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HomeMy WebLinkAboutLandfill Site Inspection Report Draft 03/1991 Vol 202 -9008 -48 -SI REV. NO. 0 FINAL DRAFT SITE INSPECTION REPORT SOUTHOLD LANDFILL CUTCHOGUE, NEW YORK VOLUME 2 OF 2 L:ku;ILRt;Ial1kl1114'. TECHNICAL DIRECTIVE DOCUMENT NO. 02-9008-48 CONTRACT NO. 68-01-7346 FOR THE ENVIRONMENTAL SERVICES DIVISION U.S. ENVIRONMENTAL PROTECTION AGENCY MARCH 29,1991 NUS CORPORATION SUPERFUND DIVISION - ,. a -_ - ____ _- --- ----«_��.�--_Q_�___ c� �`��-� - --- ------ ----- -- __ �.�-�.�----__- __ _ __. _ �----- ��5_�_��.___— - ----- -.- ---- ---------------- -- - lvo c�G� ------_--- - �, - - � ��!-��.L� ����-�___ �--------------------- _ _---- �, -- - � - - -- -, - i IS 41 DA e4 Box 5--3 CH -e ------ - - -- - --- ------ -A - ®RE c4r e:) A.J o V,41 . opltoll 77'�n az� P4)-rn o4 fZ q.i D - -- - -- �(_= 1 iD o s Q aL - fel-3 j_� - ----- -- 51-7 ;�o-7: ILLS _ ' United States Environmental Protection Agency Q* EPA Contract Laboratory Program Sample Management Office PO Boot 918 Alexandria, Organic Traffic Report Case Number SAS No. (d applicable) 703-557-2490 VA 22313 FTs 557-2490 (For CLP Use Only) 1. Type of Activity (Check one) ENF PLD RA SI 2. Region Number SampliYC�4. Date'pped Airbill�lyrp)Zer5. Sample Description (Enter in Column A) O&M RD ST BSTSI Other (Specify) N�jQ{ER Sampler (Name)Carri r 1. Surface Water ESt PA RIFS STPA C. L �^ 2. Ground Water Non-Superfund Program 3. Ship To: 3. Leachate Triple volume required for matrix $. Rinsate spike/duplicate aqueous sample. Name mentSite 5. di to t h � •�a �--�� _. , t- : 1 � --- F , (?• „�;,5,,,, � c�� u T Ship medium and high concentration 6. Oil (SAS) City, State Site Spill ID ; uF a 1 samples in paint cans. 7. Waste (W) )($ J k 3 1. !' 8. Other hW See reverse for additional instructions. CLP (Sample COM(B)e rr) R/�S Analysis alysts (E) (F) (G) Sample Descnp- [ton [ration special Dale/Time of Corresponding Number (Flom labels) IF L=lowper/ VQA BNA Handling Station Location sample Collection CLP Inorganic nn tMi=�high PCB Sample -RE4-3`l Number _Y thilyk -Gw Ph/q.- I d It F! i(I M vm w iS - 6w 4 1 (h (= F K - ) r; ) M F 1=C 5 3 k/"IV 1+- GL4 ; o I o M r F K Y - Rt x Ku S Il 90 S _F q � .EL T L + G►rG �� 1 to I-:Sr1 s -F � x -6w 1 'i � 11ST rA r- ..- 14 All r F 6L x x -X klf ItiI L - C ol-� ► o c6 -r-1. (,, -� F l �L X_ F `a 3 V„RC—F -71R rtll - ir ` �`�- - P -- 7� yX X X,,.,I. - ft - I lit- .- 0 CG - g R F-- 7 4L X X .. - ► N� . L �� 1 1 0 M P F V a vnaw �a.�va unman n..o..am rrano.w..... ryo..� ��� Contract Laboratory Program Sample Management Office Organic Traffic Report PO Box 818 Alexandria, VA 22313 r CLP Use Only) 700557-2490 M %7-2490 .---- ._.••••••�- S i 6 �. •-••. �•• •y�•••••—•-� 1. Type of Activity (Check one) ENF PLD RA . SI HSrS, ERO&M RD STOther (Specify) ESI PA RIFS STPA 2. Region Number Sampling Co. iV4lFTT 4. Date yShipp�d Vkj Ai 'I j7Jy�m 5 Sample Description (Enter in Column A) 1. Surface Water 2. Ground Water 3. Leachate 4. Rinsate 5. Soil/Sediment 7. WaSte SAS 8. Oilier (SAS) (SPAY) Sampler (Name) �� C �u� I�u Carrier r' Non-Superfund Program a Ship To: A k j _ i O Tilt t S w `� I ... Triple volume required for matrix spike/duplicate aqueous sample. Ship medium and high concentration samp les in paint cans. See reverse for additional instructions. Site Naine S 1_ y i City, State i LS. Site Spill ID CLP Sample Number (From fabe/s) Se(A) Sample Descnp- from f°^r i (B) Concern- trabon L=kM M= � H=high RAS (C) Analysis (D) Special Handling (E) Station Location (F) Date/Time of Sample Collection (G) Corresponding CLP Inorganic Sample Number VOA BNA Post/ PCB O F F -7 2 ,,, I 0-k< -'iv 1XI3G g= rt3 AlX r M" -IL -1 IM T 1 '11.1 14 Is M- 13FP 7 X X1 Y .1. ��� i1 S cy -15-6 -G-3 rrn r....., 14 1101 n^nHrna FPA Fnrm 9(175-7. which may be used. Blue - SMO Copy Pink - Region Copy White - lab Copy for Return to SMO lkHow - Lab Copy _ad ."-- _nvtr---- ........ Co..__o.._--a of 'rogr-.SamI Sege-_- Jffice ...Oi c IC —rOrt Box Alexandria, VA 22313 (For CLP Use Only) Ag"'kh EPA 703-557-2490 FTS 557-2490 I IJ`iu� L F.. 1. Type of Activity (Check one) 2. Region Number I Sampling Co. 4.1 $h ed Airbill Number 5. Sample Description (Enter in Column A) FNF PLD RA SI BSTSI _ ,� _ �( T. %t?. 1 y ��L_. �— � _�,�! 4.A.-- 1. Surface Water F R O&M RDHST Other (Specify) Sampler (Name) Carrier FSI PA RIFSSTPA Q o ��� �— 2. Ground Water Non -:3u ertund Program 3. Leachate P 9 3. Ship To: Double volume required for matrix 4. Rinsate spike/duplicate aqueous sample. 5. Soil/Sediment site wame $�(, jV,t Qa<.v�a 6. Oil (SAS) Sfk �. � j U;'c..j c Ship medium and high concentration L' V% -. I,—.i� t r C h q)' (,f;,$ samples in paint cans. 7 Waste (SAS) City. State Site Spill ID 8. Other (SAS) (Specify) Com: IU/ Y -,a- 27 5, _ See reverse for additional instructions. CLP Sam) le Co(0) (C) (D) (E) (F) (G) P RAS Analysis Date/Time of Corresponding Sample Descrip- tration Special Station Sample Organic Number tion L=low (,iom labels) (From M=med y Total Cyanide Handling Location Collection Sample box 1) H=high Metals Number Ih(�F_FKJi, NJ Wtj 6LJ'lq,, IE Fc IJ11 40 R H_ G 1— I X r EPA Form 91113.1 (8-88) Replaces EPA Form 2075.6, which may be used. Gr9A - SYO Copy Pink - Reglon dopy White - Lab Copy for Return to SYO lblkrw - Lab Copy 60 01.0 Ile iwi, BEc 4 I F KS 6 LJ S SIO I _ _ F L X G C 91� �o _ X 1 S- XS a -k: F F 6-x3 r, ^.v — V L L )I S 1 j�gL- P F P -7 l IJ11 40 R H_ G 1— I X r EPA Form 91113.1 (8-88) Replaces EPA Form 2075.6, which may be used. Gr9A - SYO Copy Pink - Reglon dopy White - Lab Copy for Return to SYO lblkrw - Lab Copy I Ste Ironr--- --' ProtE -"- '4genr Ontr, orate_, .__ ...nple ,.__jernrj_ ",.,.e I:p� PO Box 818 Alexandria, VA 22313 s 703.557-2490 FTS 557-2490 1. Type of Activity (Check one) 2. Region Numb or Sampling Co. ENI PLD _ RA RS. BSTSI ER 08M RDT Other (Specify) Sampler (Name) ESI PA RIFSTPA __ 9,6e. -t C. Won -Sul erfund Program 3. Ship To: -- --- — -- - "— --- Ii S f .) Q Sile Name -- - .. _---. ---- aa L �• A,tu'Iff / ?fit. )J.'rtt•. P C City. Stale � '^'� - -- Q S �"c.., y'' i � Site Spill ID CAI (. t � (A) (B) (c) (p) CLP [(Fro ample Concen- RAS Analysis Sample escrip- (ration --- Number lion L=low Total Special (from labels) ) M=med Metals Cyanide Handling If_high invl(ga Tranic Report -mbe- �1S N_. �.. o,�p►ic6.,,o, (For CLP Use Only) S y 4. Date §hipaed Airbill Number 5. Sample Description (Enter in Column A) I x k' 77) 11 Av,( 4 Carrier 1. Surface Water 2. Ground Water Double volume required for matrix 3. Leachate spike/duplicate aqueous sample. 4. Rinsate 5. Soil/Sediment Ship medium and high concentration 6. Oil (SAS) samples in paint cans. 7. Waste (SAS) B. Other (SAS) (Specify) See reverse for additional instructions. (E) (F) (G) Date/Time of Corresponding Station Sample Organic Location Collection Sample Number miar:N`t tis� BAF -7B F. f'� F..rm I Ip -1 (B tin) Rnfd�•.••j ---- L. r Cf .1 F r�rm ?.Q75 6, which mny be u ;r�i. _ P,ern - SMO copy Plnk - Region Copy v'lhrt- - I rb Copy rnr n�tum to SMn 1Mllev? - L.h !;cpv i1 gu m � � ,. »,n. ►�E�.►�►Ai �:� A . AW NMM rnEwrt�urraru M lwnal rad arr,yerrs rowetm awaoAao to ua ecranows. UESAONS7 AIRBILL !� ' 72 O ®® CALL LVO -238-5355 TOLL FREE, f� MCANG NU LEf4 '� �. �`••y'"?AI d , J5--�. p SENDER'S COPY T go 5 4 . +�; .' a x!'& I 1 ,� ..� �a.of a 0(u_A,,,�1�.++► ;� •�, . •� •.N� rtb) PtwD Prim iitla... DAa,. ►.Mitt rimy1117 �'{ ' , � "�„ .. [hpaifrnarlt/F1Qa, tdo. - - - --'�" ..--'�,--- %---- -- (— ) - 1 • Ito Aw hu. fir. R RAW PO. zi � cw ni Z EyA •V ` 3' -'.! •• ' `t•• � iI r•. ? � •Yy :' f t ' I �t ,AP�O+�.a f ;Iry •<. gal willIF ..�' G. , . , M"/iLR i'�(-W kilt FalG ..� �.. y r� ❑ Aftm Stas - '• �r°°b PFbglaw �' r: ti �' " ,� ;': 11CYlid arryupr � ) � , .a SP�IIL /NI�IMC ,,,�,� �r IrtataAlm (cheakawwaftMgL"m ft aw � OWLAW VALUE„ Federal -':�, •�OI+Ila6/�l Express Use ANOLAWrOFLL4BdLm _ _ Base Charges&yawmd-- Unal tlE.((xx •i�H�,rM .' :,.Mrrvbal// ni 2 45 J>H11H1 .. ----- - - II®mlr , •, . ,• bfrrvfox OOldllla. °fir d 1W bo rNpa . ' r + t { i�%pl • • 1 j ; ,.. .. ... ' T , TT- '19, N ririrdlyW I rlxEb�a "'t' a.� n .rm.. _a $t00 per Declared value Charge �prwi�.a�Iawfp�e10 n oixYa M pd -M R C7% 17 � I ' * %•t- � _ 4 ❑ f$ c�+yM`I •1 �7'-` .. t,...,. 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FWwd ���il,ehdAl� 014 T'°1. , 14 ❑ Fia no 6. ❑ F6 a no ❑ ❑ mulnYgad*A" dftmlYrr dug 4 5fi�f8939 ��. �.lOV" fir•, o ❑ m�F„�� mp 3o��mm*wswdswww a[] • til IN f ' .OBBC. � WilIN 70 M 10 5 nPul USA `a•'ti} ¢ .:i}: ; ' I ❑ O Zoon Gel S1oP Date/Time �°° ./, 'VCOfAR'rR• ,�. .,I SID❑ iDid11 allp6 IIaDIFL o+'. Fmp No. "CllYrdrbdYsd+er 12 PAiiT 106.72 MONEY-p". UM Or IM f.E.C.- b hoolo " ❑ �! GUMA'S COPY 1/00 --� .jRA.. v-RE-..«EASL. vvvFOw%,vvATIUvv JNL. NUS -FIT SAMPLING INFORMATION ite Name 5�,,. 1�\a �� , a� , i Shipping Date(s): ase No. `l gL SAS No. Laboratories: Organic S r,AC. J, DD/BRICS C-.�-���,,� -y2 /N ;Nli -1: Inorganic Field SMO: ampling Date(s) _� aT�Signature/Date Sample Type NUS Sample No. - Organic CLP No. —L - 1 Inorganic CLP No. VIBEF10, OC Information Comments -KH, WO - Lw V -cu in BE Fh -� i N t� - MM- 1- `1 . - L w `=C 5 - CLjFc ll�G-F`l a, ti- ►t - _C f,; _ 'A - C w F t= C IJ `i ki - r- M ;_ A , l S S � -s- rc � air✓ S R'C--7u ry\ �3 S u - S - - --1 I M(3 �. is same es in e e nwinn or er: oroun wa er - sur acewa er . s imen ois , sate blanks (RIN), Trip blanks (TILK) page of DRAFT PRE-RELEASE INFORMATION ONLY NUS -FIT SAMPLING INFORMATION ite Name S (. VAlI N L,�,.11 Shipping Date(s): i 1_5 << ase No. l SAS No. Laboratories: Organic DD/BRICS l: - �t�� i to It --v: Inorganic Ali,, I_kL,, Field SMO: ampling Date(s) N). I A1, «„� N k ISignature/Date _(,,.�� L q x Sample Type NUS Sample No. Organic CLP No. Inorgganic CLP No. OC Information Comments -7 M = U �' N► i SO ,.W 1\j 1 - r, � 'L - 7 CIA 6� - C, ' Z .. -- ..I\j o - ILS I L 1� List samples in the followina or er: vroun wa er _ sur acewa er ISWL sediment - 01 s ansa e blanks (RIN), Trip blanks (TBLK) paqe of Slit NAME..�1..- BOTTLE LOT NO. FORM DATE _ Q-, 3-I elf --... . SIGNATURE NUS Sample Number No. of • os. jars Supplier/ lot No. No. of 40 ml Wish Supplier/ lot No. No. of 80 0:. or tl amber Supplier/ lot No. No. of 1L Poly Oogles Supplier/ lot No. _ v 1 U 3 013 }J' -I Wti - 6w-1- N. Q L 1 03 613 _ �, -- X b�gK�u X v0j � - - - N`i tvA- Gw B 03,13 - - � _��1 �-��L3- - �_- %� C� c i q -,i 3 (3�i�3��3- a _ 0 qA3 ivi_�r__ w -- -� ����3�►3 �_ X btu) -03 -S 3 1V t N 1-1, C--U23 -.Qs,Ai,Io -3- - -- - -.. `' ul GI G 2-g�1.�3,13 -U. IC = I CIIEM EP =Eagle Picker MUMMA. .-- BOTTLE LOT NO. FORM ®ATE SIGNATURE IC = I C11EM EP = Eagle Picker No. of No. of No. of No. of. NUS Sample • ox. Supplier/ 40 ml Supplier/ 80011.01 Supplier/ tl Poly Supplier/ Number jars lot No. Wish Lot No. 1L amber Lot No. Bottles lot No. v< -- 3 t "gjlo3,JL3 — -- - WA N.t}. _ RM—wt- — �1�3�► lilt 1-_A-ka -- 1 - XvDq�Avk3 I - xoL it- —_ (� 3 ► 3 x o l c, of u 13 2 _�ti—`L � 3- N.`i N �_ N —_� -- — — -- - I- - o0460V3 v o ci C o 1 -L =o Lc -r �_ 6„/_B 010. - _ --- S _.l - Q �I.� 1 . _ -2C-):16�--- 3 3 i� `" - 3 - ;=X"`.i -3.3 - -- — - IC = I C11EM EP = Eagle Picker - COPY OF CLP DATA (REDLINED AND MARKED) -COMPUTER QA'd PRINTOUT SITE NAME: Yoc)�Ao/d CASE# AND/OR SAS#: BRICS#: �/ Pvl.)--� TDD#: CJ - �700 g /Syb'(,o 3 SITE - 30UTH( "ILL TDD1: u4 -7u08-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS VOLATILES Sample ID No. ;HYMN-GW1 HYNH-GW5 HYNH-GW6 AYHH-GW7 NYNH-GW8 NYNH-TBLX1 NYNH-GW2(MS/MSD) NYHH-GW3 NYNH-GW4(DUP) NYNH-S1 HYNH-S2(DUP) Traffic Report No. BFC39 BFC54 BFC55 BFC98 BFC99 BFF79 BFC40 BFC41 BFC53 BFF66 BFF67 Matrix WATER WATER WATER WATER WATER WATER WATER WATER WATER SOIL SOIL Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/kg ug/kg Dilution Factor 1 1 1 1 1 1 1 l 1 1 1 Percent Moisture ------------------------------------------ ---------------------------------------------------------------------------------------------------------------------------------- 5 5 Chloromethane ; 19 Bromomethane Vinyl Chloride ; Chloroethane ; Methylene Chloride ; B Acetone J J Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane ; Trans-1,2-Dichloroethene (total) ; J Chloroform 1,2-Dichloroethane J J 2-Butanone 1,1,1 -Trichloroethane Carbon Tetrachloride Vinyl Acetate Bromodichloromethane 1,2-Dichloropropane ; 9 15 15 cis-1,3-Dichloropropene Trichloroethene ; Dibromochloromethane 1,1,2 -Trichloroethane Benzene ; trans-1,3-Dichloropropene Bromoform 4-Methyl-2-Pentanone ; 2-Hexanone Tetrachloroethene J Toluene ; J 1,1,2,2 -Tetrachloroethane Chlorobenzene 24 23 Ethylbenzene ; Styrene ; Xylenes (Total) NOTES: Blank space - compound analyzed for but not detected B compound found in lab blank as well as sample, indicates possible/probable blank contamination E estimated value J estimated value, compound present below CROL but above IDL R analysis did not pass EPA QA/QC H Presumptive evidence of the presence of the material NR analysis not required Detection limits elevated if Dilution Factor >1 and/or percent moisture >0E N i1L 11111L. .UU IIIULU L-111- TDDI:--"^18-48 SAMPL--- -_._S: 1_,.,._ _2/5/9_ EPA CASE NO.: 15486 LAB: INTECH BIOLABS VOLATILES Sample ID No. NYNH-S3 NYNH-S4 NYNH-S5 NYNH-S6 HYMN -S7 HYNH-S8(MS/MSD) NYNH-S9 NYNH-RIN1 NYNH-RIN2 NYNH-RIN3 NYNH-RIN4 NYNH-TBLK2 Traffic Report No. BFF68 BFF69 BFF70 BFF71 BFF72 BFF73 BFF74 BFF75 BFF76 BFF77 BFF78 BFF80 Matrix ; SOIL SOIL SOIL SOIL SOIL SOIL SOIL NATER NATER NATER NATER NATER Units ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/L ug/L ug/L ug/L ug/L Dilution Factor 1 1 1 1 1 1 1 1 1 1 1 1 Percent Moisture ; ------------------------------------------ 2 ---------------------------------------------------------------------------------------------------------------------------------------- 15 5 36 2 9 10 Chloromethane J J J 25 15 Bromomethane I Vinyl Chloride Chloroethane Methylene Chloride B B B B B Acetone ; J 23 30 46 J J Carbon Disulfide ; 1,1-Dichloroethene l,l-Dichloroethane Trans-1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane I 2-Butanone ' 1,1,1 -Trichloroethane Carbon Tetrachloride Vinyl Acetate Bromodichloromethane 1,2-Dichloropropans cis-1,3-Dichloropropene Trichloroethene ; Dibromochloromethane ; 1,1,2 -Trichloroethane Benzene ' trans-1,3-Dichloropropene ; Bromoform ' I 4-Methyl-2-Pentanone 2-Hexanone ' Tetrachloroethene ; Toluene ; J 7 J 1,1,2,2 -Tetrachloroethane Chlorobenzene Ethylbenzene ; Styrene Xylenes (Total) NOTES: Blank space - compound analyzed for but not detected B compound found in lab blank as well as sample, indicates possible/probable blank contamination E estimated value J estimated value, compound present below CROL but above IDL R - analysis did not pass EPA AA/OC N Presumptive evidence of the presence of the material NR analysis not required Detection limits elevated if Dilution Factor >1 and/or percent moisture >02 SITE NAME: SOUTHOLD LANDFILL TDDI: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS SEMI -VOLATILES ; Sasple ID No. NYNH-GNI Traffic Report No. BFC39 Matrix NATER Units ; ug/L Dilution Factor/GPC Cleanup (Y) ; 1 Percent Moisture NATER ------------------------------------------ --------- Phenol NATER bis(2-Chloroethyl)ether SOIL 2 -Chlorophenol ; 1,3 -Dichlorobenzene ug/L 1,4 -Dichlorobenzene ; Benzyl alcohol ug/L 1,2 -Dichlorobenzene ; 2-Methylphenol ; bis(2-Chloroisopropyl)ether 1 4-Methylphenol 1 N-Nitroso-di-n-dipropylamine 1 Nexachloroethane 4 Nitrobenzene Isophorone 2-Nitrophenol 2,4 -Dimethylphenol ; Benzoic acid ; bis(2-Chloroethoxy)sethane ; 2,4-Dichlorophenol 1,2,4-Trichlorobenzene ; Naphthalene 4-Chloroaniline ; Hexachlorobutadiene 4-Chloro-3-Methylphenol 2 -Methylnaphthalene Hexachlorocyclopentadiene ; 2,4,6 -Trichlorophenol 2,4,5 -Trichlorophenol 2-Chloronaphthalene ; 2-Nitroaniline Dimethylphthalate ; Acenaphthylene 2,6-Dinitrotoluene 3-Nitroaniline ' Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol Dibenzofuran 2,4-Dinitrotoluene ; Diethylphthalate 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-tethylphenol N-nitrosodiphenylatine 4-Bromophenyl-phenyl ether Hexachlorobenzene ; NYNH-GN5 NYNH-GN6 NYHH-GN7 NYNH-GN8 NYNH-TBLK1 NYNH-GN2(MS/MSD) NYNH-GN3 NYNH-GN4(DUP) NYNH-S1 NYNH-S2(DUP) BFC54 BFC55 BFC98 BFC99 BFF79 BFC40 BFC41 BFC53 BFF66 BFF67 NATER NATER NATER NATER NATER NATER NATER NATER SOIL SOIL ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/kg ug/kg 1 1 1 1 N/A 1 1 1 4 4 ------------------------------ ---------------------------------------------------------------------------------------- N/A -- 5 5 MR NR NR NR NR NR NR NR NR NR NR HR NR NR NR NR NR NR NR NR NR NR NR RR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR RR NR NR NR SITE SOUTHI FILL TDDI: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS SEMI -VOLATILES Sample ID No. ;NYNH-GW1 NYNH-GW5 NYHH-GH6 NYNH-GW7 NYNH-GW8 NYNH-TBLK1 HYNH-GW2(MS/MSD) NYNH-GW3 NYNH-GW4(DUP) NYNH-Sl NYNN-S2(DUP) Traffic Report No. BFC39 BFC54 BFC55 BFC98 BFC99 BFF79 BFC40 BFC41 BFC53 BFF66 BFF67 Matrix WATER WATER WATER WATER WATER WATER WATER WATER WATER SOIL SOIL Units ; ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/L ug/kg ug/kg Dilution Factor/GPC'Cleanup (Y) ; 1 1 1 1 1 N/A 1 1 1 4 4 Percent Moisture ; H/A -- 5 5 ------------------------------------------ ----------------------------------------------------------------------------------------------------------------------------------- Pentachlorophenol ; NR Phenanthrene ; NR Anthracene ; WR Di-n-butylphthalate ; NR Fluoranthene NR Pyrene NA Butylbenzylphthalate WR 3,3'-Dichlorobenzidine ; MR Benzo(a)anthracene ; NR Chrysene ; NR bis(2-Ethylhexyl)phthalate ; J J J J J NR J Di-n-octylphthalate NR Benzo(b)fluoranthene NR Benzo(k)fluoranthene ; NR Benzo(a)pyrene ; NR Indeno(1,2,3-cd)pyrene ; NR Dibenz(a,h)anthracene ; NR Benzo(g,h,i)perylene ; NR NOTES: Blank space - compound analyzed for but not detected B - compound found in lab blank as well as sample, indicates possible/probable blank contamination E estimated value J estimated value, compound present below CRAL but above IDL R analysis did not pass EPA QA/QC N Presumptive evidence of the presence of the material NR analysis not required Detection limits elevated if Dilution Factor )I and/or percent moisture )0Y 9 0 T; SITE SOUTR„.„ ...JFILL TDDI: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS SEMI -VOLATILES BFF72 BFF73 8FF74 Sample ID No. ; NYNH-S3 NYHH-S4 NYHH-S5 Traffic Report No. BFF68 BFF69 BFF70 Matrix ; SOIL SOIL SOIL Units ; ug/kg ug/kg ug/kg Dilution Factor/GPC Cleanup (Y) ; 4 1 1 Percent Moisture ------------------------------------------ ; 2 15 5 Phenol ------------------------------ ; bis(2-Chloroethyl)ether ; 2 -Chlorophenol ; 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene ; Benzyl alcohol 1,2 -Dichlorobenzene ; 2-Methylphenol ; bis(2-Chloroisopropyl)ether ; 4-Methylphenol ; H-Nitroso-di-n-dipropylamine ; Hexachloroethane Nitrobenzene Isophorone 2-Nitrophenol ; 2,4 -Dimethylphenol Benzoic acid bis(2-Chloroethoxy)methane 2,4-Dichlorophenol 1,2,4-Trichlorobenzene Naphthalene 4-Chloroaniline ; Hexachlorobutadiene 4-Chloro-3-Methylphenol 2 -Methylnaphthalene Hexachlorocyclopentadiene ; 2,4,6 -Trichlorophenol 2,4,5 -Trichlorophenol 2-Chloronaphthalene ; 2-Nitroaniline Dimethylphthalate ; Acenaphthylene ; 2,6-Dinitrotoluene 3-Nitroaniline Acenaphthene 2,4-Dinitrophenol 4-Nitrophenol ; Dibenzofuran 2,4-Dinitrotoluene Diethylphthalate ; 4-Chlorophenyl-phenyl ether Fluorene 4-Nitroaniline 4,6-Dinitro-2-eethylphenol N-nitrosodiphenylasine ; 4-8romophenyl-phenyl ether ; Hexachlorobenzene HYNH-S6 NYNH-S7 NYNH-SB(MS/MSD) NYHH-S9 NYNH-RIN1 NYNH-RIN2 NYNH-RIN3 NYNH-RIN4 NYNH-TBLK2 BFF71 BFF72 BFF73 8FF74 BFF75 BFF76 BFF77 BFF78 BFFBO SOIL SOIL SOIL SOIL NATER NATER NATER NATER NATER ug/kg ug/kg ug/kg ug/kg ug/L ug/L ug/L ug/L ug/L 4 4 1 1 1 1 1 1 1 36 ------------------------------------------------------------ 2 9 10 -- -- -- N/A -------------------------------------------- 10000 SITE NAME: SOUTHOLD LANDFILL TDDA: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS SEMI -VOLATILES Sample ID No. NYNH-S3 Traffic Report No. BFF68 Matrix SOIL Units ; ug/kg Dilution Factor/GPC Cleanup (Y) 4 Percent Moisture ; 2 ------------------------------------------ Pentachlorophenol -------- Phenanthrene Anthracene Di-n-butylphthalate Fluoranthene ; Pyrene Butylbenzylphthalate 3,3'-Dichlormbenzidine Benzo(a)anthracene Chrysene ; bis(2-Ethylhexyl)phthalate Di-n-octylphthalate Benzo(b)fluoranthene Benzo(k)fluoranthene ; Benzo(a)pyrene Indeno(1,2,3-cd)pyrene ; 1 Dibenz(a,h)anthracene ; Benzo(g,h,i)perylene ; NOTES: Blank space - compound analyzed for but not detected B compound found in lab blank as well as sample, indicates possible/probable blank contamination E estimated value J - estimated value, compound present below CROL but above IDL R analysis did not pass EPA GA/OC N Presumptive evidence of the presence of the material NR analysis not required Detection limits elevated if Dilution Factor >1 and/or percent moisture >0% I NYNH-54 NYNH-S5 NYNH-S6 NYHH-S7 NYNH-SB(MS/MSD) NYNH-S9 NYNH-RIN1 NYNH-RIN2 NYNH-RIN3 NYNH-RIN4 NYNH-TBLK2 BFF69 BFF70 BFF71 BFF72 BFF73 BFF74 BFF75 BFF76 BFF77 BFF78 BFF80 SOIL SOIL SOIL SOIL SOIL SOIL NATER WATER NATER NATER NATER ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/L ugh ug/L ug/L ug/L 1 1 4 4 1 1 1 1 1 1 1 15 5 36 2 9 10 -- -- -- -- N/A ------------------------------------------------------------------------------------------------------------------------------ HR J NR HR J HR J NR J J NR J NR NR J NR J J NR J 110 230 53 HR WR J HR J HR J J NR NR NR NR SITE NAME: SOUTHOLD LANDFILL TDD4: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS PESTICIDES BFF67 Sample ID No. ;NYNH-GW1 NYNH-GW5 Traffic Report No. BFC39 BFC54 Matrix NATER WATER Units ug/L ug/L Dilution Factor/GPC Cleanup (Y) 1 1 Percent Moisture ; ------------------------------------------ alpha -BHC '-------------------- beta -BHC delta -BHC gamma -BHC (Lindane) Heptachlor Aldrin Heptachlor epoxide Endosulfan I ; Dieldrin 4,4' -DDE Endrin Endosulfan II ; 4,4' -DDD ; Endosulfan sulfate ; 4,4' -DDT Methoxychlor Endrin ketone alpha -Chlordane ; gamma -Chlordane Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 Aroclor-1242 Aroclor-1248 Aroclor-1254 ; Aroclor-1260 ; NOTES: Blank space - compound analyzed for but not detected B - compound found in lab blank as well as sample, indicates possible/probable blank contamination E - estimated value J - estimated value, compound present below CROL but above IDL R - analysis did not pass EPA OA/OC H Presumptive evidence of the presence of the material HR analysis not required Detection limits elevated if Dilution Factor >1 and/or percent moisture >02 NYNH-GW6 NYNH-GW7 NYNH-GWB NYNH-TBLK1 NYNH-GW2(MS/MSD) NYHH-GN3 BFC55 BFC98 BFC99 BFF79 BFC40 BFC41 NATER HATER WATER NATER WATER HATER ug/L ug/L ug/L ug/L ug/L ug/L 1 1 1 N/A 1 1 N/A --------------------------------------------------------------------- HR HR HR NR NR NR NR NR HR NR NR WR HR NR NR NR HR NR NR NR NR NR NR MR NR NR NR NYNH-GW4(DUP) NYHH-S1 NYNH-S2(DUP) BFC53 BFF66 BFF67 WATER SOIL SOIL ug/L ug/kg 1 1 ug/kg 1 5 --------------------------------------- 5 93 E 120 J 57 410 E 450 4' - SITE NAME: SOUTHOLD LANDFILL TDDI: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB: INTECH BIOLABS PESTICIDES Sample ID No. NYHH-S3 Traffic Report No. BFF68 Matrix SOIL Units ; ug/kg Dilution Factor/GPC Cleanup (Y) ; 1 Percent Moisture ------------------------------------------ 2 alpha-BHC -------- beta -BHC delta -BHC gamma-BNC (Lindane) Heptachlor Aldrin Heptachlor epoxide Endosulfan I Dieldrin 4,4' -DDE J Endrin Endosulfan II 4,4' -DDD Endosulfan sulfate J 4,4' -DDT 71 Methoxychlor Endrin ketone alpha -Chlordane gamma -Chlordane J Toxaphene Aroclor-1016 Aroclor-1221 Aroclor-1232 ) Aroclor-1242 Aroclor-1248 Aroclor-1254 Aroclor-1260 NOTES: Blank space - compound analyzed for but not detected B compound found in lab blank as well as sample, indicates possible/probable blank contamination E estimated value J estimated value, compound present below CROL but above IDL R - analysis did not pass EPA OA/OC N Presumptive evidence of the presence of the material NR analysis not required Detection limits elevated if Dilution Factor >1 and/or percent moisture >0t M NYHH-S4 NYNH-S5 NYNH-S6 NYNH-S7 NYNH-SB(MS/MSD) NYHH-S9 NYHH-RINI NYNH-RIN2 HYNH-RIN3 NYNH-RIN4 NYNH-TBLK2 BFF69 BFF70 BFF71 BFF72 8FF73 BFF74 BFF75 BFF76 BFF77 BFF78 BFF80 SOIL SOIL SOIL SOIL SOIL SOIL NATER MATER NATER NATER NATER ug/kg ug/kg ug/kg ug/kg ug/kg ug/kg ug/L ug/L ug/L ug/L ug/L 1 1 10 1 1 1 1 1 1 1 1 15 5 36 2 9 10 N/A ------------------------------------------------------------------------------------------------------------------------- HR NR J HR NR NR 11 MR MR NR HR J J 26 J NR NR J J HR NR J HR 76 E 32 NR MR NR NR J J J NR NR HR NR NR HR HR NR NR 12 SITE NAME: SOUTHOLD LANDFILL TDD4: 02-9008-48 SAMPLING DATES: 12/4/90-12/5/90 EPA CASE NO.: 15486 LAB NAME: ASSOCIATED LABORATORIES INORGANICS ; MBEF95 MBEG19 MBEG20 /A WATER WATER Sample ID No. ;NYNH-GW1 NYNH-GW5 NYNH-GW6 NYNH-GW7 NYNH-GWB NYNh Traffic Report No. ; MBEF92 MBEF96 MBEF97 MBEF96 MBEF99 h Matrix WATER WATER WATER WATER WATER h Units ------------------------- --------------- ; ug/L ----------------------------------------------------------- ug/L ug/L ug/L ug/L ur Aluminum J 733 F Antimony ; J R 14400 E J 63300 E h Arsenic R 12.3 20 23.4 6.9 7.3 h Barium ; J J J J J N Beryllium ; R 3440 E 10100 E 9720 E 6370 M Cadmium ; 75.6 E 85.8 74.1 R 9570 N Calcium ; 8160 E 56600 E 36500 E 28900 E J N Chromium i 0.3 0.3 R R H Cobalt ; J J I R R N Copper ; 213 E 156 E 185 E 59.2 E N Iron 335 E 246 E 284 E 1550 E J M Lead ; 13.8 I 297 E 197 E 195 E H Magnesium ; J 12400 9140 19200 J N Manganese 367 J J J N Mercury 0.7 0.B 0.7 0.6 N Nickel N Potassium ; J J J J J N Selenium ; R R R R R N Silver J J N Sodium ; 27100 12000 873D 27400 8670 N Thallium ; N Vanadium J J N zinc 23.7 405 E 38.3 214 E 22.1 N NOTES: Blank space - compound analyzed for but not detected E estimated value J estimated value, compound present below CRDL but above IDL R analysis did not pass EPA OA/QC NR analysis not required -TBLK1 NYNH-GW2(MS/MSD) HYNH-GW3 NYNH-GW4(DUP) HYNH-S1 NYNH-S2(DUP) /A MBEF93 MBEF94 MBEF95 MBEG19 MBEG20 /A WATER WATER NATER SOIL SOIL /L ug/L ------------------------------------------------------------------------- ug/L ug/L Ag/kg mg/kg R 3 301 308 4640 5320 R 89.3 E 74.4 E R 8.3 8.7 R J J J J J R J R R 14400 E 65800 E 63300 E J J R 12.3 20 23.4 6.9 7.3 R J J R 84 E 31.4 31.4 19.7 E 16.7 E R 3440 E 10100 E 9720 E 6370 7280 R 63.7 E 75.6 E 85.8 74.1 R 9570 43400 42000 J J R J 3020 2900 102 E 106 E R 0.2 I 0.3 0.3 R R I J 167000 162000 J J I R R R I J 2.7 1 21700 158000 153000 J J t ! J J J 13 13.8 I 297 E 197 E 195 E 44.6 E 44 E 04/01/91 SITE NAME: SOUTHOLD LANDFILL 1001: 02-9008-4B SAMPLING DATES: 12/4/90-1215/90 EPA EASE NO.: 15486 LAB NAME: ASSOCIATED LABORATORIES INORGANICS Sample ID No. Traffic Report No. NYNH-S3 NYNH-S4 NYNH-S5 NYNH-S6 NYNH-S7 NYNH-S8(MS/MSD) NYNH-S9 NYNH-RIN1 NYNH-RIN2 NYNH-RIN3 NYNH-RIN4 NYNH-TBLK2 Matrix MBEG21 MBEG22 MBEG23 MBEG24 MBEG25 MBEG26 MBEG27 MBEG28 MBEG29 MBEG30 MBEG31 N/A Units ; SOIL SOIL SOIL SOIL SOIL SOIL SOIL NATER NATER NATER NATER N/A mg/kg eg/kg mg/kg mg/kg eg/kg mg/kg mg/kg ug/L ug/L ug/L ug/L ug/L ----------------------------------' ---------------------------------------------------------------------- Aluminum 2140 4030 4310 12700 3080 1010 --------------------------------------------------------- 5280 J NR Antimony Arsenic ; J 3.2 3.7 15.6 6.8 J 8.5 NR NR Barium ; J J 52.2 E 693 E 61 E J JJ J J NR Beryllium 1.7 J Cadmium ; 8.5 HR Calcium ; J J 1300 E 5180 E 1500 E J J J J J J NR NR Chromium ; 3.3 6.3 5 40.9 6.6 2.6 4.7 MR Cobalt ' J Copper ; 8.4 10.8 E 16.7 E 3020 E 51.7 E 12.8 E 7.B J J J NR NR Iron ` ; 5010 4940 6120 15200 6640 1590 7800 J J J R NR Lead 49.5 20.6 117 412 24.5 13.2 28.1 8.9 E J NR Magnesium J J J J J J J J J J J NR Manganese ; 75.7 E 45.7 E 69.7 E 57.2 E 45.5 E 20.9 E 36.7 E J HR Mercury R R R 10.9 R 0.2 0.2 NR Nickel ; J Potassium J J J J J J J J J NR NR Selenium J J J 9.1 E J R R R NR Silver J J 24.3 2.2 3.1 NR Sodium ; J J J J J J J J J J NR Thallium Vanadium J J J J J J 17.9 NR NR Zinc ; 75.9 E R 134 E 1060 E 215 E R R J 36.7 J R NR NOTES: Blank space compound analyzed for but not detected E estimated value J estimated value, compound present below CROL but above IDL R analysis did not pass EPA DA/GC NR analysis not required 02-9008-48-STR Rev. No. 0 SAMPLING TRIP REPORT SITE NAME: Southold Landfill TDD NO.: 02-9008-48 SAMPLING DATES: December 4 - 5, 1990 EPA CASE NO.: 15486 1. Site Location: See Figure 1 2. Sampling Locations: See Figures 2 and 3 3. Sample Descriptions: See Table 1 4. Laboratories Receiving Samples: Sample Type Name and Address of Laboratory Organic Intech Biolabs, Inc. 158 Tices Lane l l East Brunswick, New Jersey 08816 Inorganic Associated Laboratories, Inc. 806 North Batavia Orange, CA 92668 .j S. Sample Dispatch Data: A total of fourteen aqueous and nine soil samples for organic analysis were shipped by FIT 2 personnel via Federal Express under Airbill No. 9227253000 to Intech Biolabs, Inc. on December 5, 1990 at 1800 hours. A total of twelve aqueous and nine soil samples for inorganic analysis were shipped by FIT 2 personnel via Federal Express under Airbill No. 782184964 to Associated Laboratories, Inc. on December 5, 1990 at 1800 hours. 6. Sampling Personnel: Name Paul Bauer Mike Gallagher Bob Cantagallo Claire Baruxis Dave Florin 7. 8. 9. OR Weather Conditions: 02-9008-48-STR Rev. No. 0 Organization Dates Duties on Site N US Corporation, FIT 12/4,12/5 Site Manager, Written and Photographic Documentation NUS Corporation, FIT 2 12/4,12/5 Site Safety Officer N US Corporation, FIT 12/4,12/5 Sample Management Officer NUS Corporation, FIT 2 12/5 Sampler N US Corporation, FIT 12/5 Sampler December4, 1990: Raining, 50° F, winds calm. December 5, 1990: Partly cloudy, 34°F, winds 20=30 mph out of the north. Additional Comments: All samples except for the trip blank will be analyzed for Target Compound List (TCL) organic and inorganic compounds, excluding cyanide. The trip blanks will be analyzed for volatile organic compounds only. Report Prepared By: Paul Bauer Date: December 14, 1990 Approved By: Date: /2/21/90 NUS Sample ID Number NYNH-GW1 NYNH-GW5 NYNH-GW6 NYNH-GW7 NYNH-GW8 NYNH-TBLK1 02-9008-48-STR Rev. No. 0 TABLE I SAMPLE DESCRIPTIONS SOUTHOLD LANDFILL SOUTHOLD, NEW YORK CASE NO. 15486 DECEMBER 4, 1990 CLP CLP Organic Inorganic Sample Sample Collection Sample Sample Number Number Time Type Location BFC39 MBEF92 1640 Aqueous Tapwater sample collected from outside spigot at the residence of 1 James Mason, Box 155 Tuthill Rd., Cutchogue, NY. BFC54 MBEF96 1605 Aqueous Tapwater sample collected from outside spigot at the residence of Frank McBride, Oregon Rd., Cutchogue, NY. BFC55 MBEF97 1535 Aqueous Tapwater sample collected from outside spigot at the residence of 1 John Suhoski, 11825 Oregon Rd., Cutchogue, NY. BFC98 MBEF98 1455 Aqueous Tapwater sample collected from outside spigot at the commercial I — facility, of Daval Tents & Party Services, Inc., located at Cox Lane, Cutchogue, NY. BFC99 MBEF99 1420 Aqueous Tapwater sample collected from outside spigot at the commercial `— facility of Prime Purveyors Inc., located at 8305 Cox Lane, Cutchogue, NY. BFF79 ------------ 1415 Aqueous Trip blank; demonstrated analyte - free water obtained from NUS Corporation Region 2 FIT, Edison, NJ. 02-9008-48-STR Rev. No. 0 TABLE I (CONT'D) SAMPLE DESCRIPTIONS SOUTHOLD LANDFILL SOUTHOLD, NEW YORK CASE NO. 15486 DECEMBER 5, 1990 NYNH-S6 BFF71 MBEG24 1407 Soil Surface soil sample collected from the north slope of former lagoon A. Sample depth: 0-6 inches. * MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. ** Duplicate - Indicates that a sample was designated as an environmental duplicate sample. CLP CLP NUS Organic Inorganic Sample ID Sample Sample Collection Sample Sample Number Number Number Time Type Location NYNH-GW2* BFC40 MBEF93 1125 Aqueous Tapwater sample collected from outside spigot at the Southold Town Waste Collection Center located at the Southold Landfill, North Rd., Southold, NY. NYNH-GW3 BFC41 MBEF94 1019 Aqueous Groundwater sample collected 1 from monitoring well No. S-68916. NYNH-GW4** BFC53 MBEF95 1028 Aqueous Same location as GW3. NYNH-S1 B'FF66 MBEG19 1610 Soil Surface soil sample collected at a bearing of 133° and a distance of 1 — 5 109 feet from the east post of the Tuthill Rd. gate. Sample depth: 0- 6 inches. NYNH-S2** BFF67 14 MBEG20 �,5 1615 Soil Same location as S1. NYNH-S3 BFF68 MBEG21 1458 Soil Surface soil sample collected at a bearing of 326° and a distance of 10 feet from the east post of the Tuthill Rd. gate. Sample depth: 0- 6 inches. NYNH-S4 BFF69 MBEG22 1527 Soil Surface soil sample collected at a bearing of 267° and a distance of "A" 131 feet from fence post Sample depth: 0-6 inches. NYNH-S5 BFF70 MBEG23 1556 Soil Surface soil sample collected at a bearing of 178° and a distance of 54 feet from fence post "A". Sample depth: 0-6 inches. NYNH-S6 BFF71 MBEG24 1407 Soil Surface soil sample collected from the north slope of former lagoon A. Sample depth: 0-6 inches. * MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. ** Duplicate - Indicates that a sample was designated as an environmental duplicate sample. 02-9008-48-STR Rev. No. 0 TABLE I (CONT'D) . SAMPLE DESCRIPTIONS SOUTHOLD LANDFILL SOUTHOLD, NEW YORK CASE NO. 15486 DECEMBERS, 1990 * MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. CLP CLP NUS Organic Inorganic Sample ID Sample Sample Collection Sample Sample Number Number Number Time Type Location NYNH-S7 BFF72 MBEG25 1320 Soil Subsurface soil sample collected from the center of former lagoon B, approximately 70 feet from the southwestern fence. Sample depth: 10-16 i nches. NYNH-S8* BFF73 MBEG26 1347 Soil Subsurface soil sample collected j 9 from the center of former lagoon A approximately 100 feet from the southwestern fence. Sample depth: 16-24 inches. NYNH-S9 BFF74 MBEG27 1211 Soil Surface soil sample collected at a bearing of 346° and a distance of Q 240 feet from fence. corner "B". Sample depth: 0-6 inches. NYNH-RIN1 BFF75 MBEG28 0905 Aqueous Trowel rinsate blank collected in the field. NYNH-RIN2 BFF76 MBEG29 0920 Aqueous Bowl rinsate blank collected in the field. NYNH-RIN3 BFF77 MBEG30 0845 Aqueous Auger rinsate blank collected in — the field. NYNH-RIN4 BFF78 MBEG31 0800 Aqueous Bailer rinsate blank collected in the J field. NYNH-TBLK2 BFF80 ------------ 0750 Aqueous Trip blank; demonstrated analyte - free water obtained from NUS Corporation Region 2 FIT, Edison, NJ. * MS/MSD - Indicates that additional sample volume was collected and shipped to the laboratory for matrix spike (MS) and matrix spike duplicate (MSD) analysis. 02-9008-48-STR _Rev. No. 0 6 - .. /0 13 ti 6 J - i w1 _. • 6/ oe Duck Pond /..: _r0 ' 65 .37 ` Sound Cl- �� SOUTHOLD LF =;< '�\� � off° • % / /. OCG ,� �• . O -61 pPo• 36 �, •. `9?� . (`. ' �• Cutchogue Sta 3O eu�Es `G •' / �• / • Sacred Heart , 80 • ���� �'� nom..`. �7 PO •.i Cem40 ' cutcho �0 N-F I 9tiF .•�'•• .. - v •�� H 0 D ISS y••� j:. sohgu�a u - ' _ • �•• • 33J �•J''- "� q 2el 7 = o ; o Cut hague t ` •'(� - Ile q 40 -60 41 Cutchogue •; Q ' t• 1 ``o : r . �' /c'`•o .nom _ ,• .` ;�• �` F.'• i� North Fork 20'•i o..Country Club NEW YORK - ` 1 ,73 m� • III l - i `J •�25 `\lo\�rl \ p� 111 r1 I�! �. D ��•.-' QUAD) MATTITUCK HILLS, N.Y. SITE LOCATION MAP FIGURE 1 SOUTHOLD LF, CUTCHOGUE, N.Y. NUS SCALE 1•- 20OW C 3F WmC3RA71C3N WOODED LEGEND MONITORING WELL • SURFACE SOIL SAMPLE ■ SUBSURFACE SOIL SAMPLE A GROUNDWATER SAMPLE Rev. NO. u 0 WOODED ps -69T61 X� o ❑ 0 S,, Z F 0 �GwI ❑ GATE S3• ❑ WOODED ES FIGURE 2 tf1mus EOPOORATION a 02-9008-48-STR .. Rev. No. 0 6 T 6 —61 Duck Pond ! Point:::60 s' 65 i y7 s, ocF , apP� 5 - WS c « \ Sound SOUTHOLD LF r GW 6 �•, °o t, GW o /010 36 ea -2 _:) 5°Cutchogue Sta JO Euo Fs S M• .,.,as 10 {Sacred Heart •`J n p0 • • Cern I 0 ' o 24 40 <q 10 • t • p�0 `X,Cutcho {.� i • :\'• .. .. _. Zara \yam •� g1; .;�•;...; •;- H 0 I� • • o S p�'a ,o Cutchogue ' 1 , _ . v .; 1 eo• ao ao • �'.. ' by . . SM 32. •a• m• •'• • 20 �� •' ,�• ; a` 4 tchogue 3r North Fork + <' •"`:e �` 0 moo\ 20' `• • Orri Country Club •t' BM NEW YORK ^\_ •I'� mr. is •I _ rr 2 - (:S °• • X25 D . (QUAD) MATTITUCK HILLS, N.Y. OFF—SITE TAPWATER SAMPLE LOCATION MAP FIGURE 3 SOUTHOLD LANDFILL, CUTCHOGUE,..N.Y. - NQS SCALA 19-2000f _ COF FORATION I INTECH BIOLABS DIV. OF LABORATORY RESOURCES, INC. 158 Ticea Lwo East Brunswick, New Jersey 08816 (201) 257-1050 Fax (201) 257-2790 CASE NARRATIVE Lab Name: INTECH Case No.: 15486 The following samples are included in thi BFF66 BFF67 BFF68 BFF69 BFF73 BFF74 Con tY�q '�To - 048 B F66 JA AN y Gr Sample De1i 1 SFF72 Detailed Documentation of Problems Encountered With These Samples 1. Please note that the concentration of trans-1,3-dichloro- propene is 32% of the theoretical value in the standard solution mix which is purchased by Intech from Supelco. 2. Bromomethane and carbon disulfide had percent difference greater than 25 in continuing calibrations A3506 and A3518. Since it is a CCC compound, the standards are compliant with contract requirements. 1. Di -n -butyl phthlate is in the spiking solution which is purchased by Intech. Therefore it is shown on the quant reports as well as on the chromatograms of MS/MSD for BNA fraction. 2. One surrogate is outside of contract required QC limits for BFF74, BFF70, BFF7IRE. 3. The area counts for internal standard perylene-d6 was outside of quality control limits for samples BFF67 and BFF67RE. Since this is attributable to matrix interference, both analyses are billable. 4. The area counts for internal standard perylene-d6 was outside quality control limits for samples BFF71 and BFF7IRE. One surrogate is outside of contract required QC limits for BFF7IRE. Since this is due to unknown matrix interfenerces, both analyses are billable. ®QI INTECH BIOL ABS DIV. OF LABORATORY RESOURCES, INC. 158 Tices Lane East Brunswick, New Jersey 08816 (201) 257-1050 Fax (201) 257-2790 5. Phenol and bis(2-chloroethyl)ether coeluted in initial calibrations B3693 and B3694. Spectra for these compounds are included with the chromatograms and quant reports to facilitate qualitative evaluation. . 6. 3,31-dichlorobenzidine, bis(2-chloroisopropyl)ether, hexachlorocyclopentadiene and 2,4,6-tribromophenol had percent differences greater than 25 in continuing calibra- tions B3841 and B3911. Since these are not CCCfs, the standards are compliant with contract requirements. Pesticide Fraction 1. Recovery of dibutylchlorendate is outside advisory limits for BFF73MSD, BFF66, BFF68, BFF69, BFF70 and BFF71. 2. Methoxychlor had percent difference greater than 20 in continuing calibration on INDA analyzed 12/15/90 at 21°48 on confirmation column. No sample was quantitated against confirmation column RTx-5, and also no methoxychlor was found in any samples. I certify that this data package is in compliance with the terms and Gonditions-of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer -readable data submitted on floppy diskette has been authorized by the Laboratory Manager or his designee, as verified by the following signature. 1/8/91 oo7 a o amma rso eymani CLP Project Manager IF 43 INTECH BIOLA►BS DIV. OF LABORATORY RESOURCES, WC. 158 Tim-Larm East Bnxwmck, New Jersey 08816 CASE N (201) 257-1050 Fax (201) 2! JAN 10 1991 Lab Name:. INTECH _ Contract -*ko. *% 8"S D9-- 0048 Case No.: 15486 BFC39 The following samples are included in this Sample Delivery Group: BFC39 BFC40 BFC4.1 BFC53 BFC54 BFC55 BFC98 BFC99 BFF75 BFF76 BFF77 BFF78 BFF79 BFF80 Volatile Fraction 1. Please not6 •i;hair- 'Che concentration of trans -1, 3-dichloro- plPnpastie is 3;4 of - t.he- theoretical value in the standard Volr,tinn mix which is purchased by Intech from Supelco. 2. hz6 percent difference greater than 25 in cor!..�.1.Ii�Z Alits �libr� t:iGn D1381. Since it is not a CCC compound, tkacar-R cosupj iant with contract requirements. 3. and 'T.: anc,-.I., --da �^hloropropene coeluted ­�ili'bration D1342 and in continuing calibration these compounds are included with the ciu.°c M0.-.WjX=—: a.iW' quant report to facilitate qualitative evaluation. semi -Volai:. r"- acs:ion 1: Di -n -butyl phthlate is A.n the spiking solution which is purchased by Intech. Therefore it is shown on the quant repot as well as on eche chromatograms of MS/MSD for BNA fractEiau. 2. One surrogate is outside of contract required QC limits for BFC40MS. 3. One matrix spike compound recovery is outside of quality control limits in BFC40MS. 4. One RPD is outside of quality control limits in BFC40MS/MSD. 001 s INTECH BI0La4BS DIV. OF LABORATORY RESOURCES, INC. 158 Tips Lana East &W wick, New Jersey 08816 (201) 2857-1050 Fax (201) 257-2790 5. Phenol and bis(2-chloroethyl)ether coeluted in initial calibrations B3698 .and B3694, '.Spectra for these compounds are included with' -the chromatograms and quant reports to facilitate qualitative evaluation. 6. 3,31-dichlorobenzidine.and-Hexachlorocyclopentadiene had percent differences greater than 25 in continuing calibrations B3821 and 83841. Since these are not CCU s, the standards are compliant with contract requirements. Pesticide Fraction 4 1. Two RPDe are outside of quality control limits in BFC40MS/MSD. I certify that this data package is in compliance with the terms and conditions Of the-.contract.,•both technically and for completeness, for,other than the conditions'detailed above. Release of ,the data contained in -,this hardcopy data package and in the computer-readable>data.submitted on floppy diskette has been authorized by th Laboratory Manager or his designee, as verified by the following -signature. 1/9/91 - Mohammad i eyman CLP Project Manager 001, ATTACHMENT 1 SOP NO. HW -6 PAGE 1 OF'o TOTAL REVIEW CLP DATA ASSESSMENT Functional Guidelines for Evaluating Organics Analysis Case No. SDG No. �fFU Y LABORATORY SITE W-39 DATA ASSESSMENT: The current functional guidelines (1988) for evaluating organic data have been applied. All data are valid and acceptable except those analytes which have been qualified with a "J" (estimated), "U" (non -detects), "R" (unusable) or "JN" (presumptive evidence for the presence of. the material at an estimated value). All action is detailed on -.the attached sheets. Two facts should be noted by all data users. First, the 11R" flag means that the associated value is unusable. In other words, due to significant QC problems the analysis is invalid and provides no information as to whether the compound is present or not. "R" values should not appear on data tables because they cannot be relied upon, even as a last resort. The second fact to keep in mind is that no compound concentration, even if it has passed all QC tests, is guaranteed to be accurate. Strict QC serves to increase confidence in data but any value potentially contains error. Reviewer ts- Signature: verified By: Date: 1 l 19q I %(e�Q Date : ,I/ -Y—/ 19fl— ATTACHMENT 1 PAGE"\OF� SOP NO. HW -6 DATA ASSESSMENT: 2. BLANK CONTAMINATION: Quality assurance (QA) blanks, i.e., method, trip field, rinse and water b;arks are prepared to identify any contamination which may have been introduced into the samples during sample preparation or field activity. Method blanks measure laboratory contamination. Trip blanks measure cross -contamination of samples during shipment. Field blanks measure cross- contamination of samples during field operations. If the concentration of the analyte is less than 5 times the blank contaminant level (10 times for the common contaminants), the analytes are qualified as non- detects, "U". The following analytes in the samples shown were qualified with "U" for these reasons: A) Method blank contamination m� ��:��. =FFG � , ��o y 53-G�G� � g �� �F �� � � �► B) Field or rinse blank contamination ("water blanks" or "distilled water blanks" are validated like any other sample.) c' q c,.� d _v,k— C) Trip blank contamination 6 bmc's) 391 5y,35;9F-tg9r q ATTACHMENT 1 SOP NO. HW -6 DATA ASSESSMENT: S. CALIBRATION: PAGE OF`O A) PERCENT RELATIVE STANDARD DEVIATION (%RSD) AND PERCENT DIFFERENCE ($D): Percent RSD is calculated from the initial calibration and is used to indicate the stability of the specific compound response factor over increasing concentration. Percent D compares the response factor of the continuing calibration check to the mean response factor (RRF) from the initial calibration. Percent D is a measure of the instrument9s daily performance. Percent RSD must be <30% and $D must be <25%. A value outside of these limits indicates potential detection and quantitation errors. For these reasons, all positive results are flagged as estimated, "J" and non -detects are flagged "UJ" (if %D or RSD >50%). If there is a gross deviation of $RSD and $D, the non -detects may be rejected ("R"). For the PCB/PESTICIDE fraction, $RSD for aldrin, endrin, DDT, and dibutylchlorendate must not exceed 10$. Percent D must be within 15$ on the quantitation column and 20% on the confirmation column. WIG S _t" O d- 5 ATTACHMENT SOP NO. HW -6 DATA ASSESSMENT: 6. SURROGATES: PAGE�_Or` All samples are spiked with surrogate compounds prior to sample preparation to evaluate overall laboratory performance and efficiency of the analytical technique. If the measured surrogate concentrations were outside contract specifications, qualifications were applied to the samples and analytes as shown below. NMI` ' ! ..� • .. ` - h . ltt c nx�- 4uC C� U . y- DD 7- --BFF 1 4- --70 ATTACHMENT I PAGE�OE� SOP NO. HW -f, DATA ASSESSMENT: 7. INTERNAL, STANDARDS PERFORMANCE: Internal standard (IS) performance criteria ensure that the GC/MS sensitivity and response are stable during every experimental run. The internal standard area count must not vary by more than a factor of 2 (-50% to +100%) from the associated continuing calibration standard. The retention time of the internal standard must not vary more than ±30 seconds from the associated continuing calibration standard. If the area count is outside the (-50% to +100%) range of the associated standard, all of the positive results for compounds quantitated using that IS are qualified as estimated, "J", and all non -detects as "UJ", or "R" if there is a severe loss of sensitivity. If an internal standard retention time varies by more than 30 seconds, the reviewer will use professional judgment to determine either partial or total rejection of the data for that sample fraction. f �.e P . 8 or F 6 —7 (7) aaXe ATTACHMENT 1 SOP NO. HW -6 DATA ASSESSMENT: 10. OTHER QC DATA OUT OF SPECIFICATION: PAGE�OF 11. SYSTEM PERFORMANCE AND OVERALL ASSESSMENT (continued on next page if necessary): 12. CONTRACT PROBLEMS NON-COMPLIANCE: 13. This package contains re -extraction, re -analysis or dilution. Upon reviewing the QA results, the following form I(s) are identified to be used. SY = F F Co �- I ..� � r,, -can" c� �o ,�S e,cI - nni/Ull /�(-y ✓u ►a., acuL uuLy L7V7 Type of ilevlew:_ C lute: Chs a. Project: o( ' 11111Mine: LL2� Reviewer's Initlals: Nunber of Soimples: Analytes Ilelec:tul I11e to F:Aec"ll!% Ilevlew Criteria: tes 1W flcl�ls I i i II N u ISM zo � I IUD (7) 7UN) (1) 1 Met IC�� ri Total # Rejected! !A!!! Tlmo OallbrALImi OLNLnli 11 1 11) () a - — Other Total A' 4emples Total N in all 3a� at o� I VZo ©�4% Analytes F..slinril-11I Ihlf! In h.xcccxll1!g Ilc:yl-w Crlterin for: 13 a� .o �A.SE P10. LABORATORY �� - -- SDd3 NO. —�CP to �� �1�� cj DATA USERF I T �� saw REVMW COM .EnON DAZE C1 40. OF SAMPLES WATMt SOIL. OTHER ESD (] MAT rti OTHER, CONTRAC rICONTRACTOR � I T r), VOA BNA PEST OTHM L HOLDING TIME§ 2 GC -US "IZJNF.i GC PERFORMANCE 3. KTTiAL CUM A77ONS 4° C0ONI'IIV=G CALISRAZTONS S. Fl= BLA NICS M . not applicable) 6. LABORATORY BLANKS 7. SURROGATES .& MATRIX SPEKWUPLICATES 9. REGIONAL QC M =not applicable) 10- INTBRNAL S'T'ANDARDS f• IL COMPOUND IDENIgTG?iON 1Z COMPOUND QUANTZTATZON C� 13. SYSTEM PERPOR MCB O �/ 14. OVEN O = No ptabisvas or taiaos problems that do not aif= data enbOfh►. X = No :Dore thea abort 5% of the data points are q=Uff d as either essin aW or namable. M = Mors thea ®burs 5% 09 the data points are goaligW as atsi=VmL Z = More than a6m 5% of the data points ars gaalieed as aaa mW& DPO ACTION TZESt_ atE+i1S OF CONCERN: lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Nam: INTSW Lab Code: INTI. Case No.: 15486 Matrix: (soil/mater) wATSR Sample wt/vol: 5.0 Level: (low/mad) LOW 1 Moisture: not dec. 100. Column: (pack/cap) PACK (g/mL) ML SOPA SAMPLE NO. I BFC39 I Contract: 6'8-D9-0048 ' I 1 SAS No.:: SDO No.: BPC39 Lab Sample ID: Lab Bile ID: D1347 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor.: 1.00 CONCENTRATION UNITS: CAS �d0 • COMPOUND (ug/L or Ug/Kg) UO/L Q 1 74-87-3-------Chloromthane 11 - 30. II UL1 II 74-83-9 ------- Bromomethane I 10. IV I I 75 -01 -4 -------Vinyl Chloride I 10. IU I I 75=00 -3 -------Chloroethane I 10. IU I 75-09=2--- -Methylene Chloride Iu �,I I 67 -l4 -1 -------Acetone O.. U 1 75 -15=0 -------Carbon Disulfide I 5. I IU I I 75-35-4=------1,1-Dichloroethene I 5. IU I I 75-34-3 ------- 1,1=D1Chloroethane I 5. IV I 1 540-59-0-------1, 2-Dichl'airoathene (t ota3L)'I 5. IV I I 67-66-3-------Ch2otoforw .. 