEV X= 0. 1 COEF.VAR. = 0. 55 % 1-'F: O O :D 1 AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0.601 0, 468 0. 134 PEAk:: ATEA 0.3321 0 . 26' 0. 01-14 READ----- ---c1 • --- - ------ - - -1p,�1- - 3------ -------- - - --- --- - - - - - -- AA SAA Bt; PEAK HEIGHT (ABSORBANCE) 0.609 0. 474 0 . 1.9r+ PEAK AREA (ABS-SECONDS) 0.336 0.265 0 . 0'0 READ: 50. 8 MEAN= --- - --11 . 0- - ---STD, DEV . =----- --0. 31-----CGEF. VAR. =-_C . ta--%------ -- - - - --- - -- 1P 1E. 0 0 :D AA 7AA BG PEAK HEIGHT (ABSORBANCE) 0. 00:= 0 , 005 0 , 002 PEAK AREA (ADS-SECONDS) -0. 002 0. 001 ' READ - --- - --- -0.2-- --•• -- -- - -- ------ -----a ------- -- - -------- ------- - --- - --- - - - - A A i 2AA B4O PEA':., HEIGHT (ABSORBANCE) 0. 0019 01004 0 . 001 PEAS; AREA (ABS-SECONDS) -0. 00 0 . 000 -4 . 004 READ: -0. 4 MEAN= ---- - --0 , ::,-----STD, DEV, =----- --G. 1 -----GOEF, VAR. =--_'8 , 16-%----- - - -- -- --- - -- I-"-,:E: O O :=s:=s AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0, 004 G. 001=1 0 . 001 PEAK AREA (ABS-SECONDS) -01001 0. 004 -01004 READ---- - - --- - - - - ----� -P-W-- - ------- ------------- --- -- - - - --- AA Z A A DG PEAS; HEIGHT (ABSORBANCE) 0. 004 0. 005 0. 002 PEAT: AREA (ABS-SECONDS) -0 . 001 0. 001 -0 . 002 READ-------- - - ------- --- - ---- ---- -------------------- ---------- � d - 5 --- - - -- mrnni- r n c•rn nr,; = r. . � rn�.. . �;c�'. = as . as ,� 11Ly-1111yV�Y y LY]LV• Vy,y yy yJy y! yLr r Ly Vy•y rY— y y]G,yy y �y. •y Ly.y y�][y][vyYv ay-a ♦Y ♦fryr ay.]rCy yyry�y♦y.y.�Yy�Yyy yyy� Y Y,yy y aE't ae aF��l♦*aF�*aE aE�'aE at aF'lF aF]f�']♦aE ae a�*aE T aF aF iF aF'X�{"aF aE]C*aE aE of aE aF aE�7!'4 F]C�c if']f]C 1C'1♦lC'IC]C]C� r T"Ir if�f]C�]['1C]C��f��F�1 FM El O0 -D-4 AA SAA DG PEAK HEIGHT (ADSORBANCE) 01. 26.3 0.215 0 . 050 PEAK AREA (ADS-SECONDS) 0. 137 0 . 112 0. 025 READ: -- -20, 0 -- -- - ----�3,W.2 -k13-#25--------1��1n1E4--- ---------/ov/--- ----- ---- -- --- AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0.2G3 0.214 0 . 054 PEAK AREA (ABS-SECONDS) 0. 1='F 0, 113 0 . 024 READ- 20 . 2 ----- --- - --- - ------------------------------------ ------------------------------- MEAN= 20. 1 STD, DEV, = 0.2 COEF,VAF'., = 0, 81 ' i�aF�EtiFiFE?t+FiFit#�FiF#iF�EiE�F+:+'lh-1F'3E�##YaEitiE��FiEiEiF#�F'iFiF�9F'1F�E�FiF-�'iF�F�##jF*�FiF*EiE1ESE#'iF�EyE��FiE�EiE{iE��i?��E##?FSE+ AA SAA DG PEAK. HEIGHT (ABSORBANCE) 0. 527 . , 42 0 . 107 PEAK. AREA (ABS-SECONDS) 0 ,285 2:3 1 0, 0 f5 READ- 43, E -- -- ---- - ---- - -- -- - ----�X---- - --�3 =��_ J34.�S-"-- --- --------------- — _ AA 2AA BG PEAK. HEIGHT (ABSORBANCE) 0.540 0 , 423 0 . 117 PEAK ATEA (ADS-SECONDS) 0. 287 0. 227 0 . 0E,0 READ-. 42', 8 .,- --- - -- -- - --- ---- ---- ---- - ---- ---- ---------------- ---- ------- ------- - - ---- -- -- -- ''' MEAN= ti , 2 S�TI , DEV. = 0.6 COEF, VAR, = 1 .36 X � r4ak�txiF�r+�it9E+.�F'1F�#iF'1F�#?F4-)E-?tEiF+FjFiE�iF��F�F7F?raft#-!F1F'Y;K*#iF?FiFiE��FE'?F�iFiF�#iF1F�F�#f?F�4e*?('�#SFE#'�xaF�'if AA 'AA DG PEAK. HEIGHT (ABSORBANCE) G, ;I3 0.55E G. 152. PEAK AREA (ADS-SECONDS) 0. 40i . :E18 C , 021 READ_---- -- - - ,---------- ----- - - - - -----=-�44 ----- ------ -- -l3 ----- -- -- - - -- I� AA 2AA EG PEAK HEIGHT (ABSORBANCE) 0 >/',2,10 C , 562 0, 162 PEAS; AREA (ABS-SECONDS) 0. 3938 0.31., 0. 08= READ: 61 . 5 -- ---- ------- - - ------------ ------------------ ---- -- ---------- ------- ------ - - ---- MEAN= E1 . 8 STD. DEV, = 0, 5 COEF. VAR. = 0.65 . �'#*;�*of ae a�ar aE aE at#aE aE#at ae f aE ae aE##at#at a�aE ae aE aE ae aE aE ae at aE;<*aE aE aE aE aE at ae aF of aE ae aF aE aE~r of aE aE aE a�aE ae ae aE aE of aE aE aE�of of of aE aF at a�aE R E: G O -_l AA 2AA DG PEAK. HEIGHT (ABSORBANCE) 0. 07 5 0. 03-1 C, . PEAK AREA (ADS-SECONDS) 0. 041 0 , 02: 01020 READ- 3. -- -- ------ ---- ---- Q --------- -------- ---- -------- -- - ---- EG PEA}; HEIGHT (ABSORBANCE" 0. OA7 0. 038 0 d 0 015 5�,# 041 PEAk; AREA (ABS-SECONDS) 0. 041 0. 020 0. 02'1 READ: - 2 - -------- --------- ----------- --- -- ----------------------- ------------- -- ----- --- MEAN= 3. 1-7 STD. DE'.'. = 0. 1 COEF,VAR, _ 23. 90 % AA 2AA BG PEAK HEIGHT (ABSORE:ANCE) 0. 332 0.237' 0. 095 PEAK AREA (ABS-SC-CONDS) 0. 183 0. 1.54 0. 049 READ: 24, E ---- ----- ---- ---- - -- - --- - ---- -----1--3,0�«=Oa-,4------- --- - -----L0 �------ --- AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0, 241 0. 096 PEAK AREA (ABS-SECONDS) 0. 182 0. 13 0 , 051 READ: 23, 7 - --- - - - - - ---- ------- - --�--- --- - - ----_-- -- - --- _ - --- -------- ---- - --- --- MEAN- _ETL , L_r . V0. 2_ C0_F. AF. 1 4 iEx###±F�+####iF�FIEf#�F�Ff+#?Ff•1F4�##�4+- p10 g p :Dso AA ZAA E:C; PEAK HEIGHT (ABSORDANCE) 0. 046 G. G21 G. O='= PEAK AREA (ADS-SECCONDS) 0. 021 O . G13 0, 008 READ. 119 ----------- ------MW (SC7W AA 2AA -E'r`-- -- - - - - PEAK HEIGHT ABSORBANCE) 0. 048 0, 02712' 0, 026 DEAF: AREA (ABS-SECONDS) 0, 0 :23 0. 011 0. 012 READ. 1 . E - - --- - -- - ---- - -- - -- -- --- ----- --- -- -- - --- ----- ------ ------------------ -- -- ---- --- MEAN= : , 7 STD. DE\t. = 0,2 CLEF.VAR, = 1 10 % +F�E�F�F�F�F?��F#iFt#?F�4��F�(-1F�4#�F*��##}�F*# 1F�F��E::�F�EiF�iF*�iF�iE:rt�F#iF###iF��F*�F:4+.�FiF?FifiF�F�F�##ft*•�r4�F�. Fn E: 00 -40 AA SAA yy PEAK HEIGHT (ABSORBANCE) 0 , 314 0.x'81 0 . 08? PEAS:: AREA ( ABS-SECONDS) 0, 16:. G, 122 0. 0 :1 REAL:; 0 e ----- ---------- -1�0 AA 2AA BG - ------ - ----- - -- - --- -- -- -- --- ---- - --- - - �-- ---- --- - - - PEAK HEIGHT (ABSORBANCE) 0. 314 0. 2'34 0 , 081 PEAK AREA (ABS-SECONDS) 0 , 16 0. 12111 0 . 041: PEAD: 22. 0 - ----- -- - --- ---- - --- ---- - ---- - --- - -- - ----- ----------------------- - --- - --- --- - - -- MEAN= 221, 0 STD, DEV. = 0. 0 C('jEF,VAR. = 0 . 00 . 1FiF�jEiF#�FaEjE-lE?E#aE#�F�-)FiFiF'.FjF*�?FjF#*iF�##?F?4#.iF-k ir*iEiF�(-�F9EjFjF9F#jF-fi*iFiEaFIF-1F##�F?E�#�EiF#'rF?E it#*#�iF*'k'lEiFiF'.FF� 2,E� C) O -i- 1 AA2AA BG PEAK HEIGHT (ABSORBANCE) G. 122 0. 082 0. 042 PEAK AREA (ABS-SECONDS) 0. 069 0, 047 0. 022 READ: ;, s 000015-6 �' ----— —--- —--- —-- --------—-—-— ——----- ——----- — ------------—---- —---—----—- — -— — — — -- PEAK HEIGHT (ABSORBANCE) 0. 125 0. 084 0. 042 PEAS; AREA (AES-SECONDS) 0. 071 0. 0;S 0. 023 READ: 3. 2 J 3�J-12 - 03 MWIDGvq MEA MN= ---- ---8. 1 =----STD, DEV, =--- -C,. `-----COEF, VAR. = 27. 07 --%----------- -- --- iE-1F{###iE##i######iF3E1F7F�I'################9######iF######'7F#####if'##�E1E##################f�E F O O -'t AA tAA DG PEAK HEIGHT (ABSORBANCE) 0. 370 0.278 0. 09.3 PEAK AREA (ADS-EECOND5) 0. 205 0. 153 0, 051 READ ----- ---27.9 ---------------- - -- ----o 3 ------------------- oa� ---------- - y- AA _ZAA DG PEAS: HEIGHT (ABSORDANCE) C.37 0q 2 PEAK' AREA (ADS-SECONDS) 0, 204 0; 14 0 . 051 RED: O -- --- - --- - -^` ---- - --c----E--- MEAPJ= ��, G STD, DLV, = 0: 1 0-:1-8 <. ##-lEt#�E1F##iEa4''l.#E#�F#ikiF#'#iE it#iF####1F44#il'!F1r##1t4#it#1F4t.+t:iE#rt##?F###�iElt####it+'aF#t## 1F�F?E�t#iF'E# 2,T--: O O -4:D - AA ZAA B. PEAT: HEIGHT (ABSORBANCE) O. GE4 0. 51_ 0 , 145 PEAK AREA (ADS-SECONDS) 0. 323 0 . 254 0. 069 READ: 48. 4 CSV --------- - ---- ------- -------6_: P- - ----- - --- --- ---- --- ----971---------- - - -- A y 'ZAA DG PEAK HEIGHT (ABSORDANCE) 0. E523 0, 51E 0 . 143 PEAk: AREA (ABS-SECONDS) 0. 324 G. 256 0 . 06-0- READ: . OECREAD: --- - -48, 8- ----- -- - ------------ ---- --- ---- ----- ---------------------- --- ------ - -- MEAN= 48. E STD, DEV. = 0. COEF,VAR. = 0. 61 % AA ZAA PEmY. HEIGHT (AESORBANCE) 0. 004 01004 G. 002 PEAS: AREA (ADS-SECONDS) -0 . 001 0. 001 -0 , 002 NERD: O. 3 - ---- ---- --- - -------- --- - --- - - --- - ---- -- - -------------- .----------------- ---- - -- - AA PEAS. HEIGHT (ABSORDANCE) 0. 004 0, 005 0 . 02 PEAK AREA (ADS-SECONDS) -0. 001 01002 -0 , 00 READ: -0. 1 ---------- -- -- --- -- --- ------- -- - ------------- --------- ---- ------------- - -- --- - - - MEAN= -0 . 2 STD. DEV. = 0. 1 COEF.VAR. = 53. G 0 0 015 i AA SAA D[, PEAK HEIGHT (ABSORBANCE) 0. 120 0. 0=,0 0, na2 PEAK AREA (ADS-SECONDS) 0. 064 0. 017' 0 . 047 2, 6 READ-- --- --------- ---- ------- --- - ---- ------------------------------------- ------ AA Z-AA FG PEAT; HEIGHT (ABSORBANCE) 0. 122 0. 029 0. 034 PEAK AREA (ABS-SECONDS) 0. 06.3 0. 015 0. 041 ; 3 � M --------- --- ------------- --- -- -- = ------------------ WD--- -- -- MEAN= 2, 5 STD. DEV. = 0. 2 COEF.VAR. = 8. 90 % F,IE: 0 0 -4c- AA EAA BG PEAL; HEIGHT (ABSOPE:ANOE) G. :0,0 0.230 0. 141 PEAK. AREA (ABS-SECONDS) 0. 193 0. 125 READ: 22. 5 -- ---- -- - --- - ---- --- - - --- ---- - --- --------_� _�_ __-____-______- -------- - -- A&i ABG PEAK. HEIGHT (ABSORBANCE) 0. 317,71 0. 144 PEAK AREA (AES-SECONDS). 0, 197 0, 12E 0 . 071 READ: 22. 6 MEAN= 22. 6 STD. DEV. = 0, 1 COEF.VAF. = 4 . _C, 1. ?F�F�E�tiF3E�E�tiFiE#�EaF4�FtYiE�E�F�E?E�F�#iFaE�FiFY�-iE#?F#�F'kiE?E##�+riFiFiE,t*E?EiE*�iF#iFiF4�flEiFiFir�E�F#44iF�F��F?E�FiE*iFiFiE? 2�E: 0 0 AA ZAA DG PERF: HEIGHT (APSORBANCE) 0, 21E 0. 024 0 , 194 PEAK: AREA (ABS-SECONDS) 0, 11, 0. 011 01106 t=.EAD; 1 . 5 TAW 2SGm - - ---- ---- -- -- - --------- - ---�3��s--- -----01- - ----------- ---- --- --------- - -- - AA SAA DG PEAS: HE I OHT (ABSO'tRDANCE) 0.214 0. 021 0. 194 PEAK AREA (ABS-SECONDS) G . 114 0. 011 - 0 103 READ: 1 - 5 - ----- ---- --------------- ---------- ---- -------------------- ------ - ----- - -- MEAN= 1 , 5 STE,, DEV. = 0 . 0 COEF.VAR. = 3. 05 #�EiF*iF4�FiE�E##�F�E1E:Ear*#iFaF4�E��EiE#�F�E�F�FtEiEiFiF�E?kiEiF#i��F?EBF#it.+�F�E�Ef�E�iFiF�F�F�F*�F�FiF�F*iEiE�E�F#�E�F��F*�F#�F�F?�; AA SAA BG - PEAK HEIGHT (ABSORBANCE) 0, 500 G.25r� 0 . 245 PEAK. AREA (ABS-SECONDS) 0.244 0, 12? 0 . 122 READ21 , 9 -O/ A 0 ----- - - -- ---- -- - - --- ----- ---- --- ----- - ----------- ---- ----- 1� -/-- --- -- - - - - -- AA 2=,A EG PEAK; HEIGHT (ABSORBANCE) 0. 49 0. 249 0, 242 PEAK AREA (ABS-SECONDS) 0.24: 0. 123 G . 120 READ----- ------ 2- ---- --- ----- ----- -- - ----------------------------- ---- MEAN= 22. 0 STD. DEV. = 0. 2 COEF.VAR. = 0. ,:= % 0-90U 5-9 2,E: 00 -4s PEAK HEIGHT (ABSORBANCE) 0 . 172 0. C12 0. 15E PEAS: AREA (ABS-SECONDS) 0. 092 0 , 010 0. 083 READ- 1 . 3 MW?)SGW AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0. 175 0. 020 0, 15E PEAK AREA (ABS-SECONDS) 0 . 092 0. 011 0. 082 READ. 1 . 4 --------- ---- -------- --------- ---- - -- ------- ---- ------------- ---- ---- --- ---- ---- MEAN= 1 . 4 STD, DEV. = 0, 1 COEF.VAR, = 5. 317 F'IE: 0050 AA 2AA BG PEAL: HEIGHT (ABSORBANCE) 0 , 4 0.1-7131 0. 20E PEAK AREA (ABS-SECONDS) 0. 230 0 . 122 0 . 1 +8 READ------ -- r- - ---- -- - - - --- -- - - - - - - ----- -------- ---- - / --- --- - -- - - -Da2�-- -�1� AA :Ari BC PEAK HEIGHT (ABSOREANCE) 0 . 44E, 0 0. 210 PEAK AREA (ABS-SECONDS) 0 1,2132, 0, 123 0. 110 READ.- 22, 1 MEAN= ----- -22, 0-- ---STD, DEV. _- -- - ---C , 1 -- -- -COEF. VAI=:, = 0. 44- -�------------- - - -- iEiF*#iF�F�('iF�'�('iF3E4#+f'iEIEjF#'�FiE�'�F*#1E*#��E?F+iF#*jFi#jt1#t**jFt� t !i+#jEaFiF##*3r4#jl'11E#t�i�G4�#+fir*�'3t1tiltiF'1: F:'E: 0 0 !5 1 L AA Z A A Eel; PEA:' HEIGHT (ABSORBANCE) 0, 1 E,2 0 . 026 0. PEAK AREA (ADS-SECONDS) 0. 0 4 0. 013 0 . 0;0 READ- --- - - -- - --- - - --- ----------- --- ----------- -------- ----- -- - --- A A - ----------- ------- - - ---AA 2AA BG PEA':: HEIGHT (ABSORDANCE) 0. 1 E2 0 , 027 0 . 13c PEAT; AREA (ADS-SECONDS" 0, 08:= 0. 014 C. 06 MEAN= 2. 0 STD. DEV. = 0 . 1 COEF.VAF. = =:E- `/. �E� 005^ AA 2AA BG PEAT: HEIGHT (ADSORDANCE) 0. 400 0 . 222 0 , 181 PEAK AREA (ABS-SECONDS) 0 . 220 0 . 124 0 . 09E READ, 222. 4 �3 f} - ----- --- -------- - -- ---- -- --- --- -- ------ - --- - ----------------- //°2- - - ----- -- - - -- AA =AA BG PEAK HEIGHT (ABSORBANCE) 0. 40E 0 . 22E O . 1SE PEAK AREA (AES-SECONDS) 0 . 22'2 0. 12E 0. 097 READ 22. E 0000159 ; --------- ---- ---- --- - -- - - ---- s cern nrir I ILP91V- 1 L, L/LY • - V.� vv�• . .•.. • v • r • r. il'iF iF�F�E�F?F dE iE�F•)F?F?E#iE#iE'�iF�('jF iF*iF'.E iF'4'�*�E�?F iE iF?('aF*aF je jF iF iF'lF�*•A'#�('�('i('#iE iF iF?F 9E 9E iF�F�E'3l'iE iF iF iF�('?F 9E�('jF 9E iF#*it�F iF jE F,F: O 015:-i AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 204 0. 040 0 . 166 PEAS:: AREA (ABS-SECONDS) 0. 104 0. 018 0. 086 READ: 2. 8 --------------- ---- AA -AA "7AA BIG PEA1; HEIGHT (ABSORBANCE) 0.206 0. 0:68 0. 167 PEAT; AREA (ABS-SECONDS) 0. 107 C, 0 123 C, 0 . 087 READ: S, 1 - - ----------- ---- ---- --- -- --- --- - - ---------- ----- -------- ----------- - ----- -- ---- MEAN= 2.S STD, DEV, :-, 0,3 CCIEs,VAR. = 8,55 °,4. F,IDO45-4- AA rim BG PEAS: HEIGHT (ABSORBANCE) 0 . 474 0.254 0 . 2 '0 PEAK AREA (ABS-SECONDS) 0, 24.i 0 . 13 10 READ- -- -----.- - -' ----- --- - -------- - --- ---'D l- A -- ------------ --�1 ---- --- - - - - y PEAK HEIGHT (ABSORBANCE) 0. 47.5 0, 25:j 0. ?21 PEAK AREA (AES-SECONDS) 0. 244 0. 130 0. 114 READ; '23. 4 --------- - -- - --- - ---- ---- ---- ---- - ---------- - - - --- ---- -- -- --- ----- - - ---- - - -- -- -- MEAN= 23.4 STD. DEV. = 0. 0 COEr.VAR. = 0 . 13 tik F"JE: 0 055 AA A A EG PEAL: HEIGHT (ABSORBANCE) 0. E8lf 0. 52b 0. 11 PEAK AREA (ABS-SECONDS) 0. .526 0. 255 01071 READ- --- ----48, - - ------- - - =F1 � -- -- - - - ------- ----- --- -- -,/- ---- --- ---- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.688 0 . 526 0 , 16: I PEAK AREA (ABS-SECONDS) 0. 328 0. 257 0 . 07Z, READ: 4E! . 0 MEAN= 48. S STD. DEV. 0. •lE•1FiF�F?F*jEjFjE+E#•x*lEiF4��F�E•#*#i.•#iF?EiF#*iE�'�iE#*�k•f#�iF�4'1E��(.#iE}#*4?FiF*�•?r#iEiF'F�F?F�jEi(#�EiF�F1Fit*•lF•IF�aE#�F?F�4�F 2,E: O Q 5C, AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 004 0. 005 0 . 002' PEAK AREA (ABS-SECONDS) 0. 000 0. 002 -0 , 0 22 READ: -0 . 1 (,C6 0000100 - ------------ ------ -- --- - --------------- ----- --------- ---- - - - -------- ----- --- - -- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 005 0. 005 0 . 002 PEAK AREA (ADS-SECONDS) 0. 002 0. 003 -0 . 001 READ: 0, 1 MEAN= 0 . 0 STD. DEV, = 0. 1 COEF.VAR. = 99.99 . E'E. 0 0 5-- AA SAA BG PEAL: HEIGHT (ABSOPBANCE) 0 , 202 0. 0338 0. 164 PEAK AREA (ABS-SECONDS) 0. 10 0. 021 0 . Os� READ-. := _ S MW CoOGW D - --- -- --- -- - - - --- ---- ---- - -- - --- - --- -�3 - - -------� �(, �------- ----- - -- --- AA ZAA BG PEA}; HEIGHT (ABSORBANCE! 0 . 203 0. 0:33 0 . 165 PEAK AREA (AFS-SECONDS) G . 105 0 . 085 RE AD S. 1 ----_—-— —---_ --`— — — — — — -- — — —----—- — — —-( —------- ---—-.----—- -—------- — — —— -—- —- ——— — — — MEAN- TL . DE ' � C Lr . JhR. 1, FE: 0 0 !5 a AA SAA EG PEAK HEIGHT (ABSORBANCE ) 0. 4E2 0 .24'E , 215 PEAK:. AREA (ABS-SECONDS) 0. 244 0, 1:31 0, 113 PBAD -05 _--- ----2-1- -- - ---- —-- — IZ --------------- ---�03/----- -- - -- - :. i A PEAK HEIGHT (ABSORBANCE) 0 , 470 0. 