HomeMy WebLinkAbout2015 1st Qtr
FIRST QUARTER 2015
GROUND WATER-MONITORING REPORT
FOR THE
TOWN OF SOUTHOLD LANDFILL
6155 COX LANE
CUTCHOGUE, NY 11944
Prepared for:
Southold Town Solid Waste Management District
6155 Cox Lane
Cutchogue, NY 11944
Prepared by:
Lockwood, Kessler & Bartlett, Inc.
1 Aerial Way
Syosset, NY 11791
Submitted to:
New York State Department of Environmental Conservation
Region 1 Headquarters
SUNY at Stony Brook
50 Circle Road
Stony Brook, NY 11790
April 20, 2015
First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchoque, NY
TABLE OF CONTENTS
Section Number and Title Page Number
1.0 INTRODUCTION 1
2.0 METHODS AND PROCEDURES 1
3.0 DISCUSSION OF RESULTS 2
3.1 Water-Level Results 2
3.2 Field Parameter Results
3
3.3 Leachate Indicator Results 4
3.4 Inorganic Parameter Results 5
4.0 CONCLUSIONS AND RECOMMENDATIONS 7
Figure Number and Title Follows Page Number
1. Site Location Map 1
2. Well Location Map 1
Table Number and Title Follows Page Number
1. Summary of Part 360 Routine Parameter Results for 2
First Quarter 2015 Monitoring Round
Appendices
A. Sample Results
Lockwood, Kessler & Bartlett, Inc.
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First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
1.0 INTRODUCTION
The Town of Southold has retained Lockwood, Kessler & Bartlett, Inc. (LKB) to perform
post-closure ground-water monitoring and reporting for its closed and capped MSW
landfill in Cutchogue, NY (Site). The location of the Site is shown in Figure 1.
th
This report is for the first quarter 2015 monitoring round, conducted on March 25, and
describes the work performed and the results obtained. Section 2.0 (Methods and
Procedures) details the project requirements and the specific work performed. Section
3.0 (Discussion of Results) summarizes the key findings from this monitoring round,
including comparison of the laboratory results to standards and guidance values.
Section 4.0 (Conclusions and Recommendations) provides conclusions based on this
quarters results, and recommendations for upcoming quarters. Each report section is
supported by figures and/or tables, as appropriate, which follow the page on which they
are first referenced. The laboratory results for this monitoring round are provided in
Appendix A.
2.0 METHODS AND PROCEDURES
Water-level measurements and ground-water samples were collected from each of the
Sites 12 monitoring wells, as listed below. A site plan showing the locations of the wells
is provided in Figure 2.
MW-1S MW-5S
MW-1D MW-5D
MW-3S MW-6S
MW-3D MW-6D
MW-4S MW-8S
MW-4D MW-8D
Prior to sampling, the water-level in each well was measured to the nearest 0.01-feet
from the top of the well casing utilizing a decontaminated water-level meter. Ground-
water samples were collected utilizing a Grundfos RediFlo2 variable-speed electric
submersible pump connected to 160 feet of ¾-inch diameter polyethylene hose on a
Keck Reel. Utilizing the well construction records, the pump was placed at the mid-point
of each wells screen. Each well was then purged at a low flow rate until the water was
observed to be clear and the field water chemistry parameters were stable. Turbidity
was not measured this quarter because the field turbidity meter malfunctioned. This is
not a significant data gap because the ground-water samples at this Site typically exhibit
turbidities of less than 5 Nephelometric Turbidity Units.
Lockwood, Kessler & Bartlett, Inc.
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N
SITE
FIGURE 1
SITE LOCATION MAP
TOWN OF SOUTHOLD LANDFILL, CUTCHOGUE, NY
FIGURE 2 WELL LOCATION PLAN
ANDFILL, CUTCHOGUE, NY
TOWN OF SOUTHOLD L
: Base map provided by Town of Southold
Note
First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
The ground-water samples were collected directly from the pump discharge hose into
new laboratory-supplied bottles of the type required for each specific analysis. A blind
duplicate was collected from Well MW-6S and labeled MW-7S. Matrix spike and matrix
spike duplicate samples were collected from Well MW-8S. Field notes were recorded in
a bound field notebook.
Each sample was labeled with the well number, time and date, etc., placed in a cooler
o
with ice to keep it at 4C, and shipped to the laboratory the same day. The samples
were analyzed for the 6NYCRR Part 360 Routine leachate indicator and inorganic
Parameters. The field parameters were monitored by LKB. Laboratory analyses were
performed by Spectrum Analytical, Inc. in North Kingston, RI. This laboratory is certified
by the New York State Department of Healths Environmental Laboratory Approval
Program in all required analytical categories, and employs the required internal QA/QC
procedures, including analysis of matrix spikes, matrix spike duplicates, method blanks
and continuing calibration samples. They also participate in the required biennial
proficiency testing. The field data and laboratory results were reviewed by LKB per
QA/QC Plan requirements and determined to be useable. Four of the glass bottles
containing samples for phenols analysis were broken during transport, so phenols
results are not available for these wells. This is not a significant data gap because
phenols typically are not detected at significant concentrations in ground water at this
Site, and the Class GA standard for phenols is aesthetics-based, not health-based.
3.0 DISCUSSION OF RESULTS
The field and laboratory results for the first quarter 2015 ground water-monitoring round
are summarized and compared to the New York State Department of Environmental
Conservation Ambient Water Quality Standards and Guidance Values for Class GA
(Potable) ground water, as applicable, in Table 1. A review of the results for the water-
level measurements and each analytical parameter group is provided below.
3.1 Water-Level Results
As shown in Table 1, water-table elevations in the shallow (S) wells at the Site ranged
from 6.85 feet above mean sea level (MSL) in Well MW-1S, located on the south end of
the Site, to 4.60 feet above MSL in Well MW-8S, located on the west side of the Site.
These water-table elevations are consistent with ground-water flow information
published by the United States Geological Survey in Scientific Investigations Map 3066,
Water Table Sheet 1 of 4, which indicates a relatively low horizontal hydraulic gradient
and a northerly horizontal ground water-flow direction. Based on these elevations, Well
Cluster MW-1 is located upgradient of the Site, and the other wells are located along the
downgradient boundary of the Site. Potentiometric surface elevations in the deep (D)
wells at the Site are consistent with the shallow well results, except for the anomalously
high result for Well MW-8D, and indicate flat or downward vertical hydraulic gradients.