1 5. lu 107-06-2----_--1,2-Dichl0roethano- I 5. IV I 1 78-93_3=------2-Batanoiie _... -- .. ( 10. IV f 71-55-6-------_;g;i-Tr'lchloroethane";_ 5. IV I 1` 56-23-5 ------- Catbon Tetrachloride__I ,t 5. Iu I I 108 -05 -4 -------Vinyl Acetate 1 10. IV I I 75-27=4= ------ ftowdtchlosomthane, 5. I U I I 78=87"-5-------1,X-pichldropropane' _-_f_ _I 5. IV I 110061-03-5------- cgs-1,3-Dtchloropropene _( 5. IU I S. IV I I 124=41-Nt�chlozoaethanA_=f S. IU I 1 79-0 --t,2;2-Trichloroethane I 5. IUI 71®4sensene V-. 1 5. 5. IVI11YO61-l,3-Dichloropropeno JU1 75-2f rawforat 1 108-1'---==z-U--fKithyl-2-Pentanone�,i _I - 5. 10. I U IV I I 591-74F-f-----==27-ffixanone 1 ..-10: IV I I 127-18-4z7;-===-vetrachloroethene IU I I 79-34-3------=1,1,2,2-Tetrachloroethane I V I ------- 108-88f-3 Toluene IU 108- =- 90-7------CFlorobonzene -� ----. �; IV 1 1 100-414-------Ilthylbensene l u 1 I 100 -42 -3 -=-----Styrene 1 5 IV I -r- 1 1330 -20 -7 -----Xylene (total) I 1 I S.. Iu I I_I 017 FORM I VOA 1/87 Rev. 1A. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTNM ' Lab Code: INTSCM. Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/mad) LOFT % Moisture: not dec. 100. Column: (pack/cap) PACK EPA SAMPLE No. I I I HFC54 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: D1350 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (uq/4 or uq/Kq) UG/L G I- 74-87-3- ------ Chloromthane 1 I 10. I I 1 Af11,l I 74-83-9- ------ Dromomathane 1 10. IU _: I 1 75 -01 -4 -------Vinyl Chloride 1 10. IU _ I I.. ..75.-00-3------.-Chloroithane t 10. IU I I 75-09-2-------Methy1ene Chloride L 5. IP6KI 1 67-64.-1-----,--Acetont.. t 10. 1U I Disulfide l.. 5. IU I 1 75-35-9-------1,.1-Dichloroethene I 5. IU I I 75-34-3------..-1,3.-Dichloroethane t 5., IU I 1.- 540-59-0 ---- ---1,_2.-Qichloroethene_ (total)_1 5. 1U I 1 67.-66-3.-- --- --Chlorofor• 1 5. IU I I .. 107-Q6-2.-------1,:2-bichlorpethane 15. 1U I 1. ._ 78-93.-3 ---- ---_Z,.-Hutanone t 10. 1U I I_ .71-55-b----.---1,1,.1-Trichloroethane. i 5. IU I L. .56-23-5--- ---- Carbon Tetrachloride_[ 5. IU I I 108. -,05 -4 -------Vinyl AcetateE 1. 10. 1U I 1. .75-27:-4-----.--Bro#Qd.tCbloromthane_L 5. 1U I 1 78-87-_0-------1,2-Dichlosopropane _L. 5. IU I 1.19061-01-0-------cis-1,3-Dichlosopropene;._L_. 5.. IU I I ..._. 79-0.1-.-- _----TUchloroethene 1. 5., 1 U - I I .124-4.9=&-------Dlbramchloroaethane_L. 5.. IU I 1 79.-Q-----7-1,1, 2 -Trichloroethane 1.. 5. 1U I I 71-43t*�-7---Benzene 5. IU I 11006lrO2i----tzans-1, 3-Dichloropropene. ,_L_..I _ 5. 1U I I . _ . , 75-15_-r2_"-----2ro=forn 1_ .. .. 5. 1 U 1 I 108-10-1-------.4-Methyl-2-Pentanone_L__. 10. IU I 1 591-78-b- - -----2-HeXanone I. 10. IU I I 1.27-18-4---.----Tetrachloroethene . [. • 5... 1U I 1 79-34-5-------1,1, 2, 2 -Tetrachloroethane•.,_[ _. _ .. 5. .. 1U I 1 108 -88 -3 -------Toluene L_.. _ 5. IU I [. 108-90-7 ------- Chlorobenzent. 1 _. 5. IU I I _100 -41-4-------Mthylbenzena L .. 5.____. 1 U. I I 100 -42 -5 -------Styrene 1 5. IU I 1 1330 -20 -7 -------Xylene (total) I 1 1 5. IU I I I FORM I VOA 1/87 Rev. ' i 4q lA VOLATILE ORGANICS ANALYSIS DATA SHE" Lab Nasse: INTBCN Contract: 98-D9-0048 Lab Code: INTECK' Case No.: 15466 Matrix: (soil/water) WATER Sample art/vol: 5.0 (g/mL) ML Level: ( loan/med) LOW Moisture: not dec. 100. Column: (pack/cap) PACK EPA SAMPLE NO. I I I BFC55 I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: D1351 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCZNTRATION UNITS: CAS NO. COMPOUND (uq/L or uq/Kq) UG/L Q I t l 1 74 -87 -3 -------Chloromethane I 16. Imo. 1 1 74-83-9 ------- Bromomethane I 10. IU I 1 75 -01 -4 -------vinyl Chloride 1 10. IU- I I 75 -00 -3 -------Chloroethane t 10. IU I 1 75 -09 -2 -------Methylene Chloride t 5. 1 (itI 1 67 -64 -1 -------Acetone 1 10. 1 1 1 75 -15 -0 -------Carbon Disulfide I 5. IU I 1 75-35-4 -------- 1,1-Dichloroethene, - t - 5: 1 U-- I 1 75-34-3 ------- 1,1-Dichlorcethans 1 5. IU I 1 540-59-0 ------- 1,2-Dichloroethene (totalt_r 5. IU I 1 67-66-3 ------- Ch-lorofo=, 1- 5. 1U I 1- 107-06-2 ------- 1,2-Dichloroethane t 5. IU 1 1 78-93-3--------2-Butanone- 1" 10. 1U I I' 71-55-6-------1,f-;1-Trichloroethane _t 5. 1 U- I 1 -- 56-2.3-5-------Carbon-Tetrachloride 1 5. IU I 1 108 -05 -4 -------Vinyl Acetate.. f 10. lu- I 1, - 75-•27-4-------Bromodlchlororthane i-- 5. I u I t ---� 2-Dichloroprogane- _t %. V_ 1 110061-01-5 ------- cis-1,3-Dichloropropene t 5: IU- I .t..' 79 -01 -6 -------Trichloroethene t 5. fu I I. -224-X45-3: -------Dtbrosochlorosethane 1 5. IU I 1 -79-00-90'----k;l,,2-Trichloroethane I 5. IU I 1 71-43------Densenr 5= tU - I 110061-02-#o-7---tz-1,3-Dichloropropene _,t 5a It►I 1 75-29 4 --Brosofors 1 5. 1U. I U 108-10-1-------4-Methyl-2-Pentanoneit- 10: It-- I 1 591-78-6 ------- 2-Neaanone t - 10-:- I tv I 1- 127-18-4 ------- Tetrachloroethene-- 1- 5-= 1 tf'.. I 1' 79-34-5-------1,1, 2, 2 -Tetrachloroethane -=,t- - 5: IU- I r 108 -88 -3 -------Toluene - t- 5- Itf 1- 10&-90-7 ------- Chlorob♦nzene I V 200-41-4 ------- Bthylbensene I 1 100-42-5 ------- Styrene-- 1 1330 -20 -7 -------Xylene (total) 1 I I 5. IU I 1-1 054 FORM I VDA 1/87 Rev. lA EPA SAMPLE No. VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTZCW-- Lab Code: INTECK Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (9/mL) ML Level: (low/med) LOW I I I BFC98 I Contract: 68-D9-0048 I ! SAS No.: SDO No.: BFC39 Lab Sample ID: Lab File ID: D1352 Date Received: 12/ 6/90 Moisture: not dec. 100. Date Analyzed: 12/12/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or uq/Kq) UO/L Q II ! 74 -87 -3 -------Chloromethane I 11. Imo- I 1 74-83-9 ------- Bromomethane I 10. IU I 1 75 -01 -4 -------Vinyl Chloride I 10. IU -I 1 75 -00 -3 -------Chloroethane I 10. IU I I 75 -09 -2 -------Methylene Chloride I 6. I)r L4�- I 1 67-64-1 ------- AaetonN-.. .' . I 10. IU I 1 75 -15 -0 -------Carbon Disulfide I 5. IU I 1 '75-35-4 ------- 1,1-Dichloroethane I 5. IU ! 1 75-34-3 ------- 1,1-Dichloroethane I 5. IU I 1 540=59-0 -------- 1,2-Dichloroethene•(total)_1 2. 1 J I 1 67 -66 -3 ------=Chloroform. " I 5. IU I 1 107=06-2 ------- 1,2-Dichloroethane f 5. IU I 1 78-93-3--- ---- 2-ButanonaF" _ I 10. IU I I 71-55-6-------1,1,1-'trichloroethane- I 5. IU I 1 56 -23 -5 -------Carbon Tetrachloride- I 5. IU I I 108-05-4-------V1nyl Acetate-- I 10. IU I 75-27-4-=-----Bromodich2ororthane I 5. IU I 1 78-87=5-------102-Dich1oropropene _I 5. IU- I 110061-01-5-------cis-1,33=DYchloropropene 1 5. IU 1 ( 79--01-6-------Trichloroethene 1 5. IU I I 124-48-1-------Dibromchloromthane I 5. IU- I I 79-00-W*------2-,1,2-Trichloroethane _I 5. IU I 1 71-4 5. IU 1 110061-0----trans-103-Dichloropropens- 5. I U I I 75-25-4i�------ Brosofors _I 1 5. I U I I 108-10-1-------4-Methyl-2-Pentanone• 10-. IU- I 1 591-78-i= ------ 2-Hexanone I 10.... tU I 1 127-18-4 ------- Tetrachloroethene 2. 1 1 1 1- 79-34-5-------1,1, 2, 2 -Tetrachloroethane- _0 5..-- 1 U I 1 108 -85 -3 -------Toluene- F - S. 1U- I 1 108-90-7 ------- Chlorobenzene 5. IU I 1 100-41-4 ------- Ethylbensene- I - -- S.-- I U.- I 1 100 -42 -5 -------Styrene---- 1 1330 -20 -7 -------Xylene (total) I 5. IU I FORM I VOA 1/87 Rev. 4" 1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET I I I I Lab Name: INTEC9 BFC99 Contract: 68-D9-0048 I Lab Code: INTEC5 Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 5.0 (g/mL) ML Lab File ID: D1353 Level: (low/med) LOW Date Received: 12/ 6/90 \% Moisture: not dec. 100. - Date Analyzed: 12/12/90 i Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 0 I 1 74 -87 -3 -------Chloromethane I 26. I ( I 1 74-83-9 ------- Bromomethane I 10. IU I 1 75 -01 -4 -------Vinyl Chloride I 10. IU I 1 75 -00 -3 -------Chloroethane I 10. IU I 1 75 -09 -2 -------Methylene Chloride I 5. it 1 67 -64 -1 -------Acetone I 10. I I 1 75 -15 -0 -------Carbon Disulfide I 5. IU I 1 75-35-4-------l,l-Dichloroethene I 5. IU I 1 75-34-3 ------- i,l-Dichloroethane ( 5. IU I 1 540-59-0 ------- 1,2-Dichlorcethene (total)_1 5. IU I 1 67 -66 -3 -------Chloroform I 5. IU I 1 107-06-2 ------- 1,2-Dichloroethane I 5. IU I I 78-93-3 ------- 2-Butanone I 10. IU I 1 71-55-6-------1,1,1-Trichloroethane ( 5. IU I 1 56 -23 -5 -------Carbon Tetrachloride_I 5. IU" I 108 -05 -4 -------Vinyl Acetate I 10. IU 1 75-27-4 ------- Bromodichloromethane_I 5. IU I 1 78-87-5 ------- 1,2-Dichloropropane � 5. IU 1 110061-01-5 ------- cis-1,3-Dichloropropene I S. IU I I , 79 -01 -6 -------Trichloroethene I 5. IU I 1 124-48-1 ------- Dibromochloromethane_I 5. IU I I 79-00-!L-.! ------ I 5. IU I 1 71-43-1::� ------Benzene I 5. IU I 110061-02------trans-103-Dichloropropene 5. IU I _I 1 75-25.-..«-----Bromoform I 5. 1U I 1 108-10-Y---- --- 4-Methyl-2-Pentanone_I 10. IU I 1 591-78-6 ------- 2-Hexanone I 10. IU I 1 127-18-4 ------- Tetrachloroethene I 5. IU 1 1 79-34-5 ------- 1,1,2,2-Tetrachloroethane_I_ 5. IU I 1 108 -88 -3 -------Toluene i.. 5. -IU I 1 108-90-7 ------- Chlorobenzene- I_. 5. IU I 1 100-41-4 ------- EthylbenzeneI__ 5. IU I 1 100 -42 -5 -------Styrene I 5. IU I 1 1330 -20 -7 -------Xylene (total) I 1 I S. IU I I I FORM I VOA 0(`, 1/87 Rev. lA VQ&MLE ORGANICS ANALYSIS DATA SHEET Lab Name: INTRCH- Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (q/mL) ML Level: (low/med) LOW t Moisture: not dec. 100. Zolumn: (pack/cap) PACK EPA SAMPLE NO. I 1 I BFF79 I Contract: 68-D9-0048 I 1 SAS No.: SDO No.: BFC39 Lab Sample ID: Lab File ID: D1385 Date Received: 12/ 6/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CONCRNTRATION UNITS': CAS NO. COMPOUND (uq/L or uq/Kq) UO/L p I 1 74 -87 -3 -------Chloromethane I I 19. I 1 1 74-83-9=------Bromomthane I 10. IU 1 75=01 -4 -------Vinyl Chloride (. 10. IU 1 75 -00 -3 -------Chloroethane I 10. IU 1 75-09-2-------Methylene-Chloride I 5. IBJ 1 67 -64 -1 -------Acetone E 10. IU 1 75 -15 -0 -------Carbon Disalfide I 5. IU 1 75-35-4-------1 1-Dichloroethene I 5. IU 1 75-34-3 ------- 1,1-Dichloroethane 1 5. IU 1 540-59-0 ------- 1,2-Dichloroethene (tota-1)_l 5. IU 1 67-66--3-------Chloroform I 5. -IU 1 107-06-2 ------- 1,2-Dichloroethane I 5. IU 1-- 78-93-3 ------- 2-Butanone I 10. IU 1 71-55-6-------1,1,1-Trichloroethane I 5. IU 1 56-23-5 ------- Carbow-Tetrachloride I 5. IU 1 108 -05 -4 -------Vinyl Acetate 1 10. IU 175-27-4 ------- Bromodichlororthane_1 5. IU 1 78-87-5 ------- 1,2-Dichloropropane 5. IU _I 110061--01 -cis-1,3-Dichloropropene ( 5. IU. 1 79-01-�---Trfchloroethene 1 5: IU 1 124-48---Dibromochloromethane 1 5. IU 1 79-00 1,102 -Trichloroethane 5. IU _I I' 71-43-P------9enzene ) 5' IU 110061-02-6 ------- trans-l,3-Dichloropropene_I-. 5. -IU 1 75-25-2 ------- Bromofo=r 1- 5. 1U 1 108-10-1 ------- 4-Methyl-2-Pentanone_j= 10.. AU 1, 591-78-6 ------- 2-Hexanone 1- 10. IU 1 127-18-4 ------- Tetrachloroethens I 5. IU 1 79-34-5-------1, 1, 2, 2 -Tetrachloroethane-- - - 5. - I U 1 108-88-3 ------- Toluene _1---. {-- 5.. IU I 108-90-7 ------- Chlorobenzene 1.. .' S. IU 1 100-41-4 ------- Rthylbenzene lr-- 5. IU. 1 100 -42 -5 -------Styrene 5. IU 1 1330 -20 -7 -------Xylene (total) 1 I 11,00 S. IU 1_ FORM I VOA 1/87 Rev. qft lA VOLATILE ORGANICS ANALYSIS DATA SHS" Lab Name: INTSCN Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) NATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW BPA SAMPLE NO. 0 I I BFC40 I Contract: 68-D9-0048 I 1 SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: D1359 Date Received: 12/ 6/90 % Moisture: not dec. 100. Date Analyzed: 12/13/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS N0. COMPOUND (uq/L or ug/Kg) UG/L Q ° f I 74 -87 -3 -------Chloromethane i 16. I 1 74-83-9 ------- Bromos+ethane I 10. IU I 1 75 -01 -4 ----=--Vinyl Chloride I 10. IU 1 75=00 -3 -------Chloroethane 1 10. IU I 75-09-2-------;MdthyYene Chloride I 6. WLk I I 67 -64 -1 -------Acetone I 10. IU I I 75-15-0-------Carb6n Disulfide I 5. IU I 1 75-35-4-------181"=Dichlordethene I 5. IU I 1 75-34-3 ----- ==1;1=Dichlbroethane ' 1 5. (U I 1 540--59-0 ------ =1,2-Dichlbioethene (total)_1 5. IU( 1 1 5. 1U I I" 107-06-2---=-=-10,'2-Dichloro®thane "" I 5. lu I I-"- 78-93-3----;---2-Bf2tAhona i 10. IU I 71-55-6-----=-1;1,1"-trichloroethane _I 5. IU I I 56-23-5-------CAtb6n Tetiachloride_1 5. IU I 108-05-4----=--Vlhyl'Acetate I, 10. 1U I I , 75-27-4---=---Broslbdlchloromthane�,l 5. 1U I I 78-87-5---_--=I;2-D3chYoropropane 5. IU I' �I 110061-01-5�=--=--ci"s-1,3-Dichloropropane I 5. IU I ----Trichloroethene I 5. °U I I 124-46--V-�-------Dlbsbmochloromthane_1 5. 1 U I I 79 -OW _ --=1,1,2-Trichloroethane_1 ' 5. IU I I 71-43=2`�-------Benzene' 1 5. IU I 110061-02-6-=-----tzans-1,3=Dichloropropene 5. IU _I 1 75-25-2-------Brosafor• I 5. IU I I 108-10-1---- --- 4-Methyl-2-Pentanon " 10. (U 1 591-78-6-------2- Nexanone - ' 1 _ I&.- IU I 1 127-18-4 ------- Tetrachloroethene I 5-0 IU I 1 79-34-5-------1,1,2;2-Tetrachloroethane _I 5. 1U I _ 1 108 -88 -3 -------Toluene I 5. 1U'. I 1 108-90-7-------Chlorobenzene 5. IU I 1 100-41-4 ------- Sthylbenzene I 5. IU I 1. 100 -42 -5 -------Styrene I 5. IU I 1 1330 -20 -7 -------Xylene (total) I 7 1 93 S. IU I 10 1-1 PORN I VOA 1/87 Rev. lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECHI-- Contract: 68-D9-0048 I b Code: INTECH Case No.: 15486 SAS No.: r, r-trix: (soil/water) WATER bample wt/vol: 5.0 (g/mL) ML I vel: ( low/mad ) LORA/ EPA SAMPLE NO. I I I BFC41 I 1 I SDG No.: BFC39 Lab Sample ID: Lab File ID: D1348 Date Received: 12/ 6/90 Moisture: not dec. 100. Date Analyzed: 12/12/90 l lump: (pack/cap) PACK Dilution Factor. 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 4 1 74 -87 -3 -------Chloromethane: I I 47. IIJ, I I 74-83-9 ------- Bromomethane I 10. IU I I 75 -01 -4 -------Vinyl Chloride 1 10. IU -1 I 75 -00 -3 -------Chloroethane I 10. IU -1 I 75 -09 -2 -------!!ethylene Chloride I 5. Imo( , I I 67 -64 -1 -------Acetone I 10. IU "I 175 -15 -0 -------Carbon Disulfide I 5. Iu I I 75-35-4-==----1,1-Dichloroethen4 I 5. lu I 0 75-34-3 ------ -1,1-Dichlosoethano ' I 5. 1U I 1 540-59-0 ------- 1,2-Dichloroethene (total)_1 5. IU I I 67 -66 -3 -------Chloroform I 5. IU 1 107-06-2 -------- I 2. 1 J I 78-93�3------'-2-Hdtianofle I 10. 10 1 I 71-55=6-------1'�i;l'=Trichloroethane 1 5. 1U I I 56 -23 -5 -=-----Carbon Tefzachloside 1 5. lU I 1 108=05-4-------V1ny1 Acetate I 10. lu I 75--2T-4-------9rosiodichlororthane I 5. 1U I I 2-01chlorop=opane I 15. 1 1 110061-01-5=-==-=-cis-1,"3-Dichloropsopens I' 5. IU I I 79-01=6 ------- Ttichloioethene 1 5. lu I i 124-49-3L----==-W1bronochloromethane 1" 5. IU I 79-00-;'g "-'-==-=1,.1, 2 -Ti ichioroethane I 5. 1U I as no 1 5. lu I 110061=02 _--=-=tsaiis-l,3--Dichloropropene _1 5. lu I I 75-25=Woof or* I 5: lu 1 I 108-10-1=- - -- ' 4-;-M@thyl-2-Pentanone 1 10. 16 1 1 591-7'8-6- ------ -2-Hiakanono r 10. lu I 1 127-18-4--= ---- Tetrachlosoethene 1 5. IU I 79-34-5-------1,1,2,2-Tetrachloroethane _I- 5.. 1U I 1 108 -88 -3 -------Toluene 1" 5, 1U, I 1 108-90-7 ------- Chlorobenzene 1` 24-.- I 1 100-41-4 ------- Ethylbenzene t` 5-: 1U I I 100 -42 -5 -------Styrene' 5: IU I 1 1330 -20 -7 -------Xylene (total) I I 5. lu I 1-1 1 020 FORM I VOA 1/87 Rev. lA - BPA SAMPLN N0. VOLATILB ORGANICS ANALYSIS DATA SHEAT I Lab Name: INTE-1 BFC53 Contract: 68-D9-0048 I I ib Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39- Itrix: (soil/water) WATNR Lab Sample ID: Sample wt/vol: 5.0 (g/mL) ML Lab File ID: D1349 vel: (low/med) LOW Date Received: 12/ 6/90 Moisture: not dec. 100. Date Analyzed: 12/12/90 ilumn: (pack/cap) PACK Dilution Factor: 1.00 CONCZNTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 4 Ii 1 74 -87 -3 -------Chloromethane I 26. I I iU, I 1 74-83-9 ------- Bromomethane I 10. IU 1 1 75 -01 -4 -------Vinyl Chloride I 10. IU `I I, 75 -00 -3 -------Chloroethane I 10. 1U I.. 75 -09 -2 -------Methylene Chloride 1 5. I Ulf 1 67 -64 -1 -------Acetone I 10. I t 1 75 -15 -0 -------Carbon Disulfide I 5. IU I 75-35-4-------1,1-Dichloroethene I 5. IU I 1 75-34-3-------1,1-Dichloroethane I 5. IU I 1 540-59-0-------1,2-Dichloroethene (total)_I 5. IU I 1 67 -66 -3 -------Chloroform I 5. (U 1 I 107-06-2-----77,.27DIchloroethane I 2. I J I I 78-93-3-------21_tanone I 10. IU I 1Bu I 71-55-6-----=- ,1,1 -Trichloroethane 5. IU I _I 1 56 -23 -5 -------Carbon Tetrachloride_I 5. IU I 1 108 -05 -4 -------Vinyl Acetate I 10. IU 1 1 75-21-4 ------- BromodichlorosethaneI 5. 1U I 1 78-87-5-------1,2-Dichloropropane 15. 1 I _I 110061-01-5 -------- cis-1,3-Dichloropsopenea I S. IU I I 79 -01 -6 -------Trichloroethene 1 S. IU I 1 124-48-1�-=----DlbzomochloromethaneI 5. IU I 79-00-5:: -®=---1;1, 2-Tilchloroethane •` .__ 5, I U I _I I 71-43- Benzene �-- -- I 5. IU 1 110061-02-- i-- trans-l,3-Dichloropropene 5. IU I _I 1 75-25- '-------ce--Bro■:ofora 1 5. I U I 1 108-10-i ------- 4-Methyl-2-Pentanone_I 10. IU I 1 591-78-6 ------- 2-Hexanone I 10. IU 1 127-18-4 -------- ?etrachloroethene I 5. I.0 I 1 79-34-5 --- ----1,1,2,2=Tetrachloroethane. 5. AU I _I 1 108 -88 -3 -------Toluene I 2. 1 J 1 108-90-7 ------- Chlorobenzene I 23. 1 I 1 100-41-4 ------- Sthylbenzene I 5: 1U I 1 100 -42 -5 -------Styrene 1 5. IU I 1 1330 -20 -7 -------Xylene (total) I 1 I 5. IU I I 1 ;a FORM I VOA 0 3 $ 1/87 Rev. lA VOLATILE ORGANICS ANALYSIS DATA SHEET ab Name: I NTNC3t 'ab Code: INTI=- Case No.: 15486 ..Atrix: (soil/water) SOIL - mple wt/vol: 5.0 ( g/mL ) c Level: (low/mad) LOW EPA SAMPLE N0. I I I BFF66 Contract: 68-D9-0046 i SAS No.: SDG NO.: BFT66 Lab Sample ID-: Lab File ID: A3507 Date Received: 12/ 6/90 Moisture: not dec. 5. _ Date Analyzed: 12/12/90 ^,)lumn: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG a I 1 74 -87 -3 -------Chloromethane I I 11. I I IU I 1 74-83-9 ------- Bromomethane I 11. IU I 1 75 -01 -4 -------Vinyl Chloride ( 11. IU I 1 75 -00 -3 -------Chloroethane l 11. IU I 1 75 -09 -2 -------Methylene Chloride ! 6. WrU.6I 1 67 -64 -1 -------Acetone l 5. 1 J 1 75 -15 -0 -------Carbon Disulfide I 5. _.I IU I 1 75-35-4 ------- 1,1-Dichloroethene I 5. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 5. IU I 1 .540-59-0 ------- 1,2-Dichloroethene (total)_) 5. IU I 1 67 -66 -3 -------Chloroform L 5. IU I 1 107-06-2 ------- 1,2-Dichloroethane I 5. IU I 1 78-93-3 ------- 2-Butanone I 11. IU I 1 71-55-6-------1,1,1-Trichloroethane. 5. IU I _L 1 56-23-5 ------- Carbon.Tetrachloride®t 5. IU I I __108 -05 -4 -------Vinyl Acetate I 11. IU I 1 75-27-4 ------- BromodIchloromethaneL 5.. IU 1 78-87-5 ------- 1,2-Dichloropropane 5. IU _.I 110061-01-5-------cia-1Rj.-Dichloropropene 1.. 5�. IU._ I 1 79 -01 -6 -------Trichloroethene I. 5, _ 1 U. I 1 124-48-1-------Di4s.9-gochloromthane_l 5. ILL I I 79-00----7----1,1,-Z-Trichloroethane 5. (U _l 1 71-43----Bensene I. 5.- IU_ I 110061-02- =--trans-1,3-Dichloropropene 5._ IU I 1 75-25- ._ _L I 5 � IU I ----Bromoform 1 108-10- _ --4-!ethy1-2-Pentanone__1. 11__. fu I I 591-78-6-®----2-Hexanone 0_ lla _. III. I 1 127-18-4-------TetrachlorQethene 1 _ ��. ..I U_ I 1 79-34-5-------1,1, 2, 2 -Tetrachloroethane _. 5....__1 U_ I 1 108 -88 -3 -------Toluene. _l l._ �_.. _-_ 5...-__iU. I 1 108-90-7 ------- Chlorobenzene L. ___&.-tII_ ( 1 100-41-4 ------- Rthylbenzene l _ 5.-.__lU. 1. 1 100 -42 -5 -------Styrene. l_ _ S.- I U. I- 1 1330 -20 -7 -------Xylene (total) I I I 5. IU I I I FORM I VOA 014 4 1/87 Rev. lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTZM Lab Code: INTECA Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 5.0 (g/mL) G Level: (low/med) LOW % Moisture: not dec. 5. Column: (pack/cap) PACK CAS NO. COMPOUND EPA SAMPLE NO. I i I BFF67 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: A3508 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or uq/Kq) UG/KG Q I 1 74 -87 -3 -------Chloromethane I I 1 74-83-9 ------- Bromomethane I 1 75 -01 -4 -------Vinyl Chloride I 1 75 -00 -3 -------Chloroethane I 1 75 -09 -2 ------=Methylene Chloride I 1 61 -64 -1 -------Acetone I 75 -15 -0 -------Carbon Disulfide l 1 75-35-4 ------- 1,1-Dichloroethene 1 75-34-3 ------- 1,1-Dichloroethane I 1 540-59-0 ------- 1,2-Dichloroethene (total)_l 1 67 -66 -3 -------Chloroform 1 107-06-2 ------- 1,2-Dichloroethane 1 78-93-3 ------- 2-Butanone I 1 71-55-6-------1,1,1-Trichloroethane I 1 56 -23 -5 -------Carbon Tetrachloride- 1- 108 -05 -4 -------Vinyl Acetate f- 1 75-27-4 ------- Bromodichloromethane F 1 78-87-5 ------- 1,2-Dlchloropropane -F 110061-01-5 ------- cis-2,3-D1chloropropene- f 1.. 79 -01 -6 -------Trichloroethene �-- 1 124-48-1 ------- Dibromochloromethane-- I 79-00-9r-=----lll,2-Trichloroethane F- 1 71-43l ----- 1 110061-0=-----trans-l,3-Dichloropropene- _I 1 75-2orm - 1 108-1"--"=----4-Methyl-2-Pentanone®) I 591-78-6-=-----2-Nexanone 1 129-18-4 ------- Tetrachioroethene 1 1 79-34-5-------1,1,2,2-Tetrachloroethane--=N 1 108 -88 -3 -------Toluene - �-- 1 108-90-7 ------- Chlorobenzene t�--- 1 100-41-4 ------ -Ethylbenzene f~- 1 100 -42 -5 -------Styrene 1 1330 -20 -7 -------Xylene (total) I I i. 5 11. 12. 11. 11. 6. 5. 5. 51 55. .- . 5. 5. 11. 5. 5. 11. 5. 5. 5. 5-.- 5. 5. 5. 5. 5. 11. 11. 5. 5 5. 5... 5. 5. I I IU I IU I I I IU I I J l IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I IU I lU I IU I IU I IU l IU. I Iu I I U- I IU I IU I 11 FORM I VOA 0 2 0- 1/87 Rev. C lA VOLATILE ORGANICS ANALYSIS DATA EPA SAMPLE NO. SHEET I Lab Name:.INTs- I Contract: 68-D9-0048 I 1 BFF68 I Lab Code: INTNCR Case No.: 15486 SAS No.: SDG No.: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 5.0 (g/mL) G Lab File ID: A3509 Level: (low/med) LOW Date Received: 12/ 6/90 % Moisture: not dec. 2. Date Analyzed: 12/12/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) UG/KG I 0 1 74-87-3 ------- ChloromethaneI I I 1 74-83-9 ------- Bromomethane I 10. 1U ! 1 75 -01 -4 -------Vinyl ChlorideI 10. IU I 1 75 -00 -3 -------Chloroethane 1 10. IU - I I 75 -09 -2 -------Methylene Chloride 1 67 ( 10. I 6. -1 Pd � -64 -------Acetone I 1 75 -15 -0 -------Carbon Disulfide 1 2. I 5. 5 I J I 1 75-35-4------- 1,1-Dichloroethane . IU I 1 75-34-3 ------- 1,1-Dichloroethane I. So 1 5. !U I 1 540-59-0 ------- 1,2-Dichlaroethene (total)_1 5. 1 67 -66 -3 -------Chloroform IU IU I 1 107-06-2 ------- 1,2-Dichloroethane 1 5• IU I 1 78-93-3 ------- 2-Butanone 1 5• '� IU I 1 71-55-6-------1,1,1-Trichloroethane g 1 I 56 -23 -5 -------Carbon Tetrachloride1 5. U 1 108 -05 -4 -------Vinyl Acetatei IU 1 75-27-4------- Hsododichloromethane1 ( 10. IU I 1 78-87-5 ------- 1,2-Dichloropropane 5. IU I 110061-01-5 ------- cis-1,3-Dichloropropene 1 5. 5. IU ! IU 1 79 -01 -6 -------Trichloroethene _I I I 124-48-1.= ------ Dibromochloromethane__I I 5. IU I 1 79-00-!6— �---- 1,1j,2 -Trichloroethane 5. 5. IU ! _1 _-Benzene t-7--trans-103-Dichl0ropropene. . IU ! I - 75-251-Bsomofor• _I1 IU 1 108-10 . 5gIU110061-02- 10. IU I-------4-!ethyl-2-Pentanone IU 1 591-79 6 ------- 2-Hexanone I 1 127-18-4 ------- Tetrachloroethene 1 10.--- 1U I S. 1 79-34-5-------1,1,2,2.-Tetrachloroethane 5,-.1U 108 -IU I I -88 -3 -------Toluene _)-._- 1 1 108-90-7 ------- Chlorobenzene 1- 5, J U I 1 100-41-4 ------- Rthylbenzene 51 IU- I 1 100 -42 -5 -------styrene ` 5.- IU ! 1 1330 -20 -7 -------Xylene (total) I S. IU I 0 I 5. I IU gr)� -1-1 FORM I VOA 1/87 Rev. lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECIN. Contract: 68-D9-0048 &b Code: INTECH Case No.: 15486 SAS No.: witrix: (soil/water) SOIL -ample wt/vol: 5.0 (g/mL) G avel: (low/med) LOW % Moisture: not dec. 15. - Dlumn: (pack/cap) PACK BPA SAMPLE NO. I I I BFF69 I I I SDG No.: BFF66 Lab Sample ID: Lab File ID: A3510 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q I I 1 74 -87 -3 -------Chloromethane i 12. I I IU I 1 74-83-9 ------- Bromomethane I 12. IU I 1 75 -01 -4 -------Vinyl Chloride ( 12. IU I 1 75 -00 -3 -------Chloroethane ( 12. IU I 1 75 -09 -2 -------Methylene Chloride ( 6..I 1 67 -64 -1 -------Acetone I 23. 1 I 1 75 -15 -0 -------Carbon Disulfide I 6. IU I 1 75-35-4 ------- 1,1-Dichloroethene I 6. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 6. IU I 1 540-59-0 ------- 1,2-Dichloroethene (total)_1 6. IU I 1 67 -66 -3 -------Chloroform 1 6. IU I 1 107-06-2 ------- 1,2-Dichlorcethane ( 6. IU I 1 78-93-3 ------- 2-Butanone 1 12. IU I 1 71-55-6-------1,1,1-Trichloroethane I 6. IU I 1 56 -23 -5 -------Carbon Tetrachloride 1 6. IU I 1 108 -05 -4 -------Vinyl Acetate I 12. IU I 1 75-27-4 ------- Bromodichloromethane I 6. IU I 1 78-87-5 ------- 1,2-Dichlorogropane I 6. IU 1 110061-01-5 ------- cis-1,3-Dichloropropene I 6. IU I 1 79 -01 -6 -------Trichloroethene I 6. IU I 1 124-48-1 ------- Dibromochloromethane I 6. IU 79-00-5-r-----1,1,2-Trichloroethane i 6. IU I I 71-43- ---Benzene I 6. IU I 110061-02- = --trans-l,3-Dichloropropene _I 6. IU I 1 75-25 --- Bromoform ( 6. IU I I 108-10-1-------4-Nothyl-2-Pentanone I 12. IU I 1 591-78-6 ------- 2-Nexanone I _ 12. IU I 1 127-18-4 ------- Tetrachloroethene I 6. IU I 1 79-34-5-------1,1,2,2-Tetrachloroethane -j. 6._ IU I 1 108 -88 -3 -------Toluene I 6. IU I 1 108-90-7 ------- Chlorobenzene I 6. IU I 1 100-41-4 ------- Ethylbenzene 6. IU I 1 100 -42 -5 -------Styrene i 6. IU I 1 1330 -20 -7 -------Xylene (total) I 1 I 6., IU I 11 FORM I VOA033 1/87 Rev. 0 44 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET _ I Lab Name: INTIK I BFF70 1 Contract: 68-D9-0048 1 Lab Code: INTECN Case No.: 15486 SAS No.: SDG No.. BFF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 5.0 (g/mL) G Lab File ID: A3511 Level: (low/med) LOW Date Received: 12/ 6/90 % Moisture: not dec. 5. Date Analyzed: 12/12/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 1 C 1 74 -87 -3 -------Chloromethane ( I I 1 74-83-9-------I Bzomomethane 11. IU 1 I 1 75 -01 -4 -------Vinyl Chloride I 1 75 -00 -3 -------Chloroethane 11. I (U11. IU 1 I 1 75 -09 -2 -------Methylene Chloride ( 11. 5. IU 1 I ( 1 67 -64 -1 -------Acetone I I 75 -15 -0 -------Carbon Disulfide I i 15. fu IU j 1 75-35-4 ------- 1,1-Dichloroethene I 1 75-34-3 ------- 1,1-Dichloroethane 5. IU I 1 1 540-59-0 ------- 1,2-Dichloroethene (total),_I 1 67 -66 -3 -------Chloroform 5. 5. 1U I IU I 1 1 107-06-2 ------- 1,2-Dichloroethane I 5. 5. 1U 1 1U 1 78-93-3 ------- 2-Butanone 1 ( 1 71-55-6-------1,1,1-Trichloroethane 11. 5. IU I IU _I 1 56 -23 -5 -------Carbon Tetrachloride__I 5. I 1U 1 108 -05 -4 -------Vinyl Acetate I 1 75-27-4 ------- BromodichloromethaneI 11. 1 IU i 1 78-87-5 ------- 1,2-Dichloropropane I 5. 5. 1U 1 IU 110061-01-5 ------- cis-1,3-Dichloropropene 5. 1 IU 1 79 -01 -6 -------Trichloroethene 1 1 124-48-1 --- ---- Dibromochloromethane_i 5. IU I 79-00- ------- _I � __..__._ 1,1,2 -Trichloroethane I 71-4 ------ Benzene 5. 5. IU 1 IU I I 110061013-*-----trans-l,3-Dichloropropene 5. 5. IU _( 1 75-25-'-*------Bromoform I I 1.08-10-1-------4-Methyl-2-Pentanone__I 5. IU IU 1 591-78-i-------2-Hexanone il. IU 1 127-18-4 ------- I. Tetrachloroethene 11. IU I 1 79-34-5 ----- --1,1,2.,2-Tetrachloroethane�i 5. 5. IU IU I I 108-88-3 ------- Toluene ( 1 108-90-7 ------- ChlorobenzeneI 5. IU _ 1 100-41-4 ------- Zthylbenzene 5. IU I I ...__ 1 100 -42 -5 -------styrene 5. 1U i I 1 1330 -20 -7 -------Xylene (total) I 5. 5. IU I IU I i -.1-1 FORM I VOA 040 1/87 Rev. 1A VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTIM Lab Code: INTECA Case No.: 15486 Matrix: (soil/tater) SOIL Sample wt/vol: 5.0 (g/mL) G Level: (low/med) LOW % Moisture: not dec. 36. Column: (pack/cap) PACK A EPA SAMPLE NO. I BFF71 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: A3512 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (uq/L or uq/Kq) UG/KG Q 1 1 74 -87 -3 -------Chloromethane I I 16. I I IU I 1 74-83-9 ------- Bromomethane I 16. IU I 1 75 -01 -4 -------Vinyl Chloride I 16. JU- I 1 75 -00 -3 -------Chloroethane I 16. 1U-- I 1 75 -09 -2 -------Methylene Chloride I 9. I(_1 1 67 -64 -1 -------Acetone 1 30. I - 1 1 75 -15 -0 -------Carbon Disulfide 1 8. IU I 1 75-35-4 ------- 1,1-Dichloroethene I e. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 8. lu I 1 540-59-0 ------- 1,2-Dichloroethene (total)_1 8. IU I 1 67 -66 -3 -------Chloroform I S. IU I 1 107-06-2 ------- 1,2-Dichloroethane i 8. i IU I 1 78-93-3 ------- 2-Butanone I -@. IA l(, I 1 71-55-6-------1,1,1-Trichloroethane 1 8. IU I 1 56 -23 -5 -------Carbon Tetrachloride I 8. IU 1 108 -05 -4 -------Vinyl Acetate I 16. IU I 1 75-27-4 ------- Bromodichloromethane 1 8. IU I 1 78-87-5 ------- i,2=Dichloropropane 1 S. IU 1 110061-01-5 ------- cis-1,3-Dichloropropene I 8. IU I 1 79 -01 -6 -------Trichloroethene t S. lu I I 124-48-1-------Dlbzomochloromethane I S. IU I 79-00-S-------102,2-Trichloroethane I 8. lu I 1 71 -63 -X -------Benzene. I S. IU I 110061-Wr F------trans-1,3-Dichloropropene 8. IU 1 75-25--2 -------- 01 I 8. lu I. 1 108-10;4 -------- 4-Nothyl-2-Pentanone 1 16. lu I 1 591-78-6 ------- 2-Nexanone I 16. IU I 1 127-18-4 ------- Tetrachloroethene 1 8. lu I 1 79-34-5 ------- 1,1,2®2 -Tetrachloroethane• _1 6. IU I 1 108 -88 -3 -------Toluene I 2. 1 J I 1 108-90-7 ------- Chlorobenzene I 8-. IU I 1 100-41-4 ------- Ethylbenzene I 8-. lu I 1 100 -42 -5 -------Styrene I- 8. lu I 1 1330 -20 -7 -------Xylene (total) I 1 I 8. IU I 1 I 045 FORM I VOA 1/87 Rev. lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTNM Lab Code: INTECN Case No.: 15486 Matrix: (soil/water) SOIL 10 EPA SAMPLE NO. I I I BFF72 I Contract: 68-D9-0048 I SAS No.: SDG No.: BFF66 Lab Sample ID: Sample wt/vol: 5.0 (g/mL) G Lab File ID: A3513 Level: (low/mad) LOW Date Received: 12/ 6/90 % Moisture: not dec. 2. Date Analyzed: 12/12/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q I I 1 74 -87 -3 -------Chloromethane I 10. I I IU I 1 74-83-9 ------- Bromomethane I 10. IU I 1 75 -01 -4 -------Vinyl Chloride I 10. IU I 1 75 -00 -3 -------Chloroethane I 10. IUI I 75 -09 -2 -------Methylene Chloride { 15. wr4j I 1 67 -64 -1 -------Acetone { 46. 1 ` 1 1 75 -15 -0 -------Carbon Disulfide' ( 5. IU I 1 75-35-4s------1,1-Dichloroethene { 5. IU I 1 75-34-3 ------- 1,1-Dichloroethane { 5. IU I 1 540-59-0 ------- 1,2-Dichloroethene (total)_I 5. IU I 1 67 -66 -3 -------Chloroform I 5. IU I 1 107-06-2 ------- 1,2-Dichloroethane ( 5. IU I 1 78-93-3 ------- 2-Butanone ( 12. 1 71-55-6-------1,1,1-Trichloroethane 1 5. U I 1 56 -23 -5 -------Carbon Tetrachloride- I 5. IU I 1 108 -05 -4 -------Vinyl Acetate 1 10. IU I 1 75-27-4 ------- Bromodichloromethane 1 5. IU 1 78-87-5 ------- 1,2-Dichloropropane I 5. IU 110061-01-5 ------- cis-1,3-Dichloropropene- I 5. IU I 1 79 -01 -6 -------Trichloroethene I 5. IU 1 124-48-1 ------- Dibrosochloromethane I S. IU 1 79-00-5;-------101,2-Trichloroethane i 5. IU I 1 71 -434 -=-----Benzene I 5. IU 110061-02;4.-------trans-l,,3-Dichloropropene _1 5. IU I 75-2'.!;:2®-=----IBronofors 1 5. 1U 1 108-10=1-=-----4-Methyl-2-Pentanone { 10...- IU 1 591-78-6 ------- 2-Nexanone { 10. IU I 1 127-18-4 -------- Tetrachloroethene { 5, IU 1 79-34-5-------1,1,2,2-Tetrachloroethane 5.. IU _{ 1 108 -88 -3 -------Toluene { 7. 1 1 1 108-90-7 ------- Chlorobenzene { 5. IU I 1 100-41-4 ------- 13thylbenzene { 5.- IU I 1 100 -42 -5 -------Styrene { 5. IU I 1 1330 -20 -7 -------Xylene (total) 1 1 I 5. IU I 11 FORM I VOA 053 1/87 Rev. I lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INT1IM Contract: 68-D9-0048 Lab Code: INTHCH Case No.: 15486 SAS No.: Matrix: (soil/water) SOIL Sample wt/vol: 5.0 (q/mL) G Level: ( loan/med ) LOW % Moisture: not dee. 9. Column: (pack/cap) PACK EPA SAMPLE NO. I I BFF73 I I I SDG No.: BFF66 Lab Sample ID: Lab File ID: A3514 Date Received: 12/ 6/90 Date Analyzed: 12/12/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (uq/L or uq/Kq) UG/KG Q I I 1 74 -87 -3 -------Chloromethane I 11. I I IU I 1 74-83-9 ------- Bromomethane I 11. IU I 1 75 -01 -4 -------Vinyl Chloride I il. IU I I 75 -00 -3 -------Chloroethane I 11. IU I 1 75 -09 -2 -------Methylene Chloride I 6. IgLt I 1 67 -64 -1 -------Acetone I 10. 1 1- 1 1 75 -15 -0 -------Carbon Disulfide I 5. IU I 1 75-35-4 ------- 1,1-Dichloroethene I 5. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 5. IU I 1 540-59-0 ------- 1,2-Dichloroethene (total)_1 5. IU I 1 67 -66 -3 -------Chloroform ( 5. IU I 1 107-06-2 ------- 1,2-Dichloroethane I 5. IU I 1 78-93-3 ------- 2-Butanone I ii z 1A3 Lk I 1 71-55-6-------1,1,1-Trichloroethane 1 5. IU I 1 56 -23 -5 -------Carbon Tetrachloride I 5. IU I 1 108 -05 -4 -------Vinyl Acetate I. 11. IU I 1 75-27-4 ------- Bromodichloromethane I 5. IU 1 78-87-5 ------- 1,2-Dichloropropane I 5. IU 1 110061-01-5 ------- cis-1,3-Dichloropropene I 5. IU I 1 79 -01 -6 -------Trichloroethene 1 5. IU 1 124-48-1 ------- Dibrosioehloromethane 1 5. IU I I 79-00=S-------1,1,2-Trichloroethane I 5. IU 1 71 -43`=3= ------Benzene I 5. 1U I 110061 -OV -4 -----trans-1,3-Dichloropropene 5. IU _I I 75-251-------Bromoform 1 5. IU I I 108-10=Y=------4-Methyl-2-Pentanone 1 11. IU I I 591-78-6= ------ 2-Hexanone I 11. 1U I 1 127-18-4-------Tetrachloroethene I 5. IU I 1 79-34-5-------1,1,2,2-Tetrachloroethane _I 5... IU I 1 108 -88 -3 -------Toluene I 5. IU I 1 108-90-7 ------- Chlorobenzene I 5. IU I 1 100-41-4 ------- Ethylbenzene I 5. I.0 I 1 100 -42 -5 -------Styrene I 5. 1U I 1 1330 -20 -7 -------Xylene (total) I 5. IU I OG1 FORM I VOA 1/87 Rev. M -- 1A VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH :ab Code: INTECH Case No.: 15486 Matrix: (soil/water) SOIL ;ample wt/vol: 5.0 revel: (low/med) LOW '% Moisture: not dec. 10. '.olumn: (pack/cap) PACK (g/mL) G EPA SAMPLE NO. I I I BFF74 I Contract: 68-D9-0048 I i SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: A3521 Date Received: 12/ 6/90 Date Analyzed: 12/13/90 Dilution Factor,: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q I 1 74 -87 -3 -------Chloromethane t I 11. I I IU I 1 74-83-9 ------- Bromomethane I 11. IU I 1 75 -01 -4 -------Vinyl Chloride ( 11. IU I 1 75 -00 -3 -------Chloroethane ( 11. IU I 1 75 -09 -2 -------Methylene Chloride I 6. I)r L.I 1 67 -64 -1 -------Acetone I 8. 1 J- I 1 75 -15 -0 -------Carbon Disulfide I 6. IU I 1 75-35-4 ------- 1,1-Dichloroethene I 6. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 6. IU I 1 540-59-0 ------- 1,2-Dichloroethene (total)_1 6. IU I 1 67 -66 -3 -------Chloroform 1 6. IU I 1 107-06-2 ------- 1,2-Dichloroethane I 6. IU I 1 78-93-3 ------- 2-ButanoneI . IJd(.l I 1 71-55-6-------1,1,1-Trichloroethane I 6. 1U I 1 56 -23 -5 -------Carbon Tetrachloride I 6. IU I 1 108 -05 -4 -------Vinyl Acetate 1 11. IU I 1 75-27-4 ------- Bromodichloromethane I 6. 1U I 1 78-87-5 ------- lot-Dichloropropane I 6. IU 1 110061-01-5 ------- cis-1,3-Dichloropropene I 6. IU I 1 79 -01 -6 -------Trichloroethene I 6. IU I 1 124-48-1 ------- Dibromochloromethane I 6. IU I 1 79-00-5-------1,1,2-Trichloroethane I 6. IU I 1 71 -43 -1 -------Benzene I 6. IU 1 110061-0T-�® ------ trans-1,3-Dichloropropene 6. tU I 1 75-254; ------- Bromoform _I I 6. IU I 1 108-10-1 ------- 4-Methyl-2-Pentanone I 11. IU I 1 591-78-6 ------- 2-Hexanone I 11. IU I 1 127-18-4 ------- Tetrachloroethene I 6. IU I I 79-34-5-------1,1,2,2-Tetrachloroethane _t 6. IU I 1 108 -88 -3 -------Toluene t 6.' IU I 1 108-90-7 ------- Chlorobenzene j 6. IU I 1 100-41-4 ------- Ethylbenzene 1 6. IU I 1 100 -42 -5 -------Styrene t"" 6. IU I 1 1330 -20 -7 -------Xylene (total) 1 I I 6. IU. I 1_1 oca FORM I VOA 1/87 Rev. L] lA VOLATIL>K ORGANICS ANALYSIS DATA SHEET Lab Name: INTNCH- Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 5.0 (g/mL) ML Level: (low/med) LOW Moisture: not dec. 100. Column: (pack/cap) PACK BPA SAMPLE N0. I 1 Contract: 68-D9-0048 i BFF75 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: D1384 Date Received: 12/ 6/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) UG/L Q I 1 74 -87 -3 -------Chloromethane 1 74-83-9 ------- Bromomethane I I 75 -01 -4 -------Vinyl Chloride ! 1 75 -00 -3 -------Chloroethane 10. 10. IU 1 .IU i I 1 75 -09 -2 -------Methylene Chloride ! 10. 5. IU I IB 1 67 -64 -1 -------Acetone I 1 75 -15 -0 -------Carbon isulfif 75-35-4 ------- 1,1-Dichlosoethene 10. 5. IU1 IU1 75-34-3 ------- 1,1-Dichloro®thane'(t 540-59-0 ------- 1,2-Dichlozoetheneotal)_I� 5' 5. 1U1 1U1 67 -66 -3 -------Chloroform 5. IIII IU1 1 107-06-2 ------- If' 2-bichloroethane_�__I 5. 1U I 1- 78-93-3-------2-Butanons 5. IU I 1 1 71-55-6-------1,1,1-Trichloroethane I 10. 5. IU I IU 1 56 -23 -5 -------Carbon Tetiachloride_�1 1 108 -05 -4 -------vinyl Acetate g. 1 IU 1 1 75-27-4 ------- Bromodichloromethane�_I IU I 1 78-87-5 ------- 1,2-Dichl6z6propane 110061-01=5= cis 1 3-Dichloro ro a-1 ------ - , p pane 5. 5• IU IU I 1 79-01-� Trichloroethene _1_- �----- 5• IU i I 1 124-40--==--Dibsomochlozomethane —'— - 5: IU 1 79-00-==--_1,1,2-Szichloroethani �I 1 71 -43=T -==---Benzene --I 5• 5. IU I IU 110061-02-6-------trans-l,3-Dichloro ro 1 p ane 5• 5. 1U t �! 1 75-25-2 ------- Brosofor■ IU I 1 108-10-1 ------- 4-Methyl-2-Pentanons ! 5. IU I 1' 591-78-6-------2-Hexanona-1 10: IU I 127-18-4 ------- Tetrachloroethene i 10. 1U I 79-34-5 ------- 1,1,2,2 -Tetrachloroethane_!{ 5•- 1U I 108 -88 -3 -------Toluene l---- 5• 108-90-7 ------- Chlorobenzene 5. 1U I 100-41-4 ------- Ethylbenzene ! 5. IU. 1 100 -42 -5 -------Styrene ! S. 1U 1 IU 1 1330 -20 -7 -------Xylene (total) ! 1 n 5. IU I I 1 FORM Y VOA 1/87 Rqv. lA RPA SAMPLN NO. VOLMILZ ORGANICS ANALYSIS DATA SNZZT Lab Name: INTSC» Lab Code: INTRCH Case No.: 15486 Matrix: (soil/water) WATER sample wt/vol: 5.0 Cg/mL) ML Level: (low/med) LOW Ll I I BFF76 Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: D1363 Date Received: 12/ 6/90 t Moisture: not dec. 100. Date Analyzed: 12/13/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATI0N UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L D 1 I 1 74 -87 -3 -------Chloromethane I 5. I J � I I 1 74-83-9 ------- Bromomethane10. I 1Us 1 75 -01 -4 -------Vinyl Chloride ! 10.. IU J I t 75 -00 -3 -------Chloroethane I 10. 1U I 1 75 -09 -2 -------Methylene, Chloride ( 4. IBs I I 67. -64 -1 -------Acetone I 10. IU l 75 -15 -0 -------Carbon Disulfide I 5. IU 1 75-35-4 ------- 1,1-Dichloroethene I. 5. IU I 1 75-34-3 ------- 1,1-Dichlorcethane ! 5. IU I 1 5.40-59-0 ------- 1®2-D1chloroethene .(total)_! 5. IU I. 67-66-3-------Chlorofora 5.. IU I I 107-06-2 ------- 1,2-Dichloroethans I 5. IU I 1 78-93-3. ------- 2-Butanone I 10-. IU I 1 71-55-6-------1,111-Trichloroethane- 5. IU _! 1 56 -23 -5 -------Carbon Tetrachloride_!.. 5. IU 1 1 108-05-4-------Vinyl-Acetate I 10. !U I I.• 75-27-4 ------- Bromodichloromethane__1 5. IU I I. 78-8.7-5- ------ 1,2-Dichloropropane 5.. IU I _t 110061-01**-.------cia-1,3-Dichloropropene 5. IU I _I I 79-0 -----Trichloroethene ! 5. 1U, I 1 124-4 x:---Dibromochlororthane_ 5.. fu I _t_ 1 79.-001,1,2-Tr1chloroethane 5. IU I _I 1 71 -43 -Z -------Benzene ! S. IU. 1 110061-02-6-------trans-l,3-Dichloropropene- 5. IU I _I 1 75-25-2 ------- Brosofora ! 5. IU I 1 108-10-1 ------- 4-Methyl-2-Pentanone_)- le., IN I 1 591-78-6 ------- 2-Hexanone i.._ 10, IU I 1 127-18-4 ------- Tetrachloroethene ! ---. 5. IU I 1 79-34-5-------1,1, 2, 2 -Tetrachloroethane --=t.. _.. 5,-- I U I 1 108 -88 -3 -------Toluene �.---- 3. 1 J 1 1 108-90-7 ------- Chlorobenzene t-- 5. IU I 1 100-41-4 ------- Bthylbenzene t 5. IU I 1 100 -42 -5 -------Styrene I 5. IU I 1 1330 -20 -7 -------Xylene (total) 5. IU I 1 1 -1-1 FORM I VOA 1/17 f?*T* '"I lA BPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET I I I BFF77 Lab Name: INTECM I Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAB No.: SDO No.: BFC39- Matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 5.0 (g/mL) ML Lab File ID: D1364 Level: (low/med) LOW Date Received: 12/ 6/90 Moisture: not dec. 100. Date Analyzed: 12/13/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UO/L Q 1 74 -87 -3 -------Chloromethane 1 10. 1 J 1 74-83-9 ------- Bromomethane I 10. IU I 1 75 -01 -4 -------Vinyl Chloride I 10. IU I 1 75 -00 -3 -------Chloroethane I 10. IU I 1 75 -09 -2 -------Methylene Chloride I 4. IBJ I 67 -64 -1 -------Acetone I 10. IU I I •75 -15 -0 -------Carbon Disulfide- I S. IU I 1 75-35-4 ------- 1,1-Dichloroethene I 5. IU I 1 75-34-3 ------- 1,1-Dichloroethane I 5. IU I 1 540-59-0 ------- 1,2-Dichloroethene (total)_I -67 5. IU I I -66 -3 -=-----Chloroform I 5. IU I 1 107-06-2=------1,2-Dichloroethane I 5. IU I I- 78=93-3-------2-Butanone- I 10. IU I 1 71-55-6-------1,1,1-Trichloroethane 5. IU I �1 1 56 -23 -5 -------Carbon Tetrachloride_I '108 5. IU I 1 -05 -4 -------Vinyl Acetate I 10. IU I I',-75-27-4 ------- Bromodichlororthane_I 5. IU, I I 78-87-5 ------- 1,2-Dichloropropane 5. IU I _I 110061-01-5-i cis-1,3-Dichloropropene I 5. IU I .1 79-01- Trichloroethene I 5. IU I 1 124=4---Dlbroeochloromethanet 5. IU I I 79-00'---10162-Trichloroethane I 5. IU I I 71-43=?ii�-----Hensen t 5. IU 110061-02-6--------trans-i,3-Dichloropropene 5. IU I 1 75-25-2 ------- Bsomofore _I I 5. IU I 1 108-10-1 ------- 4-Methyl-2-Pentanone_I 10. IU I 1- 591-78-6 ------- 2-Hexanone I 14, IU I ( 127-18-4 ------- Tetrachloroethene I 5-:- IU- I 1 79-34-5-------1,1,2,2-Tetrachloroethane--- 5.- IU I 1 106 -88 -3 -------Toluene I 5. IU I 1 108-90-7 ------- Chlorobenzene I 5. IU I 1 100-41-4= ------ Ethylbenzene I 5. IU I 1 100 -42 -5 -------Styrene I 5. IU I 1 1330 -20 -7 -------Xylene (total) 1 - I 5. IU I QSII I 1 FORM I VOA 1/87 Rev. lA BPA SAMPLE NO. VObATTLZ ORGANICS ANALYSIS DATA SHEET - I Lab Name: INTSC>IE I BFF78 1 Contract: 68-D9-0048 I I Lab Code:jNTBCH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water).VATER.: Lab Sample ID: Sample wt/vol: 5.0 (-g/mL) ML Lab File ID: D1365 Level: (low/mod) LOW Date Received: 12/ 6/90 Moisture: not dec. 100. Date Analyzed: 12/13/90 Column: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (uq/L or ug/Kg) UG/L p 1 74 -87 -3 -------Chloromethane I 25. 1 I 1- 74-8.3-9 ------- Bromomethane I 10. IU 1 t 75 -01 -4 -------Vinyl Chloride 1 10. IU I 1 75 -00 -3 -------Chloroethane t 10. 1U I- 75 -09 -2 -------Methylene Chloride I 4. IBJ I F 67 -64 -1 -------Acetone 1 10. IU 1 t 75 -15 -0 -------Carbon Disulfide 1 5. IU I I 75-35-4 ------- 1,1-Dichloroethene 1 5. IU I 1 75-34-3 ------- 1,1-Dichloroethane 1 5. IU I 1--540-59-0 ------- 1,2-Dichloroethene (total) 5. IU I IT 67-66--3-------Chloroform -1 t 51. AU 1 1 -107-06-2 ----- --1,2-Dichloroethane t 5. IU I 1 78-93-3 ------- 2-Butanone F 10. IU I 1- -71-55-6-------1,'1,1-Trichloroethane- S. IU I _1 1--- 56 -23 -5 -------Carbone Tetraehloride__1 g; IU I t108 -05 -4 -------Vinyl Acetate I' 10. IU, I 1 - 75-27-4 ------- Bronodichloromthane___t 5; IU 1 I 78-87-5-------r-;2-Dichloropropane 1 5. -IU I 110061-02-9 .------cis-lj,-3-Dichloropropene 1 5. IU I 1 79--0.1 --Trichloroethene I S. IU I t 124•-4---Dibromochloromethane__I 5--1 U I 2,1,2 -Trichloroethane 5, IU I _1- 1 71-43<-�------Benzene- - 110061-02-6-----.-trans-103-Dichloropropene- 5. 5. I U I IU I I 75-25-2 ------- Bromoforn _I-...- 1 5. IU I I. 108-10-1 -------- 4-Methyl-2-Pentanone_r 10:. IU I 1 591-78-6-------2-Hexanone-- 1----- 10-. 16 1 1 127-18-4 ------- Tetrachloroethene I---- -5-. 1 Lt I I, 79-34-5-------1, 1, 2, 2-Tetrachloroethane_h - 5-. - I U I 1 108-88-3 ------- Toluene-- t- 5-i- I U I 1 108-90-7 ------- Chlorobenzene I 5.. IU I 1 100-41-4 ------- Ethylbenzene- 1 5. IU I 1 100 -42 -5 -------Styrene 5. IU I 1 1330-20-7 -----Xylene (total) 1 I� I 5. IU I 1-1 FORM I VOA 1,07 Rev. lA EPA SAMPLE No. 1i�iA'!I LE ORGANICS P►NAL YS I 3 DATA 9 HgRT I l Lab Name: INTECH Contract: 68-D9-0048 13FF80 1 ;Lab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATZR Lab Sample ID: Sample wt/vol: 5.0 (q/mL) ML Lab File ID: D1367 Level: (low/med) LOW Date Received: 12/ 6/90 t Moisture: not dec. 100. Date Analyzed: 12/13/90 :olumn: (pack/cap) PACK Dilution Factor: 1.00 CONCENTRATION UNITS: COMPOU CAS NO. ND (uq/L or ug/Xg). UG/L I a 1 74 -87 -3 -------Chloromethane I I I 1 74-83-9-------I 8romonethane 15. 1 I I I - 75 -01 -4 -------vinyl Chloride I . 1010 IU _I I.0 1 75 -00 -3 -------Chloroethane I I 1 75 -09 -2 -------Methylene Chloride. I 10. 4. IU I IBJ 1 67 -64 -1 -------Acetone I , 75 -15 -0 -------Carbon Disulfide 10. IU IU II 1 75-35-4 ------- 1,1-Dichloroethane .5. 5. IUDichloroethane . 1 75-34-3-------1,1- I 5. IU I 1 54.0-59-0-- ----- 1, 2-Dichloroethene. Ltotal )`I. 1 67 -66 -3 -------Chloroform 5. fu I I 1 107-06-2 ------- 1,2-Dichloroethane I. 5. 5. 1v 1 IU 1 78-93-3-' 2-Hutanone I I.. 1 71-55-6-a-----1,1,.1-Trichloroethane-..I 10. 5. IU 1 1U 1 56 -23 -5 -------Carbon TetrachlorideI. 1 108 -05 -4 -------vinyl Acetate. ..5. I IU I 1 I - 75-27-4.-------Hromodichloromethane__l.._. ..1.0. 1U 1 1 78-87-5-------1,2-Dichloropropane I 5. 5... lU I lU 110061-01-5 ------cin-1,3-D1chloropzopene._i. . 5.... 1 IU I 79-O1-6rr.-=---- Trichloroethene 1. _ I 124-48-Zii-�--.---Dibromochloromethane__1 5. IU I I 79-00-S=-----1,1,2-Trichloroethane- 5. 5. IU l lU I _I.... 1 71 -43 -2 -®-----Benzene 110061-02-6-------trans-1 3-D1chloro I ro p pane 5._ 5. 1U 1 _1 I 75-25-2 ------- Hzomoform IU 1 I 1 108-10-1 ------- 4-Methyl-2-Pentanone�l _ 5. 1U I 1 591-78-6 ------- 2-Henanone 10. IU I I.. 1 127-18-4 ------- Tetrachlorcethene 10._ 1U I I 1 79-34-5-------1,1, 2, 2-Tetrachloroethane.._1..... 5. 5.. IU I I U 1 1 108 -88 -3 -------Toluene 1... 5.. IU I 1 108-90-7 ------- Chlorobenzene ( 5. IU I 1 100-41-4 ------- Ethylbenzene I 5. IU I 1 100 -42 -5 -------Styrene I 5. IU I 1 1330 -20 -7 -------Xylene (total) I I 5. I IUJLUV I I I FORM I v0A , , Q'7 Qs., ": S iv0lAT1LE"ORGANICS ANALYSIS DATA SHUT 1 Lab Name: INTEM Contract: 68-D9-0048 ! l BFC39 I Lab Code: INT10r, Case No.: 15486 SAS No.: SDO No.: BFC39 Matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 1000.0 (g/mL) ML Lab File ID: B3842 Level: (low/mod) LOW Date Received: 12/ 6/90 t Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/14/90 (SPC Cleanup: (YIN) N pH: 6.3 Dilution -Factor: 1.00 CAB NO. CONCRU"ATION UNITS: COMPOUND (ug/L or uVxg) UG/L p 1 108 -95 -2 -----.--phenol 1 I 1 111=44-4-------bis(2-Ehloroethy2)ether I 10. IU I 1 95-57-8-------2-Chlorophenol .._I 10. IU I f 541-73-1-------1,3-Dichlorobenzene I 10. IU I 1 106-46-7-------1#4-Dichlorobenzene ®1 10. fU I 1 100 -51 -6 -------Benzyl. alcohol -1 10. 1 U I 1 95-50-1-------1,2-Dichlorobenzene f 10. IU I 1 95-48-7 ------- 2-Methylphenol --I 10. IU I 1 108-60-1----T--b1s12-Chl0roisopropyl)ether 1 10. 1U I 1 106-44-5-------4-Methylghenol.10. 10. 1U 1 i. 621-64-7 ------- N-Mit=oso.-dl-n-propylamipe_j 10. lu IU 1 67-72-1 ------- ug"chloroethane.- I I 98-95-3-------sitsobonsene I 10. IU I 1 78-59-1 ------- 3sopJtoxone I 10. 1U I I 88-73-5-------2-Vitrophenolp I 10. IU I I •105-67-9�-s--2„4�Dtmetb 1 henol 1 .10. 1U 1 I 65-85- m-&- somotc acid ! SG. 1U I 111-9)Ca -bjs42_-Mlazoethoxy)ran th 10. I _I t 128-d +WA-$ichlorophenol 1 1 120-t$ 10. IU I IU i --1,Z#4-Trichlorcbenzene1 1 91-2 - •�-Naphthalene 10. PU I I l 166-47!'x....-+Rlosoant i 1ne l 10 l U 1 67-66-3--qam-- hiorobutadione 0� 1D. 1v i 1 59-56-7 ------- 4-gt2oxo-3- -27--=I t�thylphenof 10. I U I i u l - 1 91-57l-4------- 2 Msthyl naphthalens 1 77-47-4 ------- Mexaahl-orocyclolaentadte�l 1®. IU I I 88-06-2-------.le4•i-fttcbloropheno3L_=I 10. l u I I 95-95-4-------2#405-trichlorophenol 5D. 1U t 91-58-7-------Z-Chloronaphthalent:_i� 10r. �IUl ! I 88-74-4-------2-H1troantltne -. Sl150. f U I 131-11-3---- --- Dimethylphthalate l 1 208-96-8 ------- Acenaphthylene• . lU l P 606-20-2-------2,6-Dinitrotoluene 10t. IU I I I 10. IU FORM I Sv-1 1/89 Rev. 1C EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I I I BFC39 I Lab Name: INTIRW Contract: 68-D9-0049 I I Lab Code: INTEC!!F Case No.: 15486 SAS No.: SDG N -o-: BFC39 Matrix: (soil/water) NATER Lab Sample ID: Sample wt/vol: 1000.0 .(g/mL) ML Lab File ID: B3842 Level: (low/mod) LOW - Date Received: 12/ 6/90 t Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/14/90 GPC Cleanup: (YIN) N pH: 6.3 Dilution Factor: 1.00 CONCENTTRATION UNITS: CAS NO. COMPOUND (ug/L or uq/Rg) UO/L Q i I 1 99-09-2 ------- 3-Nitroaniline i 50. 1 I IU 1 83 -32 -9 -------Acenaphthene I 10. IU x I 1 51-28-5 ------- 2,4-Dinitrophenol I 50. IU I 1 100-02-7 ------- 4-Nitrophenol I 50. IU I 1 132-64-9 ------- Dibenzofuran 1 10. IU 1 1 121-14-2 ------- 2,4-Dinitrotoluene t 10. IU I I 94-66-Z- ------ Diethylphthalate. I 10. IU I 17005-72-3-------4-Chlorophenyl-phenylether_I 10. IU I I :86-73-7-------Fi.uozene 1 10. IU I I 100-01-6 ------- 4-Nitroaniline - I 50. IU I 1 534-5.2-1 ------- 4,6-Dinitro-2-methylphenol_I 50. IU I -1 86-30-6 ------- U-Nitrosodiphenylamine (1)_I 10. IU I 1 101-55-3 ------- 4-Browphenyl-phenylether _I 10. IU I I 118-74-1-------Hexnchlorobenzene I 10. IU i 1 87 -86 -5 -------Pentachlorophenol I 50. IU I 1 85 -01 -Q -------Phenanthrene I 10. IU I '120 -12 -7 -------Anthracene 1 10. IU I I 84-7.4-2-------Di-n-butylphthalate _I 10. IU I I 206-4+--6-------Fluoranthene I 10. IU I I 129------PyZene I 10. IU I 1 85-G4WwTv-------Butylbenzylphthalate _1 10. IU I I 91-S4C-k-------3,3k-Dichlorobenzidine_I 20. IU I 1 56-55-3 ------- Benso(a)anthracene 1 10. IU I 1 218-01-9 ------- Chrysene I 10. IU I 1 117-81-7 ------- bis(2-Ethylhexyl)phthalate_I. 2. 