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HomeMy WebLinkAboutFinfish Aquaculture Project in Gardiners Bay - 1997RECEIVED OCT 1 1997 Southold Town Clerk PREPARED FOR MARICULTURE TECHNOLOGIES, INC. FOR FINFISH AQUACULTURE PROJECT LOCATED OFF PLUM ISLAND, NEW YORK CAMERON ENGINEERING & m LP AND PECONIC ASSOCIATES, INC. SEPTEMBER 1997 0 0 PECOIVIC ASSOCIATES, INC. ENVIRONMENTAL PLANNERS & CONSULTANTS One Bootleg Alley - P.O. Boz 672 Greenport, Rev York 11944 Telephone (516)477-0030 Paz (516)477-0198 MARICULTURE TECHNOLOGIES, INC. FINFISH AQUACULTURE PROJECT GARDINER'S BAY, LONG ISLAND SAMPLING PROCEDURE REPORT AUGUST 1997 INTRODUCTION TO COMMENTS JULY REPORT Forms EPA 3320-1 reported all temperatures taken in Celsius from standard instrumentaton. Pre-printed parameters were, however, in Fahrenheit. Tables 7 and 8 incorrectly headed the chlorophyll column as mg/I instead of ug/L. DATES OF SAMPLING Water samples and field measurements were taken on August 20, 1997 and August 27, 1997. METHODS Laboratory methods used by Ecotest are summarized at the end of this report. Methods used by O'Brien & Gere are listed on their Laboratory Analytical Results opposite each parameter. Mariculture Technologies, Inc. • Finflish Aquaculture Project Gardiner's Bay, Long Island Sampling Procedure Report August 1997 A. Project Description Mariculture Technologies, Inc. has undertaken a Finfish Aquaculture Project involving the growth of summer flounder within a network of offshore net cages in Gardiner's Bay, off of the south shore of Plum Island. There are currently four net cages within the network, of which two of the four are stocked with juvenile flounder. The flounder are fed several times per day and will eventually be harvested for processing and/or marketing. In order to undertake this project, the New York State Department of Environmental Conservation (NYSDEC) required that Mariculture Technologies comply with a SPDES (State Pollutant Discharge Elimination System) monitoring program. The monitoring program, supervised by Peconic Associates, Inc. in conjunction with Cameron Engineering & Associates, LLP, operating under SPDES Permit No. NY -0226726, involves the collection of samples from the water column on a twice per month basis. Sampling will be performed during July, • August, and September only with one preliminary ambient water quality sampling session performed in June before the deployment of any fish. Samples are taken from the bottom (one meter above the sea floor), middle (half depth), and top (one meter below the surface) of the water column at 15 different sampling locations. Sample locations are discussed in detail in section C of this report. Field sampling parameters are pH, Dissolved Oxygen, Temperature, and Salinity. Samples are collected for Phosphorus, Ammonia, Nitrogen, and Chlorophyll A analyses by contracted laboratories. The sampling equipment used in the field is discussed in detail in section B of this report. The contracted laboratories are Ecotest Laboratories, Inc. of North Babylon (Phosphorus, Ammonia, and Nitrogen), O'Brien & Gere of Syracuse (Phosphorus, Ammonia, and Nitrogen), and Cosper Environmental Services of Bohemia (Chlorophyll A). B. Sample Equipment and Procedures All field sampling was performed from a chartered boat provided by Mariculture Technologies, Inc. The boat used for sampling during August was a 24' fiberglass cuddy cabin manufactured by "Romarine", powered by a 200 hp Johnson motor. Staff on board the boat is summarized with the sample data provided in section D of this report. Mariculture Technologies, Inc. - Fb!ftyh Aquaculture Project • Sampling Procedure Report - CE 332A r August 1997 Page 2 of 5 The pH meter used in the field was a SPER Scientific Model 840035 pH meter with automatic temperature adjustment. The pH meter was calibrated before each field sampling session by using a standard solution with a known pH of 7.0 and a standard solution with a known pH of 10.0. pH sampling was performed by placing the pH meter probe into a sample container filled with water from the water column sample location. The value on the pH meter was then read and recorded for each sample location. The sample container was rinsed with a portion of sample before each reading to prevent contamination from previous sample collections. The Dissolved Oxygen meter used in the field was an Oxyguard MK II D.O. meter with measurement capabilities of parts per million, % saturation, and water temperature in • degrees Celsius. Calibration of the D.O. meter was performed prior to each sample session by entering the % saturation value corresponding to the salinity of the water column. Dissolved Oxygen measurements were taken at each sample location by attaching the D.O. probe to the Niskin sample bottle and recording the dissolved oxygen in parts per million (mg/1). Water temperature readings were taken simultaneously with the D.O. meter. As discussed previously, temperature readings were read and recorded using the temperature measuring capabilities of the D.O. probe. Measurements were taken at each sample location. 5. Salinity The salinity meter used in the field was an Aquatic Eco -Systems, Inc. Optical Salinometer Model No. 9612 capable of measuring salinity in parts per thousand. Calibration of the • salinometer was performed prior to each sample session by using a sample of distilled water and adjusting the salinity setting to zero. Salinity measurements were then taken at each sample location using the sample container discussed with the pH meter. The value on the salinometer was then read and recorded for each sample location. As mentioned • Maricubure Technologies, Inc. - Fbn h Aquaculture Project &wW ing Procedure Report - CE 332A August 1997 Page 3 of 5 in the pH meter discussion, the sample container was rinsed with a portion of sample before each reading to prevent contamination from previous sample locations. The salinometer was rinsed with distilled water and cleaned with a "ldm-wipe" between each reading. Collection of the water samples for Ammonia, Nitrogen, Phosphorus, and Chlorophyll A was performed using a Niskin Non-metallic water sampling bottle, General Oceanics, Inc. Model No. 1010 having a capacity of 1.7 liters. The sample bottle was attached to a Scotty Downrigger by means of a stainless steel cable for lowering and raising of the sample bottle. A 3 pound weight was attached to the bottom of the sample bottle in order to stabilize the bottle during times of excessive currents. The downrigger is equipped with a digital counter for determining the depth of the Niskin bottle. The sample bottle was lowered to the appropriate depth (measured to the midpoint of the Niskin bottle) for each • sample location at which time a messenger was released along the downrigger cable in order to close the sample bottle and capture the sample at the desired depth. The sample bottle was then raised to the surface by the downrigger and collected in sample bottles provided by the contracted laboratories. Sample types and locations are discussed in detail in section C of this report. 