Lockwood, Kessler & Bartlett, Inc.
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No OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo OdorNo Odor
MW-8DCalciumug/LNo Standard6,20031,00028,00036,00081,000160,00011,00072,00017,00037,00050,00059,000 39,00012,000 7,00033,0005,80020,00020,00030,000Potassiumug/LNo Standard4,1001,60018,00067,00042,000
41,0003,900110,0004,7003,10052,00050,000 30,00066,000
MW-4DMW-8D
Field ObservationsN/ANo StandardClear,Clear,Clear,Clear,Clear,Clear,Clear,Clear,Clear,Clear,Clear,Clear,
N/A44.8344.8849.5049.1963.0362.9268.1467.6455.7755.7154.1655.29N/A37.9837.9043.8243.5357.8457.7663.0162.5849.9449.9049.5648.42 ConductivitymS/cmNo Standard0.1450.3790.6101.4000.7202.2200.1931.9900.18
70.4331.2901.050 11,0003,4009806201,500
Floaters or SinkersN/ANoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNoneNone
ORPmVNo Standard14.1-55.3-60.4-54.813734.126360.783.453.7-108-78.4
Total Organic Carbonmg/LNo Standard<10<105.0 J114.9 J132.0 J185.8 J<108.7 J5.9 J
18.315.5<0.131.8<0.131.68.9<0.130.15
N/A6.856.985.685.665.195.165.135.065.835.814.606.87 TemperatureoCNo Standard13.512.715.815.515.014.813.914.312.612.615.514.76.62 Dissolved Oxygenmg/LNo Standard8.134.121.402.731.981.364.401.341.432.9
21.051.280.071 J1.80.04 J0.12 J0.250.58CODmg/LNo Standard<20<202855<2051<206117 J<203818 JTKNmg/LNo Standard0.2100.2108.7558.50.56015.90.28069.70.5600.02121.317.6
Alkalinity mg/LNo Standard<20312203901305802568050<20270280 536
Hardnessmg/LNo Standard391401402002806905632067180210270
EhpHmVNo Standard1089.616.411.624.8-3.488.22.876.757.319.75.6BODmg/LNo Standard<3.0<3.05.0<3.0<3.0<3.0<3.0<3.0<3.0<3.0<3.0<3.0Cadmiumug/L5<5.0<5.03.0 J1.0 J<5.0<5.0<5.0<5.0<5.0<5.01.4
J<5.0
TurbidityNTU<5NMNMNMNMNMNMNMNMNMNMNMNM
2217013354382Sulfatemg/L250218337394690163913934382Leadug/L25<10<10<10<10<10<10<10<10<10<10<10<10
Phenolsug/L1<<8<<8<8<8<8<<<8<8<8
MW-8SMW-5DMW-6SMW-6DMW-8S
ORP= Oxygen Reduction Potential.pHmV= pH in milliVolts.N/A= Not Applicable. exceed Class GA Standard or Guidance Value.
5.315.676.41
137253370
= Degrees Celsius.ug/L= micrograms per Liter.Results in bold font and highlighted in yellow
9,10018,000
MW-6D
0.14 J0.210
<200130 J21048 J
MW-6S
T.O.C.= Top of Casing.COD= Chemical Oxygen Demand.mV= milliVolts.NM= Not Measured.
Summary of Part 360 Routine Parameter Results for First Quarter 2015 Monitoring Round
140,000
MW-5SMW-5D
6.67 67.8
833
Well Number and Result
MW-5S14,000
0.14 J
5.11
110160
MSL= Mean Sea Level.TKN= Total Kjeldahl Nitrogen.mg/L= milligrams per Liter.
Town of Southold Landfill, Cutchogue, NY
220,000
67,000
MW-4D
BOD= Biological Oxygen Demand.NTU= Nephelometric Turbidity Units.GV = Guidance Value.
1,2605,7002,7003,7003,100
6.79 14.8
260660
2.4
0.033 J0.099 J0.250.580.065 J
MW-4S4,40015,00018,00027,00018,00014,000
MW-1SMW-1DMW-3SMW-3DMW-4S
0.14 J
6.27
457<200
24
Chloridemg/L25013246410021
Table 1
21,00047,000100,000
MW-1SMW-1DMW-3SMW-3D
90,00034,000
8.1951.8
6.51Nitratemg/L103.25.3<0.13<0.13
535
6.43
Total Dissolved Solidsmg/L50097232345
6.55Ironug/L300<20063 J
Ammoniamg/L20.21<0.2
Manganeseug/L30011 J<50
C
o
Sodiumug/L20,00011,000
4.74
mS/cm= milliSiemens per centimeter.
NYSDEC Part 360Class GA
Routine ParametersStandard
GV
pHUnits6.5-8.5
35000
GV
2
Feet MSLFeet MSL
Feet
Units
Bromidemg/L
Magnesiumug/L
:
Notes
Inorganic Parameters:
Water-Level Elevation
Leachate Indicators:
:
Field Parameters:
Water-Level Data
T.O.C. Elevation
Depth to Water
First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
3.2 Field Parameter Results
Review of the field parameter results in Table 1 indicates the following key findings:
Ground-water conductivity values are higher relative to the main area of Long
Island. This may be at least partly due to the Sites North Fork location, where
naturally higher ground-water salinities may occur due to the proximity to saline
surface-water bodies. Conductivity values are highest in the deep wells located
directly downgradient of the Site (e.g., Wells MW-3D, MW-4D and MW-5D).
These highest values appear to be Site-related. There is no Class GA standard
or guidance value for conductivity.
Ground-water temperatures are approximately 1 to 2 degrees Celsius higher in
seven of the 10 downgradient wells relative to the upgradient wells. The highest
temperatures occurred in Well Clusters MW-3, MW-4 and Well MW-8. There is
no Class GA standard or guidance value for temperature.
No floaters or sinkers were noted during this monitoring round.
Ground-water pH is acidic, and is lower than the minimum Class GA standard of
6.5 Standard Units in one upgradient well and six of the 10 downgradient wells.
The results are consistent with the naturally low pH of Long Island ground water.
Ground-water pH is higher in the deep well at all six of the Sites well clusters.