253 x . 216 PEAK AREA (AFS-SECONDS) O , 245 O, 1 = . 11= REQ_ 0 - - --- ---- --- -- -- - --- - - - ------ - --- - - ------ - --- -- ----------- ------- ---- ---- - -- --- - MEAN= 23, E STD, DEV, = 0 , 2 COEF,VAR. = 1„7; 1F+:FaFaF##aFaFiF#aE###aFiEaF##ir#?EiF#aF##iF###?F##aeaF#aFiF#�F#iFiFjF###aF4aF#iFaF#iFIFiF#aFaF##aF#aF#+tt#####iF#iF## Y=D IE-' 005s) AA Z A A FG PE=;K:. HEIGHT (ABSORBANCE) 0. 512' 0.2,7 E. 0. ?: PE,rj-•,K; AREA (ABS-SECONDS) O. 2E? 0. 145 0. 124 READ- ---- ---`- - - ----- -------------- 2(F------ AA SAA F PEAK HEIGHT (ABSC)PBANCE) 0. 505 0. 2 '3 0 , CE2 PEAK AREA (ABS-SECONDS) 0, 2E5 0, 14x, 0 . 12G PEAL; 2E , 4 MEAN= - -----...6� �--- --STD, DEV. =---- - --0 . 1 -- - --CGEF, VAR. = 0 . 55 'X ISE: 0GC_ O AA SAA t.� 1.J PEAK HEIGHT (ABSORBANCE) G. 032 0. 01E 0. 01E PEAK: AREA (ARS-SECONDS) 0. 01E 0, 00; O. 009 READ: 0. 8 0000161 - - --- --------- - ---------- ---- - --- - -- - - ------- --------------- - ------- - ------- - --- o� PEAK HEIGHT (ABSORB INCE) 01033 0, 01 i 0. 0116. PEAK AREA (ABS-SECONDS) 0. 017 0. 008 01009 READ: 1 , 0 3_ Zs- __Pw_ool ______ MEAN= 0. 9 STD. DEV. = 0. 1 COEF.VAR. = 12. 11 M 1p F: o O 6 1 AA ZAA BG PEAK:. HEIGHT (ABSORBANCE) 0. SE1 01.E4S 0. 0;4 PEAK AREA (ABS-SECONDS) 0. 155 0. 118 0 , 03' READ: E1 , 2 - Q7/� - 06 -7-- ---- ----------- ------------ ---- - -- ------- --- ----- ---------1--- -- ----- - - -- AA EAA BG PEAKHEIGHT (ABSORBANCE) 0. .519 G , E45 01071 PEAK AREA (ABS-SECONDS C., 15 2.1 0. 1 17 C: . 0 F.EAD-- ---- ----- --- ---- - - - --_--- - - -- -- -- - --- - - - ------_------- --- - - --- -- - - -- - -- -- MEAN= E1 , 1 STD. DEV. = C,. 1 CC,EF.',,'AR, - 0 .51 AA "Z7aA. B, PEAK. HEIGHT (ABSORBANCE) 0. 054 G, 029 10 . 02E PEAY. AREA (ABS-SECONDS) 0. 027 0 , 015 0 . 012p READ: 2 _ - --- - - ------ --}0 —--- ------- - -------- ---131f.2s_� -- --- ------- - -- ---- - - -- , AA B PEAK; HEIGHT (ABSORBANCE) 0. 054 0 , OEC 0. 026 ` PEAK:: AREA (ABS-SECONDS) 0. 0--T,'.2 0 . 015 READ---- - --------t - -- ---- -------- -- - -- - - ------- - - - -- ----------- - ------- --- ----- - -- MEAN= r2l STD, DEV. = 010 COEF.VAR, = 0, 47 . 1 �F##?F#iFiF####�F##{#3FaF####?E##iF#:c###i'iF####?(#####aF#tjF#jF?F####il'#iF##iF#iF##c##�!#aF###af##iF#iF ► 'QOc_ :E; AA ZAA BG PEAK. HEIGHT (ABSORBANCE) 0 1 G,2:B4 0. 079 PEAK:: AREA iABS-SECONDS) 0. 17 0 . 129 G , 044 READ: 2:9, - ----------- - -- --- -------- ---- - -- - --- -—� - -- - - - --- - ---- - -- --Llq - ---- - - -- - - -- AA AA BG PEAY. HEIGHT (ABSORBANCE) 0. : 16 0 , 250 PEAK AREA (ABS-SECONDS) 011176, 0 , 12r 0 . 0`'1 READ: - ---- - --- - ------------------- ---------------- --- -------------------------- -- - - -- MEAN= 23. 0 STD. DEV, = 0, 4 COEF. VAR, = 1 . 69 0000 162 AA _AA BC PEAK; HEIGHT (ABSORBANCE) 0, 0_5 0. 010, 0 . 4-0 PEAK AREA (ABS-SECONDS) 0. 020 0. 007 0, 012 0. 9 READ------------- ---- - AA SAA BG PEAK HEIGHT (ABSORBANCE) 0. 037 0 , 01E 0, 0'?0 PEAK AREA (ABS-SECONDS) 0. 018 0. 007 0. 011 READ---------Q'a---'------ ---- --- --�-3#25-199 -------------------Pw-�-�,-��------ MEAN= 0 . 9 STD. DEV. = 0. 0 COEF.VAR. = 0.i8 E. 00C, 5 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 306 0.2:30 0 . 07.8 PEAK AREA (ABS-SECONDS) 0. 161 0. 1 0 0. 041 READ. 51 , 5 - - -- ------------- --- -------- ------ --- --D_?A - ----------- ---- ,--- -------- --- AA ::AA DC. PEAK:. HEIGHT (ABSORBANCE) 0. 3 121 01 -73=' 0 . 0_0 PEAK:. AREA (ADS-SECONDS) 0. 161 0. 119 0 . 042, FEAR: ?1 . 3 1 -^__-_-n-__--- - -- ---- --- -- -- - --- MEAPJ= �1 , 4 STD. DEV. =---- - --0-,---- - -1 �CEF,1,hF, - 0.�-,� ';< F�IFE: 00C- C- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 68 0.5:30 0. 15 PEAR:: AREA (ADS-SECONDS) 0,32' Q. ?58 0 . 0-0 READ,. 49. :_ - --- -- --- ---- - - -- ---- ------g - - -- - -- �� -- - - ---------------� /-- - - - - - --- -- - AA EAA EG PEAK:: HEIGHT (ABSORBANCE) 0.674 0,521 0. 155 PEAK: AREA (ADS-SECONDS) 0 . 3129 0.225S 0 . 070 READ-- -------- -- - -- -- ----- ------- --- ----- ---- -- - ---- ---- --- ------ --- -------- - - -- MEAN= 49. ' ETD. DEV. = 0 , 0 CO3EF. VAF, = 0. 09 '/ F":' 0 0E- AA EAA BG PEAK; HEIGHT (ABSORBANCE) 0 . 004 0. 005 G. 00 PEAK AREA (ABS-SECONDS) -0 . 00i 0. 001 -:' , 'a'0= READ-- -------0 . - --- - ---- ---- - --- ---- -- - ----------- ------ --- - -- - -- -- --- - -- AA 6 EAA BG PEAK:: HEIGHT (ABSORBANCE) 0, 004 0. 005 0, 005' PEAK AREA (ABS-SECONDS) 0 . 000 0, 00:= -0. 00=, READ: 0 . 1 ---- ----- ---- - --- --- -- ---- -- - ---- -------- -- -- -- ----------- --- - --- - - - - -- - -- --- --- MEAN= 0. 0 STD, DEV. = 0 , 2p COEF. VAR. = 99. 99 r 000016 rFl,E. 00C, a PEAK HEIGHT (ABSORBANCE) 0. 0124 0. 010, 0. 01E PEAK AREA (ABS-SECONDS) 0. 016 0. 00; 0. 010 READ----- ----G'o- --- ----- ------------- --- ----i--------------------------- AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 026 0. 012 0. 014 PEAS: AREA (ABS-SECONDS) 0. 015 0. 00; 0. 608 READ: O . E_ --------- ---- --- ------------------ -- - ------- ----- ------- -------------------- - -- - 1 MEAN= 0. 8 STD. DE`r'. = 0. 0 COEF. VAR. = 5. 59 '. tjF##?l'#�FjF##��F#iF##�##'1F###1F##}9F##1eirir##�t#�EjE## 1FiF#*###?E#*#jF###�(•?F4�EiE#iF########?F#####� F,1E: .30G %3 AA AA FG PEAK HEIGHT (ABSORBANCE) 0 , 261 0, 199 0. 06 PEAK AREA (APS-SECONDS) 0. 160 0 . 12 1 0 . 01.9'3 READ-- -- - - - -- 1------ -- --- - - - -- ------ ---- I - -- - ------------ /- 1Q - --- -- -- - - - - -io 8 BC PEAK HEIGHT 'ABSORBANCE) 0. 2E•4 0 , 2131 0. 06 PEAS: AREA (APS-SECONDS) 0. 158 0. 1 I= 0 . C="? DEAD; 21 . E MEAN=---- -- - - ---STD. UE`v'. =- ------0. 4-- ---COEF. VAR. = I . B;- -�-- ---- -- ----- -- - - �FiE?E###-It#+F#iraF#t###t:r##��#t##�#�#}�##?FiF1F?c###iF��a##-it#f}#ie###x#jF�Fir?�###x�#4iF##�##x#4 SIE: 001- 0 AA AG 0 D PEAK HEIGHT (ABSORBANCE) . 00:9 0. 00-, 0. 00S PEA;' AREA (ADS-SECONDS) -0. 001 0 . 00 ' -0 . 004 FEAT,----- ---- --- ----- �3Z41-11- �5- -- --- ---- ---- --- - --- - --- -- -- - --- ZAA BG PEAK HEIGHT (ABSORBANCE) 0 . 005 0. 00PEAK AREA '(ABS-SECONDS) 0. 00 ' -0 . 002'READ---- - --- -'J • `-)- - - -- - -- - -- ------ ------- ------- - -- - - - -- --- - MEAN= 0. 0 STD, OEF. VAR. = 99.9.1 7 1,E. 0 0 1 AA 7AA BG PEAK HEIGHT (ABSORBANCE) x", 0, 242 0. 060 PEAk: AREA (ABS-SECOPJUS) 0. 11: 0, 0?4 READ: 20 . 1 - ---- - --- ---- - -- - ---- - ----- -- ---- - -- ---- --- -------- -I-o�/-- -- - - - - - - - - - ZAA E,0. PEAk: HEIGHT (ABSORBANCE) 0 . 30c, 0 .246 0 . 060 PEAS' AREA (ABS-SECONDS) 0. 1 =;; 0. 114 0 . 0 READ: 50 , 4 MEAN= 20 , =s STD. D V. = 0 . 2 COEF,VAR. = 1 . 09 0000164 r FM E: 0 O AA ZAA BG PEAK HEIGHT (AFSORDANCE) 0, 0178 0. 061 0 , 017 PEAS: AREA (ABS-SECONDS) 0. 040 0. 03 0. 007 READ-. 5. ------ --- --- - -------- ----- -- - - ------ ---------- ------- -------- - -- AA 3Lq -Q '--------- ------- -------- - --AA ZAA E:G PEAK.: HEIGHT (ABSORDANCE) 0. i9 0. 064 0 , 016 PEAK: AREA (ADS-SECONDS) 10313 0. 031-71 0. 007 READ, 5. 3 - - -- - - --- ---- - ----- --- --- - - - - -- - - ----- - ----- -------------- -- ---- --- - ---- -- - - -- MEAlJ= 5, STD. D"ll. = 0. 0 COEF.VAR. = 0 . 27 AA SAA BG PEAK HEIGHT (ADSORBANCE) 0, 556 O, DSC r' . G74 PEAK APE" (APS-SECONDS) 0 . 178 0. 143 0 , 035 READ- 26. 0 ---- �------------- --��'��---- --- - --- AA DAh DJ PEAK HEIGHT (ADSORDANCE) . : 56 0 . '2 S 0, 0, PEAK; AREA (ABS-SECONDS') 0 . 180 0. 144 G . 0:36 READ r 21E , 1 MEAN= ?6. 1 STD, DE`', = 0. 1 COEF.VAR. = 0, S,6 % 0 O AA ZAA DG PEAK. HEIGHT (ABSORBANCE) 0, 640 0.504 G . 13rl PEAK: AREA (ADS-SECONDS) 0 . :;3c, 0.2170 . OE 6 READ__--- --._51 . 0- - ---- - - - ----- - _ __ - - ------ ------- -- - - -- - ---- - -- - --- At, --- - -- - --- At, ZAA B� PEAY: HEIGHT (ABSORB""NCE) 0, 64? 0 . 506 0 . 1.3E PEAT; AREA (AES-SECONDS) G, 'D.6.D G.26,7 G . 067 READ: 51 . 1 MEAN= 51 , 4 STD, DEV. = 0 . 6 COEF,VAR. - 1 . 1 . I ?F?EiEt1E1F�F�f'1F1E+#?�iF�E�E�F !Ex�x�iF�EaFit�iFiFiFt�F?FiF� tiFiEiEiE�E?F�E�#��F�t�F#i.�FifIE#.#1F�f4�E?fiF�F4�F#��F�F�F4�F�F4?FiF?F?F' AA SAA iJ PEAK: HEIGHT (ABSORBANCE), 0. 004 G, 00r, 0 , 00 PEAT: AREA (ABS-SECONDS) 0 . 000 0. 00? 0 . 00E READ: 0. 0 - --------------- - -- -- --- - - --- - -- -- --- -- ---- -- ----- -------- ------- - -- - -- -- - - -- - -- AA7 1 ZAA EG PEA} HEIGHT (ABSORBANCE) 0. 004 0. 004 0. 001 PEAK AREA (ABS-SECOND) 01000 0. 0012 -0 . 002, REND----- ----0 . 1 0000165 ---- - --- - - --- ---- - --- -------- ----- ----------- -------- - - ----- - --- I cZTn. r,7%). = n . i rn��. vap. = A7 Y, NYTEST ENVIRONMENTAL INC. F jRNACE ANALYSIS RUN LOG ANALYST: CALIBRAi:ON DAT-: 2 L0GLN #r's: START TINM=: f� � s END TIyL: 0:,2S 10H S IN►EGKk.,0N-TI:.tE: 5 0 secs S T.-.Ni?.:RD SOURCE: Sp�X STANDARD LOT 5--N-DAIZD PRE?.kR.- ' N D.-.T_. g I/ 192 ST.kyD D F.XP A71CN D.-.T 8 30 u STA ND"F-D, PREEPAR, TION LOGEGOK PAG= -. Q�rQCR vliti " r - N ,�i= ACCE-KA"NT s 'CE LI�tI:S I CO�Itit\' ' QC SAIIP�E . - I w.ICV ICs I < H-) CRQL CCV - 90-i 10 I I CCB I CRQL i LCS I SO-120 or E?A LIMITS I I PREPARATION BLANK ( < (_/-) CRQL I I DUPLICATE I - SPt{F REVIEWED BY: . /�• C Ci ; 00166 C AA LAA ESC PEAK HEIGHT (ABSORBANCE) 0. 01E 0 . 010 0. 015 PEAS; AREA (ABS-SECONDS) 0 . 015 0. 003 0. 011 READ: -_0. 009--- --------- -------- ---- ----------- ------------------------------- AA EAA EC PEAK HEIGHT (ABSORBANCE) 0, 014 0. 010 0. 01E PEAK AREA (ABS-SECONDS) 0 . 014 0 . 000 0. 013 READ: -0. 012 --------------- --- - -------- - -- - ---- ------------------------ ---- -------- - --- ----- MEAN= -01011 STD.DE`!. = 0. 00 COEF. `JAR. = 20 . ''9 `.. 0. 000 AUTO EFO 1 !E3� AA LAA rG PEAK HEIGHT (ABSORBANCE ) 0.554 0. 43:_ 0. 119 PEAK AREA (ABS-SECONDS) 0. 39101 0.308 0. 090 READ: 0. 306 ----------- -------- ----------- ----- ------/QQ--- ---------------------------- ----- AA LAS; BC PEAK HEIGHT (ABSORBANCE) 0. 59;' 0. 479 0, 1:9? PEAK AREA (ABS-SECONDS) 0.40.9 0 . 31=9 0 . 089 READ_ 0. 511 ------ -------- ------------ ----------------------------------- - ---- ----- MEAN= 0.309 STD.DEV. = 0. 004 COEF. VAR. = 1 . 20 % 100. 0 STANDARD 1 S� AA EAA BC PEAK HEIGHT (ABSORBANCE) 0.:92? 0 . 26:= 0. 068 PEAK AREA (ABS-SECONDS) 0. 222 0. 172 0. 050 READ: 55, 1 ------------ - ---------------- q AA EAA PC ' PEAK HEIGHT (ABSORBANCE) 0. 330 0.262 0. OT'? PEAK AREA (ABS-SECONDS) 0.223 0 . 1:1 0. 052 -BAD--------54- ---- ------------------------ -------------------------------- ----- MEAN= 55. 0 STD.DEV. = 0. 2 COEF.VAR. = 0. 42 x 50. 0 STANDARD 2 SE: AA LAA BC PEAK HEIGHT (ABSORBANCE) 0. 172 01138 0, 040 PEAK AREA (ABS-SECONDS) 0, 115 0. 082 0. 033 READ - 5 0 d ---------- ----------- --------------- ----------------- - 6 7 -- ---- --- - - 1 (CONTINUED) AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0. 174 0. 139 0. 040 PEAK AREA (ABS-SECONDS) 0. 123 0. 092 0. 030 READ: 25. 4 -------------------------------------------------------------------------------- MEAN= 23. 9 STD.DEV. = 2. 2 COEF.VAR. = 9. 14 x, 24.3 STANDARD 3 S F= AA Z AA PG PEAK HEIGHT (ABSORBANCE ) 0. 082 01063 0. 022 PEAK AREA (ABS-SECONDS) 0, 063 0. 041 0. 023 READ: 10 , 7 ---------------------------------- --------10------------------------------ ----- AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 081 0. 059 0. 024 PEAK AREA (APS-SECONDS) 0. 052 0. 035 0, 017 READ: 9.2 ----------------------- -------------------------------------------------------- - MEAN= 10, 0 STD,DEV, = 1 , 1 COEF,VAR, = 11 ,42 x 10 . 0 STANDARD 4 S� AA ZAA PC PEAT: HEIGHT (ABSORBANCE) 0. 041 0. 033 0. 018 PEAK AREA (ABS-SECONDS) 0, 032 0. 021 0. 011 READ: 5. 2 S ------------------- -------- ------------------------------------------------ ----- AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 04; 0. 0.35 0. 014 PEAK AREA (ABS-SECONDS) 0. 033 0. 020 0. 01 READ 5. 0 MEAN= 5. 1 STD.DEV. = 0, 1 COEF. VAP,. = 2. 57 % �E dF 3F iF iE�F 1E iE-1@�E iF�F iF�F iE 9E iE�F*iE iF 9E*jf iE*jt iE jE jF it iE�F iF iF��F dF jE dF 3F'k iE�E�F 9E iE�F jF iF iF iE?E*iE jF�'r jF�9E 3F iE�F�E 9E dE�E iF 4�F iF�E jF�F iE 9F�iF iE 5.3 STANDARD 5 0 • Q9�f oo � o � ss. S� AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.529 0. 420 0. 112 PEAK AREA (ARS-SECONDS) 0. 360 0.280 0. 080 READ: -- �,�l p ------------ ----- -------------------------- --------------f� --------------- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0, 521 0. 409 0. 112 PEAK AREA (ARS-SECONDS) 0.37J54 0. 274 0. 080 ' READ: 85. 1 ------------------- -------- ----------------------------------------------------- MEAN= 86, 2 STD,DEV, = 2, 1 COEF.VAP. = 2, 41 % AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 015 0 , 011 0. 010 PEAS: AREA (ABS-SECONDS) 0. 010 0. 0022 0. 009 READ 0. 0 AA ZZAA BC PEAK HEIGHT (ABSORBANCE) 01013 0. 013 0. 009 PEAK AREA (AES-SECONDS) 0. 011 0 . 006 0. 005 READ: 1 . 1 ------------------- -------- -------- --------------------------------------------- MEAN= 0, 6 STD,DEV. = 0. 8 COEF.VAP,, = 99 . 99 % E3 E_ AA ZAA BG ' PEAK HEIGHT (ABSORBANCE) 0. 043 0. 033 0101c, PEAK. AREA (ALAS-SECONDS) 0. 033 0, 0?0 0. 013 READ- ---- --- --5. 1------ - ---------------- -`_eA------------------------------- ----- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 042 0. 03--9 0. 015 PEAK AREA (AFS-SECONDS) 0. 033 0, 020 01014 READ; 5. 1 MEAN= 5, 1 STD.DEV. = 0. 0 COEF.VAP. = 0. 95 % E3T= AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.293 0, 233 0. 064 PEAK AREA (ABS-SECONDS) 0, 214 0. 165 0. 050 READ--------48- ---- -------- -------- ew------------------ ---------- ------ AA -------- ------AA ZAA BG 1 PEAK HEIGHT (ABSORBANCE) 0. 293 0,235 0. 065 PEAK AREA (ADS-SECONDS) 0.209 0. 159 0. 051 READ: 4c . 1 0 0 0 0 16-.9 ------� � ---- - ------- ----- -^------------------ ----- 2, 99 MEAN= TO STD.DEV. = 1 . 4COEF.VAP. = S)E AA ZAA PG PEAK. HEIGHT (ABSORBANCE) 01018 0. 014 01011 PEAK AREA (ABS-SECONDS) 0, 015 0. 005 0, 010 READ: 0 , 9 --------------------------- ---------------ca----------------------------------- ' AA SAA FC PEAK HEIGHT (ABSORBANCE) 0. 014 0. 01E 0. 012 PEAK AREA (ABS-SECONIDS) 0. 010 0, 003, 0 . 007 READ: 0. 4 ----------------------- --------------------------------------------------------- MEAN= 0, ; STD.DEV: = 0, 4 COEF.VAR. = 53, 82 SE: O O 1 AA ZAA PC PEA}: HEIGHT (ABSORBANCE) 0. 014 0. 011 0101 PEAK AREA (ADS-SECONDS) 0. 01= 0. 006 0. 00; READ: 1 . 1 ------------------------------ 13c�_t ---�6w---- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 020 0. 013 0. 012 PEAK AREA (ABS-SECONDS) 0. 012-1 0, 00:9 0. 010 READ: 0.2 - ------- ----- ------- `.t. ------ MEAN= 0. 7 STD.DEV. = 0. 6 COEF.VAR. = 92. 50. E3 E: O O 1 =D AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 0;'2 0. 059 0 , 021 PEAK AREA (ABS-SECONDS) 0. 