0 C. Sample Locations The following Table 1 summarizes the sample point locations in the vicinity of the net pens. Table 2 summarizes the sample parameters to be taken at each location. For each sample taken, the depth and time were recorded to further identify the sample location and coordinate readings with local tides. Tables 3 and 4 attached to this report present local tide information for each day that sampling was performed. Site tides occur approximately 15 minutes before times shown on the tide tables for Plum Gut. Table 1- Sample Locations Station No. I Station Type I Description Southeastern -most corner of the underwater property O1F Fixed Coordinates: Lat. N41"10.10' Long. W72'10.27' Marieulture Technologies, Inc. - Fin flah Aquaculture Project August 1997 • Sampling Procedure Report - CE 332A Page 4 of 5 0 0 Station No. Station Type I Descri tion 02F Fixed Southwestern -most corner of the underwater property Coordinates: Lat. N41010.16' Long. W72 ° 11.56' * 03F Fixed Northwestern -most corner of the underwater property Coordinates: Lat. N41010.57' Long. W72'11.03' 04F Fixed Northeastern -most corner of the underwater property Coordinates: Lat. N41 ° 10.52' Long. W72 ° 10.60' 01R Rotating Center of the net cage cluster 02R Rotating Eastern edge of the most heavily used net cage cluster 03R Rotating 5 meters east of 02R 04R Rotating 10 meters east of 02R 05R Rotating 30 meters east of 02R 06R Rotating 60 meters east of 02R 07R Rotating Western edge of the largest net cage 08R Rotating 5 meters west of 07R 09R Rotating 10 meters west of 07R 1OR Rotating 30 meters west of 07R 11R Rotating 60 meters west of 07R The fixed sampling locations represent the border of the leased underwater property and will remain constant throughout the entire sampling program. The rotating sampling locations were located based on the projected number of fish in each cage. Figure 1, attached to this report, presents a site plan showing the general area of the project and the coordinates of the fixed sample locations. Figure 2, attached to this report, presents a configuration plan showing the rotating sample locations used for the sampling events during the month of August. Table 5, attached to this report, summarizes the number and size of fish in each cage during the month of August. • Mariculture Technologies, Inc. - Fblgrh Aquaculture Project Sampling Procedure Report - CE 332A Table 2 - Sample Schedule August 1997 Page S of 5 Parameter Location Ammonia 1F, 3F, 1R, 2R - Bottom and Middle Nitrogen 1F, 3F, 1R, 2R - Bottom and Middle Phosphorus 1F, 3F, 1R, 2R - Bottom and Middle Chlorophyll A 1F, 3F, 1R, 2R - Top Salinity All locations - Bottom, Middle, and Top Temperature All locations - Bottom, Middle, and Top pH 1F, 3F, 1R, 2R - Bottom, Middle, and Top Dissolved Oxygen All locations - Bottom, Middle, and Top D. Sample Data • Sampling results are presented in Tables 6 through 9 of this report. Table 6 summarizes the data collected for the entire month of August. Shaded values indicate the data to be reported on the Discharge Monitoring Report (DMR) required by the SPDES permit. In addition, monthly minimum, maximum, and average values are presented to further assist 0 in the monitoring of the site. Tables 7 and 8 present the raw data recorded from sampling performed on August 20, 1997 and August 27, 1997, respectively. The field results and the laboratory results from each contracted laboratory are presented in these tables. Table 9 presents the data from the June 19, 1997 baseline sampling, which was performed before the deployment of any fish into the net cages. N:\C300-349\CA332A\AUGUST.RPT Part 1, Page 7 of _ 9 The permittee shall take samples and measurements to comply with the monitoring requirements specified this permit, at the location(s) indicated below: i c C z SOUND LONG IS LAND �Pljulylli l l lI IILAND I ,U11 I 1 1 � `EAST POINT PLUM IS ROCK BUOY N"4" (Reference) \ \ Lt N 41'10'25' Lf N 4 10' 31 " Lg W 72'10'43•• 9� Lq W 72'.10 36r .�� •,r• Lt N 41.10'34' � / �! ♦ �• LG W '7C2' 1 1 ' 02' �40j.j `` Q. 2000 v' 2' _0 A %FUTURE -PHASES �& r COuNTY SUPPOLK t TOWN o! SOUTH.OLD {� �• / tiAS I TAX MAP REFERENCE PARCEL REF. NO. 28 lV 1 ( Iv ' ` FROPERTy +.::a 132 DISTRICT IC -00 / / 6CG0 FT 8. c90 ` LI N 41'10 O6: I 02F S-0. L9 W 72.10' 16' Lt N al IC'16' Lq W 72'11'33- CO GCncr51'E , Z 2C c T M N W.:TER DEPTH it I ' P I NE �DOI NT ZZ ,' �.+w.r� SC Ts>:' MAP REF: 1000- 132 .00.01 .00.2E . 00 , r - /.. ww w w w ,r.,,�.� w.w w•ww•ww•ww•w..•ww...r...w �. r• � . s F ,M �t PROPOSED GROWOUT PEN SITr *j 200 Acres ~ SCALE: 1' = 2000 FT ol;•:Pcs_: GROWOUT FACILITY FOR THE PRODUCTICN OF SUMMER FLOUNDER (Fo'ai\chlhyf OY>:lalut) CArJw; MEAN SEA LEVEL AD:ACCNT PROPCFTY OWNE'nS: N/A 4 l� F 1 Z� o SITE MAP EASTERN LONG ISLAND GARDINERS BAY (PLUM ISLAND VICINITY) ORAWN Of: JL9 ( CNK•0 9': MW FINFISN AQUACULTURE PROJECT Mariculture Technologies GREENPORT TOWN of SOUTSCLD SUFFOLK COUNTY, NEA' YORK ft—.d q PECONIC ASSOCIATES. u.C. OW NOTUS YLP. "Ittw1a.. •• II*Y o.TE 1 1 FE897 SNEET 3 OF 33 s 12/89) NYSDEC Permit #: i-4/3tt-y-ic5aivvvv 1-v GOTATING MONITORING LOCATIONS RELATIVE TO NET PEN DEPLOYMENT SPDES #: 0226726 Part 1, Page 8 of _9 The permittee shall take samples and measurements to comply with the monitoring requirements specified in this permit, at the location(s) indicated below: North Rotating Monitoring Locations (01 R, 02R, 03R, 04R, 05R, 06R, 07R, 08R, 09R, 1 OR, 11 R) t0 m ---. m • 30 m30 m - - - 10 m 10 m S m ;_ —_� S m 11R 10R 09R OSR 07R O1R 02R 03R 04R OSR 06R Center of Not Pons OPHASE I SITE PLAN 101` LAT N AT' 101 23' LNG w 77- 1O• 57' 4 F Sao i NORTHERN PLASTICS T N 10' 23 i (TWO UNITS) 6 • Lw(, 7211 0 �N SPAR \\ \ CHNOLOGIES ' UNrT) ; \\ m m\ t= BRIDGESTONE\ (ONE UNIT) / yrs i LAT N n• 10. 15' 2 LNG N 72' 1 1• 06• 0 mJ \ v 1 \ v ATLANTIC AO UA CAGE li -------_.� (ONE UNIT) a 1 i LAT N J1• 10• 15' 165i goo SITE LNG M 7. 10. 57" r/0° e SITE PLAN SCALE: t" = 200' 0 /.A(,f3L& %;;, . Tides - Plum Gut Harbor, Plum Island Average Tides 41* 10.0'N 72° 12.0'W Daily Highs & Lows Mean Range: 2.6 ft 5:47 am -0.3 ft Low Diurnal Range: 3.1 ft Wdnesdy, August 20 1997 11:54 am 3.5 ft High ea, U Mean Tide: 1.5 ft g , 6:12 pm -0.2 ft Low Nautical Software (503) 579-1414 (Feet) (EDT) _Tide 0.50 10.01 0.50 1.01 0 2.01 2.50 1 3.01 3.50 12:00 am 3.5 ft ME 12:30 am 3.3 ft � 1:00 am 3.0 ft 1:30 am 2.6 ft 2:00 am 2.1 ft 2:30 am 1.7 ft 3:00 am 1.3 ft 3:30 am 0.9 ft 4:00 am 0.5 ft 4:30 am 0.1 ft 5:00 am -0.1 ft 5:30 am -0.3 ft 6:00 am -0.3 ft 6:30 am -0.1 ft 7:00 am 0.1 ft 7:30 am 0.5 ft 8:00 am 1.0 ft 8:30 am 1.5 ft 9:00 am 2.0 ft • 9:30 am 2.4 ft 10:00 am 2.8 ft 10:30 am 3.1 ft.: 11:00 am 3.4 ft 11:30 am 3.5 ft 12:00 pm 3.5 ft 12:30 pm 3.4 ft a d W 1:00 pm 3.2 ft 1:30 pm 2.9 ft 2:00 pm 2.5 ft 2:30 pm 2.1 ft 3:00 pm 1.7 ft 3:30 pm 1.3 ft 4:00 pm 0.9 ft 4:30 pm 0.5 ft 5:00 pm 0.2 ft 5:30 pm -0.1 ft 6:00 pm -0.2 ft 6:30 pm -0.2 ft 7:00 pm 0.0 ft 7:30 pm 0.3 ft -i 8:00 pm 0.7 ft 8:30 pm 1.1 ft 9:00 pm 1.6 ft 9:30 pm 2.1 ft 10:00 pm 2.5 ft 10:30 pm 2.9 ft • 11:00 pm 3.1 ft 11:30 pm 3.4 ft Nautical Software (503) 579-1414 0 (EDT) Tide 0.50 1 0.0 12:00 am 0.4 ft 12:30 am 0.4 ft 1:00 am 0.5 ft 1:30 am 0.6 ft 2:00 am 0.9 ft 2:30 am 1.1 ft 3:00 am 1.3 ft 3:30 am 1.5 ft 4:00 am 1.8 ft 4:30 am 2.0 ft 5:00 am 2.2 ft 5:30 am 2.3 ft 6:00 am 2.4 ft 6:30 am 2.4 ft 7:00 am 2.4 ft 7:30 am 2.3 ft 8:00 am 2.2 ft 8:30 am 2.1 ft 9:00 am 1.9 ft 9:30 am 1.7 ft •10:00 am 1.5 ft 10:30 am 1.2 ft 11:00 am 0.9 ft 11:30 am 0.7 ft 12:00 pm 0.5 ft 12:30 pm 0.5 ft 1:00 pm 0.6 ft 1:30 pm 0.8 ft 2:00 pm 1.0 ft 2:30 pm 1.3 ft 3:00 pm 1.5 ft 3:30 pm 1.8 ft 4:00 pm 2.1 ft 4:30 pm 2.3 ft 5:00 pm 2.6 ft 5:30 pm 2.8 ft 6:00 pm 3.0 ft 6:30 pm 3.0 ft 7:00 pm 3.1 ft 7:30 pm 3.0 ft 8:00 pm 2.9 ft 8:30 pm 2.8 ft 9:00 pm 2.6 ft 9:30 pm 2.3 ft 10:00 pm 2.1 ft 10:30 pm 1.8 ft 11:00 pm 1.4 ft • 11:30 pm 1.0 ft Tides - Plum Gut Harbor, Plum Island 3.50 Average Tides d 41' 10.0' N 72° 12.0' W Daily Highs 8 Lows Mean Range: 2.6 ft 12:13 am 0.4 ft Low Diurnal Range: 3.1 ft Wednesday August 27 1997 6:31 am 2.4 ft High Mean Tide: 1.5 ft > > 12:22 pm 0.5 ft Low 6:54 pm 3.1 ft High (EDT) Tide 0.50 1 0.0 12:00 am 0.4 ft 12:30 am 0.4 ft 1:00 am 0.5 ft 1:30 am 0.6 ft 2:00 am 0.9 ft 2:30 am 1.1 ft 3:00 am 1.3 ft 3:30 am 1.5 ft 4:00 am 1.8 ft 4:30 am 2.0 ft 5:00 am 2.2 ft 5:30 am 2.3 ft 6:00 am 2.4 ft 6:30 am 2.4 ft 7:00 am 2.4 ft 7:30 am 2.3 ft 8:00 am 2.2 ft 8:30 am 2.1 ft 9:00 am 1.9 ft 9:30 am 1.7 ft •10:00 am 1.5 ft 10:30 am 1.2 ft 11:00 am 0.9 ft 11:30 am 0.7 ft 12:00 pm 0.5 ft 12:30 pm 0.5 ft 1:00 pm 0.6 ft 1:30 pm 0.8 ft 2:00 pm 1.0 ft 2:30 pm 1.3 ft 3:00 pm 1.5 ft 3:30 pm 1.8 ft 4:00 pm 2.1 ft 4:30 pm 2.3 ft 5:00 pm 2.6 ft 5:30 pm 2.8 ft 6:00 pm 3.0 ft 6:30 pm 3.0 ft 7:00 pm 3.1 ft 7:30 pm 3.0 ft 8:00 pm 2.9 ft 8:30 pm 2.8 ft 9:00 pm 2.6 ft 9:30 pm 2.3 ft 10:00 pm 2.1 ft 10:30 pm 1.8 ft 11:00 pm 1.4 ft • 11:30 pm 1.0 ft (Feet) 0.50 1.0 1 1.50 2.0 2.50 1 3.0 3.50 m °M� d a m - - - - _ ? Nautical Software (503) 579-1414 Table 6 Mariculture Technologies, Inc. Monthly Sampling Summary MONTH: AUGUST 1997 SAMPLE LOCATION Depth IRI Temperature (°C) Dissolved Oxygen (mg0) Salinity (oloo) PN Nitrogen (moll - Total as N) Phosphorus (moll -Total as P) Chlorophyll A (ug/1) Ammonia Nitrogen (mglL - Total as N) STATIONS DEPTH Min. Max. Avg. Min. Max. Avg. Min. Max. Avg. Min. Max. Avg. Min. Max. Min. Max. Av¢ Min. Max. Avo. Min. Max. Avg. Min. Max. Avg. TOP 3 3 3.0 19.7 .191 19.7 &7`:: 6.9 6.8 29 0 30.0 '. 