Eh is noticeably lower in three of the five shallow downgradient wells relative to
the shallow upgradient well, and is lower in the deep well at all six Site well
clusters. There is no Class GA standard or guidance value for Eh.
DO (Dissolved Oxygen) concentrations are lower in nine of the 10 downgradient
wells relative to the upgradient wells, but dissolved oxygen is present in all 12
Site monitoring wells. There is no Class GA standard or guidance value for DO.
The ground water in all 12 Site monitoring wells was observed to be clear, and
did not have noticeable odor.
The ORP (Oxidation-Reduction Potential) of ground water is positive in the
shallow upgradient well, and in Well Clusters MW-4, MW-5 and MW-6; and
negative in Well Clusters MW-3 and MW-8 this quarter. There is no Class GA
standard or guidance value for ORP.
Overall, the field parameter results obtained this quarter are consistent with the Sites
usage and its North Fork setting. Potential Site-related impacts are relatively minor in
magnitude and limited to higher conductivity and temperature, and lower Eh, DO and
ORP in certain downgradient wells.
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First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
3.3 Leachate Parameter Results
Review of the leachate parameter results in Table 1 indicates the following key findings:
Ground-water alkalinity is significantly higher in seven of the 10 downgradient
wells relative to the upgradient wells. The highest alkalinity concentrations were
detected in Wells MW-3D, MW-4D, MW-5D and MW-8D. There is no Class GA
ground-water standard or guidance value for alkalinity.
Ammonia was detected in the shallow upgradient well and in all 10 downgradient
monitoring wells. Ammonia concentrations are low in Upgradient Well MW-1S
and Downgradient Wells MW-4S, MW-5S, MW-6S and MW-6D. Ammonia
concentrations in the other six downgradient wells exceed the 2-mg/L Class GA
ground-water standard. The highest ammonia concentrations occurred in Wells
MW-3D and MW-5D.
BOD (Biological Oxygen Demand) was only detected in one well (Well MW-3S),
at a low concentration this quarter. There is no Class GA ground-water standard
or guidance value for BOD.
Bromide was detected in all 12 Site monitoring wells, primarily at low, estimated
concentrations. Bromide concentrations in Well Clusters MW-3 and MW-8, and
Wells MW-4D and MW-5D, are higher relative to the upgradient wells. The
highest bromide concentration occurred in Well MW-4D, and is slightly higher
than the 2-mg/L Class GA ground-water guidance value.
Chloride levels are noticeably higher in five of the 10 downgradient wells (Wells
MW-3S, MW-3D, MW-4D, MW-5D and MW-8D) relative to the upgradient wells,
but with the exception of Well MW-4D are lower higher than the 250-mg/L Class
GA ground-water standard. The highest chloride concentrations occur in deep
wells, which suggests that they may be due in part to naturally saline ground-
water conditions.
COD (Chemical Oxygen Demand) was detected in seven of the 10 downgradient
wells. The highest COD concentrations were detected in Wells MW-3D, MW-4D
and MW-5D. There is no Class GA ground-water standard or guidance value for
COD.
Ground-water hardness values are higher in seven of the 10 downgradient wells
relative to the upgradient wells. Hardness was higher in the deep well at each of
the six Site well clusters, suggesting that it may be partly associated with saline
ground-water conditions. The highest hardness values occurred in Wells MW-4D,
MW-5D and MW-8D. There is no Class GA ground-water standard for guidance
value or hardness.
Nitrate is present in both upgradient wells and five of the 10 downgradient wells
this quarter. Concentrations are lower than the 10-ug/L Class GA ground-water
standard in every well except Well MW-4S.
Phenols were not detected in the eight wells for which results are available.
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First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
Sulfate is present in all 12 Site monitoring wells, at relatively similar
concentrations in the upgradient and downgradient wells. All concentrations are
lower than the 250-ug/L Class GA ground-water standard. Sulfate concentrations
are higher in the deep well at all six Site well clusters, which suggests that they
may be partly associated with saline ground-water conditions.
TDS (total dissolved solids) results are noticeably higher in eight of the 10
downgradient wells relative to the upgradient wells, and exceed the 500-mg/L
Federal MCL in Wells MW-3D, MW-4D, MW-5D and MW-8D. The highest TDS
concentration at each well cluster occurs in the deep well, which suggests that
they may be partly associated with naturally saline ground-water conditions.
TKN (total Kjeldahl nitrogen) is present in all 12 Site wells this quarter. TKN
concentrations in six of the 10 downgradient wells are significantly higher relative
to the upgradient wells. The highest TKN concentrations occurred in Wells MW-
3D, MW-4D and MW-5D. There is no Class GA ground-water standard or
guidance value for TKN.
TOC (total organic carbon) was present in nine of the 10 downgradient wells. The
highest concentrations occurred in Wells MW-3D, MW-4D and MW-5D. There is
no Class GA ground-water standard or guidance value for TOC.
Overall, the leachate parameter results obtained this quarter are also consistent with the
Sites usage and its North Fork setting. Potential Site-related impacts indicated by these
results include downgradient increases in most of the detected parameters, primarily in
the deep wells. However, it is important to note that 1) the there are no Class GA
ground-water standards or guidance values for six of the parameters; and 2) the
downgradient increases occur in a limited number of wells.
Moreover, ground water beneath the Site is naturally saline at depth, and ultimately
discharges to a saline surface-water body (Long Island Sound). Therefore, the
exceedances for ammonia, bromide, chloride, nitrate and TDS, which occur naturally in
saline ground water and seawater, are not a significant concern with respect to public
health or the environment.
3.4 Inorganic Parameter Results
Review of the inorganic parameter results in Table 1 indicates the following key
findings:
Cadmium was detected at low, estimated concentrations in three of the 10
downgradient monitoring wells this quarter, but all concentrations are much lower
than the Class GA ground-water standard for cadmium.
Calcium was detected in all 12 Site monitoring wells this quarter. Calcium
concentrations are noticeable higher in five of the 10 downgradient wells (Wells
MW-4S, MW-4D, MW-5D, MW-8S and MW-8D) relative to the upgradient wells.
There is no Class GA ground-water standard or guidance value for calcium.