051 0. 034 0 . 017 READ 9 , 2 ------- -------------------- --f�iQ W A-----------��{--------------- AA ZAA DG ' PEAK HEIGHT (ABSORBANCE) 0, 068 0, 054 0. 019 PEAK AREA (ABS-SECONDS) 0. 049 0. 0:9:8 0 . 016 ---- � 8.9 -------- ----------- - ------------------ ------- ------------- ---- -- ------- MEAN= 9 . 0 STD.DEV. = 0. 2 COEF.VAR. = 2. 48 % S E: O O J. ;# AA ZAA FG PEAK HEIGHT (ABSORBANCE) 0.260 0. 206 0 . 059 PEAK AREA (ABS-SECONDS) 0, 185 0. 141 0 . 043 READ: 40 . 7 AA ZAA- PC PEAK; HEIGHT (ABSORBANCE) 0. 26:9 0. 1106 01061 PEAK AREA (AFS-SECONDS) 0. 196 0 , 142. 0 . 048 READ, --- -------------------- ---- -------- --------------------------------------------- MEAN= 41 . 17 STD.DEV. = 1 . 4 COEF.VAR. = 8. 46 % 0000170 S E: 001 -15 AA ZAA PC PEAK, HEIGHT (ABSORBANCE) 0..=x03 0,247 0 , 06: PEAK AREA (ABS-SECONDS) 0. 221 0. 1:2 0, 049 READ_------ -50.3------- -----��------13��-�-/��-=-�b�19------g-� ' ------ AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 309 0.242 0. 060 PEAK AREA (AFS-SECONDS) 0. 223 0 . 170 0, 05:3 READ: 49.8 ------------------------------------------------------------------------------- - IMEAN= 50, 0 STD.DEV. = 0. 4 COEF:VAR.= 0. 89 % S3 I: 00 1 c_ AA ZAA B13 PEA}; HEIGHT (ABSORBANCE) 0. 0.31 0 , 021 01018 PEAK AREA (ABS-SECONDS) 0, 029 0. 013 0. 01E -- -------------------- ----- -------- - -----------.- ?------ ----- --------JA#L2- -b1--------------M ---------- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 033 0. 01;, 0. 018 PEAK AREA (RFS-SECONDS) 0. 024 0 , 006 0 . 018 READ-. 1 . 1 ------- ----- ------ - .-- -�----------------- MEAN= 2, 1 STD.DEV: = 1 . 5 COEF.VAR. = 69, 62 !E3 E: 0 0 1 Aa ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 07° 0, 059 0. 026 PEAK AREA (ABS-SECONDS) 0. 060 010:36 0. 0.24 READ: --------- 9 . 8-------------- -----------VIA----------------�� --------------- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 078 0. 056 0. 026 PEAK AREA (ADS-SECONDS) 0. 064 0 , 0:37 0. 027 READ-. 10. 0 ------- ---- -------- ------------------------ --------- ------------ ----- MEAN= 9. 9 STD.DEV. = 0. 2 COEF.VAR. = 1 , 58 ` S 1= 0 0 1 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 023 01010 0. 020 PEAS: AREA (ABS-SECONDS) 0. 020 0.006 0 . 014 READ1 . 1 --------- --- ---------------� �0�=--0'2 - ----------------` 1�C --- ----- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0, 02^ 0. 0) 2 0 . 0"'0 PEAK AREA (AFS-SECONDS) 0. 021 0, 005 G, OlE READ: 0.9 -------- --------------------------------------- ----------- ---------------------- MEAN= 1 . 0 STD.DEV. = 0, 1 COEF.VAR. = 14. .38 S E 0 0 1 S3 AA ZAA BG. ' PEAK HEIGHT (ABSORBANCE) 0. 086 0, 062 0, 025, PEAK AREA (ARS-SECONDS) 0. 059 0. 038 0. 0,121 READ: 10 . 4 ---- --- ---------------------------------AA_------------ZAA------------EG---- ----- PEAK HEIGHT (ABSORBANCE) 0. 084 0. 064 0. 01217 PEAK AREA (AES-SECONDS) 0. 0E0 0. 086 0, 024 -BAD---------9.9------------------------ -- -�°2_-� --------------/ ---------- MEAN= 10. 1 STD,DEV. = 0. 4 COEF.VAR. = 3. 58 % SE: 0020 AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 024 0, 014 0 . 02' PEAK AREA (ABS-SECONDS) 0, 021 0. 001 READ: -0 . 2 03 _ - - -------- ---- --- ------A-A _ ------------- -' W1DG - - ----- AA Zaa DG_ .c_- PEAK; HEIGHT (ABSORBANCE) 0, 024 0. 0i2 0. 020 ' PEAK AREA (ABB:-SECONDS) 0. 020 0. 00:3 0, 617 READ: 0.3 ------------------- ---- ------- ------------------------------------------------- - MEAN= 0, 1 STD.DEV. = 0. 4 COEF.VAR. = 99, 99 SE: 0021 AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0. 075 0 . 057 0. 028 PEAK AREA (AES-SECONDS) 0. 055 0. 033 0. 0213 READ: ---------8. 8-- -- ----------- ----------=------ ------------�6- --------- ----- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0 , 075 0. 051 0 . 030 PEAK AREA (ABS-SECONDS) 0. 056 0. 0:31 0 , 025 READ: 8. 4 --=------------------ --E_V --- ---COEF. AF,. = S, .i7 '�. S� 0 022 AA LAA BG PEAK HEIGHT (AESOPBANCE) 0.308 0 , :45 0, 065 PEAK AREA (ABS-SECONDS) 0 . 20: 0. 157 0 . 051 READ: 45. 7 -- ----------------- --- ----- -----LG - ---------- ----9Y_ ----------------- AA °Z ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 296 0.231 0. 068 PEA}: AREA (ABS-SECONDS) 0. 203 0. 155 0. 048 READ: --- _--_45. 0_ ----- -- --- ----- --- - ------------------------ ----------- --------- ----- MEAN= 45. 4 STD. DEV. = 0. 5 COEF.VAR. = 1 . 19 % 0000172 S E: 0 0 2:D AA ZAA Ec 1 PEAK HEIGHT (ABSORBANCE) 0. 014 0. 011 0. 010 PEAT: AREA (ALS-SECONDS) 0. 015 0. 005 0. 010 0.8 READ----------------------------------------------------------------------- ----- AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 016 0. 017 0. 012 PEAK AREA (ABS-SECONDS) 0. 012 0. 003 0. 009 READ------- 0.3 ------------ --------------------- 3--------------------------- ----- MEAN= 0. 6 STD. DEV. = 0. 4 COEF,VAR, = 60, 07 % SE: O 02-4 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 029 0. 013 PEAK AREA (ABS-SECONDS) 01030 0. 006 0. 024 REA �Z w DCvJ .-----------------------1-1--- ---- ----- -- ----------13 ---------- ------- -- AA --- -- ---- -- AA ZAA P.C, PEAK HEIGHT (ABSORBANCE) 0, 028 0. 011 O. G24 PEAS. AREA (ABS-SECONDS) 0. 0:31 0 . 002, 0 , 02; READ: 0. 4 MEAN= 0. 7 STD.DEV. = 0. 5 COEF.VAR. = 66.60 S� O025 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 092 0. 070 0, 0.3:= PEAK AREA (ABS-SECONDS) 0107:3 0. 038 0. 035 READ: 10. 4 ------------------------------ -----------'� ----------------M -- --- ----- AA ZAA BG ' PEAK HEIGHT (ABSORBANCE) 0. 088 0. 058 0 . 0:34 PEAK AREA (ABS-SECONDS) 0. 074 0. 0:38 0, 03x, READ-. 10.3 --- --- - MEAN= 10. 4 STD. DEV. = 0. 1 COEF.VAR, = 0 , 72 `X ' S31-= 0 02 AA SAA BG PEAK HEIGHT (ABSORBANCE ) 0. 076 0. 01° 0. 072 ' PEAK AREA (ABS-SECONDS) 0, 075 0. 002 0. 073 READ---------0, 1--- --- ------------------L 3 o2S==-01---------Mw Iscl-vq ----- ' AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 079 0. 013 0 . 076 PEAK AREA (ABS-SECONDS) 0. 0;3 01002 0. 071 READ: 0.2 --------------------------------------------------------------------- ----- - ----- MEAN= 0, 2 STD, DEV. = 0. 0 COEF.VAP,. = 24.86 % 0 0 0 017 3 SE: O d2; AA ZAA P.G. PEAL`. HEIGHT (ABSORBANCE) 0. 10; 0. 044 0. 072 PEAK AREA (ABS-SECONDS) 0. 098 0. 023 0. 075 READ6- 1 --------- -------------- --------------------------------------------- ----- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 107 0. 036 0. 078 PEAK AREA (AFS-SECONDS) 0. 098 0. 0220 0. 078 READ: 5*2 MEAN= 5. 6 STD.DEV. = 0. 6 COEF.VAR. = 11 . 15 % Sam OO77"o AA ZAA EC PEAS. HEIGHT (ABSORBANCE) 0. 0774 0 . 009 0 , 0;-8 PEAK AREA (ABS-SECONDS) 0, 055 -0. 003 0. 058 ---- r - 1 . 3 M W 3SC,V�1 AA ZAA FG PEAK HEIGHT (ADSORBANCE) 0. 078 0, 014 0. 0;1 PEAK AREA (ABS-SECONDS) 0. 053 0. 001 0, 0522 READ: -0. 1 MEAN=------ -0. ;---- -STD.DEV. =-------0.8 COEF.VAP,. = 99 . 99 %----------------- �**�***�*��iE�**��iF�*�*��***��t�*�*iF��**��*��**��*iF�**�*�t*iF�**�***�t�ar.it� SIE: OQ2S3 AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0. 101 0. 06E, 0. 056 PEAK AREA (ALS-SECONDS) 0, 073 0. 034 0. 01B9 READ--------------- -------- ------------- �-A--------------- -�-�/ ------------ AA ZAA BG PEAK HEIGHT (AFSORFANCE) 00113 0. 067 0. 066 PEAK AREA (AFS-SECONDS) 0. 08; 0. 0:s4 0. 0522 P.EA----------- ----- -------- -=-- -------------------------------------------- - - --- MEAN= 913 STD. DEV. = 0. 1 COEF.VAR. = 1 . 14 % AA ZAA FC PEAK HEIGHT (ABSORBANCE) 0. 056 0. 013 0 . 048 PEAK AREA (ADS-SECONDS) 0. 050 0. 005 0. 044 READ: 1 . 0----------- ----------�3LZ5-=-Q�-------- -- ti�I:_cSG --------- ' AA ZAA FG PEAK HEIGHT (ABSORFANCE) 0, 05° 0. 013 0. 050 PEAK AREA (AFS-SECONDS) 0. 050 0. 001 0. 044 ' READ. -0. 22 ------------------- ---------------------------- --------------------------- ------ MEAN= 0, 4 STD.DEV. = 0. 8 COEF,VAR. = 99 . 99 % 0000174 S E O 0 :D 1 AA ZAA BG, PEAS. HEIGHT (ABSORBANCE) 0. 099 0. 044 0 . 058 PEAK AREA (ADS-SECONDS) 0. 090 0. 030 0. 060 REA ------------- 8. 1----------- -------- ---------------------------------------- ----- AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0. 097 0. 045 0. 05E PEAS:. AREA (ABS-SECONDS) 0. 086 0 . 0:32 0. 055 READ: ---------8.6------------------------J-3#.2Y - -��- ---------- ------- 3�---- MEAN= 8. 3 STD.DEV. = 0.3 COEF.VAR. = 4. O8 % 3 !E3 0 0 at^ AA LAA BG PEAK HEIGHT (ABSORBANCE) 0. 085 0. 014 0 . 09, PEAK AREA (ADS-SECONDS) 0. 069 0. 001 0. 069 READ: ------------------- ----- ---------------1-15-=1� -- ---------------- - -- - ----- AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 090 0. 012 0. 085 ' PEAK AREA (ABS-SECONDS) 0. 074 0. 000 0. 0; READ: -0.4 M�J oc--IyV -=------------------------- ------- -- --------------------------------------- ----- MEAN= -0. 4 STD.DEV. = 0. 1 COEF.`JAR. = 18. 5:3 % SE: 0 p '�.� AA LAA BG PEAK HEIGHT (ADSORBANCE) 0. 103 0. 044 0. 094 PEAK AREA (ABS-SECONDS) 0. 116 0. 032 O . OS4 READ - 5-5------------------ ---------Q� ---- -------- A---------------- - - --- ----- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 01106 0. 04:3 0 . 080 PEAK AREA (ADS-SECONDS) 0. 110 0. 031 0 , 079 --------------• i -------- ---- -_------ ------------------_------------------ ------- - MEAN= 5. 4 STD.DEV. = 0. 2 COEF,VAR. = 1 , 93 % , E3 E: 00Z-3-4 AA LAA DG PEAK HEIGHT (ABSORBANCE) 0.299 0. 234 0. 068, PEAK AREA (ABS-SECONDS) 0.215 0. 165 0. 050 READ: 45. 0 --------------- -------- ---- - ---a��---- -------------------q7-,`----- -------- AA ZAA DC PEAK HEIGHT (ABSORBANCE) 0. 309 0.24E 0. 065 PEAK AREA (ADS-SECONDS) 0.220 0 . 170 0, 051 ' READ49, 5 -------- --- ------------------------ ----------------------- ---- MEAN= 43, 7 STD.DEV, = 1 . 1 COEF.VAR. = 2. 31 U G 0 0175 SE: 0 0Z___c5 AA LAA BG. PEA}: HEIGHT (ABSORBANCE) 0. 022 0. 017 0. 017 PEAK AREA (ADS-SECONDS) 0, 027 0. 006 0, 0 142 1 READ: 1 . 2 AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 013 0. 014 0. 014 PEAK AREA (ABS-SECONDS) 0. 015 0. 004 0. 011 -------------0.6--------------------------G ------------------------------- - MEAN= 0. 9 STD.DEV. = 0.5 CO6F.VAR. = :E3 1E 0 0 .BC, AA ZAA FG PEAK HEIGHT (ABSORBANCE) 0. 035 0. 015 0. 083 PEAK AREA (ABS-SECONDS) 01063 0. 003 0. 065 ' READ: 0, 3 ----- --------- AA ZAA, BG PEAK HEIGHT (ABSORDANCE) 0. 039 0. 014 0. 079 PEAK AREA (ADS-SECONDS) 0. 074 0. 004 0 , 070 READ: 0.6 ------ - ----- ------- ----------------- MEAN= 0. 5 STD.DEV. = 4.2 COEF.VAR, = 49. 71 % S)E 0 0 := AA 1L.AA BG PEAK HEIGHT (ABSORBANCE) 0. 108 0 . 0477 0 . 0?8 PEAK AREA (ABS-SECONDS) 0. 104 0. 030 0. 074 ' READ: ---------8, 1------ -------- ---------- OS A---------------g-- ------------- AA ZAA BG ' PEAK HEIGHT (ABSORBANCE) 0. 109 0. 050 0. 075 PEAK AREA (ABS-SECONDS) 0. 105 0. 0:31 0, 01- 4 READ- 8. 4 ---------- ------------ - --------------------------------------------- --- -- MEAN= 8. 2 STD.DEV. = 0, 2 COEF,VAR. = 2. 58 x E3 E: 00EE� AA SAA BG PEAK HEIGHT (ABSORBANCE) 0. 0, 046 01080 ' PEAK AREA (ABS-SECONDS) , 106 0. 026 0. 0:9 READ: 7. 0 ------------------- -------- -----7-----1-3# s= ---------(0 - sPkMwfcD��N_ _ !E3)E 0 0a AA �.AA BG PEAK HEIGHT (ABSORBANCE) 0. 109 0. 044 01081 PEAK AREA (AES-SECONDS) 0. 105 0. 029 0. 0176 READ: 7, 7 AA ZAA Dc PEAK HEIGHT (ABSORBANCE) 0. 104 0. 045 0. 032 PEAK AREA (ADS-SECONDS) 0. 108 01030 0. 073 ' READ: 3. 1 000017 ` ---------------------- ---------------------------------------------------- ------ MEAN= 7. 9 STD.DEV. = 0. 2 COEF.VAR.= 3. 13 % SE: 0 0 !D AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 020 0. 012 0. 016 PEAK AREA (ABS-SECONDS) 0. 018 0. 006 0. 013 ' READ: 1 . 1 07 -------------N;' -c CI ------ ' 0 0 :Hc iD (CONTINUED) AA ZAA BG PEAK HEIGHT (ADSORBANCE) 0. 018 0. 013 0, 017 PEAK AREA (ABS-SECONDS) 0, 018 0. 000 0. 018 ' 0 . 4 ----------- -- -- ------------ ------------- -------------------------------- ----- MEAN= 0. 4 STD.DEV. = 110 COEF.VAR. = 99 . 99 % SE_ 00-40 AA SAA BG PEAK HEIGHT (ABSORBANCE) 0. 069 0. 051 01021 PEAK AREA (ALAS-SECONDS) 0, 051 0. 033 0. 018 READ------ --------------------------------Q 7-A------ --------- y4r, ------------- ' AA 27AA DG PEAK HEIGHT (ABSORBANCE) 0. 077 0. 0516 0. 026 PEAK AREA (ABS-SECONDS) 0. 05' 0 . 0:34 0, 02:3 READ: (2. 1 ----------- ----------L----------------------------------------------------------- MEAN= 910 STD.DEV. = 0. 1 COEF.VAR. = 1 . 33 `b Sa 00.41 AA ZAA DG ' PEAK HEIGHT (ABSORBANCE) 0. 042 0 . 010 0 . 0:3+6 PEAK AREA (ABS-SECONDS) 0. 032 0. 004 0. 028 READ----------- ---- ---- ----------------� 3�.ZS--- ---------------- --of G CMZ - ------- AA ZAA BG PEAK HEIGHT (ABSORDANCE) 0. 046 0. 013 0. 0:37 ' PEAK AREA (ADS-SECONDS) 0. 0:34 0 . 006 0. 029 READ; 1 . 1 ------------------- ------------------- ------------------------------------------ 1 MEAN= 0. 9 STD.DEV. = 0. 3 COEF.VAR. = 3:3. 46 % E3 E: 0 0 -4 ` AA 2AA DG PEAK HEIGHT (ABSORBANCE) 0. 089 0 , 046 0. 048 PEAK AREA (ABS-SECONDS) 0. 065 0. 028 0, 037 READ: ---------7. 4--- -------- ------------ d -------------------'6-7-- 0 �1 - 7 ----- AA ZAA DC ' PEAK HEIGHT (ABSORBANCE) 0. 084 0, 048 0. 042 PEAK: AREA (ADS-SECONDS) 0. 064 0. 029 0 , 034 READ------- ---•9----------- -------------------- -------------------- ------------- MEAN= 7. 6 STD.DEV. = 0. 3 COEF.VAP.. = 4. 22 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 029 0. 014 0, 028 ' PEAK AREA (ABS-SECONDS) 0. 023 0. 000 0. 023 READ: ---------0 , 4-----------------------�� ° - /--------------------- O 3 ------ ' O 0 -4-D (CONTINUED) AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 030 0 , 014 0. 027 PEAK AREA (ABS-SECONDS) 0. 023 0. 003 0. 020 -------------- � ---- -------- ------------------------------------------------ ----- MEAN= -0. 1 STD.DEV. = 0. 5 COEF.VAR. = 99 ,99 `X ' !E3 E: 00 _4.4 AA SAA BG PEAK HEIGHT (ABSORBANCE) 0. 080 0, 050 0, 033 PEAS: AREA (ADS-SECONDS) 0, 055 0. 02; 0. 028 READ: 7. 3 --------------- ---- ---- ------- ------------ AA -------------- ---- ---- ------- ---------=-AA 7AA BG PEAK HEIGHT (ABSORBANCE) 0. 080 0. 05E 0. 0: 4 PEAK AREA (AES-SECONDS) 0. 055 0. 031 0. 024 ' READ: 8. 2 --------------- -------- ----------- -------- -------------------- ------------ ----- MEAN= 7, 8 STD,DEV. = 0. 6 COEF.VAR. = 8, 33 SI-= O 0-45 AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0.316 0 , 250 0. 066 PEAK AREA (ABS-SECONDS) 0.22.3 0. 1172 0 . 051 READ: -50 , 2 -- -JSp� flov _�Q� - ------------------------- - ---- AA `f' 2AA --------- --- -- ' ---- ----- PEAK HEIGHT (ABSOPEANCE) 0. 340 0.269 0 . 074 ' PEAK AREA (ABS-SECONDS) 0.228 0. 172 0. 05E READ: 50. 