1 1 1 1 117-84-0 ------- Di-n-octylphthalate oI_ 10. IU I 1 205-99-2 ------- Benzo(b)fluoranthene_1 IU I 1 207-08-9 ------- Benzo(k)fluoranthene 1_ --10. 10.1U 1 50-32-6 ------- Senzo(a)pyrene I_r . ._ 1U I 1 193-39-5 ------- Indeno (1, 2, 3 -cd) pyrene_t__.__ .10.. _ . _10. 1U 1 1 53-70-3 ------- Dibenz(a,h)anthracene_I 10. IU 1, 1 191-24-2 ------- Benxo(g,h,i)perylene- 1 .1 10. IU I 1 .(1) - Cannot be separated from diphenylanine 1-1 17 FORM I 9Y-2 1/87 _,q 1F SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Names INTEC*-. Contract: 68-D9-0048 Lab Code: INTECIlr Case No.: 15486- SAS No.: Matrix: (soil/water) WATER Sample wt/vol: 1000.0 (g/mL) ML 'evel: (low/med) LOW _ I Moisture: not dec. 100. dec. 0. dxtraction: (SepF/Cont/Sonc) SEPF CPA SAMPLE NO. I I I BFC39 1 I I SDG No.: BFC39 Lab Sample ID: Lab File ID: B3842 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 PC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 2 (ug/L or uq/Xq) UG/L CAB NUMBNR ! I I I I I COMPOUND NAME I RT I EST. CONC. I A 1. -- 1 UNK0OVN 1 5.69 I 10. f J 1 7• -= IUNKNOW' 1 8.56 I 10. I J I 3. 4• 5. 6• 7• S• 9• 10. 12. 13. 14 • ! I I 1 I 15. 16. 1 1_I I I 17. 18. 19. 20. 21. 22. t 1®I I I 23. I Isl I 1 24. 25. 26. 27. 28. 29. 30. FORM I SV -TIC 1/87 Rev. 1B BPA SAMPLR NO. SSMIVOLATM19 ORGANICS ANALYSIS DATA SHNNT BFC54 1 _Ab Name: INTRCH Contract: 68-09-0048- 1 1 -b Code: INTECH Case No.: 15486 SAS No.: SDO No.: BFC39 3atrix: (soil/Mater) WATER aple Mt/vol: 1000.0 (q/mL-) ML revel: (low/med) LOW 3 foisture: not dec. 100. dec. 0. ?,-' Bract i on : (SepF/Cont/Sonc) S8PF 32" Cleanup: (Y/N) N pN: 6.3 Lab Sample ID: Lab rile ID: B3843 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAB NO. COMPOUND (uq/L or uq/Kq) UO/L Q f 108'-95-2----=--Phenal _. I 10. IU i t 111-44-4 ------- bid(2-CAlosoethyl)ethes I' 10. fU I 1 95-57-0 ------- 2-Chlos.ophenol-.. i 10. fU I 1 541-73-1 ------- 1;3"Diachlorobenzene �1 10. IU I 1 106-46-7 ------- 1;4�D1chiorobenzene _I 10. IU f 1 100-51=6-------Bdnzyl`alcohal- ! 10. IU I 1 95-50-1-----==1 2-01chl-orobenzene ._1 10. IU f I 95-48-7----==-2-Nethylphenol I 10. IU I bisf2-Chlaroisopsopyl)other 1 10. fu I t 106-44-5----�-�4-i[ethYlpha'nol I 10. I U I f 62i-64-7-=l-=--N-MitYoso-df-n-piopYla�ina_t 10. fu f t 67-72-1 ------- Aeuachlotoethaao 1 10. IU 1' 98-95-3-----=-NlCtsolsiaesins I 101. fu I I 78-59-I-------IsophozoA�. I 10, IU 1 1 88-75-5------ 62-Nitsophencl 1 10. fu I f v105"67-9-- ---- 2#4:-01rthylphenol 1 10. fu I f 65-85-0=-----=lzoic acid I 50. IU I I 111-91-1---'bls(2-Chlosoethoxy)uethane_I 10. IU I t` tchlosophenol t 10. IU 1 ' 120-82--;- 1, 2; 4-Trichlorobenzene_I 10. fu I 1 91-20-9- thaldne: t 10> 1U i I 106-47-6-----ChlaroanilIng I 10. IU I 1 87-68-3 ------- Hexachlorobutadiene rt 10. IU I 1 59-50-7 ------- 4-Ch=oro-3-methylphenol ._I 10.e -IU- i 1 91-57-6 ------- 2-fethy1naphthaleno _t. 10.- IU- I 1 77-47-4 ------- Nexachlorocyclopentad lone - _I 10.1 f U l i I 86-06-2-------2,4,6-Trichlorophenol 10. IU I 1 _t 95-95-4 ------- 2,4,5-Tricblorophenol 50., IU I 1 _,..I, 91-58-7 ------- 2-Chlosonaphthalena I 1d. IU 1 88-74-4 ------- 2-Nitroanilint I 50. IU 1 131-11-3 ------- Dimethylphthalate 1 10. IU I 208 -96 -8 -------Acenaphthylene I 10. IU ! 606-20-2 ------- 2,6-Dinitrotoluene I 7 14. tU I FOR 1 SV -1 Iq 1C SBMIV0LATILB ORGANICS ANALYSIS DATA SHMT Lab Name: INTIKW Contract: 68-D9-0048 Lab Code: INT=. • Case No.: 15486 SAB No.: Matrix: (soil/water) WATBR sample wt/vol: 1000.0 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. 100. dec. 0. Bxtraction: (SepF/Cont/Sonc) szPF EPA SAMPLB NO. I I L BFC54 1 I I SDG No.: BFC39 Lab sample ID: Lab File ID: 83843 Date -Received: 12/ 6/90 Date Bxtracted:..12/ 6/90 Date Analyzed: 12/14/90 GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.00 CONCRNTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Rg) UG/L p I I 1 99-09-2 ------- 3-Nitroaniline I 50. I I IU I 83-32-9 ------- Acenaphthene. I 10, IU I 1 51-28-5 ------- 2,4-Dinitrophenol I 50. Au I 1 100-02-7 ------- 4-Mlirophenol_ I 50. IU I 1 132-6.4-9 ------- Dibenzofuran I 10. IU I I 121-14r-2 ------- 2,4-Diriitrotoluene t 10. IU I I 84-66-2 -------- Diethylphthalate 1 10. 1U I 1 7005-72-3 ------- 4-Chlorop 10. IU I I 86-73-7 ---- ---Fluoreni I 10. IU I I' 100=01-6�-==---4=NitrosnilIna 1 50. IU I 534-52-1=------4,G-0initso-2-methyiph*no1_,,,I 50. i.0 I I 86-30-6-------N-Nitsoaodphen�rla�ine (�)._I 1 101-55-3 ------- 4-Bromophenyl-phen keithnr 10. 10. U. I IU _1 1 118-74-1--- ---- Nexachlorobenzene F 10. iU I 1 87 -86 -5 -------Pentachlorophenol I 50. IU I 1 85 -01 -A -------Phenanthrene I 10. IU I 1 •120 -12 -7 -------Anthracene I 10. IU. I 1 84-74-2 ------- D1-n-butylphthalate I 10.. IU I 1 206-44-0-- ----- Pluoranthene i 10. IU I 129-OQ�___Pyrene I 10. IU I 1 85-6- Butylbenzylphthalate®I. 10. IU I I 91-9#Zf"-----3,3*-Dichlorobenzidine_1 20. IU 1 56-55=3Benzo(a)anthracene 1 10., IU I 1 218-Oi-9------- chrysene I 10. IU I 1 117-81-7 ------- bis(2-=thylhexyl)phthalate_I 3. 1 1 1 1 117-84-0 ------- Di-n-octylphthalate 10.. IU I _I 1 205-99-2 ------- Benzo(b)fluoranthene_ 10. IU I 1 207 -08 -9 -------Benzo M flnoranthens- 10. IU I 1 50-32-8 ------- Benzo(a)pyrens I 10. IU 1 193-39-5 ------- Indsno(1,2,3-cd)pyreneF 10: IU I 1 53-70-3------i-Dibenz (a, h )anthracene N. 10. I U I 1 191-24-2 ------- Benzo(g,h,i)perylene I 10. IU I (1) - Cannot be separated -from diphenylamine FORM I SV -2 213 1/87 Rev. IF SEMIVOLATILN ORGANICS ANALYSIS DATA SHEET -TEY AVIVRLY IDENTIFIED COMPOUNDS lib Name: INTI-' Contract: 68-D9-0048 Lab Code: INTIM' Case No.: 15486- SAS No.: 1 itrix: (soil/water) WATER ®-Iople wt/vol:, 1000.0 (g/mL) ML '<,-dvel : ( low/med) LOW _ Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sonc) SSPF EPA SAMPLE NO. I I BFC54 I I i SDO No.: BFC39- Lab Sample ID: Lab File ID: B3843 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 C Cleanup: (Y/N-) N pH: 6.3 Dilution Factor: 1.00 CONCENTRATION UNITS: umber TICS found: 2 (ug/L or ug/Kg) UO/L CAB NUMBER 1 I. COMPOUND NAME t RT I BST. CONC. I 0 1 sasssssassssssstssssssss�sssasssssssssssassslsasssssslssssssssssssslsssssl 1. -- 1UNKNOW- I 8.56 1 10. 1 iv I 2. -- IUNKNOVK I 11.96 1 8. 1 1 1 3. i 4. I I it I I i 5. 6. I I f I I 7. 9. 1 f I I I 10. I I I I I 112. 13. t I I t I I 14. 115. 1 I t I I 16. t I I I 17. I I I I I 18.- 8.19. 19. 20. 1 I I I I i 21. 22. 1 23. l 24. 1 25. 1 26. 1 27. 28. 29. I I_I I 1 30.211. FORM I SV -TIC 1/87 Rev. SIlfLa ORGANICIR NAXiYSIB DATA SHZRT- aPA SPLs NO. _ab Name: IINTat;- I 1 D9 Contract: 68__ I B�Css I mb Code: INT>H 0048 I Case NO.: 15486 S I Matrix: No.. ter) yA SD(; NO-: BrC39 (soil/!+a ample Wt/vol:Lab SaAple ID: 1A00.0 (VML) ML Level:- (lor/med) Low_ Lab 1ptle ID: 83844 I' Moisture: notdecDate Received: 12/ 6/90 . 100: dec. 0. S traction; Date attracted: 12/ 6/90 (SePP/Cont/Sonc) Sapp ,IFC Cleanup: Date AnalYzed: 12/14/90 (Y/N) N PH.*. 6' 5 Dilution >ractor: 1.00 CAB NO. COypOUN& "co"c" 'R"rom UNITS: i (uVL or WKS) UO/L i• 10a-9S_2_____-••phenaiI - I111-44-4------_bfst?=Chiosoathyl)et I 10. IV 1- I 95-57-8------- 1 541-73-1--_____l,`MIDorophenol. hes �i 10. IU ! .106-46-7_____-- chlosobensene �_I 10. IU I I 100-51-6------- . .01chlosobensens ��f 10. IU 1 95_50-1__--_-�Htnxyl•alcohol 10. IU I 1 95-48-7__----_l•2-Dfchlosobeii I 10. !U I 1 10a -6Q- 2-Methylphenol -1 10. Ju I osois - � 10. I 106-4l-5----®__4._1 opsoDYl3rthes 1 IU 1 I 6'21-64-7--=--- ifl®?enol I 10. !U I 1 67-72-1------��fosQ- -n-pzoPYlasine 10. IU I 1 9a-95-3 ------- Xii Xaft1a'aethane -I 10. fu I I• 78-59-1-----troftnsene 1 10. IU ! 1 88-75-5-------Isom=one 1 10. IU I 1 "103-67-9 ------ 2-Nittophlinoi I 10. IU I I 65-85-0-- ------2 i* *`18isrthylPhenol I 10. I U I I 111-91+1�.--Mos°fes acid I 10. I U I i 120-83#sr2fosoethoxy)sethane I 50. IU I I 1 120-82-Z_ _ •"iehloropheeol -10. !V I 1 9i -20 -wry 4`#chlosobensene 10. I V I 1 106-47- ~-lhalens -t 10. iu I dw--�`Ch2oroanfline - I 10. i chlosobuta�iene _ 1D. I V 1 59_"-7 ------- 4-Ch2oso- _t I J 91-57-6-------2-Meth l.na PAene1 _�I - - 10. 1 V- I 1 77-47-4------- -- 10. I m xachlosocyclolene -� 10. 1V 1 �ntad�ien� 10. 9s-9s--------24`0-?Sicblosophenol•.;- - IV - 92 -56-7 V' 1 92- ?•+•S'='tichlosophenol 1 10.. 1t1' 1 Sa-7---___-2-Chloso,ta -tet 88-74-4-- _ Phthalene _ -- 5W. I u " I 131-11-3- _ 2 sftsoanfl-ln' -I ✓_ 10. IU I -----Dirthyiphthalate 20a-96-e-------Acenaphthylb�. I .606-20-?-- - 1-0 • i U I 2�-6 Dinittotolnene I 10. - iV I ��2 n 10. IV I �v. y 7AW- SRMIV0LA?ILX- 1C ANICB ANALYSIS DATA SHZRT Lab Naso: Contract: 68-D9-0048 Lab Code: INTIM Case+No.: 15486 yatrix: (soli/.water) WATER Sample wt/vol: 1000�Q (q/mL) ML revel : (lod/rd) LOW % Moisture: not dec. 100. dec. 0. .extraction: (SepF/Cont/Sonc) Stipp ;PC Cleanup: (Y/N) N pH: 6.5 NPA SAMPLR NO. I I I BFC55 I I SAS No.: SDO NO.: BFC39 Lab Sample ID: Lab pile ID: B3844 Date Received: 12/ 6/90 Date extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CAO NO.CONCRUTRATION UNITS: COMPOUND' (uq/L or uq/lKq) Ua/L 1 G 1 99-09-2 ------- 3-Nitroaniline j .1 83-32-9-- I ---r--Acenaphthene_f .A 51,25-5-------2,4-®initrophenol_ S 0. 50. IU IU I I I 100-02-7------=4-Nitrophenol 50. IU I I I 132-64-9---- "--benzofuran 50. IU f I 121-14-2-------2,4-Dinltrot Oldene f 10. I U I 1 8.4-66-2-------Dlethylphthalatt -! 10. IU I I 1 7005=72-3-=---=-4-Chloro 10. 10. I U f- -.*nyl-phenylether_I I 86-73-7----===pl:uosine IU I f 100-01-6----=--4->llitioanilIng 10. fU I I I S34=S2-1------- 4,6-dinLtro=2-rthYlphenol_I 50. 50. IU I 86-30-6------- �Nitrosodiphenylaaina My- 1 IU 1 101-55-3 ------- 4-Broiophenyl-phenylether- 10. 10. I U i _I 1 118-74-1------=Rexachlordbenxene- IU 1 V -87-86-5 ----- --PentaoAloropheno2 10. IU I I 1 85 -02=8 ------=phenanthrene r 50. IU I I s 120-12"'-T-----v-Ant>Rsacene 10. 1U 1 1 84-74-2' =-- I -�°-- gf-i�batylphthalate '206-44- 10-• 1U 1 1 I "Wrizasanthene I _7=-"r*6G 10. 10. tU I tU 1 129-0 1 85=6A" J 1 -/atylbenxyIphthalat• i9' I IU 1 f 91-9I �=-3', 3'-Dichlorobenxidin �1 I 56-SS-31~==-=-Bbnzo(a)anthraceneI 10. 20'. fU 1 U I I 218-01-9=«---Ys�ene - 10 -. IU I --I 1 117-81-7-----bia(2-sthylhexyl)phthalate_I 10: I U I 1 11.7-84-0 ------- 0i-n-octylphthalat• I. 205-99-2-------Bensoib)fluoranthene--_ _ 1 207 -08 -9 -------Benzo KIK) fluorantheni I - _ 10-• f u I I 50-32-8-. Benxo(a)pyrene I--- 20: - tU I 193-39-5- ,,-cd)pyrene_ i0- �VI 1 53-70-3-------Dibens(a,h)anthracene- I 191-24-2- ------Benzo ( h i) _� __. 9. . perYlene___f- 10':- I u I 1 10. Iu I W - Cannot be s• parated fres d3phenylaainr- --- 221 FORM I SV --2 1/87 Rev. L] 9 SZMIVOLATIL= ORa"ICSFANALySIS DATA SHN" , T`ATIVSLY IDSNTIFIRD COMPOUNDS Lab Name: Imo -- Lab Code: INTNCW Contract: 68-D9-0048 Case NO.: 15486 SAS No.: fatrix: (9011/water) WATER Sample wt/vol:. 1000.0 �Pevel: (low/med) LOW Moisture: not dee. 100. _xtraction: PC Cleanup: (q/mL) ML dec. 0. (SepF/Cont/Sone) SEpF (Y/N) N PN: 6.5 EPA SAMPLE NO. I I BFC55 l I I SDO NO.: BPC39 Lab Sample ID: Lab bile ID~: B3844 Date Received: 12/ 6%90 Date Extracted 12/ 6/90 Date Analyzed: 12/14/90 Dilation Factor: 1.00 Number TICS found: 1 CONCENTRATION UNITS: (uq/L or uq/Kq) UO/L I I CAS NUMBER gas:s::ss:ss:s-sl-smsssss:ssssssts:ss:asEST.saOsasslasOasl I COMPOUND NAM! I I I I 1 I RT • - 1 UNKNOV e., 1 2. I f 8.57 I 10. I J N I 3. 4._ I I 7: I I l I 1 90 I I l --- l0. I l 1 I i ! I— —�I f f 13. I —I L4. • l f �—I I � I 16. 1�— I ISI 7. I l I_I 1 19. --I I I-- f i 22.- 2.4. 4. 26. I 1 7. I I 1 ---f I —1 �1®I 29. - FORM I SV --TIC e_I � 1/87 Rev. 1B EPA SAMPLE No. SRNrVMMILR ORGANICS ANALYSIS DATA SHEET I i Lab Name: IN?zm Contract: 68-D9-0048 I gFC98 I I Lab Code: INTSCH Case No.: 15486 SAS No.: SDO No.: BFC39 .4atrix: (soil/water) WATER Lab Sample ID: 3ample wt/vol: 1000.0 (g/mL) ML Lab File ID: B3845 Level: (low/mad) LOW Date Received: 12/ 6/90 Moisture: not dec-. 100. dec. 0. Date Extracted: 12/ 6/90 Rxtraction: (SepF/Cont/Sonc) 3EPF Date Analyzed: 12/14/90 IPC Cleanup: (YM N pH: 7.4 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND~ (ug/L or uq/Kg) UO/L Q 1 108 -95 -2 -------Phenol I 1 10. I I IU I 1 111-44-4 -------- bis(2-Chloroethyl)ether f 10. IU I f 95-57-8-------2-Chlorophenol I 10. IU I 1 541-73-Yi --------1,3-Dichlorobenzene 10. IU I 1 106-46-7-------1,4-Dichlorobenzene 10. IU I _1 f 100 -51 -6 ----=--Benzyl alcohol I 10. IU f I 95-50-1-------102-Dichlorobenzens 10. IU I �i 1 95-48-7 ----- --2-Methylphenol I 10. fU I I" 108-60-1------=bis42-Chloroisopropyl)ether 1 10. IU i 1 106-44-5 -------- 4-Methylohnnol I 10. IU I f..621-64-7-=--=--N-Mltzoro-di-n-propylamine_l 10. IU I f 67-72-1 ------- Ilexachloroethane. 1 10. IU I 1: 98-95-3 -------- 91trbbenzene I 10. IU I f 78-59-1 --------I 10. IU I F 88-75-5-=-----2-*1tzopheno1 I 10. IU I V 205-67-t----i=--2j,4-Dlmthylpheno3L 1 10. IU I I` 65-85-0-----=sensotc acid I 50. IU I 1 111=9 -----bls#2-Chloroethoxy)s:sthaae_1 `� 10. 1U I F 120-82 --2f4-Dichlorophenol I 10. IU I 1 120-8 ---i;l,4-Trichlorobenzen 1 10. IU I 1 91-20 --ba"thalene I 10. 1U I I 106-47-ice-----4-MISroaniline 1 10. IU I U 87-66-3=-=----ffemahlorcbutadlone 10. IU I _1 I 59-50-7-------4-Chloso-3-nothylphenol 10. IU I _I 1 91-57-6-------2-Methylnaphthalene 10._A U I _1 1 77-47-4 ------- Hexachlorocyclopentadiens 10. IU I ,_I I 88-06-2-------2;4,6-Trichlorophenol 10. IU I _1 1-95-95-4=------2,4,5-Trichlorophenol•�1 .50. IU I 1 91-58-7 ------- 2-Chlbronaphthalene 10.. IU 1 _1 I 88-74-4-------2-Nitroaniline. 1 50. IU I 1 131-11-3 ------- Dimthylphthalate i 10. IU 1 208 -96 -8 -------Acenaphthylene 1 10., IU I 1 608-20-2 ------- 2-;6-Din1trotoluene 0 1 _ 10. IU I 1_927 I I FORM I Sv-1 1/87 Rev. 1C SBMIVOLATILB ORGANICS ANALYSIS DATA SHEBT Lab Ham: I NT2 Lab Code: INTBC, Case No.: 15486 Matrix: (soil/rater) VATBR Sample wt/vol: 1000.0 (g/mL) ML Level: (low/aged) LOV �► SAMPL8 No. I BPC98 Contract: 68-D9-0048 I I SAS No.: SDO No.: BFC39 t Moisture: not dec. 100. dec. 0. Extraction: (SepP/Cont/Sonc) SBPF GPC Cleanup: (YIN) N pH: 7,4 Lab Sample ID: Lab bile ID: B3845 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CONCRNTR"r off UNITS: CAS NO. COMPOUND (ug/L or.ug/Rg-) u0/L 4 I . 99-09-2 ------- 3-Nitroaniline IVI 1 83 -32 -9 -------Acenaphthene I 10. lu IU 1 1 51-28-5 ------- 2,4-Dinitrophenol I S0. IV I 1 100-02-7-------4-Nitzophunol� I 50. IV` I 1 132'-64-9 -------- I 10. IU I I 121-14-2 ------- 2,4-D1nitrotoluene I 10. IU I 1 84-66-2 ------- 6lothylphthalate I 10. IU I 1 7005-72-3----=--4-Chlozophenyl-pltenylether_I ' 10. IU I I Ii6-73-7--- -Pluoraeif I 10 . I U I I 1.00-01-6----==-4=liitsoani l i 1 50. IV I I 534-52-1----== -f,6-Din1tro-2-eethylphenol_I 50. IV I I 86-30-6----=--N-W tso®odiphenylamine (1)_I. .T- 10, IV I 101-.55-3-------4-Bromophenyl-phenyiether 10. Iu I _I I 118-74-1-------H*xachlorobenzene r 10. IU I I 87 -86 -5 ------=Pentachlorophenol I 50. IU I I 85-01-8-------Phenanths�ne f lA. IU I 1 X120-12-7-----=-Anth=aconeI. 10:' IU I 1 84-74-2 ------- bi-n-butylphthalate 1 10. IV I I 206-44-0=r---;�Juosanthene I_ 10. fu I I 129-0 - Pyrans 10. IU I _� 8i_?7_ -_ 3ot3 1� nzylphthalate__,I_ 10. IU I ichlosobanzidine__I 20. IU I Btnso(a)anthracene t 10e,, IU I I 218-02-90----=-Chsyzann j lu I I 117-81-7-------bi�(2-EthyihexyZ)phthalate_t _10. �_ 3. 1 J I .1 117-84-0--- ---- Di-n-octylphthalate M10Q__ IU i __I_.. 1 205-99-2-------Benzo(b) f luosanthenfI 1 287-06-9 _ 10. IU I ------- Benzo(k)fluoranthene 1� ! SO -32-8 ------- Benso(a)pyrene I- 10. "IU - 10. 1 1U I 1 193-39-5 ------- Indeno(1,2,3-cd)pyreneI 1A. 1U I I 53-70-3-------Diben=(a,h)anthracene 10. IU i __I 1 191-24-2 ------- Benzo(g,h,i)perylene__I 1®. IU (1) - Cannot be separated from diphenylamtne > I SV -2 228 1/87 Rev. lF )LATILE ORGANICS ANALYSIS DATA SHEET TMTATIVZLY IDENTIFIED COMPOUNDS P,p too*.� - � Contract: 6.8-D9-0048 .0, Code: INTNM Case No.: 15486 SAS No.: ,,trix: (:to i 1/water ) WATER sample wt/vol:. 1000.0 (g/mL) ML Gavel: (low/mod) LOW _ 1 Moisture: not dec. 100. dec. 0. dxtraction: (SepF/Cont/Sons) SEPF BPA SAMPLE NO. I 1 I BFC98 I 1 1 SDG No.: BFC39 Lab Sample ID: Lab File ID: 83845 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 IPC Cleanup: (YIN) N pH: 7.4 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 1 (ug/L or uq/Kq) UG/L CAS NUMBER 1 1 1 1 I r COMPOUND NAME I RT I BST. CONC. I Q I ■asaasasasssasss•Issasssssasasssasssaaassssasslssssassalasaaasasassssltam st 1. - - IUNRNOWl1 8.56 I I 2. 1 3. 4. 5. 6' 7. 1 1 I 8. I I 9' to . 11. I 1_I 12' I I 13. 14. 15. 16. 17. 18. 19. 20.- 0.21. 21. r • I I t 22. _! 23. 24. 25. I 26. 1 27. I 28. I 29. I 30. I_I I t I . FORM I SV-T1C. 1/87 Rev. 40 :f'K BENIVOLATiLE1B . OltQANICS'ANALYSIS DATA SHm 'jab Nam-. -INTECtI< Lab Code: INTNCH Contract: 68-D9-0048 Case No.: 15485SAW No.: latrix: {doll/`crater) WATER Oammple vt/vol : 1000.0 ' (VML) ML revel: (lov/mored) LOW Moisture: not dec. 100. dec. 0-, Nxtraction: (SepF/Cont/Sonc) SEPF PC Cleanup: (YIN) N PH: 7.5 CAB NO. NPA SAMPLs NO. P 1 I BFC99 I 0 I SDG NO-: BFC39 Lab Sample ID: Lab bile ID: B3846 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 COMPOUND "'w"1-011TRATIOK UNiTs: (uq/L or 319/Rq) Ua/L Q I 108 -95 -2 -_---::Phenol-.. 1 I I . 111 -44 -4 --_-;.._bis (r-Chloroethyl) ethe 1 10. 1 U 1 95-!57-8"-""2-C hlorophenol 1 10. Iu i I 541-73-1--- 1,3-Dlchiorobensene 1 10. fU I I 106-46-7----___4 4 -Dichlorobenzene fU 1 I 100-51-6----,__eensyl'alcohol 1 10. Iu I I 95-50-1---___1,2_D1chlorobensene 1 10. IU I 1' 95-48-7----=--2-kethylphenol. 10. Ju I I 108-60-1-- :=�bist2'Chloroiso 10. IU I I 106-44-9----- 4_Methyiphene� p opyl)e hes I 10. Iu I 1 621-64-7----_--N_Nltwono-din 1 10• IU I I 67-72-1-----__Hexacltloroetn-IKopylam nene,_I 10. I U I 98-95-2----__'Nitropin;ene 1 10. IU I I 7a-59-i----� I 10. I I 88 -7s -S--_-:__ Isopho:onv--.. l u I •105-67-9---®---2-Nitiophenol. 1 10. Iu I 2' 4-Dlmethyiphenol I iQ._ Ju I 1 111-91-1-e•, .,..�_>�ata- acie- 1 'T. 1 u I btnrjZ-Chloroethox 1 r0: lu I 1 120-83- Y)methane_I . 10`. I U 1 I 120-8T�-a'_�Dichlorophenol "�"`1.1.4-Trichlorobensene F i0: _ I U I 1 91-20-3=-., -j"' 10: 1 u I I . 106-47-E--M-N4-ftlorea:atl1ne 1 10.. I u- I 187-68-3--_:___Rexachle:obntadiena 10• IU I 59-50-7-------4-Chloro-3-a�thylphene2 0 100< IU I I 91-57-6�------- 2_Nothyinaphtltalene �I 10. 1 97-47-4------- I U I H, 41 v l oz ocycl opentadi eea ! 101P I u I 1 88-06-Z-------Z•4.6_Trichlosopheno2 --� 10 IU. I I 95-95-4-------2,4,s_Trjch20ro 1._ 16: ; IU. I I 91-58-7 ------- 2-Chloronaphthalneoi 1 S0:'_ 1 U.I t 88-74-4'-------2-111-tsoanillne -I 10; IU 1 I 131-11-3 ------- Dimethylphthalate 10.E IU. I I 208-96-8 ------- Acenaphthylenw I �fuI 606-a0-2----- I --2�6-DinitrotoluI I IU I 1 i3 1 G IU I I __I FOR" BV1 IC SEMI90LA?ILE ORGANICS ANALYSIS DATA SHEN? Lao have: INTSM Lab Code: IN?!C!! Case No.: 15486 Matrix: (soil/water)- WATER Contract: '66-D9-0041' NPA SAMPLE NO. 1 I DFC99- I SAS Na.: SDQ No.: SVC" Lab Sample ID: Sample wt/vol: 1000.0 (g/mL) ML Lab File ID: B3846 Level: (low/rid} LOW - Date -Received: 12/ 6/90 t Moisture: not Sec. 100. dec. 0. Diti Extracted: 12/ 6/90 Extraction: (Sept/Cont/Sonc-) SEPT Date -Analyzed: 12/14/90 GPC Cleanup: (Y/N) N pH: 7.5 Dilution Factor: 1.00 CONCENTRATION, UMTS: CAB NO. COMPOUND (ug/L or ug/Kg) UGA 0 i 99-09-2 ------- 3-Nitroaniline 1 50• I I 1 -83-32-9 ------- ACenaphtheie ' ' * .; 1 10. I; I ' I 51-29-5 ------- 20"4-Dinitrophenol I 50. 1 E I - I. 104-02-7-----=-4-Nitiophenol t 54. IV I 1 132-64-9-------D•ibensstusan 1 10-. IV I I 121-14-T------2>4-Dllnitsotolnene 1 ls. IU I I 84-66-2-------Dietl►ylphthalate- - t -- 10. I U- f 1 7005-T-1-3 ------ -4-Cb-losophenr1-phfnylethet=f• 1016 IU 1- -- I lint 1 86-34-8-------I�Mf�sosoeiiphenyla�f•ne-41D=1-�m --..... 1a.-.- IU_ I 1 101-55-3 ----- —4-asomophenyl-phenyletheL­ IV. I I 114-74-1-=-----Hekach2osobensene--- ! -- 10-.- 1U -- -* I- I 87-86-S------.-Pentachlosophenol--- - l- —-50. IU. I ! 1. 85-41-8----w-Phenanthsener 10, Iv- I 1' 124-].�---•8atl�saeene I 10-: IV I " 1 1 i�----- Dt-e-botylphthalate--_I~ - ls, IU,- I I 2-----Flsoxanthene ! 10r �.. 1 -=On& ! _ -10.6 I r---ittglbensylphthalatf_! - -- i0. I U ! - SU-- 3,rW-Dichlorobensidlao_- •- . - - 20. 1 V I j I .. .. 56,w55.3i ,.Demse(a )anthsacen♦- } .. _.__. _... I.W. IV 1 leo IV I -� 1 117-81•-T-•-----tris-lethylhexyl) phtbelat�=t---- - - - 4. 1 J- I :yo 1 207-08-9*------lenso�I�;floosanthene----tet~- - - IA. Its- • >�_��,`°�,� (' 54-32-t•-=----®ensoia•)gysene- - ----.�-.--•.�-` w...�_.1�. Its--- ! ---� 14. 5.3-70-3.h ------ D1benv4&*h)anthsacene--_t--- - . -- la: IU 191-24-2grh-,1) pexylene-_h---.� : ls. IV ! (2). - Cannot- be separated from d iphenylantnf x r. /8T`E f -_- SNMIVDLATILE ORGANICSrANALYSIS DATA SHEET SPA SAMPLE NO. TUTAQIVRLY IDENTIFIED COMPOUNDS I I gab Nage: INTI Contract: 68 -DS -0088 I BFC99 I I ,,ab Code: INTZM> Cast No.: 15886 - SAS No.: SDO-No.: BFC39 Atrix: (soil/Vater) VATER Lab Sample ID: Sample Vt/volo. 1000.0 -(g/ML) ML Lab File ID: B3886 evel: (10V/Med) LOW _ Date Received: 12/ 6/90 Moisture: not dec. 100. dee. 0. Date Extracted: 12/ 6/90 traction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/18/90 PC Cleanup: (YIN) N pHs 7.5 Dilution Factor: 1.00 CONCENTRATION UNITS: ?lumber TICS found: 1 (uq/L or uq/Rq) UO/L I I II I CAS NUMBEIt I COMPOUND NAME I R? I EST. CONC. ess:issssss�sssslsssasssssssssssssssssssssssslsssssssslsssasessssasslssassl 1 • - - 1 UNKN0W I 8.56 1 10 . I JjJ I 2. 1 1_i I_I 3. 8. 5. t I_1 I 6. 7. 8. 9. 10. 1 11. I I 1 I 12. 13. 18. I Is1 I I 15. I I_t 16. ' 17._ 19. 20. 21. 22. 23. 28' 25. 26. 27. I 2. 299. 30. 236 FORM I 8v -TIC 1/87 Rev. 0 1H SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET ab Hama: INTNM.: Lab Code: INTRW Contract: 68-D9-0048 Case No.: 15486 SAS No.: atrix: (soil/water) NATER Sample wt/vol: 1000.0 (g/mL) MI. evel: (low/med) LOW _ Moisture: not dec. 100. dec. 0. extraction: (SepPI/Cont/Sone) SEFF NPA SAMPLZ NO. SFC40 SDG No.: DFC39 Lab Sample ID: Lab File ID: H3830 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 PC Cleanup: (Y/N) N pH: 6.5 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (uq/L or uq/Rq) UG/L Q 1 I 1 108 -95 -2 -------Phenol I 10. I IU 1 1 111-44-4 ------- bis(2.-Chloroethyl)ether I 10. Ili I 1 95=57-8-------2-Chlorophenol I 10. IU I 1 541-73-1-------1,3-Dichlorobenzene _I 10. IU I t 106-46-7-------1,4-Dichlorobenzene _I 10. IU I 1 100-51-6- ------ Hensyl alcohol I 10. IU I { 1 95-50-1-------1,2-Dichlorobenzene _I 10. IU I 1 95-48-7 ------- Z-Mathylphenol I 10. IU I 1 106-60-1 ------- bisr2-Chloroisopropyl)ether 1 10.: IU I 1 106-44-5 ------- 4-Mfthylphenol 1 10. IU I 621-64-7-------N-Nitroso-dt-n-propylamine_I 10. IU 1 67-72-1 ------- Hexaehlorcethane• 1 10. IU f 98 -95 -3 -------Nitrobenzene 1 10. IU I 1 78-59-1 ------- IsopAorone 1 10. 1U I 88-75-5-------2-N1tropheno1 1 10. IU I 1 105-67-9-------2,4-Dimethylphenol 1 10. IU I I • 65-85-0 ------- 5ensele acid 1 50. 1U 1 111-91-1-------btst.2-Chlosoethoxy)mthane_I 10. IU I 1 120-83- ­ ---2,6-01chlorophenol 1 10. 1U I 1 120-8 -=-1,2.4.-Tzichlorobenzene_1 10. 1U I �: 1 91-2 I 10. IU _----Naphthalene I* 106-t ;-4-Chloroaniline 1 10F. IU I 1 87-6E=---Nexachlorobutadiene _.1 10...10 I I 59-50-7-------4'-Chloro-3-methylphenol _I 10. IU I 1 91-57-6-------2-Methylnaphthalene _1 10. IU I 1 77-47-4 ------- Rexachlozocyclopentadiene _1 10. IU I 1 88-06-2-------2,4,6-Trichlorophenol -1 10. IU I 1. 95-95-4-------2,4,5-Trichlorophenol _t 50. 1U I 1 91-58-7 ------- 2-Chlosonaphthalene 10. IU I 88-74-4 ------- 2-Nitroanlllne I 50'4 IU. I A. 131-11-3 ------- Dlmethylphthalate I 10. IU I I 208 -96 -8 -------Acenaphthylene" 1 :' 19. IU I I 606-20-2 ------- ?,6-Dinitrotoluene 1 10. 1U I � 1/87 Rev FORM I SV -1 ...;: C] '77 1C E'PA SAMPLZ No. �MIViOLATILa ORGANICS ANALYSIS DATA SHM? I I yab Name: INTECH I BFC40 i Contract: 68-D9-0048 I I ab Code: INTLCH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER Lab Sample ID: 'ample wt/vol: 1000.0 (g/mL) ML i-zvel: (low/med) LOW Moisture: not dec. 100. dec. 0. Ktraction: (SepF/Cont/Sonc) SEPF Lab File ID: B3830 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 GPC Cleanup: (YIN) N pH: 6.5 Dilution Factor: 1.00 CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q I I 1 99-09-2 ------- 3-Nitroaniline I I I 1 83 -32 -9 -------Acenaphthene 50. IU 1 I 1 51-28-5 ------- 2,4-Dinitrophenol 10. IU I I 1 100-02-7 ------- 4-Nitrophenol 50. IU ! I 1 132-64-9 ------- Dibenzofuran 50. IU I I 1 121-14-2 ------- 2,4-Dinitrotoluene I 10. 10. 1U I 1U 1 84-66-2 ------- Diethyiphthalate I I 1 7005-72-3 ------- 4-Chlorophenyi-phenylether_I 10. 10. IU ! IU i 1 86-73-7-------Fluorene I 1 100-01-6 ------- 4-Nitroaniline 10. IU ! I 1 534-52-1 ------- 4#6-D1-nitre-2-methylphenol_I 50. 50. IU ! IU 1 86-30-6 ------- N-Nitrosodiphenylamine (1)_I 10. I IU 1 101-55-3 ------- 4-Br000phenyl-phenylether 10. IU _I 1 118-74-1 ------- Hexachlorobenzene I 10. IU i 1 87 -86 -5 -------pentachlorophenol I 50. IU 1 85 -01 -8 -------phenanthrene i 10. 1U 1 120 -12 -7 -------Anthracene I 10. IU i 1 84-74-2 ------- Di-n-butylphthalate I 10. IU 1 206-44-0 ------- Fluoranthene I 10. IU 1 1 129 -00 -0 -------Pyrene I 10. IU 1 85-68-7 ------- Butylbenzylphthalate I 10. IU 1 91-94-A ------- 3,3'-Dichlorobenzidine�l 20. IU 1 56-55-3Q-------Benzo(a)anthracene I 10. 1U I 218-01-S ------- Chrysene I 1 117-81-7 0. IU I ------- bis(2-gthylhexyl)phthalate_I �L7 I JI 1 117-84-0 ------- Di-n-octylphthalate__I 10. IU- I 1 20'5-99-2 ------- Benzo(b)fluoranthene_I 10. IU 1 207-08-9 ------- Benzo(k)fluorantheneI 10. IU 1 50-32-8-------Benzo(a)pyrene I 10. IU I 193-39-5 ------- Indeno(1,2,3-cd)pyrene_I 10. IU I 53-70-3 ------- Dibenz(a,h)anthracene 10. IU _I I 191-24-2 ------- Benzo(g,h,i)perylene I i 10. IU (1) - Cannot be separated from diphenylamine FORM I SV -2 180 1/87 Rev. V 1B SBMIViOLATILE ORGANICS ANALYSIS DATA SHBG? ' ab Name: Imo. "ab Code: INTECB Case No.: 15486 atria: (40il/water) MATER BPA SAMPLE No. I1 Contract: 68-D9-0048 i BFC41 1 I SAS No.: SDG No.: BFC39 Lab Sample ID: Sample wt/voi: 1000.0 (g/mL) ML Lab File ID: B3833 evel: (low/med) LOW _ Date Received: 12/ 6/90 : Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 -xtraction: (SepF/Cont/Sonc) SEPI+ Date Analyzed: 12/14/90 ?C Cleanup: (Y/N) N pH: 7.8 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS N®• COMPOUND (ug/L or ug/Kq) UG/L Q I 1 108 -95 -2 -------Phenol I I 1 V 111-4 ,4-4 ------- bis(2-Chloroethyl)ether I 10. fu 1 _I F 95-57-8 ------- Z -Chlorophenol - 10. IU I .I 1 541-73-1-------1,3-Dichlorobenzene 10. IU i 106-46-7----=--1;4-61chlorobonzeno I 10. IU 1 I .100-51-6 --- ---- Beinzyl alcohol I 3. i 10. 1 J 1 IU I 1 95-50-1-------i,2-Dichlorobenzene I 10. IU 1 1 95-48-7 ------- 2-Methylphenol I 10. IU I 1 108-60-1 -------- 1 10. IU I f 106-44-5-------4-Methpl0eno2 1 621-64-7------�W-bitiroso-di-nTprapYlamine_I I. 10. 10. IU 1 IU i - 67-72-1----�-=Hexachloroettiane I 10. IU 1 1 98-95-3- ------ Nittobensene I 10. IU I 1 78-59-1 ------- rsophorone- I 10. IU 1 1 88-75-5 ------- 2-Witrophenol- I 10. IU I 1 105-67-9 ------- 2,4-Dirthylphenol I I.O. IU I I 65 -65 -0 -------Benzoic acid I 50. fU I I 111-91-1-------bW 2-Chloroethoxy)mthane_1 10. IU I f 120-83-0-2-04-Dichlorophenol 1 10. IU I 1 120-02 �.. 1 2,4-Trlchlorobenzene_1 10. IU I 1 91-20 ';.. -!Naphthalene I. 10. 1 U I 1 106-47 _ 4-Ctiloroaniline I 10. IU I 1 87-60-3"' ---iaxwchlorobutadione 1 10. 1U I I 59-50=7-------4-Chloro-3-methylphenol 10. IU 1 _1 1 91-57-6-------2-Methylnaphthalene 10. IU I _I 1 77-47-4 ------- Hexachlorocyclopentadiene _1 10. IU f 1 88-06-2-------2,4,6-Trichlorophenol 10: IU _1 1 95-95-4-------2,4,5-Trichlorophenol 500= IU 1 ._I 1 91-58-7 ------- 2-Chloronaphthalene 10: IU _1 1 86-74-4 ------- 2-NItroaniline: I 50. IU I 1 132-11-3 ------- 01methylphthalate f 10. IU I 1 208 -96 -8 -------Acenaphthylene I 10: IU I 1 606-20-2 ------- 2,6-Dinitrotoluene i i 10. 1 IU I 1-1 FORM I av-i 1/87 Rev. SNMIVDLAT-rL8 ORQ 1C / I CS ANAL; YS I S DATA SHEN? Lab Name: INTXM: Contract: 68-D9-0048 Lab Code: INTACg CaBe.;No.: 15486 3AS No.: Matrix: (4011/water) WATER Sample wt/vol: 1000.0 (g/ML) ML Level: (low/Med) LOW i Moisture: not dec. 100. - dec. 0. Ixtraction: (Sept/Cont/Sonc) SEPT GPC Cleanup: (YIN) N pH: 7.8 ZPA SALE NO. I r I BFC41 I 1 1 SDO No.: BFC39 ..Lab -Sample ID: Lab bile ID: B3833 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution factor: 1.00 CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Rq) I UO/L C 1 99-09-2 ------- 3-Nitroaniline I I I I 83 -32 -9 -------Acenaphthene I 50. IU I I 51-28-5 ------- 244-Dinitrophenol 1 10. 1U I 1 100-02-7-------4-N1trop4eno1 I 50. IU I 1 132-64-9-. ------ Dibenzofusan 1 S0• IU I 1 z0toluene' 1 10. 1U I I 84-66-2-------Diethylphtte —1 hala 1®• IU 1 I 7005-72-3------=4-Chlorcphenyl-phenylather_I 10. IU 1 86-73-7 ------- fluorens 10. 1U I I 100-01-6-ine I 10. 1U I 1 534-52-1-------4,6-Dinitro-2-methylphenol_j 50. IU I I 86-30-6-------N-Nitzosodiphenylamine (1) 1 101-5�-3-------;:BzO�phenyl-phenylether 50• 10. IU I 1U 1 0 118-74-1------- �j 10. IU I 87-86-5---____Hexachlosobenzene 1 Pentachlorophenol 10. IU 1 85-01-8 ------- PhenanthreneI 50. IU I 1 120 -12 -7 -------Anthracene 1 10. IU I 184-74-2-------DI-n-butylphthalate 1 10. IU I 1 206-44-0-----Pluosanthene 1 10. 1U I 1 129-00-o'..' _pyrene I 10. 1U I 85-68-T:-+ ---_�tylbensylphthalate 10. IU I =�- 3 3 D1chlorobenzid1ns I 56-55-3��---_��o(a)anthracene --I 20' I U I 1 218-01-g-------Chrywene I 1 117-81-7 ------- I bis(2-lthylhexyl)phthalate_1 I 117-84-0-------Di-n-octylphthalate 10. 10. /o IU I IU I r. 1A�I 1 205-99-2 ---- _--Benzo(b)fluosanthene---1 10• IU I 1 207-08-9-------Benzo(t)fluoranthene�-1 10• lU I 1 50-32-8 ------- 8onso(a)pyrene _�I 10' IU I I 193-3t-5 ------- Indsno(1,2,3-cd)pyreAeI 1-0. IU I I 53-70-3 ------- D1benz(a'h)anthracene _1 10. IU 1 191-24-2 ------- Benzo(q,h,i)perylene --I 10. IU I I 10. IU I (1) - Cannot be separated Eros diphenyla�ine 1 1__I FORK I SV -2 i8C 1/87 Rev. / 1F SEMIVOLATILE ORGANICS ANALYSIS DATA B SHEET EPA SAMPLE N0. TENTATIVELY IDENTIFIED COMPOUNDS I I Lab Names IN?!Q{°- Contract: BFC41 i 68-D9-0048 I I ab Code: INTECR Case No.: 15486 SAS No.: SDO No.: BFC39 matrix: (soil/water) WATER Lab Sample ID: -ample wt/vol: 1000.0 (g/mL) ML Lab File ID: B3833 evel:- (low/med) LOW Date Received: 12/ 6/90 %.Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 xtraction: (SepF/Cdnt/Sonc) SEPF Date Analyzed: 12/14/90 SPC Cleanup: (YM N pH: 7.8 Dilution Factor: 1.00 CONCENTRATION UNITS:(uq/L Number TICa found: 7 or uq/Kq) UO/L CAS °a==sus====sssasaslases=====ssasasssass:ssasaasl==sassasl=====___=====I=====I 1 NUMBER I COMPOUND NAME I t I I I RT I BST. CONC. I O I 1. -- IUNKNOWN I 4.60 I 10. 1 JN I 2.' -- IUNKNQW I 8.62 1 10. 1 J 1 3. -- 1UNKNOVH I 14.82 1 10. 1 J I 4. 134-62-318enzaatt408men-dlethyl-3-meth 18'..48 1 5. - IUNRRO I 19.61 1 6. 934-34-912(iff)-BensothiGazolone (9CI).1 19.82 l 10. 1 J 1 7. - 1 UNKNOWN. I 24.74 1 e •. I __. I I I _I ' 10: ' 12. 1 13. .14• 15. 1 16. • 17. 19. 20. 21. 22. 1 23. 24. 25'• I I I 1 26. ' 27. I I I I I 28. 29. I I I I I 1 30. 0 I I I I I 1_I I I FORM I SV -TIC 1/87 Rev. 1H SFA SAMPLE NO. SEMI VOLATI LN ORGAV I C3 : ANALYS I S DATA S HIXT I I I DFC53 I - ■b Name: INTZW. Contract: 68-D9-0048 I 1 Lab Code: INTEM Case No.: 15486. SAS No.: SDG No.: HFC39 ktrix: (soil/water) WATER Sample at/vol: 1000.0 (g/mL) ML evel: (low/med) LOW - Lab Sample ID: Lab File ID: H3834 :.r Date Received: 12/ 6/90 Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 jaxtraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/14/90 PC Cleanup: (YIN) N pH: 7.8 Dilution Factor: 1.00 CONCZNTRATI ON- UNITS : CAS NO. COMPOUND (uq/L• or uq/Kq) UG/L 4l I I 108 -95 -2 -------Phenol I 10. I I IU I 1 111-44-4 ------- bis(2-Chlorcethyl)ether I 10. IU I { 95-57-8-------2-Chlorophenol i 10. IU I 541-73-1-------1,3-Dichlorobenzene _1 10. IU I I 106-46-7-------1i4-.Dichlorobenzene I 3. 1 1 I I 100-51-6 ------- Hensyl alcohol 1 10. IU f I 95-50-1-------1,2-Dichlorobenzene �i 10. IU I 95-48-7------=2-Metbylphenol- 10. {U I I 108-60-1-------bis�2_-Chlorolsopropyl)ether 1 10. IU I I 106 -44 -5 -----'**A— thylghenol f 10. IU I { ---- T--�N-Nitroso-di-n-propylaoine_I 10. IU i .621-64-7 L 67-72-1 ------- H4xachloroethane I 10. IU I { 98 -95 -3 -------Nitrobenzene I 10. IU I { 78-59-1 ------- Isophorone I 10. lU I { 88-75-5 ------- 2-Mitrophenol I 10. 1U 1 { 105-67-9 ------- 2,4-Diaethylphenol 1 10. IU I { 65 -85 -0 -------Benzoic acid I 50. IU I Z-(Aloroethazy) Mthan%_1 10. 1U I 120-t----2,4-Oichlorophenol I 10. IU I f 120- ---1,2,4-Trichlorobenzene_1 10. IU I g 91-2 ----Naphthalene I 10. 1U I { 106---4-Chloroanl2ine 1 10. IU 1 { 87-6;�2f�------neaachlorobutadiene _I 10. IU { 5l-5Q-'%------4-Ehloro-3-reethylphenol _I 10. I U 1 91-57-6-------2-Methylnaphthalene _I 10. 10. (U IU 1 77-47-4 ------- N•xachrarocyclopentadiene _I t 88-06-2-------2.406-lrichlorophenol _1 10.- AU I { 95-95-4 ------ 2,L4,5-TrichlorophanoV �1 50. IU I I 91-56-7-------2-Chloronaphthalens _I 10. IU I { 88-74-4 ------- 2-Nitroaniline I 50. IU I I 131-11-3-------Diuothylphthalate 1 10. IU I 208 -96 -8 -------Acenaphthylene 1 10. 10. IU 1U. I 1 606-20-2 ------- 2,6-Dinitrotoluene I 1 FORM I SV -1 1/67 Rev. 1C ZPA SAMPLE NO. BEMTVOLATILK ORGANICS ANALYSIS DATA Sif3='!' I Contract: 66-D9-0048 I 1FC53 I Lab elaae s iNT-' 1 Lab Code: INT Case No.: 15486 SAS No.: SDO-No.: 1FC39 Matrix: (soil/water) VATNR Sample wt/vol' 1000.0 (g/mL) ML Level: (low/med) LOW _ % Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sonc) S18pF GPC Cleanup: (Y/N`) N pH: 7.8 Lab -Sample ID: Lab File.ID: 13834 Date Recaived: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CA8 NO . CONCRi�ITRATi ON UNITS: COMPOUND (ug/L or uq/Kg-) U®/L G I I 1 9!-09-2 ------- 3-Nitr.eanil ine I 1 I 1 .83 -32 -9 -------Acenaphthene 50. I t1 I 1 51-28-5 ------- 2,4_pinitrophenol I ) 10. 50• IU I IU 1 100-02-7-------4-Nitzophenot I 1 132-64=9-------Dibenz t-uaan- I 50. IU r 1 221-1t-2-------2, 4-Di'nitrotoluene : 1 10. I U I I 81-66-2'=------Diethylphtha�late I 1 7005-72-3-------4opheny%- 10. 10. 1U I 1U II I 86-73-7-------yluggenP phenylether_I 10. IU I 100-®2-6-------4 ) e 10. 50. 1U IU1 534-52-1-------t6-Dn,o-.2 50. IU 1 -------N-Nitd--othy1.phenol_1 .. sosoipheny apine (1)I 10. (Ul 101-55-3-------4-p; y- _I IU 1 11a-74-1------ _10. oroenzene IIII1 87 -86 -5 -------Pentachlorophenol 10. IU1 I 1 85 -01 -8 -------phenanthrene ) '120 5A. 1U I 1 -12 -7 -------Anthracene 10. 1 U 1 84-74-2----Dt-n-bnty phthalate 10. IU I1 I 206-44 AL___ -ranthene 10. 1U 129 -00 ----Pyrene I 85-68&_ ...::.. --sutyib•nzylphthalate 10. I U I lu I I 91-94-----3:,31-Dichlorobenzidine__I I 56 -55 -3 -------so 10. 20. 1U I IU I mo(a)anthracene I 218-01-9-------CArygene I 10. I IU10. 1 117-81-7 ------- bis(2-nthylhexyl)phthalate_1 1 117-84-0 10 '40.I 1U VI I ------- Di-n-octylphthalate' .'t I 1 205-99-2 ------- Benzo{b)fluoranthene- 10. -IU I �) V 207-08-9 ------- Henzo(k)fluoranthene__I 10. IU I I 50-,32-8 ------- Bgnzo(a)pyrene 10. IU I. 1 193-39-5 ------- indeno(I,2,3-cd;pyrene-l_ 10. 10.. IU I IU I 1 53-70-3 ------- Dibenz(a,h)anthzacene _I 1 191-24-2 ------- lenzo(g,h,!?perylene__) 10. IU I I 10. IU I 1 (1) - Cannot be separated from diphenylamins I I 200 FORM I SV -2 1/87 Rev. 141 �_-M 1F EPA SAMPLE NO. ORQ S>�� IL?I�YNIDENTIg SDICOMPOtJND3�? I 1 1 BFC53 1 Contract: 68-09-0048 I 1 Name: INTI Code: INTI Case No.: 15486 SAS No.: SDG No.: BFC39 Natsix; (soil/water) WATER Lab Sample ID: aaple.wt/vol: 1000.0 (g/mL) ML Lab bile ID: 83834 Level; (low/mod) LOW - Date Received: 12/ 6/90 4 Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Nxtraction: (SepF/Cont/Sone) SEPF Date Analyzed: 12/14/90 apC Cleanup: (YIN) N pH: 7.8 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 6 (ug/L or ug/Kg) UG/L I I I I I I I CAB NUMBER 1 COMPOUND MANN I R? I ES?. CONC. f Q 1 1. -- IUNKNOW 1 8.61 1 10. I J a I 1 2. -- tUNKNOWN 1 14.82 1 8. I J I f 3. 134-62-31Benzamide, NjH-diethyl-3-meta 18.48 I 4. -- IUNKNOVN 1 19.60 1 5. 934-34-912 0H)-Benzothlazolone (9EI) 1 19.80 1 10. I J I I 6. - 1 UNKNOWN 1 24.74 1 10. I J r f I 1 T. I I I I I 1 9. 110. i 11. I I I I I 112. I I I I I 113. I I I I I 1 14. t I I I I 1 15. 1 16. f I t I I 1 17. ) I I I I 1 18. 1 19. I I I I I 1 20. r 1 o t I 1 21. r I I I 1 1 22. 1 23. 1 24. 1 25. 1 26. 1 27. I I I I I 1 28. 129. I ) I I I 130. I I I I I I I I I I I FORM I SV -TIC 201 1/87 Rev. 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I I - I BFF66 I Lab Name: IN'1'ECt Contract: 68-D9-0048 I I Lab Code: INTECW-'- Case No.: 15486__ SAS No.: SDG No.: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30.6 (g/mL) G Lab File ID: B3852 Level: (low/mad) LOW Date Received: 12/ 6/90 % Moisture: not dec. 5. dec. 5. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sone) SONC Date Analyzed: 12/15/90 GPC Cleanup: (Y/N) N pH: 6.5 Dilution Factor: 4.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q I 1 1 10.8 -95 -2 -------Phenol I 1400. I I IU ,J. 1 111-4-4-4 ------- bis(2-Chloroethyl)ether I 1400. IU I 1 95=57-8-------2-Chlorophenol I 1400. t.0 1 1 541-73-1-------1,3-Dichlorobenzene { 1400. IU I 1 106-46-7-------1,4-Dichlorobenzene I 1400. IU I 1 100 -51 -6 -------Benzyl alcohol ( 1400. IU i 1 95-50-1-------1,2-Dichlorobenzene 1 1400. IU 1 95-48-7 ------- 2-Methylphenol ( 1400. IU I 1 108-60-1.-------bis(2-Chloroisopropyl)ether I 1400. IU I 1 106-44-5 ------- 4-Methylphenol.. -. I. .1400. IU I I 621-64-7-------N-Nitroso-di-n-propylaoine_I 1400. IU I I 67-72-1-------Hexachloroethane I 1400. IU I 1 98 -95 -3 -------Nitrobenzene I 1400. IU 1 78-59-1 ------- Isophorone 1 1400. IU 1 88-75-5 ------- 2-Nitrophenol I 1400. IU 1 105-67-9-------2,4-Dimethylphenol I 1400. IU I 1 65 -85 -0 -------Benzoic acid" 1 6600. IU I I 111 -91L -U-- ----- b1s(2-Chloroethoxy)methane_1 1400. IU 1 120-8----2,4-Dichlorophenol 1 1400. IU I 1 120-8---1,2,4.-l.2.4.I 1400. IU -Naphthalene 1 1400. IU 1 1 106= °_j--4-Chloroanilina. I 1400. IU I 1 87- ,_ .-NiexachlorobutadLene 1 14.00. IU I 1 59-5 ,. - =--t-Ch3Loro-3-methylphenot- - I 1400. IU I ( 91-57-6-=-----2-Kithylnaphthalen• �I 1400. IU 1 77-47-4-------Hexachlorocyclapentadienw---_I 1400. IU I I 88-06-2-------2`', 4,.6: -Tr ichlorophenor- -- 1 14.00.- 1U I 1 95-95-4 -------- 2,4,5-Trichlorophenor" { 600. IU I { 91 -5H -r7 ------- 2-Chloronaphthalenw.. l 1400. IU I 1 88-7*-4-------XTOt l -line -- I 6600. 1U I 4 13.1-11-3-'--D$msthylphthalata _..... _ { ; T400. I U I 1 208-96-8-- ----- Acenaphthylene•- - I .,1400. IU I I 606-20-2-------2, 6-Dinitratoluene 31 FORM I 3V-1 - 1/87 Rev . 1C EPA SAMPLE NO. SXWjvMATILE ORGANICS ANALYSIS DATA SHEET - I I �= I BFF66 Contract: 68-D9-0048 I I Lb Cade: INTI_ Case No.: 15486 SAS No.: SDG NO.: BFF66 Matrix; (soil/water) SOIL Lab Sample ID: $aaple wt/vol: 30.6 (g/mL) G- Lab File ID: B3852 Level: (low/med) LOW Date.Received: 12/ 6/90 % Moisture: not dec. S. dec. 5. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) SONO Date Analyzed: -12/15/90 GPC Cleanup: (YIN) N PH: 6.5 Dilution Factor: 4.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or I uq/Rg) UG/RG Q I 99-09-2 ------- 3-Nitroaniline I I 1 1 83 -32 -9 -------Acenaphthene ( 6600. IU = I 1 51-28-5-------2 ,4-Dinitrophenol 1 1400.. IU I 3 1 100-02-7 ------- 4-Nitrophenol ( 6600. IU I 1 132-64-9 ------- Dibenzofuran I 6600: IU I 1 121-14-2 ------- 2p4-Dinitrotoluene ( 1400. IU I 1 84-66-2 ------- Diethylphthalate 1 1400:- IU- I 1 7005-72-3 ------- 4-Chlorophenyl-phenylether r 1400. fu I 1 86-73-.7 ------- Fluorene —1 1400-: I u I 1 100-01-6 ------- 4-Nitroaniline1 1400. lu I 1 534-52-1 ------- 4,6-Dinitro-2-meth 1 henol ( 6600` Iu I 1 86-30-6-------N_Nitzoaodiphenylamine (ly-1 1 101-55-3 ------- 4-Bromophenyl-phenyletherI i4po-;. �U 1 I- 118-74-1-------Hexachlorobenzene —1 1400•- IU- I 1 87-86-5 ------- pentachlorophenol 1 1400-: IIi I 1 85 -01 -8 -------phenanthrene I 6600-. IU I 1 120 -12 -7 -------Anthracene 1 1400. ju I 1 84-74-2 ------- Di_Q-butylphthalate( 1400.- lu I I 206-44-0-------rin®s4nthene I 1400. IU I I 129-00-0�--.---- Pyrene 1 1400. l u I I 85-6 ----Butylbenzylphthalate 1 1400: IU I 1 91-9 -----i, 3.'-Dichlorobenzidine 1 56-5 I 1400. 2700. IU I IU ---Benzo(a)anthracene --1 1 218-0--;-�yaene I 1400: ! IU I I 117-81-7t-------bia(2-)8thylhexyl)phthalate_I 1 117-84-0------_Di_n_octylphthalate 1,4001400. 400-, IU { I 205-99-2 ----- --Bonzo(b)fluoranthene�-1 1400: IU I 6 207-08-9 ------- Benzo(k)fluoranthene-----1 140IU I L 50-3�2-8------- Benzo(a)pyrene --_-I 1400-r- 400:1 1193-39v-5 ------- Indeno (l, 2, 3 -cd) pyLener _ 1400-:- -. - I u ! ! S3"7t)-3------- Diberez(a,h)anthraeene --f`_ 1 191-24-2 ------- Benzo(q,h,i)perylene --r 1400: 140@: - Iu- I Iu I...... I __r - .1400. I u- I (1) - Cannot be separated from diphenylamine .r FORM i 3V-2 132" 1/87 Rev. i L] 3EMIVOLATILE ORGANICSFANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: INTECH Lab Code: INT3-- Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 30.6 (g/mL) G Level: (low/med.) LOW Contract: 68-D9-0048 Moisture: not dec. 5. - dec. 5. Extraction: (SepF/Cont/Sonc) SONC GPC Cleanup: (YIN) N pH: 6.5 EPA SAMPLE N0. I I I BFF66 1 I I SAS No.: SDG NO.: BFF66 Lab Sample ID: Lab File ID: B3852 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/15/90 Dilution Factor: 4.00 Number TICS found: 3 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG I I I CAS NUMBER I COMPOUND NAME II I I RT I EST. CONC. I U I =aas:a=sa=ss==sa==sa1===s=aasl==sa=a======als==ss1 IUNKNOWN 1 2. -- IUNKNOWN 1 7.87 I 700. I J I 1 3. - IUNKNOWN 1 37.41 I 1000. I J h) I 1 4.1 38.53 I 1000. 1 J N I I 5. I I II 1 I 6. -� I I I _f 1 7'. I 8. 10. 111. I I I I 1 ' 12. 13. 14.I I_I I I 1 15. 16. I I I I 17. I I I 1 18. I I ( I 19. 20. 1 21. I I I I � 22. I�- 23. I I I I 24. I I 1 25. I I I 26. 27. 1 28. I I 29. 30. I I FORM I S`/ -Tac 133 1/87 Rev. 1B SEMIVOLATILF, ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH Lab Code: INTEC* Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 30.4 (g/mL) G Level: (low/med) LOW EPA SAMPLE NO. I I I BFF67 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 % Moisture: not dec. 5. dec. 5. Extraction: (SepF/Cont/Sono) SONC GPC Cleanup: (Y/N) N pH: 6.4 CAS NO. COMPOUND Lab Sample ID: Lab File ID: B3853 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/15/90 Dilution Factor: 4.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG Q 108 -95 -2 -------Phenol I I 1400. I I IU 1 111-44-4 ------- bis(2-Chloroethyl)ether I 1400. IU 1 95-57-8-------2-Chlorophenol I 1400. IU 1 541-73-1-------1,3-Dichlorobenzene f 1400. IU 1 106-46-7-------1,4-Dichlorobenzene 1 1400. IU 1 100 -51 -6 -------Benzyl alcohol ( 1400. IU 1 95-50-1-------1,2-Dichlorobenzene 1 14.00. IU 1 95-48-7 ------- 2-Methylphenol ( 1400. IU I 108-60-1 ------- bis(2-Chloroisopropyl)ether 1 1400. IU 1 106-44-5 ------- 4-Methylphenol 1 1400. IU 1 621-64-•7 ------- N-Nitroso-di-n-propylamine_l 1400. IU 1 67-72-1 ------- Hexachloroethane 1 1400. IU I 98 -95 -3 -------Nitrobenzene 1 1400. IU 1 78-59-1 ------- Isophorone ( 1400. IU 1 88-75-5---- --- 2'-Nitrophenol ( 1400. IU 1 105-67-9 -------- 2,4-Dimthylphenol 1 1400. IU 1 65 -85 -0 -------Benzoic acid 1 6600. IU 1 111-91-1 ------- bis`2-Chloroethoxy)nezthane_1 1400. IU 1 120-83-2 ------- 2,4-Dichlorophenol 1 1400. IU 1 120-82-17-- --1,2,4-Trichlorobenzene' 1 1400. 1U I ---Naphthalene 91 -V__, 1 1400. IU 106- ---4-Chloroaniline I 1400. IU 1 87- ---Nexachlorobutadiene ( 1400. IU I 59-5 ---4-Chloro-3-methylphenol I 1400. IU I 91-5.'i_6;==----2-Methylnaphthalene- I 1400. IU 1 77-47-4 ------- Rexachlorocyclopentadiene 1400. IU 1 _I 88-06-2-------2,4,6-Trichlorophenol 1400. IU �I 95-95-4-------2,4,5-Trichlorophenol- I 6600. IU 91-58-7 ------- 2-Chloronaphthalene--- I .1400. IU 1 88-74-4 ------- 2-Nitroaniline i 6600. IU 1 131-113 ------- Dimethylphthalate ( 1400. IU 1 208 -96 -8 -------Acenaphthylene 1 1400. IU 1 606-20-2 ------- 2,6-Dinitrotoluene- I 1400. IU I I I I 140 FORM I SV -1 1/87 Rev 04 A 1C SZMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE N0. Lab Name: INTECH Contract: 68_ I BFP67 I Lab Code: "IN7'! D9-0048 I I Case No.: 15486 SAS No.: I Matrix: (soil/water) SOIL SDG No.: BPP66 Sample wt/vol: 30.4 (g/mL) G Lab Sample ID: Level: (low/med) LOW Lab File ID: B3853 s Moisture: not dec.5. Date Received: 12/ 6/90 _ dec. 5. Extraction: (SepF/Cont/Sone) SONC Date Extracted: 12/ 7/90- GPC Cleanup: (YIN) N Date Analyzed: 12/15/90 pH. 6.4 Dilution Factor: CAS 1V0 . 4. 0 0 COMPOUND CONCENTRATION UNITS: I (u9/L or ug/Kg) UG/KG 4 I 99-09-2-______3_Nitroanfline I I 83-32-9------ 1 I 51-28-5--Zcenaphthene I 6600. IU I 1 100-02-7 ------- .4-Dinitrophenol I 1400. I I' 132-64-9 ------- 4-Nitrophenol I 6600. IU I -DibenzOfuran I 6600. IU I I 121-14-2---- I IU I I 84-66-2 ------- 2.4-Dinitrotoluene 1400. IU 17005-72- Diethylphthalate I 1400. IU 3------- I 86-73-7------- Fluorene phenyl-phenylether_j 1400. IU I I 100-01-6--- __4_Nirene line 14.00. IU 1 534-52_ ( 1400. I 1------'4.6-Dinitro- I IU I I 86-30-6-"'---N-Nitroaodi 2-methYlphenol_I 6600. IU I I 101-55-3_______4_Bromo Phenylamine (1) 6600. IU I I 118-74-1--_-___ Phenyl-phen I 1400. IU I Hexachlorobenzene ylether _I 1400. I 87-86-5---____pentachloro I IU I I 85-01-8---____Phenanthrenehenol I 6600. IU I 120-12-7------- I Anthracene I IU I I 84-74-2---_---Di-n-but I 1400. IU I I 206-44-0-- Y1Phthalate 1400. IU I I 129-00-0....... Fluoranthene 1400. IU I i 85-68-7---_ PYrene I 1400. IU ___ -ButylbIchlo htIN!' ��� 1400. i 91-94-1---'3.3'-Dichlorobenzidine IU I I 56-55-3---�___ 1400. IU I 218-01- Senzo(a)anthracene -I 2700. 9-- - IU I 117-81-7--- -_ ls(2- t I 1400. IU I 117-84-0--_____bis(2-St hylhexyl)phthalate I 1400. IU I I 205-99-2-----__Di-n-octylphthalate -I �`lDop, �-.�- I 207-08-9--_____Benzo(b)fluoranthene ��I 1400. IU� I 50-32-8--- _Benzo(k)fluoranthene� I 1400. I 193- Benzo IU I 1 39-5-- Indenoa)PYrene 1400. IU 53-70-3 ------- (1e2,3-ed)pyrene__�� 1400. 1U 191_24_ Dibenz(aph)anthracene -I 1400. I 2"'----Benzo ( - I tJ I g•h,i)perylene-I 1400. IU (1) Cannot be separated I 1400-• IU I from diphenylamine I I FORM I SV -2 141 1/87 Rev. EPA SAMPLE N0. ,,, IVOORGANICS ANALYSIS EET TENTATI VELYI DENTIFIED COMPOUNDS I I INTI-- Contract: 68-D9-0048 BFF67 f � I Code: INTZC'f Case No.: 15486 SAS No.: SDG No.: BFF66 pptrix: (soil/water) SOIL Lab Sample ID: Sale at/vols 30.4 (g/mL) G Lab File ID: B3853 Level: (low/med) LOW Date Received: 12/ 6/90 S Moisture: not dec. 5. _ dec. 5, Date Extracted: 12/ 7/90 zxtraction: (SepF/Cont/Sonc) SONC Date Analyzed: 12/15/90 Gpc Cleanup: (YIN) N pH: 6.4 Dilution Factor: 4.00 Number TICS found: 13 CONCENTRATION UNITS: I (ug/L or ug/Kg) UG/KG I I CAS NUMBER I COMPOUND D NAME I I I 1.. 694-87-11B1cyclo[4.2.0]Octa-1,315-tril I RT ==4.97=1- I EST CONC.I _ - =1=s=ssl Q I 1 2. 98-82-81Benzene, (1-methylethyl)- 2000. I J N I 1 3. (91 103-65-11Benzene, propyl- (8CI9CI) 5.78 1 1000. 1 J f 1 4. - - (UNKNOWN _I 6.46 1 700. 1 J ' I 1 5. - - (UNKNOWN I 7.88 1 700• I J I I 1 6. 20071-09-41Benzene, 1,1'-(1,2-cyclobutai 18.66 700. 1 J I 1 7. - - (UNKNOWN 20,93 1000. 1 J I 8. - (UNKNOWN I 29.33 I 2000. 1 J f 9• --•(UNKNOWN 1 30.46 1 6000. 1 J f . 10. - - (UNKNOWN I 30.52 1 2000. 1 J f 1 11. -- (UNKNOWN I 30.63 1 2000. 1 J f 12.31.51 - - (UNKNOWN HYDROCARBON I I 800. 1 J f 1 14. - 1UNKNOWN-700. 33.87 1 15. I I I 38.53 I I 1000. 1 J f\1 I 16. 1 I 17. f I I I I 118. 1 I I 19. � ( I I -1 20. I I 1 21. I 22. 1 f I 23. 24. I 1 I � 25. I I 26. 27. 1 28. I 1 I I I 1 29. I 1 I I I 1 30. I I I I I I_I I FORM I SV -TIC 1462 1/87 Rev. I 1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECIIV-- Lab Code: INTECR Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol.: 30.2 Level: (low/med) LOW % Moisture: not dec. 2. EPA SAMPLE NO. I I I BFF68 I .Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 (g/mL) G dec. 2. Extraction: (SepF/Cont/Sonc) SONC GPC Cleanup: (Y/N) N pH: 7.1 Lab Sample ID: Lab File ID: B3893 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: X12/17/90 Dilution Factor: 4.