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First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
Iron was detected in one background well and eight of the 10 downgradient wells
this quarter. The iron concentrations in Wells MW-3S, MW-3D, MW-4D and Well
Cluster MW-8 exceed the 300-ug/L Class GA ground-water standard. The
highest iron concentrations occurred in Wells MW-3S and MW-8S. The fact that
these highest iron concentrations occurred in the shallow wells at these clusters
suggests that they are Site-related.
Lead was not detected in any of the Site monitoring wells this quarter.
Magnesium was detected in all 12 Site monitoring wells this quarter, and the
concentrations in six of the 10 downgradient wells are noticeably higher relative
to the upgradient wells. The magnesium concentration in Well MW-4D is higher
than the 35,000-ug/L Class GA guidance value. At each well cluster, magnesium
concentrations are higher in the deep well, which suggests that they may be
partly associated with saline ground-water conditions.
Manganese was detected in one upgradient well at a low, estimated
concentration, and in all 10 downgradient wells. The manganese concentrations
in nine of the 10 downgradient wells exceed the 300-ug/L Class GA ground-water
standard. The highest manganese concentrations occurred in Wells MW-3S and
MW-5D. Most of the higher manganese concentrations in the downgradient wells
occurred in the shallow wells and therefore appear to be Site-related.
Potassium was detected in all 12 Site monitoring wells this quarter. Potassium
concentrations in seven of the 10 downgradient wells are noticeably higher
relative to the upgradient wells, and appear to be Site-related. The highest
potassium concentration occurred in Wells MW-3D and MW-5D. There is no
Class GA ground-water standard or guidance value for potassium.
Sodium was also detected in all 12 Site monitoring wells. Sodium concentrations
in six downgradient wells (Wells MW-3S, MW-3D, MW-4D, MW-5D, MW-8S and
MW-8D) are noticeably higher relative to the upgradient wells, and exceed the
20,000-ug/L Class GA ground-water standard. The sodium concentration in Well
MW-1D also slightly exceeded this standard. At each well cluster, the highest
sodium concentration occurs in the deep well, which suggests that the sodium
results are partly associated with naturally saline ground-water conditions.
Overall, the inorganic parameter results obtained this quarter are also consistent with
the Sites usage and its North Fork setting. Potential Site-related impacts indicated by
these results include downgradient increases in calcium, iron, magnesium, manganese,
potassium and sodium.
However, it is important to note that 1) many of these increases are relatively minor in
magnitude, sporadic, and/or do not result in exceedances of the Class GA ground-water
standards or guidance values; 2) there are no Class GA ground-water standards or
guidance values for calcium or potassium; 3) the Class GA ground-water standards for
iron and manganese are aesthetics-based; 4) the limit for magnesium is based on a
guidance value rather than an actual standard; and 5) sodium is not considered to be
particularly hazardous.
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First Quarter 2015 Ground Water-Monitoring Report
Town of Southold Landfill, Cutchogue, NY
Moreover, since ground water on the North Fork is naturally saline at depth and
ultimately discharges to Long Island Sound, the exceedances for magnesium and
sodium, which occur naturally in saline ground water and seawater, are not a concern
with respect to public health or the environment.
4.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the results of the first quarter 2015 monitoring round, LKB concludes the
following:
Water-level elevations, horizontal and vertical hydraulic gradients, and ground
water-flow directions are consistent with local/regional hydrogeologic conditions.
In general, ground water-quality conditions are consistent with the Sites North
Fork setting near saline surface-water bodies.
Comparison of upgradient and downgradient results indicates potential Site-
related impacts consistent with an old MSW landfill, however further assessment
indicates that the impacts are not a significant concern with respect to public
health or the environment.
The current annual monitoring schedule for the Site requires monitoring ground water
for 6NYCRR Part 360 routine parameters during three calendar quarters and for Part
360 baseline parameters during one calendar quarter, in rotating quarters. The last
baseline monitoring round was performed during the second quarter of 2014. Therefore,
the next baseline monitoring round is not due until the third quarter of 2015. The second
quarter 2015 monitoring round should be for Part 360 routine parameters.
The Town of Southold has petitioned the NYSDEC to reduce the current scope and/or
frequency of post-closure monitoring, and is awaiting that determination. In the
meantime, LKB recommends that the above monitoring schedule be followed.
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APPENDIX A
Sample Results
Report Date:Final Report
14-Apr-15 11:29
Re-Issued Report
Revised Report
Laboratory Report
Lockwood Kessler & Bartlett Inc.Work Order:P0384
One Aerial WayProject :Southhold Landfill Routine Parameters
Syosset, NY 11791Project #:
Attn: John Gerlach
Laboratory IDLaboratory IDClient Sample IDClient Sample IDMatrixMatrixDate SampledDate SampledDate ReceivedDate Received
Laboratory IDLaboratory IDClient Sample IDClient Sample IDMMaattrriixxDate SampledDate SampledDate ReceivedDate Received
P0384-01MW-3DAqueous25-Mar-15 08:3026-Mar-15 14:00
P0384-02MW-3SAqueous25-Mar-15 09:0026-Mar-15 14:00
P0384-03MW-5DAqueous25-Mar-15 09:3026-Mar-15 14:00
P0384-04MW-5SAqueous25-Mar-15 10:0026-Mar-15 14:00
P0384-05MW-4DAqueous25-Mar-15 10:3026-Mar-15 14:00
P0384-06MW-4SAqueous25-Mar-15 11:0026-Mar-15 14:00
P0384-07MW-8DAqueous25-Mar-15 11:3026-Mar-15 14:00
P0384-08MW-8SAqueous25-Mar-15 12:0026-Mar-15 14:00
P0384-09MW-6DAqueous25-Mar-15 12:3026-Mar-15 14:00
P0384-10MW-6SAqueous25-Mar-15 12:4526-Mar-15 14:00
P0384-11MW-7SAqueous25-Mar-15 13:0026-Mar-15 14:00
P0384-12MW-1DAqueous25-Mar-15 13:3026-Mar-15 14:00
P0384-13MW-1SAqueous25-Mar-15 14:0026-Mar-15 14:00
I attest that the information contained within the report has been reviewed for accuracy and checked against the quality control requirements for each method. The results
relate only to the samples(s) as received. This report may not be reproduced, except in full, without written approval from Spectrum Analytical.
All applicable NELAC or USEPA CLP requirments have been meet.