4 ------------------- -------- --- --------------------------------------------- ----- ' MEAN= 50. 3 STD. DEV. = 0. 1 COEF.VAR. = 0 . 23 x !E3 TE O 0 -4C, AA 2AA Ell PEAK HEIGHT (ABSORBANCE) 0. 017 0, 011 0, 012 PEAK AREA (APS-SECONDS) 0. 013 0. 004 0 . 009 ' READ: ------------------------------- ----�----------------------0000178 - ------ AA� ZAA BG". PEAK HEIGHT (ABSORBANCE) 0. 019 0. 012 0. 01; PEAK AREA (ABS-SECONDS) 0, 024 0. 005 0, 01s READ 1 . 0 ---------- ----------- -------- ---------------------------------------- ----- MEAN= 0. 8 STD.DEV. = 0. 8 COEF.VAR. = 41 .97 % ' SE: O 047 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 022 0. 011 0. 018 ' PEAK AREA (ABS-SECONDS) 0. 018 -0. 001 0. 019 ` , READ------ --------- ---- ------------ ----------��------------------- ��O1Z`------ ' 00 -47-• (CONTINUED) AA ZAA BG PEAK. HEIGHT (ABSORBANCE) 0. 024 0. 011 0 . 019 PEAK AREA (ABS-SECONDS) 0 . 018 0. 001 0. 01; ' 0 . 1 ------------- ------------------------------------------------------- ---- ----- MEAN= -0. 4 STD.DEV. = 0. 4 COEF.VAR.. = 99, 99 x AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 065 0. 045 0. 027 ' PEAK AREA (ABS-SECONDS) 0. 049 0. 027 0. 022 READ: 7, 2 -�� -- ------------- ---- --- ----- ------- ------ -1/, ------------- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 064 0. 044 0. 026 PEAK AREA (AES-SECONDS) 0. 046 0 . 025 0. 021 ' READ- 6. 6 ----------------------------------- ---------------=----------------------------- MEAN= 6 . 9 STD.DEV. = 0. 4 COEF.VAR.. = 5.74 % E31=- 00 -4s AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 0 I1- 0. 012 0 . 01E PEAK AREA (ABS-SECONDS) Z 0. 004 0. 008 READ---------0 , 6------- -- -/3 3�-__P-Z -------------------- - ZAA FG PEAK HEIGHT (ABSORBANCE) 0. 016 0. 010 ' PEAK AREA (ABS-SECONDS) 0. 004 0. 00: READ: 0.5 ------------------------- ---------_-------------------------- MEAN= 0. 5 STD.DCOEF.VAF.. - 5, 96 % !E3 E: 000 ' AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 06 0. 056 0. 021 PEAK AREA (ABS-SECONDS) 0. 4 0. 03 0. 01;' Pas 79 READ-------- 10 , 1----------- ------- ---- ---------------� �10 1 ------ AA SAA BG-. ' PEAK HEIGHT (ABSORBANCE) 0. 0;0 0. 056 0. 019 PEAK AREA (ABS-SECONDS) 0. 048 0. 0:32 0, 016 P.EAB---------------------------------------------------------------------------- MEAN= 9. 7 STD.DEV. = 0. 1 COEF.VAR. = 1 . 50 % S E 0 0 5 5 AA A EG PEAK HEIGHT (ABSORBANCE) 0. 033 . 012 0. 030 ' PEAK AREA (ABS-SECONDS) 0. 049 0. 002 0. 04; READ: 0. 14-1 -.ow ----------------------- O 0 5 5 (CONTIN ED) ' AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 018 0 . 010 0. 014 PEAK AREA (ADS-SECONDS) 0. 014 0. 002 0. 012 ' READ------------------ ---- ------------------------------------------------------ MEAN= 0. 1 ,TD.DEV. = 0. 1 COEF.VAR. = 54. 72 `X ' E3E: 0056 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 067 0. 05 0. 020 ' PEAK AREA (ABS-SECONDS) 0. 0- 0. 031 0. 018 READ: -------------V' ---- -------- --- - ---- --- - / ------------ �1-�//-------------- ' AA ZAA DG PEAK HEIGHT (ADSORDANCE) 0. 074 0. 055 0. 012 PEAK AREA (ADS-SECONDS) 0. 068 0 . 037 0 . 031 ' READ: 10. 2 MEAN= 9. 2 TD.DEV. = 1 . 4 COEF.VAR. = 14.98 E3 005: AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 307 0. 242 0. 06E PEAK AREA (ABS-SECONDS) 0. 211 0. 159 0. 052 ' --------------- ---- --- ----- ---- ----- ---READ:- ------------- --- ----- ---- ---8---------C&-------------�3 ----- --------- AA T 2AA PG PEAK HEIGHT (ADSOREANCE) 0. 308 0. 37 0. 072 ' PEAK AREA (ADS-SECONDS) 0.213 0. 160 0. 053 READ: 46.6 MEAN= 46. 4 STD.DE1. = 0.2 COEF.VAR. = 0. 4; E: 0 0 5 ' AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 019 0. 010 0 . 011 PEAK AREA (ABS-SECONDS) 0101.3 0. 001 0. 012 READ--------------- -------- -----------------w------------------0000180 - -- ---- AA S. ZAA DG PEAS: HEIGHT (ABSORBANCE) 0. 016 0. 013 0. 011 PEAK: AREA (ADS-SECONDS) 0. 015 0. 005 01010 READ 1 . 0 MEAN= 0. 4 STD.DEV. = 0. 9 COEF,VAR.= 99,99 % SE: o 05s AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 068 0. 052 0, 01P0 PEAK AREA (ABS-SECONDS) 0. 046 0. 032 0. 014 READ: 8.5 ----------------------------- --------11�= 5p�----------- --- -------- ------ 0 050 (CONTII` ED) AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. Gf9 0. 056 0, 01-7 PEAK AREA (ABS-SECONDS) 0. 051 0. 037 0. 014 F,EAB_ 1011 ------- ----- ------------- ----------- - -------- MEAN= 9. 3 D.DEV. = 1 . 1 COEF.VAP.. = 11 ,71 % S E: 0 0 s 0 - AA SAA BG PEAK HEIGHT (ABSORBANCE) 0. 022 04013 0. 01;' ' PEAK AREA (ABS-SECONDS) 0. 02:�s 0. 005 0. 0I8 READ: ----0 . 8--- --------- ---- ---- ---- ------- -3 AA ------ --------- -- --- - - - -- --- ' AA 7AA EG PEAK HEIGHT (ABSORBANCE) 0, 016 0. 011 0. 010 PEAK AREA (ADS-SECONDS) 0. 011 0. G4 01009 READ. 0.3 ' MEAN= 016 ST . EV. = 0. 4 COEF.VAP... = 73. 76 % S I= 0 0 c_ 1 AA 7AA pG PEAK HEIGHT (ABSORBANCE) 0. 072 0. 060 0 . 016 PEAK AREA (ARS-SECONDS) 0. 048 / 0. 03 0 . 010 READ: 10. 3 / ' - --------- --------- ---- ------------ ----------- ------------- --- - --- ----- / AA ZAA EG PEAK HEIGHT (AESORBANCE) i/ 0. 081 0. 050 0. 0=10 ' PEAK AREA (ADS-SECONDS) 0. 070 0. 0.139 0. 0S I READ: 10.7 ------------------- ------z -------- ------------ - , ------------- - -----MEAN= 10. 5 STD.D0.3 COEF. VAR. = 17 % E3 E O O E XA ZAA RG PEAK HEIGHT (ABSORBANCE) 0. 014 0, 016 PEAK AREA (ABS-SECONDS) 0. 005 0. 010 ' READ: 1 . 1 0000181 . -------------------------------- -1 8=o----------------------- --- ----- AA ZAA PC PEAK HEIGHT (ABSORBANCE) - / 0. 022 0. 012 0. 016 PEAK AREA (AES-SECONDS) 01016 0. 006 0 , 010 NYTEST ENVIRONMENTAL INC. FURNACE ANALYSIS RUN LOG ANALYST: p,C�•CMM� EL= 74 DATE: Z 2 -- U-2.?r iD ' — CALIBRA.T!ON DATE: /� Z LOGIN N's: -20 START TINME: 3 ENT TDME: s ff {{ Y _ .. { STSOURCE: cSp�X i ' STANDARD LOT = . b7- TJ-- S AN— ARD PREP.—.RA-110's DAT—,::: STA`+-DFX?iR.=TION DAT- 13D zf STANDARD PREFAR•=.TION LOGBOOK PAGS 7 3 � t QC SA. P, tiCCBt'"1�\'CELI)rtITS .`: ` CO�IIIE`'TS :jCv I 96 ,10 I ` IC5 I < (:I—) CRQL. CCV 90—i IO I I ' CCB I < (j/—) CRQL I LCS I SO-120 or E?A LIN-1ITS I I PREPARATION BLANK I < (=1—) CRQL I ' DUPLICATE I = SPIKE I REVIEWED BY: 0000182 1 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 008 0. 010 0. 00? PEAK AREA (ABS-SECONDS) -0. 001 0. 000 -O. 00L READ-------0. 000- ---- --- --------- ------�--- -- --------------------------- ------- AA ZAA Br-. ' PEAK: HEIGHT (ABSORBANCE) 0. 008 0, 014 0. 005 PEAK AREA (ABS-SECONDS) -01003 -0. 001 -0. 002 READ: -0. 002 -------------- MEAN= -0. 00, c1 - _ �TD, DEV, = O. 00-1 COEF.VAR. = 99.99-%---------- ------- 0, 000 AUTOZERO T L AA ZAA BG PEAK HEIGHT (ADSORBANCE) 1 . 068 0. 4 71Z 0.596 PEAK: AREA (ABS-SECONDS) 0.668 0. 330 0, 338 ' READ---- - ------------ ----------------_ --------------------------- -------- --- 1�0 AA ZAA BG PEAK: HEIGHT (ABSORBANCE) 0.995 0. 462 0. 5.38 ' PEAK AREA (ABS-SECONDS) 0. 65'9 0, 225 0,:3::Bq READ: 0.326 - --- --- -----`�- - -- -------------------- ---------------- ---- MEAN= 0. 328 STD. DEV. = 0. 004 COEF.VAk. = 1 . 07 7. 100. 0 STANDARD 1 T L AA SAA BG PEAS: HEIGHT (ABSORBANCE) 0. 590 0, 300 0.291 PEAK: AREA (ABS-SECONDS) 0.:955 00186 0. 170 READ. --------56.' 50- AA ZAA BG PEAK: HEIGHT (ABSORBANCE ) 0.592 0. 302 0 . 2925 ' PEAK AREA (AES-SECONDS) 0,357 0. 188 0. 169 READ- 57. 5 -------- - ---- ---- ---- ------------ ----------------------------------- ' MEAN= 57. 1 STD. DEV, = 0.5 COEF. VAP. = 0. 94 . 50. 0 STANDARD 2 T L AA Z. AA BG PEAS: HEIGHT (ABSORBANCE) 0. 3:914, 0. 180 0 . 156 PEAK: AREA (ADS-SECONDS) 01199 0. 105 0. 093 READ----------------------------- ------------------------------- -------- ---- --- 0000183 1 (CONTINUED) AA SAA BC PEAK HEIGHT (ABSORBANCE) 0. 330 0. 1;9 0. 155 PEAK AREA (AFS—SECONDS) 0. 196 0. 105 0. 091 ' READ- 26.3 — -------- —---------------—------ — ---—---- ---------------------------—---— --— -— -- MEAN= 26.;=c STD. DEV, = — 0. G COEF. VAR, = 0 . 0:9 7,. 25. 0 STANDARD = ' T L AA ZAA BG PEAS: HEIGHT (ABSORBANCE) 0. 1=9° 0. 077 O. G64 ' PEA}: AREA (AFS—SECONDS) 0. 079 0 , 045 0. 084 READ: 9.5 — —------------------- ----—------— ---—------ -----------—- --—-------— ---- —----- — ' AA ?AA Dll: PEAK HEIGHT (ABSORBANCE) 0. 150 0. 085 0. 068 PEAK AREA (ADS—SECONDS) 0. 086 0. 045 0 . 042 ' READ: 913 MEAN= 9. 4 STD. DF.V, = 0. 1 COEF.VAR. = 1 . 45 % 9. 8 STANDARD 4 0000184 TL ' AA LAA EG PEAK; HEIGHT (AESOREANCE) 0. 908 0.423 0. 486 PEAK AREA (AES-SECONDS) 0.604 0.307 0. 297 1 READ --------91 .9--------- --------------4�---------------�-Q� --------- ------- AA LAA BC 1 PEAK HEIGHT (ABSORBANCE) 0.892 0. 424 0. 484 PEAK; AREA (ABS-SECONDS) 0, 601 0. :302 0.299 READ: 90. 2 - ------- ----- -------- --------- --------------------------------- ------- MEAN= 91 . 1 STD. DEV. = 1 ,4 COEF.b'AR, = 1 .51 % 1 TL AA LAA EC PEAK: HEIGHT (ABSOREANCE) 0. 011 0. 010 0. 006 PEAK AREA (AES-SECONDS) 0. 003 0. 003 0 . 000 1 READ: 016 -------- ----------------- --------------L�------ ----------------------- - ------- AA LAA BC PEAK HEIGHT (ABSOR.EANCE ) 0. 009 0. 010 0 . 009 PEAK AREA (AES-SECONDS) 0. 000 0100 -O . 00c 1 READ- 0. 6 -------- ----- ------------- ------------------------------ ----- -------- --- MEAN= 0.6 STD, DEV. = 0. 0 COEF. VAR. = 2. 58 1 TL AA LAA EC 1 PEAK; HEIGHT (AESORBANCE) 0. 148 0. 082 0. 067 PEAK AREA (AES-SECONDS) 0. 083 0. 044 0. 040 READ: 9.5 -- ----------- -------- - -------- --- -- ------ fw=-------- ---------------- ----- ------ AA LAA PC. PEAK HEIGHT (ABSORBANCE ) 0. 147 0. 084 0. 065 1 PEAK: AREA (ADS-SECONDS) 0. 083 0. 046 READ: 9. 9 MEAN= 9. 7 STU, DEV, - 0. 4 COEF. VAR. = 3.76 % 1 TL AA LAA PC PEAK HEIGHT (AESOREANCE) 0. 592 0, 314 0 .279 PEAK. AREA (AES-SECONDS) 0. 7-(62 0. 19.3 0. 169 READ: 51 .7 ------------------------- ----- �1_'�------ - -f----------- /01/--- ---- ------- AA LAA EG ' PEAK HEIGHT (ABSORBANCE ) 0.558 0,292 0, 269 PEAK: AREA (AES-SECONDS) 0. 354 0. 184 0. 1;70 READ----- ----- 0000185 --- - ------- ----------- -------------------------- ------ --- MEAN= 50.'9 STD, DEV. = 2. 1 COEF.VAR. = 4.25 % TL AA ZAA . BG PEAK HEIGHT (ABSORBANCE) 0. 009 0, 014 0. 00: PEAK AREA (ABS-SECONDS) 0. 003 -0. 001 0100.3 READ: ------0. 1----- ------------------- ---------------------------------- AA ZAA PC PEAK. HEIGHT (ABSORBANCE) 0. 010 01011 0. 006 PEAK AREA (ABS-SECONDS) 0 . 000 0. 001 -0 . 001 READ: 0. 2 ----------------------------------------------------------------------------- --- MEAN= 0. 0 STD. DEV. = 0.2 COEF.VAR. = 99.99 % TL 0011 AA ZAA BG PEAK HEIGHT (AESOF.DANCEZEV. = OO'2- 0. 011 0. 016 PEAK AREA (ABS-SECONDS) -01001 0 . 013 READ: ---------D* i-- --- -- --------------- ---------------- --- ZAA. BC. PEAK HEIGHT (ABSORBANCE0 , 012 0. 013 PEAK AREA (ABS-SECONDS) 0. 000 0 . 016 READ: 0, 1 MEAN= 0. 0 STDOEF.VAR, = 99. 99 TL 001 ^ AA LAA BG PEAK HEIGHT (ABSORPANCE) 0, 274 0, 141F. 0 . 130 PEAK AREA (ABS-SECONDS) 0, 151 0 . 0;'9 0. 072 pp F.EAD-------- 18, 1- ---- ------- - ---- ---- ---J ------------ 1- ----------- --- AA ZAA BG PEAS. HEIGHT (ABSORBANCE ) 0.268 0. 152 0. 12.3 PEAK AREA (ABS-SECONDS) 0, 148 0. 0,•9 0. 069 READ: 18. 2 - -------- --------------- -------- -------------- MEAN= 18. 2 STD/.'DEV. = 0. 1 COEF.VAR. = 0. '38 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 459 0.239 0.220 PEAK AREA (ADS-SECONDS) 0..31, 0. 160 0. 157 READ--------41 • --- ---------lax------ ---/---02 -Az2-- -------------------- --- AA ZAA Br PEAY. HEIGHT (ABSORBANCE) 0.455 0, 299 0. 224 PEAK AREA (ABS-SECONDS) 0.316 0. 160 0 . 15.•' READ: 41 . 2 ------------------------ - MEAN= 41 .3 STD, DEV. = 0. 1 COEF.VAR. = 0.22 % Q 0 0 018 6 T L 0 0 1 44 AA LAA BG PEAK HEIGHT (ABSORBANCE) 0. 625 0.319 0.?10 VCAV nnr_n l AlQ_ctnnMnc l n A O n DOM n X 1 0 --------- --------- --------- ---- - -- ------ ------- READ: 62. 4 _10�-- -� - -�GSS �1/Z -�- -F�f'- AA ZAA BG PEA}: HEIGHT (ABSORBANCE) 0.615 0.316 0. 301 PEAK AREA (ABS-SECONDS) 0, 430 0,216 0.214 READ: 59. 4 -- . ---- --- MEAN= 60.E STD, D -------------------------------------------- _r .4COEF.VAR. = 3. 32 �--- --- ----- ----- -- ----------------- TL 4 O 1 t5 ' AA ZAA BG _ PEAK HEIGHT (ABSORDANCE) 0, 02° 0. 011 0 . 026 PEAK. AREA (ABS-SECONDS) 0. 0 0. 000 0. 01;` READ: - --------0. 1- --- - -------- ---- --- ---�318 -------------------- -------- AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0. 0`32 0. 014 0, 022 PEAK AREA (ABS-SECONDS) 0. 018 -0. 00: 0 . 020 READ: -0. 3 -------- ----- ---- ---- --- -----------0.2-- -------------------------------- --- MEAN= -0, 1 ST . DEV. = COEF.VAR, = 99. 99 ' . T L 00 1 C AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0, 212 0. 117 0. 102 PEAY. AREA (AFS-SECONDS) Z0, 0, 082 0. 081 READ:--------- -------- ---- ---- -------------19. 0 -A------------ �- ------------ ZAA BG PEAY. HEIGHT (ABSORBANCE0, 115 0. 101 PEAK AREA (ABS-SECONDS) 0. 082 0. 080 P..EA18. 9 -- - -- --------- - MEAN= 19. 0 STDF. VAF'. = 0.60 K T L 0 O 1 ? Z. DEV, = O.041 SAA BG PEAK HEIGHT (ABSORBANC6 0. 011 0. 021 PEAK AREA (ABS-SECONDS0. 003 0. 013 READ; 0. 6 �=---� --------------------------- ZAA B"� PEAK HEIGHT (ABSORBANC8 0. 012 0, 023 PEAK AREA (ABS-SECONDS0 0. 000 0, 020 READ: 0 . 0 MEAPJ= 0.:3 STCOEF.VAR. = 99.99 0000187 AA LAA BG PEAK HEIGHT (ABSORBANCE) 0X* 15 26 0. 147 0. 124 PEAK AREA (ABS-SECONDS) 0. 080 0, 069 READ; 18.5 ----------------- ---------- ------------�3-;/------- --- ZAA BG PEA}: HEIGHT (ABSORBANCE) 0. 144 0. 120 PEAK: AREA (ABS-SECONDS) 0. 061 0. 065 READ: 18. 7 MEAN= 18.6 STD.DEV . = 0.97 '%. T L 00113 AA SAA F;G PEAK; HEIGHT (ABSORBANCE) 0, 449 0. 235 0.220 PEAK AREA (ABS-SECONDS) 0.•311 0. 162 0. 149 REA --------------------- -------- -----------42. 0----- --------��- --- ---�3°� =- S� -2---------------- --- ---- AA LAA BG PEAK HEIGHT (ABSORBANCE) 0.450 0 , .. ".+9 0 . ??? PEAK: AREA (ABS-SECONDS) 0, 320 0. 161 0. 159 lREAD: 41 . 7 MEAN= 41 ,8 STD, DE.V, = 0,2 COEF, VAR, = 0,59 % TL 000 ZO.07 LAA EC_. PEAK: HEIGHT (ABSORBANCE) 0 , 601 0. :306 0.308 PEAY. AREA (ADS-SECONDS) 0.219 0.212 READ---- - ---60. 4- ---- ---- -A---------------l6 - ---- --- ---- LAA BC. PEAK HEIGHT (ABSORBANCE) 0. 306 0. 310 PEAK: AREA (ABS-SECONDS) 0. 2?i 0 .216 READ: 61 , 3 -------- ----------------- MEAN=------60,9---- STD. DCOEF,VAR. =-- 1 . 11 - - ----------- --- --- T L O O ZZ, 1 AA LAA BG PEAK; HEIGHT (ABSORBANCE) 0. 550 0.26E 0.265 PEA}: AREA (ABS-SECONDS) 0.956 G. 18:3 0, 17.3 READ 48.6 ------------ ------------6_�f��----- ----------------- AA AA LAA BG PEAK HEIGHT (ABSORBANCE) 0.551 0. 286 0.268 PEAK: AREA (ABS-SECONDS) 0. 362 0. 184 Q. 178 READ: 48. 