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q I 108 -95 -2 -------Phenol 1 1300. I i IU I 111-44-4 ------- bis(2-Chloroethyl)ether I 1300. IU 1 95-57-8-------2-Chlorophenol ( 1300. IU I 541-73-1-------1,3-Dichlorobenzene 1300. IU 1 _I 106-46-7 ------- 1,4 -Dichlorobenzene-- I 1300. IU I 100 -51 -6 -------Benzyl alcohol I 1300. IU 1 95-50-1-------1,2-Dichlorobenzene I 1300. IU I 95-48-7 ------- 2-Methylphenol ( 1300. IU 108-60-1 ------- bis(2-Chloroisopropyl)ether 1 1300. IU I 106-44-5 ------- 4-Methylphenol I 1300. IU I 621-64-7 ------- N-Nitroso-di-n-propylamine_I 1300. IU 1 67-72-1 ------- Hexachloroethane J 1300. IU 1 98 -95 -3 -------Nitrobenzene I 1300. IU 1 78-59-1 ------- Isophorone I 1300. IU 1 88-75-5 ------- 2-Hitrophenol I 1300. IU 1 105-67-9-------2,4-Dimethylphenol I 1300. IU 1 65 -85 -0 -------Benzoic acid 1 6500. IU 1 111-91-1-------bla(2-Chloroethoxy)methane_1 1300. IU I 120-83-----204-Dichlorophenol I 1300. IU 120-t ---1,2,4-Trichlorobenzene I 1300. IU 1 - 91-2 ---Naphthalene I 1300. IU I 106-4 --4-Chloroaniline I 1300. IU 1 87-66-3,��-----Hexachlorobutadiene 1300. IU 1 �I 59-50-7-------4-Chloro-3-methylphenol I 1300. IU 1 91-57-6-------2-Methylnaphthalene I 1300, IU 1 77-47-4 ------- Hexachlorocyclopentadiene 1300._ IU 1 _I .88-06-2-------2,4,.6-Trichlorophenol I 1300. IU 1 95-95-4-------2,4,5-Trichlorophenol I 6500. IU 1 91-58-7 ------- 2-Chloronaphthalene 1300. IU 1 _I 88-74-4 ------- 2-Nitroaniline I 6500. IU 1 131-11-3 ------- Dimethylphthalate 1 X1300. IU .I 208 -96 -8 -------Acenaphthylene I 1300. IU 1 606-20-2 ------- 2,6-Dinitrotoluene I 1300. IU 11 FORD! I 3V-1 1/87 Rev. 1C SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name; INTECIIi Contract: 68-D9-0048 Lab Code: INTECH . Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 30.2 (g/mL) Level: (low/med) LOW % Moisture: not dec. 2. - dec. Extraction: (SePP/Cont/Sonc) SONC EPA SAMPLE NO. I 1 I BFF68 I I I SAS No.: SDG No.: BFF66 Lab Sample ID: G Lab File ID: B3893 Date Received: 12/ 6/90 2• Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 GPC Cleanup: (Y/N) N pH: 7.1 Dilution Factor: 4.00 CAS N0. COMPOUND CONCENTRATION UNITS: (uq/L or uq/Kq) UG/KG p II 1 99-09-2 ------- 3-Nitroaniline I I 1 83 -32 -9 -------Acenaphthene I 6500. IU I 1 51-28-5 ------- 2,4-Dinitrophenol I 1300. IU 1 100-02-7 ------- 4-Nitrophenol I 6500. IU I 1 132-64-9 ------- Dibenzofuran I 6500. IU I 1 121-14-2 ------- 2,4-Dinitrotoluene I 1300. IU I 1 84-66-2 ------- Diethylphthalate I ( 1300. 1300. IU I IU I 1 7005-72-3 ------- 4-Chlorophenyl-phenylether_I 1300. IU I 1 86-73-7-------Fluorene I 1300. IU I 1 100-01-6 ------- 4-Nitroaniline I 6500. IU I 1 534-52-1 ------- 4,6-Dinitro-2-methylphenol_I 6500. IU I 1 86-30-6 ------- N-Nitrosodiphenylamine (1)_1 1300. IU I 1 101-55-3 ------- 4-Bromophenyl-phenylether "118-74-1 1300. IU 1 ------- Hexachlorobenzene _I I 1300. IU I 1 87 -86 -5 -------Pentachlorophenol I 6500. IU 1 85 -01 -8 -------phenanthrene I 1300-. IU I 1 120 -12 -7 -------Anthracene I 1300. IU I 1 84-74-2 ------- D.i-n-butylphthalate 1300. IU I _1 1 206-44-0 ------- Fluoranthene I 1300.' JU I I 129-00-0�------pyrene t 1300. IU I 85-68-""-----Butylbenzylphthalate_I 1300. IU I I 91-94---3,3`-Dichlorobenzidine ` 1 2700. IU I 1 56-55- ----Benzo(a)anthracene 1 218-01-�=-----Chryaene 1 1300. IU I 1 117-81-7---%---(Z_gthylhexyl)phthalate_I t 1300. IU I 1 117-84-0 ------- Dl-n-octylphthalate 1300. 1300. IU IU _I 1 205-99-2 ------- Benzo(b)fluoranthene_I 1300. CU I I 207-08-9 ------- Benzo(k)fluoranthene_V 1300. IU I 50-32-8-------Benzo(a)pyrene i -- 1300'. IU I I 193-39-5 ------- indenc(1,2,3-cd)pyrene_j 1300. IU I I 53-70-3 ------- D1benz(&,h)anthracene 1300. IU. I _r. I 191-24-2 ------- Benzo(q,h,i)perylene__I 1300. IU (1) - Cannot be separated from diphenylanine FORM I SV -2 179 1/87 Rev. 1F SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. TENTATIVELY IDENTIFIED COMPOUNDS I BFF68 I /j� Name: INTECH Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30.2 (9/mL) G Lab File ID: B3893 Level: (low/med) LOW Date Received: 12/ 6/90 % Moisture: not dec. 2. dec. 2. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) SONC Date Analyzed: 12/17/90 GPC Cleanup: (YIN) N pH: 7.1 Dilution Factor: 4.00 Number TICS found: 2 CONCENTRATION UNITS: (u9/L or u9/K9) UG/KG I I I I I CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q I - I UNKNOWN 1 5.67 1 700. I J �J I 1 2. 1UNK�NOWN I 7.88 I 900. 1 3. i 4.5. I I I I I 6. I I I I I I I_1 I I I 7.8. I I ( I I 9. .1 10. 11. 12. I 13. 1 14. I I I I I 15. 16. I I I I I I_I I I I 1. 188. ► I._I I I 19. ) 20. 21. 22. 23. 1 24. I I ( I I I I 25. I I I 26. I ( I I I 1 27. I I I I I 28. I I I I I 29. � 30. I I I I I I I I_I I I FORM I SV -TIC 180 1/87 Rev. M 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I I I BFF69 1 Lab Name: INTECK Contract: 68-D9-0048 I Lab Code: INTECH Case No.: 15486 SAS No.: Matrix: (soil/water) SOIL Sample wt/vol: 30.5 (g/mL) G Level: (low/med) LOW % Moisture: not dec. 15. dec. 15. Extraction: (SepF/Cont/Sone) SONC SDG No.: BFF66 Lab Sample ID: Lab File ID: B3897 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90. GPC Cleanup: (YIN) N pH: 6.3 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 1 108 -95 -2 -------Phenol I 380. IU I 1 111-44-4 ------- bis(2-Chloroethyl)ether I 380. IU I j 95-57-8-------2-Chlorophenol I 380. IU = I 1 541-73-1-------1,3-Dichlorobenzene I 380. IU I 1 106-46-7-------1,4-Dichlorobenzene I 380. IU I 1 100 -51 -6 -------Benzyl alcohol I 380. IU I 1 95-50-1--------1,2-Dichlorobenzene I 380. IU I 1 95-48-7 ------ =2-Methylphenol I 380. IU I 1 108-60-1 ------- bis(2-Chloroisopropyl)ether.1 380. IU I I 106-44-5-------4-Methylphenol I 380. IU I 1 621-64-7 ------- N-Nitrowo-di-n-propylamine_1 380. IU I 1 67-72-1 ------- Hexachlaroethane± I 380. IU I 1 98 -95 -3 -------Nitrobenzene I 380. IU I 1 78-59-1 ------- Isophorone• I 380. IU I 1 88-75-5 --- ----2-Nitrophenol 1 380. IU. I 1 105-67-9.-------2,4-Dimethylphenol I 380. IU I 1 65 -85 -0 -------Benzoic acid 1 1900. IU 111-91-S-------bis(2-Chloroethoxy)mothane_I 380. IU I 1. 120-.----2 .4r-Dichlor.ophenol I 380. IU I 1 120- _-----1, Z,4-Trichlorobenzene I 380. IU I 1 91- -----Naphthalene I. 380. IU I• 106----4-Chlorcaniline I 380. IU I I 87-6A3►----- Nexachlorobutadiene I 380'. IU ( 59-50=7=- --4-Chloro-3-methylphenol I 380. IU 1- 91-57-6--- ---- 2-Nothylnaphthalene, I 380. IU .I 77-47-4 ------- Hexaehloroeyclopentadiene _I 380._ IU 1 88-06-2-------2,4,6-Trichlorophenol I 386. IU I 1 95-95-4-------2,4,-5-Trichlorophenol I 19-00. IU I 1 91-58-7 ------- 2-Chloronaphtha•lene I 380. IU F 88-74-4 ------- 2-Nitroaniline- I 1900. IU I 1 131-11-3 ------- Dimethylphthalate t �' 380. IU 1 208 -96 -8 -------Acenaphthylene I 380. IU 1 606-20-2 ------- 2,6-Dinitrotoluene I 380. IUB I II sa I FORM I Ski -1 1/87 Rev. 1C SSMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Na": INTWX Lab Code: INTECH Case No.: 15486 fatrix: (soil/water) SOIL Sample wt/vol: 30.5 evel: (low/med) LOW % Moisture: not dec. 15. (g/mL) G EPA SAMPLE NO. I I Contract: 68-D9-0048 I BFF69 1 I SAS No.: SDG -No.: BFF66 dec. 15. xtraction: (SepF/Cont/Sonc) SONC Lab Sample ID: Lab File ID: B3897 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 -?C Cleanup: (YIN) N pH: 6.3 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) UG/KG I Q 1 99-09-2 ------- 3-Nitroaniline 1 I I 1 83 -32 -9 -------Acenaphthene 1900. IU i 1 51-28-5 ------- 2,4-Dinitrophenol I 380. IU I 1 100-02-7 ------- 4-Nitrophenol I 1900. 1U I 1 132-64-9 ------- Dibenzofuran I 1900. IU i I 121-14-2------- 2,4-Dinitrotoluene I 380. I 380. 1U i 1 84-66-2 ------- Diethylphthalate 1U I 1 7005-72-3 ------- 4-Chlorophenyl-phenylether_i I I 380. 380. 1U 1 IU 86-73-7 ------- Fluorene I I 100-01-6-------4-Nitroaniline ( 380. IU I 1 534-52-1 ------ -4,6-Dinitro-2-methylphenol_1 1 86-30-6 ------- N-Nitroscdiphenylaeine I 1900. 1900. IU i 1U 1 (1)_1 1 101-55-3 ------- 4-Bromophenyl-phenylether 1 380. 380. IU 1 1U 118-74-1 ------- Hexachlorobenzene _1 I 1 87 -86 -5 -------Pentachlorophenol ( 380. IU I 1 85 -01 -8 -------phenanthrene I 1900. 1U 1 120 -12 -7 -------Anthracene 1 380. IU 1 1 84-74-2 ------- Di-n-butylphthalate I 3800' 1U I -moi 1 206-44-0 ------- Fluoranthene - 380. 1U I 129 -00 -0 --`=--Pyrene I 380. 1U 1 1 85-68-7- ButylbenzylphthalateI I 91-94-I :47-3v3'-Dichlorobenzidine_t I 380. 380. IU I 1U 1 1 56-55-3-------Benzo(a)anthracene 760. IU I 218-01-9-------Chryaene I 380. 1U 1 117-81-7 ------- bia (2-gthy1hexy1) phthalate_I I 380-. 370 -9-}; IU I -,d,-(_ 1 117-84-0 ------- Di-n-octylphthalate I 380. I 1 205-99-2 ------- Benzc(b)fluoranthene( IU 1 207-08-9 ------- genzo(k)fluoranthene__I- 380. IU I 1 50�-32-8-------Benzo(a)pyrene 380: IU I 1 193-39-5 ------- 1ndeno(1,2,3-cd)pyrene_1 ' 1 380':--- 380:----1U-- IU- I 1 53-70-3 ------- D1benz(a,h)anthracene 1 191-24-2 ------- Benzo(g,h,i)perylene I 380: I IU I I __I 380. IU I (1) - Cannot be separated from diphenylamine FORK I SV -2 186 1/87 Rev. L� code: = 1F SV0VV iTILS ORGANICS ANALYSIS DATA SHEET TWTATIVELY IDENTIFIED COMPOUNDS Ii�- v Contract: 68-D9-0048 INTUM Case No.: 15486 SAS No.: �pttixs ( sol l/water ) SOIL aawle we/vol: 30.5 ( q/mL ) G Level: ( low/med ) Low 1 Moisture: not dec. 15. - dec. 15. Extraction: (SepF/Cont/Sonc) SONC GPC Cleanup: (YIN) N pH: 6.3 Number TICS found: 17 EPA SAMPLE N0. I I BFF69 1 I � SDG No.: BFF66 Lab Sample ID: Lab File TD: B3897 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or u9/Kq) UG/ CAS NUMBER I KG COMPOUND _____ __________= I 1. NAME I ( RT 1 I I _ - (UNKNOWN =___= - I E 3T. CONC. I U I 3. 3' - (UNKNOWN I 5.70 I 1 4. - - IUNKNOWN 544-63-8 ITetradecanoic 1 7.90 1 200. 1 600. 1 J N I I 5. 6• acid 4655-34-912-propenoic (9CI)�1 14.80 21.06 1 5000. J1 1 1 Jr I ' 7' acid -methyl-,1 2091-29-419-Hexadecenoic 21-64( 400. I JI I I 8. - acid - (UNKNOWN 5.7-10-31Hexadecanoic (8CI9CI)I 23.63 j 7000. 8000. I Ji 1 I 9. acid 10544-50-013ulfur 1 (9CI) 23.67 j 200. J 1 110. 1 11. 2091-29-! g_ ' mol. (S8) 1 Hexadecenoic I (8CI9CI) 1 23.92 24.63 9000. 1 J I I J I I '.2. acid 57-11-410ctadecanoic acid - - (UNKNOWN (8CI9CI)I (9CI) I I 26.13 1 200. 20000. 1 1 J I J 3' 1 14. - - - 1UNKN0WN I 26.27 26.88 j 600. 1 I J I 15' -- (UNKNOWN I 28.51 1 2000. I J 1 6. - - -I UNKNO 3i1NN I 32.99 1 1000. I J I 7. - - 1UNKNOWN I 35.72 I 200. 1 J I 18. - - I UNKNOW(( I 35.87 1 200. 1 J I 1 I 37.24 I 300. I J �' I 1-----------j 25. 1 1 1�1 ► I • 1 1� j 1 I 28. � 1-------- ��I 2 1�1 -1 --1I 3 FORM I 3V -TIC 187 1/87 Rev. M 1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTEC* Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 30.1 (g/mL) G Level: (low/med) LOW _ EPA EPA SAMPLE NO. I I I BFF70 1 Contract: 68-D9-0048 I 1 SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: B3914 Date Received: 12/ 6/90 $ Moisture: not dec. 5. dec. 5. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sone) SONC Date Analyzed12/18% GPC Cleanup: (YIN) N pH: 6.9 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 1 108 -95 -2 -------Phenol I 350. IU 1 111-44-4 ------- bis(2-Chloroethyl)ether I 350. IU 1 95-57-8-------2-Chlorophenol I 350. IU 1 541-73-1-------1,3-Dichlorobenzene I 350. IU 1 106-46-7-------1,4-Dichlorobenzene 350. IU _ _I 1 100 -51 -6 -------Benzyl alcohol 1 350. IU 1 95-50-1-------1,2-Dichlorobenzene I 350. IU 1 95-48-7 ------- 2-Methylphenol I 350. IU 1 108-6-0-1 ------- bis(2-Chloroisopropyl)ether 1 350. IU 1 106-44-5 ------- 4-Methylphenol_. 1 350. IU 1 621-64-7 ------- N-Nitroso-di-n-propylamine_1 350. IU 1 67-72-1 ------- Hexachloroethane I 350. IU I 98 -95 -3 -------Nitrobenzene 1 350. IU 1 78-59-1 ------- Isephorone I 350. IU 1 88-75-5 ---- ---2-Nitrophenol ( 350. IU 1 105-67-9-------2,,4-Dimethylphenol i 350. IU 1 65 -85 -0 -------Benzoic acid I 1700. IU I 111-91!rl------- b1x(2-Chloroethoxy)methane_1 350. IU I 120-8V ----2-,4-Dichlorophenol I 350. IU 1 120-2----1,2,4-Trichlorobenzene I 350. IU 1 91 -2 ----Naphthalene 1 350. IU 1 106-4----4-Chloroaniline 1 350. IU 1. 87-68-3+=-----Hexachlorobutadiene 1 350« IU 1 59-50-7 ------- 4-Chloro-3-methylphenol I 350. IU 1 91-57-6-------2-Methylnaphthalene 1 350. IU 1 77-47-4 ------- Hexachlorocyclopentadiene 350. IU _I 1 88-06-2-------2,4,6-Trichlorophenol 1 350. IU 1 95-95-4-------2,4,5-Trichlorophenol 1 1700. IU 1 91-58-7 ------- 2-Chloronaphthalene 1 350. IU 1 88-74-4 ------- 2-Nitroaniline I 1700. IU 1 131-11-3 ------- Dimrethylphthalate 1 350. 1 208 -96 -8 -------Acenaphthylene 1 350. .IU IU 1 606-20-2 ------- 2,6-Dinitrotoluene 350. IU I 0$ -1- FORM I SV -1 1/87 Rev. i 1C SBMIVOLATILE ORGANICS ANALy313 DATA SHEET EPA SAMPLE NO. • I N?8 I eab. Nam' Contract: 68-D9-0048 BFF7Q I ( Lab Code: INTEM Case No.: 15486 SAS No.; I SDG No.: BFF66 Matrix: (soil/water) SOIL Sample wt/vol: 30.1 (g/mL) G Lab Sample ID; Level: (low/med) LOLab File ID: B391LOW _ % Moisture: not dec. 5. Date Received: 12/ 6190 dec. 5. Date Extracted: 12/ 7/90 Extraction: (SePP/Cont/Sone SONC Date GPC Cleanup: (YIN) N Analyzed: 12/18/90 pH' 6®9 Dilution Factor; 1.00 CAS N0. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG I Q I 99-09-2 ------- I I 3-Nitroa 83=32-9 ------- niline I I I 51 -28 -5 --_____Acenaphthene 1 1700• IU I I 100-02-7-______2,4-D1nitrophenol 1 350. IU I 132-64-9---____4-Nitrophenol 1 1700. IU I I 121-14-2---____Dibenzofuran 1 1700. IU I 1 84_66_2__---_-2,4-Dinitrotoluene 1 350. IU I DIethylphthalate 1 350. IU 17005-72-3---____ I I 86-73-7---____ rophenyl-phenylether 1 350. IU I I 100-01-6--_____FlUoreluorene� -1 350. IU I I II -Nitroanilne � 350. IU534-g2_1_______�'6-Dinitro-2- 1700. IU86-30-6----___ - o eypenol 1700. IL101-55-3-= ----- 4-BrOmophenyl-nylamine (1)_i 118-74-1 ------- phenylether III 350. IU I 1 87-86-5---____Hexachlorobenzene -1 350. IU I 1 Pentachlorophenol 1 350. IU 85-01-8 ------- I I 120 -12 -7 ---__--Phenanthrene I 1700. IU' I I 84 -74 -2 -----__Anthracene 1 76. _f J I I Df-n-butylphthalate 1 350., 1t1 206-44 129-00 I slucranthene �1 350. IU -4---Q--________Pyrene I 100. 1 85-68-7-.,�__ I I J I 91_94-1- Butylbenzylphthalate 110. I J �=a-3.3'-Dichlorobenzidine - 350. IU 1 ___Unzo(a)anthracene I I 218-01-9-----_- 690. II! I I 117-81-7----___�srysena 1 40. 1 J I 1 117-84-0--_____bia(a-8thylhexyl)pht)balate I 59. 1 1 1 1 205-99-2----___Di-n-octylphthalate _I ��� '� I I I 207-08-9---____Benzo(b)fIuoranthene�1 -350. IU�1 1 50-32-8--_____Benzo(k)fluoranthene�-I 46. 1 J I I 150-39-5---____Benzo(a)pyrene -I 53. 1 .1 I I 53-70-3---____Indeno(1,Z,3-cd)pyrena� I. 43. 1 J I I 191-24-2--- __Dibenz(a,h)anthracene ' 350. 1I1 I 1 Benzo(g.h.i)perylene_-I 350. IU I (1) - Cannot be separated from diphenylamine 350. IU I I 1 I FORM I SV -2 20,11 1/87 Rev. FORM I SV -TIC 210 1/87 Rev. 1F SEMIVoLATILE ORGANICS ISHEET EPA SAMPLE NO. TENTATIVELY IDENTIFIED COMPOUNDS II N:.I Contract: 68-D9-0048 BFF70 1 I Lab Code: INTI= Case No.: 15486 SAS No.: SDG No.: BFF66 matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30.1 (g/mL) G Lab File ID: B3914 Level: (low/med) LOW Date Received: 12/ 6/90 a Moisture: not dec. 5. dec. 5. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) soNC Date Analyzed: 12/18/90 GPC. Cleanup: (YIN) N pH: 6.9 Dilution Factor: 1.00 Number TICS found: 16 CONCENTRATION UNITS: II (ug/L or ug/Kg) UG/KG I CAS 1=ssm=s==aasass=sla:sss=aa=ss=:s===== NUMBER I COMPOUND NAME1 I I I RT I EST. CONC. I I Q I _ s==$==s3sl:ss=sssslsaass:=== (UNKNOWN ===al=====I 1 2. - 1 UNKNOWN 1 4.04 1 3000. 1 1 3. -- (UNKNOWN 1 5.67 1 500. 1 J 1 1 4. -- IUNKNOWK 1 6.87 1 300. 1 J I 1 5. -- (UNKNOWN 1 7.91 1 1000. 1 J I 1 6• -- (UNKNOWN 1 23.56 I 100. 1 J I 1 7. 544-63-81Tetradecanoic acid (9C1) I 25.86 I 200, I J I 1 8. - - (UNKNOWN 1 26.13 ( 200. 1 J I I 9. 2136-70-11Ethanol, 2-(tetradec lox I Y 1 28.07 I 29.78 100. 1 J I 1 10. - - (UNKNOWN Y1 ( 300. 1 J i I I1. 1 12. -- (UNKNOWN HYDROCARBON 1 31.81 1 35.30 1 -300. 1 J I - - (UNKNOWN ------1 300. I J I 1 13. _ IUNKN®WN 1 35.45 I 100. 1 J 1 1 14. -- IUNKNOWN 1 35.68 I 200.- 1 J 1 1 15. 83-46-51.beta.-Sitoater0.1 1 36.85 1 600. 1 J I 1 16. - - 1UNKNOWN. 1 37.33 ( 500. I J I 1 17.1 1 38.54 I 200. 1 J N I 118. I ------- _I 1 19. 1 I 1 20. 1 21. I I I 1 1 22. I I I I 1 23. 1 1 I 1-I 124. I 25. ( ( 1 I I 11 26. I I 1 I I 1 2 7. I I 128. 1 I 1 I -i I 1 29. 130. I 1 I I I FORM I SV -TIC 210 1/87 Rev. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECK gab Code: INTECH Case No.: 15486 -Iatrix: (soil/water) SOIL Sample wt/vol: 3 0.2 ( g/mL ) evel: (low/med) LOW $ Moisture: not dec. 36. dec. (traction: (SepF/Cont/Sone) SONC G 36. -?C Cleanup: (YIN) N PH: 5.3 OV EPA SAMPLE N0. I I Contract: 68-D9-0048 j BFF71 I I SAS No " SDG No.: BFF66 Lab Sample ID: Lab File ID: B3899 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed ` /17/90j Dilution Factor: 4.00 CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug Kg) UG/KG I p I 108-95-2 ------- Phenol I I '111-44-4 ------- bis(2-Chloroeth 1 I 2000. IU I I 95-57-8 ------- 2_Chlozophenol Y )ether _-I 2000. IU. I I 541-73-1 ------- I 2000. 1 106-46-7 ------- 2'3'Dichlorobenzene �I IU I '4 -Dichlorobenzene I 100-51-6 ------- 2000, IU I Benzyl alcohol -I 2000. IU I I 95-50-1 ------- 1,2_Dichlorobenzene 1 2000. IU I 95-48-7 ------- 2-Methylphenol _I 2000. IU I I 108-60-1-----__bis(2-Chloroiso I 2000. IU I I 106-44-5_____-_4_Methylphenol proiY )ether I 2000. IU I I 621-64-7 ------- N_Nitsoso-di-n- 1 2000. IU I 67-72-1-______Hexachloroethane opYlamine_I 2000. IU I 98-95-3 ----___Nitrobenzene I 2000. IU I 78-59-1 ------- Isophorone I 2000.I I 88-75-5------- IU I ! 105-67-9-______2-Nitrophenol I 2000. IU I 2,4-Dtsethylphenol I 2000., IU I 65-85-0 ------- Benzoic -acid I 2000. IU I I 111-91-1 ------- bis(2-Chloroethox _� 9900. IU I 120-83-2---12 �2, 4_Dtchloroeih-o l )m thane 2000. I U I I 120-82-1-- Phenol ( 2000'. IU I 91-20-3- `.w-lraphtdTrlch I 2000. 1 106-47-6- IU I 4-Ch1 2000. IU I I 87-68-3----___Hexachlorobutadiene 1 10000. 1 I 59-50-7---____4-Chloro-3-meth 1 2000. IU I 91-57-6 ------- Ylphenol I I 77-47-4_______2-Hethyinaphthalene _1 2000, IU I 88-06-2- 2000,..- 1 2000-•.' IU... I I 95-95-4----___2'4'6-Trichlorophenol _1 2000.. IU I 2.4,5 -Trichlorophenol 1 2000. IU I I 91-58-7 ------- 2_Chloronaphthalene 1 9900... IU I I 88-74-4-------2-Nitroaniline. 006: IU I 99 131-11-3 ------- Dimethylphthalate 00&- IU I 208-96-8---____ACenaphthylene I 2000. I I 606-20-2- 1 IU I I IU 2000. IU I I 2000. IU I FORM I SV -1 1/87 Rev. r Ic SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET lName: INT2=, Contract: 68-D9- bats 0048 Lab Code: INTECK Case No.: 15486 SAS No.: Matrix: (soil/water) SOIL Sample vt/vol: 30.2 (g/mL) G Level: (low/med) LOW Moisture: not dec. 36. dec. 36. Extraction: (SePP/Cont/Sone) SONC GPC Cleanup: (YIN) N pH: 5.3 EPA SAMPLE NO. ------------- i I I BFF71 I I SDG No.: BFF66 Lab Sample ID: Lab File ID: B3899 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 Dilution Factor: 4.00 • CAS NO. COMPOUND CONCENTRATIOK UNITS: (ug/L or ug/Kg) UG/KG I Q 1 99-09-2 ------- 3-Nitroaniline I I I 1 83-32-9 ------- AcenaphtheneI 9900. 1U I 1 51-28-5------- Z,4-Dinitrophenol I 2000. IU I 1 100-02-7 ------- 4-Nitrophenol 1 132-64-9 ------- Dibenzofuran I 9900. I U 1U 1 121-14-2 ------- 2,4-Dtnitrotoluene I 2000. ( 2000. I IU 1 84-66-2 ------- Diethylphthalate I 1 7005-72-3 ------- 4-Chlorophenyl-phenylether_1 I 2000. 2000. IU I IU 1 86-73-7 ------- Fluorene I 1 100-01-6 ------- 4-Nitroaniline ( 2000. IU I 1 534-52-1 ------- 4,6-Dinitro-2-methylphenol_I I 9900. 9900. IU I IU 1 86-30-6 ------- N-Nitrosodiphenylamine (1)_1• 2000. I IU 1 101-55-3-= ----- 4-Bromophenyl-phenylether 1 118-74-1 ------- Hexachlorobenzene _I• 2000. I iU I 1 87 -86 -5 -------pentachlorophenol I 2000. I 9900. 1U 1 85 -01 -8 -------Phenanthrene IU 1 1 120 -12 -7 -------Anthracene I 2000. IU I 1 84-74-2 ------- Di-n-butylphthalate I 2000. IU I 1 206-44-0 ------- FluorantheneI- I 2000.. IU I I 129-00:-0 ------pyrene. 2000. IU I 85-68-t!-------Butylbenzylphthalate1 1 320. 1 J I I 91-94-*--i-----3,3'-Dichlorobenzidine_I I 56-55-30�------ Benzo(a)anthracene 450. 4100. 1 J IU 218-01-9-------Chrysene 1 2000. 1U 1 1 117-81-7 ------- bia(2-Ethylhexyl)phthalate_1 I 117-84-0-------Di-n-octylphthalate. 1 420.. .ZOOd i8$A, 1 J I�(�I 2000. IU Z- I �I 1 205-99-2 ------- Benzo(b)fluoranthenet. 1 207-08-9 ------- Benzo(k)fluoranthene_oL 2000. IU 1 50-32-8-------Benzo(a)pyrene 2000. 14 1 1 193-39-5 ------- Indeno(1,2,3-cd)pyrene_ 1 53-70-3 ------- Dibenz(a,h)anthracene I. 590. _I, 2000. 1 J 1 IU 1' I _(._•_ 1 191-24-2 ------- Benzo(g,h,i)perylene_I 1I 2000.. 2000. IU I IU (1) - Cannot be separated from diphenylamine I I FORK I SV -2 239 1/87 Rev. lF gZMrV0LATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Lab Code: INTECK Case No.: 15486 ,,tzix: (soil/water) SOIL Sample wt/vol: . 30.2 (g/mL) G Level: (low/med) LOW Contract: 68-D9-0048 Moisture: not dec. 36. dec. 36. Extraction: (SepF/Cont/Sone) SONC GPC Cleanup: (YIN) N pH: 5.3 EPA SAMPLE NO. I I I BFF71 I I 1 SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: B3899 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 Dilution Factor: 4.00 Number CONCENTRATION UNITS: TICS found: 24 - (ug/L or ug/Kg) UG/KG I I CAS I I NUMBER I COMPOUND NAME I I RT I EST. CONC. I I 1 0 1 I.=asas__sasssammissszsasaa.ssa�_oaa_sssasas:slaasssssslassxaas=:rsaalassaal 1 1. 464-17-51Bicyclo(2.2.11hept-2-ene, 1,1 8.22 1 2000. 1 J N 1 1 2. 3320-83-OIBenzene, 1-chloro-2-isocyanal 10.55 1 8000. I J 1 1 3. 5392-82-51Benzene, 1,4-dichloro-2-isocl 13.83 1 2000. 1 J 1 1 4. 95-76-11Benzenamine, 3,4-dichloro- (1 16.02 1 4000. 1 J I 1 5. 294-62-21Cyclododecane (8CI9CI) 1 17.76 1 2000. 1 J 1 6. -- (UNKNOWN 1 20.20 1 3000. 1 J 1 1 7. 104-40-51Phenol, 4-nonyl- (9CI) 1 20.44 1 3000. 1 J 1 1 8. -- (UNKNOWN 1 20.51 1 2000. 1 J 1 1 9. 25154-52-31Phenol, nonyl- (8C19CI) I 20.59 1 2000. 1 J 1 1 10. 1632.8-62-412H-Imidazo(4,5-blpyridin-2-o1 20.73 1 2000. 1 J I 111. -- (UNKNOWN 1 20.79 1 2000. 1 J 1 1 12. 294-62-21Cyclododecane (8CI9CI) I 20.85 1 4000. 1 J 1 1 13. -- (UNKNOWN I 20.91 1 2000. 1 J I 1 14. -- IUNKNOVN I 23.11 1 6000. 1 J 1 15. 295-65-81Cyclohexadecane (8CI9CI) I 23.63 1 2000. 1 J 1 1 16. 57-10-31Hexadecanoic acid (9CI) 1 23.84 1 4000. 1 J 1 1 17. 544-76-31Hexadecane (8CI9CI) .I 25.27 1 2000. 1 J 1 1 18. 111-14-81Heptanoic acid (8CI9CI) 1 26.29 1 8000. 1 J 1 1 19. --=IUNKNOVN. 1 35.46 1 8000. 1 J 1 1 20. --`IUMKNOVN 1 35.71 1 1000. 1 J 1 21. - (UNKNOWN 1 36.60 1 8000. I J 1 22. -- IUNKNOVN 1 3 7.07 1 2000. 1 J I 23. -- IUNKNOVN 1 38.34 1 2000. 1 J I 1 24. -- (UNKNOWN 1 38.89 1 1000. 1 1 1 25. I I I I I 26. I I I I I 1 27. I 1 I I I ' 28. I I I I I 29. I I 1 I I 30. 1 I I I I I FORM I SV -TIC 240 1/87 Rev. 1B SSMIVOLATIL$ ORGANICS ANALYSIS DATA SHZZT Lab Name: INTEL -H Contract: 68-D9-0048 Lab Code: INTECK Case No.: 15486 SAS No.: Matrix: (soil/water) SOIL Sample wt/vol: 30.7 (g/mL) G Level: (low/med) LOW = % Moisture: not dec. 2. dec. Extraction: (SepF/Cont/Sonc) SONC EPA SAMPLE N0: I I I BFF72 I ___ SDO No.: BFF66 Lab Sample ID: Lab File ID: B3900 Date Received: 12/ 6/90 2. Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 GPC Cleanup: (Y/N) N pH: 6.6 Dilution Factor: 4.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kq) UG/RG Q 1 I 1 108 -95 -2 -------Phenol 1 1300. I I IU I 1 111-44-4 ------- bis(2-Chloroethyl)ether I 1300. IU 1 95-57-8-------2-Chlorophenol I 1300. IU 1 541-73-1-------1,3-Dichlorobenzene I 1300. IU 1 106-46-7-------1,4-Dichlorobenzene I 1300. IU 1 100 -51 -6 -------Benzyl alcohol I 1300. IU 1 95-50-1-------1,2-Dichlorobenzene I 1300. IU 1 95-48-7 ------- 2-Methylphenol I 1300. IU 1 108-60-1 ------- bis(2-Chlorcisopropyl)ether 1 1300. IU 1 106-44-5 ------- 4-Methylphenol I 1300. IU 1 621-64-7 ------- N-Nitroso-di-n-propylamine_I 1300. IU V 67-72-1 ------- Nexachloroethane 1 1300. IU 1 98 -95 -3 -------Nitrobenzene I 1300. IU 1 78-59-1 ------- Isophorone I 1300. IU I 88-75-5 ------- 2-Nitrophenol I 1300. IU I 105-67-9-------2,4-Dimethylphenol I 1300. IU I 65 -85 -ice. ------Benzoic acid I 6400. IU I 111-9--b1s(2-Ch1oroethoxy)aethane_I 1300. IU I 120-6 ---2,4-Dichlorophenol I 1300. IU I 120-6 ----2,2,4-Trichlorobenzene I 1300. IU I 91-2 �_---Naphthalene-• 1 1300. IU 1 106-44 .---4-ChloroaniIIna I 280. 1 J 1 87-66;4�=---Nexachlorobutadiene _t 1300. IU 1 59-50-7=------4-Chloro-3-methylphenol- I 1300. IU 1 91-57-6-------2-Methylnaphthalene --- I 1300. IU 1 77-47-4 ------- Nexachlorocyclopentadiene _I .1300. IU 1 88-06-2-------2,4,6-Trichlorophenol--- I 1300. IU 1 95-90-4 ------- 2,4,5-Trichlorophenoi-_I .6400. IU 1 91-5t--7 ------- 2-Chloronaphthalens I 1300.. IU k 88-74-4 ------- 2-Nittoaniline. I 6400. IU l 131-11-3 ------- Dimethylphthalate I -,1300. IU 1 208 -96 -8 -------Acenaphthylene 1. 1300. IU 1 606-20-2 ------- 2,6-Dinitrotoluene I 1 I_ 1300': IU I I it 308 FORM I SV -1 1/87 Rev. SBMIVCLATILE Lab Name: INTECIi Lab Code: INTBM ORGAKIC� �ALYSI3 DATA SHEET Case NO.: 15486 Matrix: (soil/Water) SOIL Sample wt/vol: 30.7 (9/mL) Level: (low/med) LOV % Moisture: not dec. 2._ dec. F P Extraction: (Se /Cont/Sonc) SONC GPC Cleanup: (YIN) N PH: CAS N0. COMPOUND G 2. 6.6 EPA SALE NO. I Contract: 68-0-0048 BPP72 1 I SAS No.: 1 SDG No.: BPP66 Lab Sample ID: Lab File ID: B3900 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 Dilution Factor: CONCENTRATION UNITS: (ug/L or uq/Kq) UG/KG I 89-09-2 -3-Nitroanil I 4.00 C -32-9------- Arena ine 1 -1 1 -------51-28-5 ------- Phthene 6400. IU 1 101-02-7---____2'4-D1nitrophenol I 1300. IU 1 'I 132-64-9---___ 4-Nitzophenol 1 6100. IU I I 121-14- __ -Dibenzofuran 1 6400. -IU I 2- "'-2,4-Dinitrotoluena 1 I 8l-66-2------- 1300. IU I 1 7005-72_3_______ Diethyiphthalate 1 1300. IU I 86-73-7-_-____4-Chlorophenyl_Phen lethes_I 1300. IU I 100-01-6---____Fluorene y I 1300. IU I 1 534-52-1______-46-Dln aniline I 1300. IU 1 86-30-6-------4'6-Dinitro-2-Wathylphenol i 6400. IU I 101-55-3 ------- N-Nitrosodiphenylamine (1)_I 6400. IU 118-74-1-------4-8 oWaPhenyl-Phenylether -1 1300. IU 1 87-86-5---____HlxachlOrobenzene -1 1300. IU 1 85 -01 -8 ---____Pentachlorophenol 1 1300. IU 1 120-12-7 ------- Phenanthrene 1 6400. IU I I 84 -74 -2 -------Anthracene 1300. IU I 206-44-0 ------- D3-n-butylPhthalate 1300.- IU I 129-00-0---___Pluosantheno -1 1300;- IU I 85-68-7- pyrene I 1300. IU I I 91-94- Hutylbenzylphtha,at, 1300-. IU 1-`"-"3.3'-Dichlosobenzidine -" 1300. I 56-55-3-�..�_-_ I U I I 218-01-9--.•,_ 8enza(a)anthsacene 2600. IU I 117-8i-7--:_--irl+iene I 1300. I U I I 117-84_0_______br (2-lethylhexyl)phthalate 1 1300. IU I I 205-99-2------- D!-R-octylphthalate .I _14w. 1 207 -08 -9 -----__Ben o(b)fluoranthene __-----1 1300. IU 1 50-32-8---____ Benso (k ) fluoranthene�I 1300. IU 1 193-39-5-------Benzo(a)pyrene ��.I 1300. IU I 53-70- Indeno(1,2,3-cd pyrene 1 1300. IU I 191-24_2_______ eebeoz(a,h)anthraesn• �� 1300. IU I (q.h,.i)Desylene�l . IU I CannoI 1300'•- I U t be separated I Parated froo diphenylamine FORM I SV -2 309 1/87 Rev. 1F EPA SAMPLE NO. TSNDATA TATIVELYORGNICS IDENTIFIEDICOMPOUNDSEET I I BFF72 Contract: 68-D9-0048 I 1 I lb�00 0 INT209 Case No.: 15486 SAS No.: SDG No.: BFF66 Irab Code get=ix: (soil/water) SOIL Lab Sample %D: Sample wt/vol: 30.7 (g/mL) G Lab File ID: B3900 Level: (low/med) LOW Date Received: 12/ 6/90 4 Moisture: not dec. 2. dec. 2. Date Extracted: 12/ 7/90 8xtraction: (SepF/Cont/Sonc) SONC Date Analyzed: 12/17/90 GPC Cleanup: (YIN) N pH: 6.6 Dilution Factor: 4.00 Number T%Cs found: 10 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/KG I I I I I I I CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I Q I Issssssssssssassslssss:ssssssssssssss:sasssssslmssssssslssassassssssslssss�fi( I 1. 67-64-112-Pro.panone (9CI)1 5.73 1 500. 1 J N 1 1 2. -- 1UNKNOWN 1 7.95 1 800. I J I 1 3. 57-10-31Hexadecanoic acid (9CI) 1 23.77 I 500. I J t 1 4. 10544-50-OISulfur, mol. (38) (8C19CI)_1 24.78 ( 7000. f J 1 1 5. - 1UNKNOVY 1 32.78 1 2000. I J I 1 6. --' I UNKNOTAt 1 33.04 1 1000. I J I 1 7. - 1UNKNOW. 1 34.55 1 700. I J I 1 8. -- 1UNKNOVN 1 35.45 1 5000. I J I 1 9. - 1 UNKNOWN 1 35.71 1 2000. I J I 1 10. -- IUNKNOVN 1 36.59 1 4000. 1 J N 1 111. I 1-1 11 1 12. 1 I I I I 113. 114. 1 15. 1 16. 117. 118. { I I I I 1 19. I I I I I 1 20. I I I I I 1 21. I I I I 122. 1 23. 129. 125. I 126. 1 2®7. I I 0 I I 1 28s 1 129. I 1 30. I I FORM I SV -TIC 310 1/87 Rev. SEMIVOLATILE ORGANICSBANALYSIS DATA SHEET Lab Name: INTM Lab Code: INTZCA Case No.: 15486 Matrix: (soil/water) SOIL Sample wt/vol: 30.5 (g/mL) G Level: (low/med) LOW % Moisture: not dec. 9. M. dec. 9. Extraction: (SePP/Cont/Sonc) SONC GPC Cleanup: (YIN) N pH: 6.7 EPA SAMPLE NO. I1 Contract: 68-D9-0048 I BFF73 SAS NO.: SDO No.: BFF66 Lab Sample ID: Lab File ID: B3894 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/90 Dilution Factor: 1.00 CAS N0.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) I UG/KG 0 I 108 -95 -2 -------Phenol ( I I I 111-44-4 ------- bis(2-Chloroethyl)ether1 I 95-57-8-------2-Chlorophenol 1 360. 360. IU I IU 541-73-1 ------- 1p3_D1chlorobenzene 1 360. I IU I I 106-46-7 ------- 1�4_Dichlorobenzene1 I 100 -51 -6 -------Benzyl I 360. 360. IU I IU I alcohol 95-50-1 ------- I 1'2- Dichlorobenzene '95-48-7 360. I IU I ------- I 2-Methylphenol 1 108-60-1 ------- bis(2-Chloroisopsopyl)thes 3.40. 360. IU IU e 106-44-5 ------- 4-Methylphenol 360. I IU I 1 621-64-7 ------- N_Nitzoao-di-n-propYla4lne 1 67-72-1 ------- Hexaehloroethane -1 360. 360. IU IU I 98 -95 -3 ------_Nitrobenzene I 360. IU I I- 78-59-1 ------- Iso horone I 360. IU I 88-75-5 ------- 2-Hitrophenol 1 t 105-67-9 ------- 2-*4_Dimthylphenol 1 360. 360. IU I IU I I 65-85-0 ------- Benzoic acid _1 360. IU I 111-91-1 ------- bla(2-Chlorosthoxy)eethane 1 I 120-83-2 ------- 2v4_Diehiorophenol -1 1700. 360. IU IU 120-82- -----1,2,,4.-Tr1chlorobenzene 1 91 -20+► 360' 360. IU -__Naphthalene- - �1 106-47-#4-Chloroarriline 1 87-68-----Hexachlozobutadi• 360. I U IU 1 59-50-7'•-----4-Chloro-3-methylphenol I 1 360. 360. IU I IU 91-57-6 ------- 2_NOthylnaphthalene"-1 1 77-47-4 ------- Hexachlorocyclopentadiene I 360• 360. IU IU 1 88-06-2-------2,4,6-Trichlorophenol -I 1 360. IU 95-95-4-------2,4,5-Trichlorophenol -�I I 91-58-7 ------- 2_Chloronaphthalens �-I 360. 1700. IU IU I 88-74-4 ------- 2_Nitroaniline I 360. IU 1 131-11-3 ------- Dlaothylphthalate1 '1 208 -96 -8 -------Acenaphthylene ---1 1700. 360. IU I IU. I 1 606-20-2 ------- 2,6-Dinitrotoluene 1 1 360. IU I I 360. IU I I - FORM I 8v-� "' I 1/87 Rev. I 1C EPA SAMPLE NO. SSMIVOLATILB ORGANICS ANALYSIS DATA SHEET I : IN!>�9 Contract: 68-D9-0048BFF73 ICX I : INTECA Case No.: 15486 SAS No.: SDG No.: BFF66 (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30.5 (g/mL) G Lab File ID: B3894 Level: (low/med) LOW Date Received: 12/ 6/90 1 Moisture: not,dec. 9. ""dec. 9. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sone) SONO Date Analyzed: 12/17/90 GPC Cleanup: (YIN) N pH: 6.7 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) I UG/KG 0 1 99-09-2 ------- 3-NitroanilineI I I 1 83 -32 -9 -------Acenaphthene I 1700. ITl I I 51-28-5-------2 ,4-Dinitrophenol I 360. I -U" I 1 100-02-7 ------- 4-Nitrophenol I 1700. IU I 1 132-64-9 ------- Dibenzofuran I 1700. IU I 1 121-14-2 ------- 2p4-Dinitrotoluene 360. ju I 1 84-66-2 ------- Diethylphthalate I 360. lU 1 7005-72-3 ------- 4_Chlorophenyl-phenylethex_) I 360. lU I 1 86-73-7 ------- Fluorene 360. IU I 1 100-01-6 ------- 4-Nitroaniline I 360. IU 1 534-52-1 ------- 4,6-D1nitro-2-methylphenol_I I 1700. IU 1 86-30-6 ------- N-Nitrosodiphenylamine (1)_I 1700. Iu 1 I 101-55-3 ------- 4-Hromophenyl-phenylether 360. 360. IU _) 118-74-1 ------- Hexachlorobenzene IU 1 1 87 -86 -5 -------Pentachlorophenol I 360. IU 1 85 -01 -8 -------Phenanthrene f 1700. IU 1 120 -12 -7 -------Anthracene I 360. IU 1 84-74-2 ------- Di-n-butylphthalate I 360. lu �i 1 206-44-0 ------- •luoranthene 67. 1 J 1 129 -00 - -------Pyrene I 360. IU I ' 85-00-7-------Butylbenzylphthalate ( 360. l _i I 91--1_Dichlorobenzidine__I I 56-�►.-____ 360. 710. IUu I IU 1 Benzo(a)anthracene 1 218-0t-�----__Chzyaene I 360. IU I 117-82-7 =------ bis (2-Sthylhexyl) phthalate -1 1 117-84-0 -------- Di-n-octylphthalate I 360. 3GO '?0. IU I I -i-AJ __I 1 205-99-2 ------- Senzo(b)fluorantheneI 360: 360. IU 1 207-08--9 ------- Benzo(k)fluoranthene_I 360. lU I 1 50-32-8----__-Benzo(a)pyrene 360. IU I 1 1 193-39-5 ------- Indeno(1,2,3-cd)pyrene__I 360. lu 360. I 53-70-3 ------- D1benz(a,h)anthracene. r 360. 1 191-.24-2 --_--_-Benzo(g,h,i)per IU IU I i Y len• K% _ 360. I U i Cannot be se I : parated from diphenylasine I I 3 26 FORM I SV -2 1/87 Rev. 1)Ir 00ORGANICS ORGANICS ANALYSIS DATA SHENT IiTATIVSLY IDENTIFIED COMPOUNDS 1 _ Cane NO.: 15486 (soil/ester ) SOIL a`x= - is vt/vol .. 30.5 ( 9/mL ) G Oval: (.low/med t LOW s Molature: not dec. 9. _ dee. 9. Xxtraction: (SepF/Cont/Sone) SONC GPC Cleanup: (YIN) N pH: 6.7 Contract: 68-D9-0048 SAS No.: BPA SAMPLZ NO. I 1 I BFF73 I I I SDG No.: BFF66 Lab Sample ID: Lab -File ID: B3894 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/17/g0 Dilution Factor: 1.00 Number TICS found: 8 CONCENTRATION UNITS: I (uq/L or uq/Kq) UG/KG 1 I CAS NUMBERI COMPOUND NAM RT II I lsssassss:s:=sasslsss:ssssasssssssslsasEI1 :s sI1 I 1. T.0ONC. I Q I I 2. EST. IUNKNOVN I 4.67 1 2 0 0. I J 1 3. - - 1UNKNOVU 1 5.67 1 .600. I 1 4. 565-69-513-Pentanons, 2 -meth 1_ I 6.04 1 1 J I 1 5. Y (8CI91 6.86 1 100. 1 J I 1 1 6. 10544-50-013ulfurp7.8q" 1 mol. (S8) (8CI9CI 400. 1 J 1 7. 1 I 800. I J - - I UNKNOVw )®1 24.60 1 200. 1 J 1 I S. -- 1UNKNOvy I 26.16 1 I 9. 100. 1 J f 1 I 36.50 I 1000. 1 J I I 10. I I ( � I 111. I i 1 12. 1 13. I I I I I 1 14. I I 115. I I 1 16. 1 17. 118. 1 I®I I I 1 19. I 1 -i I I 1 20. 1 1-1-1 .I I 1 21. ( 1 I I t I I I 122. I 1 1 23. 1 24. 1 25. 1 I 1 1 26. 1 I -I----------- 27. 27. I I-------- 29. -29. 1 30. I 1 FORM'I SV -TIC 3 0? 1/87 Rev. 1B SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECW- Lab Code: INTECR Case No.: 15486 - Matrix: (soil/water) SOIL EPA SAMPLE NO. 1 I BFF74 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 Lab Sample ID: Sample wt/vol: 30.1 (q/mL) G Lab File ID: B3913 Level: (low/med) LOW _ Date Received: 12/ 6/90 Moisture: not dec. 10. dec. 10. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sone) SONC Date Analyzed: -12%18/90 GPC Cleanup: (YIN) N pH: 5.2 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or uq/Kq) uG/ICG Q I I I 108 -95 -2 -------Phenol I 370. I I lu I 1 111-44-4 ------- bis(2-Chloroethyl)ether I 370. lu I 1 95-57-8-------2-Chlorophenol ( 370. .lu I 1 541-73-1-------1,3-Dichlorobenzene 370. Iu I _.I 1 106-46-7-------1,4-Dichlorobenzene ! 370. IU 1 100 -51 -6 -------Benzyl alcohol I '95-50-1-------1,2-Dichlorobenzene 370. lu I 1 3.70. IU I �i 1 95-48-7 ------- 2-Methylphenol I 370. IU 1 108-60-1 ------- bls(2-Chlorcisopropyl)ether 1 370. lu 1 106-44-5 ------- 4-Methylphenol 1 370. lu 1 621-64-7 ------- N-Nitroso-di-n-propylaaine_I 370. lu 1 67-72-1 ------- Hexachloroethane 1 370. lu I- 98 -95 -3 -------Nitrobenzene I 370. to 1 78-59-1 ------- Isophorone ( 370. lu 1 88-75-5 ------- 2-Nitrophenol ( 370. lU 1 105-67-9-------2,4-Dimethylphenol I 370. lu 1 65-85-0 ------- Benzoic acid I 1800. IU 111-91-1 ------- bis(2-Chloroethoxy)methane_I 370. Iu I 120-83-2r------2,4-Dichloropheno1 I 370. lU 1 120-82' x=-----1,2,4-Trichlorobenzene I 370. IU 1 91-2.`' ----Naphthalene I 370. lu 1 106-47- =----4-Chloroaniline I 370. IU 1 87-68- =---.-Hexaehlorobutadiene 370. IU �I I 59-50-7-------4-Mloro-3-mthylphenol I 370. lu 1 51-57-6-------2-Methylnaphthalene 1 370: lu _I 1 77-47-4 ------- Hexachlorocyclopentadiene 370. IU I _I 1 88-06-2-------2,4,6-Trichlorophenol 370. lu _1 1 95-95-4-------2,4,5-Trichlorophenol I 1200. IU 1 91-58-7 ------- 2-Chlozonaphthalene I 370. IU 1 88-74-4 ------- 2-Nitroaniline I 1800. IU 1 131-11-3 ------- Dimethylphthalato ! 370.. IU 1 208 -96 -8 -------Acenaphthylene I 370: lu 1 606-20-2 ------- 2,6-Dinitzotoluene I 1 I 370. IU I I FORM I 3V-1 340 - 1/87 Rev. SZMIVOLATILS ORGANICS ANALYSIS DATA SHEET EPA SAMPLE N0. Contract: 68-D9-0048 I BFF74 lb aar: I ( Lab Code: INTI= Case No.: 15486 SAS No.: SDG No.: 8FF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30.1 (g/mL) G Lab File ID: 83913 Level: (low/med) LOW Date Received: 12/ 6/90 % Moisture: not dec. 10. dec. 10. Date -Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) SONO Date Analyzed: 12/18/90 GPC Cleanup: (YIN) N pH: 5.2 Dilution Factor: 1.00 CAS N0.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) I UG/KG 0. 1 99-09-2 ------- 3-Nitroaniline 1 I I 1 83 -32 -9 -------Acenaphthene I 1800. IU I 1 51-28-5 ------- 2,4-Dinitrophenol 1 370. IU I 1 100-02-7 ------- 4-Nitrophenol I 1800.. IU =' I 1 132-64-9 ------- Dibenzofuran ( 1800. 1U I 1 121-14-2 ------- 2 '4-Dinitrotoluene I 370. IU I I 84-66-2 ------- Diethylphthalate I 370. IU I 7005-72-3 ------- 4-Chlorophenyl-phenylethes_I I 370. IU I 1 86-73-7 ------- Fluorene 370. IU I 1 100-01-6 ------- 4-Nitsoaniline I 370. IU I 1 534-52-1 ---- 4'6-Dinitro-2-methylphenol-I I 1800. IU I I 86-30-6 ------ N-Nitrosodiphenylanine (1)-I 1800. IU I 1 101-55-3 ------- 4-Bro®ophenyl-phenylether 370. IU 1 118-74-1 ------- Rexachlorobenzene -1 370. IU 1 87-86-5 ------- Pentachlorophenol 1 3700 IU 1 85-01-8 ------- phenanthreneI 1800. IU i 1 120-12-7 ------- Anthracene I 370. IU I 1 84-74-2------_Di-n-butylphthalate i 370• IU I 1 206-44-0 ---- ___Fluoranthene ( 370. IU 129-00+0� ------ Pyrene I 370. IU I 85-6a='�------_Bntylbenzylphthalate I 370. IU I 91-98-t- nne ,----__3,3'-Dichlorobenzidi 56-30�,t+_-___)�nzota)anthracene 370• 730. IU lU I -I I 218-01-9---_Chrysene I 370. IU I 1 117-81-7 ------- bis(2-Ethylhexyl)phthalate_I 370. ju 1 117-84-0 ------- Di-n-octylphthalat• 370. IU l 205-99-2------- Senzo(b)fluoranthene 370• tU1 207-08-9 ------- Benzo(k)fluoranthen-­�I 370. --Iu1 -� 50-32-8 ------- Benzo(a)pyrene1 370. IU1 193-39-5-------Inden®(1,2,3-cd)pyrene 370.. II IU 1 53-70-3 ----- __pibenz(a,h)anthracene_370._ IU 1 191-24-2 ------- Benzo(g,h,i)pes lene .370.- IU 1 370.. I U I (1) - Cannot be separated from diphenylasine I I 1 FORM I SV -2 341 1/87 Rev. 1F 8X,1V0InWISHEET ATIVELY IDEN IFIEDCOMPOUNDS Contract: 68-D9-0048 a Case Ne.: 15486 SAS No.: Cie: aNT$� EPA SAMPLE NO. I I I BFF74 I I I SDG No.: BFF66 x: (soil/meter) SOIL Lab Sample ID: Pe+tri se�10 at/vol: 30.1 (g/mL) G Lab File ID: B3913 Level: (loan/med) LOW Date Received: 12/ 6/90 S Moisture: not dec. 10. dec. 10. Date Extracted: 12/ 7/90 Nxtraction: (SepF/Cont/Sonc) SONC Date Analyzed: 12/18/90 GpC Cleanup: (YIN) N pH: 5.2 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 25 (ug/L or ug/Kg) UG/KG I I CAS I I NUMBER I COMPOUND NAME I RT I I EST. CONC. I I 1 0 I lassssssssssssssslasssssssssasaaasasssassassasl:sssssaalas:s::asses:slasaasl 1. - - 1UNKNOWN 1 4.04 1 4000. 1 4-A 1 2. -- 1UNKNOWN 1 7.91 1 1000. - I J I 1 3. -- (UNKNOWN 1 .13.27 1 3000. 1 J 1 1 4. -- (UNKNOWN 1 15.75 1 400. 1 J I 5. 57-10-31Hexadecanoic acid (9CI) I 23.70 1 500. 1 J I I 6. 544-63-81Tetradecanoic acid (9CI) 26.14 1 400. 1 J I 1 7. -1 19047-85-91Phosphonic acid, dioctadecyll 27.62 1 400. 1 J I 1 8. 593-49-71Heptacosane (8CI9CI) 1 27.66 1 700. 1 J I 1 9. 629-60-11Hexadecanal (ACN)(9CI) 1 29.07 1 300. 1 J I 1 10. 19047-85-91Phosphonic acid, dioctadecyll 29.77 1 6000. 1 J 1 11. 57-11-41,Octadecanoic acid (9CI) 1 30.53 1 2000. 1 J I 1 12. 74685-33-913-Ricoseno, M- (9CI) 1 30.84 1 400. 1 J 1 13. 6624-79-911-Dotriacontanol (8CI9CI) _1 31.81 1 4000. 1 J I 1 14. 506-30-91E1cosanoic acid (8CI9CI) 1 32.51 1 1000. 1 J 1 1 15. 629-80-IIH*xadecanal (ACN)(9CI) 1 33.05 1 100. 1 J 1 1 16. 6624-79-911-Dotriacontanol (8CI9CI) 33.69 1 700. 1 J 1 1 17. _1 -- IUNKNOYN 1 34.58 1 200. 1 J I 1 18. 56554-93-9115-Octadecenal (9CI) 1 34.83 1 200. 1 J I- 1 19. -- 1UNKNOW HYDROCARBON 1 35.31 1 400. 1 J I 1 20. -- IUNKNOYN 1 35.51 1 200. 1 J 1 21. 629-80-118euadecanal (ACN)(9CI) 1 36.51 1 200. 1 J_ 1 22. - - IUNKNOW HYDROCARBON 36.67 1 100. 1 J 1 1 23. _1 -- (UNKNOW 1 37.15 1 300. 1 J 1 1 24, -- IUNKNOWN 1 37.75 1 800. 1 J 1 1 25. - 1UNKNOWN 1 38.11 1 440. 1 J N 1 1 26. 1 27. 1 I I I I 1 28. I I I I I 1 29. I I I I I 1 30. I I I 1 1 1 I I 1 I 1 FORM I SV -TIC 342 1/87 Rev. 93KIVOLATIL& OR1B G"ICS ANALYSIS DATA SHE=? Lab Nam: I NTg= Lab Code: INTZCH Case No.: 15486 Matrix: (soil/water) NATER Sample wt/vol: 1000.0 (g/mL) ML Level: (lor/®ed) LOW t Moisture: not dec. 100. dec. 0. Extraction: (SePF/Cont/Sons) Sgpp OPC Cleanup: (Y/N) N pH-: 8.1 N EPA SAMPLs NO. i 1 Contract: 68-D9-0048 1 BFF75 I SAS No.: SDQ No.: BPC39 Lab Sample ID: Lab Pile ID: 83847 Date Received: 12/ 6/90 Date xxtzacted.: 12/ 6/90 Date Analyzed: 12/14/90 Dilution pactos: 1.00 CAB NO. COMPOUND CONCRNTRAT1ON-UNrTs: (ug/L or u9/xq )- UO/L I .I 108 -95 -2 ------_phenol I I 1 I 111-44-4 ------- bis(2-Chlozoethyl)ether 1 10. IU I 1 95-57-8--- -2-Chlorophenol —! 30. IV I I 541-73-1----=-®1,3-Diehlorobenzae ! it. II► I I 106=46-7 ----- -_1,4-Dichlorobenzenne- I 10. IV I 1 100-51-6 ------ -Benzyi alcohol 1 iD. IV I 1 95-50-1 -------- It2_Dichlorobenzene 1 10. IU I I 95-48-7----___2_Methylphenol ! 10. IU I 1 108-80-1= .._�dis(2=ChToroiso ro 1 ethos j 10. 1U I I 206-44-5----=--4-Meth -1p henoI-. p PY } 10. IU I I-_621-64-7------ Y P d 10. IU 1 1 67-72T1----=--Nitsoso-dt=B-propYlaulne_,! He�cachlesoethane l00 1U I 1 98 -95 -3 ---_le 10. IV I I 78-59-1=-- 1 .a8 -75-s--= Is®1troph6 1 4C iv I __ Z-ltatrophenok- � 10. I V j 0' 163-85-6-r!". —?960201~a acid t 10. IV 1 I 111-91- - _'- bist2-Chlosoethoxy)Mthan� r SO. IV I I 120-83-2,4-pichlosaphenol --1 10' IU I I 120-82 . ' `'=- _1 10. I U :x: 19 2i 4=Trlchlorobenaenw,�-! 30. r I 91-20 10ipbtheIene. IU I 4-ftloroaniline 1 l0'. IV I I 87-6a-3--'---Nexachlosobutadien• t it IV I I S9 -SO -7------- - =[ 10: IV I 1 91-57-6------_4-Ehloso-3-methylphenot _-E 2-t40thytnaphthalen� ZQ: -IU J I I 77-47-4 --- ----Nexachlorocyclopentadienei-- f 1 IV 1 88-06-2-------2,4.6-Trichloso _f 1 ° 1 95-95-4------- _ Phenol l� IV r ------- 2.4. s Trtchioroph60o1 . I 9l-Sa-7 2-Chloronaphthalene rd I 1 88-74-4 -------- 1 —�# 1 131-11-3 ------- Dirthylphthalatet 5�: IV. I 1 208-96-8 ------- Acenaphthylen6 f iV•' IV I 1 606-20-2 ------- 2,6-D1nitsotoiuen6 f 1 1 I U 1 1_1 FORK- I SV=1 - ---- - --- $/87 Rev. i` 1C SBMIVOLATILE ORGANICS ANALYSIS DATA SHEET Lab . Name: INTS H ab Code: INT&M Case No.: 15486- -Atri.x: (soil/water) WATER Sample wt/vol: 1000.0 evel: (low/med) LOW % Moisture: not dec. 100. BPA SAMPLE NO. i I BFF75 1 Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39' (g/mL) ML dec. 0. xtraction: (SepF/Cont/Sonc) SEPF Lab Sample ID: Lab File ID: 83847 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 -PC Cleanup: (YIN) N pH: 8.1 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg} UG/L p I I 1 99-09-2 ------- 3-Nitroaniline I I I I 83 -32 -9 -------Acenaphthene 50. IU 1 I 1 51-28-5 ------- 2,4-Dinitrophenol 10. IU I 1 100-02-7 ------- 4-Nitrophenol 50. IU 1 .I 132-64-9 ------- Dibenzofuran I 50. IU 1 I 121-14-2-------2,4-Dinitrotolnene I 10. IU 1 1 84-66-2-------Diethylphthalate I 20. IU 1 1 7005-72-3-------,-Chlorophenyl-phenylether_I. 10. 10. 1U IU I I 86-73 -- I 10 IU j I 100-O1-�aJ-----W�tso�ni line 1 50. ju 1 534-52-1 ------- 4,6-D1nitro-2-saethylphe.nol_I 50. IU I 1 86-30-6 ------- N-Nitrosodiphenylamine.(1)_I 10. IU i 1 101-55-3 ------- 4-Bromophenyl-phenylether 10. -1 1 118-74-1 ------- Hexachl:orobenzene I 10. IU I IU 1 87 -86 -5 -------pentachlorophenol I 50. IU I 1 85 -01 -8 -------Phenanthrene I 10. lu l 1 -120-12-7-------Anthracene 1 10. IU I 1 84-74-2 ------- Di-n-butylphthalate t. 10. IU I 1 206-44-0-------pluoranthene I 10. IU I I 129 -00 -0~ --_------Pyrene I 10. IU I I 85-68-7------@utylbenzylphthalate_I 10. IU I I 92-94-1-=-----3,3�-Dichlorobenzidine_I 20. IU I 1 56-55-3-------Benzo(a)anthracene I 10. IU I 1 218 -al -9 ------- Chrysene I 10. IU I 1 117-81-7 ------- bis(2-Bthylhexyl)phthalate_0 3. 1 J. I 1 117-84-0 ------- Di-n-octylphthalate _1 10. IU I I 205-99-2 ------- Benao(b)fluoranthene�l 10. IU I 1 207-08-9 ------- Benzo(k)fluoranthene_I 10- IU I 1 50-32-8 ------- Benzo(a)pyreno I IU I 1 193-39-5 ------- Indeno(1,2,3-cd)pyrene_1 .10. 10- IU I 1 53-70-3 ------- Dibenz(a,h)anthracene I •10 1U I 1 191-24-2 ------- Benzo(g,h.i)perylene_ I I , 10.. IU I I (1) - Cannot be separated from diphenylamine 1 1 24? FORM I SV -2 1/87 Rev. 1: 1F EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVBLY 'IDENTIFIED COMPOUNDS I I 1 1 Lab Name: INTECH BFF75 Contract: 68-D9-0048 I Lab Code: INTECH Case No.: 15486 SAS No.: SW No.: BFC39 Matrix: ($oil/water) NATER Lab Sample ID: Sample wt/vol: 1000.0 (g/mL) ML Lab File ID: B3847 Level: (low/med) LON _ Date Received: 12/ 6/90 % Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/14/90 GPC Cleanup: (YIN) N pH: 8.1 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 1 (ug/L or ug/Kg) Uta/L 1 I I I I I CAS NUMBER I COMPOUND NAME 1 RT I EST. CONC. I Q I (ssssssssssssssaalss:asssssssassssssasssssassslsssssssslassssass:sssslsssaffi1 i 1. - 1UNKNONN 1 8.55 I 10. 1 J 1 t a. I I 3. I 4. j l01 1 I 5. I 6. I 7. I 9. I 10. 111. i I I I -I I I 112. I 13. I fir 1 I 114s t 15. 116. I I 117. 118. I I '1 lol I I 119. I 20. F 21. 122. 12 3. 124. 125. 126. 1 27. t 128. 1 29. t 1 30. I FORM I SV -TIC 243 1/87 Rev. 1-1110 1" 1B SEMI` ATILE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECM Lab Code: INTECH Case No.: 15446 Matrix: (soil/crater) WATER Sample-wt/vol: 1000.0• ( g/nig, ) ML Level: (low/mad) LOST EPA SAMPLE NO. 1 1 I BFF76 1 Contract: 68-D9-0048 1 t SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: 83848 Date Received: 12/ 6/90 Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/14/90 GPC Cleanup: (YIN) N pH: 8.3 Dilution Factor: 1.00 CONCENTRATION UNITS-: CAS NO. COMPOUND (ug/L or- ug/Kg )• UG/L Q I 108 -95 -2 -------Phenol I 10. IU I 1 111-44-4 ------- bis(•2=Chloroethyl)ether I 10. IU 1 1 95-57-8 ------- 2-Chlorophehdl I 10. IU I 1 541-73-1 ------- 1,3-Dichlorobenzene'�I 10. IU I 1 106-46-7 ------- ls4-Dichlorobenzene 10. IU I _i I 100-51-6-------Benzy1.:alcoh'ol I 10. IU I I 95-50-1-------11;..-Dichlorobenzene 10. IU I 1 95-548-7 ------- 2-Methylphenol I le. IU I 1 108-60-1------ other I 10. IU I 1 106-44-5 -------- .4-iWity2°Q enolt:. I 10. IU I I 621-64-7-------N"Ri=tslosordl-n-propyiamLne_I, 10. IU I 1 67-72-1 ------- Hexachloroethane 1 10. IU i 1 98-95-3 ------- Nitrobbnzene 1 10. IU I 1 78-59-1 ------- Isopborone I' 10. 1U I I 88-75-5-------2-N1trnpheno1 I 10. IU I 1 -105-67-9 ------- 2,4-Dinethylphenal 1 10. 1U I I 65-85-if-------soic acid 1 50. 1U I I 111-91-------b$s(2-ChloroethoxyYmethane_F 10. IU I I 120-83------2,4-Dichleraphenol' I 10. IU I 1 120-82!"- l,2,4-Trichlorobenzene_1 10. IU I I 91-2o."! -Naphthalene I 10. lU 1 1 106-47-��------4-loroaniline 1 10. lU I I 87-68-3-------Hoxachlorebutadiene 10. IU I _t 1 59-50-7 ------- 4-Chloro-3-methylphenol 1 10. IU I 1 91-57-6-------2-Methylnaphthalene 10. IU I _1 1 77-47-4-------Mexachiorocyclopentadiene 10. IU I _I- 1 88-06-2-------2,4,i-Trichlorophenol I 10. lU I 1 95-95-4-------2,4,.5-Trichlorophenol 50. IU I _F 1 91-58-7 ------- 2-Chloronaphthalene 10. IU I ._1 I 88-74-4----r--2-N.1troaniline 1 50. lU I 1 131-11-3 ------- Dimethylphthalate t 10. IU I 1 208 -96 -8 -------Acenaphthylene 1 10. lU I 606-20-2 ------- 2,6-Dinitrotoluene1 10. 124 IU I I 1 FORM I SV -1 1/87 Rev. f ° 1C SZMIVOLATILR ORGANICS ANALYSIS DATA SHEET ib Name: INTECH Contract: 68-D9-0048 Lab Code: INTECH Case No.: 15486 SAS No.: f trix: (soil/water) WATER Sample wt/vol: 1000.0 (g/mL) ML vel: (low/mad) LOW - f Moisture: not dec. 100. dec. 0. 1sxtraction: (SepF/Cont/Sonc) SSPF ( C Cleanup: (YIN) N pH: 8.3 CAS NO. COMPOUND EPA SAMPLE NO. I I I OFF76 I f I SDG No.: BFC39 Lab Sample ID: Lab File ID: 83848 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L I I 1 99-09-2 ------- 3-Nitroaniline I 1 83 -32 -9 -------Acenaphthene I 1 51-28-5 ------- 2,4-Dinitrophenol I 1 100-02-7 ------- 4-Nitrophenol I 1 132-64-9 ------- Dibenzofuran I 1 121-14-2 ------- 2,4-Dinitrotoluene l 1- 84-66-2 ------- Diethylphthalate° I 1 7005-72-3 ------- 4-Chlorophenyl-phenylether_I 1 86-73-7 ------- Fluorene I 1 100-01-6 ------- 4-Nitroaniline 1. f 534-52-1 ------- 4,6-Dinitro-2-methylphenol_I 1 86-30-6 ------- N-Nitrosodiphenylamine-(1)-1 1 101-55-3 ------- 4-Dromophenyl-phenylother­ _I 1 118-74-1 ------- Hexachlorobenzene f 1 87 -86 -5 -------Pentachlorophenol 1 1 85 -01 -8 -------Phenanthrene I 1 '120 -12 -7 -------Anthracene I I 84-74-2 ------- bi-n-butylphthalate I I 206-44-0-------Fluoranthene I I 129 -00 -0 --------Pyrene I I 85-68-7-�-----Butylbenzylphthalate_I f 91-94-i- 3,3'-Dichlorobenzidine I I 56-55-3-------Bensa(a)anthracene I I 218-02-9-------Chrysene I 1 117-81-7 ------- bis(2-Ethylhexyl)phthalate_I 1 117-84-0 ------- Di-n-octylphthalate _I I 205-99-2-------Benzo(b)fluoranthen _I--- 1 207-08-9 ------- Benzo(k)fluoranthene_I 1 50-32-8-------Benzo(a)pyrene f -.- 1 193-39-5 ------- Indeno(1,203-cd)pyrene I -..R..- 1 53-70-3 ------- Dibenz(a,hranthracene J- 1 191-24-2 ------- Benzo(g,h,i)perylene_I 1 I (1) - Cannot be separated from diphenylamine FORM I SV -2 50. 10. 50. 50. 10. 10. 10. 10. 10. 50. 50: • 10. 10. 10. 50. 10. 10. 10. 10. 10. .10.. 20. 10. 10. 110: 10. 10. 10. 10. 10.- 10-. 10. 24J 1.00 1/87 Rev. / IF SEMIVOLATILB ORGANICS ANALYSIS DATA SHEET TENTATIVELLY IDENTIFIED COMPOUNDS Lab Name: INTECIt Contract: 68-D9-0048 Lab Code: INTI! Case No.: 154.86 SAS No.: Matrix: (soil/water) WATER Sample wt/vol: 1000.0 (g/mL) Mir Level: (low/mad) LOW s Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (YIN) N pH. 8.3 EPA SAMPLE NO. I 1 I BFF76 I I ! SDG No.: BFC39 Lab Sample ID: Lab File ID: 83848 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilation Factor: 1.00 Ll Number TICS found: 1 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L I I CAS I NUMBER I I I I I COMPOUND NAME I RT I EST. CONC. I Q I Isssssasass:ss:aslasssssassssss:asasasssssassslsssssssslssassasa3as==Isssssl I 1. -- IUNKNOWN I 8.55 1 10. 