Spectrum Analytical (Rhode Island) is accredited under the National Environmental Laboratory Approval Program (NELAP) and DoD Environmental Laboratory
Accreditation Program (ELAP), holds Organic and Inorganic contracts under the USEPA CLP Program and is certified under several states. The current list of our
laboratory approvals and certifications is available on the Certifications page on our web site at www.spectrum-analytical.com.
Please contact the Laboratory or Technical Director at 401-732-3400 with any questions regarding the data contained in the laboratory report.
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Client:
MW-3DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0103/25/15 8:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
Cadmium1.0J5.0ug/L104/02/2015 12:0281504
Calcium36000800ug/L104/02/2015 12:0281504
Iron34000200ug/L104/02/2015 12:0281504
LeadND10ug/L104/02/2015 12:0281504
Magnesium27000500ug/L104/02/2015 12:0281504
Manganese270050ug/L104/02/2015 12:0281504
Potassium670001000ug/L104/02/2015 12:0281504
Sodium1000001000ug/L104/02/2015 12:0281504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 7 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-3SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0203/25/15 9:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
Cadmium3.0J5.0ug/L104/02/2015 12:0681504
Calcium28000800ug/L104/02/2015 12:0681504
Iron90000200ug/L104/02/2015 12:0681504
LeadND10ug/L104/02/2015 12:0681504
Magnesium18000500ug/L104/02/2015 12:0681504
Manganese570050ug/L104/02/2015 12:0681504
Potassium180001000ug/L104/02/2015 12:0681504
Sodium470001000ug/L104/02/2015 12:0681504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 8 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-5DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0303/25/15 9:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 12:0981504
Calcium72000800ug/L104/02/2015 12:0981504
Iron130J200ug/L104/02/2015 12:0981504
LeadND10ug/L104/02/2015 12:0981504
Magnesium33000500ug/L104/02/2015 12:0981504
Manganese1100050ug/L104/02/2015 12:0981504
Potassium1100001000ug/L104/02/2015 12:0981504
Sodium1400001000ug/L104/02/2015 12:0981504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 9 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-5SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0403/25/15 10:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 12:1381504
Calcium11000800ug/L104/02/2015 12:1381504
IronND200ug/L104/02/2015 12:1381504
LeadND10ug/L104/02/2015 12:1381504
Magnesium7000500ug/L104/02/2015 12:1381504
Manganese16050ug/L104/02/2015 12:1381504
Potassium39001000ug/L104/02/2015 12:1381504
Sodium140001000ug/L104/02/2015 12:1381504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 10 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-4DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0503/25/15 10:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 12:2481504
Calcium160000800ug/L104/02/2015 12:2481504
Iron660200ug/L104/02/2015 12:2481504
LeadND10ug/L104/02/2015 12:2481504
Magnesium67000500ug/L104/02/2015 12:2481504
Manganese310050ug/L104/02/2015 12:2481504
Potassium410001000ug/L104/02/2015 12:2481504
Sodium2200001000ug/L104/02/2015 12:2481504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 11 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-4SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0603/25/15 11:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 12:2881504
Calcium81000800ug/L104/02/2015 12:2881504
IronND200ug/L104/02/2015 12:2881504
LeadND10ug/L104/02/2015 12:2881504
Magnesium18000500ug/L104/02/2015 12:2881504
Manganese370050ug/L104/02/2015 12:2881504
Potassium420001000ug/L104/02/2015 12:2881504
Sodium140001000ug/L104/02/2015 12:2881504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 12 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-8DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0703/25/15 11:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 12:3181504
Calcium59000800ug/L104/02/2015 12:3181504
Iron12000200ug/L104/02/2015 12:3181504
LeadND10ug/L104/02/2015 12:3181504
Magnesium30000500ug/L104/02/2015 12:3181504
Manganese150050ug/L104/02/2015 12:3181504
Potassium500001000ug/L104/02/2015 12:3181504
Sodium660001000ug/L104/02/2015 12:3181504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 13 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-8SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0803/25/15 12:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
Cadmium1.4J5.0ug/L104/02/2015 12:3581504
Calcium50000800ug/L104/02/2015 12:3581504
Iron39000200ug/L104/02/2015 12:3581504
LeadND10ug/L104/02/2015 12:3581504
Magnesium20000500ug/L104/02/2015 12:3581504
Manganese62050ug/L104/02/2015 12:3581504
Potassium520001000ug/L104/02/2015 12:3581504
Sodium300001000ug/L104/02/2015 12:3581504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 14 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-6DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-0903/25/15 12:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 13:0181504
Calcium37000800ug/L104/02/2015 13:0181504
Iron48J200ug/L104/02/2015 13:0181504
LeadND10ug/L104/02/2015 13:0181504
Magnesium20000500ug/L104/02/2015 13:0181504
Manganese98050ug/L104/02/2015 13:0181504
Potassium31001000ug/L104/02/2015 13:0181504
Sodium180001000ug/L104/02/2015 13:0181504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 15 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-6SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-1003/25/15 12:45
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 13:0481504
Calcium17000800ug/L104/02/2015 13:0481504
Iron210200ug/L104/02/2015 13:0481504
LeadND10ug/L104/02/2015 13:0481504
Magnesium5800500ug/L104/02/2015 13:0481504
Manganese340050ug/L104/02/2015 13:0481504
Potassium47001000ug/L104/02/2015 13:0481504
Sodium91001000ug/L104/02/2015 13:0481504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 16 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-7SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-1103/25/15 13:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 13:0881504
Calcium16000800ug/L104/02/2015 13:0881504
Iron210200ug/L104/02/2015 13:0881504
LeadND10ug/L104/02/2015 13:0881504
Magnesium5600500ug/L104/02/2015 13:0881504
Manganese330050ug/L104/02/2015 13:0881504
Potassium46001000ug/L104/02/2015 13:0881504
Sodium90001000ug/L104/02/2015 13:0881504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 17 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-1DSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-1203/25/15 13:30
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 13:1281504
Calcium31000800ug/L104/02/2015 13:1281504
Iron63J200ug/L104/02/2015 13:1281504
LeadND10ug/L104/02/2015 13:1281504
Magnesium15000500ug/L104/02/2015 13:1281504
ManganeseND50ug/L104/02/2015 13:1281504
Potassium16001000ug/L104/02/2015 13:1281504
Sodium210001000ug/L104/02/2015 13:1281504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 18 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Lockwood Kessler & Bartlett Inc.