9 00001818 --- - -- �� ----- ---- --- ----- --�----------------- MEAN= 48.7 STD, DEV, = 0.2CQEF, VAR, = 0 , 4:3 T L 0 O ^17=1 AA ZAA EG PEAK HEIGHT (ABSORDANCE) 0. 012 0. 016 0. 010 PEA}. AREA (ABS-SECONDS) 0, 005 0. 000 0. 005 READ- ---------0. 0- ---------------- ---------� --------------------------------- AA Y_ ZAA BC- PEAK HEIGHT (ABSOP.BANCE) 0, 012 0. 010 0. 009 PEAK AREA (ABS-SECONDS) 01003 -0. 004 0. 007 READ0. 7 --------- --------------------------------------------------------- ------- MEAN= -0. 4 STD. DEV. = 0. 5 COEF,VAR. = 99.99 % AA LAA EG PEAK HEIGHT (ABSORBANCE) 0. 036 0. 010 0. 0:9.3 PEAK AREA (ABS-SECONDS) 0. 02 -0. 00:' 0. 026 READ----------------- -------------- ---Lltv--=---zi-------------------- ------- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 033 0. 012 0. 032 PEAK AREA (ABS-SECONDS) 0, 024 0, 002 0. 022 READ------------ - -- --- ---- ------- ---- MEAN= 0. 1 ST . DEV. = 0.6 COEF.VAR, = 99,99 °X. T L O 0 7=1-4 AA LAA BG PEAS; HEIGHT (ABSORBANCE) 0 , 212 0. 110 0. 107 PEAK AREA (ABS-SECONDS) 0. 179 0 . 084 0. 095 READ: 1915 -- ------- ------------ ----------------- ----�7- -----------� -/--- - -------- --- AA LAA FG PEAK HEIGHT (ABSORBANCEZEV, = 0.210 0. 116 PEAS: AREA (ABS-SECONDS) 0. 172 0. 0°3 0. 085 READ: 20 . 4 --------------------- -- ----------------- ---------------- ----------- MEAN= 20. 0 STD0.7 CUEF.VAR. = 3. 47 . TL C} O ^S AA ZAA BG PEAK HEIGHT (ABSORBANCE)XA 0. 020 0. 027 PEAK. AREA (ABS-SECONDS) 0. 006 0, 025 READ--------- i,- ----- --- ZAA P.:;PEAK HEIGHT (ABSORBANCE) 0. 012 0. 028 PEAK AREA (ABS-SECONDS) 0. 00.3 0. 023 READ: 0 . 6 MEAN= 1 . 0 STD. DEV. = 0. 5 COEF. VAR. = 48.21 T L 0 0 6 AA LAA BG PEAK HEIGHT (ABSORBANCE) 0. 19LC3 0. 112 0. 096 PEAK. AREA (ABS-SECONDS) 0. 174 0. 084 0. 090 ------------ 19. 4-----------------------� -js- ------------� - ��------------ A LAA BC PEAK HEIGHT (ABSORBANCE) . 192 0. 098 0. 096 PEAK AREA (ABS-SECONDS) 0. 176 0. 084 0. 098 READ: -------- 19.5----------- ---- ----------------------------------------------- MEAN= 19.5 STD. DEV 0. 0 COEF.VAR. = 0. 15 . ZLAA BG PEAK HEIGHT (ABSORBANCE) 00. 012 0. 025 PEA}: ,AREA (AES-SECONDS) 00. 002 0, 025 READ---------0. 5- ---- -- --------------- ---- �-------------- --- AA LAA PG PEAY. HEIGHT (ABSORBANCE ) 0. 0:32 0 , 012 0, 028 PEAK AREA (ADS-SECONDS) 0. 029 0, 005 0. 024 READ: 1 . 1 MEAN= 0.8 STP. DE`J. = 0.4 COEF. VAR. = 52.71 �. T L 0 0 2! AA LAA DG PEAS; HEIGHT (ABSORDANCE) 0, 200 / 0. 106 0. 101 PEAK AREA (ABS-SECONDS) 0. 171 0. 085 0, 086 READ: 1916 - --------------------- - AA =AA Dr; PEAK HEIGHT (ABSORBANCE ) � 0.^c02 0 , 10° 0. 099 PEAK AREA (ABS-SECONDS) / 0, 1;4 0. 065 0. 0219 READ: 19 . 6 - ------------------------ ---=- ----- -------- --- -------------------- - --- MEAN= 19. 6 STD, DE.V = 0. 0 COEF. VAR. = 0. 03 % TL O O ^9:) AA LAA- $G PEAK HEIGHT (ABSORBANCE) 0. 40E 0. 209 0 .205 PEAK AREA (ADS-SECONDS) 0.::-�68% 0. 183 0. 185 READ. 48.6 X ------------- ---- ---- ---- ---- ---- ----- ------- �� ,� ---- --- ----- --- AA LAA E;G PEAK HEIGHT (ADSORBANCE) 0.405 0, 208 0. 202 PEAK AREA (ABS-SECONDS) 0. 873 0. 188 0 . 185 READ: 50 . 1 (l 0 0 0 1 `? 0 ------------- - ------------ --------- ------------------------------------ ----- - -- MEAN= 49- -.3- 9,:j STD, D}=� , = 1 . 1 COEF. VAR. - 2.29 �- TL 00 : 0 AA ZAA BG PEAK HEIGHT (ADSORDANCE) 0. 564 0.296 0 .273 PEAY. AREA (ADS-SECONDS) 0.365 0. 189 0. 175 READ- 50.6 Cov. --------------------{ ------------ ' AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0.552 0. 287 0. 272 PEAK AREA (ADS-SECONDS) 0,357 0. 185 0. 172 READ: 49. 2 MEAN= 49. 9 STD. DEV. = 1 . 1 COEF,VAR. = 2. 26 . T L 0 0 -.D 1 AA ZAA DG PEAK: HEIGHT (ABSORDANCE) 0 . 014 0. 010 0. 012 PEAK AREA (ABS-SECONDS) 0. 00; -0. 001 0. 00° READ.- ----------------- ------------ ------------ EAD:----------------- ------------ ------------ ------ -----------3 ------ f'------ --- AA `AA F PEAK HEIGHT (ABSORBANCE) 0. 012 0. 012 0. 009 PEAK AREA (ABS-SECONDS) 0. 002 -0. 0015 0. 007 READ1 . 0 --------- --------- ----- ----------- -------------------------------- ------- MEAN= -0.6 STD, DEV, = 0.5 COEF.VAF.. = 91 . 53 % AA ZAA PC PEAS: HEIGHT (ABSORBANCE) 0XAA 018 0. 010 0. 020 PEAY. AREA (ADS-SECONDS) 0 . 001 0. 012 READ- --------- 0.2------------------ ----- ---- -------- ------ ---ZAA $GPEAY: HEIGHT (ABSORBANCE) 0, 010 0 . 016 PEAS: AREA (ABS-SECONDS) 0. 011 -0. 002 0. 013REAP: 0. 4 ------------------------_ ------ ----- --------------------------------- ---- --- ---- MEAN= -0. 1 STD./DEV. = 0.4 COEF.VAR. = 99.99 X. T L 0 O :B-Hc AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0, 213 0. 117 0. 099 54 PEAK AREA (ABS-SECONDS) 0. 1 0. 079 0 . 074 ZCd READ-------- 1V--- --------------------- fgs- ------------------ --------- AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0.210 0. 114 0. 103 PEAK AREA (ABS-SECONDS) 0. 15:j 0. 072 0 . 081 READ: 16 . 4 0000191 .� MEAN=------i'+ :-J-----STD. DEV. =----- -- 1 .5-----COEF.VAR. =--��-------------------- AA 2AA PC PEAK; HEIGHT (ABSORBANCE) X213 0,224 0.200 PEAK AREA (ABS-SECONDS) 0. 149 0, 141 READ--------- •8-------------- - 15- � #&2/.2---------------------- 2AA Bc. PEAK HEIGHT (ABSORBANCE) 0. 211 0, 204 PEAK AREA (ARS-SECONDS) 0. 145 0. 141 READ-. 36. 7 ---------------------------------------------------- MEAN= 97. 2 STD. , = 0.8 COEF, VAR, = 2.23 �. AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 58- 0.299 0. x°7 PEA} AREA (ABS-SECONDS) 0.4 0.209 0. 20'3 READ- 55. 1 u� .4 - ---------------- ---- --------------- ---- ---------------s-- ------ ------- AA 2AA P. PEAK HEIGHT (ADSORBANCE) 0.564 0, 207 0. 281 PEAK AREA (ADS-SECONDS) 0, 403 0.20c 0. 198 READ56 , 0 -------- -------- ----------------------------------- ----------- - - -- - --- MEAN= -- ------------------------------ ----------- - -- - --- MEAN= 55.6 STL?.l�EV. = 0.7 COEF, VAR, = 1 .34 %. T L O O G AA SAA 9G PEAS: HEIGHT (APSORDANCE) 0 . 027 0. 011 0 . 022 PEAK AREA (ADS-SECONDS) 0. 01; -0. 001 0, O1 P,EAB---------0. 1- ---- ---------------�.33/ --= ��- ------------ --------- -- -------- AA 2AA DG PEAK HEIGHT (ABSORBANCE ) 0. 029 0. 019 0, 027 PEAS: AREA (AES-SECONDS) 0 , 021 0. 001 0. 020 READ: 0. 2 j i MEAN= 0. 1 STD. DEV, - 0,2 COEF.VAR. = 99. 99 . TL O O : f AA 7AA BG PEAK; HEIGHT (ABSORDANCE) 0 , 1224 0. 121 0. 10 PEAK AREA (ADS-SECONDS) 0. 1 0, 079 0, 085 READJ � -------------- ----- -------- ----- ----- ---- ------------- - `- /------- ---- --- IZ AA .:.AA B0 PEAK HEIGHT (ABSORBANCE ) 0.231 0, 121 0. 110 PEAK AREA (AES-SECONDS) 0. 1E+6 0. 080 0. 086 READ: 10. 6 000019 ? -------- ------------- ----------------- ---------------------------------- - ------- rTT TT-„ - A rnrC l)AM - 1 Art ./ i'ILHIV- lO,Y .0. 121. LlLV , v+.. vva-a r 't—.1 a •�v ro '1F�E�E�E iF IE 1E jE jF if�E 1F iF IE�F 9F�F iF�E jE iF iE�F jF 1F�F 9F?4 1E jE*jE*jE��F 1F 3E jF dF iF dE aF�F 3E�F jF 1E iF-1F$�F iF jF?F iF��F iE�F�F iF iE�F�E-1E jF 9F 9F�E 9F�F-1E?E 9F 3F��E�k T L O O ',=s L AA SAA PG PEAK HEIGHT (ABSORBANCE) X0. 1 5 0. 013 0. 07 PEAK AREA (ADS-SECONDS) 2 0. 001. 0. 022 READ: 0.2 ------------- -------- ----- 33/_S O Ofh°------------ ----------- ' ZAA PC PEAK HEIGHT (ABSORBANCE) 9 0. 012 0. 02'3 PEAK; AREA (ABS-SECONDS) 1 0, 00: 0. 019 READ---------------------- -------------------------------------- MEAN= 0,:3 STP, DECOEF.VAF;. = 44. 00 '. T L O 0 ._ S) AA / 2AA FC PEAK: HEIGHT (ABSORBANCE) 0 . 231 0. 125 0. 106 PEAK AREA (ARS-SECONDS) 0. 1 i 0. 083 0. 0°10 READ. 19.2 ------------------------------------ ---o---- ----- ------- /---- ---- --- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0.2:32 0. 127 0. 111 PEAK; AREA (ABS-SECONDS) 0 , 168 0. 080 0. 089 READ: 18. 3 ----------------- --------- -- - ----------- --------------- ---------------- ----- --- MEAN= 18* 8 STD, D V, = 0,7 COEF, VAR, = 3.59 � TL 00 -40 AA ZAA PC PEAK: HEIGHT (ABSORDANCE) 0. 468 0. 247 0.232 PEAK AREA (ABS-SECONDS) 0.349 0. 178 0, 1'1 READ: 47, 0 - ----- --------------- -------- ----------- ----S- --------- ------- AA ZAA FSC PEAK HEIGHT (ABSORBANCE-) 0.478 0, 248 0 . 234 PEAK: AREA (ABS-SECONDS) 0, :341 0, 174 0 . 167 READ: 45. 8 ------ -- --- --------- ----------------- --- MEAN= 46. 4 STD. DEV1 . 0 COEF.VAR. = 2. 10 %. T L 0 O -4. 1. AA 2AA PC PEAK: HEIGHT (ABSORBANCE) 0, 531' 0. 284 0 .161 PEA}: AREA (ABS-SECONDS) 0.:356 0 . 187 01159 READ ----- ---49.9----- --------- --- -�'-f5 eM--- ----cC ---- ------Z1 ---- - ------ AA ZAA PC PEAS: HEIGHT (ABSORBANCE) 0.535 01280 0. 257 PEAK: AREA (ABS-SECONDS) 0. :3621 01189 0 . 173 READ: 50, 5 0000193 --------------_---- ---n------- --------------------------------- --- Mrnni_ WAD - n pCi M ��Mry JV. t 01U0 uLv . v.-r \.vi:li 0 90n %f viva r.• TL 004^ AA ZAA DG PEAK HEIGHT (ABSORDANCE) 0. 015 0, 014 0. 010 PEAK AREA (ABS-SECONDS) 0. 009 0. 002 0. 008 READ. 0,4 ca - ---------------- -------- ---------------AA--- t----ZAA-------------- -- ------- PEAS. HEIGHT (ABSORBANCE) 0. 011 0. 014 0. 009 PEAT; AREA (ABS-SECONDS') 0. 003 0. 002 0. 001 READ: 0. 5 ----------------------------- -------------------------------------------- ---- --- MEAN= 0. 4 STD, DEV, = 0. 1 COEF. VAR. = 21 . 46 �. T L O O 4:Ec AA ZAA DG PEAK HEIGHT (ABSORDANCE) 0, 025 0. 011 0. 0L1 PEAS. AREA (ABS-SECONDS) 0. 01 0, 001 0, 017 READ: 0.3 - --- - --- -------------------- -------- ---J3 31 5-=ar2----------------------- ----- AA ZAA Dc., PEAK HEIGHT (ABSORBANCE) 0. 022 0. 013 0 . 020 PEAK AREA (ADS-SECONDS) 0. 0,15 0. 002 0. 013 READ: 0 , 5 MEAN= 0. 4 STD, V, = 0. 1 COEF, VAR, = 28,32 % TL 00 -4-4- AA ZAA DG PEAK HEIGHT (ADSORDANCF-) 0,212 0. 111 0. 105 PEAK AREA (ADS-SECONDS) 0. 165 0. 078 0. 087 READ--------17--------------- ----------- -- -�----------------Y��-------- --- AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0.221 0 . 120 0. 108 PEAK AREA (ADS-SECONDS) O , 1F7 0. 030 0. 087 READ: 18, 5 i MEAN=------ 18.2-----STD, D-- / =-------o�c-----COEF. VAR. =--`:�:�t--.�---------- ---- --- TL 004 AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 012- 0, 012 0, 022 PEAK AREA (ADS-SECONDS) 0. 9 0 . 000 0. 019 REA - ------------0. 1--------- ------------ ------------0. 1------ ----------- --- --- -- ----------- -- --- -------- --- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 021 0. 011 0, 017 PEAK AREA (ADS-SECONDS) 01016 0. 00.3 0. 013 READ: 0, 6 0000194 - ----------------------------------------------------n --------------------------- mcnni= n <t cT• nrw - n . d rn �r . WAD. - o ___ __ _ _ yyyY yyyy yyY Y Yyyy y y y yV l y2".yy y2",Lyy.yy♦Y♦ �Yy Y yyVy1 yTyy yyyVyV y2"•Y y♦yIy'l lY\•y y�yy yJ'yJ♦ YV y yYNYyyy y yYYY y y y.y y y ],lC]♦�"7f]♦�7C]C'��'�1C"1C��lC-lf��'!C T],lC 7C'1C��1C��1C'X'lC l♦-!C 1C]C�]C lC"I.7f 1C 7[if'1.7C 1['!f'F iC'JC]C��]f]f 7C 1C 1C'lr 7C 7C�if�F i]f�7C]C'lf��T TL 00 -4C- AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0, 228 . 126 0. 110 PEAK: AREA (ADS-SECONDS) 0. 164. 0. 079 0. 085 READ- ------- 18. 1-------------------------1-`3 3� ---0-`'�-�------- ---------- AA ZAA �_/ BC PEAK: HEIGHT (ABSORBANCE) 0. _ _5 0. 124 0. 106 PEAK AREA (AES-SECONDS) 1163 0. 083 0. 080 READ: 19. '2 _ ---- -- .7----- - --�----------------- MEAN= 13STD. DEV. �� 0.9 COEF,VAR, = 4.69 AA ZAA BG PEAK HEIGHT (ABSORBANCE) X__ 0. 01? 0 . 017 PEAK AREA (ADS-SECONDS) 0. 001 0, 012 READ_-__- -_--0♦ 3----- -------------- -------------- - --ZAA - E.2" - ------- PEAK HEIGHT (ABSORBANCE) 0. 016 0. 016 PEAK AREA (ABS-SECONDS) 0. 005 0 . 011 READ: 0. 7 -------- ----- ---- -------- -------- -------------------- ----- ------------------- --- MEAN= 0 .5 STD, DEV,,=' 0.:3 COEF.VAR. = 50.4E % TL 004E AA ZAA BG PEAS: HEIGHT (ABSORDANCE) 0, 219 0. 119 0. 10E PEAK: AREA (ABS-SECONDS) 0. 159 0. 080 0. 079 READ-- --- ------- --- - - - -- ---- ---- --- -----= ----------- f------------- X` . - - - -/ A-A ZAA B J PEAK HEIGHT (ABSORBANCE ) p;223 0. 1'20 0. 108 PEAK AREA (ABS-SECONDS) 0, 160 0. 083 0. 072 READ: 19 . 1 MEAN=---- -- 13.8-- ---STD, DEV. =/- - ---0,5 COEF, VAR+ = 2.54- -��------ -------- --- AA ZAA BG PEAK HEIGHT (ABSORPANCE) 0 . 017 0. 014 0. 020 PEAK: AREA (ADS-SECONDS) 0. 011j 0. 001 0, 010 READ: ----- -------- 0. 2-------- ------------- / moi--t-R -------------------------------- - --- A A ZAA BC PEAK HEIGHT (ADSOP.BANCE) 0. 02"1 0. 011. 0. 018 PEAK AREA (ABS-SECONDS) 0, 014 -0. 002 0. 01' READ- -0 . 4 � � G f1 191 n.,rnnl__ __ ____^_ __ ___^mT Tr1/ - ______�' ./----- - -- -- --- ----- --- 4 f^nTr ,.n Ll O�7 G1O M I'IGHIV= -V. 1 =IL• VLV , - V• Y 1 VLf • VM!' . - 77. 77 k �F lE�F dE iF iE-1F 3E�F 3E jE jF iE-IF iF?E aF fF 1E�F iF iF iF jE aF 3F iE 1F 1E iF�?lE dF�jE iE�F��e dF dF 3E iE iE�E-1F iE jE$iE iF�iF�F 9E j('*jf jF 9E jl'��jf''1F'1F iE�9F�F iE 9E*IF��F'JF 1E�E jF TL 0050 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0,224 0. 117 0. 110 PEAK AREA (ABS-SECONDS) 0. 161 0. 080 01081 READ-------- --------------------- -J-`��--- --------------------- �------------ AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.223 0. 123 0. 10: PEAK AREA (ABS-SECONDS) 0. 161 0. 080 0. 081 READ: 18.3, - --------------------------- ---------------------------------------- ------ MEAN= 18. 4 STD. DE�7. = 0. 0 COEF. VAR. = 0. 23 % TL 0051 XAASAA PC PEAK HEIGHT (ABSORBANCE) 0. 016 0. 030 ' PEAK AREA (APS-SECONDS) 0. 002 0. 031 READ: 0. 4 (�---------------------------- ------------------- -------- --- IZAA BC PEAK HEIGHT (ABSORBANCE) 0 . 01.3 0. 032PEAK AREA (ABS-SECONDS) -0. 004 0. 0:64 READ: -0. 8 i ----------- --------- - ------ MEAN= -0. 2 STD. DE1. . = 0.8 COEF. VAR. = 99.99 % TL 005^ AA SAA PC PEAK HEIGHT (ABSORBANCE) 0, 210 0. 120 0. 106 PEAK AREA (ABS-SECONDS) 0. 171 0. 083 0. 088 READ ----- --- 19.2----- ---- ---- ------- ---- --b�-- -------------/ _/------------ --- AA Z_AA BG PEAK HEIGHT (ABSORBANCE) 0.212 0. 10°. 0. 107 PEAK AREA (ABS-SECONDS) 0. 171 0. 076 0. 094 READ: 17. 5 ZZ ---- --- --------- ----- --- MEAN=------ 18.:=�-----STD, DEV• = 1 . 4 COEF. VAR. = 7, 45 '� TL 005-B AA LAA BC PEAT: HEIGHT (ABSORBANCE) 0. 539 0.274 0 . 266 PEAK AREA (ABS-SECONDS) 0. :368 0. 190 0. 170 READ: 50 .: --------------------- ------ --------- 5---------------- poi/------- ---- --- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.531 0. 27E 0. 26:6 PEAK AREA (ABS-SECONDS) 0. 366 0. 189 0. 17,• READ: 50. 5 0 0 0 rl 1 n 6 1 ----------------------------_------- ---------------_-_------------------- ---- --- MrA11I- Sn G CTT T1 %l A 113 rf1CC UAD ♦1 ID1 'N 1'1 Lf'11V- •JV.Q 11J, NL.V . - V.L LVLi snit, - V••Jt ro �F iE dF dE iE iF�F�E�l•iE��il•if•iF•%•jF iF•iE jF jF j(•iF?F�(••1F j(•�{••1F•1F jE?E?F•IF•1F iE jF jl•jE 9F�F iF jE�E�iE�E�F jF�F�h j(••1F jF jE 9E-��(•3F•1F iF iF jE iE�F•1F•!F jF�F iF�E�F jE jF jF�E•*••iF�E TL 005- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0, 012 0. 