1 J 1 1 2. I I 1 I 1 3. 1 I I I I 1 4. 1 5. I ! I I I 1 6. I I I I I 1 7. ! I I I I 1 8. I I I I I 1 9. ! I 1 I I 1 10. 1 11. I I I I I 1 12. I I I I I 1 13. I 1 1 I I 1 14. I I I I I 1 15. I I ! I I 1 16. I I I I I 1 17. 1 18. 1 I I I I 1 19. I I I I I 1 20. I I I 1 21. 1 I 1 I I 1 22. I I I I I 1 23. 1 24. I I I I I 1 25. ! I I I I 1 26. ! 1 I I I 1 27. 1 I 1 I I 1 28. I I 1 I I 1 29. I I 1 I I 1 30. I I I I 1 I I I I I I 250 FORM I SV -TIC 1/87 Rev. 1B BPA SAMPLE NO. SZM I VOLATI LE' ORGAN I C8 ANALYSIS DATA SHEET I BFF77 Lab Name: INTECH I contract: 68-D9'-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: 3DO No.: BFC39 matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 1000.0 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sone) SEPF Lab File ID: 83849 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 GPC Cleanup: (Y/N) N pH: 6.9 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND- (ug/L or uq/Kg) UG/L Q I I 1 108 -95 -2 -------phenol 1 10. I I IU 1 111-44-4 ------- bis(2-Chloroethyl-)ether I 10. .1 IU 1 1 95-57-8-------2-Chlorophenol 1 10. IU I 1 541-73-1-------1.,3-Dichlorobenzene _I 10. 1U I 1 .106-46-7-------iB4-Dichlorobenzene 1 10. IU i 1 100-51-6 ------- Benzyl=alcohol I 10. IU I I 95-50-1 ------- 1,2` -Dichlorobenzene• I 10. 1U I 1 95-48-7 ------- 2-Methylphenol I 10. IU I 1 108-60-1 ------- bis(2-Chloroisopropyl)ether 1 10. IU I 1 106-44-5------=4-Methylphenbl- I 10. IU I 1_, 621-64-7 ------- N-nitroso-d1-h-propylamine_I 10. 1U i 1 67-72-1 ------- Hexachloroethane V 10. IU I 1 98 -95 -3 -------Nitrobenzene I 10. IU I 1 78-59-1 ------- Isophorone I 10. IU I 1 88-75-5 ------- 2-tiitrophenol- I .10. 1U I I '105-67-9-------2,4-Dimethylphenol- i 10. IU I 1 65 -85 -0 -------Benzoic acid I 50. IU I 1 111-91=1 ------- bis(2-Chloroethoxy)methane_I 10. IU I I 120-83- ------2,4-Dichlorophenol I 10. IU I I 120-8Z-Vi------1,2.,4'-Trichlorobenzene- I 10. IU I I 91-20-*�-w ------ Naphthalene- I 10. 1U I I l06 -47;--&--i ------ I 10. IU I 1 87-68-3 ------- Hexachlorobutadiene I 10. IU I 1 59-50-7 ------- 4-Chloro-3-methylphenol I 10. IU I 1 91-57-6-------2-Methylnaphthalene _.I 10._ -IU I 1 77-47-4 ------- Hexachloroeyclopentadlene.._I. 10. IU I 1 88-06-2-------2,4,6-Trichlorophenol I 10. IU i 1 95-95-4 ------- 2,4,5 -Trichlorophenol_. I 50. IU I 1 91-58-7 ------- 2-Chloronaphthalene- I i0. IU I 1 88-74-4 ------- 2-Nitroaoiline I - 50. IU I 1 131-11-3 ------- Dimethylphthalate I 10. IU I I 208 -96 -8 -------Acenaphthylene 1 10. IU I 1 606-20-2 ------- 2,6-Dinitrotoluene I 10. IU I FORM I SV -1 1/87 Rev. 1C SEMIVOLATILB-ORGANICS ANALYSIS DATA SHEET Lab:Name: INTICIL, Contract: 68-D9-0048 Lab.Code: INTECK. Case No.: 15486 SAB No.: Matrix:, (soil/water) WATER Sample wt/vol :. 1000;. 0 (g/mL) per, Level: .(low/ped) LOW 1 Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: WN) N' pH: 6.9 EPA SAMPLE NO. 1 1 I BFF77 t I 1 SDG No.: BFC39 Lab Sample ID: Lab File ID: B3849 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed:' 12/14/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg)- UG/L Q I I 99-09-2-------3-Nitroaniline I I 50. I I IU I I 83 -32 -'9 ------Acenaphthene 1 10. IU I 1 51-28'-5 ------- 2,4'-Dinitrophenol 1 50. IU I I 100-02•-7---==--4-Nitrophenol 1 50.- IU I 1 132-64-9 ------- Dibenzofuran 1 10. IU I 1 121-14-2 ------- 2,4-Dinitrotoluene 1 10. IU I I' 84=66-2 ------- Diethylphthalate 1. 10. 1U I 17005-72-3-------4-Chlorophenyl-phenylether_1 10. IU I f 86-73'-7 ------- Fluoiene 1 10. IU I I 100-01-6 ---- =-=4-Nitzoaniline 1 50. tU I I' 534-52-1----=--4-,6-Dinitro-2-mthylphenol_1. 50. IU I 1 86=30-6=----=-N-Ifitrosodiphenylamina_(1)_1_. 10. 1U I -I 101-=55'-3 ------- 4-Bromophenyl-phenylether _I 10. IU I 1 118-74'=1 ------- Hexachlorobenzene 1 10. IU I 1 87=86-8=------Pentach-iorophenol' 1 50. IU I I 85-01-8--------Phenapthrene I 10. IU I I -X120-12-7== ----- Anthracene- t 10. IU I I 84-74-2-------Di-n-butylphthalate.. 1 10. IU I I 206-4+E`=-------Fluoranthene i 10. 1U I I 129-00;=---=-P3►rene 1 10. 1U I 1 85-6-=------Hatylbenzylphthalate 1 10. IU I 1 91- ---aVV-D1chlorobenzid1ne 1_ 20. 1U I I 56-500Q�------Benzo(a)anthracene- 1_._ 10. lU I I 218-01-,ffi-------ehrysene- 1_._ 10. IU I 1 117-81'-7 ------- bis(2-athylhexyl)phthalate_I_- .230. 1 I 1 117-84-0 ------- Dt-n-octy2phthalats-'. l -.-.. _.._ 10. 1U I 1 205-99-2' ------- Benzatb) fluoranthena_1 �.- _..,_ 10: 1U I I 207-09-9-------Benzo(k)fluoranthene I...__- 10. IU I 1 50 -32=8 -------Benzo (a) pyrene' I_._. 10 . I _..10. _ _1U 1 U I.. -... ­S3, -3-- ` (a, hanthracene..- 1U I I 19.1-24-2--=----Benzo(gih,i)perylene_ I__- 10. IU I t �I (1) - Cannot be separated from diphenylasinei-_. �__ ►-� _ _ FORK I SV -2 1/87 Rev-: SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET 'PMATIVELY IDRNTIF`IRD COMPOUNDS Lab Name: INTECW."- Contract: 68-D9-0040 Lab Code: INTECH= case No.: 15486- SAS No.: Matrix: ($oil/water) WATER Sample wt/vol: 1000.0 (g/mL) ML Level: (low/med) LOW _ % Moisture: not dec. 100. dec. 0. Extraction: (SepF/Cont/Sone) SEPF GPC Cleanup: (Y/NY N. pH: 6.9 - BPA SAMPLE NO. I I I BFF77 I I I SDG No.: BFC39 Lab Sample ID: Lab File -ID: B3849 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CONCENTRATION UNITS: Number TICS found: 2 (ug/L or ug/Kg) UG/L I I I I i' CAS NUMBER I COMPOUND NAME I RT i EST. CONC. I Q 1 Issasasasssasaassl�ssassssssasaasssaaaaassssaslssssassalsssssassaaasslssaaal I 1. - 1OVXXONV 1 8.56 I 10. 1 J I 1 2. - IUNKNOVN 1 18.67 1 10. I J 1 1 3. 1 4. I I I I I 1 5. 1 r r I I '6 • t 0 I I 1 I 7. I I I 1 I a. ( I I I I I 9. I I I I I 1 10. I I I I 111. I I I I I 1 12. 1 13. I I I 1 I 1 14. I I I 1 I 1 15. 1 I I I I 1 16. I I I I I 117. E I I I 118. 119. I I I I I 1 20. I 1 21. I I I 1 t 1 22. I I I t I 1 23. I I I I I 1 24. I I I I I k 25. I I I I I 1 26. I I I I I 127. I I I I I 128. I 1 29. I I I I 1 30. I I I 1 I I I t I I I FORM I SV -TIC f 25 7 1/87 Rev. k 1B EPA SAMPLE NO. SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET I I I EFF78 I Lab Name: INTECH Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: SDO No.: BFC39 Matrix: (soil/water) WATER Sample wt/vol: 1000.0 (g/mL) ML Level: (low/mad) LOW % Moisture: not dee. 100. dec. 0. Extraction: (SepF/Cont/Sonc).SEPF Lab Sample ID: Lab File ID: B3850 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 GPC Cleanup: (YIN) N pH: 7.2 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q I 108 -95 -2 -------Phenol I 10. 1U I i 111-44-4 ------- bis (2-Chloroethyl)ether I 10. IU- I I 95-57-8-------2-Chlorophenol I 10. IU I 1 541-73-1-------10-Dichlorobenzene t 10. IU I I 106®46-7--!--=--r-1,4-DichlorobenzeneI 10. IU I 1 .100 -51 -6 -------Benzyl alcohol I 10. IU I I 95-50-1 -------- 1,2-Dichloaobenzene I 10. IU I I 95-48-7-------2-Methylphenol 1 10. IU I I 108-60-1--r-.�-�bisf2�Chloroiaopropyl)ether 1 10. IU I I 106-44-5---"---4-Ne.thylpheno1 1 10. IU I I 621-64-7-------N®Nitroso-di-n-propylamine_I 10. IU I I 67-72-1-------Hexachloroothane I 10. IU I I 98-95-3-------N1trobenzene 1 10. IU I I 78-59-1--,r---Isophorobe 1 10. 1U I V 88-75-5-------2-Hitrophenol I 10. IU I 1 X105-67-9-,-,---114-Disethylphenol t 10. IU I I 65-85-0-------B6ns01c acid 1 50. IU I I 111-9;t-1c-------Hin(2-Chloroethoxy)methane_t 10. IU I I 120-t�------2,4-Dichlorophenol I 10. IU I I 120--=----T�,2,4=Trichlorobenzene 1 10. IU I I 91-1t. ----Naphthalene I 10. I U I I 106-47~-8 ------- 4-Chloroaniline I 10. IU I i 87-68-3 ------- Hexaehlorobutadiene I 10. IU I I 59-50-7 ------- 4-Chloro-3-methylphenol I 10. IU I I 91-57-6-------2-Methylnaphthalene I 10. tU I 77-47-4 ------- Hexachlorocyclopentadiens _I 10. IU I 1 88-06-2-------2,4,6-Trichlorophenol I 10. IU I 95-95-4-------2,4,5-Trichlorophenol t' 50. IU I I 91-58-7 ------- 2-Chloronaphthalene _I 10. IU I i 88-74-4-------2-Nitroaniline I 50. IU I 1 131-11-3 ------- Oimethylphthalate I 10. IU I I 208 -96 -8 -------Acenaphthylene I 10. IU I I 606-20-2 ------- 2,6-Dinitrotoluene 1 10. IU I 2 G 3 FORM I SV -1 1/87 Rev`?. SSMIVOLATILB ORGANICS 1CANALYSISDATA SHEET Lab Name: INTECH Lab Code: INTECH Case No.: 15486 Matrix: (Soil/water) WATER EPA-SAMPLR NO. .I I Contract: 68-D9-EFF78 0048 I- I I SAS No.: SDG No.: BFC3.9 Lab Sample ID: Sample wt/vol: 1000.0 (g/mL) ML Lab File ID: 83850 Level: (low/med) LOW _ Date-Receiveds 12/ 6/90 % Moisture: not dec. 100. dec. 0. Date Extracted: 12/ 6/90 Extraction: (SePP/Cont/Sonc-) SSPF Date Analyzed: 12/14/90 GPC Cleanup: (Y/N) N pH: 7.2 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) I UG/L Q 1 99-09-2 ------- 3-Nitroaniline I I 1 1 83-32-9----- --Acenaphthene 1 50. IU 1 51-28-5-------2 ,4-Dinitrophenol 1 10. IU I �� � 1 100-02-7 ------- 4-Nttrophenol 1 50. 1U 1 1 132-64-9 ------- Dibenzofuran I 50. IU I 1 121-14-2-------g ,4-Dinttrotoluene I 10 . 1U 1 1 84-66-2 ------- Diethylphthalate I' 10. 1U 1 1 7005-72-3 ------- 4-Chlorophenyl.-yphen lather 1 10. 1U I 1 86-73-7 ------- Fluorene -1 10. 1U 1 I 100-01-6--------91trzoaa:iliaa- I 10. 1U 534-52-1-------4 6-Di-n�itra.-2-motl:ylphenol- 1 50. 1 IU I 86-30-6 ------- N-Nitrosodiphenylanine.(11-1- 50.. . IU I 1 101-55-3 ------- 4-Brosophenyl-phenyl.ether 10. 1 -1 1 118-74-1-------Hexachlorebenzene 10. IU I 1 87 -86 -5 -------Pentachlorophenol I 10. IU 1 1 85 -01 -8 -------phenanthrene 1 50. 1U i 1 •120-12-7 ------- Anthracene_. 1 10• 1U 1 I 84-74-2 ------- Di-n-batylphthalate 1 10. IU I --'--1 1 206-44-0 ------- Fluaranthene 10. 1U 1 . t 129 -00 -@-------Pyrene I 10. IU I I 85 -68 --------Hat 1 Y-Dlchllphthalate_-20. 10. (U 1 I 91-94-i------- 1 3,3 Dichlorobenzidine 10. IU 1 Den 1 56-55-3 ------- zota)anthracene �1 ju t 1 218-01-9-------Chrysene 10. 1U I t 117-81-7------- I..----- b1s(2-Sthylhexyl)phthalate_,1- 10.. ..1U. I 117-84-0 ------- Di-n-octylphthalate 53.- 1 I I 205-99-2 ------- Benzo(b)fluoranthene---1 10 :IU _ 1 1 207-08-9 ------- Benzo(k)fluoranthene 1 -_10 ..- , lit i I.._.. 1 50-32-8-------Benzo(a) pyrene 10. 1U 1 1 193-39-5------- 1,. Indeno(1,2,3-cd)pyrenei _- _-- 10._ I U... I - __ 1 53-70-3 ------- Dibenz(a,h)anthracene _ IU. I` t 191-24-2-------Benzo(g,h,i)perylene --1 10. IU r I __ I- 10. - 1U 1 (1D - Cannot be separated from diphenylanine I 1-1 FORM I SV -2 0 264 1/87 Rev. 1F IEMIVOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDRNTIFIED COMPOUNDS ab Pia me : I NTR'CH, Lab Code: INTECH Contract: 68-D9-0048 Case No.: 15486-- SAS No.: trix: (soil/water) WATER Sample wt/vol: 1000.0 (g/mL) ML :vel: (low/med) LOW Moisture: not dec. 100. dec. 0. xtraction: (SepF/Cont/Sonc) SEPF IC Cleanup: (Y/N) N pH: 7.2 EPR SAMPLE NO. I I I BFF78 I I SDG No.: BFC39 Lab Sample ID: Lab File ID: B3850 Date Received: 12/ 6/90 Date Extracted: 12/ 6/90 Date Analyzed: 12/14/90 Dilution Factor: 1.00 CONCENTRATION UNITS: lumber TICS found: 0 (ug/L or ug/Kg) UG/L I I I I I CAS NUMBER I COMPOUND NAME I RT I EST. CONC. I C I ssassssssssss:slsss:asassaassas:asssffisassssslsssasssslssssss:=::aaslsssssl i• I I 1 1 I 2. I I I I I 3. I I I I I 4. 5• I I I I 6. I I I I f 7. I I I I I 9. I f I I I 10. ii. I I I I I 12. f I I I I 13. I I f I I 14• 15• I 1 I t i 16.17. I t I I I is. I I I I 19. r I t I I 20. I I I I I 21. 22. I f I I I 23. I I I I I 24. I f 1 I I 25. 1 r r I I 26. 27. I I I 1 I 28. 29. I I I I I 30. I I I I I I I I I I FORM I SV -TIC 2�jrJ 1/87 Rev. 114 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I I I BFC39 I Contract: 68-D9-0048 I I Lab Name: INTECH Lab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 t Matrix: (soil/water) WATER Lab Sample YD: Sample wt/vol: 1000. (g/mL)ML Lab File ID: GP4417 Level: (low/med) LOW Date Received: 12/ 6/90 % Moisture: not dec.100. - dec. 0. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/ 9/90 GPC Cleanup: (Y/N) N pH: 6.3 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q I 1 319-84-6-----alpha-BHC II I .050 I I IU i IU I 1 319-85-7-----beta-BHC .050 i IU I ' 1 319-86-8-----delta-BHC ,050 IU I 1 58-89-9-----gamma-BHC (Lindane) ,050 050 IU I 1 76 -44 -8 -----Heptachlor , I .050 IU I 1 309 -00 -2 -----Aldrin IU I I 1024 -57 -3 -----Heptachlor epoxide .050 IU I 1 959-98-8 ----- Endosulfan I ,050 I IU I 1 60 -57 -1 -----Dieldrin .10 .10 lU I I 72-55-9-----4,4'-DDE .10 IU I 1 72 -20 -8 -----Endrin I IU I i 33213-65-9 ----- Endosulfan II .10 1 IU I 1 72-54-8-----4,4'-DDD .10 IU I 1031-07-8 ----- Endosulfan sulfate I .10 IU I 1 50-29-3-----4,4'-DDT .10 IU I 72 -43 -5 -----Methoxychlor .50 I IU I 1 53494 -70 -5 -----Endrin ketone .10 IU I 1 5103-71-9-----alpha-Chlordane I .50 IU I 1 5103-74-2 ----- gama-Chlordane ,50 1.0 IU I 1 8001-35-2 ----- ToxapheneI IU i I 12674"-11-2 ----- Aroclor-1016 .50 I IU I I' 11104,T28-2-----Aroclor-1221 .50 IU I I 11141-11-5-----Aroclor-1232 I .50 1 1U I 1 53469-21-9 ----- Aroclor-1242 .50 I IU I 1 12672-29-6 ----- Aroclor-1248. .50 1.0 IU I I 11097-69-1-----Aroclor-1254 I 1 1.0 IU I 1 11096-82-5 ----- Aroclor-1260 I I I _I 3�5 1/87 Rev FORM I PEST 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I I I BFC54 1 Lab Name: INTECH Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER Sample wt/vol: 1000. (g/mL)ML Level: (low/med) LOW % Moisture: not dec.100. - dec. 0. Extraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (Y/N) N pH: 6.3 Lab Sample ID: Lab File ID: GP4421 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L Q I I 1 319-84-6-----alpha-BHC 1 .050 IU 1 319-85-7-----beta-BHC I .050 IU 1 319-86-8-----delta-BHC I .050 IU 1 58-89-9-----gamma-BHC (Lindane) I .050 IU 1 76 -44 -8 -----Heptachlor I .050 IU 1 309 -00 -2 -----Aldrin I .050 IU 1024 -57 -3 -----Heptachlor epoxide i .050 IU 1 959-98-8 ----- Endosulfan I I .050 IU 60 -57 -1 -----Dieldrin. I .10 IU 72-55-9-----4,4'-DDE I .10 IU 72 -20 -8 -----Endrin i .10 IU l 33213-65-9 ----- Endoaulfan II I .10 lu 1 72-54-8-----4,4'-DDD I .10 IU 1 1031-07-8 ----- Endoaulfan sulfate I .10 lu 1 50-29-3-----4,4'-DDT I .10 1U 1 72 -43 -5 -----Methoxychlor I .50 (U 1 53494 -70 -5 -----Endrin ketone I .10 lu I 5103-71-9-----alpha-Chlordane I .50 IU I 5103-74-2-----gamma-Chlordane I .50 IU 1 8001 -35 -2 -----Toxaphene ( 1.0 IU:. 1 12674-11-2 ----- Aroclor-1016 I .50 IU 1 11104-28-2 ----- Aroclor-1221 I .50 IU I 11141-16-5 ----- Aroclor-1232 I .50 IU I 53.469-21-9 ----- Aroclor-1242 1 .50 IU i 12672-29-6 ----- Aroclor-1248 1 .50 IU 1 11097-69-1 ----- Aroclor-1254 ( 1.0 IU 1 11096-82-5 ----- Aroclor-1260 I 1 1.0 IU 1 11 FORM I PEST 34 1/87 Rev. OF" M 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECK lab Code: INTECM Case No.: 15486 Matrix: (soil/water) WATER ample wt/vol: 1000. (g/mL)ML .-eve1: (low/med) LOW Moisture: not dec.100. - dec. xtraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND I I I BFC55 1 Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4422 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 5 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC I I .050 I I IU 1 319-85-7-----beta-BHC I .050 IU 1 319-86-8-----delta-BHC I .050 IU 1 58-89-9-----gamma-BHC (Lindane) I .050 IU I 76 -44 -8 -----Heptachlor I .050 IU 1 309 -00 -2 -----Aldrin I .050 IU 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU 1 959-98-8 ----- Endosulfan I I .050 IU 1 60 -57 -1 -----Dieldrin I .10 IU 1 72-55-9-----4,4'-DDE I .10 IU 1 72 -20 -8 -----Endrin I .10 IU 1 33213-65-9 ----- Endosulfan II I .10 IU 1 72-54-8-----4,4'-DDD ( .10 IU 1 1031-07-8 ----- Endosulfan sulfate I .10 IU I 50-29-3-----4,4'-DDT I .10 IU 1 72 -43 -5 -----Methoxychlor ( .50 IU 1 53494 -70 -5 -----Endrin ketone I .10 IU I 5103-71-9-----alpha-Chlordane ( .50 IU 1 5103-74-2-----gamma-Chlordane I .50 IU I 8001 -35 -2 -----Toxaphene 1.0 IU I 12674 -IX -2 ----- Aroclor-1016 I .50 IU I 11104-2t-2 ----- Aroclor-1221 I .50 IU 1 11141 -IS -5 ----- Aroclor-1232 I .50 IU I 53469-21-9 ----- Aroclor-1242 ( .50 IU I 12672-29-6 ----- Aroclor-1248 I .50 IU 1 11097-69-1 ----- Aroclor-1254 I 1®0 IU 1 11096-62-5 ----- Aroclor-1260 I 1.0 I IU I 11 346 FORM I PEST 1/87 Rev. 1D PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 1000. (g/mL)ML Level: (low/med) LOW % Moisture: not dec.100. - dec. Extraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (YM N pH: CAS NO. COMPOUND EPA SAMPLE NO. I I I BFC98 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4423 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 4 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC I I .050 I I IU 1 319-85-7-----beta-BHC I .050 IU 1 319-86-8-----delta-BHC I .050 IU 1 58-89-9-----gamma-BHC (Lindane) I .050 IU 1 76 -44 -8 -----Heptachlor I .050 IU 1 309 -00 -2 -----Aldrin I .050 IU 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU 1 959-98-8 ----- Endosulfan I 1 .050 IU 1 60 -57 -1 -----Dieldrin ( .10 IU 1 72-55-9-----4,4'-DDE I .10 IU 1 72 -20 -8 -----Endrin I .10 IU 1 33213-65-9 ----- Endosulfan II I .10 IU 1 72-54-8-----4,4'-DDD I .10 IU 1 1031-07-8 ----- Endosulfan sulfate I .10 IU 1 50-29-3-----4,4'-DDT I .10 IU 1 72 -43 -5 -----Methoxychlor I .50 IU I 53494 -70 -5 -----Endrin ketone I .10 IU 1 5103-71-9-----alpha-Chlordane I .50 IU I ' 5103-74-2-----gamma-Chlordane I .50 IU 1 8001 -35 -2 -----Toxaphene I 1.0 IU 1 12674-11-2 ----- Aroclor-1016 I .50 IU 1 11104-26-2 ----- Aroclor-1221 I .50 IU 1 11141-16-5 ----- Aroclor-1232 I .50 IU 1 53469-21-9 ----- Aroclor-1242 I .50 IU 1 12672-29-6 ----- Aroclor-1248 ( .50 IU 1 11097-69-1 ----- Aroclor-1254 I 1.0 IU 1 11096-82-5 ----- Aroclor-1260 I 1.0 IU I 1 350 FORM I PEST 1/87 Rev. 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I I I BFC99 I Lab Name: INTECH Contract: 68-D9-0048 I I f ib Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER Lab Sample ID: _ample wt/vol: 1000. (g/mL)ML Lab File ID: GP4425 Bvel• (low/med) LOW Date Received: 12/ 6/90 Moisture: not dec.100. - dec. 0. Date Extracted: 12/ 7/90 xtraction: (SepF/Cont/Sone) SEPF Date Analyzed: 12/ 9/90 GPC Cleanup: (Y/N) N pH: 7.5 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L 4 I 1 319-84-6-----alpha-BHC I I .050 I I 1U I 1 319-85-7-----beta-BHC I .050 IU I 1 319-86-8-----delta-BHC I .050 IU I I 58-89-9-----gamma-BHC (Lindane) I .050 IU I I 76 -44 -8 -----Heptachlor I .050 IU I 1 309 -00 -2 -----Aldrin I .050 IU i 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU I 1 959-98-8 ----- Endosulfan I I .050 IU I 1 60 -57 -1 -----Dieldrin I .10 IU I I 72-55-9-----4,4'-DDE I .10 IU I 1 72 -20 -8 -----Endrin I .10 IU I 1 33213-65-9 ----- Endoaulfan II I .10 IU I 9 i 72-54-8-----4,4'-DDD I .10 IU I I 1031-07-8 ----- Endoaulfan sulfate I .10 IU I I 50-29-3-----4,4'-DDT I .10 1U I 1 72 -43 -5 -----Methoxychlor I .50 IU I 53494 -70 -5 -----Endrin ketone I .10 IU I 1 5103-71-9-----alpha-Chlordane I .50 IU I I 5103-74-2 ----- gamma -Chlordane_ I .50 IU I 1 8001 -35 -2 -----Toxaphene I 1.0 IU I 1 12674-11-2 ----- Aroclor-1016 I .50 IU I ; 1 11104-2E-2 ----- Aroclor-1221 I .50 IU I I 11141-16-5 ----- Aroclor-1232 i .50 IU I 1 53469-21-9 ----- Aroclor-1242 I .50 IU I 1 12672-29-6 ----- Aroclor-1248 I .50 IU I 1 11097-69-1 ----- Aroclor-1254 I 1.0 IU 1 I 11096-82-5-----Aroclor-1260 I 1.0 IU I 3511 FORM I PEST 1/87 Rev. { 1D PESTICIDE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. I � I BFC40 I Lab Name: INTECH Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 1000. (g/mL)ML Level: (low/med) LOW % Moisture.: not dec.100. - dec. 0. Extraction: (SepF/Cont/Sone) SEPF GPC Cleanup: (Y/N) N pH: 6.5 CAS NO. COMPOUND Lab File ID: GP4414 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 8/90 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC 319-85-7-----beta-BHC 319-86-8-----delta-BHC 58-89-9-----gamma-BHC (Lindane) 76 -44 -8 -----Heptachlor 309-00-2 ----- Aldrin* 1024 -57 -3 -----Heptachlor epoxide 959-98-8 ----- Endosulfan I 60 -57 -1 -----Dieldrin 72-55-9-----4,4'-DDE 72-20-8 ----- Endain 33213-65-9 ----- Endosulfan II 72-54-8-----4.,4'-DDD 1031-07-8 ----- Endosulfan sulfate 50-29-3-----4,4'-DDT 72 -43 -5 -----Methoxychlor 53494 -70 -5 -----Endrin ketone 5103-71-9-----alpha-Chlordane 5103-74-2-----gamma-Chlordane 8001 -35 -2 -----Toxaphene 12674-11-2 ----- Arcclor-1016 11104=2* -2 ----- Aroclor-1221 11141-1.6-5 ----- Aroclor-1232 53469-21-9 ----- Aroclor-1242 12672-29-6 ----- Aroclor-1248 11097-69-1 ----- Aroclor-1254 11096-82-5 ----- Aroclor-1260 FORM I PEST I 1.0 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .10 IU I I .10 IU I I .10 IU I I .10 IU 1 I .10 IU I I. .10 IU I I .10 IU I I .50 IU I I .10 IU I I .50 IU I I .50 IU i I 1.0 IU I I .50 IU I i .50 IU I I .50 IU I I .50 IU I I .50 IU I I 1.0 IU I I 1.0 IU I 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH ab Code: INTECH Case No.: 15486 matrix: (soil/water) WATER _ample wt/vol: 1000. (g/mL)ML evel: (low/med) LOW % Moisture: not dec.100. ' dec. xtraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND I I I BFC41 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4419 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 8 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC 1 1 .050 1 1 IU 1 319-85-7-----beta-BHC 1 .050 IU 1 319-86-8-----delta-BHC 1 .050 IU I 58-89-9-----gamma-BHC (Lindane) I .050 IU 1 76 -44 -8 -----Heptachlor I .050 IU 1 309 -00 -2 -----Aldrin 1 .050 IU 1 1024 -57 -3 -----Heptachlor epoxide i .050 IU 1 959-98-8 ----- Endosulfan I ( .050 IU 1 60 -57 -1 -----Dieldrin I .10 IU 1 72-55-9-----4,4'-DDS i .10 IU 1 72 -20 -8 -----Endrin 1 .10 IU 1 33213-65-9 ----- Endosulfan II 1 .10 IU 1 72-54-8-----4,4'-DDD 1 .10 IU 1 1031-07-8 ----- Endosulfan sulfate 1 .10 IU 1 50-29-3-----4,4'-DDT 1 .10 IU 1 72 -43 -5 -----Methoxychlor 1 .50 IU 1 53494 -70 -5 -----Endrin ketone 1 .10 IU I 5103-71-9-----alpha-Chlordane I ..50 IU 1 5103-74-2 ----- gao -Chlordane 1 .50 IU 1 8001 -35 -2 -----Toxaphene 1 1.0 IU 1 12674-11-2 ----- Aroclor-1016 I .50 IU 1 11104-2Q6-2= ---- Aroclor-1221 I .50 IU 1 11141-16-5 ----- Aroclor-1232 I .50 IU 1 53469-21-9 ----- Aroclor-1242 ( .50 IU 1 12672-29-6 ----- Aroclor-1248 I .50 IU 1 11097-69-1 ----- Aroclor-1254 I 1.0 IU 1 11096-82-5 ----- Aroclor-1260 I 1.0 I IU I I I 333 FORM I PEST 1/87 Rev. PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH b Code: INTECH Case No.: 15486 {atrix: (soil/water) WATER 3 aple wt/vol: 1000. (g/mL)ML gel : ( low/med ) LOW Aoisture: not dec.100. - dec. 0. °:i Taction: (SepF/Cont/Sonc) SEpF 'PC Cleanup: EPA SAMPLE NO. I I Contract: 68-D9-0048 I BFC53 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4420 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or ug/Kg) I UG/L Q I 319-84-6-----alpha-BHC I I I 319-85-7-----beta-BHC I .050 IU I I 319-86-8-----delta-BHC I •050 IU I I 58-89-9-----gam-BHC (Lindane). 050 IU I 76 -44 -8 -----Heptachlor I .050 IU I I 309 -00 -2 -----Aldrin I .050 IU I I 1024 -57 -3 -----Heptachlor epoxide. 050 IU I I 959-98-8 ----- Endosulfan I 1 .050 IU I I 60 -57 -1 -----Dieldrin 1 .050 IU I I 72-55-9-----4,41-DDE I .10 1U i 72 -20 -8 -----Endrin I .10 IU I 1 33213-65-9 ----- Endosulfan II 1 .10 IU I 1 72-54-8-----4,4'-DDD I .10 IU I 1 1031-07-8 ----- Endosulfan sulfate. 10 1U I 1 50-29-3-----4,4'-DDT I .10 IU I 1 72 -43 -5 -----Methoxychlor ( .10 IU I I 53494-70-5=----Bndrin ketone I .50 lu I 1 5103-71-9 ----- alpha-ChlordaneI .10 1U I I 5103-74-2-----gam-Chlordane I .50 IU I I 8001 -35 -2 -----Toxaphene i .50 IU I 1 12674-11-2 ----- Aroclor-1016 I 1.0 1U I I 11104-28-2-----Aroclor-1221 1 .50 (U I I 11141-16-5-----Aroclor-1232 I .50 IU I 1 53469-21-9 ----- Aroclor-1242 I .50 IU I 1 12672-29-6 ----- Aroclor-1248 I ..50 IU I 1 11097-69-1 ----- Aroclor-1254 I .50 IU i 1 11096-82-5 ----- Aroclor-1260 i 1.0 IU I 1 i 1.0 1U, I I_I FORM I PEST 333 1/87 Rev. A* 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I i I BFF66 ,ab Name: INTECN Contract: 68-D9-0048 I I .a Code: INTECH Case No.: 15486 SAS No.: atrix: (soil/water) SOIL a ple wt/vol: 30. (g/mL) G el: (low/med) LOW moisture: not dec. 5. = dec. 5. x ;action: (SepF/Cont/Sone) SONC PC Cleanup: (YIN) N pH: 6.5 SDG No.: BFF66 Lab Sample ID: Lab File ID: GP8821 Date Received: 12/ 6/90 Date Extracted: 12/12/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG a I 1 1 319-84-6-----alpha-BHC I 8.4 I I IU 1 319-85-7-----beta-BHC I 8.4 IU I 1 319-86-8-----delta-BHC I 8.4 IU I I 58-89-9-----gamma-BHC (Lindane) I 8.4 IU I- _76-44-8-----Heptachlor 76-44-8 ----- HeptachlorI 8.4 IU I 1 309 -00 -2 -----Aldrin I 8.4 IU 1 1024 -57 -3 -----Heptachlor epoxide 1 8.4 IU I 1 959-98-8 ----- Endosulfan I I 8.4 IU 1 60 -57 -1 -----Dieldrin I 17. IU I 1 72-55-9-----4,4'-DDR 1 93. ice' I 1 72 -20 -8 -----Endrin I 7.8 I J I 1 33213-65-9 ----- Endosulfan II I 17. IU I I 72-54-8-----4,4'-DDD I 17. fU 1 1031-07-6 ----- Endosulfan sulfate 1 17. IU 1 50-29-3-----4,49-DDT i 410. -17:1- 1 1 72 -43 -5 -----Methoxychlor I 84. IU I 53494 -70 -5 -----Endrin ketone 1 17. IU 1 5103-71-9-----alpha-Chlordane I 84. IU I 1 5103-74-2 ----- ga -Chlordane I 4.6 1 J 1 8001 -35 -2 -----Toxaphene I 170. IU 12674-iI-2-----Ar0clor-1016 I 84. IU 1 11104-26-2r----Asoclor-1221 I 84. IU I 1 11141-16-;=---Araclor-1232 I 84. IU I. 53469-21-l------Aroclor-1242 I 84. IU 1 12672-29-6 ----- Aroclor-1248 I 84. IU I 11097-69-1-----Aroclor-1254 I 170. IU I 1 11096-82-5 ----- Aroclor-1260 "I 170. IU I FORM I PEST' 440 1/87 Rev. ID EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I i Lab Name: INTECH. Contract: 68-D9-0048 I BFF67 I I ab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: ample wt/vol: 30. (g/mL) G Lab File ID: GP8822 evel: (low/med) LOW Date Received: 12/ 6/90 Moisture: not dec. 5. ' dec. 5. Date Extracted: 12/12/90 xtraction: (SepF/Cont/Sonc) SONC Date Analyzed: 1.2/15/90 GPC Cleanup: (YIN) N pH: 6.4 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or uq/Kq) UG/KG p I I 1 319-84-6-----alpha-BHC 1 8.4 I I IU I 1 319-85-7-----beta-BHC I 8.4 IU I 1 319-86-8-----delta-BHC 1 8.4 IU I 1 58-89-9-----gamma-BHC (Lindane) I 8.4 IU I 1 76 -44 -8 -----Heptachlor I 8.4 IU I 1 309 -00 -2 -----Aldrin I 8.4 IU I 1 1024 -57 -3 -----Heptachlor epoxide I 8.4 IU I 959-98-8 ----- Endosulfan I ( .8.4 IU I 60 -57 -1 -----Dieldrin I 17. IU I 1 72-55-9-----4,4'-DDS 120. 1 1 1 72 -20 -8 -----endrin I 17. IU I 1 33213-65-9 ----- Endosulfan II I 17. IU 1 72-54-8-----4,4'-DDD ( 17. IU I 1 1031-07-8 ----- Endosulfan sulfate I 57. 50-29-3-----4,4'-DDT I 450. I I 72 -43 -5 -----Methoxychlor 1 84. IU 1 53494 -70 -5 -----Endrin ketone I 17. IU I 5103-71-9-----alpha-Chlordane I 84. IU I 5103-74-2-----gases-Chlordane I 7.0 1 J 8001 -35 -2 -----Toxaphene I 170. IU 12674-11-2-----Areclor-1016 I 84. IU 11104-29-2-----Aroclor-1221 1 84. IU 1 11141-1i-5 ----- Aroclor-1232 1 84. IU I 53469-21-gr-----Aroclor-1242 I 84. IU 1 12672-29-6 ----- Aroclor-1248 I 84. IU 1 11097-69-1 ----- Aroclor-1254 1 170. IU 1 11096-82-5 ----- Aroclor-1260 I 170. IU- I r I FORM I PEST" 1/87 Rev. ID PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH EPA SAMPLE NO. I I I BFF68 I Contract: 68-D9-0048 I I ib Code: INTECH Case No.: 15486 SAS No.: Pda�trix: (soil/water) SOIL -.lmple wt/vol: 30. (g/mL) G 1 vel: (lov/med) LOW % Moisture: not dec. 2. - dec. 2. ;traction: (SepF/Cont/Sonc) SONO GPC Cleanup: (YIN) N pH: 7.1 CAS NO. COMPOUND SDG No.: BFF66 Lab Sample ID: Lab File ID: GP0825 Date Received: 12/ 6/90 Date Extracted: 12/12/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or uq/Kq) UG/KG a 319-84-6-----alpha-BHC 3.19-85-7-----beta-BHC 319-86-8-----delta-BHC 58-89-9-----gamma-BHC (Lindane) 76 -44 -8 -----Heptachlor 309 -00 -2 -----Aldrin 1024 -57 -3 -----Heptachlor epoxide 959-98-8 ----- Endosulfan I 60 -57 -1 -----Dieldrin 72-55-9-----4,4'-DDS 72 -20 -8 -----Endrin 33213-65-9 ----- Endosulfan Ii 72-54-8-----404'-DDD 1031-07-8-----Endosulfan sulfate 50-29-3-----404t-DDT 72 -43 -5 -----Methoxychlor. 53494-70-5 ----- Nndrin ketone 5103-71-9-----alpha-Chlordane 5103-74-2-----jaws-Chlordane 8001 -35 -2 -----Toxaphene 12674-11-2 ----- Aroclor-1016 11104-26--2-----Aroclor-1221 11141-H-5-----Asoclor-1232 53469-21-9 ----- Aroclor-1242 12672-29-6 ----- Aroclor-1248 11097-69-1 ----- Aroclor-1254 11096-82-5 ----- Aroclor-1260 FORM I PEST 8.2 8.2 8.2 8.2 8.2 8.2 8.2 .8.2 16. 11. 16. 16. 16. 9.5 71. 82. 16. 82. 1.4 160. 82. 82. 82. 82. 82. 160. 160. 45? 1/87 Rev. 1D PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTNCH ab Code: INTECH Case No.: 15486 Matrix: (soil/water) SOIL ample wt/vol: 30. evel: (low/med) LOW (q/mL) G s Moisture: not dec. 15. ~ dec. 15. xtraction: (SepF/Cont/Sonc) SONC EPA SAMPLZ NO. I I I BFF69 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFF66 GPC Cleanup: (YIN) N pH: 6.3 Lab Sample ID: Lab File ID: GP8826 bate Received: 12/ 6/90 Date Extracted: 12/12/90 Date Analyzed: 1.2/15/90 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG II 1 319-84-6-----alpha-BHC ( 9.4 I I IU I 1 319-85-7-----beta-BHC ( 9.4 IU I 1 319-86-8-----delta-BHC I 9.4 IU I 1 58-89-9-----gamma-BHC (Lindane) I 9.4 IU I 1 76 -44 -8 -----Heptachlor I 9.4 IU I I 309 -00 -2 -----Aldrin I 9.4 IU i 1 1024 -57 -3 -----Heptachlor epoxide I 9.4 IU 1 959-98-8 ----- Sndosulfan I I .9.4 IU 1 60 -57 -1 -----Dieldrin. I 19. lU I 1 72-55-9-----4;4'-DDE I 9.9 1 J I 1 72 -20 -8 -----Endrin I 19. IU I 1 33213-65-9-----Sndosulfan II. ( 19. IU I 72-54-8-----4,,4_@-DDD ( 19. I U 1 1031-07-8 ----- Sndosulfan sulfate I 19. IU I 50-29-3-----t)4'-DDT I 19. IU I 1 72 -43 -5 -----Methoxychlor 1 94. IU I 53494 -70 -5 -----Endrin ketone I 19. lu I 1 5103-71-9-----alpha-Chlordane I 94. IU 1 5103-74-2-----gam-Chlordane I .69 1 J I 8001 -35 -2 -----Toxaphene I 190. IU I I 12674-13.-2 ----- Aroclor-1016 I 94. IU I 1 11104-28-2 ----- Aroclor-1221 I 94. 1U I 1 11141-16-5 ----- Aroclor-1232 I 94. IU I 1 53469-21-9 ----- Aroclor-1242 I 94. IU I 1 12672-29-6 ----- Aroclor-1248 I 94. 1U 1 11097-69-1 ----- Aroclor-1254 I 190. IU I 1 11096-82-5 ----- Aroclor-1260 i 190. IU I I 158 FORM I PEST 1/67 Rev. 1D SPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I I I BFF70 I Lab Name: INT3CH Contract: 68-D9-0048 I I Lab Code: INTECH Case No.: 15486 SAS No.: SDG No®: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: Sample wt/vol: 30. (g/mL) G Lab File ID: GP8827 7,.evel: (low/med) LOW Date Received: 12/ 6/90 A Moisture: not dec. 5. = dec. 5. Date Extracted: 12/12/90 xtraction: (SepF/Cont/Sonc) SONC Date Analyzed:.12/15/90 GPC Cleanup: (Y/N) N pH: 6.9 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG Q 319-84-6-----alpha-BHC 319-85-7-----beta-BHC 319-86-8-----delta-BHC 58-89-9-----gamma-BHC (Lindane) 76 -44 -8 -----Heptachlor 309 -00 -2 -----Aldrin 1024 -57 -3 -----Heptachlor epoxide 959-98-8 ----- Endosulfan I 60 -57 -1 -----Dieldrin 72-55-9-----4, 4' -DDR 72 -20 -8 -----Endrin. 33213-65-9 ----- Rndoseu-lfan II 72-54-8-----4,4'-DD' 1031-07-8 ----- Nndosulfan sulfate 50-29-3-----4,4'-DDT 72 -43 -5 -----Methoxychlor 53494-70-5 ----- Bndrin ketone 5103-71-9-----alpha-Chlordane 5103 -74 -2 -----gas -Chlordane 8001 -35 -2 -----Toxaphene 12674-11-2 ----- Aroclor-1016 11104-28-2 ----- Aroclor-1221 11141-16-5 ----- Aroclor-1232 53469-2I-9----,Aroclor-1242 12672-29-6-----Aroclor-1248 11097-69-1 ----- Aroclor-1254 11096-82-5 ----- Aroclor-1260 FORM I PBST I I 8.4 I I IU I 8.4 IU I I 8.4 IU I i .20 1 J I I 8.4 IU I I 8.4 IU I I 8.4 IU I I .8.4 IU I I 17. IU I 17. IU I I 17. IU I I 7.1 1 J 1 I 17. IU I I 17. IU I I 76. ? I i 84. IU I I 17. 1u I I 84. IU I I 84. IU I I 170. IU I I 84. IU I I 84. IU I I 84. IU I I 84. IU I I 84. IU I I 170. IU I 1 170. IU I I I 464 1/87 Rev. 1D EPA SAMPLZ NO. PHSTICIDR ORGANICS ANALYSIS DATA SHE$T Lab Name: INTBCH.-•- .- sb Code: INTSCH Case No.: 15486 matrix: (soil/water) SOIL Imple wt/vol: 30. (g/mL) G :vel: (low/med) LOW I I I BFF72 I Contract: 68-D9-0048 I. f SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: GP0031 Date Received: 12/ 6/90 Moisture: not dec. 2. - dec. 2. Date Extracted: 12/12/90 traction: (SepF/Cont/Sonc) SONO Date Analyzed: 12/15/90 GPC Cleanup: (Y/N) N pH: 6.6 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/KG 0 I 1 319-84-6-----alpha-BHC I 1 8.1 I I IU I 1 319-85-7-----beta-BHC I 8.1 IU I 1 319-86-8-----delta-BHC t 8.1 IU I I 58-89-9 ----- ga=a-BHC (Lindane) I 8.1 IU I I 76 -44 -8 -----Heptachlor I 8.1 IU I i 309 -00 -2 -----Aldrin I 11. 1 1 1 1024-57-3 ----- Heptachlor.epoxide i 8.1 IU I I 959-98-8-----Endosulfan 1 I .8.1 IU I 1 60 -57 -1 -----Dieldrin I 16. IU I 1 72-55-9 ----- 4,4'-DDZ I 26. 1 I 1 72-20-8 ----- Hndrin I 16. IU i 1 33213-65-9 ----- gndosulfan II I 16. IU t 1 72-54-8-----4,4•-DDD. I 16. IU I 1 1031-07-8 ----- Endosulfan sulfate I 16. IU I 1 50-29-3-----4,4'-DDT I 16. IU I 1 72 -43 -5 -----Methoxychlor I 81. IU I 1 53494-70-5 ----- gndsin ketone I 16. IU 1 5103-71-9-----alpha-Chlordane 1 81. IU I 1 5103-74-2-----gassy-Chlordane I 13. 1 J 1 1 8001 -35 -2 -----Toxaphene t 160. IU I 1 12674-11-2 ----- Aroclor-1016 I 81. IU I 1 11104-26-2 ----- Aroclor-1221 I 81. IU I I 11141-16-5-----Aroclor-1232 t 81. IU I 1 53469-21-9 ----- Aroclor-1242 I 81. IU I 1 12672-29-6 ----- Aroclor-1248 I 81. IU I 1 11097-69-1 ----- Aroclor-1254 I 160. IU I I 11096-82-5-----Aroclor-1260 I I 160. I IU I I I 417G FORM I PEST 1/87 Rev. 1D PES?ICIDS ORGANICS ANALYSIS DATA SHEET EPA SAMPLE N0. I Lab Name: IN?BCH Contract: 68 -Dg -0048 BFF73 I I Lab Code: INTZCCN Case No.: 15486 SAS No.: SDG No.: BFF66 Matrix: (soil/water) SOIL Lab Sample ID: sample wt/vol: 30. (g/mL) G Level: (low/med) LOW k Moisture: not dec. 9. dec. 9. Extraction: (SepF/Cont/Sonc) SONO ;PC Cleanup: (YIN) N pH: 6.7 Lab File ID: GP8816 Date Received: 12/ 6/90 Date Extracted: 12/12/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CAS NO.CONCENTRATION UNITS: COMPOUND (ug/L or uq/Kq) I UG/KG 0 I 319-84-6-----alpha-BHC I I I I 319-85-7-----beta-BHC ( 8.8 IU I I 319-86-8-----delta-BHC I 8.8 IU I I 58-89-9-----gam-BHC (Lindane) I 8.8 IU I I 76 -44 -8 -----Heptachlor I 8.8 IU I I 309 -00 -2 -----Aldrin I 8.8 IU I I 1024 -57 -3 -----Heptachlor epoxide I 8.8 IU I 959-98-8 ----- Sndosulfan I i 8.8 IU I 60 -57 -1 -----Dieldrin 1 8.8 IU I 72-55-9-----4,4'-DDS I 1U I I 72 -20 -8 -----Endrin 1 18. IU I 1 33213-65-9 ----- Endosulfan I1 I 18. IU I I 72-54-8-----4,4'-DDD I 18. 1U I 1 1031-07-4 ----- Endosulfan sulfate I 18. IU I 50-29-3-----4,4®-DDT I 18. IU I 72 -43 -5 -----Methoxychlor I 18. IU 1 53494 -70 -5 -----Endrin ketone I 88. IU I 1 5103-71-9 ----- alpha-ChlordaneI 18. IU 1 5103-74-2 ----- qaW-Chlordane I 88. 1U I 1 8001 -35 -2 -----Toxaphene 1 Be. 1U I 1 12674-11-2 ----- Aroclor-1016 I 180. IU I I 11104-26-2-----Aroclor-1221I 88. IU I I 11141-1�s-----Aroclor-1232 I 88. IU I I 53469-21-5-----Aroclor-1242 I 88' 1U I 1 12672-28-6 ----- Aroclor-1248 I 88. IU I 1 11097-69-1 ----- Aroclor-1254 I 1U I 1 11096-82-5 ----- Aroclor-1260 I 180. 1U I I i .180. 1U I I=1 '483 - FORM I PSS? 1/87 Rev. PBSTICIDR ORGANICS ANALYSIS DATA SH83T Lab Name: INTZCH Lab Code: INTRCH Case No.: 15486 Matrix: (soil/wEter) SOIL Sample wt/vol: 30. (g/mL) G Level: ( lora/med ) LOV % Moisture: not dec. 10. z dec. 10. Extraction: (SaPP/Cont/Sons) SONC GPC Cleanup: NPA SAMPLN N0. I I Contract: 68-D9-0048 I BFF74 I I SAS No.: SDG No.: BFF66 Lab Sample ID: Lab File ID: OP8832 Date Received: 12/ 6/90 Date Extracted: 12/12/90 Date Analyzed:,12/15/90 Dilution Factor: 1.00 CAS N0.CONCUTRATION UNITS: COMPOUND (ug/L or ug/xg) I UG/xG � I 319-84-6-----alpha-BHC I I I I 319-85-7-----beta-BHC I 8.9 1U I .319-86-8-----delta-BHC I 8.9 1U I I 58-89-9 ----- gaeUa-BHC (Lindane)i 8.9 lu 1 I 76 -44 -8 -----Heptachlor ( 8.9 IU I I 309 -00 -2 -----Aldrin I 8.9 lu I I 1024 -57 -3 -----Heptachlor epoxideI 8.9 1U I 1 959-98-8-- --- 8ndosulfan I I 8.9 IU I I 60 -57 -1 -----Dieldrin I •8.9 lU I I 72-55-9-----4,4'-DDR I 18. IU I I 72 -20 -8 -----Endrin I 13. -1 1 1 1 33213-65-9 ----- gndosulfan II I 18' 1U I I 72-54-8-----4,4'-DDD I 1.6 1 1 1 I 1031-07-8 ----- 3ndosulfan sulfate I 18. 1U I I 50-29-3-----4,4'-DDT I 15• 1 1 I 72 -43 -5 -----Methoxychlor I 32. 1 1 I 53494 -70 -5 -----Endrin ketone I 89. 1U I 1 5103-71-9 ----- alpha-ChlordaneI 18. lu I 1 5103-74-2-----gam-Chlordane i 89. lu I 8001 -35 -2 -----Toxaphene I 89. lu I 1 12674-11.-2 ----- Aroclor-1016 I 180. IU I 1 11104-26-2 -----I 89. lu I I 11141-19-5-----Aroclor-1232 I 89. 1U I 53469-21-9-----Azoclor-1242 I 89. lu I I 12672-29-6-----Aroclor-1248 189. lU I 1 11097-69-1 ----- Aroclor-1254 89. 1U I 1 11096-82-5 ----- Asoclor-1260 I 180. lu I 1 180. lu I I_I 488 FORM I PEST 1/87 Rev. 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECK Lab Code: INTECH Case No.: 15486 I I I BFF75 1 Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Matrix: (soil/crater) WATER Lab Sample ID: IU I Sample wt/vol: 1000. (g/mL)ML Lab File ID: GP4426 IU I Level: (low/med) LOW Date Received: 12/ 6/90 Moisture: not dec.100. - dec. 0. Date Extracted: 12/ 7/90 Extraction: (SepF/Cont/Sonc) SEPF Date Analyzed: 12/ 9/90 GPC Cleanup: (Y/N) N pH: 8.1 Dilution Factor: 1.00 CONCENTRATION UNITS: CAS NO. COMPOUND (ug/L or ug/Kg) UG/L p I I 319-84-6-----alpha-BHC I I .050 I I IU I I 319-85-7-----beta-BHC I .050 IU I I 319-86-8-----delta-BHC I .050 IU I I 58-89-9-----gamma-BHC (Lindane) I .050 IU I I 76 -44 -8 -----Heptachlor f .050. IU I I 309 -00 -2 -----Aldrin I .050 IU I 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU I 1 959-98-8 ----- Endosulfan I I .050 IU I 1 60 -57 -1 -----Dieldrin I .10 IU I I 72-55-9-----4,4'-DDE I .10 IU I I 72 -20 -8 -----Endrin I .10 IU I 1 33213-65-9 ----- Endosulfan II 1 .10 IU I 1 72-54-8-----4,4'-DDD I .10 IU I 1 1031-07-8 ----- Endosulfan sulfate ( .10 IU I I 50-29-3-----4,4'-DDT I .10 IU I I 72 -43 -5 -----Methoxychlor I .50 IU I 53494 -70 -5 -----Endrin ketone I .10 lU I 15103-71-9-----alpha-Chlordane I .50 IU I 1 5103-74-2-----gamma-Chlordane I .50 IU I 1 8001 -35 -2 -----Toxaphene I 1.0 IU I I 12674-11-2-----Aroclor-1016 I 50 IU I 11104-26-2 ----- Aroclor-1221 1 .50 IU I 11141-16-5-----Aroclor-1232 ( .50 IU I 53469-21-9 ----- Aroclor-1242 I .50 IU I 12672-29-6-----Aroclor-1248 1 .50 IU I 11097-69-1 ----- Aroclor-1254 1 1.0 IU I 11096-82-5 ----- Aroclor-1260 1 1.0 IU I FORM I PEST I i i j 1/87 Rev..; 1D PESTICIDE ORGANICS ANALYSIS DATA SHEET Lab Name: INTECH Lab Code: INTECH Case No.: 15486 Matrix: (soil/water) WATER Sample wt/vol: 1000. (g/mL)ML 'Level: (low/med) LOW % Moisture: not dec.100. - dec. Extraction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND EPA SAMPLE NO. i I BFF76 Contract: 68-D9-0048 I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4427 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 3 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC I i .050 I I IU I 319-85-7-----beta-BHC I .050 IU I 319-86-8-----delta-BHC I .050 IU 1 58-89-9-----gamma-BHC (Lindane) I .050 IU 1 76 -44 -8 -----Heptachlor I .050 IU 1 309 -00 -2 -----Aldrin I .050 IU 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU 1 959-98-8 ----- Endosulfan I I .050 IU 1 60 -57 -1 -----Dieldrin I .10 IU 1 72-55-9-----4,4'-DDE i .10 lU 1 72 -20 -8 -----Endrin I .10 IU I 33213-65-9-----Endosulfan II ( .10 IU 1 72-54-8-----4,4'-DDD I .10 IU I 1031-07-8-----Endosulfan sulfate I .10 IU 1 50-29-3-----4,4'-DDT I .10 IU 1 72 -43 -5 -----Methoxychlor I .50 IU 1 53494 -70 -5 -----Endrin ketone I .10 IU 1 5103-71-9-----alpha-Chlordane I .50 IU I 5103-74-2-----gamma-Chlordane I .50 IU 1 8001 -35 -2 -----Toxaphene I 1.0 IU I 12674-11-2 ----- Aroclor-1016 I .50 IU I 11104-2$-2 ----- Aroclor-1221 I .50 IU I 11141-16-5 ----- Aroclor-1232 I .50 IU I 53469-21-9 ----- Aroclor-1242 I .50 IU I 12672-29-6 ----- Aroclor-1248 I .50 IU I 11097-69-1 ----- Aroclor-1254 I 1.0 IU I 11096-82-5 ----- Aroclor-1260 I 1.0 IU I 362 FORM I PEST 1/87 Rev.! IV PESTICIDE ORGANICS ANAL ijab Name: INTECH ri Code: INTECH Case No.: 15486 Aatrix: (soil/water) MATER S aple wt/vol: 1000. (g/mL)ML L rel: (1 ow/reed ) LOW Moisture: not dec.100. ' dec. 32 :raction: (SepF/Cont/Sonc) SEPF GPC Cleanup: (Y/N) N pH: CAS NO. COMPOUND EPA SAMPLE NO. YSIS DATA SHEET i I I BFF77 I Contract: 68-D9-0048 I I SAS No.: SDG No.: BFC39 Lab Sample ID: Lab File ID: GP4428 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/ 9/90 9 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC 1 .050 IU 1 319-85-7-----beta-BHC ( .050 IU 1 319-86-8-----delta-BHC I .050 IU I 58-89-9-----gamma-BHC (Lindane) 1 .050 IU 1 76 -44 -8 -----Heptachlor 1 .050 IU 1 309 -00 -2 -----Aldrin ( .050 IU 1 1024 -57 -3 -----Heptachlor epoxide I .050 IU 1 959-98-8 ----- Endosulfan I 1 .050 IU 1 60 -57 -1 -----Dieldrin I .10 IU 1 72-55-9-----4,4°-DDE ( .10 IU I 72 -20 -8 -----Endrin 1 .10 IU 1 33213-65-9 ----- Endosulfan II I .10 IU 1 72-54-8-----4,4'-DDD I .10 IU 1 1031-07-8 ----- Endosulfan sulfate I .10 IU 1 50-29-3-----4,4'-DDT I .10 IU 1 72 -43 -5 -----Methoxychlor 1 .50 IU 1 53494 -70 -5 -----Endrin ketone I .10 IU I 5103-71-9-----alpha-Chlordane I .50 IU 1 5103-74-2-----gamma-Chlordane i .50 IU 1 8001 -35 -2 -----Toxaphene I 1.0 IU 1 12674-11-2 ----- Aroclor-1016 I .50 IU 1 11104-28=2 ----- Aroclor-1221 I .50 IU 1 11141-16-5 ----- Aroclor-1232 I .50 IU 1 53469-21-9 ----- Aroclor-1242 I .50 IU 1 12672-29-6 ----- Aroclor-1248 1 .50 IU 1 11097-69-1 ----- Aroclor-1254 1 1.0 IU 1 11096-82-5 ----- Aroclor-1260 1 1.0 I IU I I I FORM I PEST 365 1/87 Rev, 1D EPA SAMPLE NO. PESTICIDE ORGANICS ANALYSIS DATA SHEET I I Lab Name: INTECHI BFF78 I Contract: 68-D9-0048 I I ab Code: INTECH Case No.: 15486 SAS No.: SDG No.: BFC39 Matrix: (soil/water) WATER _ample wt/vol: 1000. (g/mL)ML evel: (low/med) LOW Moisture: not dec.100. ' dec. 0. xtraction: (SePP/Cont/Sone) SEPF GPC Cleanup: (Y/N) N pH: 7.2 CAS NO. COMPOUND Lab Sample ID: Lab File ID: GP8814 Date Received: 12/ 6/90 Date Extracted: 12/ 7/90 Date Analyzed: 12/15/90 Dilution Factor: 1.00 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q 319-84-6-----alpha-BHC 319-85-7-----beta-BHC 31.9-86-8-----delta-BHC 58-89-9-----gamma-BHC (Lindane) 76 -44 -8 -----Heptachlor 309 -00 -2 -----Aldrin 1024 -57 -3 -----Heptachlor epoxide 959-98-8 ----- Endosulfan I 60 -57 -1 -----Dieldrin 72-55-9-----4,4'-DDE 72 -20 -8 -----Endrin 33213-65-9 ----- Endosulfan II 72-54-8-----4,4'-DDD 1031-07-8 ----- Endosulfan sulfate 50-29-3-----4,4'-DDT 72 -43 -5 -----Methoxychlor 53494 -70 -5 -----Endrin ketone 5103-71-9-----alpha-Chlordane 5103-74-2-----gamma-Chlordane 8001 -35 -2 -----Toxaphene 12674-11-2 ----- Aroclor-1016 11104-28=2 ----- Aroclor-1221 11141-16-5 ----- Aroclor-1232 53469-21-9 ----- Aroclor-1242 12672-29-6 ----- Aroclor-1248 11097-69-1-----Aroclor-1254 11096-82-5 ----- Aroclor-1260 I I .050 I I IU I .050 I U_ I I .050 IU I I .050 IU I I .050 IU I I .050 IU I I .050 IU I i .050 IU I I .10 IU I I .10 IU I I .10 IU I I .10 IU I I .10 IU I I .10 IU I I .10 IU I I .50 IU I I .10 IU I I .50 IU I I .50 IU I I 1.0 IU I ( .50 IU I I .50 IU I I .50 IU I I .50 IU I I .50 IU I I 1.0 IU I I 1.0 - I IU I I I 369 FORM I PEST 1/87 Rev. ARD OPERA=M PROCURE Page 27 of 35 Title: Evaluation of Metals Data for the Date: Feb. 1990 Contract Laboratory Program NXmiber: W-2 Appendix A.2: Data Assessment Narrative Revision: 10 case# f&4 96 Site SvLAO i Matrix: soil SDG# P)P) C F S m 8E 3) Lab ALL water Contractor t:7 / -r a Reviewer C. other '— A.2.1 The case description and exceptions, if any, are noted below with reason(s) for rejection or qualification as estimated value(s) J. ..e- _ S0& MP)EF9-L ftl PAF F `N . I15 Ci („ -41 PROC=URE Page 28 of 35 Title: Evaluatian cf Metals Data for the Date: Feb. 1990 Cantract Laboratory Program Umber: W-2Appeix A. 2: Data Assessment Narrative Revision: 10 A.2.1 wl o/ a --- S (,1.64)- s --, me,r c a ter) 2 67o D I _ � CCL -..J., ma�F ra - Cr 4, rne-)EGa9 ) 9- a-7 Mn _ "J" , M6r= & 19 -a 7 m86 F 93- 5 (p, 9 7) m6EG ig- d 1, d3 -,?5 s OPMA= P�aoc� Page 29 of 35 Title: Eraluaticn of Metals Data for the Contract laboratory Program Date: Feb. 1990 Appendix A.2: DataNLm ber: HW -2 Asses-Qt�t Narrative Revision: 10 A. 2.1 (Continuation)wCO. Zn -- C M /9- C� 0=3I.Q.1. d;L)Y SSD OPEPATIM PRQCmiTRE Page 30 of 35 'itle: EvaluatiCn of Metals Data for the Date: Feb. 1990 Contract Laboratory Program NLmlber: HW -2 Appendix A.2: Data Assessment Narrative Revision: 10 11J lli 1C�.lG(Y TC Irl(' V�:Nc P�illj I Ir't a nFA -M--M ,L;I QYl Pb - mt n nam F9 9,91, q e, Cao x ab, a�C ( a (a5 nntbEc� C��) rY)bEG IG, ate , �-7 M615Ga4 x�r mR���g3'Cl�x) N n I I i i Al I � i • � tea' . •l .,! A.2.2 C it ct-p le'ms G 5 . /Non�rpliance m����J / �ecau-� MSB Reviewer: Date: Contractor Reviewer: Verified by: Date: , Date:_ l �__-- a U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I I b Name: ASSOCIATED LABORATORIES_ Contract: 68-D9-0079 MBEF92 b'�_'ode: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 t -ix (soil/water): WATER 00012 Lab Sample ID: MBEF92 V=i (low/med): LOW_ Date Received: 12/06/90 S. Lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L ICAS No. I Analyte IconcentrationlCI Q IM 1.7429-90-5 1Aluminum 1 36.01U1 Ip_1 17440-36-0 1Antimony_1 •31.01U1 Ip_l 17440-38-2 IArsenic_I 2.01U1 IF_I 17440-39-3 1Barium 1 56.7 1 B 17440-41-7 1Berylliuml ••3.OIU I _ Ip_1 17440-43-9 1Cadmium 1 5.01U1 Ip_I 17440-70-2 1Calcium_I -81601 �—Ip_1 17440-47-3 1Chromium 1 .6.0 U p_ 17440-48-4 (Cobalt 1 -12.0IUJ - IP 17440-50-8 Kopper I 2131_ r --T —Ip_I -1 17439-89-6 17439-92-1 (Iron 1 (Lead l 3351_17 N I 17439 95-4 IMagnesiuml 20.0 U WN —IIP 44901B1 F Ip _ 17439-96-5 IManganesel 3671_1 _I IpI 17439-97-6 IMercury_I 0.701_1 IC_I 17440-02-0 INickel I 25.OIU1 Ip_I 17440-09-7 IPotassiuml 46001B1 IP_I 17782-49-2 -..�w i 6.8 e• -1_I F-1 i 17440-22-4 ISilver I 1 7.0 U1 IP-1 17440-23-5 ISodium 1 27100 17440-28-0 (Thallium I 3.01U MWN_IF_1 17440-62-2 lvanadium_1 4.01Ul IP 17440-66-6 1Zinc 1 23,71_1 -1 Ip_1 Cyan1de_1 I_I I_I 1NR1 1_1 for Before: COLORLESS Clarity Before: CLEAR Texture: Lc After: COLORLESS Clarity After: CLEAR Artifacts: = nts: FORM'j - IN V 7/88 U.S. EPA --CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET 1 ab Name:ASSOCIATED_LABORATORIES_ Contract: 68-D9-0079 MBEF96 a, !Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 atrix (soil/water): WATER Lab Sample ID: MBEF96 ei _'Bl (low/med) : LOW 1)0016 Date Received: 12/06/90 lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L_ I ICAS No. I I I I I Analyte IConcentrationlCl Q 1 IM 17429-90-5 1Aluminum_1 CLEAR ip_1 36.01UI 17440-36-0 1Antimony_1 37.81BIj• 1P_1, 17440-38-2 1Arsenic_1 2.0 U I I IF_I 17440-39-3 (Barium 1 36.6 B.T 17440-41-7 IBerylliuml 3".01U1 _ Ip_I 17440-43-9- (Cadmium 1 5.0 U p_ 17440-70-2 1Calcium l 56600 1_ 17440-47-3 1Chromium l _ 6.01UJjk IP -1 ; 17440-48-4 (Cobalt 1 12.01U1 IP -17440-50-8 17440-50-8 (Copper i -1 - 1561_1Z_Ip_I 17439-89-6 11ron I 2461_1�N Ip_I 17439-92-1 (Lead 1•- 20.0 1 UIWN 17439-95-4 IMagnesiuml 124001_1 _ Ip_1 17439-96-5 1Manganesel 5.91B1 1p_1 17439-97-6 IMercury_1 i lcvi 17440-02-0 (Nickel 1 -0.801_1 25.0 U 17440-09-7 IPotassiuml 45601BI _ 1p_1 17782-49-2 1 17440-22-4 (Silver 1 7.01U1 Ip_1 17440-23-5 (Sodium 1 12000 17440-28-0 1Thallium 1 3.01U LWN 1F 17440-62-2 1Vanadium 1 5:61BI IP 17440-66-6 1Zinc 1 -1 4051_1_Ip_1 Cyanide_i 1_1 INRI I_I I_I olor Before: COLORLESS Clarity Before: CLEAR 0.)r After: COLORLESS Clarity After: CLEAR or rents : FORM I - IN .. ..�: .. :=v:���.3�.%:.-*iii'.at"¢�-.i'+i�'-��.C"y?;rn"f .i3'Av�i,'ir•.;'�.�,`•-�r0,.�� hj�?�'a7h,.-ti�».�.. +�� _ Texture: Artifacts: 7/88 U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET ,ab Name: ASSOCIATED LABORATORIES_ J� Code: ALI Case No.: 15486 z,4 -rix (soil/water): WATER Contract: 68-D9-0079 I EPA SAMPLE NO. 1 MBEF97 I I SAS No.: SDG No.: MBEF92 Lab Sample ID: MBEF97 (low/med): LOW 00017' Date Received: 12/06/90 olids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L_ I ICAS No. I I I I Analyte IConcentrationlCl Q I IM 17429-90-5 (Aluminum 1 36.01U1 Ip_1 17440-36-0 1Antimony_1 31.0IU1 1p_1 17440-38-2 IArsenic_1 2.01UI IF_I 17440-39-3 (Barium I 36.21B1,�r 17440-41-7 1Berylliuml 3.0IU1 -Ip_I Ip_1 17440-43-9 1Cadmium I 5.0 U I Ip_I 17440-70-2 ICalcium_1 365001_ E 17440-47-3 (Chromium 1 6.01U�Ip_1 _ 17440-48-4 (Cobalt 1 12 01U1 IP 17440-50-8 (Copper 1 -1 1851_(y IP 17439-89-6 (Iron I 2841_1,2__N -1 Ip_1 17439-92-1 I Lead 1•• 20. 0 U AWN_ 17439-95-4 1Magnesiuml 91401_1 Ip 1 17439-96-5 1Manganesel 4.OIB1 IP_1 174.39-97-6 IMercury_I 0.701_1 ICV( 17440-02-0 INickel 1 25.0 U 17440-09-7 1Potassiuml 41901B1 _ IP_1 17782-49-2 F_I 1 17440-22-4 _ ISilver I 7.0 I U I8730 I p_ 17440-23-5 ISodium 1 17440-28-0 I Thallium 1 _ 3 .01 U kz-WN_ I F_ 1 17440-62-2 (Vanadium 1--3. 4.01U1 IP_I 17440-66-6 (Zinc 1 -38.31_1 Ip_t I 1Cyanide_I i I I I INR1 'olor Before: COLORLESS Clarity —I-1-1-1 Before: CLEAR Texture: 'a :)r After: COLORLESS Clarity After: CLEAR Artifacts: 'o vents: FORM I - IN 7/88 'z -� l'+•:.6','i�Z' ,*M'�• `+.�e1iw.?a�i-n!�'w==r'S,.+�.