Client:
MW-1SSouthhold Landfill Routine Parameters
Client Sample ID:Project:
P0384-1303/25/15 14:00
Lab ID:Collection Date:
AnalysesResultQualRLUnitsDFDate AnalyzedBatch ID
SW846 6010C -- Metals by ICPSW6010_W
CadmiumND5.0ug/L104/02/2015 13:1581504
Calcium8200800ug/L104/02/2015 13:1581504
IronND200ug/L104/02/2015 13:1581504
LeadND10ug/L104/02/2015 13:1581504
Magnesium4400500ug/L104/02/2015 13:1581504
Manganese11J50ug/L104/02/2015 13:1581504
Potassium41001000ug/L104/02/2015 13:1581504
Sodium110001000ug/L104/02/2015 13:1581504
ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
Qualifiers:
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 19 of 89
RPDLimitQualRPDLimitQualRPDLimitQual
B - Analyte detected in the associated Method Blank
20 J
20
20 20 20 20 20 20
04/07/2015
1.379 8.7950400 2.5238870 1.210 0 19630 2.52621.9 2.4751770 0.49630400 0.951
RPD Ref Val%RPDRPD Ref Val%RPDRPD Ref Val%RPD
OPTIMA3_150402AOPTIMA3_150402AOPTIMA3_150402A
Date:
0 0 0 0 0 0 0 0
224582322458242245835
ANALYTICAL QC SUMMARY REPORT
SeqNo:SeqNo:SeqNo:
Run ID:Run ID:Run ID:
LowLimitHighLimitLowLimitHighLimitLowLimitHighLimit
109 80 120 103 80 120 110 80 120 109 80 120 111 80 120 110 80 120 109 80 120 111 80 120 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0
04/01/15 11:3004/02/15 11:5504/01/15 11:3004/02/15 11:5804/01/15 11:3004/02/15 12:39
SPK valueSPK Ref Val%RECSPK valueSPK Ref Val%RECSPK valueSPK Ref Val%REC
MDL - Method Detection Limit
Analysis Date:Analysis Date:Analysis Date:
Prep Date:Prep Date:Prep Date:
SW846 6010C -- Metals by ICP
0
0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
Reporting Limit
RL -
227.0 22700 4550 455.0 22700 2270 22700 22700
0 0 0 0 0 0 0
0_W
S - Recovery outside accepted recovery limits
SW601
R - RPD outside accepted recovery limits
5.0 800 200 10 500 50 1000 1000 5.0 800 200 10 500 50 1000 1000 5.0 800 200 10 500 50 1000 1000
SW6010_WSW6010_WSW6010_W
RLRLRL
ug/Lug/Lug/L
Spectrum Analytical Inc. - North Kingstown RI --
TestCode:TestCode:TestCode:
Units:Units:Units:
ND0.89 ND110 ND31 ND4.2 ND76 ND10 ND76 ND29 23410 110 5020 31 25110 76 2490 10 24750 76 25280 29 0.89 49140
110 38400 31 19140 76 606.8 10 51520 76 30110 29
0.89 4.2 4.2
Southhold Landfill Routine Parameters
MDLMDLMDL
Lockwood Kessler & Bartlett Inc.
J - Analyte detected below quanititation limits
815048150481504
MBLK
DUP
LCS
ResultResultResult
246.4 494.7 1.263 ND
SampType:SampType:SampType:
Batch ID:Batch ID:Batch ID:
ND - Not Detected at the MDL
P0384-08DDUP
P0384
LCS-81504LCS-81504
504
MB-81504
MW-8S
1
8
-
Work Order:
B
M
Qualifiers:
Sample ID:Sample ID:Sample ID:
CLIENT:
ManganeseManganeseManganese
m15.03.22.2229
MagnesiumMagnesiumMagnesium
Client ID:Client ID:Client ID:
Project:
PotassiumPotassiumPotassium
CadmiumCadmiumCadmium
AnalyteCalciumAnalyteCalciumAnalyteCalcium
SodiumSodiumSodium
LeadLeadLead
IronIronIron
P0384Page 20 of 89
RPDLimitQualRPDLimitQual
B - Analyte detected in the associated Method Blank
S
10 10
10 10 10 10 10 10
1.379 0 50400 4.0638870 1.930 0 19630 0.235621.9 0.10251770 5.4930400 4.81
RPD Ref Val%RPDRPD Ref Val%RPD
OPTIMA3_150402AOPTIMA3_150402A
0 0 0 0
22458362245837
ANALYTICAL QC SUMMARY REPORT
SeqNo:SeqNo:
Run ID:Run ID:
LowLimitHighLimitLowLimitHighLimit
104 80 120 74.4 80 120 106 80 120 108 80 120 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0
0 0 0 0
04/01/15 11:3004/02/15 12:4204/01/15 11:3004/02/15 12:46
SPK valueSPK Ref Val%RECSPK valueSPK Ref Val%REC
MDL - Method Detection Limit
Analysis Date:Analysis Date:
Prep Date:Prep Date:
SW846 6010C -- Metals by ICP
0
1.379 38870 0 621.9 0 0 0 0 0 0 0
Reporting Limit
RL -
227.0 4550 455.0 2270 0
0 0 0 0 0 0
0_W
S - Recovery outside accepted recovery limits
SW601
R - RPD outside accepted recovery limits
5.0 200 10 50 25 4000 1000 50 2500 250 5000 5000
SW6010_WSW6010_W
RLRL
ug/Lug/L
TestCode:TestCode:
Units:Units:
42250 31 3064 10 48400 550 39630 160 ND21 19580 380 622.6 50 54700 380 31900 150
0.89 4.2 4.5
Southhold Landfill Routine Parameters
MDLMDL
Lockwood Kessler & Bartlett Inc.