014 0. 009 ' PEAK AREA (ABS-SECONDS) 0. 001 -0. 0012 0, 0073 AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 014 0. 012 0. 011 PEAK AREA (ARS-SECONDS) 0, 012 0. 00.3 0. 009 READ: 0. 5 ----------------------------------------- -------------------------------- ---- --- MEAN= 0. 1 STD. DEV, = 0.E COEF. VAR. = 99.99 % T L O O 5 5 AA ZAA FG PEAK HEIGHT (ABSOF.BANCE) 0. 0?= 0. 014 0. 0:'12 PEA}:: AREA (ABS-SECONDS) 0. 019 0. 000 0. 019 READ: 0. 0 -------- ------------------------------ 9315-- 07 -- --------- - - --------- ------- AA ZAA PC PEAK. HEIGHT (ABSORBANCE) 0. 023 0. 010 0. 0120 PEAK AREA (ABS-SECONDS) 0, 01E -0. 001 READ: 0. 1 -- ------------ ---- - ------ MEAN= 0. 0 STD.;D V. = 0, 1 COEF.VAR. = 99, 99 . TL 005C, AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 214 0. 117 0 . 09° PEA}; AREA (AES-SECONDS) 0. 163 0. 01,:3 0, 07'3' READ----- --- 19.:9- ---- ---------------- --- --D 7-j4---- -----------% --- - ---- --- AA SAA F;�: PEAK HEIGHT (ABSORBANCE) 0.209 0. 11= 0. 101 PEAS; AREA (ABS-SECONDS ) 0. 153 0. 077 READ; 17. 5 --------------------------- _---------------- --------=--'- ---------------- --- - -- MEAN= 18.4 STD. DEV. = 1 .•B COEF. VAR. = 7.323 . T L 0 0 5:r AA ZAA PC PEAK HEIGHT (ABSORBANCE) XAA 0. 012 0. 0:90 PEAK. AREA (ARS-SECONDS) 0. 001 0. 032 READ: 0. :3 /5 - $ --------- ---- ---- ---- ------ -----Q----------- ---------- ------ --- ZAA F:C PEAK HEIGHT (ABSOP,BANCE) 0, 013 0. 03:jPEAK AREA (ABS-SECONDS) 0. 000 0. 0:34 READ: 0. 0 00001 Qt ----------------- ---------- ---------------------------------- --- INrnnl- n . CTT nfll - n ^1 f-r%=f 1/nZ - 00 OO •V rmml V- V. 1 AIL. LLV . - Vft 6.VL'1 1vmr, TL OC? .1-5o AA ZAA DG PEAK HEIGHT (ABSORDANCE) 0, 207 0. 106 0. 105 PEAK AREA (ADS-SECONDS) 0. 172 0. 078 0. 094 READ. 18. 0 ---------------------------------------J3_ ._4. 8 -------- -- �� ------------ LAA PC PEAK HEIGHT (ABSORBANCE) .210 0. 111 01108 PEAK AREA (ADS-SECONDS) 0, 174 0, 07; 0, 096 READ: 1:. 8 MEAN= 17.9 STD, D---_-------0.2-----COEF, VAR, = 0. 91 N----------------- AA 7AA PC PEAK HEIGHT (ABSORBANCE) 0. 009 0. 01= 0. 005 PEAK AREA (ADS-SECONDS) 0. 001 0. 005 -0. 005 READ: 1 . 1 ------------------ --- ----------------- ---3.3L =p6r1l ------------------ -------- AA 7AA EC, PEAK HEIGHT (ABSORBANCE) 0. 0100. 012 0, 007 PEAK AREA (ABS-SECONDS) 0. 001 -0. 002 0. 002 READ; -0. 3 -- -------- ----------------------- MEAN= 0. 4 STD EV. = 1 . 0 COEF. VAR, = 99. 99 . T L O O E O AA SAA PC PEAK HEIGHT (ADSORDANCE) 0,210 0. 115 0. 099 PEAK AREA (ABS-SECONDS) 0. 1.39 0. 075 0, 065 READ-------- ---- ---------------------- -- ----- ---------- - - ------- ---- _ paw g� AA 7AA PC PEAK HEIGHT (ABSORDANCE) O.il6 0. 124 0. 098 PEAK AREA (ADS-SECONDS) 0, 145 0. 077 0. 068 READ; 17. 8 MEAN= 17. 4 STD, DEW ------------ --------�------^-o-- -------------- --- 0. 5 COEF. VAR. _ TL 0 0c 1 2AA PEAT: HEIGHT (AI SORF:ANCE) DG 0,AA 370 0. 196 0. 17 PEAK AREA (ADS-SECONDS) 0.27 0. 146 0. 125 READ: 36.9 ------------- -----------------� x-- -------13 zs= "�.��s&-------------- --- --- AA P.C. PEAK HEIGHT (ABSORBANCE) 0.•�96; 0. 19E 0. 1:9 PEAK AREA (AFS-SECONDS) 0. 26E 0. 145 0. 121 READ----- ----------------- ----------------------------------------------------G1 -------- i Mr An.- ;,r O CTT% ncV - n '? rnrc t/AD - n d= - 1 11. 1JL V . -• V,t U%J Ll . V ni,. '�iE�F�'jE*jE�dE-1F�•�f••1F•3E�•�F jF iE?E�F al•iF$3E iF•��E dF•1F•1F�••�jF iF�F 3E*•1F$iF�F•1E jE j(•�h!F•1f�F jE jE#jE jF•1F•1h•1E�h iE iF•��F iE 9F�jF$iE�E•!h iF jF�•iF ih jF•J(•iF iF��• TL OOC � AA ZAA BG PEAK HEIGHT (APSORBANCF_) 0, 576 0..502 0.285 PEAK: AREA (ADS-SECONDS) 0.404 0. 211 0, 292 READ: 5,• .9 X -----------------------------------------1 -p-------��----- A ZAA BG PEAK HEIGHT (ABSORBANCE) 0 580 0.236 0. 289 PEAK AREA (ARS-SECONDS) 0. 408 0. 212 0. 196 READ: 58. 5 ----------------- -------------------------- MEAN= 58. 1 STD. DEV. 0.5 COEF.VAR, = 0.50 % T L 0 0 6 :tet AA SAA PC PEAT; HEIGHT (ABSORBANCE) 0. 012 0. 010 0. 003 PEAK AREA (ABS-SECONDS) 0. 002 -0. 004 0, 006 READ: _ T ----- ---- ----------------------------- ---3 3/S-_O_�-------- --- --------- ------- AA LAA PC PEAK: HEIGHT (ABSORBANCE) 0. 013 0. 011 0 . 009 PEAK AREA (ABS-SECONDS) 0. 00? 0. 001 0100, READ: 0. 2 --------------------- - ----- MEAN= -0.2 STD. DEV. = 0.7 COEF, VAR. = 99. 99 *Y,. TL OOC, -4 AA ZAA EG PEAK HEIGHT (APSORBANCE) ZO 0. 122 0. 104 PEAK AREA (ABS-SECONDS) 0. 0:8 0. 0; READ. - ---- --- 18. 0- ---- ----- - --- ---------- --- - ---- - -- - 0YA _ -�3-/-- ?AA E; PEAK. HEIGHT (ABSORBANCE) 1 0. 12° 0. 106 PEAK AREA (ABS-SECONDS) 0. 08 0. 076 READ: 19 . 1 -------- - - - - ----------------- MEAN= 18. 6 5TD, DECOEF.VAR. = 4. 4; . TL OOGS AA ZAA FG PEAK HEIGHT (ABSORDANCF_) 0, 5?9 0.2;4 0. 258 PEAK AREA (ABS-SECONDS) 0. _i59 0, 1°° 0, 170 READ: 50.3 M -------------------------- _11/--------- -- --------------& -- ---- -- - - --- AA LAA PEAK HEIGHT (ABSORBANCE) 0.526 0. 2?8 0 , 2G:' PEAK AREA (ABS-SECONDS) 0. 358 0. 1S% 0. 171 READ50, 0 - ------- ----- ----------------------------------- --------- - - -- --- ----- MCAril_ cA t QT TT T'%r., _ n rrnCr %IAL — A c:� a C.!Al. 1✓L V . - V.L� �..V L l . V P•il♦f - V.•J 1 M TL 00C, c_ PEAK HEIGHT (ABSORBANCE) AA ZAA PC 0. 014 0. 013 0. 010 PEAK AREA (ABS-SECONDS) 0. 006 0. 000 01006 READ: 0. 1 ----------------------------------------aA-- ----------------------------- --- LAA BG PEAK. HEIGHT (ABSORBANCE) 0. 011 0. 012 0. 010 PEAK AREA (ARS-SECONDS) 0. 006 -0. 002 0. 009 READ: -0, 4 ---------- ----- -------------- MEAN= -0. 2 STD. DEV, = 0.3 COEF. VAR. =--49.99- -------------- --- TL 0061 AA LAA RG PEAK HEIGHT (ABSORBANCE) 0, 014 0. 012 0. 008 PEAK. AREA (ABS-SECONDS) 0. 00 0. 000 0. 005 READ: 0. 0 _ ------------------------------------ - -3�5-o9_---------- --------------- ---- AA LAA PC PEAK HEIGHT (ABSORBANCE) 0. 019 0. 011 0. 012 PEAK AREA (ABS-SECONDS) 0. 011 0. 002 0. 009 rREAD: 0. 5 ---------------------- - /EV. = ------------------- P1EAN= 0.2 STD 0, 4 COEF, VAR. =--g5. og------------------- TL 00cQ 21 ZAA BC PEAK HEIGHT tABSORF�ANCEi 0X 211 0. 119 0. 101 PEAK. AREA (ADS-SECONDS) 0. 083 0. 069 READ: 1911 - ---- ---- ---- ---- ---- --------------- -- -------- ------ --- PE _AA F;rAK. HEIGHT (ABSORBANCE) 0. 119 O. D99 PEAS; AREA (ABS-SECONDS) 0. 150 0, 08 0. 070 READ: 1$1 .3 - ----------- ----------------- _ _____________ --- ---------------------- _ ___ MEAN= 18.7 STD. DEV, = 0.6 COEF, VAR. = 3.25 N. TL 006~ 13 ' AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0, 5290278 0•.�51 PEAK. AREA (ADS-SECONDS) 0.38 p,. `81 1�1 0. 15;• READ: 417. 9 9 ------------- --------- --------------- - -1 ------------ ----------- AA ----------- ----------- AA ZAA PC; PEAK: HEIGHT (ABSORBANCE) 0.5.34 0. 274 PEAK AREA (ABS-SECONDS) 0.260 0. ,335 0. 178 0. 2 S7 READ: 47. 00 0 0 0 0 ------------ coni= A?. .i CTT). n7w.. rri�r� �r • -r v.air ua.v r v•. vvi• • .r u.. • �- n *�.*jE..x..�.**�.*j(.*�..X..g9F�"*��'�'�"��'��'��{"�'�"**'*'1�'*�•%'�Fjh�h�l'i('iF K'*'��'*��*��'�'��'�'��'�"��'��'�'�'X'�'*��'�"��f'* T L 007- 0 AA ZAA E:G PEAK HEIGHT (ABSORBANCE) 0. 534 0.21-6 0.261 ' PEAY. AREA (ABS-SECONDS) 0.365 0. 191 0. 1; READ 51 .6 �'1_-------C�7---------------��.3_1------------ AA ZAA FG PEAY. HEIGHT (ABSORBANCE ) 0.541 0.283 0, 263 PEAT: AREA (ARS-SECONDS) 0, 364 0. 190 0. 173 READ: 51 . 0 --------------------- ------------------------------------- ---------------------- MEAN= 51 ,:9 STD. DEV, = 0.5 COEF,VAR, = 0. 91 %. TL00 -1- 1 AA SAA F;G PEAK HEIGHT (ABSORBANCE) 0. 014 0. 011 O, OOa ' PEAK AREA (ABS-SECONDS) 0. 010 -0. 001 0. 011 READ: -0.2 - ----- ---------- ----- - --- -------- - -------6CA------------ ------------ -------- --- AA 7 2AA BC. PEAK HEIGHT (ABSORBANCE) 0, 013 0. 014 0. 010 PEAK AREA (ABS-SECONDS) 0. 009 0. 005 0. 004 IREAD: 1 . 0 ------- ---- --------------------------------------------------------- -- MEAN= 0.4 STD, DEV. = 0. 3 COEF, VAR, = 99.99 % TL O O :- AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0. 011 0. 013 0. 006 PEAK AREA (ABS-SECONDS) 0. 001 0, 002 -01001 READ: 0.502 p�,. --------- ---- -------- - -----�3171 _f_j3}�S =-- - ----- ----------- ----------- AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0. 010 0. 010 0. 012 PEAS: AREA (APS-SECONDS) 0, 004 -0. 002 0. 006 READ: -0. 4 ----- -------------------------------------------------------- ---------------- --- MEAN= 0. 1 STD. DEV, = 0.6 COEF.VAR. = 99.99 . TL Q O ; PEAK HEIGHT (ABSORBANCE) AA ZAA PC 0. 222 0. 130 0. 103 PEAY. AREA (AFS-SECONDS) 0. 143 0 , 0770 . 066 READ- ----------------- ---- ---- ----------------- - EAD-------- ---- ---- ---- -----------------P%l�/9------------- q ---- -fQ ' ------- -- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.221 0. 126 0. 103 PEAK AREA (ABS-SECONDS) 0, 142 0. 0%9 0. 064 READ: 18. 1 0000201 ---- --;' r,-----r+.rn ----^-^-----r`/'1CCn�--M------ -------- Mr-nn.. li ♦ 7 ,71LrLLYr - V.s: 4VLr ♦ VNA+ - 1 • ti k. iE�F 9E 9F 1F 1F�E jF*�jF�jF 9E�E jE�F jE jE 9F iE�F��F�E iE iE 9F 9F aF��I'iE iE jE�E�F dF�h dF jE iE jF�E�F 1F�h�E iF jF 9F�F 9E�F jF jE 1E iE�F 1F iF iF 9F�F iF�E jF�F iF?E 9F 1F jE jF�F iF�F'* TL 007'-4 AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0.489 0. 259 0.236 PEAK AREA (ADS-SECONDS) 0.317 0. 167 0. 150 READ -- -------43.3-------dv------�� f I3Lfp2Sr -----1"'`�'-i-v----------------------- AA 7:AA EG PEAK HEIGHT (ABSORBANCE) 0.493 0. 258 0. 246 PEAK AREA (ABS-SECONDS) 0. 320 0. 169 0. 151 iREAD: 44. 1 -------------------------------------------------------------------------------- MEAN= 43.7 STD. DEV. = 0.6 COEF.VAR. = 1 . 47 % TL 00 �- 5 AA SAA PC PEAK HEIGHT (ABSORBANCE) 0, 505 0, 256 0.201 PEAK AREA (ABS-SECONDS) 0.379 0, 200 0. 1;:8 READ--------5-}--------------------------- - ---------------6] ----------- � AA LAA BC PEA}: HEIGHT (ABSORBANCE) 0.514 0. 267 6: 251 PEAK AREA (ABS-SECONDS) 0 , 382 0. 198 READ: 53# 5 5 -------------- ---- --------- ----------------------- ----- ----------- --------- -- MEAN= 53.8 STD, DEV, = 0. 6 COEF,VAR. = 1 . 06 7. TL O O :- 6 AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 030 0, 012 0. 02'9 PEAK AREA (ABS-SECONDS) 0. 027 0. 000 0 . Q27 READ: 0, 0 MW I SG�N - -----------------------------------13#L2= p ---------------------- ---- ---- --- AA LAA BC PEAK HEIGHT (ABSORDANCF- ) 0. 029 0. 014 01029 PEAK AREA (ABS-SECONDS! 0, 022 -0, 001 0 . 022 READ: -0. 1 --------------------- -------_---- --- ----- ---------------- - ----------- --- MEAN= -0. 1 STD, DEV. = 0. 1 COEF. VAR. = 72.78 TL O O AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 178 0. 091 0. 088 PEAK AREA (ABS-SECONDS) 0. 184 0. 087 01097 --- ----20. 2 ----- -------------- --------- - 0/ 4 ----------------Lal- ��- -------- --- AA LRA BC: PEAK HEIGHT (ABSORBANCE) 0. 175 0. 090 0. 091 PEAK AREA (ABS-SECONDS) 0. 189 0. 092 0, 09; READ; 21 . 5 0000202 AO ----.•-'? - ----- -=-------;-n-- --- ^ - - �--�---------- ---- --- Mf/.AI- f1 0 CTT TCII ( r1CC l//�L7 AA ZAA BG PEAK. HEIGHT (ABSORBANCE) 0. 023 0. 013 0. 018 PEAK AREA (ADS-SECONDS) 0. 013 0. 004 0. 009 READ- 0.8 _ do2-----------WNISc�vJ ----- PEAK HEIGHT (ABSORBANCE) AA ZAA EG 0. 017 0. 009 0, 01E PEAK AREA (ARS-SECONDS) 0. 011 -0. 001 0. 012 1 READ: -0. 2 - MEAN= 4.:=s STD, DEV. = 0.7 COEF. VAR, = 99.99 �------ ----------- AA ZAA DG PEAK HEIGHT (ABSORBANCE) 0. 18E 01100 0. 091 PEAK AREA (ABS-SECONDS) 0. 182 0. 09: 0, 091 READ: 21 , 5 -------- ------- - AA ZAA BC: PEAK HEIGHT (ABSORBANCE) 0. 185 0. 09E 0. 09' PEAK: AREA (ADS-SECONDS) 0. 188 0. 095 0, 09:3 READ: 22, 4 ------------------------ - --- ----- ---- ------- MEAN= 222. 0 STD. DEV. = 0.6 COEF. VAR. = ? �� T L O Q e Q AA ZAA DG PEAK HEIGHT (ADSOP,DANCE) 0, 025 0. 014 0. 023D PEAK AREA (ADS-SECONDS) 0. 021 0. 005 0, 01E READ,, 1 , 0 'MW �D --------- -------------------------------1 3Z° -=03------ -------------------- --- AA ZAA FG PEAK HEIGHT (ABSOP..EANCE) 0. 0:90 0. 012 0, 022n PEAK AREA (ADS-SECONDS) 01024 O. Od2 G. G22 READ: 0, 5 ------------------ ---------------------------------- - --------- - ------- MEAN= 0.: STD, DEV, = 0.4 COEF. VAR, = 51 . 85 T L 0 O o 1 AA ZAA EG PEAK HEIGHT (ABSORBANCE) 0. 184 0. 0197 0. 092 PEAY. AREA (AES-SECONDS) 0. 182 0. 090 0, 092 ---------------0---- --------- ------------ AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 185 0. 038 0. 090 PEAK AREA (AES-SECONDS) 0. 183 0. 088 0. 095 READ: 20. 4 rwr.A I_ �n71 n ncu n cz rncc i�nc - � �� - •y 1'IL PItY • LV.! J I L, LL V 1 - V 1 •J V VLI • r rilt 1 TL 00a22 AA ZAA BG � PEAK HEIGHT (ABSORBANCE) 0. 554 0.286 0.270, PEAK AREA (ABS-SECONDS) 0.369 0. 191 0. 1178 READ: 51 .2 ------------------------------lip ------- ------------------log/----------- j AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.554 0.280 0. 282 PEAK AREA (ARS-SECONDS) 0, 3;1 0. 191 0. 19 READ: 51 . 3 -------------- ------------_------------- MEAN= 51 .2 STD, DEV, = 0. 1 COEF.VAR, = 0.25 ' TL 004B AA 'AA BG PEAK HEIGHT (ABSORBANCE) 0 . 010 0. 010 0, 00;: PEAK AREA (ABS-SECONDS) 0. 00.3 -0. 00'3 0. 00E READ: -0. 5 - ----- --- -------------------------------C - --------------------------- -------- AA ZAA BC, PEAK HEIGHT (ABSORBANCE) 0. 013 0. 012 0. 008 PEAS: AREA (ABS-SECONDS) 0, 007 0. 001 0. 005 READ: 0. 3 ---------- ---------------- - ----------------- MEAN= -0. 1 STD, DEV. = 0. 6 COEF. VAR. = 99.99 % TL O044 I AAZAA BG PEAK HEIGHT (ABSORBANCE) 0. 040 0. 01.' 0. 033, PEAK AREA (ABS-SECONDS) 0. 039 0. 002 01031 -R--A- ; 1 .6 C�.V� - ----- ----- ---------------- ---------L3L�=1�#----------------------- A,4 ZAA E'1`•----- ---- PEA},: HEIGHT (ABSORBANCE ) 0. 044 0. 013 0, 042n PEAK AREA (ABS-SECONDS) 0. 039 0. 001 0. 0*3 READ: 0. 3 MEAN= 1 . 0 STD, DEV, - 0.9 COEF. VAP.. = 95,89 % TL 0045 AA 4 AA F;G PEAK HEIGHT (ARSORDANCE) 0, 2200 0. 105 0. 103 PEAK AREA (ABS-SECONDS) 0.200 0. 086 01114 rREAD: 20. 1 _ - ------- ------------- -------- -----------AA-� --------------LOo/-- --- - ---- --- 2AA BC: PEAK HEIGHT (AB5OF.BANCE) 0. 194 0, 105 0. 1.01 PEAK AREA (ABS-SECONDS) 0. 193 0. 086 0. 10; READ20. 1 ----- --- ------------------------- ---- ---- tur. nn,_ r,n 4 CTT T11-%I _ n n rnrc tIA0 I'IG MIV- 4-V• 1 .7 1.V. 1)L v . - V. V L.1JLl . v nr.• _A- n• 9F iF�E jF 1F iE�jE iE ik iE jE jE iE iE jF dE iF 9E�F�F it-1F jF-1E iE iE iE jF•!F-1E iF•IE-IE jE�F iF 1E iF 9F iF iF•3F�F�F jE 9F jF jF•iF jE 9E jE iF�jE�F iF$iF 9F iF iE��F iE•!E�f•jF jF��F�E�f�F iF�E�E�E T L O O g C, AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 08:3 0. 