-�: s.:'—�r�l:� U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET Name: ASSOCIATED_LABORATORIES_ Contract: 68-D9-0079 1 b Code: ALI Case No.: 15486 t ix (soil/water): WATER SAS No.: EPA SAMPLE NO. MBEF98 SDG No.: MBEF92 Lab Sample ID: MBEF98 .vel (low/med) : LOW �1t10�� Date Received: 12/06/90 S Lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L ICAS No., I Analyte 1ConcentrationlCl Q IM 17429-90-5 1 IAluminum_1 1111 36.01U1 IP 17440-36-0 1Antimony_1 38.31B1�IP_1 -1 17440-38-2 1Arsenic_1 2.0 U 17440-39-3 (Barium 1 78.51BI _ IP 17440-41-7 1Beryllium1 3.OIU1 -1 IP_1 17440-43-9- ICadmium_1 5.OIU1 IP_I 17440-70-2 ICalcium_I 289001_IZ_E IP_I 17440-47-3 (Chromium I 6.01UI�t IP_1 17440-48-4 (Cobalt 1 12.01U11P_1 17440-50-8 Kopper I 4.01U1 IP 17439-89-6 (Iron I 15501_ 1N -1 IP_I 17439-92-1 (Lead I.. 20..OIUI- IF_1 17439-95-4 IMagnesiuml 192001_1 IP_I 17439-96-5 IManganesel 7.91BI 1P_1 17439-97-6 IMercury_I 0.201UI ICV1 17440-02-0 INickel 1 25.O1UI 1P_1 17440-09-7 1Potassiuml 20101BI IP_1 17782-49-2 1 17440-22-4 _ ISilver I11 IP_1 17440-23-5 ISodium 1 274001_11_1 17440-28-0 IThallium_I 3.01UI�IF_1 17440-62-2 IVanadium 1 8.21BI IP 17440-66-6 IZinc 1 2141_11r-IP—I 1 ICyanide_1 1 1_I 1_I INRI 1_1 :)1-r Before: COLORLESS Clarity Before: CLEAR Texture: Dlor After: COLORLESS Clarity After: CLEAR Artifacts: mi ents : FORM I - IN 7/88 U.S. EPA - CLP 1 EPA SAMPLE. NO. INORGANIC ANALYSES DATA SHEET I I ah Name: ASSOCIATED LABORATORIESMBEF99 _ Contract: 68-D9-0079 1 a- Code: ALI Case No.: 154R6 SAS No.: SDG No.: MBEF92 a 'rix (soil/water): WATER Lab Sample ID: 1 dMBEF99_ =vel ow meLOW 00019. ( / )� _ Date Received: 12/06/90 lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L 1 ICAS No. I Analyte IConcentrationlCI Q IM I 17429-90-5 1 (Aluminum 1 7331_1 IP_1 17440-36-0 IAntimony_1 31.OIUI IP 17440-38-2 1Arsenic_1 2.01UI -1 IF_I 17440-39-3 1Barium 1 27.81BIj_IP_1 17440-41-7 1Berylliuml 3.01U[ IP 17440-43-9 1Cadmium 1 S.OIUI • -1 IP 17440-70-2 ICalcium_1 40401BI,IP_I -1 17440-47-3 1Chromium 1 6.01U1-1, 17440-48-4 (Cobalt 1 _1P_I 12.OIUI' IP 17440-50-8 Kopper I '59.21_1:_IP_1 -1 17439-89-6 lIron 1 96.71BQZ_N IP_1 17439-92-1 [Lead I '' 2.0 U WN 17439-95-4 IMagnesiuml 27701BI. IP 17439-96-5 IManganesel 1.01UI Ip_I 17439-97-6 IMercury_I 0.601_1 1CV1 17440-02-0 1Nickel 1 25.01UI IP 17440-09-7 IPotassiuml 14301BI -1 Ip_1 17782-49-2 I P 17440-22-4 ISilver I 7.61B[ IP_I 17440-23-5 ISodium 1 86701_1_ 17440-28-0 IThallium 1 3.01U,WN IF_1 17440-62-2 IVanadium [ 4.OIUI 1P_1 17440-66-6 1Zinc I Ip_I I I Cyanide_ I-22.1.1_1 I_ I 1-1 -11 I NR I o' -)r Before: o -Lor After: of tents: COLORLESS Clarity Before: CLEAR Texture: COLORLESS Clarity After: CLEAR Artifacts: FORM I - IN 7/88 U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET ,ab Name: ASSOCIATED-LABORATORIES— Code: SSOCIATEDLABORATORIES Code: ALI Case No.: 15486 :?(rix (soil/water): WATER ,G, el (low/med) : LOW_ olids: 0.0 EPA SAMPLE NO. I MBEF93 1 Contract: 68-D9-0079 I SAS No.: SDG No.: MBEF92 Lab Sample ID: MBEF93 011013 Date Received: 12/06/90 Concentration Units (ug/L or mg/kg dry weight): UG/I,_ ICAS No. II 1 I Analyte IConcentrationlCl Q IM 17429-90-5 (Aluminum I ip-1 44.3181 17440-36-0 (Antimony -1 31.01U1 IP 17440-38-2 IArsenic_I 2.01UI -1 IF 17440-39-3 (Barium 1 -1 32.91BI'.T_.IP—I 17440-41-7 IBeryll' I 3.01U1 Ip 17440-43-9 (Cadmium I 5.01 U 1 -I Ip 17440-70-2 ICalcium_1 .144001- �E -I. IP-1 17440-47-3 IChromium I 12.3 17440-48-4 (Cobalt I 12.01U1 -IP-1 1 I 1P-1 17440-50-8 1Copper IP 17439-89-6 (Iron 1 34401_ N 1 1 ITN -1 IP 17439-92-1 I Lead 1•• 20, 0 U -1 17439-95-4 IMagnesiuml-20,01 95701-1 IP 17439-96-5 IManganesel 7,91BI -1 IP 17439-97-6 IMercury_1 0.201-1 -1 ICV1 17440-02-0 INickel 1 25.01U 17440-09-7 IPotassiuml 19201BI IP 17782-49-2 1 S e VVIIIF- -1 1 17440-22-4 (Silver I 7.01 U 1 IP 17440-23-5 ISodium 1 21700 -1 17440-28-0 IThallium l 3.01U�--- �F_� 17440-62-2 (Vanadium I 4.8(81 IP 17440-66-6 (Zinc 1 297- I IIP -1 (cyanide_ 1. I 1_1 1-1 -1 INRI I_I olor Before: COLORLESS Clarity Before: CLEAR Texture: , o; )r After: COLORLESS Clarity After: CLEAR Artifacts: or --tents: -c AUX FORM I - IN 7/88 _ U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L_ I I I I I I ICAS No. I Analyte JConcentrationlCl Q IM 17429-90-5 lAluminum_l 1 EPA SAMPLE NO. lAntimony_I INORGANIC ANALYSES DATA SHEET IArsenic_1 2.OIU1 3b Name: ASSOCIATED LABORATORIES— Contract: I I 68-D9-0079 I l MBEF94 l 1 * Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 3}"'ix (soil/water): WATER 1p_I Lab Sample ID: MBEF94 2"„d1 (low/med) : LOW 17440-47-3 17440-48-4 Date Received: 12/06/90 )lids: 0.0 1 13.OIB1 IP Concentration Units (ug/L or mg/kg dry weight): UG/L_ I I I I I I ICAS No. I Analyte JConcentrationlCl Q IM 17429-90-5 lAluminum_l 3011_1 IP_I 17440-36-0 lAntimony_I 89.31_1,- IP 17440-38-2 IArsenic_1 2.OIU1 -1 IT 17440-39-3 (Barium l -1 1281B1,T IP 17440-41-7 lBerylliuml 3.01U1 -1 IP_1 17440-43-9 1Cadmium 1 5.01U1 1p_I 17440-70-2 ICalcium_1 658001_ E IP_1 17440-47-3 17440-48-4 lChromium 1 lCobalt 20.01_ IP -1 1 13.OIB1 IP 17440-50-8 Kopper l •31.41_1. -1 1P_1 17439-89-6 (Iron 1 101001_ 1 -Ip 1 17439-92-1 (Lead 1•• 63.71_1�SN—IF_I 17439-95-4 1Magnesiuml434001_1 Ip_I 17439-96-5 IManganesel 30201_I IP_1 17439-97-6 IMercury-1 0.301_1 ICV 17440-02-0 (Nickel I 25.0 U 17440-09-7 lPotassiuml 1670001_1 _ IP 17782-49-2 1 _ -1 F i. 17440-22-4 (Silver l 7.OIUl IP 17440-23-5 ISodium 1 158000 -1 -17440-28-0 1Thallium 1 _ 3.01UI,4f � _ IF_1 17440-62-2 IVanadiuml 10.21B1 IP 17440-66-6 (Zinc 1 1971_QT_IP_1 -1 Cyanide—i 1 _1 -1 —1 I NR I 1-1 olor Before: BROWN Clarity Before: CLOUDY Texture: o: ,r After: COLORLESS Clarity After: CLEAR Artifacts: of gents: FORM I - IN 7/88 + _ � � ..: .. •=�`y'•:L�T�4 � � ..+i1::i'�+r+:8'ai�Jr,'�`t�:ri�r'.��:: �: � - _c.' Zr:�. '; '.�. Ims�ni ^'-. =.n, fir.-: U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET > Name: ASSOCIATED_LABORATORIES Contract: 68-D9-0079 ;ode: ALI Case No.: 15486 .x (soil/water): WATER EPA SAMPLE NO. MBEF95 SAS No.: SDG No.: MBEF92 Lab Sample ID: MBEF95 t�uoss rel (low/med): LOW_ Date Received: 12/06/90 3' Lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L ICAS No. I Analyte IConcentrationlCI Q IM 17429-90-5 lAluminum 1 3081_1 IP -1 17440-36-0 IAntimony_1 74.41_IZ_IP_1 17440-38-2 1Arsenic_1 2.OIUI IF_I 17440-39-3 1Barium 1 1231B1:3 IP -1 17440-41-7 1Berylliuml 3.01U1IP_I 17440-43-9 ICadmium 1 5.01U1 IP 17440-70-2 1Calcium_I 633001_I -1 IP_1 17440-47-3 1Chromium 1 23.41_1-1P_1 17440-48-4 1Cobalt I 12.01U1 IP -1 17440-50-8 Kopper I .31.41_1 JP_1 17439-89-6 (Iron 1 97201_1�IP_1 17439-92-1 1Lead 175.61_1�LSN_IF_I 17439-95-4 IMagnesiuml 420001_1 IP_1 17439-96-5 IManganesel 29001_1 IP 17439-97-6 IMercury_I 0.301_1 -1 1CV1 17440-02-0 (Nickel I 25.OIU1 IP -1 17440-09-7 1Potassiuml 1620001_1 IP_I -17782-49-2 i 1 1. 17440-22-4 _ (Silver I _ 7.O1Ul _ IP_1 17440-23-5 ISodium 1 1530001_1 IP_1 17440-28-0 IThallium 1 3.01U1j­WN_1F_1 17440-62-2 IVanadium 1 9.21BI 1P_1 17440-66-6 1Zinc 1 1951_1:tP�1 I ICyanide— I I I 1_1 INRI )1^r Before: BROWN )I -r After: COLORLESS )n ents : OIL Clarity Before: CLOUDY .. Texture: Clarity After: CLEAR Artifacts: YES FORM I - IN 7/88 U.S. EPA - CLP D0(2)a0 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET ab Name: ASSOCIATED LABORATORIES I 1 MBEG19 I Contract: 68-D9-0079 I I Code: ALI Case No.: 15486 SAS No.: < • rix (soil/water) : SOIL SDG No.: MBEF92 Lab Sample ID: MBEG19 .evel (low/med): LOW_ Date Received: 12/06/90 olids: 88.3 Concentration Units (ug/L or mg/kg dry weight): MG/KG I CAS No. I I i Analyte iConcentrationlCl Q IM 17429-90-5 IAluminum_1 1-1-11 IP 46401_1 17440-36-0 lAntitony_1 6.61U1 -1 1P_1 17440-38-2 IArsenic_1 8,31_1 IF_I 17440-39-3 1Barium 1 17.9IBIa IP 17440-41-7 1Berylliuml 0.671B1 -1 1p_1 17440-43=9 (Cadmium 1 1.11U1 Ip_I 17440-70-2 1Calcium_1 7211BI_lp_I � 17440-47-3 1Chromium l 6.91_1 Ip_I 17440-48-4 1Cobalt 1 2.6 U 17440-50-8 1,Copper 1 _ 19.71_I_IP_1 17439-89-6 11ron 1 63701_1 IP 17439-92-1 (Lead18.81_1_1 5 -1 F_1 17439-95-4 IMagnesiuml 6451BI IP 17439-96-5 IManganesel 1021_1ZE -1 IP_1 17439-97-6 1 17440-02-01Nickel _ 1 5.31U1 Ip_I 17440-09-7 IPotassiuml 2101BI IP_1 17782-49-2 ISelenium_1 0.481UI_SN_IF_1 17440-22-4 ISilver 1 2.018( IP 17440-23-5 ISodium 1 110 B -1 17440-28-0 IThallium 1 0.66IUI _ IF_I 17440-62-2 IVanadium 1 13.01_1 P-1 17440-66-6 (Zinc 1 —1 44.61_I__Ip_1 Cyanide -1 I_I INRI —11 —1-1 :olor Before: BROWN Clarity Before: Texture: MEDIUM :c_or After: BROWN Clarity After: Artifacts: YES :c rents: STONES FORM I - IN 7/88 U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET .ab Name: ASSOCIATED -LABORATORIES Code: ALI Case No.: 15486 -E-rix (soil/water): SOIL Contract: 68-D9-0079 SAS No.: EPA SAMPLE NO. 1 MBEG20 1 I SDG No.: MBEF92 Lab Sample ID: MBEG20 .evel (low/med) : LOW ()10021 Date Received: 12/06/90 olids: 88.3 Concentration Units (ug/L or mg/kg dry weight): MG/KG ICAS No. I Analyte IConcentrationlCl Q IM 17429-90-5 (Aluminum I 53201_1 Ip_1 17440-36-0 IAntimony_1 6.51U1 Ip_I 17440-38-2 1Arsenic_I 8.71_1 17440-39-3 (Barium 1 '1Bery11iumI 19.61BI,.r 17440-41-7 0.631U1 _Ip_1 1p_1 17440-43-9 ICadmium 1 1.0 U1 IP 17440-70-2 (Calcium_( -1 659 B � p_ 17440-47-3 (Chromium 1 7.31_1 Ip_I 17440-48-4 (Cobalt 1 3.71B1 11U 17440-50-8 [Copper I 16.71_ p_1 17439-89-6 (Iron 1 72801_1 .1 Ip_I 17439-92-1 (Lead -1 74.1 17439-95-4 IMagnesiuml _ _W 7471BI _ Ip_1 17439-96-5 IManganesel 1061_f�E Ip_1 17439-97-6 I -_-r , 17440-02-0 INickel I 5.21U 17440-09-7 IPotassiuml 2411BI _1 Ip_1 17782-49-2 ISelenium 1 0.421UI_N IF_I 17440-22-4 ISilver I 2,71_1_1 ]�__j 17440-23-5 ISodium 2 17440-28-0 1Thal lium I 0641U IF-1 17440-62-2 (Vanadium i 13.81_1 - Ip 17440-66-6 IZinc 44.01 mo— I Cyanide_ I I 1 _1_1 INR I olor Before: BROWN Clarity Before: Texture: MEDIUM o )r After: BROWN Clarity After: Artifacts: YES vents: STONES FORM I - IN 7/88 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): MG/KG I ICAS No. INORGANIC 1 EPA ANALYSES DATA SHEET SAMPLE NO. (Aluminum I gab Name: ASSOCIATED -LABORATORIES— Contract: 68-D9-0079 I I MBEG21 J� Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 Iz'Lrix (soil/water): revel (low/med) : SOIL LOW — Lab Sample ID: 00022 Date Received: MBEG21 12/06/90 olids: 90.8 _ 17440-41-7 Concentration Units (ug/L or mg/kg dry weight): MG/KG I ICAS No. I I Analyte 1ConcentrationlCl Q IM 17429-90-5 (Aluminum I 21401_1 Ip_I 17440-36-0 (Antimony -I 6.81UI Ip_1 17440-38-2 1Arsenic-1 1.8 B 17440-39-3 1Barium 1 9.11B�_Ip—I _ 17440-41-7 1Bery1liuml 0.661UI IP 17440-43-5 ICadmium 1 1.11U1 -I Ip 17440-70-2 ICalcium I 625 B �r -I p_ 17440-47-3 IChromium 1 3.31_1 Ip 17440-48-4 (Cobalt 1 j 2.61UI -I Ip—I 17440-50-8 ICopper 1 Ip_I 17439-89-6 (Iron 1 501011_1 Ip_1 17439-92-1 (Lead 1•• 49.5I IF-1 17439-95-4 IMagnesiuml 4421B 17439-96-5 IManganesel 75.71_-�-�Ip—I 17439-97-6 I M 17440-02-0 INickel _ IP 17440-09-7 1Potassiuml 1911IBI -1 1 I_ 17782-49-2 ISelenium l 0.471BI1 y IFI 17440-22-4 ISilver 1 1.51U1 Ip—I 17440-23-5 ISodium 1 88,0I81 Ip 17440-28-0 IThallium l 0.561U1 -I IF-I 17440-62-2 1Vanadium l 7.18 1 1 1P—I 17440-66-6 (Zinc 1 75,9II IP_I I 1Cyanide 1 —� _ I_I I_I INR1 I—I :olor Before: BROWN Clarity Before: Texture: MEDIUM 'o_ -)r After: BROWN Clarity After: Artifacts: YES 'o vents: ;TONES AND ROOTS FORM I - IN 7/88 r: ';�.e���.. ... ... .. i.., $A: y+'rt rn•'G%<tiiK�; �•ia-'tn�:�� ..: ....•.��rT _.__ ..ti �.....,� ....,�. .. .v ....._ _ __ � " U.S. EPA - CLP 1 INORGANIC ANALYSES DATA SHEET ab Name: ASSOCIATED LABORATORIES Contract: 68-D9-0079 EPA SAMPLE NO. I MBEG22 1 1 a Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 a rix (soil/water): SOIL_ Lab Sample ID: MBEG22 W3023 evel (low/med): LOW_ Date Received: 12/06/90 olids: 75.4 Concentration Units (ug/L or mg/kg dry weight): MG/KG I ICAS No. I I I I I I Analyte IConcentrationlCI Q I I IM 17429-90-5 I 1Aluminum 1 1-1-11 IP 40301_1 17440-36-0 IAntimony_1 7.61UI -1 IP 17440-38-2 1Arsenic_1 3.21_1 -1 IF 17440-39-3 1Barium 1 14.41BI�IP_1 -1 17440-41-7 IBerylliuml 0.741UI IP_1 17440-43-9 (Cadmium 1 1.21UI IP 17440-70-2 1Calcium 1 983IBIT -1 IP 17440-47-3 (Chromium I 6.31_1 -1 IP 17440-48-4 1Cobalt 1 i 2.91U1 -1 IP 17440-50-8 (Copper -1 •10.81_1—_IP-1 -1 17439-89-6 (Iron 1 49401_1 IP 17439-92-1 1Lead 1 20.61_1 -1 IF_j 17439-95-4 IMagnesiuml 9711BI IP 17439-96-5 IManganesel 45.71_1 -1 1P_1 17439-97-6 1M —E 17440-02-0 _ 1Nickel 1 6.1 U1 17440-09-7 1Potassiuml 2861B IP I 17782-49-2 (Selenium 1 0.541B�—IF-I 17440-22-4 ISilver 1 2.11B1 1P_I 17440-23-5 ISodium 1 1061B1 IP_1 17440-28-0 1Thal 1ium 1 0.771U1 IF_I 17440-62-2 1Vanadium 1 8,71BJ Ip_I 17440-66-6 1 Siim Cyanide_1I_I I_I INRI 1_1 :o'or Before: BROWN .o -,Dr After: BROWN :o nents : STONES Clarity Before: Clarity After: FORM I - IN Texture: MEDIUM Artifacts: YES 7/88 U.S. EPA - CLP 0 0 a 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I MBEG23 1 3b Name: ASSOCIATED LABORATORIES_ Contract: 68-D9-0079 a_ Code: ALI Case No.: 15486 , SAS No.: a pix (soil/water): SOIL SDG No.: MBEF92 Lab Sample ID: MBEG23 evel (low/med): LOW Date Received: 12/06/90 ;)lids: 87.4 Concentration Units (ug/L or mg/kg dry weight): MG/KG ICAS No. I Analyte IConcentrationlCl Q IM 17429-90-5 (Aluminum 1 I_I 43101_1 I_I IP 17440-36-0 1Antimony_1 6.61U1 -1 IP 17440-38-2 1Arsenic_1 3.71�1F_1 -1 17440-39-3 1Barium 1 52.21_ IP 17440-41-7 IBerylliuml 0.64IUI -1 1P_I 17440-43-3 1Cadmium I 1.11U1 IP 17440-70-2 (Calcium -1 13001_ �_IP_1 -1 17440-47-3 1Chromium 1 5.01_1 IP 17440-48-4 (Cobalt 1 2.51U1 -1 IP 17440-50-8 (Copper I 16.71_1T_IP_1 -1 17439-89-6 (Iron I 61201_1 1P_1 17439-92-1 I Lead 1 -- 317 I_ I 1 F_ I 17439-95-4 IMagnesiuml —S 5591BI IP 17439-96-5 IManganesel 69.71_1'ZE_IP_1 -1 17439-97-6 1 Merury_ rr, rcvt-- 17440-02-0 (Nickel -1 5.31U1 IP 17440-09-7 IPotassiuml 3161B1 -1 1P_1 17782-49-2 ISelenium 1 0.961E rM.+N_IF_l 17440-22-4 ISilver 1 1.91B1 IP 17440-23-5 (Sodium I 83.51BI -1 1P--1 17440-28-0 IThallium 1 0.60IUI IF_I 17440-62-2 IVanadium 1 9.31BI JP_I 17440-66-6 (Zinc I 1341_I_IP_1 I I I cyanide_ 1 I I 1_ 1 I_I I I I_I 7elor Before: BROWN Clarity Before: Texture: MEDIUM .c -or After: BROWN Clarity After: Artifacts: YES .c Bents: ROOTS - FORM I - IN 7/88 U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET ,ab Name: ASSOCIATED LABORATORIES Contract: 68-D9-0079 I MBEG24 Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 [,':rix (soil/water): SOIL- Lab Sample ID: MBEG24 .,evel (low/med) : LOW— 00025 Date Received: 12/06%90 s solids: 53.1 Concentration Units (ug/L or mg/kg dry weight): MG/KG I I I ICAS No. I Analyte 1ConcentrationlCl Q IM I 17429-90-5 1Aluminum ( 12700I_I IP_I 17440-36-0 (Antimony -1 9.9,1U1Ip_I 17440-38-2 1Arsenic-1 15.61_1 IF_1 17440-39-3 (Barium 1 6931_117IP_I 17440-41-7 lBerylliuml 1.71_1 IP_1 17440-43-§ ICadmium-1 8.51_1 IP 17440-70-2 (Calcium_( 51801_I' -1 Ip_1 17440-47-3 IChromium l 40.91_1 Ip_1 17440-48-4 (Cobalt I 17440-50-8 K opper i 30201B1'�—IP I 17439-89-6 lIron 1 152001_( _I p_ I 17439-92-1 [-Lead 14121_1_1F_1 17439-95-4 IMagnesiuml 11801B1 1P--117439-96-5 IManganesel 57.21_IME 1P I 17439-97-6 1Mercury_ I �' gai p�, ICVI 17440-02-0 INickel I -I 8.51B1 1p_I 17440-09-7 IPotassiuml 3471BI IP 17782-49-2 (Selenium l 9.11_1? SN_IF-1 -1 17440-22-4 (Silver 1 24.31_( Ip_I 17440-23-5 ISodium I 1631BI IP 17440-28-0 IThallium 1 1.11UI -1 IF_I 17440-62-2 IVanadium I 15.91B( 1p_l 17440-66-6 (Zinc l 10601-I-' Ip Cyanide_ i I_ I I I -1 I NRI I_I 101or Before: BROWN Clarity _ Before: Texture: MEDIUM :c --or After: BROWN Clarity After: Artifacts: YES 2c ments: ROOTS J FORM I - IN 7/88 U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I ah-Name:me: ASSOCIATED LABORATORIESMBEG25 _ Contract: 68-D9-0079 1 a. Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 (soil/water): SOIL Lab Sample ID: MBEG25 svel (low/med) : LOW 00026 Date Received: 12/06/90 )lids: 89.4 Concentration Units (ug/L or mg/kg dry weight): MG/KG I ICAS No. I I I I I Analyte IConcentrationlCI Q I IM I 17429-90-5 (Aluminum -1 oL_r Ip_�I 30801_1 17440-36-0 IAntimony_1 5.91U1 IP 17440-38-2 1Arsenic_1 6.81_" 1 -1 IF 17440-39-3 IBarium I _1 61.01_IIP_1 17440-41-7 IBerylliuml 0.591BI 1p_) 17440-43--3 ICadmium_1 0.951u1 IP 17440-70-2 ICalcium 1 -1 1500.I_Iif-Ip_I 17440-47-3 IChromium 1 6.61_1 IP 17440-48-4 (Cobalt 1 2.31U1 -I IP 17440-50-8 ICopper 1 -1 51.71_1�Ip_1 17439-89-6 (Iron 1 66401_1 IP 17439-92-1 ILead 1 24.51_1 -1 17439-95-4 IMagnesiuml 5091BI _ IP 17439-96-5 IManganesel 45.51_1E -I Ip_I 17439-97-6 1 17440-02-0 1Nickel _ 1 4.71UI Ip_1 17440-09-7 1Potassiuml 285IB1 Ip_I 17782-49-2 ISelenium I 0.591BT:LWN_IF_1 17440-22-4 (Silver 1 I I ip_I 17440-23-5 ISodium 1 -2.21_1_ 1111BI 1p_I 17440-28-0 (Thallium -1 0.631UI 1F_1 17440-62-2 IVanadium 1 7.81BI Ip_I 17440-66-6 IZinc I 215I_IT IP Cyanide_i 1_I -1 INRI I_I I_I olnr Before: BROWN Clarity Before: oL_r After: BROWN Clarity After: oz ents : TONES -AND -ROOTS e �. FORM I - IN I Texture: MEDIUM Artifacts: YES 7/88 U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET a' --Name: ASSOCIATED LABORATORIES Contract: 68-D9-0079 MBEG26 a.., Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 3 :ix (soil/water): SOIL- Lab Sample ID: MBEG26 spiel (low/med) : LOW_ 00027 Date Received: 12/06/90 )lids: 84.5 Concentration Units (ug/L or mg/kg dry weight): MG/KG ICAS No. 1 I Analyte IConcentrationlCI Q 1 IM 17429-90-5 1 (Aluminum l 10101_1 IP 17440-36-0 (Antimony_( 6.21U1 -1 IP 17440-38-2 IArsenic_I 0.761BI -1 1F_1 17440-39-3 (Barium. I 7.7181-1P_I 17440-41-7 1Beryll1um1 0.601U1 IP_I 17440-43--9 (Cadmium I 1.OIUI IP 17440-70-2 ICalcium_1 2471BI -1 IP_1 17440-47-3 (Chromium I 2.61_1 IP 17440748-4 (Cobalt 1 2.41U -1 IP 17440-50-8 (Copper -1 12.81_IIP_1 -1 17439-89-6 Ilron 1 15901_1 IP 17439-92-1 (Lead 1 13.21_1 -1 IF_1 17439-95-4 IMagnesiuml 2461BI IP_1 17439-96-5 IManganesel 20.9I_ILE IP_I 17439-97-6 IMercury_I 0.091UI ICV( 17440-02-0 INickel I 5.OIU1 IP 17440-09-7 IPotassiuml 225IBI -1 IP_I 17782-49-2 ISelenium 1 0.40IU1 IF_I 17440-22-4 ISilver I _N 1.41U1 IP_I 17440-23-5 ISodium I 1291BI IP 17440-28-0 IThallium 1 0.601U1 -1 IF_I 17440-62-2 IVanadium I 2.81BI IP_1 17440-66-6 1Z• , Ft i I i cyanide_ 1 I_ I I_I I NRI I_I :o- )r Before: BROWN Clarity Before: 'olor After: BROWN Clarity After: 'o nents : 20OTS FORM I - IN Texture: MEDIUM Artifacts: YES 7/88 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): MG/KG i ICAS No. I 1 I Analyte IconcentrationlCI Q I 1 EPA SAMPLE NO. 52801_1 INORGANIC ANALYSES DATA SHEET 7.21U1 IP �a.b Name: ASSOCIATED_LABORATORIES_ (Arsenic_( Contract: 68-D9-0079 1 MBEG27 Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 4 ;rix (soil/water): SOIL 17440-43-:§ Lab Sample ID: MBEG27 revel (low/med): LOW 0..'0078 Date Received: 12/06/90 solids: 80.7 Ip_I 17440-48-4 (Cobalt 1 Concentration Units (ug/L or mg/kg dry weight): MG/KG i ICAS No. I 1 I Analyte IconcentrationlCI Q I IM I 17429-90-5 I lAluminum 1 52801_1 Ip_1 17440-36-0 1Antimony_I 7.21U1 IP 17440-38-2 (Arsenic_( 8.51_1 -1 1F_I 17440-39-3 (Barium 1 10.71BI-7- IP 17440-41-7 1Berylliuml 0.691U1 -1 Ip_1 17440-43-:§ I Cadmium_( 1.2 U 17440-70-2 1Calcium 1 _ 1641Br�a7_IPa- 1 17440-47-3 1Chromium I 4.71_1 Ip_I 17440-48-4 (Cobalt 1 2.81U1 Ip_I 17440-50-8 (Copper 1 7.81_1 1p_I 17439-89-6 lIron I 78001_1 Ip_1 17439-92-1 (Lead 1•• 28.11_1 17439-95-4 IMagnesiuml 4601BI _ IP 17439-96-5 IManganesel 36.71_ 1 -1 Ip_I 17439-97-6 IMercury_1 0.101U1 1CV1 17440-02-0 (Nickel I 5.8 U 17440-09-7 1Potassiuml 208 BI _ Ip_1 17782-49-2 IS.elenium I 0.521UI'SIF_1 17440-22-4 ISilver 1 3.11_1 Ip_1 17440-23-5 (Sodium 1 105 B 17440-28-0 1Thallium 1 0.71JUj _ IF_1 17440-62-2 iVanadium 1 17.91_1 Ip_1 17440-66-6 1 I II I Cyanide_ I I I — I_I I_I _ (NRI I_I �c'or Before: BROWN :oj-or After: BROWN .c ments: ROOTS -AND -GRAVEL Clarity Before: Clarity After: Texture: MEDIUM Artifacts: YES FORM I - IN 7/88 U. S . - EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I MBEG28 1 gab Name: ASSOCIATED_LABORATORIES_ Contract: 68-D9-0079 I i Code: ALI Case No.: 15486 SAS No.: SDG No.: MBEF92 t:, -;rix (soil/water): WATER Lab Sample ID: MBEG28 ,evel (low/med) : LOW_ 00029 Date Received: 12/06/90 olids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L ' I ICAS No. I I Analyte IConcentrationlCI Q IM I 17429-90-5 1Aluminum_1 .3.6.01U1 IP_I 17440-36-0 1Antimony_1 31.01U1 Ip_I 17440-38-2 1Arsenic_1 2.OIU1 IF_I 17440-39-3 (Barium 1 2.11B) IP 17440-41-7 1Bery1l17umI 3.OIU1 -1 Ip_l 17440-43-9 ICadmium 1 5.OIU1 Ip_I 17440-70-2 1Calcium_1 232 B 17440-47-3 (Chromium l _E 6.OIUl=* _IP 17440-48-4 (Cobalt 1 12.01U1 -1 Ip_I 17440-50-8 (Copper -1 4.51B IP 17439-89-6 (Iron I 45.21B -1 Ip_I 17439-92-1 (Lead I.. 8.9 N I F-1 17439-95-4 IMagnesiuml _U 66.41BI IP 17439-96-5 1Manganesel 1.01UI -1 IP 17439-97-6 IMercury_I 0.201_1 -1 1CV1 17440-02-0 (Nickel I 25.01UI Ip_I 17440-09-7 IPotassiuml 3501U1 Ip I 17782-49-2 17440-22-4 ISilver Ir 7.01U1 17440-23-5 ISodium 1 461 B 17440-28-0 1Thalli1 um 3.01U MN jF_j 17440-62-2 (Vanadium l 4.OIU1 IP 17440-66-6 1Zinc I 12.6 I -1 Ip_I Cyanide_ i IIB_ I I_1 I NRi 1_I :olor Before: COLORLESS 2c --or After: COLORLESS % ments: Clarity Before: CLEAR Texture: Clarity After: CLEAR Artifacts: FORM I - IN 7/88 U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET ab Name: ASSOCIATED LABORATORIES .a Code: ALI Case No.: 15486 a'rix (soil/water): WATER I Contract: 68-D9-0079 MBEG29 SAS No.: SDG No.: MBEF92 Lab Sample ID: MBEG29 ,evel (low/med): LOW 00030 Date Received: 12/06/90 lids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L_ ICAS No. I I Analyte IConcentrationlCl Q I IM I 17429-90-5 I IAluminum_1 1-111 36.OIUI' IP 17440-36-0 IAntimony_1 31.0IU1 -1 IP 17440-38-2 IArsenic_1 2.0IU1 -1 IF_1 17440-39-3 (Barium 1 4.11BI Ip_1 17440-41-7 IBerylliuml 3.0IU1 iP_I 17440-43--5 I Cadmium_( 5.01U1 IP -1 17440-70-2 I Calcium_1 378 I BI'E—I P_I 17440-47-3 IChromium I 6.01UI IP_I: 17440-48-4 (Cobalt 1 12.0IU1 IP 17440-50-8 (Copper I - 4.31BI -1 IP 1 7439-89-6 I Iron 1 61.5 1 B'I-;' N -1 I P_ I 17439-92-1 I Lead 1 2.8 1 B I YN gni I F_ 1 17439-95-4 IMagnesiuml 1251B1 IP 17439-96-5 IManganesel 1.0IU1 -1 1P_1 17439-97-6 IMercury_1 0.201U1 ICV( 17440-02-0 INickel I 25.OIU1 1P_1 17440-09-7 IPotassiuml 5901B1 IP_1 17782-49-2 _ -`. 17440-22-4 (Silver I 7.0IU1 p 17440-23-5 ISodium I 8711B1 IP 17440-28-0 1Thal 1ium l 3.01UI N -1 IF_1 17440-62-2 (Vanadium I 4.OIU1 1P_1 17440-66-6 (Zinc 1 36.71_1 IP_I Cyanide_i 1_1 —1-1 —1-1 INRI :01or Before: COLORLESS Clarity Before: CLEAR Texture: .-or After: COLORLESS Clarity After: CLEAR Artifacts: :o nents : FORM I - IN 7/88 U.S. EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I ab Name: ASSOCIATED LABORATORIESMBEG30 _ Contract: 68-D9-0079 .a Code: ALI Case No.: 15486 SAS.No.: SDG No.: MBEF92 :aLrix (soil/water): WATER Lab Sample ID: MBEG30 revel (low/med) : LOW_ 00031 Date Received: 12/06/90 olids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L_ I ICAS No. I I i I Analyte IConcentrationlCI Q I IM 17429-90-5 I IAluminum_I 36.0IUI IP_1 17440-36-0 IAntimony_I 31.OIUI IP_1 17440-38-2 (Arsenic_( 2.0IU1 IF_I 17440-39-3 (Barium 1 2.71B1 IP_I 17440-41-7 IBerylliuml 3.0IU1 IP_1 17440-43-q I,Cadmium I 5.0IUI Ip_l 17440-70-2 ICalcium_1 213 B E 17440-47-3 1Chromium I _ 6.01UI�-IP_IZ- 17440-48-4 (Cobalt 1 12.0IUI 1p_I 17440-50-8 ICopper I 4.0IBI IP_1 17439-89-6 (Iron I 44.41B13 N 1P--1 17439-92-1 (Lead -1 2.0 U _N 17439-95-4 IMagnesiuml 39.21BI Ip 1 17439-96-5 IManganesel 1.0IUI 1P_I 17439-97-6 IMercury_1 0.201_1 1cv1 17440-02-0 INickel 1 25.0IU1 IP_I 17440-09-7 IPotassiuml 3501U1 Ip_I_ 17782-49-2 1ST 7f t 1 1 17440-22-4 _ ISilver I 7.OIUI IP 17440-23-5 ISodium I 339 U -1 17440-28-0 1Thallium_1 3.01U Z- 17440-62-2 I'Vanadium 1 -4.0IUI Ip_1 17440-66-6 (Zinc I16.6 I B I IP- Cyanide_ i I I_ I I_I I NR I I_I '010r Before: COLORLESS Clarity Before: CLEAR ,a -Dr After: COLORLESS* Clarity After: CLEAR 'o vents: FORM I - IN Texture: Artifacts: 7/88 U.S: EPA - CLP 1 EPA SAMPLE NO. INORGANIC ANALYSES DATA SHEET I I I MBEG31 ne: ASSOCIATED_LABORATORIES_ Contract: 68-D9-0079 l 3 ALI Case No.: 15486 SAS No.: SDG No.: MBEG31 -(soil/water): WATER Lab Sample ID: MBEG31 00009 Date Received: 12/06/90 (, ow/med) : LOW_ _0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L_ I I I Q I I IM I ICAS No. I Analyte .lConcentrationiCl 11 1-1 1 1 1 .1_17429-90-5•IAluminum I 55.7IBI 31.01U1 IP_I IP_I 7440-36-0 17440-38-2 IAntimony_1 IArsenic_1 2.01'UI IF_I 17440-39-3 17440-41-7 (Barium I lBerylliuml 2.01U1 3.01UI IP.I IP -I 17440-43-9 ICadmium_I 01UI 2 701BI IP_1 IP 7440-70-2 17440-47-3 1Calcium 1 IChromium 1 6.OIUI -1 IP -I IP_I 17440-48-4 (Cobalt I 12.01UI 4.01UI IP 17440-50-8 (Copper I -1 17439-89-6--1 on_, 2,0IUI IF 17439-92-1 17439-95-4 ILead 1 IMagnesiuml 1B1 12812SIBI -1 IP -1 IP_1 17439-96-5 IManganesel 0.201UI N Ip 1 17439-97-6 17440-02-0 1Mercury_I (Nickel I 25.01UI I 1 IP 17440-09-7 17782-49-2 1Potassiuml lSelenium I 1BI -1 461 4611U IF -1 ,17440-22-4 (Silver -1 7.OlU�N 342 2 1ST Ip_I IF 17440-28-0 ISodium I I Thallium I 1BI 3 17440-23-5 I IP -1 17440-62-2 (Vanadium l 4.01 U I 17440-66-6 — I_I_ 1 NRI ll�°I I ICyanide I 1— I or Before: COLORLESS Clarity Before: CLEAR_ Texture: .o: After: COLORLESS Clarity After: CLEAR_ Artifacts ments : FORM I - IN 7/88' NUS CORPORA TION SUPERFUND DIVISION PROJECT NOTES TO. /T%!n J F :r-' I . DATE: ar i u ! &)FCOPIES: SUBJECT: GAIr�/ATiony� 1�n�.%Ton iZPSi�a`�a (iii-r!J ;v �ZW �T dP s;Te. REFERENCE: n n1 42"�' !�_s,'rOP ��r c N,'nJ ADD 1'7 n f TN -!�i Te - NUS "3A 58 1182 �3PuESZ SENT REPORT ON THE OCCURRENCE AND MOVEMENT OF AGRICULTURAL CHEMICALS IN GROUNDWATER. - NORTH FORK OF SUFFOLK COUNTY �R CWT oa.Reourr w ow"m swear SUFFOLK COUNTY DEPARTMENT OF HEALTH SERVICES DAVID HARRIS, M.D., M.P.H. COMMISSIONER ALDO ANDREOLI, P.E. DIRECTOR, DIVISION OF ENVIRONMENTAL HEALTH PREPARED BY: BUREAU OF WATER RESOURCES JOSEPH H. BALER, P.E., CHIEF SY F. ROBBINS, HYDROGEOLOGIST AUGUST, 1982 II. Introduction The residents of Suffolk County's North Fork rely solely on groundwater for their supply of drinking water (Figure 2-1). In recent years there has been increasing concern about the contamination of this resource by agricultural chemicals (fer- tilizers, insecticides, herbicides, fungicides). This concern has led to the establishment of an observation well network by SCDHS to obtain general water quality data, and a massive sampling program by SCDHS and Union Carbide to identify com- munity and private wells contaminated with the pesticide aldicarb. The NYSDOH and SCDHS entered into a contractual agreement in April, 1981 to obtain detailed water quality information at selected locations on the East End, including three on the North Fork (Figure 2-1). The objective was to more precisely identify the overall horizontal and vertical distribution of aldicarb, nitrate, and dichloropropane, and to assess the hydro - geologic processes that control groundwater movement and may affect the quality of the groundwater resource in the future. This report presents the data collected on the North Fork of Suffolk County by the SCDHS under the NYSDOH contract which, along with data from previous studies and ongoing monitoring programs, are used to evaluate the general hydrogeologic and water quality situation. Groundwater management implications are then assessed. - 4 - IV. Hydrageolo y A. HYDROGEOLOGY - GENERAL A number of reports have previously been published that describe the geology of the North Fork and its relationship to water resources (Woodward -Clyde Consultants, 1977; H2M Corp., 1978; H2M Corp., 1970; Crandall, 1963). They describe the sequence of stratigraphic units on the North Fork, which is similar to that found on the main body of Long Island (Table 4-1). A longitudinal cross section of the North Fork was de- veloped during the present study using well logs of test holes drilled during previous studies (e.g., H2M Corp., 1970) and geologic interpretations provided by the U.S. Geological. Survey. The contact between upper glacial aquifer and Magothy aquifer deposits was found to vary in depth from about -200 to -430 feet MSL (Figure 4-1). Although a thick clay layer was found at a depth of -65 to -85 feet MSL in each of the test holes, it does not appear to form the contact between the two aquifers, as the Gardiners clay does on the south shore of the main body of Long Island. It is not certain whether the clays encountered are all part of a continuous layer that underlies the entire North Fork, or whether they occur as isolated lenses. Fresh groundwater under the North Fork is believed to exist as a series of four separate, irregularly shaped lenses (Figure 4-1). The position of the freshwater -saltwater inter- face, however, has only been measured in a few places (Figure 4-1).: - 22 -t TABLE 4-1 MAJOR HYDROGEOLOGIC UNITS: NORTH FORK* Nydrogeologic Unit Geologic Name Upper Glacial Aquifer Holocene and upper Pleistocene deposits, and Mannetto Gravel Magothy Aquifer Matawan Group-Magothy Formation, undifferentiated (Foot -Raritan, upper Cretaceous) Raritan Clay Clay member of the Raritan Formation (upper Cretaceous) Lloyd Aquifer Lloyd Sand Member of the Raritan Formation (upper Cretaceous) Bedrock Undifferentiated crystalline rocks (Precambrian?) Daucription and Mater-Bearinq Character Mainly brown and gray sand and gravel of moderate to high hydraulic conductivity; also includes deposits of clayey glacial till and lacustrine clay of low hydraulic conductivity. A major aquifer. Gray and white fine to coarse send of moderate hydraulic conductivity. Generally contains sand and gravel beds of low to high hydraulic conductLvity in basal 100 to 200 feet. Contains much interstitial clay and silt, and beds and lenses of clay, of low hydraulic conductivity. Gray, black, and multicolored clay and some milt, fine sand, and sand and gravel lenses. Unit has low hydraulic conductivity and tends to confine water in underlying aquifer. White and gray fine -to -coarse sand and gravel of moderate hydraulic conductivity and some clayey beds of low hydrau- lic conductivity. Not highly developed as An aquifer. Mainly metamorphic rocks of low hydraulic conductivity; surface generally weathered; considered to be the bottom of the groundwater reservoir. Not a source of water in Suffolk County. 'Modified froms Woodward -Clyde Consultants, 1977, Table 1. LEVEL FRESH GROUND WAVED I FRESH GROUND WATER / fRES GROUND WATERFRESH GROW/ W►TER loo / _ _ SALTY GROttaO WATER -loo I CHLORIDE > 250 MS /I I ' // U. G. 200 . mo / \ M.g • -2x0 M.g. / •250 -300 / SALTY GROUND WAFER .300 I CHLORIDES) 290 .t/11 11�g. 0 !SO Solid gray or brow clay. • e00 Y.G. Ypper Glacial Aquifer. U.f._, Sar. Rnr. .400 U.G. MEG. Ihgothy Aquifer. Meg. -110 4Par. .4SOc. Sarlca0 Aquifer. l.yd. Lyd. Lloyd Aquifer. - Opp . >Da a Map thl deposits completely graded away. Bar. -330 later All formation contact depths are approximate. Lyd. -ass 10.19100 of the top 09 the rasa 0f diffusion. (chloride contest In excess _gaao0p of ISO mg/1) as detormload by analysts of pogo water centrifuged from Ilnyd Care samples. hrdrnrk -650 _ fositloa of frgahwateg/ealrwmtec Interface as computed from Ghyben-Uerrberg Loyd -650 prisclple using water levels In cast wells. Sedgack .100 Estimated position of the gap of the some of diffusion in areas where notoo cost well data are available. ' Sass map. Interface Use. and Ghybeo-largbsrg lime from UZM(1910). Kato 0o walls S-1707717. S -7279M. and S-1111517 gram Jensen and Soren (1971) aad SCMS file•. 1010 os walla "I'D and 3-169 from Julian Sores (personal co®. 4/S/82), 5111 map FIG. 4-1 GEOLOGIC CROSS SECTION AND SALT -WATER INTERFACE: NORTH FORK vertical exaggeration 100x. r .loosR,d .goo ey 9 a .-A "� � DEAN SEA •.rte wu Y , i LEVEL FRESH GROUND WAVED I FRESH GROUND WATER / fRES GROUND WATERFRESH GROW/ W►TER loo / _ _ SALTY GROttaO WATER -loo I CHLORIDE > 250 MS /I I ' // U. G. 200 . mo / \ M.g • -2x0 M.g. / •250 -300 / SALTY GROUND WAFER .300 I CHLORIDES) 290 .t/11 11�g. 0 !SO Solid gray or brow clay. • e00 Y.G. Ypper Glacial Aquifer. U.f._, Sar. Rnr. .400 U.G. MEG. Ihgothy Aquifer. Meg. -110 4Par. .4SOc. Sarlca0 Aquifer. l.yd. Lyd. Lloyd Aquifer. - Opp . >Da a Map thl deposits completely graded away. Bar. -330 later All formation contact depths are approximate. Lyd. -ass 10.19100 of the top 09 the rasa 0f diffusion. (chloride contest In excess _gaao0p of ISO mg/1) as detormload by analysts of pogo water centrifuged from Ilnyd Care samples. hrdrnrk -650 _ fositloa of frgahwateg/ealrwmtec Interface as computed from Ghyben-Uerrberg Loyd -650 prisclple using water levels In cast wells. Sedgack .100 Estimated position of the gap of the some of diffusion in areas where notoo cost well data are available. ' Sass map. Interface Use. and Ghybeo-largbsrg lime from UZM(1910). Kato 0o walls S-1707717. S -7279M. and S-1111517 gram Jensen and Soren (1971) aad SCMS file•. 1010 os walla "I'D and 3-169 from Julian Sores (personal co®. 4/S/82), 5111 map FIG. 4-1 GEOLOGIC CROSS SECTION AND SALT -WATER INTERFACE: NORTH FORK Those measurements that are available indicate that the depth of the interface is somewhat greater than would be predicted by the Ghyben-Herzberg relation, which states that the -inter- face will be located 40 feet below sea level for each foot of elevation of the water table above sea level (Figure 4-1). B. HYDROGEOLOGY - NORTH FORK TRANSECT Three geologic test holes were drilled for the NYSDOH study along a northwest -southeast transect (Depot Lane) that crosses the North Fork at Cutchogue, Town of Southold (wells S-71044, S-71170, and S-71279; Figure 4-2).3 Driller's logs and core samples from these wells indicate a highly permeable sand and gravel formation that extends from land surface to a depth of about -120 feet MSL (Figure 4-3). Beneath these porous glacial deposits lies a clay layer that varies in thick- ness from about 85 feet near the center of the fork, to about 200 feet, and possibly more, under the northern and southern portions of the transect. Another sand and gravel layer, of unknown thickness, underlies the clay layer at the center of the fork (see well S-71170; Figure 4-3). The stratigraphic sequences of other test holes near the center of the fork show a similar layering of clay and sand beds (see wells S-68831 and S-32390, Figures 4-2 and 4-4).4 The upper surface of the 3. The mud rotary method was used; a drag bit with an open center was employed to facilitate the collection of core samples with a split -barrel corer., 4. The apparent local dip of the beds, including the top surface of the uppermost clay layer, is toward Depot Lane (see Figure 4-4 and Appendix F). 25 - Ouck Pond %W Point sue Sound 471044 • . _ .i .068831E;st Utchogue. A g,e 71170 /`?/onjve •'eat Sacred Heart Cam • V 32390 ho Z.: H 0 L C., 0 71279 Cutchogup.:./ 0 am 32 le 0 JO oQ %S "Gra fork a covollfv club Marsh jp Pt aLITTLE P • cutekogue 2 North Foris Coun- ry Ciub New \> ';UffQLk ld Cove 5 am 3 Pt Point FIG. 4-2 GEOLOGIC TEST HOLE LOCATIONS: NORTH FORK TRANSECT - 26 - of, IF m LJ 0 Cl rn 0 r 0 v n M 0 N N N m c -j --1 0 Z z 0 7o --1 x m 0 7c b Z N m n '-1 v n ' Z n m_ O 3 Z 0 x i N x 0 m 0 CD m F i G ELEVATION (FT) 50 MSL -50 UL Z O -100 _ W J W -150. -200 -250 -3 ALVABs LA. S-32390 SAND, coarse brown, w—gravel SAND, fine to medium brown, with grit SUMP (DEPOT LA.) S-71170 CLAY, solid grafi- CLAY, gray, with coarse sand and gravel 'SAND, coarse brown, wwl g gravel CLAT.. 8o1id gray layi)1V o!•,poarse, solid c%qy 1. SAND:•jine to NgditsL coarse,'uk" gri�.and�. lump clay ` SAND, coarse brown, ww__ grit and gravel LPLNDFILL S -6B®31 coarse brown, 1 ..grit and much grrfel CLAY, brownish gray san y, hard, with some gravel SAND, coarse brown, w1tF grit and gravel, and acme clay No horizontal scala. FIG. 4-4 GEOLOGIC CROSS SECTION: NORTH FORK TRANSECT AREA - 28 - ":O s� SAND, coarse brown, d wit grit and gravel oa, o� ,Q p SAND, fine to medius c brown, with grit and small gravel SAND, layers of fine D0 brown and brown silt_, with gravel SAND, fine to coarse mown, with grit and =� SAND, Fina to coarse brown gravel :.SAND, fine brown i 'J = CLAY, solid and silty brownish gray CLAY, solid brownish gray ' x! SAND, very fine to ane brownish gray, with some clay, mica MAY, very fine brown W-.. 'may and soli¢' CLAY, solid brown •' SAND, fine to coarse %p a._ grown, with grit, gravel, some clay coarse brown, 1 ..grit and much grrfel CLAY, brownish gray san y, hard, with some gravel SAND, coarse brown, w1tF grit and gravel, and acme clay No horizontal scala. FIG. 4-4 GEOLOGIC CROSS SECTION: NORTH FORK TRANSECT AREA - 28 - clay layer in each of these test holes is found at an elevation similar to that found throughout the region (compare Figures 4-1, 4-3, and 4-4). Pore waters from core samples from the northern and southern transect wells were analyzed for chloride; the results indicated that the freshwater -saltwater interface occurs at about -270 feet and -280 feet MSL, respectively (Figure 4-3). These depths are much greater than would be predicted by the Ghyben-Herzberg relation, and are probably due to the osmotic effects of the low permeability clay.5 Cores from the center well (S-71170) were not analyzed, but earlier tests from a nearby well (5-32390) showed the interface to be at about -290 feet MSL (Figures 4-2 through 4-4).6 Thus, there may be some fresh water below the clay layer (below -228 feet MSL) at well 5-71170, but the quantities would be extremely limited (if any) and any attempts to pump this water would probably cause up - coning of salt water from below as it did during tests at well 5-32390.7 C. HYDROGEOLOGY - CUTCHOGUE AND MATTITUCK HOT SPOTS The deepest wells drilled at the Cutchogue and Mattituck hot spots reached a depth of about -50 to -60 feet MSL.8 5. Although clay is very, porous and holds a large volume of water, its low permeability makes this water unavailable for water supply purposes. 6. H2M, 1970, Vol. II, p. 269. 7. Ibid. 8. These wells were drilled with a hollow -stem auger. - 29 :`ar. The driller°s logs for these wells indicated that the shallow subsurface geology consists almost entirely of sands deposited as glacial outwash; a few thin (-1 foot thick) clay lenses were also encountered just below the surface. No major confining beds or other significant hydrogeologic features were discovered. The freshwater -saltwater interface was found right at the shore- line in both areas. - 30 - wy� V. Groundwater Hydrology A. GROUNDWATER HYDROLOGY - GENERAL The direction of groundwater flow on the North Fork can be determined from maps of the water table (Figure 5-1). Ground- water elevations are highest near the center of the fork (-4 ft.) and lowest near the shorelihe. Flow is perpendicular to the water -table elevation contour lines, moving outward from a cen- tral groundwater divide toward either shoreline (Figure 5-1). The rate of flow depends on the magnitude of the hydraulic gradient (slope of the water table) and on the hydraulic con- ductivity (permeability) of the material. B. GROUNDWATER HYDROLOGY - NORTH FORK TRANSECT Water -table elevations were measured at transect wells during the five months October, 1981 to February, 1982 (see Appendix D, Figure D-4). Water levels of 4-5 feet MSL were found along the central groundwater divide. On either side of the divide the water table slopes gently seaward; within 1,000 feet of the shoreline the water table starts to slope more steeply, dropping from about 2 feet MSL to sea level it- self right at the shoreline (Figure 5-2). Temporally, the water levels increased from October to February, with the greatest increases near the divide (-2 feet) and the smallest increases near the shorelines (-h foot). - 31 - rJY From: SCDHS Bureau of Water Resources •NJr pl(i!/ 6 •mow • ! \ 'w d r .� i •J.N � OJMJJ • OwJ \ fA 6"Air NCONN: Mt r,CONIC 1V9O \ �r•/ ................ of �N. •J.JN Water table 'contours for March 1981. Datum is Mean Sea Level. Groundwater divide. FIG. 5-1 WATER TABLE AND GROUNDWATER FLOW DIRECTIONS: NORTH FORK FIG. 5-2 GROUNDWATER FLOW PATTERN: NORTH FORK TRANSECT 110 GREGOM .0 RT. 37 LIRA RT. is 10 N N VV NO AS 60 Je.% .I Nw wa M .A N N N A A �qq0 A A 1/ A A d d �S .. Curc.00u. A OARIOR ad 20 . L.S.S.WICKMAN 2.10' 2.02' .2 96, ]. ' 3. air, 7.)0' R7 2.K' 1.6411 CR.. MiC.FLSST1 *2L 1 do,1• 1 .��I• 1-4�1 •1,0.61` S� � • I 1.0 / I 1 � � 1.0 1 O l.. 0 2.0 1 1 • 17.1) / 1 .2 M-1 1 !.0 ]./ 1.0 (].1) 3.6 3.0 w 11 \ 1 1 1 1/ / 1 1 �( .] .21 -10 _111 .AL! lal.s IRltdl.. .11 1 • ` ®_t_L__ • 1 1 1 : •170 it Average Velocities (Lt/day) Por the CLAY .Oubl"ay � I Period 10/81-2/02. i M .ALT uATsa Hots -110 0 Read Measurement Point ($)-Shallow well -- .quipoteatial Line (Lt) (o) -Map Mall •160 ] 1 ] 7 1 1 10 11 li •1] 11 J5 11 i1 11 11 is DISTANCE FROM NORTH SHORE (1000 FT) FIG. 5-2 GROUNDWATER FLOW PATTERN: NORTH FORK TRANSECT Subsurface flow patterns for the transect were determined using five-month average water -level values for each shallow and deep well (Figure 5-2). Near the central groundwater divide, flow was found to be vertical, with velocities of approximately 0.1 ft/day.9 The major portion of the transect was found to be dominated by horizontal flow, with calculated velocities on the order of .2 to .4 ft/day; some downward recharge also occurs in these areas. Within 1/4 mile of the shorelines, the vertical component of flow is upward as groundwater is influenced by the boundary effects of the saltwater interface and is discharged via seepage and underflow to surface waters. The above results imply that water percolating through the soil and reaching the water table near the center of the fork will take 100 years or more to complete its movement through the aquifer before being discharged to surface waters. Water recharged to areas with shallow, horizontal flow will have residence times ranging up to about 30 years (see Appendix D). C. GROUNDWATER HYDROLOGY - CUTCHOGUE AND MATTITUCR HOT SPOTS The direction of groundwater flow in the area of the Cutchogue hot spot'is determined by the slope of the water table, which generally follows the slope of the land surface down toward East Creek (Figure 5-3). Because of the sharp drop-off of the water table in this area, horizontal flow 9. See Appendix D for a discussion of the groundwater velocity calculations. - 34 - APPENDIX F DISCUSSION OF CHLORIDE DATA: NORTH FORK TRANSECT Figure 5-2 (reproduced as Figure F-1) shows that the freshwater -saltwater interface along the north shore above the clay is a sharp boundary; chloride levels increase from 42 to 540 ppm in just 10 feet, and then increase to 18,000 ppm in another 10 feet. The interface above the clay appears to closely follow the Ghyben-Herzberg relation; the water level in well 5-71286 is about 2.1 feet MSL (Figure D-1), while the interface is found approximately 40 times as deep (-85 feet MSL). The position of the -interface on the south (Cutchogue Harbor) is inferred from data for well S-71276. The chloride (and nitrate) values at well S-71171 appear to be close to natural background levels, except at the level just above the clay layer (see Figures F-1 and 7-2). This well is located at a recharge basin that drains County Route 27 (Middle Road) and receives runoff from agricultural fields (primarily during early spring, when the ground is frozen). Since the basin is located at the top of the groundwater di- vide, flow is essentially vertical, and the well is probably sampling only recharged runoff, which appears to be of better quality when compared to water that leaches through active farm fields. Data for well S-71171 should not be interpreted as implying that the central portion of the fork has escaped the impacts of agricultural chemicals. N F-1 to as 6a 44 as x5L DISTANCE FROM NORTH SHORE (1000 FT) FIG. F-1 CHLORIDE CONCENTRATIONS: NORTH FORK TRANSECT The anomalous chloride (and nitrate) values for well S-71171 just above the clay layer may indicate the presence of a leachate plume originating at the Southold Town landfill lo- cated 2,000 feet to the north (see Figure 3-4). Previous drill- ing at the landfill has indicated that the clay layer is at a higher elevation than at the sump (see Figure 4-4). Landfill leachate, which is denser than surrounding waters, may be travelling down the slope of the clay layer, even though this direction is somewhat against the regional gradient of ground- water flow. This hypothesis is supported by sampling results for wells downgradient of the landfill, which have not shown leachate contamination. F-3 SUFFOLK COUNTY COMPREHENSIVE WATER RESOURCES MANAGEMENT PLAN VOLUME 1 MICHAEL A. LOGRANDE COUNTY EXECUTIVE DAVID HARRIS, M.D., M.P.H. COMMISSIONER ALDO ANDREOLI, P.E. DIRECTOR OF ENVIRONMENTAL QUALITY PREPARED BY: DIVISION OF ENVIRONMENTAL HEALTH, SCDHS DVIRKA & BARTILUCCI, CONSULTING ENGINEERS MALCOLM PIRNIE, INC. JANUARY 1987 5.0 GROUNDWATER RESOURCES This chapter describes the geology, hydrology, and hydro- ^eology of Suffolk -County. The chapter begins with an overview f Suffolk's geology -- from bedrock to land surface. This is followed by an updated summary of data on the components of the ydrologic water budget equation that balances inputs to and _discharges from the groundwater system. These components in- lude precipitation, evapotranspiration, direct runoff, stream -.Daseflow, and underflow. A separate discussion of recharge is lso presented. The chapter then describes Suffolk's hydro- 7eology -- its aquifer system, water table, saltwater inter - Face, and groundwater flow patterns and rates. Groundwater models used to predict the impacts of pumping ,'and sewering on groundwater levels and streamflows are de- cribed next. The chapter concludes with a discussion of groundwater quantity management concepts, such as safe yield, end saltwater upconing due to pumping. Most of the data pre- sented in 'this chapter were provided by the Syosset office of .he U.S. Geological Survey. 5.1 Geology The size and availability of Suffolk County's groundwater !resource is dependent to a large degree on its geologic forma- tions, which consist of thick deposits of unconsolidated, water- -.bearing sediments resting upon a relatively impermeable, crys- talline bedrock surface. The sequence of events that shaped „Suffolk County's geology is not known with certainty, but they probably began with the formation of the original basement rocks in early Paleozoic to Precambrian (?) time more than 400 million years ago. These were heated and compressed (metamor- phosed) by folding and faulting to produce a rugged, mountain- ous topography. During the subsequent period ending with the Late Cretaceous Epoch 100 million years ago, erosion reduced :.the land to a nearly planar surface that gently tilted to the southeast. 5-1 During the Late Cretaceous Epoch (60-100 million years ago) , streams brought sediments from the north and west to the Long Island area on the continental margin, forming a permeable sand layer (Lloyd Sand Member of the Raritan Formation) and overlying clay layer (clay member of the Raritan Formation)i9 upon the bedrock surface. After a short period of erosion or non -deposition, thick, permeable beds of river -delta clay,.A sand, and gravel were deposited on the Raritan Formation; these' deposits comprise the Magothy aquifer. Toward the close of;,"; late Cretaceous time (approximately 60 million years ago), a; sand and clay unit (Monmouth Group) of low permeability was,: deposited in shallow marine waters in the area that now consti-� tutes Suffolk's south shore. A long period of non -deposition, or possibly deposition-= followed by erosion, occurred after Cretaceous time. Geologic :r activities during this time left few sedimentary traces, but- streams flowing across Long Island cut some deep valleys intoy the Magothy. It was not until late Pleistocene (Wisconsinan)iyT glaciation -- some 20-200 thousand years ago -- that there were any significant additions to Long Island's geologic record.." Valleys were filled, and the older deposits were almost com=�":, pletely buried by glacial deposits. F Prior to the southward movement of the Pleistocene ice<; sheets to Long Island, an extensive clay unit (Gardiners Clay).. was deposited in shallow marine and brackish waters along the., shores of what is now Suffolk County. This unit rested upon" { the Magothy and Monmouth Group, and*acted as a confining layer:;;• The northern portions of the Gardiners Clay were subsequently`; eroded by advancing .ice and glacial meltwaters, and Gardiners:' Clay beds are now found only in the south shore area. The Pleistocene glaciation created the hilly Ronkonkoma moraine along. Suffolk's "spine" and South Fork, and the Harbor. Hill moraine along the North Shore and North Fork (Figure 5-1):, Erosion of these morainal deposits (as the glacier melted away,.; from Long Island) created. extensive outwash plains of sand ands" 5-2 Ln I W A' B' I C' 5 1_5 10--, 1 20 25 MILES 5 0 5 10 15 20 25 KILOMETERS M EXPLANATION ® Harbor Hill Moraine Ronkonkoma Moraine --A lGeohydrologic sections 'Geology adapted from Fuller(1914); Crandell (1962); Lubke (1964); Pluhovski and Kantrowitz(1964); Soren (1971); Krulikas and Koszalka (1982); Soren (1984). Figure 5-1 .SUFFOLK COUNTY GLACIAL` MORAINES AND CROSS SECTION KEY gravel in the intermorainal area and south to the Atlantic Ocean. These highly permeable deposits comprise the upper glacial aquifer and represent the majority of Suffolk's sur - ficial sediments. Some local confining clay units (e.g., the Smithtown clay) were also formed from glacial materials in :> intermorainal lakes and tidal lagoons. Since the end of glaciation about 12,000 years ago, Holocene beach and marsh deposits have been formed along the marine edge, and, within stream corridors and ponds. ;n u The sequence of stratigraphic units below Suffolk County is presented in Table 5-1 and can be summarized, in ascending order, as follows: o Early Paleozoic to Precambrian (?) Bedrock: impermeable, crystalline basement rock more than 400 million years old. o Late Cretaceous Deposits: deltaic clays, sands, and gravels; deposited by streams along the continental margin or as mar ine sediments comprising the Lloyd Sand (aquifer), Raritan; clay (confining unit), Magothy Formation (aquifer), and Mon mouth Group (confining unit); (60-100 million years old). o Pleistocene (Wisconsinan) Deposits: marine clays and various•; glacial materials (till, outwash sand and gravel, inter-'. morainal clay) comprising the Gardiners Clay, upper glacial (aquifer), and Smithtown clay (20-200 thousand years old). o Holocene Deposits: recent beach and marsh deposits less than'.;; .a .12 thousand years old. Several geologic cross sections through Suffolk County are, presented in Figures 5-2 through 5-6 (see key Figure 5-1). These figures are included to illustrate the areal extent and thickness of the various hydrogeologic units corresponding to, the geologic units listed in Table 5-1. A detailed description of each of the geologic units is presented in the following subsections. 