J - Analyte detected below quanititation limits
8150481504
MS
SD
ResultResult
236.6 480.7 ND
SampType:SampType:
Batch ID:Batch ID:
ND - Not Detected at the MDL
P0384
-08DMS
P0384-08DSD
MW-8SMW-8S
P0384
Work Order:
Qualifiers:
Sample ID:Sample ID:
CLIENT:
ManganeseManganese
m15.03.22.2229
Magnesium
Client ID:Client ID:
Project:
Potassium
CadmiumCadmium
AnalyteAnalyteCalcium
Sodium
LeadLead
IronIron
P0384Page 21 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-3D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-01 Collection Date:03/25/15 8:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)2004.0mg/L CaCO3104/02/2015 12:0281504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride100B03/27/2015 9:5110mg/L581443
Bromide0.580.13mg/L103/26/2015 16:0281443
Nitrogen, Nitrate (As N)ND0.13mg/L103/26/2015 16:0281443
Sulfate39B5.0mg/L103/26/2015 16:0281443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)39020mg/L CaCO3104/06/2015 12:5481596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand5520mg/L103/30/2015 14:5481462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total1110mg/L104/01/2015 12:1181509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 22 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-3S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-02 Collection Date:03/25/15 9:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)1404.0mg/L CaCO3104/02/2015 12:0681504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride64B03/26/2015 16:142.0mg/L181443
Bromide0.250.13mg/L103/26/2015 16:1481443
Nitrogen, Nitrate (As N)ND0.13mg/L103/26/2015 16:1481443
Sulfate37B5.0mg/L103/26/2015 16:1481443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)22020mg/L CaCO3104/06/2015 13:0181596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand2820mg/L103/30/2015 15:0081462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total5.0J10mg/L104/01/2015 12:3881509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 23 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-5D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-03 Collection Date:03/25/15 9:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)3204.0mg/L CaCO3104/02/2015 12:0981504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride170B03/27/2015 10:0310mg/L581443
Bromide1.80.13mg/L103/26/2015 16:2681443
Nitrogen, Nitrate (As N)ND0.13mg/L103/26/2015 16:2681443
Sulfate39B5.0mg/L103/26/2015 16:2681443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)68020mg/L CaCO3104/06/2015 13:0981596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand6120mg/L103/30/2015 15:0681462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total1810mg/L104/01/2015 13:0481509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 24 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-5S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-04 Collection Date:03/25/15 10:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)564.0mg/L CaCO3104/02/2015 12:1381504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride22B03/26/2015 16:382.0mg/L181443
Bromide0.071J0.13mg/L103/26/2015 16:3881443
Nitrogen, Nitrate (As N)1.8B0.13mg/L103/26/2015 16:3881443
Sulfate16B5.0mg/L103/26/2015 16:3881443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)2520mg/L CaCO3104/06/2015 13:1781596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen DemandND20mg/L103/30/2015 15:1281462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total2.0J10mg/L104/01/2015 13:3181509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 25 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-4D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-05 Collection Date:03/25/15 10:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)6904.0mg/L CaCO3104/02/2015 12:2481504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride260B03/27/2015 10:1520mg/L1081443
Bromide2.40.13mg/L103/26/2015 16:4981443
Nitrogen, Nitrate (As N)ND0.13mg/L103/26/2015 16:4981443
Sulfate90B5.0mg/L103/26/2015 16:4981443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)58020mg/L CaCO3104/06/2015 13:2581596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand5120mg/L103/30/2015 15:1881462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total1310mg/L104/01/2015 13:5781509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 26 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-4S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-06 Collection Date:03/25/15 11:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)2804.0mg/L CaCO3104/02/2015 12:2881504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride21B03/26/2015 17:012.0mg/L181443
Bromide0.065J0.13mg/L103/26/2015 17:0181443
Nitrogen, Nitrate (As N)24B1.3mg/L1003/27/2015 7:3081443
Sulfate46B5.0mg/L103/26/2015 17:0181443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)13020mg/L CaCO3104/06/2015 13:3381596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen DemandND20mg/L103/30/2015 15:2481462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total4.9J10mg/L104/01/2015 14:2481509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 27 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-8D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-07 Collection Date:03/25/15 11:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)2704.0mg/L CaCO3104/02/2015 12:3181504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride82B03/27/2015 10:266.0mg/L381443
Bromide0.580.13mg/L103/26/2015 17:3681443
Nitrogen, Nitrate (As N)0.15B0.13mg/L103/27/2015 7:4281443
Sulfate82B5.0mg/L103/26/2015 17:3681443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)28020mg/L CaCO3104/06/2015 13:4181596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand18J20mg/L103/30/2015 15:3081462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total5.9J10mg/L104/01/2015 14:5181509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 28 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-8S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-08 Collection Date:03/25/15 12:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)2104.0mg/L CaCO3104/02/2015 12:3581504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride43B03/26/2015 17:482.0mg/L181443
Bromide0.250.13mg/L103/26/2015 17:4881443
Nitrogen, Nitrate (As N)ND0.13mg/L103/27/2015 7:5481443
Sulfate43B5.0mg/L103/26/2015 17:4881443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)27020mg/L CaCO3104/06/2015 13:4981596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand3820mg/L103/30/2015 15:3681462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total8.7J10mg/L104/01/2015 15:1781509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 29 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-6D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-09 Collection Date:03/25/15 12:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)1804.0mg/L CaCO3104/02/2015 13:0181504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride35B03/26/2015 18:232.0mg/L181443
Bromide0.12J0.13mg/L103/26/2015 18:2381443
Nitrogen, Nitrate (As N)8.9B0.65mg/L503/27/2015 8:2981443
Sulfate93B5.0mg/L103/26/2015 18:2381443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)ND20mg/L CaCO3104/06/2015 14:1281596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen DemandND20mg/L103/30/2015 16:0081462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, TotalND10mg/L104/01/2015 17:3081509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 30 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-6S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-10 Collection Date:03/25/15 12:45
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)674.0mg/L CaCO3104/02/2015 13:0481504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride13B03/26/2015 18:352.0mg/L181443
Bromide0.040J0.13mg/L103/26/2015 18:3581443
Nitrogen, Nitrate (As N)1.6B0.13mg/L103/27/2015 8:4181443
Sulfate13B5.0mg/L103/26/2015 18:3581443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)5020mg/L CaCO3104/06/2015 14:2081596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand17J20mg/L103/30/2015 16:0681462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total5.8J10mg/L104/01/2015 17:5681509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 31 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-7S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-11 Collection Date:03/25/15 13:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)644.0mg/L CaCO3104/02/2015 13:0881504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride13B03/26/2015 18:472.0mg/L181443
Bromide0.042J0.13mg/L103/26/2015 18:4781443
Nitrogen, Nitrate (As N)1.6B0.13mg/L103/27/2015 8:5281443
Sulfate13B5.0mg/L103/26/2015 18:4781443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)4720mg/L CaCO3104/06/2015 14:2881596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen Demand2220mg/L103/30/2015 16:1281462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, Total6.5J10mg/L104/01/2015 18:2381509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 32 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-1D Project:Southhold Landfill Routine Parameters
Lab ID:P0384-12 Collection Date:03/25/15 13:30
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)1404.0mg/L CaCO3104/02/2015 13:1281504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride24B03/26/2015 18:592.0mg/L181443
Bromide0.099J0.13mg/L103/26/2015 18:5981443
Nitrogen, Nitrate (As N)5.3B0.39mg/L303/27/2015 9:0481443
Sulfate83B5.0mg/L103/26/2015 18:5981443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)3120mg/L CaCO3104/06/2015 14:3681596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen DemandND20mg/L103/30/2015 16:1881462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, TotalND10mg/L104/01/2015 18:4981509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 33 of 89
Spectrum Analytical Inc. - North Kingstown RI -- Rhode Island Division
04/07/2015
Client:Lockwood Kessler & Bartlett Inc.