01.9 0. 0T8 PEAK AREA (ABS-SECONDS) 0. 079 0. 000 0, 079 READ; 0. 0 -----------------------------------------I--37�s_-----------Mw�s�---------- AA ZAA BG PEA}: HEIGHT (ABSORBANCE) 0, 077 0. 01E 0. 071 PEAK AREA (ABS-SECONDS) 0. 03:3 0. 00.9 0. 080 READ: 0. -------------------------------------- :3 MEAN= 0. STD. DEV, = 0.5 COEF.VAP. = 99,99 % TL O 0 S- AA 9- PC AA HEIGHT (ABSORBANCE) 0, 228 0, 107 0. 134 PEAK. AREA (ABS-SECONDS) 0.2.97 01086 0 , 151 -01 READ- --------20. 0--------------------------- ------- AA ZAA B: PEAK HEIGHT (ABSORBANCE) 0.227 0110.9 0. 197 PEAK AREA (ABS-SECONDS) 0, 225 0. 035 0 . 140 READ; 19. 7 ----- ------------------------------- MEAN= 19.9 STD. DEV1 = 01 B. COEF.VAR. = 1 . 48 % TL 00IS,a AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0. 069 0. 016 0. 060 PEAK AREA (ABS-SECONDS) 0. 07.1 0. 003 01066 READ: ---- ----- 1 .6------------- ---- - -- - --------------- ----- -- - --- AA ------------ --- -- - --- AA ZAA PC, 1 PEAK: HEIGHT (ABSOREANCE) 0, 066 0. 013 01060 PEAK AREA (ABS-SECONDS) 0. 0613 O, GG5 0 . 064 READ; 111 --------- ----- - ------------- ----- ------- ---------- ------------- - -------- --- MEAN= 1 . 3--- --STD1DEV. = 0.3 COEF.VAR. = 25,5.9 % T L 0 0 S� AA 7AA PC PEAK HEIGHT (ABSORBANCE) 0,22.5 0. 105 PEAL: AREA (ABS-SECONDS) 0.221 0. 089 READ: 20,8 _ ----- ---------------- ------------------- -----------------�� -- ----- ------ AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0.222 01104 0. 120 PEAK AREA (ABS-SECONDS) 0. 216 0. 033 0. 1.9:3 READ---- ------- G r G O ------------------------------ ----------------- _ 05 - ---- - -- MT n111- nn A CTT Tf\/ - t _ rnC'C %)ACl - C 1 6 M 1'iLht1V- 2V+ V J11J. JlLV . - i .i t,va,.t . vna�. - W. iv ro �F lE jE 9F jF-)E**jF�F 1F*�F�E dF�E dE iF�F�F jE iE�F�F�E iF 9E jF jF�3E�iF iE 9E 9E aF iF jE$iF iF�E dE iF�F 3F iE iE 1F 9F�F iF iF jE 9E�F iE�E jE�F$jF�F lF 9F�E jE�E iF iE�F 9F iF iE�*jE�jF TL 0 00 0 AA ?AA BG PEAK: HEIGHT (ABSORBANCE) 0. 038 0. 014 0. 040 PEAK AREA (ABS-SECONDS) 0. 044 -0. 0012 0. 045 READ-- ------- -------- ---------------- =5-03--------------- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 045 0. 012 0. 040 PEAK: AREA (ABS-SECONDS) 0. 045 -0. 001 0. 046 READ: 0. 0 -------------------------------------------------------------------------------- MEAN= -0. 1 STD, DEV, = 0. 1 COEF.VAR. = 93.75 % TL O0s 1. ! AA SAA BG i PEAK; HEIGHT (ABSORBANCE) 0, 2.12 0. 105 0. 11E PEAS: AREA (ABS-SECONDS) 0.1206 0, 086 0. 121 READ4,1 _ 19.9 _03� --- - ----------- ------------------ - ------------- -- ----�o -,-------------- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.22.3 0. 110 0, 114 PEAK: AREA (ABS-SECONDS) 0. 2'05 0. 491 0. 111 F,EAD: ?1 , 9 -------------------- -------- ---- -------------------- ------------------------ --- MEAN= 20.9 STD. DEV. = 1 .5 COEF.VAR, = 7. 40 'A. T L 0 0 D AA ZAA BG PEAK: HEIGHT (ABSORBANCE) 0. 054 0. 012 0 . 054 PEAK AREA (ABS-SECONDS) 0. 066 0, 004 0. 062 -------------- o----- ---- ------------/-------_--------------0174 MWC°� - W ----- --- AA �"A PC r PEAK HEIGHT (ABSORBANCE) 0. 051 0. 010 0. 048 PEAK: AREA (ABS-SECONDS) 0, 062 0. 002 0. 060 READ: 0. 4 MEAN= 0.6 STD. DEV, = 0.:9 COEF.VAR. = 49. 53 % TL OOS9L AA ZAA EG PEAK: HEIGHT (ABSORBANCE) 0.226 0. 106 0. 11213 PEAK AREA (ABS-SECONDS) O.211 0. 08;' 0. 1124 READ: 20. 2 �a� - -------- ---- -- , ----- -------- ---- ------------ ----------------- � ---- ---- ---- --- AA ZAA PC _. PEAK HEIGHT (ABSORBANCE) 0. 229 0. 104 0. 126 PEAK AREA (ABS-SECONDS) 0. 2221 0. 084 0. 136 READ: 19. 6 0000 . 06 ' narnnl_------ to-Q-----cTn nrt,-=-------n-S-----rnrr uon _-------------------------- �. �n yyyy.�yy yy i yyJ. Jyy �l YL. LL.v . - yyy yy yy yyV♦y V vV1 ♦ •ryl.�♦ - r.y. TYV YN yyy y... y Y y if 7C]C'�'�'��]1'"1��']C)I'lC'lC�s�'��'�"-F if'IC�']A-'�'*]C f��C]CA"llQCT]C�']C�'�"!f*�"��'��*'�'**�'��f*'lC��C�if'1♦�C��"F*�'if��F�*�]f' T L O O g 4 AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 606 0.304 0.305 PEA}: AREA (ABS-SECONDS) 0..390 0. 202 0, 188 READ: 54.: ----------------- ------------��= -- -------� ------- �,�-l� AA LAA BG PEAK HEIGHT (ABSORBANCE) 0.590 0. 3021 0. 290 PEAK AREA (ABS-SECONDS) 0.38:3 0. 199 0. 1?.4 READ; 53. E ------------ -------------------- - - MEAN= 54. �, 22 STD. DEV, = 0.9 COEF. AR, = 1 .61 ---------- ------- TL C) 0 � 5 AA ZAA gG PEAK HEIGHT (ABSORBANCE) 0. 010 0. 012 01. 009 PEAK AREA (ABS-SECONDS) 0. 005 -0. 001 0, 006 , REA ----------------------------------------- ( ----------------------- ---- ---- --- AA / LAA B1�; PEAK: HEIGHT (ABSORBANCE) 0. 010 0. 012 01005 PEAK AREA (ABS-SECONDS) 0, 000 01000 01000 READ; 0. 1 ---------0. 2 --- ----- -------- -- -------------- _ ______ -- MEAN= -0. 1 STD, DEV. = 2 COEF. VAR. = 99199 /. -FL- 1 C) C) !D G AA ZAA F;G PEAK HEIGHT (ABSORBANCE) 0. 057 0. 012 0. 05E PEAK AREA (AE;S-SECONDS) 0. 062 0. 003 0. 059 READ---------0-6- ---------------- ----- 05 = ------ - - AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 054 0. 010 0. 054 PEAK AREA (ABS-SECONDS) 0, 055 -0. 004 O. Os9 READ: -0. 6 ---------------------------------------- ------------------------- ________ _______ MEAN= 0. 0 STD, DEV, = 0. 9 COEF.VAR. = 99.99 . T L 0 C) !9 PEAK HEIGHT (ABSORBANCE) AA ZAA BG 0, 214 0. 100 0. 115 PEAK: AREA (ABS-SECONDS) 0.209 0. 082 0. 127 READ-_------ 1910 , --------------------- ---------os_k-------------q-'/------ - ---- --- AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.220 0. 112 PEAK AREA (ABS-SECONDS) 0. 11'3 O. 2211 G. 0°8 �� 0. 1214 ------------20. 4- -------------------------------- --------------- -----------20. 4----------------------------- --------------- MTAN1� 11 T ITT RTl! - � 1 ----� rnrlc ,lnu - c �q ,� ..Lrnv i�,i 0JJJ9LJLv . - t . i �.vcr . vnr,, - ,�., •� K. 9E aE 3E•1F�F iF iE jF 9F iE jE�k�F iF dF�F dF iF iE*iF iE iF�F 9E iE jE�F iF iE jE•JF iF iE�E�F•1F�E dF�jF�F$9F iE iF�E�F 3E 9E jF�iF•IE jE dE dF•1F 9F iE�F iF�F 9F iF dF iF•1F�F iF•!E jE iF iF iE�aI-�F iE iE TL 00sa AA LAA F:G PEAK HEIGHT (ABSORBANCE) 0, 418 0. 198 0.220 PEAK AREA (ABS-SECONDS) 0.389 0. 179 0. 215 READ: 45.5 --------- ------------------------------- ------- )---------- ' AA ZAA BG PEAK HEIGHT (ABSORBANCE) 0.418 0. 202 0. 21E PEAK AREA (ABS-SECONDS) 0, 30-18 0. 178 0.210 tREAD: 47. 0 M W S --------- ---- -----------------------------------------------------°------------- MEAN= 46.2 STD, DEV. = 1 ,2 COEF.VAR. = 22.64 % TL 00 � � AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0, 01:3 0. 014 0. 010 PEAK AREA (ABS-SECONDS) 0. 007 0. 000 0, 008 READ ------------- D. C'- --- ---------------------1� z�S=�1 ------------ ---- ------- AA ------- ' AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 011 0, 009 0. 010 PEAK AREA (ABS-SECONDS) 0. 007 -0. 002 0. 006 READ: -0. 3 ---------------------- --------------------------------------- MEAN= -0. 1 STD. DEV. = 0.2 COEF. VAR. = 99,99 % TL 0100 AA ZAA PC PEAT; HEIGHT (ABSORBANCE) 0. 211 0, 113 0. 102 PEAK AREA (ABS-SECONDS) 0. 178 0. 093 01Q$5 ' READ21 . 8 ----- --- ----- -------- --- ----------- ------------- ------ ---- --- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0.203 0. 108 0, 099 PEAK AREA (ABS-SECONDS) 0. 089 0. 0°5 READ: 20, 9 -------------- ----------------------------------- MEAN= 21 .:i STD, DEV. = 0.7 COEF.VAR. = 3, 25 % jF iE�F*�iE�E jF jE iF�F jE iF jF 9F dE*iF•3E•lF�E•1F dF�F•1F iF•!F•1E dF iF iF�3F iF�F 9E 9F�E jF jE iF iE 9E iF�E�F�F jF�F•)F•1E jF iF�E�F*��F 9E�M 4 iE�*iE�t��$iF��E 9F�F•1E 3f-iF iF�E TL 0101 AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0, 022 0. 01.3 0. 022 PEAK AREA (ABS-SECONDS) 0. 01; 0. 001 0. 016 READ. 0# 2 ------------------- AA ZAA BC PEAK HEIGHT (ABSORBANCE) 0. 023 0. 013 0. 021 PEAK AREA (ABS-SECONDS) 0. 0121 -0. 0012 0. 014 READ- -0. 4 ----- ------- ---------------- ---------------------------------00002os ----- --- 1 QTT% T1CV - f1 d rnrC* VAD - GC] Q 9/ .Y.v..• - yyyy. _—yV�� 7! YL.LL.V.7 y� yy,�.. __ YYVy.TY y Y1d VLlY ♦ vP71yvI yJYJ♦Y JYJ /YPY yyY yYyy y T L 0 1 0 2 AA 2AA BG PEAK HEIGHT (ABSORBANCE) 0, 217 0. 114 0. 110 ' PEAK AP,F_A (ABS-SECONDS) 0. 133 0. 091 0. 092 READ: -- --- ---21 ♦ 4---------------------- -?`�- LS__�g------------ - ---- �U , ------ - - ' AA '47-AA BG PEAK HEIGHT (ABSORBANCE) 0.219 0. 110 0. 112 PEAK AREA (ARS-SECONDS) 0. 190 0. 097 0. 093 READ: 23. 0 MEAN= 22.2 STD. DEV. = 1 ..3 - COEF. VAR. =- 15.70 �------ ----- ------ AA SAA PC PEAK HEIGHT (ABSORBANCE) 0. 017 0. 015 0. 017 PEAK AREA (ABS-SECONDS) 0. 009 -0. 001 0, 009 READ: -0. 1' p_WCG3 -------------------------------------- y------- -------- ---- - -- ---- AA 7AA BG PEAK HEIGHT (ABSORBANCE) 0. 020 0. 015 0, 019 PEAK AREA (ABS-SECONDS) 0 . 010 0. 000 0. 010 READ: 0. 1 ---------------------- ---- ---- ------ - - --- MEAN= 0. 0 STD, DEV. = 0. 1 COEF.VAR. = 99.99 % TL 010 .4 AA ZAA BC 1 PEAK HEIGHT (ABSORBANCE) 0. 21 , 10E PEAK AREA (ABS-SECONDS) 0. 130 0. 093 0. 086 READ. 22, 0 - ---------------- ---- -------------------X09- -------------- 1 -------- --- AA 7AA �/ F;r: PEAK HEIGHT (ABSORBANCE) 0♦221 0. 118 0. 111 PEAK AREA (ARS-SECONDS) 0. 1160 0. 09? 0. 03' READ: 21 . 7 ----- ------------ ---- ---- -------- -------------------- -- 1 MEAN= 21 .16 STD. DEV. = COEF.VAR, = 0. 95 ------ -------- --- O00009 T L 0 1 0 5 AA ZAA EEC PEAK HEIGHT (ABSORBANCE) 01603 0.316 0.300 ' PEAK AREA (ABS-SECONDS) 0.379 0. 198 0, 131 READ: 53.5 --------- ----------------- k"1--------� 0--------------��6-/----------- PEAS. HEIGHT (ABSORBANCE) 0.60° `AA EEG 0, :91.3 0, 298 PEAK AREA (ABS-SECONDS) 0. 370 0. 195 0. 175 R52, 4 ----------- ----- ----------------------------------------------------------- MEAN= 52.9 STD. DEV. = 0.9 COEF.VAR. = 1 .67 ')i. T L 0 1 0 6 AA ZAA EEG ' PEAK HEIGHT (ABSORBANCE) 0. 013 0. 010 0. 006 PEAK AREA (APS-SECONDS) -0. 003 -0. 00.3 01000 READ: -0.5 AA ZAA BC PEAK HEIGHT (AEESORBANCE) 0. 011 0. 012 0. 009 PEAK AREA (ABS-SECONDS) 0, 004 0. 002 0. 002 READ: 0. 4 --------------------- ------------ -------------------------------------------- --- ' MEAN= 0. 0 STD. DEV, = 0.6 COEF.VAR. = 99.99 '%. T L O 1 O 7' AA ZAA PC PEAS: HEIGHT (ABSORBANCE-) 0 . 014 0, 012 0. 019 PEAK AREA (ABS-SECONDS) 0. 006 -0. 002 0. 003 READ: -0. 4 ----------------- --- -------------I_� �----=-io-------------------F �c�� --- --- AA LAA B_ PEAK HEIGHT (ABSORBANCE ) 0. 014 0. 012 0. 012 PEAK AREA (ABS-SECONDS) 01011 0. 006 0. 005 READ: 1 . 2 ---------------- ---- ------- ---- ------------------ ------------------------- --- MEAN= 0. 4 STD. DEV. = 1 . 1 COEF.VAR. = 99.99 % T L 0 1 0 Q AA ZAA FEC PEAK HEIGHT (ABSORBANCE) 0, 240 0. 134 01112 PEAK AREA (ABS-SECONDS) 0. 136 0. 09: 0. 039 READ----- ------------ -------- ---------- '-4------------------ ----- ------- �� ,r AA ZAA FEC: PEAK. HEIGHT (ABSORBANCE) 0. 232 0. 125 0. 114 PEAK AREA (ABS-SECONDS) 0113:9 0. 099 0. 034 READ: 23. 5 O O O 0 __ I 0 MEAN=---- -- s-.3------STD, DEV. =-------- -----------VAR-= 1 .27------------- ---- - -- T L 0117, AA ZAA PG PEAK HEIGHT (ABSORBANCE) 0, 57:3 0.298 0.280 PEAK AREA (APS-SECONDS) 0.360 0. 191 0. 189 ' READ: 51 .3 --------------------- --------- -- --------- __# ------- --- AA ZAA PC PEAK HEIGHT (ABSORBANCE) 0.567 0.287 0. 280 PEAS: AREA (ABS-SECONDS) 01369 0. 194 0. 175 ' READ------------------------------------- -------------------------------- ------- MEAN= 51 .8 STD. DEV. = 0.8 COEF. VAR. = 1 .5.1 T L 0 1 1 a AA ZAA PG PEAK HEIGHT (ADSOP..PANCE) 0. 010 0. 012 0. 010 PEAK. AREA (APS-SECONDS) -0. 003 -0. 001 -0. 001 READ. ---------0-�----- -------- ----------------6415 -------------------- ---- ------- AA If ZAA BG PEAK HEIGHT (ABSORBANCE) 0. 012 0. 014 0. 007 PEAK AREA (ABS-SECONDS) -0. 002 0. 000 -0 . 001 READ: 0. 0 -- -------- ------------ ---------------------------- ---- ------- MEAN= -0. 1 STD. DEV. = 0. 1 COEF. VAR. = 99.99 �. TL O 1 1 s AA ZAA BG PEAS: HEIGHT (ABSORE:ANCE) 0. 437 0. 233 0.208 PEAK AREA (APS-SECONDS) 0.351 0. 187 0. 163 READ: 49. 9 ------ ------- -------- ---- -- - ----------- - �-�=�=-l��-spy-------------- -- ------ AA ZAA BG PEAK HEIGHT (ABSORBANCE ) 0.44,7 0. 23:, 0. 214 PEAK AREA (ABS-SECONDS) 0. 361 0. 18;' READ: 50. 0 --------- ----------`- ------------------- ---- --- MEAN= 49. 9 STD EV. = 0. 1 COEF. VAR. = 0. 10 % T L 0 1 ^ 0 AA 7AA PC PEAK HEIGHT (ABSORBANCE) 0, 099 0. 014 0. 09E PEAK: AREA (APS-SECONDS) 0. 101. 0, 002 0 , 0919 --------- ----0----------- ------------ f S 7-Ov2----------------- --------- --- AAZAA P PEAK HEIGHT (ABSORBANCE) 0. 092 0'012 0, 080 PEAS: AREA (ABS-SECONDS) 0, 099 0. 001 0. 097 READ: 0 3 ' ----- -- - - -- - ------ -0 0 0 X-- --- ---- ----- ------- MEAN= 0. 4 STD-- ------- EV. - 0. 1 -- ---COEF. VAF,. =--31 .84 '�. - - 71 C4_)� ?'()-0 t0 Co..,.aim 0.i,;Pt .1 11 7 1 2 3 4 5 9—mG LAP- L� 4 - � tI j 5 1 6� I 6 7 6 5 70 c v o0 100 � 7 - � 13 P• 06 f� 14 o 1 15 �. . O0 15 1' W 5 100 I q.33 M 3s w 1 a5 4n zo 21 Mw pG w w o� 13 a5 p SPS woc� 13a� 72 23 25q CQV .� OA tol 31 'r 32 M 1 S W 312 -C W 13y1�. 13�t� 1 foo 3435 VD 03 ,? 36 E , 37 O � ! 39 / 13 Iq 13� �9-01 to �/ 40 239 000012 �s > 72 '0 Cnhimns Fn:h' � � r 3 4 (nI 5 p 6 7 S 9 VY1Q ^1 7 t0�n� u Z �1YI11 �e:. GI 1 � _ 3 ' - Kcjt , 5 I ✓ 1 O - �� 7 kil 5c IFS 9 2P.-()a 10 11 10 I <v a {{( .13 '511 'i 12 r k' 13 II�� . I J �O 14 �, �► 15 i 16 ( rl p Ip o 17i 0.4 f i, 13 1'0 O•-1 19 ' �.oa, -, .0 /a :1 0.0 10.1 X. Il Z. t 23 � p.0 I<o• C .5 2° 3C TO i 13 - 100 1100 O l po i s h 11 - CCSB � � I �o• � 1 � I� G 10 36 137 35 9 I1b o lot J9 y „ 000013.._. - 72 '3 13 14 is 16 17 18 19 L 20 II C II - T I I f1�51 I ' I1A 11� 1=inq ��a I�= vlu II �m>;II U rrm r n lI 1 1 2 2 131 b 5 loo to3�ia. 3 3 ..� 4 4 9.O 5 5 ! 1 <o• L 6 6 i i 7 Is 131b I oo I lIiwni I u�{,��p�1 �a�I)�I I iiI►' 0�JFI'bI`\DOl y ®1 IJI1'I1I I'Il�3��i V`3�11'�3�44�j��iI J1"'��b1bf��6��b�1u�_'yl.1 r 0 O1�1II1n') OII�ooIII O I 1 l111100 O II IIIIit'1Io—O II iI IIII!II <��L/�<�II IlI'I!{Oop`oC-�l<��,\�,q•O..•' 11s19111L0 1 Q �(v 191�01112121 3 vv CO. ;y 15 145 00 0, 16 16 17 17 1818 19 19 L, 3w 0loc JA1 Co o. 20 20 21 2 3 1 22 23 3 24 24 2 5 26 26 L 2 727 P8 28 29 2 9 30 3 3 1X 323' -3 3 3 3 40 33 35 - i� t� i; O I I I Co I 35 36 0� ig i M45 I 0 :100 ii36 MoI ,, <o. i 1 3, 37 to 1.0 I ' 38 134$5 a / 38 39 39 { 40 40 41 41 42 az , 00002, 14 a ' 7! 7 't �J -ecr S Exro 1 2 3 4 6 6 7 8 9 10 1 1 II I 1110 9. dna I _ WV- 1 I a is � 2 u �, 6I 3 61- 1' o( /� i s�00 r ' 3 7 �/� �- 8 O \O ioo 10 !O,a - 1l) 13 qq I 0 WCC i }— :2 IogAq ' I- I� �. 13 14 1 I ` 16 ►3�qq ' o.a .