29.5 7.0.5 - 7.05 : 1.28 1.6$ 1.47 1F MIDDLE 17.5 18 17.8 198 ,19.8 '.: 19.6 O.7 6.9 6.8 290 29.0.. 29.0 7.01: T.05 0.3 .0.70.50 0.03 0.¢ :' 0.32 0.02 OG3 0.03 BOTTOM 32 33 32.5 196 ',19.7 " 197 6.T' '' 8.9 6.8 290 29.0 29.0 6.99 8,03 0.3 0.6 0.45 0.04 0.5 0.27 0.05 0.05 1 0.05 TOP 3 3 3.0 19.3 19.0 t: 19.6 63: '. 6.8 6.8 30.0 :32,0 I' 31.0 2F MIDDLE 7 7 7.0 193 119,6;. 196 (0.: 6.8 6.8 300 31,0 :. 30.5 BOTTOM 11 11 11.0 19 2 :19.9 `: 19.6 " 0.T; 6.8 6.8 30.0 30.0 `-: 30.0 TOP 3 3 3.0 19.6 '19.9 19.8 0.T 6.8 6.8 290 33.0 "' 31.0 703 '7.0¢ 1.47 ;160„', 1.54 3F MIDDLE 7.5 7.5 7.5 19.5 ':20.0 19.8 8.8. 6.8 6.8 29.0 '32.0. 30.5 7.03' 1.10 : 0.3 1 0.7 0.50 0.06 0.7 0.38 0.04 0.12 :, 0.08 BOTTOM 12 12 12.0 19.5 20.0 19.8 6.7 '. 6.8 8.8 29.0 31.0 30.0 7.00 7.03 0.3 `: 1.0 1 0.65 0.03 0.4 0.32 0.08 0.1.. 0.09 TOP 3 3 3.0 19.6 -:' 19.9 '- 19.8 0:8 -. 6.7 6.7 30.0 34.0 < 32.0 4F MIDDLE 12.5 12.5 12.5 196 ;19.4 = 19.8 6.7 6.7 6.7 30.0 33,0 I. 31.5 BOTTOM 22 22 22.0 19.6 `I 20,0' -> 19.8 6,7 " 6.7 6.7 30,0 ; 33.'Q, 31.5 TOP 3 3 3.0 196 -20,1.1 19.9 6A. 7.3 7.1 300 j3&0 : 31.5 6.94: 7,D0 :' 1.01 1.74 : 1.38 1R MIDDLE 12.5 18 14.3 12.5 20.1 19.8 &¢ 8.6 6.8 30.0 '320 - 31.0 8.94'. 6." 0.2 ` 0.5 0.35 0.04 4.3 ;. 0.27 0.04 0.06 0.05 BOTTOM 22 29 25.5 19.5 -. 20.0 19.5 6,4 '. 6.5 6.5 30.0 - $2.0 ':. 31.0 1 694' 8.95 -.. 0.4 '' 0.6 I. 0.50 0.08 0-5 :� 0.29 0.06 p.1 '.. 0.08 TOP 3 3 3.0 196 ' 20.1 :- 199 6.0 6.9 6.9 30.0 .3110 305 7.0$I 7.05 1.10 -1.79 -. 1.45 2R MIDDLE 15 16 15.5 19 8 20.0 19.8 6.7 6.8 6.8 30.0 30.0 -., 30.0 7.03 7.03 0.4 0.7 ' 0.55 0.04 0.7 0.37 0.02 0.02 0.02 BOTTOM 27 29 28.0 1 19.8 1 20.1 r 19.8 1 0.7 -.. 8.8 8.8 300 :....30.0'. 300 7.01 '7.01 0.3 0.7 -. 0.50 0.04 0,7 --i 0.37 0.02 0.06 :. 0.04 TOP 3 3 3.0 197 20.2 200 0.6 - 6.8 6.7 300 '.:3110=: 30.5 311 MIDDLE 15 16 15.5 197 20,1 I. 199 6.8 ` 6.8 6.8 300 -31,0 30.5 BOTTOM 27 29 28.0 19.8 20.2 -.' 20.0 87 : 8.8 6.6 30.0 30.5 TOP 3 3 3.0 19.7 20.2 ':' 20.0 6.6 6.8 5.7 30.0 5 31.0 '.' 30.5 414 MIDDLE 15 10 15.5 19.7 ;. 20.1 '. 19.9 6.5 .. 6.8 6.8 30.0 '30.0 * . 30.0 BOTTOM 27 29 28.0 197 20.1 ` 19.9 6.8- 6.8 6.8 30.0 :32.0 31.0 TOP 3 3 3.0 19.7 20.1 19.9 0.8 6.9 6.9 30.0 32.0 ': 31.0 SR MIDDLE 16 18 15.5 19.7 : 20,1 19.9 s0.6 6.6 6.8 30.0 320: 31.0 BOTTOM 27 29 260 19.7 �; 20,2.`'" 20.0 <Sj v �;.':. 6.7 6.7 30.0 a x1.0, ;, 30.5 TOP 3 3 3.0 19.7 7.1 7.0 30.0 32.9-z 31.0 BR MIDDLE 14 15 14.5 19.8 20.0 ' 19.9 &7 `'-r 8.6 8.8 300 31.0 : 30.5 BOTTOM 25 27 26.0 19.8 +. 20.0 19.9 6.6 6.8 6.7 300 320 : 31.0 TOP 3 3 3.0 19.4 : 20.3 -: 19.9 &8 :. 7.1 7.0 310 31.0 31.0 711 MIDDLE IS 16 15.5 19.5 ,:. 2Q.2" 19.9 6.711' 5.8 6.8 300 31.0:.. 30.5 BOTTOM 27 129 28.0 19.5 ,' 20.1`, ' 19.9 '86 8.7 6.7 31.0 1 31.0 : 31.0 TOP 3 3 3.0 19.4 20.1'.. 19.8 8.6 -. 7.0 6.9 310 ! 32.0 31.5 - 8R MIDDLE 15.5 16 15.8 19.4 20.0 197 &6.`; 6.8 6.7 300 - 31.0 30.5 BOTTOM 28 29 28.5 19.4 '2M0 :' 19.7 . GA .° 6.7 6.7 31 0 31.0 31.0 TOP 3 3 3.0 19.4 20,0 19.7 6.8 ,7 8.9 6.9 31.0 33.0 '. 32.0 9R MIDDLE 15.5 18.5 16.0 19.4 J. 20.0 -: 19.7 43 6.8 6.8 320 ` 33.0 '. 32.5 BOTTOM 28 30 29.0 19.4 '. 20.0 19.7 &.¢ 6.5 6.6 31.0 1 ; `31.0 31.0 TOP 3 3 3.0 19.5 20,1 19.8 &8 :. 7.2 7.0 320r S3,0 " 32.5 IGR MIDDLE 15.5 17 16.3 19.5 20.9 '. 19.8 "As : 6.8 6.7 32.0 .. 33.0 32.5 BOTTOM 28 31 29.5 19.5 20.2 '. 19 9 5.8 6.7 8.7 32.0 $3,0 ". 32.5 TOP 3 3 3.0 19.4 20,2 ,:;. 19.8 63 '. 7.1 6.9 31.0 " 31,0 31.0 11R MIDDLE 15 15.5 15.3 19.4 20.2: 19 6 '&T -:- 8.8 6.6 32.0 33,0'.- 32.5 BOTTOM 27 26 27.5 19.4 20.3 !: 19.9 6.6 8.8 6.7 33.0 , 33.0 33.0 - INDICATES VALUE TO BE REPORTED ON MONTHLY DMR Table 7 Mariculture Technologies, Inc. Sampling Summary • DATE: AUGUST 20, 1997 Weather: Mostly Cloudy 78° Staff: Merlon Wiggin, Tim Malone, Melanie Douglass, Eric Wagner, Andre Miller • • AMMONIA NITRATE PHOSPN . T.K.N. NITROGEN CHLOROPHYLL A 3AMPLE LOCATION I TIME TIDE DEPTH (FT) D.O. ImWI► TEMP. (OC) 9ALJNITY (Woo) pH (3U) 10191L) (1"911-) 11"91L) (1"9A.► (MWL) (9WL1 3TATHM t OEM STAR STOP 3TART STOP O t 0 EeoTeet O i 0 EeoTat O i 0 EeoT4ut O i 0 EeoT88t O i G EwTM Coepor TOP 8:26 8:30 Flood3 6.7 19.7 29 7.05 1.28 1F MIDDLE 8:21 8:25 17.5 6.9 19.6 29 7.01 0.02 <.05 <.01 <.05 <.05 <.02 0.6 0.7 0.6 0.7 (35 FT D BOTTOM 8:10 8:20 Flood 32 6.9 19.6 29 8.03 0.05 <.05 <.01 4,05 0.1 <.02 0.5 0.3 0.5 0.3 TOP 8:41 8:42 Flood3 6.8 19.3 30 2F MIDDLE 8:39 8:10 1 6.8 19.3 30 (14 FT DEEP) BOTTOM 8:36 8:38 Food 11 6.6 19.2 30 TOP 9:01 9:05 Flood 3 6.7 19.6 29 7.08 1.47 3F MIDDLE 8:37 9:00 7.5 6.8 19.6 29 7.10 0.12 <.05 <.01 <.05 <.05 <.02 0.7 0.5 0.7 0.5 (15 FT D BOTTOM 8:53 8:56 Flood 12 6.8 19.5 29 7.03 0.08 <.05 <.01 <.05 <,05 <.02 0.6 1.0 0.0 1.0 TOP 9:17 9:18 Flood 3 5.8 19.6 30 4F MIDDLE 9:14 9:18 12.5 6.7 19.6 30 (25 FT DEEP) BOTTOM 9:10 9:13 Food 22 6.7 19.6 30 TOP 10:36 10:41 Flood 3 7.3 19.8 30 7.00 1.01 1R MIDDLE 10:30 10:35 /6 8.6 19.5 30 6.99 0.04 <,05 0.01 <.05 0.06 <.02 0.5 0.4 0.5 0.4 (32 FT DEEP) BOTTOM 10:21 10:29 Flood 29 6.5 19.5 30 6.94 0.1 <.05 <.01 <.05 <.05 <.02 0.5 0.6 0.5 0.8 TOP 9:39 9:47 Flood 3 6.8 19.6 31 7.03 1.10 2R MIDDLE 9:35 9:38 16 8.7 19.8 30 7.03 0.02 <.05 <.01 <.OS <.05 <.02 0.7 0.8 0.7 0.6 (32 FT DEEP) BOTTOM 9:31 9:34 Flood 29 6.8 19.8 30 7.01 0.05 <,OS <.01 <.OS <.OS <.02 0.7 0.7 0.7 0.7 TOP 9:51 9:52 Flood 3 8.8 19.7 30 3R MIDDLE 9:48 9:50 166.8 19.7 30 (32 FT DEEP) BOTTOM 9:45 9:47 Flood Z I 8.7 19.8 30 TOP 9:58 9:59 Flood 3 8.8 19.7 30 4R MIDDLE 9:56 9:57 16 6.8 19.7 30 (32 FT DEEP) BOTTOM 9:54 9:55 Flood 29 6.8 19.7 30 TOP 10:04 10:05 Flood3 8.8 19.7 30 5R MIDDLE 10:02 10:03 16 6.8 19.7 30 (32 FT DEEP) BOTTOM 10:00 10:01 Flood 29 6.7 19.7 30 TOP 10:13 10:14 Flood 3 7.1 19.7 30 6R MIDDLE 10:11 10:12 15 8.7 19.8 30 (30 FT DEEP) BOTTOM 10:09 10:10 Flood 27 8.8 19.8 30 TOP 10:51 10:52 Flood 3 7.1 19.4 31 7R MIDDLE 10:49 10:50 16 6.8 19.5 31 (32 FT DEEP) BOTTOM 10:47 10:48 Flood 29 6.6 19.5 31 TOP 10:58 10:59 Flood 3 7.0 19.4 31 8R MIDDLE 10:56 10:57 16 6.8 19.4 31 (32 FT DEEP) BOTTOM 10:54 10:55 Flood 29 8.7 19.4 31 TOP 11:05 11:07 Flood3 6.9 19.4 33 9R MIDDLE 11:05 11:08 16.5 6.8 19.4 33 (33 FT DEEP) BOTTOM 11:03 11:04 Flood 30 5.6 19.4 31 TOP 11:15 11:18 Flood 3 7.2 19.5 33 MIDDLE 11:13 11:14 17 6.8 19.5 33 EP) BOTTOM 11:71 11:12 Flood 31 8.6 19.5 32 LFT TOP 11:22 11:23 Flood 3 7.1 19.4 31 MIDDLE 11:20 11:21 1S.5 6.8 19.4 33 EP) BOTTOM 11:18 11:19 Flood 26 6.8 19.4 33 • • Table 8 Mariculture Technologies, Inc. Sampling Summary DATE: AUGUST 27, 1997 Weather. Mostly Sunny 78° Staff: Merlon Wiggin, Tim Malone, Eric Wagner, Bob Cameron AOIIA PHOSPOIOUS T.K.N. NITROGEN CHLOROPHYLLA SAM (FT) (W1 (oCl A(aoo) S)SAN MOIL) (M (MOIL) (MOIL) DEPTH STAR STOP START STOP O t o E..Ta O t o EooTsst o i 0 EeoTut O i 0 EeeTW Cospsr TOP 8:12 8:14 Flood 3 5.9 19.7 30 7.03 1.65 1F MIDDLE 8:05 8:11 18 5.7 19.a 29 7.OS 0.03 <.OS 0.01 <.05 0.06 0.03 0.3 0.4 0.3 0.4 (3e FT DE BOTTOM 8:00 8:05 Flood 33 0.7 19.7 29 6.99 0.05 <,OS <.01 <.05 0.2 0.04 0.5 0.6 O.S 0.0 TOP 8:55 9:00 Flood 3 6.7 19.8 32 2F MIDDLE 8:24 8:27 7 8.7 19.8 31 (14 FT D BOTTOM 8:20 823 Flood 11 6.7 19.9 30 TOP 9:21 9:23 Flood 3 6.8 19.9 33 7.03 1.60 3F MIDDLE 9:16 9:20 7.5 6.8 20.0 32 7.03 0.04 <,OS <.01 105 0.06 <.02 0.3 0.5 0.3 0.5 (15 FT BOTTOM 9:10 9:15 Flood 12 6.7 20.0 31 7.00 0.1 <.05 0.01 <.05 0.06 0.03 0.3 0.5 0.3 0.5 TOP 9:31 9:32 Flood 3 6.7 19.9 34 4F MIDDLE 9:30 9:31 12.5 