Client Sample ID:MW-1S Project:Southhold Landfill Routine Parameters
Lab ID:P0384-13 Collection Date:03/25/15 14:00
AnalysesResultQualUnitsDate AnalyzedRLDFBatch ID
SM 2340B -- HARDNESS by CalculationSM2340_W
Hardness, Ca/Mg (As CaCO3)394.0mg/L CaCO3104/02/2015 13:1581504
EPA 300.0 -- Anions by Ion Chromotography (LOW)E300IC_W
Chloride13B03/26/2015 19:102.0mg/L181443
Bromide0.033J0.13mg/L103/26/2015 19:1081443
Nitrogen, Nitrate (As N)3.2B0.13mg/L103/27/2015 9:1681443
Sulfate21B5.0mg/L103/26/2015 19:1081443
SM 2320B -- Alkalinity (Total)SM2320_W
Alkalinity, Total (As CaCO3)ND20mg/L CaCO3104/06/2015 14:4481596
SM 5220D -- COD by Closed Reflux Colorimetric MethodSM5220
Chemical Oxygen DemandND20mg/L103/30/2015 16:2481462
SM 5310B TOC -- Total Organic Carbon by combustionSM5310B_TOC_W
Organic Carbon, TotalND10mg/L104/01/2015 19:1681509
Qualifiers: ND - Not Detected at the Reporting LimitS - Spike Recovery outside accepted recovery limits
J - Analyte detected below quanititation limitsR - RPD outside accepted recovery limits
B - Analyte detected in the associated Method BlankE - Value above quantitation range
DF - Dilution FactorRL - Reporting Limit
P0384Page 34 of 89
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Monday,April06,2015
Attn: Ms.AgnesR.Huntley
SpectrumAnalytical
Rhode IslandDivision
646CampAvenue
NorthKingstown,RI02852
Project ID:SOUTHOLDLANDFILLROUTINEPARA
Sample ID#s:BH89597- BH89604
This laboratory isincompliancewith theNELACrequirementsofproceduresused
exceptwhere indicated.
Thisreportcontainsresults for theparameterstested,under thesamplingconditions
describedon theChain Of Custody,asreceivedby the laboratory.
AscannedversionoftheCOC formaccompanies theanalyticalreportand isanexact
duplicateof theoriginal.
Ifyouhaveanyquestionsconcerning thistesting,pleasedonothesitate tocontact
PhoenixClientServicesatext.200.
Sincerelyyours,
PhyllisShiller
LaboratoryDirector
NELAC - #NY11301NJLabRegistration#CT-003
CTLabRegistration#PH-0618NYLabRegistration#11301
MALabRegistration#MA-CT-007PALabRegistration#68-03530
MELabRegistration#CT-007RILabRegistration#63
NHLabRegistration#213693-A,BVTLabRegistration#VT11301
587 EastMiddleTurnpike,P.O.Box370,Manchester,CT06040
Telephone(860)645-1102Fax(860)645-0823
P0384Page 63 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/158:30
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89597
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-3D
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page1of 8Ver 1
P0384Page 64 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1510:00
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89598
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-5S
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page2of 8Ver 1
P0384Page 65 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1510:30
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89599
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-4D
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page3of 8Ver 1
P0384Page 66 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1511:00
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89600
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-4S
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page4of 8Ver 1
P0384Page 67 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1511:30
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89601
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-8D
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page5of 8Ver 1
P0384Page 68 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1512:00
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89602
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-8S
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page6of 8Ver 1
P0384Page 69 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1512:30
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89603
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-6D
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page7of 8Ver 1
P0384Page 70 of 89
Environmental Laboratories, Inc.
587EastMiddleTurnpike, P.O.Box370,Manchester,CT06045
Tel.(860)645-1102Fax(860)645-0823
AnalysisReport
FOR:Attn: Ms.Agnes R. Huntley
SpectrumAnalytical
April06,2015
Rhode Island Division
646 CampAvenue
NorthKingstown, RI 02852
SampleInformationCustody InformationDateTime
Matrix:WATERCollected by:03/25/1513:30
Received by:
LocationCode:SPECTRUM-RILB03/30/1514:17
Rush Request:StandardAnalyzed by:
see"By" below
P.O.#:P0384
LaboratoryData
SDGID:GBH89597
Phoenix ID:BH89604
Project ID:SOUTHOLD LANDFILL ROUTINEPARA
MW-1D
ClientID:
RL/
ParameterResultPQLUnitsDilutionDate/TimeByReference
<0.0080.008mg/L104/02/15BSE420.4
Phenolics
Comments:
If thereareanyquestionsregarding thisdata,please call PhoenixClient Servicesatextension200.
Thisreportmustnotbereproducedexceptin fullasdefinedbytheattached chainof custody.
Phyllis Shiller,Laboratory Director
April06,2015
ReviewedandReleasedby: DebLawrie,ProjectManager
Page8of 8Ver 1
P0384Page 71 of 89
QA/QC Batch303336(mg/L),QC Sample No: BH89602 (BH89597, BH89598, BH89599, BH89600, BH89601, BH89602,BH89603,
BH89604)
Phenolics
85 - 11520
P0384Page 72 of 89
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