� 16 16 o. e �- �I aq " to j�o a 21 0 3 I <"a n �' 2532 � 314 I o 3s b 35 36 - �II , q 37 38 EPR 13 I 00 39 — so 42 ` 60 l 0000 , 15 1 Folder: LP Page 1 12:02: 13 13 Aug 1992 Protocol : LP Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- *** Standard: 1 Rep: 1 Seq: 683 122:02:13 13 Aug 1992 HG ' Hg .0000 PPR 5259 Ave. Int. = 5259 S. D. = 0 *** Standard: 2 Rep: 1 Seq: 684 12:04:33 13 Aug 1992 HG Hg .5000 PPB 10226 ' Ave. Int. = 10226 S. D. = 0 *** Standard: 3 Rep: 1 Seq: 685 12:06:53 13 Aug 1992 HG Hg 1. 000 PPB 18793 Ave. Int. = 18793 S. D. = 0 ' *** Standard: 4 Rep: 1 Seq: 686 12:09:17 13 Aug 1992 HG ' Hg 2. 000 PPP 395411 Ave. Int. = 39549 S. D. = 0 *** Standard: 5 Rep: 1 Seq: 687 12: 11 :42 13 Aug 1992 HG ' Hg 5. 000 PPB 89287 Ave. Int. = 89287 S. D. = 0 ** Standard: 6 Rep: 1 Seq: 688 12:14:17 13 Aug 1992 HG Hg 10. 00 PPB 187210— Ave. Int. = 187210 S. D. = 0 0000216 Protocol: LB Rey: ME Tim: 12:14:47 13 Aug 1992 Folder: LB Seq: 689 Print: On User: Batch: Id: Std6Rep1 Cup: Gas: 8.25 LPN State: Idle XAit: Off Autosamler: On CALIBRATION: Line Calibration ine: Ng Accepted Conc. Calc. Dev. LiNear 1 .BBQ .1881 .1881 Quadratic .5898 .4588 -.8412 MtdLinear 1.888 .9257 -.8743 C ' 4 2.808 2.857 .851 Accept o / SS SAO 4.767 -2328 n / 18.00 10.18 .1835 StdAdd c / .8888 r .999243 5.44946e-5 C -9.846W)e-2 Mean i.RSD Relative Ahsorhance ' 1 5259 8 5259 18226 8 10226 18793 8 18793 4 39.549 8 39549 35 89287 8 89287 ' 1 187218 0 187218 New cal coefficients stored 000021 Folder: LB Page 2 12:17:14 13 Aug 1992 Protocol : LB Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- *** Sample ID: ICV Seq: 689 12:17:14 13 Aug 1992 HG ' Hg 6.328 PPB .0000 6. 328 *** Sample ID: ICP Seq: 690 12:20:00 13 Aug 1992 HG Hg —. 1386 PPP .0000 —. 1386 ' *** Sample ID: CCV Seq: 691 12:22:16 13 Aug 1992 HG Hg 4.965 PPB .0000 4.965 ' *** Sample ID: CCR Seq: 692 12:24:49 13 Aug 1992 HG ' Hg —.0705 PRP . 0000 —. 0705 - *** Sample ID: PB Seq. 693 12:27:05 13 Aug 1992 HG Hg —.0356 PPB .0000 —. 0356 *** Sample ID: LCS Seq: 694 12:29:21 13 Aug 1992 HG ' #212 6* Hg 5. 827 PPB .0000 5. 827 ' *** Sample ID: 13459-07 Seq: 695 12:32:18 13 Aug 1992 HG SPK Hg .7583 PPB, .0000 . 7583 *** Sample ID: CCV Seq: 696 12:34:43 13 Aug 1992 HG Hg 4.792 PPB .0000 4. 792 *** Sample ID: CCR Seq: 697 12:37:22 13 Aug 1992 HG ' Hg —. 1454 PPB .0000 —. 1454 *** Sample ID: 13459—05 Seq: 698 12:39:36 13 Aug 1992 HG Hg . 1305 PPB .0000 . 1305 *** Sample ID: 13459-06 Seq: 699 12:41 :50 13 Aug 1992 HG ' DUP Hg .0210 PPB .0000 .0210 *** Sample ID: 13459-07 Seq: 700 12:44:03 13 Aug 1992 HG ' SPK Hg .9387 PPB .0000 .9387 00001.8 1 Folder: LR Fuge 3 12:46:221 13 Aug 1992 Protocol: LR Line Cone. Units SD/RSD 1 2 3 4 5 1 -------------------------------------------------------------------------------- * Sample ID: 13476-01 Seq: 701 12:46:21 13 Aug 1992 HG 7/29 WCC Hg . 1500 PPR .0000 . 1500 ' *** Sample ID: 13476-02 Seq: 702 12:48:34 13 Aug 1992 HG Hg -. 0688 PPR .0000 -.0688 *** Sample ID: 13476-03 Seq: 703 12:50:47 13 Aug 1992 HG Hg -.0625 PPR .0000 -.0625 ' *** Sample ID: 13476-04 Seq: 704 12:53:00 13 Aug 1992 HG ' Hg -. 1623 PPP . 0000 -. 1623 *** Sample ID: 13476-05 Seq: 705 12:55:13 13 Aug 1992 HG ' Hg -. 0668 PPP .0000 -.0668 *** Sample ID: 13476-05D Seq: 706 12:57:26 13 Aug 1992 HG ' Hg -. 0109 PPR .0000 -.0109 *** Sample ID: 13476-05S Seq: 707 12:59:39 13 Aug 19922 HG Hg 1.251 PPP .0000 1.251 ' *** Sample ID: CCV Seq: 708 13:01 :57 13 Aug 1992 HG Hg 4.709 PPP . 0000 4.709 *** Sample ID: CCP Seq: 709 13:04:28 13 Aug 1992 HG ' Hg -. 1372 PPR . 0000 -. 1372 *** Sample ID: 13476-01 Seq: 710 13:06.. 42 13 Aug 1992 HG DISS Hg -.0433 PPB .0000 -. 0433 *** Sample ID: 13476-02 Seq: 711 13:08:56 13 Aug 1992 HG ' Hg -.0917 PRP .0000 -.0917 *** Sample ID: 13476-03 Seq: 712 13: 11: 11 13 Aug 1992 HG ' Hg -. 1770 RPB .0000 -. 1770 OOOO1: i Folder,: LB Page 4 13:13:25 13 Aug 1992 protocol : LB ' Line Conc. Units SD/RSD 1 2 ------------------------------------------------------------4 ' ------------------- *** Sample ID: 13476-04 Seq: 713 13: 13:25 13 Aug 1992 HG ' Hg -.0578 PPR .0000 -.0578 ' *** Sample ID: LCS#212 Seq: 714 13:15:39 13 Aug 1992 HG Hg 6. 322 PPB .0000 6.322 ' *** Sample ID: PB Seq: 715 13: 18:15 13 Aug 1992 HG Hg -.0616 PPB .0000 -.0616 *** Sample ID: 716 13:20:29 13 Aug 1992 HG tHg .0018 PPP .0000 .0018 *** Sample ID: 13476-05D Seq: 717 13:26:15 13 Aug 1992 HG ' Hg -.0845 PPB . 0000 -. 0845 *** Sample ID: 13476-05S Seq: 718 13:28:30 13 Aug 1992 HG Hg .7643 PPB .0000 .7643 ' *** Sample ID: 13461-01 Seq: 719 13:30:49 13 Aug 1992 HG 7/29 NYSDEC Hg -.0678 PPR .0000 -. 0678 *** Sample ID: CCV Seq: 720 13:33:03 13 Aug 1992 HG Hg 4.955 PPB .0000 4. 955 ' *** Sample ID: CCR Seq: 721 13:35:33 13 Aug 1992 HG Hg -.0875 PPB .0000 -. 0875 *** Sample ID: 13461-02 Seq: 722 13:37:49 13 Aug 1992 HG DUP Hg . 1332 PPR .0000 . 1332 �y�► *** Sample ID: 13461-03 Seq: 723 13:40:04 13 Aug 1992 HG SPE'. �yg" .6595 pF'R .0000 . 6595 *** Sample ID: 13484-01 Seq: 724 13:42:19 13 Aug 1992 HG 7/30 D & R Hg -.0002 PPB .0000 -.0002 ' 121 (2 00001 ( 0 1 Folder: LP Page 5 13:44:35 13 Aug 1992 protocol: LP Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- *** Sample ID: 13484-01D Seq: 725 13:44:35 13 Aug 1992 HG Hg —. 0084 PPA .0000 —. 0084 ple ID: 13484—OIS Seq: 726 13:46:51 13 Aug 1998 HG g .3712 PF'P .0000 .3712 ' *** Sample ID: 13484-02 Seq: 727 13:49:08 13 Aug 1992 HG Hg .0022 RPB .0000 .002:3 *** Sample ID: CCV Seq: 728 13:51 :24 13 Aug 1992 HG Hg 4.718 PPP .0000 4. 718 *** Sample ID: CCP Seq: 729 13:53:56 13 Aug 1992 HG Hg —.0819 PPP .0000 —.0820 *** Sample ID: 13485-01 Seq: 730 13:56:12 13 Aug 1992 HG 7/30 TOWN Hg .0547 PPP .0000 .0547 *** Sample ID: 13485-01DSeq: 731 13:58:28 13 Aug 1992 HG — Hg —. 1075 PPP .0000 . 1075 *** Sample ID: 13485—OIS Seq: 732 14:00:44 13 Aug 1992 HG Hg 1.006 PPP .0000 1. 006 *** Sample ID: 13485-02 Seq: 733 14:03:02 13 Aug 1992 HG Hg —. 1352 PPP .0000 —. 1352 - *** Sample ID: —1 Seq. 734 14:05:16 13 Aug 199 HG Hg —. 1950 PPB .0000 —. 1950 *** Sample ID: 13461-03 Seq: 735 14:07:31 13 Aug 1992 HG 0 Hg 1.081 PPB .00000 1.081 �* Sample ID: 13484—OIS Seq: 736 14:09:51 13 Aug 1992 HG Hg 1.501 PPR .0000 1.501 0000 � � 1 I Folder: LB page 6 14:12: 12 13 Aug 1992 protocol : LB Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- *** Sample ID: 13484-01S Seq: 737 14: 12:12 13 Aug 1992 HG Hg .9016 PPB . 0000 . 9016 *** Sample ID: CCV Seq: 738 14:14:29 13 Aug 1992 HG Hg 4.781 PPB .0000 4. 781 *** Sample ID: CCP Seq: 739 14: 17:05 13 Aug 1992 HG Hg —. 1344 PPB .0000 —. 1344 *** Sample ID: 13499-01 Seq: 740 14:19:20 13 Aug 1992 HG 7/30 WCC Hg .2139 PPB .0000 . 2139 *** Sample ID: 13499-01D Seq: 741 14:21:35 13 Aug 1992 HG Hg . 1297 PPB . 0000 . 1297 *** Sample ID: 13499-01S Seq: 742 14:23:49 13 Aug 1992 HG 1 Hg 1. 159 PPB .0000 1. 159 *** Sample ID: 13499-02 Seq: 743 14:26:08 13 Aug 1992 HG Hg .8155 PPB .0000 .8155 *** Sample ID: 13499-03 Seq: 744 14:28:25 13 Aug 1992 HG Hg .7420 PPB . 0000 .7420 *** Sample ID: 13499-04 Seq: 745 14:30:42 13 Aug 1992 HG Hg .2652 PPB .0000 .2652 *** Sample ID: CCV Seq: 746 14:32:56 13 Aug 1992 HG Hg 4.759 PPB . 0000 4.759 *** Sample ID: CCR Seq: 747 14:35:26 13 Aug 1992 HG Hg —. 1569 PPR .0000 —. 1569 *** Sample ID: 13499-05 Seq: 748 14:37:40 13 Aug 1992 HG Hg . 1095 PPB .0000 . 1095 0000222 r r Folder: LP Page 1 08:21:21 13 Aug 1992 Protocol : LB ' Line Conc. Units SD/RSD 1 2 3 4 J ' ------------------------- -------:J-------------------- *** Standard: 1 Rep: 1 Seq: 603 08.1:21 13 Aug 1992 HG Hg .0000 PPR -1770 Ave. Int. = -1770 S. D. = 0 *** Standard: 2 Rep: 1 Seq: 604 08:23:41 13 Aug 1992 HG Hg . 5000 PPB 11715 Ave. Int. = 11715 S. D. = 0 *** Standard: 3 Rep: 1 Seq: 605 08:26:47 13 Aug 1992 HG Hg 1.000 PPB 23847- Ave. Int. = 23847 S. D. = 0 *** Standard: 4 Rep: 1 Seq: 606 08:29: 12 13 Aug 1992 HG Hg 2.000 PPB 52397 Ave. Int. = 52397 S. D. = 0 *** Standard: 5 Rep: 1 Seq: 607 08:31 :46 13 Aug 1992 HG Hg 5. 000 PPB 124462- Ave. Int. = 124462 S. D. = 0 *** Standard: 6 Rep: 1 Seq: 608 08:34:29 13 Aug 1992 HG Hg 10.00 PPB 251698 Ave. Int. = 251698 S. D. = 0 r r r r r 000022 ; 1 ' Protocol. LB Rey: 2.885 i ire: 08:34-41 13 Aug 1992 Folder: U Seq: 689 Print: On ' User: Batch: Id: Std6Rep1 Cup: Gas: 8.25 LPN State: Idle Xnit: Off Autosmter: On CALIBRA?ION: Line Calibration Line: H9 Accepted Cone. Calc. Dev. LiNear 1 .8888 -.8384 -.83$4 Quadratic .5888 .4956 -.8844 Minear 1.8M .9761 -.8248 C 4 2.8O 2.187 .1867 Accept o 5.888 4.961 -.8394 n 18.88 9.999 -.8885 StdAdd c .8888888 r .999898 3.96822e-5 C 3.16583e-2 +� Nun i.RSD Relative Ahsorhauce 1 -1778 8 -1778 11715 8 11715 23947 8 23847 4 52397 8 52397 124462 8 124462 SG 251698 8 251698 Hea cal coefficients stored r 000024211 t Folder: LR Page 2 08:38:35 13 Aug 1992 Protocol: LR Line Conc. Units SD/RSD 1 c^ 3 4 5 -------------------------------------------------------------------------------- *** Sample ID: ICV Seq: 609 08:38:35 13 Aug 1992 HG Hg 6.542 PPR .0000 6.542 *** Sample ID: ICP Seq: 610 08:41:21 13 Aug 1992 HG Hg . 0005 PPA .0000 . 0005 *** Sample ID: CCV Seq: 611 08:43:37 13 Aug 1992 HG Hg 4. 678 PPP .0000 4.678 *** Sample ID: CCR Seq: 612 08:46: 13 13 Aug 1992 HG Hg . 0136 PPA .0000 .0136 *** Sample ID: PR Seq: 613 08:48:29 13 Aug 1992 HG Hg .0674 PPR .0000 . 0674 *** Sample ID: LCS Seq: 614 08:50:45 13 Aug 1992 HG #212 6* ' Hg 6.246 PPR .0000 6. 246 *** Sample ID: PPW Seq: 615 08:53:27 13 Aug 1992 HG rHg .0195 PPP .0000 .0195 *** Sample ID: LCS#212 Seq: 616 08:55:43 13 Aug 1992 HG 6* DIL Hg 5.781 PPA .0000 5. 781 *** Sample ID: 13425-01 Seq: 617 08:58:23 13 Aug 1992 HG 7/24 TOWN Hg .3275 PPS .0000 . 3275 *** Sample ID: 13425-02 Seq: 618 09:00:39 13 Aug 1992 HG Hg . 4052 PPR .0000 . 405:2 *** Sample ID: 13425-03 Seq: 619 09:02:55 13 Aug 1992 HG Hg .6920 PPA .0000 . 6920 *** Sample ID: 13425-04 Seq: 620 09:05:12 13 Aug 1992 HG Hg . 1901 PPP .0000 . 1902 0000225 : t Folder: LR Rage 3 09:07:27 13 Aug 1992 Protocol: LR Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- 1 *** Sample ID: 13425-05 Seq: 621 09:07:27 13 Aug 1992 HG DUP ' Hg . 1882 PPR .0000 . 1883 *** Sample ID: 13425-06 Seq: 622 09:09:41 13 Aug 1992 HG SPK Hg 1.053 F'PR .0000 1. 053 *** Sample ID: CCV Seq: 623 09:12:05 13 Aug 1992 HG Hg 5. 004 PPB .0000 5. 004 *** Sample ID: CCP Seq: 624 09:14:42 13 Aug 1992 HG Hg -.0093 PPP .0000 -.0093 *** Sample ID: 13425-07 Seq: 625 09:16:56 13 Aug 1992 HG Hg .3892 PRP .0000 . 3892 *** Sample ID: 13425-08 Seq: 626 - 09:19: 10 13 Aug 1992 HG Hg .3623 PPP . 0000 . 3623 *** Sample ID: 13425-09 Seq: 627 09:21 :24 13 Aug 1992 HG Hg .2364 RPB .0000 .2364 *** Sample ID: 13245-10 Seq: 628 09:23:39 13 Aug 1992 HG Hg .2029 PPB . 0000 . 2029 *** Sample ID: 13412-01 Seq: 629 09:25:53 13 Aug 1992 HG 7/23 TOWN Hg . 1686 RPB . 0000 . 1686 *** Sample ID: 13412-02 Seq: 630 09:28: 10 13 Aug 1992 HG Hg . 1874 PPB .0000 . 1874 *** Sample ID: 13412-03 Seq: 631 09:30:26 13 Aug 1992 HG Hg .2464 PGP . 0000 .2464 ^� *** Sample ID: 13412-04 Seq: 632 09:32:,x8 la Aug 1992 HG NHg . 3435 PPP .0000 . 3435 f1 r 0 0 0 0 L L G , Folder: LR Page 4 09:34:51 13 Aug 1992 Protocol: LB Line Conc. Units SD/RSD 1 2 3 4 5 -------------------------------------------------------------------------------- * Sample ID: 13419-01 Seq: 633 09:34:51 13 Aug 1992 HG 7/24 D & B Hg .3108 PPB .0000 ..3108 *** Sample ID: 13419-01D Seq: 634 09:37:07 13 Aug 1992 HG Hg . 1609 PPB .0000 . 1609 *** Sample ID: CCV Seq: 635 09:39:20 13 Aug 1992 HG Hg 4.704 PPB .0000 4.704 *** Sample ID: CCR Seq: 636 09:41 :54 13 Aug 1992 HG Hg .0911 PPB .0000 .0911 *** Sample ID: 13419-01S Seq: 637 09:44:07 13 Aug 1992 HG Hg .8683 PPB .0000 . 8683 r *** Sample ID: 13419-02 Seq: 638 09:46:22 13 Aug 1992 HG Hg .2368 PPB . 0000 . 2368 *** Sample ID: 13438-01 Seq: 639 09:48:36 13 Aug 1992 HG 7/27 D & B Hg . 2790 PPB .0000 . 2790 *** Sample ID: 13438-02 Seq: 640 09:50:50 13 Aug 1992 HG ' DUP Hg .2385 PPB .0000 . 2385 *** Sample ID: 13438-03 Seq: 641 09:53:09 13 Aug 1992 HG SPK Hg .8197 PPB .0000 . 8197 *** Sample ID: 13438-04 Seq: 642 09:55:27 13 Aug 1992 HG Hg . 1024 PPB .0000 . 10:4 *** Sample ID: 13438-05 Seq: 643 09:57:44 13 Aug 1992 HG Hg .0889 PPP .0000 .0889 *** Sample ID: 13450-01 Seq: 644 10:00:00 13 Aug 1992 HG 7/28 WCC Hg . 1658 PPB .0000 . 1658 0000Lc7 DRfE OF ANALYSIS: (1.'> ANA T: �y NYTEST LOG BOOK M n , LYS � � ETHOD NO.: ANALYTE: jluc (EPA/STD METHOD) AL.Gs le- Date eDate Client ID Log No. ,(1 �- -� zq, e a/o R Recd (Sample ID) u' �� , %RPD Nyte Environmental, I NaMf Ot Maim t a Meth d # ;51332A Sour e of Stock tandard: 1cloo ' Correlption Valu c. /-3 ��L., .sem. 9 0,B I TCS,' DATE OF ANALYSIS: "10,7 1,�.li ANALYST: �t"� NYTEST LOG BOOK METHOD NO.: . a � n — ANALYTE: e y—a at'dx- ALL . (EPA/STD METHOD) Date Client IDlog No. U -LL Lt= %R Recd (Sample ID) V �� C L. �' �!G C�'v %RPD J Aj M 0,,-- /—c -- ,tee L1.' I /V w a,G' Ue-t�' 10, �c. l >f ' Njw - .2S � � Lv' 0 002 DATE OF ANALYSIS: �-flof* NYTEST LOG BOOK s' ANALYST: �� METHOD NO.: ANALYTE: (EPA/STD METHOD) -� Date Client ID L No. /�� /o R Recd (Sample ID) /.�J �-% , 1G /e %RPD LAP,13:n 09. dd 1p 12; by 3'�. 9 �, ✓�� t � cam. � �'Ii/ •;' •` � O; Q �U r t C7 2� /71EI-P ,B L k - 0/0 /► �o, o l.L. oo n inn J i DATE OF ANALYSIS: Pfloj— 9„aj r ANALYST: c NYTEST LOG BOOK cn-u- Q� METHOD NO.: ANALYTE: (/!},' (EPA/STD METHOD) f ✓��f�L L,v�✓G�. 2 Date Client ID Log No. re %R Reed (Sample ID) _ ,.{L ' %RPD y l •fit lam'-(1' 0. / �� .3.�. / G: �:9.� ,y.�� ' I 1'et- . a y . y r 9:", J D, D PB�zriT o, c � �c�U j o�C�v 6ow �,� %G�✓= ;113 (.= t - /_h,-G� D, G A LI S - 67009Xe "Z 1 0 -JI sty- I C Y 1 DATE OF ANALYSIS: NYTEST LOG BOOK ANALYST: ��. METHOD NO.: � --� ' ANALYTE: LLL �9�%t• (EPAISTD METHOD) Date Client ID Log No. � %R Rec'd (Sample ID) /.6'' 1�, At �- , /OR P D 67 i Z�L t. I �2 SG%' D ,INV 111.3 /,-'o -57 �y 491 [?j10 cu °!TE OF ANA SIS.• D �' D:' s �� s�� NYTEST LOG BOOK ' ANALYST: METHOD NO.: 1j j 2, At ANALYTE: LI, rL.z L�'`G;�L (EPA/STD METHOD) At GL � Date Client ID Log No. RPD L' Lt J Q �C� / Rec'd (Sample ID) %,;� ��p Dr egg, v/ .4,1, -'J - errg r i I a �'C-� �^ :�/r r 1. �•'� '-" G;;'..� " f • I I � I � � � t� � { li 71 I �T - + 1 � i II it ; j I 1 1 hill It i 17 II III � I i � i I�• I iI I I - -I - -- I-1 I , T� I I -�-•-¢- - - ! I I I i I � ( , I , I � rri; I I %ilri�r I i ; I I I � j � • I I I 1 I j I I i I � �----, - i I I i I I I •'' G1�3' I i j� I � I S I I j I , I � I I I ' i l I I ! ( I I ( i l l I ! I ' I i •, I ��,�� _ I 1q1 i �, ; i r I I I wil J_ - !-- - - - _ - I --- - -I I ,41 I i i Q•LZ „ I, I, ' I I . 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