6.7 19.9 33 (25 FT DEEP) BOTTOM 9:27 9:29 Flood 22 8.7 20.0 33 TOP 9:45 9:48 Flood 3 8.8 20.1 33 6.94 1.74 1R MIDDLE 9:41 9:44 12.5 6.6 20.1 32 6.94 0.06 <.05 0.02 <.05 0.06 0.04 0.2 0.5 0.2 0.5 (25 FT DEEP) BOTTOM 9:37 9:40 Flood 22 0.4 20.0 32 6.95 0.05 <.05 0.02 <.05 0.08 <.02 0.4 0.5 0.4 0.6 TOP 10:40 10:43 Flood 3 6.9 20.1 30 7.05 1.79 2R MIDDLE 10:36 10:39 15 6.8 20.0 30 7.03 <.01 <.05 0.01 <.05 0.08 0.04 0.4 0.5 0.4 0.5 (30 FT DEEP) BOTTOM 10:32 10:35 Flood 27 6.7 20.1 JO 7.01 0.02 <.05 <.01 -.OS 0.08 0.04 0.3 0.5 0.3 0.5 TOP 10:48 10:49 Flood 3 6.8 20.2 31 3R MIDDLE 10:46 10:47 15 6.8 20.1 31 (30 FT DEEP) BOTTOM 10:43 10:45 Flood 27 6.8 20.2 31 TOP 10:51 10:52 Flood 3 6.8 20.2 31 4R MIDDLE 10:50 10:51 15 8.8 20.1 >D (30 FT DEEP) BOTTOM 10:49 10:50 Flood 27 e.8 20.1 32 TOP 10:58 10:59 Flood 3 e.9 20.1 32 SR MIDDLE 10:56 10:57 15 6.8 20.1 32 (30 FT DEEP) BOTTOM 10:51 10:55 Flood 27 6.7 20.2 31 TOP 11:03 11:04 Flood 3 6.9 20.0 32 6R MIDDLE 11:01 11:02 14 6.6 20.0 31 (28 FT DEE BOTTOM 11:00 11:01 Flood 25 9.8 20.0 32 TOP 10:25 10:28 Flood 3 6.5 20.3 31 7R MIDDLE 10:24 10:25 15 6.7 20.2 30 (30 FT DE BOTTOM 10:23 10:24 Flood 27 6.7 20.3 31 TOP 10:20 10:21 Flood 3 6.8 20.1 32 8R MIDDLE 10:19 10:20 15.5 6.8 20.0 30 (31 FT DEEP) BOTTOM 10:16 10:18 Flood 28 5.6 20.0 31 TOP 10:15 10:16 Flood 3e.a 20.0 31 9R MIDDLE 10:14 10:15 15.5 6.7 20.0 32 (31 FT DE BOTTOM 10:12 10:13 Flood 28 6.6 20.0 31 TOP 10:04 10:06 Flood 3 6.8 20.1 32 10R MIDDLE 10:02 10:03 15.5 8.8 20.0 32 (31 FT DEE BOTTOM 10:00 10:01 Flood 28 8.7 20.2 33 TOP 9:57 9:59 Flood3 6.7 20.2 31 11R MIDDLE 9:55 9:58 15 6.7 20.2 32 (30 FT DEEP) BOTTOM 9:53 9:54 Flood 27 6.6 20.3 33 Table 9 Mariculture Technologies, Inc. Sampling Summary DATE: JUNE 19, 1997 (Baseline Sampling) Weather: Sunny 85' Staff: Merlon Wiggin, Jamie Gaskil, Tim Malone, Mark Wagner, Eric Wagner AMMONIA PHO8PHOROUB T.K.N. NITROGEN CHLOROPHYLL A SAMPLE LOCATION TIME TIDE DEPTH IFT) D.O. 0911) TEMP. (OC) SALIMTV (oloo) PH ISU) (mWL) NITRATE ImWL IMWLI (MWL) (MOIL) (uw STATION 8 DEPTH START STOP START STOP 0&0 EeoTM 0 i O EeoTM 1 0 i 0 EeoT9ri 1 O i O EtoT.q 1 0 6 0 EeoT9ri I Cooper TOP 11:53 12:05 Ebb 3 11 15.0 30 7.28 2.63 1F MIDDLE 11:39 11:52 1 19 9.0 11.6 31 7.29 <0.05 <0.05 0.04 0.3 0.3 (38 FT DEEP) BOTTOM 11:25 11:38 Ebb 35 6.3 11.9 31 7.25 <0.05 c0.05 0.04 0.3 0.] TOP 1:22 4:25 Ebb3 8.8 15.5 32 2F MIDDLE 4:19 4:21 1 15.5 9.0 14.6 32 (31 FT DEET) BOTTOM 4:15 4:18 Ebb 28 9.3 14.8 33 TOP 10:58 11:10 Ebb3 8.4 14.9 31 7.38 2.16 3F MIDDLE 10:14 101.57 9.5 8.6 14.3 31 7.36 <0.05 <0.05 0.04 0.3 0.3 (19 FT DEEP) BOTTOM 10:30 10:43 Ebb 16 8.8 14.5 30 7.37 <0.05 <0.5 0.04 0.8 0A TOP 4:01 4:05 Ebb 3 8.8 14.5 32 4F MIDDLE 3:56 4:00 12 8.8 14.4 32 (2{ FT DEEP) BOTTOM 3:50 3:55 Ebb 21 8.8 11.5 73 TOP 9:36 9:55 Ebb 3 8.6 11.8 30 7.43 1.92 1R MIDDLE 9:11 9:]5 15 8.5 11.5 31 7.41 <0.05 <0.05 0.03 <0.1 <0.1 (30 FT DEEP) BOTTOM 8:57 9:10 Ebb 27 8.3 14.8 30 7.27 <0.05 0.05 0.03 0.3 0.3 TOP 10:19 10:25 Ebb 3 8.3 11.9 30 7.12 1.92 2R MIDDLE 10:11 10:18 16 8.6 14.4 30 7.37 <0.05 <0.05 0.04 0.2 0.2 (32 FT DEEP) BOTTOM 10:00 10:10 Ebb 29 8.5 14.8 30 7.41 <0.05 0.05 0.03 0.1 0.1 TOP 1:44 1:50 E.3 8.3 14.2 28 3R MIDDLE 1:35 1:43 15 8.3 14.1 30 (30 FT DEEP) BOTTOM 1:25 1:34 Ebb 27 9.1 14.3 28 TOP 2:06 2:10 Ebb 3 8.3 14.3 31 4R MIDDLE 2:01 2:05 15 8.5 14.0 31 (30 FT DEEP) BOTTOM 1:55 2:00 Ebb 27 8.9 14.4 30 TOP 2:26 2:30 Ebb 38.8 14.4 31 SR MIDDLE 2:21 2:25 15 8.7 14.2 31 (30 FT DEEP) BOTTOM 2:15 2:20 Ebb 27 8.9 14.3 31 TOP 2:38 2:40 Ebb 38.6 14.5 31 8R MIDDLE 2:35 2:37 15 6.7 14.4 31 (30 FT DEEP) BOTTOM 2:32 2:34 Ebb 27 8.8 14.7 31 TOP 3:36 3:38 Ebb 3 8.6 15.3 32 7R MIDDLE 3:33 3:35 14.5 8.6 14.7 33 (29 FT DEEP) BOTTOM 3:30 3:32 Ebb 26 8.9 14.6 32 TOP 3:26 3:28 Ebb 38.6 15.4 33 8R MIDDLE 3:23 3:25 1 14 8.7 14.8 35 (28 FT DEEP) BOTTOM 3:20 3:22 Ebb 25 9.0 14.6 33 TOP 3:13 3:15 Ebb 3 8.5 14.9 33 9R MIDDLE 3:09 3:12 13.5 8.7 14.8 33 (27 FT DEEP) BOTTOM 3:05 3:06 Ebb 24 8.9 14.8 32 TOP 2:57 3:00 Ebb 3 8.8 14.9 33 10R MIDDLE 2:54 2:55 13.5 8.8 14.8 33 (27 FT DEEP) BOTTOM 2:50 2:53 Ebb 24 8.9 14.5 33 TOP 4:37 4:40 Ebb 38.8 15.6 31 11R MIDDLE 4:34 4:36 13.5 8.9 14.8 31 (27 FT DEEP) BOTTOM 4:30 4:33 Ebb 24 9.0 15.0 31 -, HMI I ILL NAMLiA#URU S lhcr.e. Fo...... -... ..j-,p.,..,, NAME. MAI. ITECHNt:)LJGIF=S? INC ADDRESS MARICULTURF TLCH N'rT PEN PC PiOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO• PRESIDENT NATIONAL VOLLUT ANT DIS 44W WW%ATION SYSTEM DISCHARGE M RING REPORT (DA 2-16 17• PERMIT NUMBER ascH FROM TO 120.21) (22-23) 124-251 (1 271 (28-29) (3431) Form Approve FIXED WQM OFFSHORrWf9r2 4 ( SUB R 01) pproval1 '� I!!q tO5-31-98 F — FINAL MINOR FLUE _ # ND DISCHARGE TE: R,od insbucdons Mforo oompktinp this form. PARAMETER (32-371EX (3 Card On/yl QUANTITY OR LOADING 146-5 /54-61 (4 Cefd Only/ WV -OR CON TION 138-45/ t6- 61-61 NO. (62 -63) FREOUENCY SAMPLE of ANALYSIS TYPE t64-681 169-701 AVERAGE MAXIMUM UNITS MINIMUM GE MAXIMUM UNITS !TEMPERATURE, WATER u• CENTIGRADE SAMPLE MEASUREMENT ***#** #***** ****#* *#***# % ( 04) ,Q PERMIT #><c>Ic>Ic** *#**#* ##*##* REPORT WIGEJ RA$ 10010 T G 0 #****# *** jEE COMMENTS BELOW REQUIREMENT *### DEG• C MONTH I EMPERATURE, WATER 'TG• CIFNTIGRADE SAMPLE MEASUREMENT /�.6 ( O4) o?136 61RAB PERMIT RE PORT TWICE/GRAS 10016 J 0 0 :E`: COaMMElT S $ELOW REQUIREMENT ** DAILY MX; DEG.0 MONTH 7-MPERATURE, WATER r`. CENTIGRADE SAMPLE MEASUREMENT ��r 7 04) a`30 6RM !0010 W 0 0 PERMIT REPORT WICE) RAB E` COMMENTS BELOW REQUIREMENT #*# MX > DEG.0 MONTH ,X..YGUNI DISSOLVED•- ( Da ) SAMPLE MEASUREMENT ,7 **##*# —DAILY ##*### ( 19) / Q !� GRAB '0300 T U 0 PERMIT #*** * #** * ## REPORT *##**# *#* ## WICEI RAB SEE CO.MM1NTS BELOW REQUIREMENT *#* DAILY MN MG/L MONTH XYGENV DISSOLVED;'SAMPLE ( 00) MEASUREMENT Lit / 19) ?B o1-36 PERMIT REPORT WICE/ RAB :0:300 U 0 0 *EE COMMENTS 3ELOW REQUIREMENT #�k* FiAYLi t+IN MG%L M©IV7H XYGEN? DISSOLVED (00) SAMPLE MEASUREMENT #**##* ##**** �• ##*#*# #**#*# ( 19) a7 6 /. ���Q :3300 W 0 0 PERMIT REPORT a##** ****#* WICE/ RAS JEE COMMENTS 3ELOW REQUIREMENT ### DAILY MN MG/L MONTH f SAMPLE( MEASUREMENT 7-D-6' '7.,6" D 1Z) , /3& ;`7400 T 0 0 PERMIT 9.0 WICE RAB :_E CrOPMENTS BELOW REQUIREMENT ### MINIMUM MAXIMUM ISU Mi3l+iTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE AREli SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING'/) THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C. f 1319. tPrm0m u"Wr aWm eese/tes may Intrude fines up toS 10,000 and ormex"wnlrnp"awwwrtofbetween 6monMswd 5 years.) l / TELEPHONE DATE - l Ord�'ItD Qg' CED ' Vh SIGNATURE PRINCIPAL EXECUTIVE OFFICER O AUTHORIZED AGENTCODE TYPED OR PRINTED NUMBER YEAR MCI 1 DAY :UMMEN 15 ANU tArL.ANA I wN Ur ANr VIVLA 1 wives (I7B/aleACe an 8C(NlCIN/AO/I[S Hale/ )NITORrNG LOCATION "T" INDIGATFS TOP? "U" INDICaTL:S MIDDLE? ^41' INDICATES BOTTOM. ._ ?E= MIT :JR AO!IITI l l N RTES? ' ; Mr:NTS AiN:_ RF= C+UlI ; _M—NTS. 0A Form 3320-1 (08-95) Previous editinf� -, `Te used. (REPLACES EPA FORM T -A.0 -1 HR j 'NOOO1/..'7r' s17-1435 1 f ,HMI 1 ILL NAMLiAUJY, 11--l" - .: y,....,r1 NAME MAR IC URE TECHNOLOGIES, INC ADDREss MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION NTTN: VITO L CAPORUSSn_ PRFSTDFNT NAIIUNAL POLLUTANT DISLAdlIkE EOMINATIUN 5Y5TLM /Nf UESI DISCH?AR16E M RING REPORT DMRI PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO DAY I I YEAR MO DAY FROM Vil 081 01LIT01 12&211 122-23) 124-2HI nn -»r 12A-1411 ._'n Iff Form Approved FIXED WQM OFFSHOR4 (SUBR 01) pprove4altpi► -31-98 F — FINAL 1103 MINOR EFFLUE _ *** NO DISCHARGE 1_1## NOTE: Read Mntruadolls before enmoletina thin form_ PARAMETER (32-371 (3 -Cord Only) QUANTITY OR LOADING (46-63 54-61 (4 Cord Only) QUANTITY OR CONCENTRATION (38-45) (46 154-61 NO. EX 2-63 FREQUENCY OF ANALYSIS (64-68) SAMPLE TYPE (69-70) AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS SAMPLE MEASUREMENT *#dt#** ###*** �j / ► Q / 7.495 ( 12) a s J0400 U 0 O . .EE COMMENTS BELOW ***# SU PERMIT �{EQu�REMENI`; 6.0 M M �•O WICE MONTH RAB �H SAMPLE **#**# **#**# 97MEASUREMENT w/4- ###*## 8, Q ( 12) #.? 