5-4 WRMY '!'able :.)--L SUFFOLK COUNTY STRATIGRAPHY AND HYDROGEOLOGIC UNITS ne;f`it) Geologic Description System Series Geologic unit Hydrogeologic unit — Sand. grovel, clay, silt, organic mud, peat, loan, and.hello. — — lJLZ::IIt Colors; gray, brown, green, black, and yellow. Accent Recent shore, beach, 0-60 sr clflclal-fill deposit, of gravel, ..ad, clay, sad rubbish. Holocene and salt -marsh deposits 12,000 yrs Upper gla Bial Till compo,ed of clay, sand, gravel and boulder.; fora, Harbor eel Ronkonkoma termla.l mo rain::. Ovtw uh deposit. e, and grave 1. Moraine deposits aquifer :ad coast t of quarts .and. It.. to vary co. n (Salthtowr pebble to boulder a ked. Clealolacu.trl ae de pa.lts Gla ciollu vial deposits 0-700 cI.,) can, let of silt. clay, +ad some ■a^d and gr. vel l•f•re. Colors .re ethic gray. brwn, and yellow. Confabs •hell+ Smithtown clay (informal .ad plant rem.las g,^arallY In finer grola.d beds. usage) Quaternary Unconformity Marine deposit. of C14Y and silt with some t^terbedded sand end gravel. Color. gree nlsh -g ny and grey. ►otu lnlfera Pleistocene and llgn lie preseet, and aLo locally gleuconl[a. Gardiners Clay Gardiners Clay o -)s Unconformity Sand, (in. to coarse. Calor is brown. Identified so a distinct unit only on South fork to date. , post -Cretaceous(?). Upper glacial 0-140 In deposits aquifer Ln 200,000 yrs Unconformity Interbedded narine de po+lis of clay, silt, and end. calor, 60 mil yrs d. rt gree nleh-gr.y to black. Canisins auto g'I.uconl a and Monmouth lignite. o-:oo Monmouth Group greensand Unconformity Sond, fine [o eo. roes clayey In part; lnterb added with leases •ad l.y,rs o[ light- to dark -grey clay. 581.1 100-200 feat beds. Send Magolhy Formation — oth Mag y 0-1000 is generally composed of coarse send and gravel end gravel are quartaose. Lignite and pyrite are c—n. Upper Matawan Group aquifer Calora or. gray, white, red, brwn, and yellow. Cretaceous Cretaceous undifferentiated Disoorifonnity? Clay, solid and silty; raw lenses and Iq ars or Band; little gravel. Lignite and pyrite common. Ca lora .re gray, red, Raritan and white, eoessonly variegated. clay 0-250 Raritan member confing unit Formation --- Disoonfolmity— Lloyd Sand Lloyd aquifer sand, ['ae to coarse, and gravel with Intercalated beds and . Lenses of light- to dark -gray clay, silt, clayey and silty and and some ,!Rohe and pyrite. Locally had gradational Member 0-550 contact with overlying terpin cloy. Color■ are yellow, gray, and vh lies clay la roe locally. 100 toil yrs Unconformity. Crystalline me tomo rph lc and igneous cork,: ouecovl[e-b tat lie Early 400 mil yrs -c hist, gneiss, and granite. Surface of bedrock Is cammonlY Paleozoic highly weathered to a greents'h-white residual clay. W Bedrock Bedrock at Precambrian(?) knawa i >550 mil yrs Ce) _ +200 U -200 -400 Lrl Ql -600 .-Boo Ol 4-4 -1000 0) -1200 4-1 -1400 -1600 -180a -2000 th fn Figure 5-2 HYDROGEOLOGIC CROSS-SECTION A - A' t200 0 -200 -400 -600 -800 -1000 -1200. -1400 -1600 —Iaoo -2000 Ln I v +200 0 -200 -400 41 -1000 .r{ J� r -I -1200 -.4 -1400 -1600 -1800 -2000 Figure 5-3 HYDROGEOLOOIC CROSS SECTION B - B' 4 4 Q �G r• , `n n m m o o o 41 -1000 .r{ J� r -I -1200 -.4 -1400 -1600 -1800 -2000 Figure 5-3 HYDROGEOLOOIC CROSS SECTION B - B' D' 4-200 0 -200 -400 X00 -800 -1000 -1200 -1400 -1600 -1800 -2000 -200 -4100 -600 n iJ v 01 -800 W v -1000 7 L L -1200 r -i C -1400 -1600 -ld00 -2000 +2 0 Figure 5-5 HYDROGEOLOGIC CROSS SECTION D — D' CL e S • n 4 E A E t ^' o �. g a " w r. a -200 X00 -600 L C1 Q) W -800 v N b 7 -1000 L rl L -1200 -1400 -1600 -1800 -2000 E' +zoo 0 -200 -400 -600 -800 -1000 -1200 _1660 -1600 -1800 -2000 Figure 5-6 HYDROGEOLOGIC CROSS SECTION E - E' 5-9 C +20, -20( -400 4J -600 41 O1 4.1 �! -800 C1 b l-1 -1000 1J -1200 -1400 -1600 -1800 -2000 R O N 4 Y Y w aq 4 0 n N H h y Figure 5-4 HYUROGEOLOGIC CROSS SECTION C - C' +200 0 -200 - 4 (j0 -600 -806 -1000 -1200 -1400 -1600 -1800 -2000 5.1.1 Bedrock Bedrock below Suffolk County is comprised of crystalline metamorphic rocks (gneisses and schists) that are similar to those found in Connecticut. The original basement rocks are believed to have been early Paleozoic (Cambro-Ordovician) to Precambrian (?) granite •or sandstone more than 400 million years old. These rocks were crystallized by heat and pressure during folding and faulting caused by tectonic forces during early Paleozoic time (200-300 million years ago). The bedrock surface below Suffolk County is tilted south- east to south at a slope of approximately 50 to 70 feet per mile. It is, therefore, closest to land surface (within 500- ... 600 feet) in northwest Huntington and at Orient, and deepest along the South Shore (over 2,000 feet deep at the western part of Fire Island). In many places; the upper surface of the bed- rock is weathered to a residual clay. Since the water bearing capacity of the unit is extremely low, the bedrock surface is considered to be the bottom of the groundwater reservoir, 5.1.2 Llovd Sand Member of the Raritan Formation The sediments comprising the Raritan Formation lie on the•; bedrock surface and are believed to have been derived from stream erosion of areas to the north- and west during late. Cretaceous time (60-100 million years ago). The formation is made up of a lower sand and gravel member (Lloyd Sand) and• upper clay member (Raritan clay).. The Lloyd Sand Member has a moderate overall hydraulic" conductivity and consists of sand and gravel interbeds, with occasional lenses of•clay and silt. The Lloyd's beds are about. parallel to the bedrock surface below. Its upper surface lies about 400 feet below sea level in northwest Huntington and at Orient, and over 1,500 feet below sea level at western Fire Island. The unit is believed to terminate somewhere close to: the North Shore beneath Long Island Sound, and is not found in Connecticut. The thickness of the Lloyd increases from north 5-10 t -_ to south; it is about 200 feet thick in northwest Huntington, 100 feet thick at Orient, and over 500 feet thick at western Fire Island. 5.1.3 Clay Member of the Raritan Formation The clay member of the Raritan Formation (Raritan clay) overlies the Lloyd Sand Member throughout Suffolk County. In some locations, however, the clay has been eroded, and glacial deposits overlie the Lloyd, thus providing good hydraulic con- ductivity between the glacial deposits and the Lloyd aquifer (see Section 5.3). The Raritan clay, although composed mainly of clay and silt, does contain some sand and gravel beds .and lenses; overall, however, the hydraulic conductivity of the clay member is low, and it confines the water in the Lloyd aquifer. The Raritan clay parallels the Lloyd Sand Member and term- inates just offshore in Long Island Sound. The surface of the clay member lies between 300 and 400 feet below sea level in northwest Huntington and at Orient, and about 1,100-1,300 feet below sea level at western Fire Island. Clay member thickness- es range between 50 and 100 feet in the northern areas, and reach nearly 300 feet in the western part of Fire Island. 5.1.4 Magothy Formation - Matawan Group Undifferentiated The Magothy Formation - Matawan Group undifferentiated (informally "Magothy") is composed of river delta sediments that were deposited on top .of the Raritan Formation during the late Cretaceous after a period" of erosion. It consists of highly permeable quartzose sand and gravel deposits with inter - beds and lenses of clay and silt that may have local hydrologic significance (see Section 5.3). The. Magothy was' -eroded during the time period between the end of Cretaceous and the Pleistocene. The surface was scoured by glaciers, particularly in northwest Huntington, where it is completely eroded. Glacial- meltwaters also shaped the Mago- 5-11 thy's surface, creating north -south valleys that are now buried below the -areas of Huntington -Deer Park; St. James -Ronkonkoma - Sayville, and Miller Place -Selden. In addition, the Connec- ticut River is believed to have created the buried valley that runs through the vicinity of Orient-Amagansett during a period of lowered sea level. Unlike the upper surfaces of bedrock and the members. of the Raritan Formation, the highly eroded upper surface of the Magothy does not exhibit any distinctive tilt to the southeast, although bedding planes within the formation have this orienta- tion. Because the upper surface is so irregular, the thickness of the Magothy varies; however, the thickness generally in- creases from north to south, with the greatest thicknesses (around 1,000 feet) found along the South Shore. 5.1.5 Monmouth Group The -Monmouth Group is the youngest Cretaceous unit. It was deposited in a shallow marine environment and consists of interbedded clay, silt, and sand, giving the unit a Low overall permeability. The Monmouth contains much of the mineral glau- conite, which gives the unit a dark greenish color, and is the basis for the hydrogeologic unit's name -- Monmouth greensand. The Monmouth Group overlies the Magothy Formation along most of the South Shore, except for portions of the South Fork. Post Cretaceous erosion by glacial meltwater streams is evident on the surface of the unit, but it appears to have been spared the glacial scouring seen in other Cretaceous formations loca- ted further north. The upper surface ranges from about 70 to 165 feet below sea level, and has beenfound in thicknesses up to 200 feet.' 5.1.6 Gardiners Clay The Gardiners Clay is a shallow marine or brackish -water deposit of late Pleistocene age. It is typically grayish -green to gray; the variation in color is due to the content of miner - 5 -12 i�s als such as glauconite. The unit contains some beds and lenses of sand and silt, but its overall hydraulic conductivity is low, making it a confining layer for underlying aquifer forma- :, tions, particularly the Magothy. The Gardiners Clay is found along most of the South Shore. Its northern extent varies from 3 to 5 miles inland and is in- dented by long, narrow north -south channels, which indicate the effects of erosion by glacial meltwater streams and areas of nondeposition. The upper surface of the unit ranges in alti- tude from 40 to 120 feet below sea level. The thickness of the unit increases southward toward the barrier islands, reaching thicknesses of over 100 feet. 5.1.7 Glacial Deposits (,I Continental glaciers of Wisconsinan age (20 to 86 thousand years ago) brought to Long Island the materials that now com- prise nearly all of its surficial sediments. Glacial material j i was deposited in two terminal moraines -- the Ronkonkoma mor- I, aine, which forms Suffolk's "spine" and .South Fork, and the Harbor Hill moraine, which runs along the North Shore 'and forms the North Fork. Some of the original glacial material (till) can still be seen along the north shore of the South Fork, at Montauk, and on Shelter Island, where it acts to retard. the downward movement of recharge. Most of the glacial material was reworked by meltwater to form large, sandy outwash plain deposits south of and between the two moraines. ' These highly permeable, stratified sand and gravel deposits filled in the valleys eroded on the surface of the Magothy (although some filling may have occurred prior to. the ice sheet's advance to Long Island). The glacial deposits can reach thicknesses of up to 700 feet (e.g., in the "Ronkonkoma Basin"). They generally overlie Magothy deposits, except in areas of the North Shore where the Magothy was scoured away by glaciers, and 1. in areas of the South Shore where the Gardiners Clay or Monmouth Group intervene. 5-13 Clay materials were also eroded .from the moraines and de- posited in freshwater lakes or shallow marine lagoons. An ex- ample of such a clay is the Smithtown clay unit, located in northeast Huntington, northern Smithtown, and northeast Brook- haven. It occurs within the sequence of outwash deposits and ranges in depth from 90 feet above sea level to 150 feet below sea level. Its thickness ranges up to 170 feet. Because of its overall low conductivity, the clay acts as a local confining unit between upper and lower portions of the glacial aquifer. 5.1.8 Recent Deposits Beach and marsh deposits of Holocene age are found pri- marily along the shoreline, and within stream corridors and ponds. Beach deposits consist primarily of sands eroded from the outwash plain or bluffs by wind, runoff, and wave action. Marsh deposits consist of mud and peat, which accumulate along streambeds, in ponds, and in tidal marshes and shoals. These deposits are generally thin, but may be of local hydrogeologic significance (e.g., on the barrier islands). 5.2 Hydrology The hydrologic water budget equation, which balances in- puts to and outputs from Suffolk's groundwater system under natural (pre -development) conditions, is written as follows: P- E- R= S+ U where P = precipitation, E = evapotranspiration, R = runoff (direct), S = stream baseflow, and U = underflow. The left side of the equation is equal to the amount of water recharged to the..aquifer system. The right side of the equa- tion represents losses from the system. No term for the change in groundwater storage is included in the equation; since steady-state (dynamic equilibrium) conditions are assumed. 5-14 a:„3 1' Discussions of the various elements that make up the water budget equation have been presented in a number of previous publications (Cohen, et al., 1968; Holzmacher, et al., 1970; Franke and McClymonds, 1972). The purpose of this subsection � is to present an updated summary of information on the budget elements, including new estimates of the rate of precipitation recharge to the groundwater aquifer system. 5.2.1 Precipitation All naturally occurring fresh water in Suffolk County originates as precipitation. The long-term precipitation rate has been found to be fairly evenly distributed throughout the calendar year, so that no distinct wet or dry seasons are distinguishable (see below). A considerable amount of winter precipitation is caused by low-pressure systems that move northeastward along the Atlantic coast. Accompanied by strong winds, such low-pressure storms are known as "northeasters." Rain, snow, or sleet can develop, depending on air temperature. Summer precipitation is largely due to- thunderstorms or showers, which are usually associated with the passage of cold fronts. These storms can have significant localized effects, resulting in large differences in rainfall records between near -by stations. Tropical storms also affect Suffolk County, having their greatest frequency from June through November. Although the centers of most of these storms pass by Long Is- land, their effect on precipitation can still be considerable. Precipitation Records The oldest and longest precipitation records in the region are -those for New York City; these date back to 1826, and ..are now kept by the National Oceanographic and Atmospheric Admin- istration (NOAA). Suffolk County has had over 46 recording sites during the past century, but many have records of only two or three years, and cannot be considered useful for county- wide analyses. The longest continuous record in Suffolk County 5-15 is for the NOAA station in Setauket, where data have been col- lected since 1886. The next longest precipitation record is for Cutchogue; it was begun in 1899, but was discontinued in 1979, and contains numerous data gaps. A summary of data,for 18 operating stations is presented in Table 5-2. Average Precipitation The county -wide average precipitation rate is about 45 inches per year. This rate can vary + 10 percent or more, depending on location (Table 5-2). Yearly fluctuations are usually less than + 8 inches for most locations (Table 5-2). Average precipitation values for the long-term stations at Setauket, Cutchogue, Bridgehampton, and Riverhead are presented in Table 5-3. These averages cover various 30 -year normal per- iods utilized by NOAA. Mean monthly precipitation values for the Setauket sta- tion, and combined monthly averages for all Suffolk stations, are presented in Table 5-4. These figures indicate that Setau- ket values are fairly representative of the county as a whole, and that the average yearly total for the county is approxi- mately 45 inches. Table 5-4 also indicates a fairly small range of monthly values around the overall monthly mean of 3.75 inches, with no clear seasonal trends (wet and dry seasons). A snap of average yearly precipitation values in Suffolk County (Figure 5-7) was prepared by the USGS based on an anal- ysis of records at 41 stations for the 15 -year period 1951 to 1965 (Miller and Frederick, 1969). There is a close match be- tween map values and the mean values for those stations with long records (i.e., longer than 15 years) listed in Table 5-3. In most cases the match is within a few tenths of an inch; the largest difference is about 2 inches, or less than 5 percent of total annual precipitation. The 1951 to 1965 map, therefore, was used during the WRMP study to represent long-term average precipitation patterns in the calculation of groundwater re- charge rates (see Section 5.2.4), which were then utilized in groundwater modelling studies (see Section 5-.4). 5-16 LM I F1 J WRMP Table 5-2 PRECIPITATION DATA FOR EIGHTEEN OPERATING SUFFOLK COUNTY STATIONS STATION OPERATOR YEARS MEAN FULL STAND MAXI- YEAR MINI- YEAR YEARS DEV MUM MUM ---------------------------------------------------------------------------------------- Belmont Lake State Park I S.C.D.H.S. 1 8 1 44.43 6 8.1. 1 52.90 1975 1 35.51 1976 1 Bridgehampton I N.O.A.A. 1 53 1 45.00 51 7.2 1 63.71 1953 1 30.67 1963 1 Caleb Smith St. Park I U.S.G.S. 1 5 1 44.55 4 1 53.58 1979 1 36.66 1981 1 i N i ssequogue R. i Calverton (Grumman Aerol 29 1 43.66 20 7.4 1 57.13 1972 1 29.79 1965 1 Connetquot R. St. Park I U.S.G.S. 1 4 1 40.22 3 1 43.24 19H2 1 36.06 1980 1 Greenport I N.O.A.A. 1 31 1 43.35 25 7.0 1 53.58 1953 1 25.94 1965 1 Huntington Village I Joy= R i s?o 1 10 1 52.72 0 9.4 1 66.66 1975 1 41.32 1901 1 Kings Park I .U.S.B.S. 1 17 1 47.82 16 7.2 1 62.45 1977 1 40.49 1968 1 Lake Ronkonkoma I U.S.G.S. 1 '7 1 54.97 5 11.4 1 68.27 1951 1 28.71 1965 1 L.I. MacArthur Airport I' N.O.A.A. 1 20 1 43.04 19 7.2 1 54.32 1979 1 25.87 1965 1 Medford I S.C.D.H.S. 1 8 1 39.7.2 10 7.0 1 40.65 1975 1 20.71 1900 1 Oakdale I S.C.W.A. 1 18 1 42.63 16 5.7 1 51.71 1972 1 34.37 1966 1 Patchogue I N.O.A.A. 1 46 1 45.57 44 6.9 1 62.45 1979 1 30.66 1963 1 Riverhead Research Farm I N.O.A.A. 1 45 1 44.56 45 6.:5 1 58.59 1972 1 31.98 1980 1 Seldon I U.S.G.S. 1 11 1 46.50 10 6.4 1 54.0.1 1977 1 36.60 1901 1 Setauket I N.O.A.A. 1 97 1 44.79 97 6.2 1 59.26 1897 1 26.55 1965 1 Upton I B. N. L. 1 40 1 46.32 40 6.9 1 58:63 1972 1 31.82 1965 1 Vanderbilt Museum I N.O.A.A. 1 7 1 47.21 6 8.1 1 57.09 1979 1 38.22 1982 1 INDEX -TO- OPEARORS B. N. L. - Brookhaven National Laboratory N. 0. A. A. - National Oceanic and Atmospheric Administration S. C. D. H. S. - Suffolk County Department of Health Services. S. C. W. A. - Suffolk Coutny Water Authority U. S. G. S. - United States Geological Survey -Water Resources Division WRMP Table 5-4 Riverhead 43.76 45.70 AVERAGE MONTHLY'PRECIPITATION AT SETAUKET AND FOR ALL OF SUFFOLK COUNTY PRECIPITATION STATIONS THROUGH 1982 Month Setauket WRMP Table 5-3 January 30 -YEAR NORMAL PERIOD PRECIPITATION 3.91 FOR FOUR LONG-TERM RECORD STATIONS Normal 4.09 4.11 Bridge - Period Setauket Cutchogue hampton 1891-1920 44.96 --- --- 1901-1930 44.02 45.16 --- 1911-1940 44.04 45.30 --- 1921-1950 43.62 45.48 --- 1931-1960 44.57 45.88 44.21 1941-1970 43.24 42.28 44.13 1951-1980 44.95 --- 46.00 WRMP Table 5-4 Riverhead 43.76 45.70 AVERAGE MONTHLY'PRECIPITATION AT SETAUKET AND FOR ALL OF SUFFOLK COUNTY PRECIPITATION STATIONS THROUGH 1982 Month Setauket Suffolk January 3.86 3.91 February 3.55 3.41 March 4.09 4.11 April 3.77 3.89 May 3.50 3.61 June 3.22 3.17 July 3. 69 3.27 August 4.05 4.07 September 3.64 3.59 October 3.61 3.62 November 3.85 3.98 December 3.94 4.30 44.77 44.93 5-18 I; 9 After Miller and Frederick (1969). Water years 1951-1965. Fiyure.5-7 --45.5--- Line of equal mean annual precipitation 0 5 10 15 1 inch with dashed supplemantal S 20 25 MLLES Interval 0.5 -inch line 5 0 S 10 IS 20 25 KILOMETERS AVERAGE ANNUAL PRECIPITATION: SUFFOLK COUNTY i 1702-1973. However, longer periods of generally below-average precipitation have occurred, most notably the 50 -year period 1751-1806, when over 70 percent of the years were drier than the 280 -year average. 5.2.2 Evapotranspiration The evapotranspiration term in the hydrologic water budget equation encompasses a number of physical and biological pro- cesses, including: o evaporation of precipitation from paved and plant surfaces, o transpiration of root -zone moisture by vegetation, o evaporation of fresh surface water (streams and ponds), and o evaporation and transpiration of shallow groundwater. The first two processes are the most significant, and need to be factored into the budget equation. Direct evaporation of ' fresh surface water can be significant locally, but the total Area of such waters in Suffolk County is small ( less than one- half percent). Direct evapotranspiration p piration of groundwater from the saturated zone is. -generally limited to areas where the water table is close to land surface (within 3 to 5 feet); such conditions occur in areas along the shoreline and adjacent to fresh surface waters, which comprise only a small percentage of Suffolk's land mass. The latter two processes, therefore, are generally ignored when applying the water budget equation. The evaporation of P precipitation from paved and plant i surfaces, and the transpiration of soil moisture by vegetation, are affected by a number of meteorologic factors, including i rainfall, insolation, temperature, humidity, and wind. Vege- tation will respond to and influence soil moisture levels; each species will.vary in leaf mass, moisture needs, depth of root i penetration, and length of growing season. In addition, phys- ical parameters will affect evapotranspiration processes; these include topography, soil type, and extent of impervious surfaces cover, which affect leaching and runoff rates. 5-22 p,, The meteorological, biological, and physical factors that affect evapotranspiration rates will vary spatially and/or tern - orally. It is therefore extremely difficult to determine a aepresentative average rate for an area as diverse in climate, -egetation, and physical make-up as Suffolk County. Neverthe- ess, a number of attempts have been made to estimate an aver- age evapotranspiration rate for the county; these are summar- .zed in Table 5-5. Thornthwaite Method The method of Thornthwaite and Mather was used by Lubke 1964) to estimate an overall annual evapotranspiration rate .or Long Island of 22-26 inches (Table 5-5). The Thornthwaite nethod uses meteorological, vegetation, and soil type informa- .ion. Meteorological data are used to determine monthly poten- tial evapotranspiration rates; these are then compared to nonthly rainfall records, and where the potential evapotrans- piration rate exceeds rainfall, some soil moisture is assumed .o be lost From storage. Such soil moisture 'losses ars most likely to occur during the summer. The applicability of the rhornthwaite method to Long Island summer (May -August) condi- tions was supported by the results of- a 1968 study in Melville (Holzmacher, at al., 1970). Peterson (1986) used the Thornthwaite method to calculate annual evapotranspiration values for various locations on - Long Island where precipitation and temperature data for the 8 -year "average condition" period 1968-1975 were available (Table 5- 6). The values listed in Table 5-6 are generally within the 22-26 inch range reported by Lubke (1964). Typical vegetation and soil types were used in the calcu- lations, but these were not necessarily the most representative of the weather station.locations. For example, Patchogue rain- fall data ware used in conjunction with forest vegetation in order to develop a number that would reflect conditions in the pine barrens, and not the farm areas of the south shore. 5-23 A .s WRMP Table 5-5 ESTIMATES OF AVERAGE ANNUAL EVAPOTRANSPIRATION FOR LONG ISLAND Reference Location ET -(in) Comments Burr, et al. Southern L.I. 17 constant 17" for precip. (1904) Watersheds range of 35"-43" Jacob (1945) Long Island — 40% of precipitation Greeley and Nassau County 19.4 assumes 1.4" annual irri- Hansen (1963) gation added to precip. Pluhowski and Babylon -Islip 22-24 based on studies by Kantrowitz Williams, et al. in (1964) Penn. and Mass. Warren et al. Central S.C. 20-22 based on diff. between (1968) precip. and estimated groundwater discharge Lubke (1964) Long Island 22-26 Thornthwaite Method Hoffman (1961) Southold Town 21-26 for precip. range 35"-62"; Cutchogue precip. data Crandell (1963) Southold Town 22-30 based on Hoffman's est. and Greenport pan evap . data Holzmacher, et Melville, Hun- 18.7 May -Aug., lysimeter tests al. (1970) tington Town conducted for CPWS-24 Franke and L.I. Water — based on previous studies McClymonds Budget Area and water budget balance (1972) Steenhuis, et L.I. Horticul- 19.6 all precip. 5/15-10/15, 10% al. (1983) tural Lab rest of year (see T. 5-7) 5-24 4 WRMP Table 5-6 L EVAPOTRANSPIRATION RATES CALCULATED BY THE THORNTHWAITE METHOD (AVERAGE FOR 1968-19751 Station Precip ET $ET Root Zone or Crop Type Soil Type ($) (in) M Brid gehampton 45.42" 21.2" 46.6 1.7' - shallow root sandy loam 46.8" 23.0 21.4" 47.2 2.1' - shallow root silt loam Mineola 46.75" 25.1" 53.7 3.3' - moderate root sandy loam 43.1 25.8 25.5" 54.5 5.6' - orchards 45.9 Patchogue 47.72" 25.5" 53.5 8.3' - mature forest fine sand Riverhead 45.39" 22.4" 49.3 1.7' - shallow root sandy loam 24.8" 54.7 5.6' - orchards Setauket 46.28" 26.8" 57.9 6.7' - mature forest sandy loam Upton 49.44" 23.9" 48.4 4.2' - deep root silt loan 23.0" 46.5 3.3' - mod./deep root sandy loam WRMP Table 5-7 EVAPOTRANSPIRATION AND RECHARGE RATES BASED ON THE CORNELL FORMULA (AVERAGE FOR 1968-1975) 5-25 Evapotranspir. Recharge Station Precip. (in) ($) (in) M Bridgehampton 45.4" 17.8 39.3 27.6 60.7 Mineola 46.8" 23.0 49.3 23.7 50.7 Patchogue 47.7" 21.7 45.4 26.0 54.6 Riverhead 45.4" 19.6 43.1 25.8 56.9 Setauket 46.3" 21.2 45.9 25.1 54.1 5-25 5.2.4 —Recharge As indicated at the beginning of this section, natural recharge is equal to precipitation minus evapotranspiration and runoff (i.e., the left side of the hydrologic water budget equation). Recharge, therefore, is that portion of precipita- tion that seeps through the soil and reaches the water table. Estimates of average annual recharge by previous investi- gators (Table 5-10) have generally been equal to about one-half of average annual precipitation. Except for Jacob and Steen- huis, at al., all estimates fall within the range of 20-24 in- ches per year (1.0-1.1 mgd/sq mile), or between 43 and 51 percent of annual precipitation (as assumed by the investiga- tors). In the case of Steenhuis, et al., the study area did not produce any runoff, and the vegetation involved (turf) had, Reference Jacob (1944) Lubke (1.964) Pluhowski & Kan- trowitz (1964) Cohen, et al., . (1968) Holzmacher, et al., (1970) Franke & McCly- monds (1972) Porter. -&'- Baskin (1977) Steenhuis, et al., (1983) WRMP Table 5-10 ESTIMATES OF AVERAGE ANNUAL RECHARGE FOR LONG ISLAND Recharge Estimates Location in % precip. mgd sq mi Long Island -- 60 -- Hunt.-Smith. 21 43 1.0 Babylon -Islip 24 52 1.1 Nassau Co., 23 51 1.1 W. & Cen. S.C. S..C. Water 20.5 44 1.0 Budget Area L.I. Water 21.7 49 1.0 Budget Area Nass. & Suff. 20.7 48 1.0 Riverhead, 25.8 57 1.2 (see T. 5-7) II� r 5-29 _ f a shallow root zone (low transpiration potential); both these factors would tend to increase the recharge percentage. The other investigators considered runoff, but it constituted only a small portion of precipitation loss; recharge, therefore, was approximately equal to precipitation minus evapotranspiration (see evapotranspiration values in Table 5-5). Average annual recharge rates were calculated and mapped by the USGS for this study and are presented on.Figurc 5-9 (Peterson, 1986). These calculations utilized the mean annual precipitation values derived by Miller and Frederick (1969) and discussed in Section 5.2.1 (Figure 5-7). Evapotranspiration values were calculated by the Thornthwaite and Mather method (see Section 5.2.2) using data on county -wide monthly tempera- tures, soil conditions (from 1975 Soil Conservation Service Soil Survey maps), and land use patterns (from 1981 Long Island Regional Planning Board maps). Runoff values for the average condition period 1968-75 were calculated using the percentage differences between total and baseflow values for continuously gauged streams during the period, and extrapolating these run- off percentages to other streams in the county with similar degrees of urbanization (see Sections 5.2.3 and 5.2.5). The recharge values shown on Figure 5-9 compare favorably with previous regional estimates (see Table 5-10). The average annual recharge rate for the main body of the county is 23.5 inches, or 51.1 percent of the 45.9 inches of average precipi- tation for the main body. This translates to an average re- charge rate of 1.12 mgd per square mile on the main body of Suffolk. Recharge percentages are generally lower in the ur- banized western towns of Babylon and Islip, where increased runoff to streams is experienced. Recharge rate estimates for the North and South Forks Ara/ somewhat lower than those for the main bodv. Estimates fnr f.-hra North'Fork range between 19 and 21 inches per r (ERM, 1983). The estimated rate for the South Fork is 22 inches per year (Nemickas and Koszalka, 1982). 5-30 Ln E4 ?4 Z16 Z4 (C ( L/ Yom: Source: Peterson (1986). Contour interval = 2 Figure.5-9 AVERAGE ANNUAL RECHARGE: MAIN BODY OF SUFFOLK inches per year. NEW YORK STATE WELLHEAD PROTECTION PROGRAM SUBMITTAL .To UNITED STATES ENVIRONMENTAL PROTECTION AGENCY IN APPLICATION FOR IMPLEMENTATION FUNDS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION DIVISION OF WATER ALBANY, NY MAY 1990 numerous 3 to 12 square mile WHPA's (1-2 _. mile radius) for non -community wells intersect or nearly intersect across the State. It must be recognized that all fresh groundwaters in bedrock aquifers are classified as GA groundwaters and thus are already protected by substantial statewide protection programs which use rigorous — ambient water quality standards in their - design. 3. Mapping and Case Studies: Mapping will be performed according to the phasing priorities described in Section 3.3. Case studies of fixed radius approaches are not considered to be of significant benefit. As proposals for revisions based on alternative approaches are submitted to the Department of Environmental Conservation, they will be evaluated for potential use as models for comparable hydrogeoiogic conditions. 4. Public Water Supply Significance: Relatively few municipal community systems utilize bedrock aquifers In New York State and those that do are generally with low population dependence. Public water supplies in bedrock aquifers are typically non -community wells serving small numbers of people. Magothy and Lloyd Aoulfers - Lona Island 1. WHPA Definition: The boundaries of the wellhead protection area for public water supplies using the Magothy and Lloyd aquifers are the boundaries of the Deep Flow Recharge Area as recognized by the Department of Environmental Conservation. Refinements within the overall WHPA may include further definition of Wellfield Management Areas, pending approval by the Department of Environmental Conservation. 2.. Rationale: The Deep Flow Recharge Area was determined to be the most Important overall groundwater protection area for wells in the Magothy and Lloyd aquifers in the Long Island Groundwater Management Program already adopted and certified by the Governor of New York as an element of the New York State Water Quality Management Program. The delineations have also been adopted in the Suffolk County Sanitary Code. - -- 3. Mappina and Case Studies: Mapping of the Deep Flow Recharge Area Is already completed. Additional case _. studies are not considered appropriate. __ -23- 4. Public Water Suppiv Sianificance: Most public water In Nassau County is withdrawn from the Magothy aquifer. The majority of public water supplies in Suffolk County are also withdrawn from the Magothy aquifer. Of those public water supplies in Suffolk County utilizing the Glacial aquifer, approximately half are located within the Deep Flow Recharge Area Thus, these wells are included within the overall wellhead protection area for the deeper aquifers. 1. WHPA Definition: The boundaries of the wellhead protection area for public water supplies using the Glacial aquifer are defined as a fixed variable shape zone with a fixed radius in the upgradient groundwater flow direction of 1,500 feet and a fixed radius in the downgradient direction of 500 feet. Revisions may be made, pending approval by the Department of Environmental Conservation. TABLE 2 PERMEABILITY OF GEOLOGIC MATEBIAIS* Freeze, B.A. and J.A. Cherry, Groundwater, Prentice -Hall, Inc., New York, 1979 15 Approximate Range of Assigned Type of Material Hydraulic Conductivity Value Clay, compact till, shale; unfractured clo-7 cm/sec 0 metamorphic and igneous rocks Silt, loess, silty clays, silty 10-5 - 10-7 cm/sec 1 loans, clay loans; less permeable limestone, dolomites, and sandstone; moderately permeable till Fine sand and silty sand; sandy 10-3 - 10-5 cm/sac 2 loans; loamy sands; moderately permeable limestone, dolomites, and sandstone (no karst); moderately fractured igneous and metamorphic rocks, some coarse till Gravel, sand; highly fractured 'lOr3 cm/sec 3 igneous and metamorphic rocks; permeable basalt and lavas; karst limestone and dolomite *Derived from: Davis, S. N., and Permeability of Natural Materials in Flow -Through IPorosity Porous Media, B.J.M. DeNest ed., Academic Press, New York, 1969 Freeze, B.A. and J.A. Cherry, Groundwater, Prentice -Hall, Inc., New York, 1979 15 GSC -:R®645 GRAPHICAL MMSURE MODELING SYSTEM (GEMS) USER"S GUIDE. VOLUME 2. mOOELING Prepared for: U.S. EMRODIIWMAL PR07W.ION AGE= OFFICE OF PESTICIDES ANo TOXIC SUBSTANCES EXPOSURE E.V=ATION OMS ION Task No. 3-2 Contract No. 68023979 Project Officer: RUssell Kinerson Task Manager: Loren Hall Prepared by: CMJERAL SCIENCES CORPORATION 8401 Corporate Drive Lardo"r, Maryland 23783 SUbnitted: Deember 1, 1.986 GEMS> I SOUTHOLD LF LATITUDE 41: 1:40 LONGITUDE 72:30: 0 1980 POPULATION SECTOR K:i°i 0.00-.400 .400-.810 .810-1.60 1.60-3.20 3.20-4.80 --------- 4.80-6.40 ------------------ TOTALS ------------ S 1 --------- 0 --------- 0 1086 --------- 980 3671 2615 --------- 8352 --------- RING --------- e --------- x)` 1086 --------- 980 --------- 3671 --------- 2615 8352 TOTALS (0q -7-7 GEMS> I SOUTHOLD LF LATITUDE 41: 1:40 LONGITUDE 72:30: 0 1980 HOUSING SECTOR Kil 0.00-.400 .400-.810 .810-1.60 1.60-3.20 3.20-4.80 4.80-6.40 TOTALS ----------- ------ --------- --------- --------- --------- --------- S 1 0 0 398 368 1385 996 3147 --------------------------------------------------------------- RING o,-+ /0-4 398 368 1385 996 3147 TOTALS d, q -lou5er covNT CCA -T-6�cPT o f=�N��J'-;oti� v_s. Gs. TopvzApti Y" ,<«�Y"A � i 7a rye � �v u f C� s PJZ � e,s �n q Tr� J Ai;��Nolo i'Nv kL:v g6— zx a uz-- &,o,((�e.�, iv 0.3�/ n Co ✓1ve�s,o� v PPu(RTo,•1 11 515U g35-1. 0 S ( 4 7 = 2,o(�,5 KEY TO MAP 590 -Year Flood Boundary ZONE B 100 -Near Flood Boundary---' Zone Designations* 100 -Year Flood Boundary ZONE B 500 -Year Flood Boundary Base Flood Elevation Line 513 With Elevation In Feel -- Base Flood Elevation in Feet ML 987) Where Uniform Within Zone— Elmatitm Reference Mark RM7X Zone D Boundary — River Mile a M 1.5 --Referenced to the National Geodetic Vertical Datum of 1929 *EXPLANATION OF ZONE DESIGNATIONS ZONE EXPLANATION A Areas of 100 -year flood; base flood elevations and flood hazard factors not determined. AO Areas of 100 -year shallow flooding where depths are between one (1) and three (3) feet: average depths of inundation are shown, but no flood hazard factors are determined. AN Areas of 100 -year shallow flooding where depths are between one (1) and three (3) feet; base flood elevations are shown, but no flood hazard factors are determined. Al -A30 Areas of 100 -year flood; base flood elevations and flood hazard fxtors determined. A99 Areas of 100 -year flood to be protected by flood protection system under construction; base flood elevations and flood hazard factors not determined. a Areas between limits of the 100 -year flood and 500- year flood; or certain areas subject to 100 -year flood- ing with average depths less than one (1) fool or where the contributing drainage area is less than one square mile; or areas protected by levees from the base flood. (Medium shading) C Area of minimal flooding. (No shading) O Areas of undetermined, but possible, flood hazards. V Areas of 100 -year coastal flood with velocity (wave action l; base flood elevations and flood hazard factors not determined. VI -V30 Areas of 100 -year coastal flood with velocity (ware action); base flood elevations and flood hazard factors determined. NOTES TO USER Certain areas not in the special flood hazard areas (zones A and V) may be protected by flood control structures. This map is lot flood Insurance and flood plain management pur— poses only; It does not necessarily show all areas subject to flood- ing In the community or all planlmetrit features outside special flood hazard areas. The coastal flooding elevations shown may differ significantly from those developed by the National Weather Smite for hurricane evacuation planning. For adjoining map panels, we separately printed Index To Map Panels. Coastal base flood elevatlons shown on this map Include the effects of wave acilon. Coastal base flood elevations apply only landward of the shoreline axavlz on this map. NATIONAL FL000 INSURANCE PROGRAM FIRM FLOOD INSURANCE RATE MAP TOWN OF SOUTHOLD, NEW YORK SUFFOLK COUNTY PANEL 93 OF 120 (SEE MAP INDEX FOR PANELS NOT PRINTED) COMMUNITY -PANEL NUMBER 360813 0093 D APRIL 1 REVISED: Federal Emergency Management Agency INITIAL IDENTIFICATION: NOVEMBER 29. 1974 FLOOD HAZARD BOUNDARY MAP REVISIONS: NONE FLOOD INSURANCE RATE MAP EFFECTIVE: MARCH 18. 1980 FLOOD INSURANCE RATE MAP REVISIONS: June 3. 1980 - to change none destignations June 1 S. 1983 - to add the effects of wave action, to add spatial flood hazard areae. to reduce, accent flood hazard areas end to add base flood elevations. April 17. 1988 -to change bene flood elevation, and to reduce special flood hozard sten. To determine if flood insurance is available in this community, contact your insurance agent, or call the National Flood Insurance Program, at (800) 638-6620. \\ 11 ROAD HARTFORD, CONN.; N.•Y.; N. J.; MASS. 1962 REVISED 1975 Scale 1:250,000 5 0 5 10 15 20 Statute Miles --=r—T 5 0 5 10 15 20 25 30 Kilometres 0 ---- 4 — 1- 5 0 5 10 15 Nautical Mlles CONTOUR INTERVAL 100 FEET WITH SUPPLEMENTARY CONTOURS AT 50 FOOT INTERVALS TRANSVERSE MERCATOR PROJECTION BLACK NUMBERED LINES INDICATE THE 10,000 METRE UNIVERSAL TRANSVERSE MERCATOR GRID, ZONE 18 1975 MAGNET IC ERLY THE CENTER OF THE DWEST NEDGE HTO FR14• 1250 MM TRUE FLSHWWESTERLY VARIES FRFOR THE iCENTER OF TO MILS, THE EAST REDGE FOR SALE BY U.S. GEOLOGICAL SURVEY, RESTON, VIRGINIA 22092 LOCATION DIAGRAM, 6:3° 43 B. N YO�NK �-5 VER QNj__T W FAT PSH E NK 18.4 ANY K 19• N K 18.6 gTON EI MIR• , _ �I ASETT MMnFORD tj I.?AOVI NK 18.7NK'18.8 I !CONNECT 7_ • SCAAWFON �N WILLIAM pRT P • LNNSYLVA1NIA ,N[wA1NEw NK 18.10I NEW' Pillar— NK 1 NK 18.12 \' • MARRI BU11RG ,� t\`• MARYLAN ,.VA e•ulNo J 18• \ , VIR I7'ilA DEL WARE 8,jq 18-5 soulau" 38' 38.78' 68° NEW YORK, N.Y.; N.J.; CONN. 1960 REVISED 1979 CONTOUR INTERVAL 50 FEET WITH SUPPLEMENTARY CONTOURS AT 25 FOOT INTERVALS EHT of 7y TRANSVERSE MERCATOR PROJECTION S.2— THE W BLACK NUMBERED LINES INDICATE THE 10,000 METER UNIVERSAL TRANSVERSE MERCATOR GRID, ZONE 18 1979 MAGNETIC DECLINATION FROM TRUE NORTH VARIES FROM 1116' (200 MILS) WESTERLY FOR CENTER OF THE WEST EDGE TO 1314' (240 MILS) WESTERLY FOR THE CENTER OF THE EAST EDGEFOR SALE BY U.S. GEOLOGICAL SURVEY, RESTON, VIRGINIA 22092 LEGEND - Figures in red denote approximate distances in miles between stars ROADS POPULATED PLACES o Primary, all-weather, hard surface BOSTON Secondary, all•weather,.hard surface Over 500.000 Light•duty. all-weather, improved surface 100,000 to 500.000 RICHMOND Fair or dry weather, unimproved surface- 25,000 urface25,000 to 100,000—EVANSTONTrail 5,000 to 25,000 Newnan Interchange 1,000 to 5.000 Bar Harbor 99 Nl Less than 1,000 Flshkill Route markers: Interstate, U.S., State RAILROADS S'�Vie IraCk Double or Mull-cl, Standard gauge+•-4—+� O an School; Church; Other_ t 1 Narrow gauge_��-+——� Landplane airport Depth curve In feet BOUNDARIES Landing area— Limit of danger; Reef— International— State eef InternationalState _ _ _ _ Seaplane airport Rocks: Awash County—___ Foreshore flat : Mud Seaplane anchorage_ ••.. Park or reservation_ ------------ Mine 5i` Power Ilne Intermittent or dry stream Spot elevation In feet .22/ Woods -brushwood. t_J Marsh or swamp IK RES'. (� \, \ v "RT ,..i • Ia.N D a 4° \ _•p � `( ` ` 'V. � Attav v. �Beac lay r k"� *Giants Blacbfo. f `Stony' 0 J * ' � � I r ok _ PO t, Sou d+i* ` Blatfl� reeD � ° "' �y.,,� i *-- Manb I;� _- 'White *View nK * fl.1�•� eavi I Gr M * kSands J rc r 'G - i r - C • /5- YBeach * 60 Beach �ir� * *' .� Clinton '-�Y�,rhruu/ Knollwood Lights �I� gq a—xaMtvta�ASS£� BEACk �. a ch Ilur NO w Sacfi STATE PARK H aMnorwi"t I G, Olaf Light 60 1 �itv�i O Lt' �Qf� / I ,':s ient ggq/��h-,,mt bI n h}/,i ORIENT BEACH " I a - V �r�\ Zhur,cnr -<-STATE PAR(f 10 Com'�60�ighthouse I �iArs11 J e * on ) `* D Harbor t 6Il.lil 5 j Li tp - a '1 e� 1a e1g h*s I l C 5ySMNbrAslsnq / N �_.elxedoq s "'ms Ca r S , outhold' `Sho - �% .i r as La Ing #ter; i.til. \ y - *r, \,* a4dstone r r R_6I 8 Indlan Neck - North . H ven I t / 5 \ ,1•'u uck led, Fes. t ..� l' y L Iff • I • . ni I '6MTON E A R "File ' B Ll IOWA ti a ea "Peconit+ `\ J MR e enbu riches - ' gadio'taWftr'- JiLW 6 f � FIREI( �llltt9, �Pik��/ 60, I / I i it i r . <<r t \ ' Sho I n I t N W R HarbO�' jl �t r ewe, _j E A M ON Mattitdtllr(� -4LZiSuffolk\\ NWR�- - 41.!11le 'conic arf y p -e S8 r ' ittitaCk ` ' Lelirel �i 8r7 y'• Rotrw U r~' 3q a o 0 �Iql � 55 0 0 (amespor Creat Peconic b�v a tQ. n CONSCIENMFT� �j0 o ' r > -/South ay r Se I z Jamesport J r a pt a In, t l'6n,.;.•,.• I 1 ,� �Rsditi �' Ma�rpm�d � e3/ /(� Srr n ack atco ,• <M111 p � p 28 ulvat wn FI t a ti.. lJ r rt vltS�iIn i� �? 9 f • D ptolt ana / IM1 p4' t. r Is Boys :Pine / o� Eakt. . Neck-'- k o L►gtit uogug­-- ri¢C 1 2 Sao Biological Services Program Qwwmw� FWS/OBS-80/51 September 1980 Atlantic Coast EcologicalInventory USER'S GUIDE jor AND INFORMATION BASE �IBFtARY ,. U.'- S. ENW= EDISON, H.. L 1 49,66 80/51 1 and Wildlife Service Department of the Interior Ww- Terrestrial Resources Terrestrial and biotic resources of this subsection are protected by numerous parks and management areas. a. Widespread species. Important bird concentration areas are scattered throughout the section and are identified below. Mammals are distributed evenly in the area, but occur in such limited numbers that their densities are not significant. b. Geographic inventory. Between grid references DR26 and CR67 are several shorebird and wading bird nesting areas as well as waterfowl migratory areas. The most significant portion of this interval is Muskeget Island (grid reference CR97) which supports shorebirds, marsh hawks, short -eared owls, and the only known population of beach meadow voles. This species of vole has been proposed as an endangered species. Between grid references CR56 and BR95 are other important shorebird and wading bird areas; several areas with osprey nests also are shown. A special interest area is Bird Island (grid reference CS51), which supports approximately 40 percent of the U.S. breeding population of roseate terns (900 pairs). The three largest colonies of this species represent approximately 95 percent of the breeding population. The next interval of importance (grid reference BR85) is the Block Island area. Because of its remoteness Block Island supports a variety of terrestrial species, including wading birds, shorebirds, migrating waterfowl and songbirds, and marsh hawks. The endangered peregrine falcon is a common visitor to Block Island during its migration. This island is one of the few areas the falcon is known to use regularly. Also, the only known population of the Block Island meadow vole is found on the island. This vole also has been proposed for inclusion on the Federal endangered species list. 5.3.2 Long Island Sound (Grid Reference BR55 to XA02) This subsection encompasses the Long Island Sound and adjacent shoreline of Connecticut and New York, as well as the northern shore of Long Island. The Long Island Sound estuary is a semi -enclosed body of water measuring 145 kilometers (90 miles) long and 24 kilometers (15 miles) wide. The sound opens to Block Island Sound and the Atlantic Ocean on the east, and is fed by the East River, a part of the Hudson estuary, on the west (figure 5). Long Island Sound is a moderately stratified estuary dominated by strong tidal currents and freshwater inflow on its northern side. Several rivers (the largest being the Connecticut River) drain into the sound from the north shore, but most of this water is rapidly exchanged with the Atlantic Ocean. The bays which separate the northern and southern tips of eastern Long Island, principally Flanders, Great Peconic,. Little Peconic, and Gardiners Bays, also are included as a part of this section. Aquatic Resources a. Widespread species. Throughout Long Island Sound, the occurrence of the major commercially and recreationally important organisms is dependent on sea- sonal changes in water temperature. Sessile invertebrates, such as bay scallops, RF oysters, and hard and soft clams, are located in beds throughout the Long Island Sound region. Oysters are one of the most valuable commercial fisheries in the Long Island Sound estuary. Several fish species are year-round residents, including the winter floun- der, one of the most abundant fish, tautog, and cunner. The latter two species are mainly fished for recreation. Coldwater species, such as cod and pollock, move into the sound from waters during the winter while more temperate water species, such as bluefish, scup, -summer flounder, striped bass, and weakfish, inhabit the area during the summer. Anadromous fish such as American shad blueback herrn alewif e, and the en�ere s ortnose sturgeon �n a it the soup an coastal tributaries during eir spawning migra ions. b. Geographic inventory. The eastern end of the Long Island Sound subsec- tion (grid reference BR55) provides winter habitat for cod and pollock popula- tions, which generally inhabit cold offshore bottom waters. This area represents the southernmost point where large numbers of pollock occur inshore. Cod move offshore in March and April and pollock leave in June. The Connecticut River (grid reference YA27) is a major anadromous fish spawning stream. The Federally endangered shortnose sturgeon migrates up this river; in 1977, the total adult population in the river was estimated at 450 fish. Alewife, American shad, rainbow smelt, and American tomcod also migrate up the Connecticut River to spawn. The Peconic-Gardiners Bay Complex (grid references YA03 to YA35) is one of the more important northern centers for concentrations of weakfish. Weakfish use this complex as a spawning, nursery, and feeding ground. Shellfish also are abundant in this complex; some of the major mid-Atlantic coast bay scallop beds are located in the shallows and eelgrass beds of this area. Hard clams and oysters also are abundant. Although other shallow water, hard bottom areas have important commercial oyster populations, Oyster Bay (grid reference XA23) is one of the more produc- tive areas. Much of the oyster fishery in Long Island Sound, including Oyster Bay, is maintained by hatchery seed production and intensive bed management. Terrestrial Resources a. Widespread species. The characteristic upland habitats on Long Island are the pitch pine and scrub oak forests and the extensive tidal wetlands which occur throughout the coastal areas. Several common wading bird and shorebird species inhabit the wetland areas during the spring and summer months. These species, and estimates of nesting pairs, include great black -backed gull (1,400 pairs), herring gull (5,400 pairs), common tern (3,100 pairs), least tern (1,400 pairs), roseate tern (800 pairs), black -crowned night heron (600 pairs), snowy egret (200 pairs), and glossy ibis (30 pairs). b. Geographic inventory. An especially important wildlife area of Long Island, between grid references YA15 and YA55, contains many species, including nesting wading birds, shorebirds, songbirds, and ospreys. During fall and early winter, many songbirds and wintering hawks reside near the sound. A majority of the great black -backed and herring gulls of the zone nest in this locality. In addition, the bog turtle, which is an endangered species in New York, breeds in this area. Peregrine falcons are known to frequent the area to the west (grid reference XA52) during migrations. In spring, northern Nassau County (grid reference XA12 to XA31) is the focal point for many migratory birds, especially songbirds; several raptors nest in the county on a seasonal basis. In winter, many ducks and geese remain in the bays and marshes. Osprey, an endangered species in New York, also nests in this area. 5.4 NEW YORK BIGHT (GRID REFERENCE BR55 TO WU00) This section encompasses the exposed outer coast from Montauk Point, New York, to Cape May, New Jersey, and the Hudson River. The New York Bight has been divided into three subsections: the South Shore of Long Island, the Hudson River, and the New Jersey Shore. 