0400 N. U O SEE COMMENTS BELOW *** **#* SU PERMIT REQUIREMENT ****** ****** 6*0 MINIMUM 9 0 MAXIMUM WICE/ MONTH RAS SALINITY SAMPLE MEASUREMENT / a O ( 32) r7� „ 19 j0480 T 0 0 JEE COMMENTS BELOW *#* ***# PPTH PERMIT REQUIREMENT ****** **#*** ****** ****## REPi)RTTWICE/ DAILY MX: MONTH '.RAB SALINITY SAMPLE MEASUREMENT ****** *>e<**** ***##* **##*# p? 9• ( 32) '0480 U 0 O SEE COMMENTS BEL QW ***# PPTH PERMIT REQUIREMENT REPORT DAILY MX WICE/ MONTH RAB :ALINITY SAMPLE MEASUREMENT ***#*# ####** #****# ####** �9.: D ( 32) aAOer 3x3480 W 0 O I -EE COMMENTS BELOW PPTH PERMIT REQUIREMENT REPIf;T t1AiLY l4X' WICE/ MONTH RAB 'ITROGEN! TOTAL (AS N) SAMPLE MEASUREMENT �.' 19) ac/3D �RAL7 ,0600 U 0 0 IEE COMMENTS BELOW *#** MG/L PERMIT REQUIREMENT REPORT GAILY MX WICE/ MONTH RAB tITROGENV .TOTAL (AS N) SAMPLE MEASUREMENT *****# ***#*# ****#* ***#** O. �Q ( 19) �/� nD Q CarlcAU 10600 W 0 0 .EE COMMENTS BELOW MG/L I PERMIT REQUIREMENT REPORT DAILY X WILE MONTH RA NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I gERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN. AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE, SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1-1 AND 33 U.S.C. 1 1319. owwo " "wer puss mens msy kwluas Nn" W to $ to And r Immkiw.n �wfmawaw of berwsn 6 m as and 5 ysr:) ATInMc roar .e,. -n _.._ �...e r.___1 TELEPHONE DATE mcw S f o 6 q77��7 5"/AREA ID ? J Q / SIGMA000 OF f7pNCVAI EXECUTIVE OFFR" OR AUTHORIZED AGENT TYPED PRINTS -nuuCM7C Alun CYPI AMA'nnlu nC euV XIMI COQ NUMBER CODE YEAR MO DAY LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLES "i11" INDICATES BOTTOM, EE PERMIT FOR ADDITIONAL NOTES? COMMENTS AND REQUIREMENTS. -PA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00002/970917-1436 PAGE 2OF 11, NA ME MAP IST URE TECHNJLOGIES, INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRFSIDFNT l.Y —NA, I",LL(U IANI UI' hC.�c..l 11���.LiiJN ;.i:IiLM i14PL/L.�lj FUrrll/- ppr(,Vb DISCHARGE ORING REPORT (DMR/ 2-16 17-19 FIXED NQM OFFSHORr"2 4 ' (SUBR Ol) PProve1 eac os"31-9s PERMIT NUMBER IDISCHAnoE NUMBER F — FINAL 1 G MONITORING PERIOD MINOR YEAR I MO I DAY YEAR I MO DAY EFFLUE _ FROM TO ##* NO DISCHARGE /?Q?fl /7?.931 /9L761 19r-971 nw-101 fwl. ata NATE: Real biat ladmw befam nnmnietind thin farm PARAMETER r3 Card Onlyl QUANTITY OR LOADING 14 Card Only/ '- QUANTITY OR CONCENTRATION NO FREQUENCY SAMPLE 132-371 146-5 54-61 38-46 146 64-61 OF TYPE AVERAGE MAXIMUM UNITS MINIMUMEX AVERAGE MAXIMUM UNITS AN/1LYSIs 2-6J r64-66) 169-700 PHOSPHORUS, TOTAL SAMPLE MEASUREMENT #*#**# ***#** ****** ##**#* / D ( 19) '? (AS P) �/ 00665 U 0 O PERMIT RE PORT, 1:ICE/ RAB SEE COMMENTS BELOW REQUIREMENT #>«## DAILY NX. MG/L MONTH PHOSPHORUS1 TOTAL SAMPLE Q„� ( 19) %��-7 A/..7� (AS P) MEASUREMENT 00665 it 0 0 PERMIT REPORT NICE/ 'RAID SEE COMMENTS BELOW REQUIREMENT ##1Ic# DAILY MX MG/L MONTH CHLOROPHYLL A SAMPLE MEASUREMENT /r65 ( 2$) 01/ --.3 0, ego 32230 T 0 0 PERMIT REPORTI"1ICE/ RAS SEE COMMENTS BELOW REQUIREMENT' ##* DAILY MX UG/L MONTH NITROGEN, AmmnNIA, SAMPLE #***#* ****#� ***#*# ****** ( 19) TOTAL (AS NH3) MEASUREMENT 6403 �/�o 6ej* 34726 U 0 0- PERMIT REPORT IMONTH WICE RAB ' SEE COMMENTS BELOW! REQUIREMENT #** DAILY MX MG/L �iITROGEN, AMMONIA, SAMPLE *####* *#*#** **#**# *##*** ( 19) TOTAL (AS NH3) MEASUREMENT I� 341�7Z6 W O 0 ## PERMIT * # *###** ### # #*#**# REPORT iiIGE RA$ SEE COMMENTS BELOW REQUIREMENT' ### OAILY= NX' MG/L MONTH SAMPLE MEASUREMENT PERMIT REQUIREMENT` SAMPLE MEASUREMENT PERMIT REQUIREMENT': NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER AM FAMILIAR WITH �THE INFORMATION ALTY OF LAW TSUBMITTED I HAVE SHER NY MID Blas o OED N MY INQUIRY. OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS 'TRUE, ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE L tCE Q SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE IS U.S.C. f 1001 AND 33 ' O U.S.C. 1 1318. Iftnawrs uador ON” ssrmaes may include rams ap to $ 10,000 SIGNATURE PRINCIPAL EXECUTIVE —17 CSE NUMBER YEAR MO I DAY TYPED PRINTED sndorm�im. krrpsarnnrtofbotwen6nwMs.aws oovj r OFFICER AUTHOR¢EDAGENT 'rr3NI#ORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE, "M" INDICATES BOTTOM. ,EE PERMIT FOR ADDITIONAL :NOTESy COMMENTS ANi; REQUIREMENTS. -PA Form 3320-1 (06-95) Previous edi;io-s - _ _ he used. (REPLACES EPA FORPkA T-40 1jK'HICu u*,_^ -N-7 110003/9'79917-1436 - 3' If 1511111111111 n LJ PERMITTEE NAME/ADDRESS,l—.d.Fa J,i).l.—. NAME HARICUL TI_J'.E: TLCHN,JL(.;',i _Jj Ifl- ADDRESS MARICULTURE TECH ,i=T }-:_Y PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTAI- VTTn i rADnawzCfi_ PQPf T111=PIT • NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPDES) DISCHARGE MONITORING REPORT (DMR) (2-16) (17-19) NY02267 02F 14 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR MO DAY I I YEAR I MID I DAY FROM virl udl TO 120-21) 122-23) 124-25) 12&271128-291 130-31) LJ Form Approved. FIXED &;,4 OFF—SHC%h BWE4D40- ($UB R 01) APProval, ax�tI, 5-31 98 F — FINAL liLL MINOR EFFLUE *** NO DISCHARGE NOTE: Read instructiorn before completing this form. PARAMETER 13 Card Onlyl QUANTITY OR LOADING 14 Card Only/ QUANTITY OR CONCENTRATION NO. FREOUENCY SAMPLE (46-531 (54-61) 138-451 146-53 (54-61J OF EX TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS (32-371 ANALYSIS (sz asJ (64-68) (69-70) TEMPERATURE7 WATER SAMPLE ###### #***** ###### *####* ( 04) DEGe CENTIGRADE MEASUREMENT PERMIT RtPORI` ; ' WIDE/ RAS flfliilfl T 0 0 SEE COMMENTS BELOW REQUIREMENT ***#QA ILY1� DEG* G ttf}!�1 EMPERATUREI WATER SAMPLE ###### *#**#* **#*** *#***# �/ 19fo ( 04) �,3'O AB EG. CENTIGRADE MEASUREMENT PERMIT *�k#*�k�k ####�R ##Jk#tT WICERAFT 00010 U G 0 ####3kJk #** EE COMMENTS BELOW REQUIREMENT ##* €3AIi M DEG.0 MONTH EMPERATURE, WATER SAMPLE MEASUREMENT ###### ###### #*#### ###### nn �7•� { 04) j ��17 RAL EG. CENTIGRADE 'PERMIT **##** ?u*#### #*#*** RE P!]RT WIDE/ "RAB 0010 W 0 0 ***#*# *## EE COMMENTS BELOW REQUIREMENT**# IIAILY xx DEG.0 MONTH XYGEN9 DISSOLVED SAMPLE #####* ###*** / 7 ###### *##### ( 19) .'� /3 (DO) MEASUREMENT (p / D '4R/4,6 PERMIT REPORT ***### ##*### ` TWICE/GRAB 0300 T G 0 EE COMMENTS BELOW REQUIREMENT ### DAILY MN MG/L MONTH XYGEN9 DISSOLVED SAMPLE MEASUREMENT ###### *#*##* 6. 7 #*#### ##*##* ( 19) a�3a �R•'�= (DO)_ PERMIT #**#*# REPORT TWICEARAB 0300 U + 0 *####* ### EE COMMENTS BELOW REQUIREMENT ### DAILY MN MG/L MONTH XYGENI DISSOLVED SAMPLE MEASUREMENT � / *##### #*#*## ( 19) 1/— ( 00) ij -PERMIT #*#*## REPORT *####* ****## BICE/GRAB 0300 W 0 0 ###### * ## EE COMMENTS BELOW REQUIREMENT *## DAILY MN MG/L MONTH ALINITY SAMPLE #####* ##*#* *##### #*#### 30110 32 07/gyp C�2191B MEASUREMENT 0480 T 0 Q PERMIT REPORT WIC A EE COMMENTS BELOW 1REnUIREMENT *** DAI Y MX PPTH MONTH NAMEITITLE PRINCIPAL EXECUTIVE OFACER I CERTIFY CINDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN: AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE ;- OBTAINING 7HE INFORMATION, I BEUrA THE SUBMITTED INFORMATION IS ^,,' TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIPNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING L-868ros Pies 1796 THE POssIBK1TY OF FINE AND IMPRISONMENT. SEE to U.S.C. 1 toot AND 33 V/ 1'114771777 10 It t U.S.C. 1 1318. #WwAim unsw o s. saiufts �y brch,* /bss up to t 10,000 SIONA OF PRINCIPAL EXECUTIVE ARENUMBER TYPED PRINTED sndwMAWNInbnodawnwue/berwssn6nwnrAssnd6yom,&J OFFICE ORAUTHORIZED AGENT CODE YEAR MO DAY COMMENTS AND EAPLANA IIVN Vr ANT VILlLA I IUMM, 1rr rarOnCa N/ al(8CnM&nr8 n0/Bl MONITOrRING LOCATION "T" INDICATES TOPv "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM. SEE PERMIT FOR ADDITIONAL NOTES1 COMMENTS AND REQUIREMENTS. EPA Form 3320-1 108-951 Previous editions mny he used. (REPLACES EPA FORM T-40 WHICH MAY NOT RE USED.)nnn 13 /�7^4 7_1 A PAGF 1 r i AMI I ILL NAMLiAU ,�rMwe,r.,,,,,,, NAME MARK URE m. ., .. ...; ..,,,,, TtCNNUL�IGIEST INC NATIONAL POLLUTANT DIS E ELIMINATION SYSTEM /NPDESI Form Approve DISCHARGE M�RING REPORT OMR) ift 2-fs 17-1 FIXED WQM OFF-SHrN 1fF 1-98 ADDRESS MARICULTURE TECH NFT PEN (SUER 01) PPfO1 PO BOX 461 PERMIT NUMBER DISCHARGE NUIIMBER F — FINAL YEAR GREENPORT NY 11944 MONITORING PERIOD MINOR ?OF FACILITYYEAR I MO DAY I YEAR MO DAY EFFLUE _ LOCATION FROM 971 081 011 To 1 971 031 311 *** NO DISCHARGE ATT N : V I TO L . CA POR U S S O PRESIDENT 124211 122-23) 124-261 126-271 128-29) !30.311 NOTE: Read kwUuedons before completing this form. PARAMETER (3 Card only! QUANTITY OR LOADING (4 Card only! QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE 132-371 1>< 46-6 54-61 36-451 146-63 164-61 EX TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2-63 ANALYSIS ANALYSIS /64-6M (69.701 SALINITY SAMPLE 4444** 4444** 4444** 4444#* ( 32) MEASUREMENT 100480 U 0 O PERMIT WICE/ RAS I�SEE COM N REQUIREMENT' 4444 -REPORT (SALINITY SAMPLE ( 32) QQ MEASUREMENT J0480 W 0 0 mak# PERMIT #*** * **#**# 4444** ***mss* REPORT VICE RAR SEE COMMENTS BELOW REQUIREMENT' 4444 AIIf 147t< PPTH MONTtq SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT NAME/TITLE PRINCIPAL EXECUTIVE OFFICER i CERTIFY UNDER PENALTY OF LAW THAT 1 HAVE PERSONALLY EXAMINED AND ARI FAMIUAR HATH THE INFORMATION SUBMITTED HEREIN; AND BASED ON TELEPHONE MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE r'1 r S+T SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING r7 X77 Vl {� V THE POSSIBILITY OF RNE AND IMPRISONMENT. SEE 18 U.&C. S 1001 AND 33 s A pplN Al EXECUTIVE AO U.S.C. i 1318. /13/MMiib uWer tlrar abetter may hckI174 ling w to S 10,000 TYPED PRINTED and ortrralrhaan A�ManYatrnant dbtwaan a trwnrba and 6 1"ana / O OR AUTHORIZED AGENT CODE NUMBER COMNlENTS AND EXPLANATION OF ANY VIOLATIONS (Reference aN etfechments here) zONITORING LOCATION "T" INDICATES TOP( -U- INDICATES MIDDLE AND -W- INDICATES BOTTOM. =EE PERMIT FOR ADDITIf:SAL NOTES( COMMENTS AND REQUIREMENTS. PA Form 3320-1 108-951 Previous editions may be used. IREPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00014/970917-1436 DATE YEAR MO DAY ?OF PAGE ,tHMITTEE NAME/AU/lncWe.ix,6n ..,,.,. .... ,,,,.,.: ,-,,,U.,rnq NAME. MAR IC URE TECHNULOGIES, INC ADDRESS MAR ICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANT DIS ELIMINATION SYSTEM (NPDES/ Form Approve DISCHARGE M* RING REPORT DMR/ 2-16 17-19 FIXED NQM OFF-SHO!MtME, '26 OAF M(S U8 R 01) APP'ove4 e�}, 5-31-95 PERMIT NUMBER DISCHARGE NUMBER F — FINAL 1 MONITORING PERIOD MINOR YEAR I MO I DAY I I YEAR I MO I DAY EFFLUE _ FROM V11 Ual 011TO1*** NO DISCHARGE (20.211 122-231 124-251 126-27) 12e-29, X30 s11 NOTE: Read kntruedone before completing this form. PARAMETER (3 Cord Only) QUANTITY OR LOADING 14 Cord Only) QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE 132-37i1>< 146-5 54-61 138-45 146-53 64-61 OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS =-6J AN-MFX 1644-68 )) r69 -7a �TEMPERATURE, NATER SAMPLE ****** ****** *1 *** #****# ( 04) n 'Q/4 ,)EG, CENTIGRADE MEASUREMENT Q /q, / d�/3O IJ0010 T 0 O PERMIT REPORT NICE/ RAS 'SEE COMMENTS BELOW REQUIREMENT *#* DAILY )tX DEG.0 MONTH TEMPERATURE, NATER SAMPLE ****** ***** ****** ****** ( 04) )EG. CENTIGRADE MEASUREMENT aO•Q �/ dQ �7to )0010 U 0 O *** PERMIT *�k*rk## #### ****** ***##* REPORT MICE/ RAS ;SEE COMMENTS BELOW REQUIREMENT *yI*# DAILY -MX DEG.0 MONTH TEMPERATURE, NATER SAMPLE ****** ****## ****** *#***# ( 04) A130 )EG. CENTIGRADE MEASUREMENT -617 /PAI )0010 W 0 0 **# PERMIT #####* #**#** **#*** **#### REPORT - MICE/ 'RAS ,-EE COMMENTS BELOW REQUIREMENT #** DAILY MlE> DEG.0 = MONTH sXYGEN, DISSOLVED SAMPLE MEASUREMENT ***** **#** // /� ****** ***** ( 19) nn/ (DO) ')0300 T 0 0 *** PERMIT *****# **#*** REPORT *********** NICE/ RAS :iEE COMMENTS BELOW REQUIREMENT *** DAILY MN MG/L MONTH )XYGEN, DISSOLVED SAMPLE ***##* #*** p r ***mss# **>t<*** ( 19) a (DO) MEASUREMENT D 108 )0300 U 0 O ** PERMIT **###�* *##*** REPORTMiGE/ PIMONTH RA$ .'EE COMMENTS BELOW REQUIREMENT *it* DAILY MN MG/L "XYGENI DISSOLVED SAMPLE ****** ****** *****# ****** ( 19) (00) MEASUREMENT �j l t 6 j03OO N O O ** PERMIT #***** ###**# REPORT *#**** ****** MAS 3EE .COMMENTS BELOW REQUIREMENY- *# DAILY MN MG/L MONTH 'H SAMPLE *#*#*# �k###*# *#**** /� L ( 22 'A/3O MEASUREMENT /��� /f D v S ,10400 T 0 0 * PERMIT *#**tklk **#**# 6.0 ****** 9.0 ifiCE RA8 FE COMMENTS BELOW REQUIREMENT *** MINIMUM 4 MAXI M SU MONTH NAMEn TLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAN THAT I HAVE PERSONALLY EXAMINED AND TELEPHONE AM FAMILIAR WITH TWE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR DATE OBTAINING THE INFORMATION, i BELIEVE THE SUBMITTED INFORMATION IS _ - / r TRUE, ACCURATE AND COMPLETE I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING VN L'. Y * G� V,-6 THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE tB U.S.C. 17001 AND 33 U.S.C. f 1318. Mendtlss www ffiiss mftfts msy &wAi It rs+ss Itv to $10,000 sndormawNma"krwiswwwWofbetw~6monthsand 6ywnl wTin 1l SIGN TURF PRINCIPAL EXECUTIVE OFFICER OR AUTHORIZED AGENT trYPED 09 PRINTED wu ATgnV ne AKIW \IIn1 C0� NUMBER YEAR MO DAY ?9NITORING LOCATION "T" IMDICATFS TOP, t'U'r INarCATES MIDDLE ANO -W- INICATES BOTTOM* EE PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS. PA Form 3320-1 (08-95) Previous editio-s tie used. fREPLACES EPA FORM T -an VlrPirw u . -- N ?E USED ' 00023/')7 7-1435 - 1° u e r ,-0AM111LL NAML/AU ll—dlk-ll— - - Panii NAS MARK URE TECHNOLOGIES, ADDREss MARICULTURE TECH NET PFN PO BOX 461 GREENPORT NY INC 11944 FACILITY LOCATION ATTN: VITO L.CAPORUSSD. PRESIDENT MAliONAL PULLUTANT DISC E ELIMINATION SYSTEM /NPDES/ DISCHARGE MING REPORT OMR( 2-16 17-19 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO DAY - YEARMO DAY FROM 97 OS 1 TO 971 081 8 31 120-211 122-231 (24-251 /26271 (28-291 130-31) Form Approved FIXED WQM OFF—SH� (SUER 01) ^�ovkaa�r31-88 ' F — FINAL MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read irwoucdone before completing this form. PARAMETER (32-371 >< (3 Cord Ont/ QUANTITY OR LOADING 6 (453 (51-61 14 CoEN Card Only/ QUANTITY OR CONCENTRATION /36-451 14653 - 64-61) NO ' EX 2 -ba) FREQUENCY OF SAMPLE ANALYSIS TYPE 164-681 169-71p AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS PH SAMPLE12) MEASUREMENT / 00400 U 0 0 SEE COMMENTS BELOW ##* Su PERMIT REQUIREMENT * *#>te* #***** 6*0 KINIMUM, *****# 900 MAXIKUK, MICE/ RAB MONT PH SAMPLE MEASUREMENT ###### *##### #*#### ( 12) 00400 N 0 O ### PERMIT �k*##*# #*###* 6.0 ****## 940 NICE RAB 1 SEE COMMENTS BELOW REQUIREMENT ' **** MINIMUM MAXIMUM SU MONTH SALINITY SAMPLE MEASUREMENT ##**** ****## ##**** ****#* ( 32) ! g 00480 T 0 0 *** PERMIT ****** *##**� �k#�k*** - ##*# l l aREPt1RT MICE RAB SEE COMMENTS BELOW REQUIREMENT:. **** 3AIL'Y, MX PPTH MONTH SALINITY SAMPLE MEASUREMENT #*###* *****# **#*#* *****# ( 32) 00480 U 0 0 SEE COMMENTS BELOW **# **** PPTH PERMIT REQUIREMENT' at** # #*##*# #*###* #*#### REPORT DAILY < XX MICE/ RAW MONTH SALINITY - } SAMPLE MEASUREMENT *****# **##*# ****** ****#* ( 32) Q 00480 fit O 'b *#* PERMIT ##*# *##### #***#* *##*# REPORT MICE/;RAS SEE COMMENTS BELOMt REQu�REMENT #*#* DAILY MX PPTH MONTH NITROGEN, TOTAL (AS N)'• SAMPLE MEASUREMENT *#***# ***##* **#*## ****#* C%/� ( 19) - -:1130&P0600600 U -0 D **# PERMIT ****** #***** ****** . REPORT MICE RAS SEE .COMMENTS BELOW REQUIREMENT' - #*## DAILY MX MG/L MONTH NITROGEN, TOTAL ' (AS N) SAMPLE MEASUREMENT ****## *�***# *#**#* ****#* i Q ( 19 2/ 00600 M 0 O ### PERMIT ***** ***** #** ** *# *# ';REPORTTWICE/ ', a SEE COMMENTS BELOW REQUIREMENT -1:: *#* dAILY M7f MI6/L 140NTH NAMElTITLE PRINCIPAL EXECUTIVE OFFICER f:PENALTY ONIVNTNVLYNDI�OVVIE IfOAno8UB1lrED HIABASED o1 MY WOUBTY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTANIING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION. INCLUDINGIX THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.G. 1 1001 AND 33 U.S.C. f 1319. (f -oldes .nd r Ann s&*,ft, n.y k cAwb Anes qe w $10,000 and o.m�rhM.nimlaiawnunraeawow6�narasand6y..sJ ' 4V , 1weA SIONA of wllNcaAL EXECUTIVE O oRAUTHORREDAGENT TELEPHONE GATE ` LJ r r4a rticso f ICED { /6 ! 