5.4.1 South Shore of Long Island (Grid Reference BR55 to WV98) The South Shore of Long Island, from Montauk Point on the east to Sea Gate on the west, is dominated by barrier islands which protect an extensive system of bays and marshes on their landward side. This system includes Jamaica, Great South, Moriches, and Shinnecock Bays. The biotic resources for this subsection are keyed geographically using north -south UTM grid swaths. Aquatic Resources a. Widespread species. The South Shore of Long Island is an extremely critical area for spawning and nursery grounds as well as beds for major commer- cial and recreational shellfish and finfish, such as hard clam, bay scallop, soft shell clam, Atlantic menhaden, weakfish, striped bass, winter and summer floun- der, and bluefish. Other fishery species are the surf clam, scup, Atlantic mackerel, and two coldwater species, cod and pollock, which move inshore during the summer. Species of special status which inhabit these coastal waters include six marine mammals, five sea turtles, and one fish (table 9). At the interface between the complex and the ocean, lobsters and mussels inhabit rocky areas. b. Geographic inventory. Cod and pollock generally are coldwater, offshore bottom species, but during the fall individual schools move inshore. Both species may remain through the winter; cod move offshore in March and April and pollock leave in June. Montauk Point (grid reference BR65) is the southernmost area where large numbers of adult pollock occur nearshore. The eastern portion of Long Island's South Shore, from Montauk Point to Moriches Inlet (grid reference BR65 to XA81), harbors an abundance of marine species, such as bluefish, striped bass, and black sea bass, which move inshore during the spring and summer. These species are not only of commercial value, but they also are of even greater recreational importance. Adult bluefish inhabit nearshore waters, but the eastern portion of the South Shore of Long Island is one of the- few places along the Atlantic coast where bluefish can be caught from shore. Striped bass occur and are harvested along the entire Long Island South Shore. However, after adults spawn during the spring in the Hudson River, their largest summer concentrations are along the eastern portion of the subsection. 36 60 lio do ien . I Rose: fit ORIENT -</STATE PARkC- 36 0 36 A __�on e Harbor /L' t ej -5 eix a st r ca d- TE *n e S as La in Ater ffidian NeLk N rth F 11f, A immTom S :1 -1' ye W ft- "Who - New 01� ldmlZgcdfg, 13 Matti NQ TI 14 7-6.' 149f, �60cdf, I f 178f ortrivill RTC) 19,woo �,V. 4d& 30 0 5 Gent ne 14BAciff, 5 1jj%702, 34 16 cdt, 177cdf R r 7,4(12� _':r��129cd "138cdf, Jam s orp. Gruat'poco 'Hollow 2S C9ASCIERCE P01 d 1 60cdf it: 1 4Zf,; 149 h, doV.- 459abdf;.. 1.77cdf, VQcd u u—tielk Wl� F E Rive ame Do v e rb epa amDt f506 Peconic River Ha rou J. T_ 7.5 -443h, 442h I nK Can c wa an Add 411111111, pans Plant b 161 ITT IV402 41 0"133f, 134f rt e c 295 184f\ y Radii wer.' 9 thumpton Cern West Tiana 9i Md, "V406h amp T 262abcdf, 66abedf, \04 6 d 67abcdf,"Ill"149abcd 141 Pine "I ib Neck— x0\dffi\ - 4 Spadaro Dr -4-402h,403h,412h 1000 b uogu ,j .0% UAW pt6n a 0 129cdf g, 138acdf, 147bcd 149a S a n 160cdf,177cdf N AO ch .Wer Oft ught -1-402h, a e �Aa ---I mas�c a cove rg62abcdf, 66abcdt, 67abcdf, 4111w 149abcdf X 062abcdf, 66abcdf, 67abedf, 41111"14710f, 149abcdf 9c -W402h,403h,412h 3 f, 160cAf 177cd 52abcdf k \SM1TiF(Hf4T-00UNTVF`Af1X--- cd,., j6abcdf, 67abcdf, cilf, 129bcdfg, 130 f, f, lbcdf, 149abcdf,- 14000 XA! YA -0 xv, YV 10 TERRESTRIAL ORGANISMS ► New York �VV Shown in BROWN: species with special status shown I � in FCD-iF! or (5) indicates species protected by Federal or State ! e¢islation (see text) SYMBOL SPECIES N. Y.—CONN.—N. J. � G[-�S�AT 4 PLANTS (301-350) 301 Eastern 4 95 302 spleenwort ort (S) (S) 303 Spider lily (S) 304 Pond bush (S) 1:250 000-scale 305 Watermdfod (S) 306 Hooded pitcher plant (S) Atlantic Coast 307 Tree 308 Prickly pear cactus (S) 309 Trailing arbutus (S) 310 Eastern bumelia 311 Pitcher plant 312 Baldcypress Ecological Inventory 313 Redbay 314 Seaside alder 315 Box huckleberry 316 Purple fringeless orchid 317 Pink lady's slipper 318 Ebony spleenwort (S) 319 Orchids (S) 320 Golden club (S) 321 Florida beargrass 322 East-coast coonti coontie 323 Fall-flowering ixia 324 Jackson-vine 325 Spoon-flower 326 Curtiss milkweed 327 Sea lavender 328 Hand fern 329 Needle palm 330 Yellow squirrel-banana 331 Beach creeper 332 Florida coontie 333 Four-petal pawpaw 334 Bird's nest spleenwort 335 Burrowing four-o'clock 336 Beach star 337 Silver palm 338 Dancing lady orchid 339 7amarindillo 340 Fuch's bromeliadiy" 341 Everglades peperomia 342 Buccaneer palm 343 Slender spleenwort 344 Pineland jacquemontia +_6 345 Mahogany mistletoe 346 Florida thatch !,u;'�: 347 Twisted air plant : 1. z xn�j'�- 348 Long's bittercress ; '' x^ti' 349 Venus's flytrap { INVERTEBRATES (351-400) 351 Monarch butterfly 352 Zebra butterfly BIRDS (401-600) SHOREBIRDS (401-430) 401 Shorebirds 402 Terns 403 Gulls 404 Forster's tern 405 Arctic tern 406 Least tern (S) 407 Roseate tern (S) 408 Common tern 409 Great black-backed gull 410 Herring gull Produced by 411 laughing gull t1T Os 412 Black skimmer (S) �� r 413 Turnsfories Plover 414 Plovers a� s U. S. FISH AND WILDLIFE ---_ 415 Piping plover SERVICE 416 American oystercatcher (S) �• � .7GI1Va�.+ Z WADING BIRDS (431-460) r 431 Wadingbirds r'�ua iN 1980 432 Herons 433 Egrets 434Rails — 435-' ibises.• - - 436 Bitterns AQUATIC ORGANISMS 437 Great blue heron (S) 438 Wood ibis (S) Shown in BLUE; species with special status shown 439 Anhinga in RED49 or (S) indicates species protected by 440 Little blue heron (S) Federal or State Legislation (see text) 441 Yellow-crowned night heron (S) SYMBOL SPECIES 442 Black-crowned night heron 443 Florida sandhill crane (S) ,/, PLANTS (1-50) 444 Louisiana heron (S) 1 1 Irish moss 445 Limpkin (S) 2 Rockweed 446 Roseate spoonbill (S) INVERTEBRATES (51-100) 447 Snowy egret (S) 448 Magnificent frigate-bird (S) 51 Crabs 449 Reddishegret (S) 52 Mussels 450 Clapper rail 53 Oysters d51 King-rail 54 Scallops 452 Virginia rail 55 Clams 453 Sora rail 56 Warms WATERFOWL (461-500) 57 Shrimp 461 Waterfowl 58 American lobster 462 Swans 59 Blue crab 463 Geese 60 Eastern oyster 464 Dabbling ducks 61 European oyster 465 Diving ducks 62 Bay scallop 466 Common eider 63 Deep-sea scallop 467 Harlequin duck 64 Calico scallop 468 Wood dunk 65 Surf clam r;r; Wo ,i 1- 462 Swans 463 Geese Dy Owd udo 60 Eastern oyster 64 Dabbhne ducx; !65 Diving 61 European oyster dUCkS =A6 Common eider 62 Bay scallop 63 Deep-sea scallop 467 Harlequin duck I 468 Wood duck 64 Calico scallop i169 Fulvous tree duck 65 Suri clam 66 Hard clam 470 Loons 471 Grebes 67 Soft shell clam I 172 Brant geese 68 Brackish -water clam 69 Bloodworm 473 Snow goose 474 Gadwall 70 Sandworm 475 Black duck RAPTORS 71 White shrimp 72 Brown shrimp (501-530) 73 Northern shrimp 501 Raptors 74 Rock crab 502 Owls 75 Jonah crab 503 Kites 76 Whelk 504 Hawks 77 Ocean quahog 505 Bald eagle (F) 78 Pink shrimp 506 Osprey (S) 79 Stone crab 507 Peregrine falcon (F) 80 Spiny lobster 508 Copper's hawk (S) « FISH (101-200) 509 Swallow-tailed kite 101 Sharks, skates, rays 510 Marsh hawk (S)102 Herring 511 Southeastern American kestrel tSl 103 Salmon and trout 512 Florida burrowing owl (S) 104 Catfish ,j SEABIRDS (531-550) 105 Cod J 531 Seabirds 106 Sunfish and bass 532 Petrels, shearwaters. and albatroses 107 Drum 108 Flatfish 533 Pelican and allies 534 Alcids 109 Longnose gar 535 Brown pelican (F) 110 Shortnose sturgeon (F) 536 Black guillemot 1I1 Atlantic sturgeon (S) 537 Leach's petrel 112 American eel 538 Razorbill 113 Blueback herring 539 Common puffin 114 Hickory shad 540 Double -crested cormorant 541 Gannet 115 Alewife 116 American shad (S) 542 Wilson's petrel 117 Atlantic menhaden 543 Northern phalarope 118 Atlantic herring 544 Audubon's Shearwater 119 Gizzard shad 545 Greater Shearwater 120 Tarpon 546 Shearwaters 121 Atlantic salmon 547 Petrels 122 White catfish 548 Jaegers 123 Channel catfish 549 Wh to pelican 124 Yellow bullhead SONGBIRDS ANO OTHERS (55l -6001 125 Brown bullhead 126 Flat bullhead 551 Songbirds and others 127 Sea catfish 552 Red -cockaded woodpecker (F) 128 White perch 553 Chachalaca 129 Striped bass 554 Bachman's warbler (F) lack sea Mass 555 Wild turkey 131 Redbreast sunfish 556 American woodcock 132 Warmouth 557 Pileated woodpecker 133 Bluegill 558 Swainson's warbler 134 Largemouth bass 559 Ruffed grouse 135 Black crappie 560 Bobwhite 136 Sheepshead 561 Mourning dove137 562 Warblers Spotted seatrout 563 Ring-necked pheasant 138 Weakfish Po 564 Bank swallow 140 Atlanticcroaker 565 Dusky seaside sparrow (F) 141 Southern kingfish 566 While -crowned pigeon (S) 142 Northern kingfish 7� REPTILES AND AMPHIBIANS (601-700) 143 Gulf kingfish 601 Eastern narrow -mouthed load (S) 144 Red drum 602 Eastern indigo snake (F) 145 Star drum 603 American alligator (F) 146 Black drum 604 Northern diamondback terrapin 147 Summer flounder 605 Amphibians ou ern flouncer 606 Greater siren 149 Winter flounder 607 Bog turtle (S)am _ wsmell 608 Gopher tortoise (S) 15l Atianhc tomrcd 609 Eastern tiger salamander (S) 152 Threadtin shad 610 Northern fence lizard 153 Carp 611 Five -lined skink 154 Atlantic mackerel 612 Map turtle 155 Chain pickerel 613 Plymouth red -bellied turtle (F) 156 White bass 614 Eastern diamondback rattlesnake 157 Northern puffer 615 Carolina gopher frog 158 Silver perch 616 Florida gopher frog (S) 159 Florida pompano 617 Atlantic salt marsh watersnake (F) 160 Bluefish 618 American crocodile (F) panic mackerel 619 Florida Keys mole skink (S) 162 Cobia I 620 Florida black -headed snake (S) 163 Mullet 621 Pine barrens tree frog (S) 164 White crappie 622 Northern pine snake (S) 165 Redear sunfish 623 Corn snake (S) 166 Smallmouth bass 624 Timber rattlesnake (S) 167 Yellow perch 625 Southern gray tree frog (S) 168 Pumpkinseed MAMMALS (701-800) 169 Atlantic halibut 701 Beaver 170 Atlantic cod 702 Whitetail deer 171 Pollock 172 Haddock 703 European fallow deer 704 Blackbeard Island deer 173 Hake 705 Opossum 174 Bluefin tuna 706 Marsh rabbit 175 Walleye 707 Rice rat 176 Northern pike 708 Raccoon 177 SCUD 709 St. Simon Island raccoon 7autog 710 Mink 711 River otter (F) an rc spa eiisfi 180 Bay anchovy 712 Feral hog 713 Feral cow 181 Butterfish 182 Little tunny 714 Cumberland Island pocket gopher 183 Atlantic bonito 184 Brown trout 715 Anastasia Island cotton mouse 185 Gunner 716 Aquatic furbearers 717 Black bear (S) 186 Yellowtail flounder 718 Bobcat 187 Gulf flounder 719 Eastern gray squirrel 720 Eastern fox squirrel 188 Pinfish 189 King mackerel 721 Eastern cottontail 722 Delmarva fox squirrel(F) 190 Pinfish 191 White grunt " r 723 Muskrat 724 Red fox 192 Tripletail 193 Ladyfish 725 oar, 194 Snook • j 721 cdstefn fox squarer Eastern cottontail - 722 f Delmarva fox squirrel (F) 723 Muskrat 724 Red fox 725 Bats 726 Gray fox 727 Striped skunk 728 Nutria 729 Longtail weasel 730 Colonial packet gopher (S) 731 Wild ponies 732 Sika deer ' 733 Beach meadow vole 734 Block Island meadow vole 735 Pallid beach mouse (S) 736 Sherman's fox squirrel (S) 737 Florida mouse (S) 738 Florida panther (F) 739 Goffs packet gopher (S) > 740 Key Largo wood rat (S) 741 Lower keys cotton rat (S) 742 Key Largo cotton mouse (S) HABITAT USE Shown in RED for species with special status. BLUE for aquatic organisms and BROWN for terrestrial organisms a Spawning ground f Sport fishingthunting area b Nursery g Migratory area c Commercial harvesting area It Nesting area d Adult concentration i Unusual distribution e Overwintering area ' or specimen 191 white grunt 192 Tripletad 193 Ladyfisn 194 Snook 195 Jack 196 Snapper 197 Grouper 198 Sailfish 199 Great barracuda 200 Maryland darter (F) i REPTILES AND AMPHIBIANS (201-250) 201 Green sea turtle (F) 202 Loggerhead sea turtle (F) 203 Hawksbill turtle (F) 204 Atlantic ridley turtle (F) 205 Leatherback turtle (F) MAMMALS (251-300) 251 Florida manatee (F) 252 Atlantic bottlenose dolphin 253 Pigmy sperm whale 254 Short -finned pilot whale 255 Harbor seal 256 Gray seal 257 Right whale (F) 258 Atlantic spotted dolphin Hi�fI salinity estuarine habitat (generally 16.5 to tarts per thousand); � arrows used for wide estuaries. Mid salinity estuarine habitat (generally a� ass e>• e. 5 to 16.5 parts per thousand). Low salinity estuarine habitat (generally 0.5 to 5 parts Per thousand) and tidal trahwatar. .•«.««............. Nan.tlAai hw.hr�r...i.,..�.....w ,..ter ._..._. LAND USE -LAND COVER SYMBOLS Study area (coastal zone boundary to three- \ mile limit)...................................................� � Marsh ...............�� \ Special land use areas, including refuges and wildlife management areas, parks and seashores; may be used in lieu of habitat Beach/Dunes.......... boundary.................................................... -x ry Subdivision of a special land use area into ,ter r, 2Y' ' Seas grasr more than one designation ,�•_•�• Swamp ........................... .t; 's-'• Reef ................. POINT AND AREA FEATURE SYMBOLS (shown in RED for species with special status; shown in BLUE for aquatic organisms; and shown in BROWN for terrestrial organisms) Localized concentration of species ............................. eonM General habitat boundary for indicated �• species; may be supaceded by special land use boundary .......................... ATLANTIC COAST ECOLOGICAL INVENTORY NEW YORK, N. Y. -CONN. -N. J. 1980 k 0ES-5 Scale 1:250,000 10 15 20 Statute Miles 5 0 , Q— 5 10 15 20 25 30 Kilometers 5 0 5 10 15 Nautical Miles TRANSVERSE MERCATOR PROJECTION BLACK NUMBERED LINES INDICATE THE 10.000 METER UNIVERSAL TRANSVERSE MERCATOR GRID, ZONE 18 FOR SALE BY U. S. GEOLOGICAL SURVEY, RESTON, WtGIMA 22092, OR DENVER, COLORADO 80225 NOTES SPECIES WITH SPECIAL STATUS Shortnose sturgeon (-ow110) is found in coastal waters depicted on the New York sheet and migrates up the Hudson River. American shad («116) is threatened in New Jersey. Bald eagle and peregrine falcon ( f 505.507) migrate along coastal areas depicted on the New York sheet. AQUATIC ORGANISMS Due to scale limitations, only representative estuarine and riverine systems are shown. Species that can be found from the shoreline to the three-mile limit depicted on -the New York sheet include: 0-110g.116g,258cdf.59de.65abcdf.0"1119,113g,115g. 117cd.129c df g.130cdf.138acdf. 139d.140d.142ad1.147b cdl, 149cdf. 15711.160cdl.173cdf.177c df.178f.183f.1851.186cdf. Generally includes the following species: or —116g. ! 59abcdef.Ow1119.112cdf.113g.115g.117cd.128cfg. 129cdf g.1301.138abcdf.139d.140d.142f.147bcdl.149bcdf.157f. 160cdf.177cdf. 178d1. Generally includes the following species: Q'116g. 1! 59bcf.,=4111g.112cdf.113g.115g.117bc.128bcfg, I29cdfg. 138bcf.139bd.140bd.149b,151bg,158bd. I60bcdl. I80abd. Species of importance in a particular river, creek, or sound are denoted on the map. TERRESTRIAL ORGANISMS During spring and fall migration many species of shorebirds, wading birds, raptors, seabirds, and songbirds ( '"rQi. ik 431. 501, i 531.551) concentrate at bays, inlets, harbors, and islands throughout Long Island Sound. Many species of geese, dabbling ducks, and diving ducks (9463.464.465) overwinter in the bays, inlets, and harbors depicted on the New York sheet. LOCATION DIAGRAM 78' 43' 4KV R QNS.I NE YOR L HrNK 18.4 K 18.6 ELMLAA• T SINE' aPT, E•NART. ORNK18-7 N-CONNEC'S�N �WILLIAN PORPENNSYLV NIAewNK18.10 T IJNK 18.12 VIR y1JIA I,'� WARE 8- 18.5 T E s Iseuar 38'78° T—Topographic map T/B—TopographiclBthymetnc map E—Ecological inventory map E'—Includes portion of Albany 6843' NK 19 t'� STO USETT I d+AOVI Ckl 7w T A� GF' GO 38° 68' NUS CORPORA TION PROJECT NOTES PROOECT NO.: Od, 9cbg-4S TAB*-rtc—.. .. DATE: ds `l PROJECT TITLE: SUL � ` � r— � CA ( A T ► © r, a -C o u l,i Ton oAj G ,9UJA lc-- COMMENTS: u )-p- I � -LeL& n c'r zAj2 � �,' Tzi -;4 -.K o rMe- 62572AZL5 A o2 /o C A 2,CQ `A - 721 S 7- S P6 ujA/; C'N lkILiIL 140:6/ -FTA- 72-L-41 GfiA ren/� -{Pd2 Tf/c_ (rQee ,&j&:Z �'°T/�/ �P I f�/L�40CA ,?,/ _ ,'L'571UU_ 124N!�j. -rHe- CT�,u�rir �U���-► d f Ti4/4- C.r.�, r aA44 i (a -p A J.6. 3s i 76 x0oLl- c") -t- GeM -5 DA i 3 NUS 085A REVISED 0483 NATIONAL WETLANDS INVENTORY UNITED STATES DEPARTMENT OF THE INTERIOR OF Tm Vm moiR t R«io t*,ALM. URVICE �.�«.+ ►n all�s.f � wwc.. ow w. N"Im r w.b.i ky IJ A —11,:9 t,)A j UJ-P-T-4AWIL):� Avj GWdsni& 30' .,lee '000� 51TE- OW. Ole 29 A AlW 10, 10 4M& jw cvtcbftw SON432.- lot club MOP ;k1 W I f WJ A YnA rl; iu M; le EZ85N RA&ut, s , _EZ/FLM - • Duck Pond([�"'�� / .;;• � � \ ,e Poin as-- /K Oi .� '• 400 �.o • s •J6 s (rE � fro. • ' 't. 57 y' \ ,PEM5A)L �- o c ,� afar">.I • � •O �. a EMN as a • - ' \ A \ Ph . mac^ ` Waterville \ v 0 40 a 100 swis POWZ CA %(i O \ AMA LN • � Ia{�aa•�t•iiOLOaKNIaYl1V aV. w•aMlt•��W. Or _IAt �' ;a .70 ___JP i2El _-' P A% - of .� \A SPECIAL NOTE This document was prepared primarily by stereoscopic analysis of high altitude aerial photographs. Wetlands were identified on the photographs based on vegetation, visible hydrology, and geography in accordance with Ciessitka- *m of Wetlands and Deep -water Hobltate of the United States IAn Operational Draft). Cowerdin, at al, 1977. The serial photographs typically reflect conditions during the specific year and season when they were taken. In addi- tion, there is a margin of error inherent in the use of the serial photographs. Thus, a detailed on the ground and historical analysis of a single site may result in a revision of the wetland boundaries established through photographic interpretation. In addition, some small wetlands end those obscured by dense forest cover may not be included on this document. Federal, State and kcal regulatory agencies with jurisdic- tion over wetlands may define and describe wetlands in a different manner than that used in this inventory. There is no attempt, in either the design or products of this inven- tory, to define the limits of proprietary jurisdiction of any Federal. State or local government or to establish the geographical scope of the reguistory programs of govern- ment agencies. Persons in tendkV to engage in activities in- volving modifications within or adjacent to wetland areas should Beek the advice of appropriate Federal, State or local aganci« concerning specified agency mgulatory progfOrm and proprietary pwiarictions that may dhct such activities. SYMBOLOGY EXAMPLE 8 SYSTEM SUBSYSTEM ,CLASS E2EM5N USCLASS, WATER REGIME IKON -WETLANDS) Pf orPKI FARMED WETLANDS CONTROLLED WATER REGIME WETLAND LEGEND Q — Primarily represente upWW areas, but may include unclaseIMW wooenole such as man -modified areas, non phowidentiflable areae end/or unintentional omissions. l e "1. - .., . G.C. NOTES TO THE USER • Wetlands which have been field examined are indicated on the map by an asterisk I*). • Dominance type (either vegetative or sedentary antmall can be added to the map by the interested user. • Additions or corrections to the wetlands information displayed on this map are solicited. Please forward such information to the address indicated._ • Some areas designated 11468, R4SBW, or R460i (intermittent streams) may not meet the dotinitionof wetlands. AERIAL PHOTOGRAPHY DATE: 3 / ISO SCALE: 1-80000 TYPE: 5—W—W DATE: SCALE: TYPE: DATE: / / SCALE: TYPE: M — MO I - subtUel Ile - NOCK E — ESTUAFAM t OW - OFEN WATT BOTTOM BOTTOM All AOUATIC WD OF - 11EEF L4*ne w be Na 1 e..«. . 1 i reFwl Ay 1 Cw.1 7 saLa 2 — Blesrttatl t Mwrrp^M V1IKYII 7 Waw, 7 MW AOUATIC KD IIF - IIUF Ft - FIAT so - STMrAIAM Ile - NOCRT shield M - MACHO" EM - EM am"T f5 SCIIULSNAUS FO - FOMSTED ----� 7 Wa"' ; 90"n 2 MM M NrwwFr• t Il .. r.•h/ •.N plimi um t D•Mmendft1w.M ivwpw� s D.n&m S DW"soft1w.N Ev�sh••^ s Dea*.an a t V.a.InW N11POW w w 6 &•4011 M•..pow" d... T re" T Ear. l e "1. - .., . G.C. NOTES TO THE USER • Wetlands which have been field examined are indicated on the map by an asterisk I*). • Dominance type (either vegetative or sedentary antmall can be added to the map by the interested user. • Additions or corrections to the wetlands information displayed on this map are solicited. Please forward such information to the address indicated._ • Some areas designated 11468, R4SBW, or R460i (intermittent streams) may not meet the dotinitionof wetlands. AERIAL PHOTOGRAPHY DATE: 3 / ISO SCALE: 1-80000 TYPE: 5—W—W DATE: SCALE: TYPE: DATE: / / SCALE: TYPE: M — MO I - subtUel Ile - NOCK lis - UNCONSOIIDATID OW - OFEN WATT BOTTOM BOTTOM All AOUATIC WD OF - 11EEF L4*ne w be Na 1 e..«. 1 GMM+Gn..I 1 i reFwl Ay 1 Cw.1 7 saLa MM t Mwrrp^M V1IKYII 7 Waw, 7 MW a W+w.+w f,Awraww • O-@ . ECOLOGICAL SYSTEM l.Mbr..t ♦I+MtrMeMwl CLAD E.ic1.w ECOLOGICAL SYSTEM no owwyow w cuka lei+� ECOLOGICAL SYSTEM •BBb%at �BIBwI CLAM Br•r ouA AL Il..i,rl[1S HAII ....ACA, —I 1485 TEL. 607-256-6520 shouio —1, UQ 91 ap—ito Stat- — l ;al Mna Mean eciti nevi «Y l------na Mud preprW N Wed ctWm that may affect such ectiAties. WETLAND LEGEN — PALUSTMW IM - 010" UB - UNCONBOUDATY BOTTOM BOTTOM Y - AQUATIC BED 14L - low - - N - NAT LK:1wN EM - EMEIIOENT !M - BCIIIJIVIN" ow - OrEN *An* Nl - N11rBT/D Ilntlww BMlrw 1 B.r�.m 1 C.MMI.iOrM 1 Br�wwBwrMW ! 4.Mw ! Yr ! Mi.1rBrK Ynnrr Q — Primarft represents upW1d area. but R 1 Br�MM.MOrrWr� DUN*~ —in--"-d- 4..wrl. A Ogws tl O �eNIPMO-lawmadKwE+A :l 0 11 111 Will Illoodb4orAd E�wwn w.�Mn Mw1�MA 4 MMA4wr Bw1M� unchwailled weNsrtds such a mat»rtodi d , • ryuwA Mw/rw ANMMI�I R — IWERINE photo -WNW Esbiaarm�d/ar wtit�w�gi I - TMMd - I+BMBr rT.Iw11Iw .1 - th*w t1wou" 4 - MMwwAnom • - 1M & a PWOO t mmv SM - i1f11BENTI tI ME1� ~ Y - AQUATIC BBD N - NAT a - 01MM� Y B110a - 6119001111111w -h P"4 wB� / w /lr 1 B � B 4w11 V- � I = E — ESTUAR NE • TM1rrM1T . i;V� subwapiwK Me" t — s,IMaw 4 OBri 2 — MMIwddW M - HOCK IA - UNCO MIOLIDATED BOTTOM BOTTOM OW - OMEN WATIN Y - AQUATIC KD Ki - Kw Utino— BMW- Y - ADUATIC MED M - 11110F R - NAT M - {TIIM11111110 BIIOIM a - w�AcHle" EY - Er11DENT M - Be' MIr/ Y.iNr 1 Wow1 /IM1Y*rwM 1 ~Imallmoll Y~ it EiE1n 1 w,a �� �8 1 C�� 0" e 1 tl BM - wMBMM w &* ftwo in wB mbalM t1Y owns"" WNW tir1L%q b.y.M Wn� Y Mr..11MMw �ynf ■ rB AIMIIIM �M BiMKI�K +M` ��w1 1 . Brw Mrli~D Fft���Bl1{ M j Kiw►Mlrrn �1 M.�M�MINB �.MY. M. eMMBEDIM/ ft - 9 1 — PALUSTMW IM - 010" UB - UNCONBOUDATY BOTTOM BOTTOM Y - AQUATIC BED 14L - low - - N - NAT LK:1wN EM - EMEIIOENT !M - BCIIIJIVIN" ow - OrEN *An* Nl - N11rBT/D Ilntlww BMlrw 1 B.r�.m 1 C.MMI.iOrM 1 Br�wwBwrMW ! 4.Mw ! Yr ! Mi.1rBrK Ynnrr 1 C.M1IHO'" 1 Mrs 1 1►r.Iry 1 BNRMwBB.1r1.q ! slow ! 1rt11.w ! plo— i W.A4M.M4 brNI1. 1 Br�MM.MOrrWr� DUN*~ —in--"-d- 4..wrl. A Ogws tl O �eNIPMO-lawmadKwE+A :l 0 11 111 Will Illoodb4orAd E�wwn w.�Mn Mw1�MA 4 MMA4wr Bw1M� {MYwow swomm� , • ryuwA Mw/rw ANMMI�I R — IWERINE I - TMMd - I+BMBr rT.Iw11Iw .1 - th*w t1wou" 4 - MMwwAnom • - 1M & a PWOO t mmv SM - i1f11BENTI tI ME1� ~ Y - AQUATIC BBD N - NAT a - 01MM� Y B110a - 6119001111111w -h P"4 wB� / w /lr 1 B � B 4w11 V- � I = p� • TM1rrM1T • lrLYwY N�rNw�r / Mr/ subwapiwK Me" 4 OBri 146K104119r • ewft • pB1�1 : v w IM41rrw IIMWwww �B e 1 tl BM - wMBMM w &* ftwo in wB mbalM t1Y owns"" WNW tir1L%q b.y.M Wn� Y Mr..11MMw �ynf ■ rB AIMIIIM �M BiMKI�K (1 � !. 7' '. j�f t ,.,M��Z, ',4-, �.i�•�.'I .:.17•jv.,,.,5l' 1'�.,.` �''.' �v ,4i, i^ V DATE: SCALE: TYPE: 1AND LEGEND esents upland areas, but may include 'stlands such as man -modified areae, ran 4blss are" and/or unintentional omissions. MODIFYING TERMS In order to mors edo"tely, describe wsttBnd and pustic habitats one of nr's of M10 war' rsgk"@. Vista' chemistry, soil, or spacial modifiers may be applied at the class or lower level in the hierarchy. The for modifier may also be applied to the ecological system. WATO 11lMr11I Wpm Clfiiiliiiiilm roe M - MARINE NWTMM TW larWarfor r FfeA wow sr i @rwF a.sl■dNwodd INVOWN frrewl.nl [ Aa•drrt B sed■wnl T10 t � ! � t CYwnn■u[r 1 FrwM ■ �ictg111 •d■r•aY J FI■oAed ! T ?le■IiI" I �Irrn■ � ��r 1 AA■IMo a tTltMl`t S A W=W■ner M I.O."d � IWe■idN WAS&1d Fd•A 4WPo bar..l wy90" somM awl mend lIN i+.� �M r r..rJ. u urwd.n wren. r �wnraF e'er Y 1►■sal.•.II . t - arrwr - M - 11OC[ us - UNCONSOLIDATEO BOTTOM As • AQUATIC 00 Ow - OF•N WATt1U OF - MtF 1Frrrrn Ba•ern AS - AQUATIC NO W - MEF FL - FLAT M IIpC[Y 204M•: MAr.0r10M1 tIJLSS IN - r KRUNT 1 Frro■rre IS sc"Is"" 1 Mor Nerid Ooaalrur FO - FOMSTED 1 Wood-Nd.od DocrMrnre 06406A 1 sodroce 1 CMMUOro.r 1 $Wbw pre AMI ! V 1 Car 1 CoBN■Rir■vr 7 Werw 7 •end 1 B.r..■. 1 Caawlard.r ! B■1laT/ 7 tIN @ 7 Md■ssrl•raa 7 Wood Iso.ed Evwp 7 Wedel-MFvN E.a�edn 7 Budbr sow � ! •tleeld°pIa Va■■u1■r 7 catch■ • IAdMw. WlwwSwa • Un►rrrw LAwrrprn • M■a • vopldlod rsllar�Irwole NalFwwlan i WeedDeads 1•o. W 11-9 n ` Nodrrra.M @wrpMn rrt • vq■neda New errs base • o. Nwyrruw • Ner�AE..N�■ • D«�rw. • thf+wrd■d e A11.aN«.d T Ewer•+` T @..� L — LACUGTM* : - tttta/ef 6d@" sub&""= I — UHWMWs Mt - [OC[ LN UNCONSMIDAT@O Ow- UFEN WATU4 /N - I Oc[ UB UNCO095OCIDATE0 115 - IIOC[Y FL FLAt SNORE M MACHSM EM OW - OF•N WATSar tAMaO•NT he'r'o §Gn" CLASS BOTTOM BOTTOM As - AQUATIC NO Unene`■n 001a, BOTTOM BOTTOM As AQUATIC s!0 1 BiFWwS 1 CaeaorOr■.eI 1 &A—pnl Ayr 1 Bedret► 1 CeM101COW.r 1 fr�pre AIB' 1 CeM4`Cre.r 1 Beare& ! se"w' 1 Cebb*,Crwtil J N■n/waadel ! Sona 7 Narow re.w Nsr�■.uM■M B■1FbM ! Becher ! Bona 7 suYwasF^I Vo1cuW 7 so.,a.r 7 bent 7 Wrd ! Mw 7 Br■sdrll 1 Mr . Brwd re.M Ner�ermMrN 7 Mrd • O'ge— 7 iuBnrrpre Mea • FNrYIB1oo.■d • Orarerc ` F 1■o.M VOONNed Henwr •LMarrrw 1q::=W l • Voptord Nen rarer 1 thaw■ sr 7 Leaner. 4■le■a MODIFYING TERMS In order to mors edo"tely, describe wsttBnd and pustic habitats one of nr's of M10 war' rsgk"@. Vista' chemistry, soil, or spacial modifiers may be applied at the class or lower level in the hierarchy. The for modifier may also be applied to the ecological system. WATO 11lMr11I Wpm Clfiiiliiiiilm roe MECIAL M00111Efn NWTMM TW larWarfor r FfeA wow so i @rwF a.sl■dNwodd INVOWN frrewl.nl [ Aa•drrt B sed■wnl T10 t � ! � t CYwnn■u[r 1 FrwM ■ �ictg111 •d■r•aY J FI■oAed ! T ?le■IiI" I �Irrn■ � ��r 1 AA■IMo S A W=W■ner M I.O."d � IWe■idN WAS&1d Fd•A 4WPo bar..l wy90" somM awl mend lIN i+.� �M r r..rJ. u urwd.n wren. r �wnraF e'er Y 1►■sal.•.II . • � go" topes' Fgiwa abedhers fount an thle leY•Iad, but rest fe-W In ONdBBsNieatien system, may M ab" 1FSFtl tM *00rased soewee. nl. I. x.:'11. �. .k1 �.1,':ti4ry �'a'';�y ,. Iti; Hyl ';�;'+Y' �' fi; ! ,■a_ ertrctr�'�—,r; -,�' B ! = .. r STATE.I��� y;: RAAit ast J wata C�a # Qie i; LL ASR• "Lyrt+g: •r5r `i a. Sao 44 F f. r : t it �f .•� t, R ~ Lo Ws �! —`� - A7 '� q•riw3r• •?UWwNEM[M.-�jfe}Qe:. CIO '314. r, Qld. ° y .• S°• .�� "i3 •GIok7 lice, . .1 r.= a ti eE All , S_.,M? i c • fw :.t rii/iCH - • .Y. ~•,r - • no ;n:axJ lieMs ; (SF i3J TE PARR• -' _ __�T - ._ . - j.� �' ~}?' OTF,_ iS tb.•lo,an•r-. .. �NrSf'S1 fJJ..rp 7 i 0 - �- i1 �•� J ION S 52-046ata Fr, S�DQ�nt of AQrtcwtwe. �� '{` `I _.1. - _ �� `' �lf1M►1SLIN0 r _ __ 1R 580 �� SW 456 �5 �� `" :,yJ- r ...tet •.r,.... 73 f c>at Ki)< - �. ORIENT BEACH SW 32-062 ' `i•it• = .. } r !'TATE PARK' SW 52 _ °L1EAtt+onstr S L.Mkoltt. !J-- 16 $ r i it . 550 ate•r. .'ra \a!! f 32'060 455 !d FE 018 `/ `rte 3 -050 �\ J ;ytlr • � itt•r � � � ` a .,=q . •t,r, • + • a dGtu $W 32'042nTNeR WrAw yl IiMNrtE r'u ne, {� �' 1 01 M w R ` SM A ' 740,. s rte., •iMll_ ,. 1a _�lt3ttO0QfEE�Mt.1r.�lt ;ty.-• 72'�7C'. 13 ■ s SIGNIFICANT HABITAT OVERLAY_ MW ttAtii74r•e f _ _ NEW YORK STATE DEPARTMENT'OF ENVIRON DIVISION OF FISH AISWt' T�~�; ♦ r"� '. .. • .. • , lA�- ' � � � �. ia6Yl.lttN• Mrefr:,�T• i- . BUREAU OF WILDLIFE' -- +� i< r>rMwB�w�lUrfeRiiw� jj Ic. t.w w...fttnla� ree T.e.w trMlr►.: `., . ' i:'• �' ..� tr,�nletnlftetrea.•tas.w...; , �. PREPARED FOR: SIGNIFICANT HABITAT UN _,. f`•; r. rr6 tt WILDUFE RESOURCES_ C DELMAR,,'N9�'�Wr YORK I.S y ' ' ,1.-! .,-: .•- • 6AAMi.� rdy �iv[�-Ntt _.. .,, •a:�' - ii _. 43\ i .,rpt. . ,r,+M.... ...,...wr.+ ♦.a 18/457—SM _``- ■�..,.,.w.• .rte..: t ' PREPARED BY: HABITAT INVENTORY ,.:�:-=s..: � 1FfiK 4l�.FeW.if��r`�. `''� 5• _ r °:•.:'Tiz�i .. _...., a-_=,15i:�-k., .:. ...4n:++t�+:_�xL_v.�}.. ."�'��c':ji���::,: .-...uw.*+•�,�n. a"`.. _ . ...^ui. _, <v � • ° rr.sl ..,n 3 ' �-" .tet d z • � •. _ 'mow �•UL . 7 ■ I � , •'o klo 41b .�..�, 15' b— ' °' Ci1ltecs �:. •., - - - •r. •-,0 1 , s 1 it ;!1. � , 9 est{ Haverstrs Z !f: volerO- ventkaw rs Lu A i I ack at a 455. Y / � • .r � l° � �' ,, 16 ' ♦ Ion" View- _ ! Ui' 1 •i :1 r.► 16 n•MuOsan ,r t•a. Of wirer c 43 I err M ,k• a r••• � •.l fw 9t a Irvin .i.ijrALLMArt t I / �� • •, Sip MTM IIs - ... -•er y3iAT6 PAik•i ,� • a, 'L�' sdo/ s s 41, '00 i. 200000 f e ::.:C:lttt{ 1.. d3• 2 00000 F L tfit-t Li.i 30, _ �11R � o w x a/y�.aL I ,./- M�tS +OAn :• •T7 ,f1 w raSv •01rA C,t'► II' �w L• EGE •^�•t' �D1t��,•i'J"'t•'+�'7�r��rI�IM.T�'!•A�R711. ._. '.Ay :Xx'. ' `) .r. ';H 9^` ena:rs 1'1JL:• = 2 o.qul)LA1F'.; t'l.Ai.F.`i n ..�.. an •1► . ...n ;,', • �tGl�tfleANT`•'!� �t;�, _tiµ �.....__. -- . BOSTON 'i S : f .. Q, RiC,�HN �ND f r .. „• •�•,.� r,b" St6MFrRiGiAf11'i '•iiR�r�ll(ILDLIFE AND PLANS;.',:.:rxy.maa RIO TON 1• .1. 't'••11st.•car ..,reCnawS WILD0 > .. _..`_.�... �`� a ItRm•r�., .. (.:r,) • G.t1h'} p1 (.:)n I'.g�t„t11 Lcx7'!: •• ate .•:'rt•V dif AieA tI —TI' an.,� M•���M•�•i+i� a'WFE'l T,1ALXY`I9*INIFICANTFOR PLANTa�-.uR ,•.eo�a�..:•l. rt ... .,. . •t,. r'J�It,- ::;•,tmi �sIAcw11r1".r,•t �q+4. + n..tr ate.,,-+c.•t •isl'�►�_ ":F ` "° IGNI` tCA il'f"FOR - W ILDLlF�'. .�� �.r�� �_ •.i.r COTOTHER fe-g. UNIQUE GEOLOGICAL FOR , 4.580 458 f an \. 4. '� _ �� - 1 :L,; _ • ttawan' -� _ <'i - WARtlmes? MEM Qfgw. ST PK _ DQ Ai •Ciia1M• IACw raOtr.t b tpdt'\ +mak SwctrClih a isOsa •• Buck. - wt• s 'Drew • • Poenr now e �S Beach 0• e'M A Senda '. )AAtlp • Lnton w �4:emrr.,tr •• �# aeach -/ Fisherv, ;, • e wood litsb)ts f_ r.ra.�r,, -. - - - _ I' pT 457 7� E PARK i - rQ- _ •\\i _. bp :• + t - - - oa' - US Deo•rtm••t o, AEriculttom lile 560 •rent fk11n1�.. ` � ,.pA ._� .•.__ ORIENT PEACH �itSlATE PARR'- �' - �i k AI., Z Ao ..#�, � l , i�, a%` 1 ;•a . •. • '��_yp lit f6 ' �oLiagMtlrrp f .;n1/DIlmS lorlYaitl�. - � b. teas i rstmqm t ng telt ? -.• (• •idatone Far ' r �'' t`ndur# �IeGa ... �/ , � w _ .l -•.... - _ 39 1 -SGisE vK - i Sri ^ • .. 4�,} ' �FdT 4 � ,.y,+.x t�vNmn .0 ..a� �- :.eel ,1 '�'�� r.r Z �a�Atr T� -��_.�. J, lyNwR 8 T Bmms Nol 41.00' F.IQ0.000 FEET JN C.EPMJ- _ ... IS.- IZW. �rlr•«.a •u r• w RAST w•r/N}M • lam. - [A1T+raaY�urf • rrN SIGNIFICANT HABITAT- OVERLAY - - iiAt:::2A Gt To �i.• NEW YORK STATE DEPARTMENT OF ENVIRONMrAl- (XVISIC4 OF FISH ANC WILT D(� _....�� titsl XB { ya r c«�•ragtttearrwroUlf QWREAU OF WIDUIrE { _i �o Ii awl.twr.rwfsrw•r+.fr r �•� _ , j ; Hr YN sow 01111111 11• M boom' _ - VfA i�1�blMiM 11�f71tM rMwR . c PREPARED FOR: SIGNIFICANT HABITAT UNI g 0646 it t «l• u wow; �_..r N&LIFE RESOURCES ffilt�tf MAT } aaaft as�rar aalU tl�atalF f _ OELrAfM,NEW 1fORK t 2-100 ' M .�; •y 'l L �Z Ulm e1 sATR WOW t KPIN M 'tM P jVN •, f��{ `Y- N: =J ., AS' • ka South<r-- olo! n i paugwn Shore End • 3f - rno rns 9-, r4'.1ra�i1al 10 is, M 4W�ta Wt" 0- 5 IO is 20 211 30 Kit wn-v, DA DEER CONCENTRATION MOPAWFEET MTH SUPPLEMENTARY CONTOUR'S AT 50 FOOT INTERVALS EXCLUDED AREA rRANSVERSE MERCATOR PROJECTION FOR &ftL, BY U.S. OWLOGWAL SUIrM. RMTQN. VIAMIA 220 1 7)j;v;jMFmWJFbint Beach. VE* GAHM ST FIL Walnut Beach bone I Nam b k Rock LOW% kFIELD Sam Farms WAND (P 050 —410 ale BIG r4'.1ra�i1al 10 is, M 4W�ta Wt" 0- 5 IO is 20 211 30 Kit wn-v, DA DEER CONCENTRATION MOPAWFEET MTH SUPPLEMENTARY CONTOUR'S AT 50 FOOT INTERVALS EXCLUDED AREA rRANSVERSE MERCATOR PROJECTION FOR &ftL, BY U.S. OWLOGWAL SUIrM. RMTQN. VIAMIA 220 1 VON m ��IpD Bp 1\� f.r—c Jr "rOR/YL P M/ trA"~ ARCA • LO ArmAi. Q o �w. r :n pfsf L c �L' �Vc �ALII MIAJf �Yr � v ROAD O � �0 a — � ,VauccEs o /ta♦ �— oc �wff" ecor % v 0 C".+r 1A.,.1 au F«t LEGEND for Sm.wr------- i -- YII I.SaLD d�rT--- VdraHyfr.n} 18-N �c � DAN` SAV r _ - E V J �� nnTT 00 � r 0 rl a 1 3 i V : SUFFOLK COUNTY WATER AUTHORITY WESTHAMPTON D15TRICT Low ZONE 3• MATTITUCK T"NSTR B HOLD NOV.2Ir1/98 18-0 DISTRIBUTION SYSTEM Ar. s. rslic• NUS CORPORATION AND SUBSIDIARIES TELECON NOTE CONTROL NO.: DATE: DISTRIBUTION: �-'�7 TIME: BETWEEN: n AyAl v` T Q e/iVl AND: U OF: oi.vN J S ���• Ou�X `37'g� PHONE: II ll 1 / 15/ C� I -76 5-- 31 i4d (NUS) DISCUSSION: J _f f it �, �T�Y K.) "A i n 5� /�n/ iyS %r� rY) %�i�( % �. A,) V4�- 77V,Aw 4A e ACTION ITEMS: 1nl�<1911 nua wi nerneu uwa NUS CORPORATION AND SUBSIDIARIES CONTROL NO.: DATE: o�. Lloo$ DISTRIBUTION: nj� 2/a s/ 7 TELECON NOTE TIME: ys� BETWEEN: AND: ^/ C° !� p Op:PHONE: /•, ( j pQ `5�h 7%^ I % 4 A (NUS) DISCUSSION: l. Ou A -I_, C.- Q/vr^ %�✓P . y n lv Q Y� /.(/ C%I `C �/�P� -4 h�A Y� 1 �J �� Tye - AV C -,g Co� % P R , en r'3 7 Iq "/ Te f /-4e, < i,meT il,, , 77i/e sv� 4i'% C) be �e -IlP V Ane /"u i To1 ACTION ITEMS: mw3 us/ ncvl]cw u"3 AeroGraphics Corp. Precision Aerial Photography P.O. Box 248 Bohemia, NY 11716 (516) 589.6045 DATE OF PIIOTOGIZAPFIy Z _�✓ EXPOSURE —�cl "PROX. SCALE:�— NUS PHOTO I,D, SITE NAME: 59"tficx SGL LOCATION: our-,Ocx TDD DATE: SCALE: SOURCE: �G � r .r :Y� ��,� ', �, >s,.,�`✓� •. -�t •,i 'ter,, �.: � `l�-A'� ` 1•, mac.• � -_� •1' "' �,�;., ;eft%,', ,n, .. �', ,��• 1 \ it ti � y • � • �. ` �i•�'•:. fit' e�. / ,,T •ice' � �+ty�'w?a,'�,� _ �'' '\ 0. ,1 1 \•\', •k;�� ,�i .;� t. .'��y:� ti' moi" Y •!� zv• '���� 'f"•r��'� 7, - x,• r .f��I\.` J ', i 1 1� '�`vt�J• Ifi �/��� .. r,':21 _ `\ OF • r ,-'• �'' r•s • .•1';%,r, r � r/'r � �,.i „ �n . s"�� L�p�l�� 'i�' ) ;''`f - " : f„ '; .�y�• �'� .raw .-':� `��•f^ �.`s - - � \ ����,� f � V OM1' � 1 � .. '•, t #' . '. ... - ✓ � .✓� . .�- s'�```�. ..� � '' .���`. ,i •1• �`�„'� �I ...5��"Y����rEar.?• .v"°� .rr ,�- �.'+'�•.�r" .• 7�..•.�,/. �.'/ ~ •�41c1 LEVEL: REGI(Ui. J2 U.S. EPA SUPERFUND PROGRAM PAGE: 452 SELECTION: INTEGRATED RUN DATE: 03/06/91 SEQUENCE: REG, ST, SITE NAME ** C E R C L I S ** RUN TIME: 16:00:09 LIST -4: SITE ALIAS LOCATION LISTING VERSION: 1 REGION: 02 SITE/ALIAS NAME STREET ALIAS CITY STATE ZIP SEQ. NAME FED EPA ID COUNTY NAME COUNTY CODE #' SOURCE FAC NYD025597048 SOUTHERN CONTAINER EPA N 140 WEST INDUSTRY COURT DEER PARK NY 11729 SUFFOLK 103 NYD980762603 SOUTHOLD LF EPA N NORTH RD - RTE 27 CUTCHOGUE NY 11935 SUFFOLK 103 NYD986914547 SOUTHWEST ONEIDA COUNTY LANDFILL (SWOCO) N HATALLA ROAD BOX 17 AUGUSTA NY 13425 ONEIDA 065 NYD000848440 SPAULDING FIBRE CO HWDMS N 310 WHEELER ST TONAWANDA NY 14150 ERIE 029 SPAULDING FIBRE 3 01 SPAULDING FIBRE 2 02 NYD057982993 SPECIAL METALS CORP NOT1S N WILLOWBROOK AVE DUNKIRK NY 14048. CHAUTAUQUA 013 NYD002241669 SPECIAL METALS CORP HWDMS N MIDDLE SETTLEMENT RD NEW HARTFORD NY 13413 ONEIDA 065 SPECIAL METALS CORP 01 ONEIDA NY NYD980641658 SPECTRAGRAPHICS D BRAYTON COURT COMMACK NY 11725 SUFFOLK 103 y ♦.il.Rl-a,•.it NEW YORK Congressional District Identification -Continued Table 1A. COUNTY SUBDIVISIONS.- Continued mmm ,:. a .•,�+1 `JI�.I r1Cl )YSTER BAYTOWN . . . . . . . NASSAJ 7,4 -TrNE To AN . . . . . . . H11Nraxii.,Y . . . . , . , , . . . .2S �M0 TORN. . . . OSREGO .29 Y R A TOWN. . . . . . WAY `It. . . . . . . . . . . . ,29 ' L:A TOWN. . . . . . . . JEFFE iSON, .26 =ANIS TOWN. . . . . . . . .."ILA .e': =Aa ISM TOWN . . . OiAEGO .29 SriVILLE TUAN. ST. LAWRENCE . . . . . . . . . . .26 = A TOWN. M.)!IMOE . . . . . . . . . . . . . .3'I ' EASON TOWN. , . . . . . . . . . PJTNAV . . . . . . . . . . . . . .21 'AVILION TO0 'ENE SEE..3V =A aLING TOWN. . . . . . . . . UITCHESS . . . . . . ,21 •')AM TOWNWN . . . . , . . . AESi, , CHESTEH. . . .2u RO-E TOGENESES. ,3u ILETON TORN. . . . . . . . . . . NIAGAPA. . . . . . . . . . . . . .37 :IELU TOWN. . . . . . . . . . . . NONROL . . . . . . . . . . .G4 .E.IPTON 10WH . . . . . . . . . . . M.f:a0E . . . . . . . . . .30 'E4!TY TUWN. of YU.11 NG, . . . . . . . . . . .31 IYSPU RG TOWN CATTARAUGUS, .34 IA TOWN . . . . CATTARAUGUS. • ,31 'h TUAN. . . . . . . . FAIL TO!1 'Eall TORN q1NTUN. .26 'ETFRSRURU TOWN HENCSELAER . . . . . . . . . . . .24 1.AASALIA TOWN. . . . . . . . . . CHLNLNGO . . . . . . . . . . . . .25 •PS T0.1.4 . . . . . . ONTARIO . . . . . . . . . . . . . .31 .AL)ELPHIA TOWII . . . . . . . . . JEFFLNSU:A. . . . . . . . . . . . ...(• IPSTnWN TOWN. P11TNAM , . , . . . . . . .2L =IFRCEFIELD T0" . Sr. LAW11i'ICE . . . . . . . . . . .26 -IFR EPOt1T TOWN ST. LAAHEICI .%t W r%VIHIi, .31 TOr:I LF.n IS. C.; NEr TORI u:24 E PLAINS TOYN. U•1TrMESS .ITCH I" TOA•. . . . . . . . . . . . ir. LAARQUI t . . . . . . . . . . .26 °ITCHER TORM. . . . . . . . . . . CtiE•7AN60 . . . . . . . . . . . . .29 -ITTSFIELO TOW4 . . . . . . . . . . OTSEGJ . . . . . . . . . . . . . .25 TSFOH;r TURN. . . . . . . . . . . M•)!IROE . . . . . . . . .1u TSTOaN TO,N. RENSSELAER , . . . . . . . .24 INFIELD TC-; UrSEGO ,25 SLAT TEKILL TORN . . . . . . ULSTER .29 PLATTSBURGH TOWN. . . . . . . . . . CL14TON. . . . . . . . . . . . . .21: ASANT VALLEY T06 -N. . . OTITCMESS.24 '40UTr7 TOWN CnENANGO . . . •2c STENKILL TOWN. RENSSELAER . . . . . . . . . . . .24 �VLAIIO TOWN CHA,jTAUOJA . . . . .34 =OMFRE7 T0KN. CHAUTAUQUA . . . . .34 '1PFY T1W11 Ui10NDAGA .27 ASPATUf.K 111D,RE5. SUFFOLK, . • • ' • ,11 ITAGE TJAN. . . . . . LIVINGSTON , . . . . . . . ITER TOWN NIA.ARA. . . . . . . . .32 'OPTLAN0 TOWn . . . . . . . . . . . CHAUTAUQUA . . . . . . . . . .34 CATTARAUGUS, .34 'o r0A" E TOFN. ST. LAWRENCE . . . . • • • ,26 rSO4M TORN. 34 rTER TORN YATES. . . . . . ,13HKEEPSIE TOWN . . . . . . DUTCHESS . . . . . . .21 _JND RIDGE TOWN. . . . . • . . . . .ESTCMESTER. . . . . . . . . . . .21 =RATISRURG TORN SIEUOEN. . . . . . . . . . . . . .34 GNEENE •24 "'t TTSV ILLS TOWN. • • • FILE TOWN . . . CORTLAND . . . . . . . . . . . . .25 ESTO:, TORN. CHENANGO . . . . . . . . .25 iNCLTOIIN TOWN SCHENECTADY. . . . . . . . .27 PHOVIOENCErORN . . . . . . . 5 "ATOGA . . . . . . . . . . . . .24 -ULTENEY TaA14 STTIIIYEN .14 ITNAM TORN .24 ITNAM VALLEY TOWN. . . °"PUTNAN . . • . . . •21 1FEN5RuRY TORN . . . fANREN:•. .24 iAVAPU T1,r11 . IIICILAND' . . . . . . . . . . . .22 RANOOLPH TOWN , , . • . CATTARAUGUS. . . . . ,34 ARTHSONE TOWN . . . . . . . . . . . STEUBEN. . . . . . . .34 AJlNG TORNSCHUYLER., .34 . DFIELD TOWN . . . . . JSWEGO . . . . . . . . . . . . . .29 .. D HOOK TOWN . . . DUTCHESS . . . . . . . . . . . . .24 RED HOU SF TOWN. . . . CATTARAUGUS• . . . . . . . . . . .34 REMSEN TOWN ONEIDA . . . .25 .NSSELAERVILLE TORN. ALBANY . . . . .23 i1NF8ECK TO,? • . . . . . . DUTCHESS . . . . . . . . . . . . .29 ICHFIELDTOWN• OTSEGO .25 RICHi0AD TOWN TIOGA. .2B RICHLAND TOWN . . . . . . OSWEGO . . . . . . . . . . . .29 RICHMOND TOWN ONTARIO• . . . . . . . . . . .31 1CHMONDVILLE TOAN. . . . SCHOHARIE. . . . . . . . . . . . .2S R IOGLIIAY TUAN RIGA TOWII RIPLLY TOWN . . . . . . . . . . H(VLRHEAO I"WN. HOCHLSTER TO. HUCKLANCI TUWII . . . . . . . Ir •7U MAN TVWN H1)HULUS TOhN. . . . . . . . . . . . R1)OT TORN ROSE TOt1 RUiEuuuN (DAN HOSFNOALL TOWN, ROSSIE TOWN N. . . ROTTtHII..M TUKI1• . , . . . . , . HUx BURY T(,MN. . . . . . . . . . . . HJYALI•)R 10R11 . . . . . . . . . HUSH TOWN , . . . . . . . . . . H,ISP.I-CH11 rcxN . . . . . . . . . . . RI15bLLL TGWU. . . • . . . HUS, IA TUWI. • . . . . . . RYE TO 1 , AHMAIIU• r0.N , , . . . . . . ST, Jf•HNSVILLE TURN . . . . . . . . Sr, hEuIS INL,hES.. . . . . . . . . :LAMANCATOl'I •.. S..LEM TUWt1. . . . . . . . . . . . . SALINA TUPI. . . . . . . . . . . . . SALISI'Illry TURN• SAND IArt TOWN. SANDY L4LLr TUAN. SANFOHO TOWN. SANGEPFIF.LU TUW:+. . . . . . . . . SL4TA CL.ARA IUWII. . . . . . . . . . ,,ARANAC TORI .. . . . . . . . . . . . SAn ATOUA IOWN SARnIh IA IC•AN SAUUENTILSTOWN SAVANN An TURN . . . . . , , , . , SCAMSUALL TORN., . . . . . . . . . . SCHAUHTiCUr.E TOW!' . . . . . . . . . SCHODACK TORN SCHOHA?fE TORN. . SCHRUFPPEL TOWN . . . . . . . . . . SCHNOON TOWN. . . . . . . . . . . . SCHUYLLR 1UWN . SCHUYLEK FALLS TOWN . 1 C10 TUrt. . SCIPIO TORN SCOTT TOWN . . . . . . . . . . . . . SCRIBATOWN SF.MPRON 10S TOWN SENLCA TOWI1 . . . . . . . . . . SENLCA FALLS TOWN SENNETT TOKN. . . ORL t ANS. rt IUNhOL . 7C Cr,LUTA•nI�!L . . . . . . .1V . . . . . . . . . t LSI Ell . . . . . . . . . . . . . ..e _UI.LIV•AI: JtFFE,'SJt:, '6 SEhLC+ . . . . . . . . . . . .. . . . . . . . . . . . MAYNE. . . . . . . . . . . . . . .74 ITStl tILSTFH c ST. LAAHt KLE , . . . . . . . . '6 cCntJACTADY. IL L 40,111L t IAU:h A. . 1G F•�r.hot . so tLI.t GA11Y . . . . . . . . . . .14 IT. L:RHtNLL . . . . . . . . . . .70 tEHKIHEH . . . . . . . . . . . . .•'6 SERAMO TOWN . . SHANUAAENTURN. SIIAMUh TOWW. SHAWANUUI1K TORN . . . . . . . . . SHELBY TOWN . . . . . . . . . . . SA'L'ONTUWN. . SHELTEII ISLANn TOrN . SHERBURNE TOWN. SHEhIDAN IOWh SHERMAN TOWN. . . . . . . . . . . . SIIINNEL'OLK INn.MLS. . . . . . . . . SIDNEY TOWN . . . . . . . . . . . SKANEATELES TOWN. . . . . SMITHFIELD TOWN . . . . . 51/1THT00h TOWN. . . . . . . . . . . SMTTMVILLE TORN . . . . . . . . . . SMYNNA TORN . . . . . . • • . . . . SOOUS TOWN . . . . . . . . . . . . . SOLON TORN. . SOMERS TOWN . . . . SOMERSLT IUWN . . . . . . . . . SOUTHAMPTON TOWN. . . . . . . . . . SOUTH BRISTOL TORN. . . . . . . . . SOUTHEAST TOWN. SOUTHOLD TOWN . . JtI-I-th;ul., . . . . . . . . . • O .E`, TCHt Sit 11. :O I.Gr:TGGhEHY . . . . . . . F11-1,1(LIN . . . . . . . . . . . . .'t L..T T Ah AU'Al', .7r 1A-INuVa, , . . . . , . . . . ;4 rN11NUA,;A . . . . . . . . . . . 77 HtHKIPLH �.. .76 +L•1SSt LAYn CNt IUA , . . . . . . F'w..1Kl IN • • • f • .76, CL NITON . . . . . . . . . . . . .26 FN1L .Tl UL+TF.H . . . . . . . . . . . .`'c R1.yhE. ?() AE:TCnES(tn, .20 FLI:S�EL4EH 24 hEt;SSELAEh .74 SCnOHAM I E. . . . . . . . 25 . OShEGO . . . . . . . . . . . . . .79 FSiEx. . . . . . . . . . . . . . .76 I.LrKIMFh !0 CLINTON. .76 ALLEGANY . . . . .34 CAYUGA . . . .79 CUATLA . . . . . . . . . . . . .25 r•5ALG0 . . . . . . . . . . . . ;4 CAYUGA . . . . . . . . . . . . .2i ONTARIO . . . . . . . . . . . . . . 31 SLr.ECA . . . . . . . . . . . . . .29 CAYUGA . . . . . . . . . . . . . .29 CCII)HARIE. . . . . . . . . . . . .?5 I'LSTER . . . . . . .7d SCMOMAHIE. . . . . . . .25 L ULSTER . . . . . . . . . . . ..2R (,(LEANS• . . . . . . . . . . . . •72 V .. . . . . . . . . . . . . . 71 SUrFOLK. . . . . . . . . . . . 1 CMENANGJ . . . . . . . . . . . .25 CHAUTAUQUA ,34 CH+UTAIIOUA .3V SUI -F OL K. . . . . . . . . . . . l DELAraHE . . . . . . . . . . . . .75 ONONOAUA . . . . . . . . . .77 NAU l SON. 77 SUFFOLK. 1'. 1 CMLNAN GU . . . . . . . . . . . . .'S CHENANGO . . ... . . . . . . . . . 25 RAYNE, . . . . . . . . . . . .29 COATLAIID .25 WESTCHESTER. .71 NIAUAMA. . . • . . . , . . . . . .12 5UFFOL K . . . . . . . . . . . . . . 1 ONTARIO . . . . . . . . . . . . . .21 PUTNAM . . . . . 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E /' , Iri r `__' .t �:yr" - '^.h \ ! / i �\ \ i I J / all° - _ \ \ I , a 1 ) ,-� /_ ) I� \' n \ / o µ� - � , ^40., 1 j i�EM • ° ° �9� \ '" i. _ to \:I \ "J I 1 n) /.1, / / / �.- /1 \ ,� , _ �_ 1 Cr1 l'` ' i 11 �/ _ l c` \" `� /Z\,\' '� 'O \ '�. `/• •:\� ;fNattltuck 6 r \\\ / _ \ \ \ \--�i 1 \� \h` Dlstnct Beach / \ \ ` ` / \ \ c—'/ x o Wit:' /" - O ( r /. , / 1 -- _ � ` �`> \\ P •moo �/ \ _ \ \ .\'��', • 'T:A. � - / � :I < �l _ ' / \ z% : ° _ \ \ �o \Camp !/ . 1 I. ';��-. � \0 ,.- ` _ %_, �__-_ - �' t \ �I Immaciilate /3 �' -- t' Z ;. i \ R -� D j !\ _ = ) ^�` > j \ 1 SCALE 1:24 060 1 . . `' % - \ / Q ~ 0 1 MILE ( ` {tom o i37 ? \�,�� \ �\ 0 \ \ y\ \ o _ \, _\ a \ - \ \ - `a ••t '' . I 1000 0 1000 2000 3000 4000 5000 6000 7000 FEET ) I i\::: - / ♦ ° / �- 5 0 1 KILOMETER / 3p :, Oo - �. �\ 25 \R Staff ` �\ \' T_�, \ S/�\2y ! h \ - • , - - as \ c. :; �\ \.\ JA`s �`.` `.\,1 \\ , l(•\\\`F, g C NTOUR INTERVAL 10 FEET _ " ,` - - °� M .. -. lr ` CLmm- TKDN TITLE: FOUR MILE VICINITY MAP SITE �OUTHHOLD, LF' CUTCHOGUE, N.Y. . DATE : 09/ 11/ 90 TDD : 02-9008-48 QUAD : MATTITUCK HILLS, N.Y. FIGURE NUMBER: SCALE: 1" =20001 . P \ S ;\ . {" \ . �� \ V - ' -4 \ - /. I " ,C . - 1 - 'i� 7 �+� W... . ,(' �•` � �.l ? _ t'- r., - - Standard _ `o - ^\ NUS CORPORA TION SUPERFUND DIVISION p _ goo g— � PROJECT NOTES TO: FROM: p 2 DATE: /PA rIP COPIES: SUBJECT: CA 1 I CiIA -7-V,-) y � � D Aiy � C 2QA c, REFERENCE: az So- Me-% ��a A2Dt1u () 1 4 R -2, A.v l(n d0ke l��A D[ l2('i✓A <e l0/Jc� T ,g��;T_,1�/]A� �d u,u� A 2r'P_ 5 .� R f-fA �h�/i'�P:✓� � ) CAM A hm n ink. ArL_ q o (�l-feflx-u rA- tiu w,A en_. 7 uj ; T M T LJ.e , 1 Mg A i' i Pt;V nuc, ilJ �'� NUS 443A 58 1182 TOWN OF SOUTHOLD LANDFILL DISCUSSION ITEMS APRIL• 26, 1983 1. Landfill Operations uncovered refuse unorganized dumping . ponding of water final grades n n scrap metal/paper bales�s�/%�ri���� equipment/personnel 2. Planning adjacent property - plans/liner . immediate operational plans for current site �3. Groundwater Monitoring location of wells additional wells — tary 'n 2w- routine monitoring . plume rdefinition - remedial action `4. Methane Monitoring probe location . routine monitoring venting migration control 5. Closure establish final grades, closure and vegetation pp / 6. Septage status of Greeport project immediate plans for handling of septage IFSnQ. L 7. Recycling . expanded program - glass, metals, paper leaf composting NUS CORPORATION AND SUBSIDIARIES TELECON NOTE CONTROL NO.: �. m/ i -�1 /♦JRt r i .: �. m WAW -4 wa 01 WN 71 r• �. � !.tri � L ACTION ITEMS: i wUS 067 REVISED O"S NUS CORPORATION AND SUBSIDIARIES TELECON NOTE CONTROL NO.: -` c�' ^ ��� DATE: a� TIME: s s DISTRIBUTION: ( % Cr r So `^ l��o LG. �. l 1 1 BETW PEEN: r, (-) � � s C -A&--127 PHONE: AND: 4 (NUS) DISCUSSION: �= c �s �S�L Q t S. 6 (e f -� Cl r✓ lz�(c d LA I 1\2CL K-2, 13 C71L ACTION ITEMS: xw Ub/ KGNIO[U Ub6b