7 177 1 D + TYPED PRINTED � NUMBER YEAR MO DAY COMMENTS AND tMgLANA I wN Ur ANY V IULA I TUNS Inererence an errecrUnenrs neral MONITORING LOCATION "T" INDICATES TOP1 "U" INDICATES MIDDLE AND "i!" INICATES BOTTOM. >FE PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS* EPA Form 3320-1 f08-951 Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) OJT D24/ 9799 17-143 6 PAGE 2 O 0 NAME MARIG URE TLCHNOLUGIES, INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT U14A1 IULLUTANl UsL L LL111-AhUN S151LM INNDES) Form Approved. DISCHARGE M RING REPORT (DMR) 2-16 17-19FIXED WQM OFF—SHORWI WE40 r26 03F: ( SUB R 01) Approvaie2lr4 -31-88 PERMIT NUMBER DISCHAIwE NUMBER F — FINAL MONITORING PERIOD MINOR YEAR I MO I DAY I I YEAR I MO I DAY EFFLUE _ FROM Vrl Ut5l 011TO1*** NO DISCHARGE r *#* 1242 f/ 122-23/ 124-25) t2B27i I2a-291' tin wo NOTE: Read inatrucdona before oonwielirm thio form. PARAMETER (3 Card Only/ QUANTITY OR LOADING (4 Cord Oddy) QUANTITY OR CONCEN I RATION NO. FREQUENCY SAMPLE !32-371 I>< 46-5 (64.61 38-46 46 54-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS z -6s ANALYSIS 164-66i (6s-701 �'HOSPHORUS, TOTAL SAMPLE MEASUREMENT *#**** **#*## **##** *****# M ( 19) � (AS P) NV 1 Q ��Q6 =10665 U 0 0 ##* PERMIT 1Ir>K## �k1k**## ****** ###*#* REP13RT NICE/ RAS ;SEE COMMENTS BELOW REQUIREMENT. *#* DAILY l4X M619j MONTH "3HOSPHORUS, TOTAL SAMPLE *#**** #*#*#* **#*** ****** (AS P) MEASUREMENT Q / � 3� j7665 W 0 0 1R#* PERMIT *>iL1ic##>I< �k**#>{�# *#**## ##(�t�tApk REPt?RT WICE/ RAR 7EE COMMENTS BELOW REQUIREMENT #**# IIAIL 'MiL< M6/L IMONTH --HLOROPHYLL A. SAMPLE **#*** **#*#* #*#**# **##*# ( 28} MEASUREMENT // ��% a 3Q 2230 T 0 0 *# PERMIT **#*#*> **�k*** *####1k #1R#**#. RE PORT TWICE/ GRAB EE COMMENTS 3EL04i REQUIREMENT ### DAILY RK UG/L MONTH -ITROGEN, AMMONIAlt SAMPLE. #####* #**##* **#*** ##*# ( 19} TOTAL (AS NH3) MEASUREMENT '-4726 U 0 0 PERMIT REPORT WICF/FAB �F COMMENTS BELOW REQUIREMENT' ### DAZLr MX. M6/L MONTH NITROGEN, AMMONIAO' SAMPLE #**#** ****** *##**# ##**, / t 19) TOTAL (AS NH3) MEASUREMENT Qr 54726 W 0 0 # PERMIT :Ic1R>l[rillt #*�Ic#1k 1I[ #1k�k#*# #*#*## ifEPf1RT WIGS% SEE COMMENTS 3ELOW REQUIREMENT #*# DAILY 14X MG1L MONTH SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND TELEPHONE AM+FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS DATE ` L• TRUE, ACCURATE 'AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING r }� 2 D S , f THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE IS U.S.C. s 1001 AND 33 U.S.C. 1 1319. IArndd" wtdw P -, sonvnea m.y incudo files up ro $ 70,000 and ornwrimlrrlknpdswwwrofMMNn6months rrdsy.) ATInIC I��t�-_��� _II_u__I.___._ SIONA E OF PRINCIPAL EXECUTIVE OFFI OR AUTHORIZED AGENT �b % %77 ' c� PED PRINTED •In cVd A�IATIA\I Ac AVIV \/1 nt AREA CODE NUMBER YEAR! MO DAY )NI-TORING LOCATION "T" INDICATES TOP, NU" INDICATES MIDDLE AND OWN INICATES 130TTOM. `E PERMIT FOR ADOITICNAL NOTES, COMMENTS ANO REQUIREMENTS. PA Form 3320-1 (08-95) Previous editions -,pv be used. (REPLACES EPA FORM T -AO WHICH V,=` -N^7 ?E USED 1� 17c 00025/97+7917-143b 3 c^ 'LHMITTEENAME/AUilkWd.rsahr,I.,.,.,.,.,r,..rnfJ..mr "A""E. MARICUCTURE TECHNOLOGIES9 ADDRESS MARICULTURE TECH NFT PEN PO BOX 461 GREENPORT N YINC 11944 FACILrrY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANT OIELIMINATION SYSTEM /(NPDES) DISCHARGE M ING REPORT DMRf f17 -d) F26 04F M PERMIT NUMBER (NBCHINW NUMBER . MONITORING PERIOD YEARI MO DAY I YEAR MID I DAY FROM Vfj UUJ TO V11 U451 31 (20.21) 122-231 r24-25) 126.271 128-29/ (30 If Form Approv FIXED WQM OFF—SHO W- 10, (SUER 01) �fO4� 31 -as F — FINAL MINOR EFFLUE _ w** NO DISCHARGE NOTE: Read Instructions before completing this form. PARAMETER ' /32-371[>< (3 Gid Onlyl QUANTITY OR LOADING 146-5 /51-61 N Card Only) QUANTITY OR CONCENTRATION 38 -IS I6-6 64-61 NO. EX 2_6s FREQUENCY SAMPLE OF ANALYSIS TYPEr6� ss) (699.701 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS ;TEMPERATUREI WATER _1EG, CENTIGRADE SAMPLE MEASUREMENT ****** *###*# #*#**# ****rt*%9� ( 04) '70010 T 0 0 )EE COMMENTS 6ELOW ###�Ir DEG•C PERMIT REQUIREMENT REPORT (-1 ILY Nx ' WICE/ RA$ MONTH TEMPERATURE, WATER IEG• CENTIGRADE SAMPLE###### MEASUREMENT **###* #**#*# **#**# G /9. / ( 04) -0/3-0 612WI :0010 U 0 0 SEE COMMENTS BELOW ###### ### *#* DE6.0 PERMIT REQUIREMENT ##I#Ik## ###### #*### REPORT DAILY' MX' WICE/ RA$ MONTH -I'EMPERATUREV WATER Eu• CENTIGRADE SAMPLE MEASUREMENT ***#*# *>�**** #**##* ****** nn �Q� i.� ( 04) ;,t&g g 10010 W 0 0 ;EE COMMENTS BELOW ### DE-G.C. PERMIT REQUIREMENT: F***##*' ***## REPORT DAILY; 14X'' WILE/GRAS TMONTH XYGENI DISSOLVED. (DO) SAMPLE MEASUREMENT ###### #####* /0 40 ##*### #**### ( 19) :0300 T 0 0 PERMIT REPORT ##*#*"P ##'P'P*# WICE/ RAB EE COMMENTS BEL W REQUIREMENT` *## DAILY MN MG/L MONTH iXYGEN9 DISSOLVED (00) SAMPLE MEASUREMENT ##rk#*# ###### 7 ####*# ###### ( 19) R 10300 U 0 . 0 PERMIT REPORT*** ***# TWICE /GRAB EE COMMENTS BELOW REQUIREMENT *** DAILY MN MG/L MONTH IXYGENa DISSOLVED (DO) SAMPLE MEASUREMENT *****# ##**** �j ' *#***# ****#* ( 19) a, 3 o 6) X300 W 0 0 *##**# *# PERMIT #**### REPORT #***** **#*** WICE RAB EE COMMENTS BELOW REQUIREMENT ##* DAILY MN MG/L MONTH ;ALINITY - SAMPLE MEASUREMENT �'�i d Q 32) a�3o`J :0480 T 0 0 **#*#* ** PERMIT *#**** ***##* ****# REPORT idICE rRA3 t COMMENTS BELOW REQUIRE NT #�c# DAILY MX PPTH MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I OERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE IN SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FWE ANO IMPRISONMENT. SEE IS U.S.C. 1 1001 AND 33`0 U.S.C. 1 1319. Iftwi nlm weds( dross sdndox nwy incWa renes up to s 10,000 and ormsxrmsni�aisarr�snrdbonvoon6monMssnd5ywsl - TELEPHONE DATE - �c 10 It—q' r.. W4 CSI) SKiNATURf EXECUTIVE OFFICER AGENT AUTHORIZED PED OR PRINTED AREA CODE NUMBER YEARS MO 1 DAY .vmm�nr� ..rev �... �.+............. .-.... .,..,�.. ,..,,.., n.o.Q.o....o w. o..o.......onw .,o.oi `➢NITORING LOCATION "T" I"IUICATES TOP, "U" INDICATES MIDDLiL- AND -Wx' INDICATES BOTTOM, =E PERMIT FOR ADDITIONAL NOTES9 COMMENTS AND RF'�UIREMENTS. PA Form 3320-1 (08-95) Previous editions ev ',e used. (REPLACES EPA FORM T- O }Arwlr;ia V! N^- PE UScn I `� `�Q033/�7i���17-1436 I PL14MI t TEE NAME/AU t]—A,d. {xd,,. NAME MARK URE TECHNOLOGIES, INC ADDRESS MARICULTURE TECH NFT PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION NATIONAL POLLUTANT DISCAME ELIMINATION SYSTEM /NPDES) Form ApprovedAh DISCHARGE MCMFRING REPORT DMR) 246 17-19 ED WQM n4,p j4 (SUER Ol) FIXOFF-BHI ppr,??e 1-98 PERMIT NUMBER DISCHARGE NUMBER F - FINAL °°�� -- MONITORING PERIOD MINOR YEAR I MO I DAY YEAR MO DAY -EFFLUE _ FROM VII P81 OlITO[***,NO DISCHARGE A 1 1 M= V 1 1 U L I.A P U K U 5 bUq N 1: t S 1 Ut N 1 /20.211 122-23) 124-251 /26271 (28-291 /30.31) 11100TC Ke" Instrualloris beton cot *10 this form. PARAMETER 132-371I>< /3 Cerd 0n/y1 QUANTITY OR LOADING 4653 54-61 /4 Card OnMI QUANTITY OR CONCENTRATION /38 451 /465 164-61 NO. EX 2-" �E Ct' OF ANALYm (6I-881 SAMPLE TYPE (69-700 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE, MAXIMUM UNITS SALINITY SAMPLE MEASUREMENT *****# *#*#** ****** ***** 331 ( 32) SAMPLE 8 00480 U 0 O SEE COMMENTS BELOW *** ***>!c PPTH PERMIT REQUIREMENT *#*# ****** ***** *#**** ;RPtIRT `:itKE Y' MX.' t- N KAH SALINITY SAMPLE MEASUREMENT *****# ****** *,«,«*** ****** 32)/3D 00480 W 0 O SEE COMMENTS BELOW **** PPTH PERMIT REQUIREMENT RFPitRT AI.'T'rMX MON ffl SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT ioNITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W" IMDICATES BOTTOM. 'SEE PERMIT FOR ADDITIONAL NOTES? COMMENTS AND 'REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. IREPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) J0=334/970917-1+36 PAGE 2 O "b PERMIT REQUIREMENT SAMPLE t- MEASUREMENT PERMIT REQUIREMENT > SAMPLE MEASUREMENT PERMIT - - REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT NAM�/TITI.E PRINCIPAL EXECUTIVE OFFICER FAMILIAR V TH THE DER w�lA ONTSUBMrrTEED Mme; AND EXAMINED MY INQUIRY OF THOSE SIOIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE BIFORMATRMI, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. 1 AM -AWARE :THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND WPIYSONMENT. SEE 11 U.S.C. s 1001 AND 33 U.S.C. S 1319. 0%owNes widw Nom sa*ms nwy kwkl& lives qo to S 10.000 n and ornUxkM igarb0ARww0fb0rw0n6nwn0wand5Vw I t:N3NA PRINCIPAL EXECUTIVE OFFICER AUTHORIZED AGENTA TELEPHONE DATE VRD pies -t C-) TYPED OR PRM"® 7-I?7 7 10 CODE NUMBER YEAR MO DAY COMu.gNTS AND EXPLANA OF ANY VIOLATIONS IRef~cs aff attachments here/, ioNITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W" IMDICATES BOTTOM. 'SEE PERMIT FOR ADDITIONAL NOTES? COMMENTS AND 'REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. IREPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) J0=334/970917-1+36 PAGE 2 O "b -'LFIMITTLE NAML/AUtl—Ad,i—I... .... NAME. MARK*URE TECHWILOGIESV INC ADOREss MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANT DISq9ftE ELIMI%ATION SYSTEM /NPDES) Form Approv DISCHARGE M RING REPORT DMR) 2-16 1Oink 7-19 ROTATING WQM OFFS%)"- S (SUER 01) Approve` sY 147; -98 PERMIT NUMBER DISCHARGE NUMBER F — FINAL 1 L 74 MONITORING PERIOD MINOR Y AR I IdO I DAY I I YEAR I MO I DAY EFFLUE _ FROM _ TO I V f 1 015 1 = *** NO DISCHARGE !20211 122;231124-26J 126-271 128-291 130311 NOTE: Read instructions b•fom completing this form. PARAMETER /3 Card Onlyl QUANTITY OR LOADING (4 Card Only) QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE /32-37/ �>< (46-6 (54-61) (38.46) 46-63 64-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2-63 ANALYSIS 164-681 (69-701 TEMPERATURE, WATER SAMPLE MEASUREMENT /� { 04) sS13D /�� )EG• CENTIGRADE Q�LJI 6A45 �J0010 T 0 0 #***#* ##* PERMIT * #* # ****## ##*#** REPORT WICEf -RAO SEE COMMENTS BELOW �' REQUIREMENT' *,«*# Q Y Y< MX DEG• C ': t4flNTH TEMPERATURES WATER SAMPLE *##### ##*### ****** ****** { 04) �j ?F_G• CENTIGRADE MEASUREMENT �D, gf�3Pg 1'10010 U 0 0 #**#** #** PERMIT *3k** *#*** **#*## REPORT WICE/ RAO !;EE COMMENTS BELOW REQUIREMENT ### DAILY '< MX DEG•C MONTH TEMPERATURE, WATER SAMPLE MEASUREMENT �Q/Q 04) Q/ grR .,EG, CENTIGRADE .)0010 W 0 0 PERMIT'**#* REPORT WIDE/ RA8 ;:SEE COMMENTS $,ELOQ. REQUIREMENT; *** DAILYMX DEG.0 MONTH )XYGENj DISSOLVED, SAMPLE MEASUREMENT ****** ***#** ****** ****** ( 19) (do) )0300 T 0 0 ##****' ## PERMIT ****4i* REPORTWICE/ RAO ;EE COMMENTS BELOWREQUIREMENT **# DAILY MN MG/LF-MONTH- 3XYGENjDISSOLVED. SAMPLE ###### ##*##* *****'� **�`*'I`* ( 19) (DO) MEASUREMENT a0 G1QAg )0300 U Q 0 *##*#* *# PERMIT *#* ** REPORT ****** *** ** TWICE/ GRAB SEE COMMENTS BELOW REQUIREMENT #*# DAILY MN MG/L MONTH 3XYGEN, DISSOLVED SAMPLE **s*** **x�*** // 1p `t ****** *** * ( 19) n (DO) MEASUREMENT i 'al fSRA6 70300 W 0 0 # **#* ** PERMIT #***#* REPORT *##*** ****** COMMENTS BELOW REQUIREMENT' *# DAILY hIG/L H"H SAMPLE ***#** �k**##* �M%N *##### 12MEASUREMENT jWICE/RABSEE 1 �"7 1'10400 T 0 0 PERMIT 6.0###*1k# • (} 'IEE ItOMMENTS BELOW REQUIREMENT < *** MINIMUM 141IXIMUM SU MONTH NAMEMTLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT 1 HAVE PERSONALLY EXAMINED AND TELEPHONE AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR111,1A DATE OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS -t �p TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING614-n-1777.10 /1,w. SIO A OF PRINCIPAL EXECUTIVE OFFICE OR AUTHORIZED AGENT L'. e o r THE POSSIBILITY OF FWE AN IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C. S 131 Y. IPends/su wider /Mss saruns m y kwjti*e Pees ys ro $T0,000 sndormexrnurrinrpiaarrrwltolbenveNl6monMswld6ysMs) ATIAI.IC /��t�-_��� �tl �w__�.—__._ c___, , ! O TYPED OR PRINTED AMI1 CVDI AKIATIAL1 AC A/,IV \11! 1 AREA CODE NUMBER YEAR MO DAY ONITORTNG LOCATION "T" I°)DICATFS TOP? "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM, =E PEtRMIT FiIR ADDITIONAL hOTES9 COMMENTS ANi , REQUIREMENTS. -PA Form 3320-1 108-95) Previous editio-s — v be used. ,REPLACES EPA FORM T -Z0' - -slaw M. - a ccn 1 E'J.,0O07/97`a)I7—�4�. -LHMITTEL NAME/ADd-Ad,k-11m .:T. ,•.,:,.,,,. ,.lr..enq NAME MARK URE TECHNOLOGIES, INC ADoftEss MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANT OISCjjIft ELIMINATION SYSTEM (NPDES) DISCHARGE MOWRING REPORT OMR) 2-16 17-19 ROTATING NQM Form Approved Aft ql, OFFS""'.`NMI (4 Gid Only/ QUANTITY OR CONCENTRATION FREQUENCY SAMPLE (SUER 01) pproval,excll� 8 1 C 3 /46-63 (54-611 PERMIT NUMBER EX EX aSCHARGE NUMBER F- FINAL AVERAGE MAXIMUM MONITORING PERIOD MINOR AVERAGE MAXIMUM YEAR I MO I DAY V I YEAR I MO DAY EFFLUE ANALYSISN (64-688ts ) FROM V f I Ukil U1 I TO I V11 001 NO DISCHARGE (20-21/ (22-23) (24-251 /26-27) 128-291 (30.3311 NOTE: Read instructions before completing this form. PARAMETER (3 Gid On/yl QUANTITY OR LOADING (4 Gid Only/ QUANTITY OR CONCENTRATION FREQUENCY SAMPLE (32-371 >< /46-63 (54-611 /38-45) (rs-53 (54-61 EX EX OF PE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2-631 ANALYSISN (64-688ts ) (69-701 SAMPLE MEASUREMENT ##**## #####�k j� ****** ( 12) )0400 U 0 0 *** PERMIT **** #***** 6.0 ***** 9.0 MICE/GRAS -,EE COMMENTS BELOW REQUIREMENT:', *#*,t MINIMUM MAXIMUML U tMONTH PH SAMPLE ##**## ###### 1.94 ***##* fp 9� ( 12) MEASUREMENT • 20400 W O 0 ### PERMIT ###*?## ####*# 600 **#*## 00 WIC E/ RAB ,.IEE COMMENTS $FLOW REQUIREMENT, #### MINIMUM 14AXI.NUM SU 114ONT `ALINITY SAMPLE ****#* ****** ****** **#*** ( 32) MEASUREMENT �3� (� -1/30 )04$0 T 0 O PERMIT *#**# ###7R## �:REPORT fwrcmus ';EE COMMENTS BELOW REQUIREMENT; **** 3AIL-Y- MX PPTH MONTH SALINITY SAMPLE ###### #*#*## ###### ****** ( 32) MEASUREMENT 30O - 0 Gjw ")0480 U O 0 ### PERMIT **#**# ### ## ##**#* ***### ;REPORT MICE/ RAB SEE COMMENTS BELOW REauI1EMENT' ***# DAILY 14X' PPTH MONTH SALINITY SAMPLE**#*** ####** ****** ****** �a ( 32) 7 « MEASUREMENT 6 J0480 W 0 0 PERMIT: RE PORT WICE/ RAS ;EE COMMENTS BELOW REQUIREMENT *##* DAILY MX PPTH MONTH ilTROGENV TOTAL SAMPLE ****#* *#**#* #***#* *#**** ( 19) � (AS N) MEASUREMENT '_)0600 U O -0 PERMIT ##***# *#**## *** **#*** *****# REPORT' WILE/ AB `IEE -COMMENTS BELOW REQUIREMENT. **** DAILY MX MG/L MONTH JIT OGEN* TOTAL SAMPLE ###### #*#*#* #***** ****** { 19) (AS NY MEASUREMENT 0600 N 0 0 PERMIT RE PORTMICE MR -A-8 EE - COMMENTS BELOW :REQUIREMENT #### i)AI Y MX MG/L MONTH NAMEMTLE PRINCIPAL EXECUTIVE OFFICER I SERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR /A' i* Z TELEPHONE DATE . I OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS //�� TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING , 6—dw SIGN F PRINCIPAL EXECUTIVE �Qs' �/- 1,.�� THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C. 1 1318. (A nsi*# mdr ew.. so•tut*s my kwAtdo lows up to $10,000 b lo i TYPED OR PRINTED .ndornw�l� krwns now ofkotw . 6mondwand 5 yow�) OFFICER AUTHORIZED AGENT CODE NUMBER YEAR MO DAY ummCIY1a #%NW cnrv^nn t IWIM yr n—ouommmiw nvrv/ A.ONITORING LOCATION "T" INDICATES TOP* "U" INDICATES MIDDLE AND -W- INDICATES 60TTOM. FE PERMIT FOR ADDIT10i*SAL NOTES, COMMENTS AND RF�)UIREMENTS. -PA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED) ' 9008/97C917-143)6 PAGE 2 O NAME MAR IC URE TECHNOLIJCIESj INC ADDRESS MARI CULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 j FACILITY LOCATION ATTN: VITO L CAPORUSSO, PRESIDENT r. r.i—N/ VuLW[AN I ois �L I A;,QN yv51W lNNUESt Form Approved DISCHARGE M ORING REPORT (DMR) 24e 17-19 ROTATING WQM OFF CJS (SUBR 01) PProvel nr -31-98 PERMIT NUMBER DISCHARGE NUMBER F — FINAL 1 L MONITORING PERIOD MINOR YEAR I MO I DAY YEAR MO DAY EFFLUE _ FROM Yll UtJj 011TO1*** NO DISCHARGE (20.211 122-23) (24-261 /2627) /28-291 13-31/ NOTE: Read Instructions before oomvietin9 this form. PARAMETER (32-37) 1>< M Card Only/ QUANTITY OR LOADING 14663 64-81 14 Gid Only/ QUANTITY OR CONCENTRATION 13815/ (466 64-81 NO. EX z es FREOUENCY OF ANALYSIS (64-e8► SAMPLE TYPE res -lad AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS PHOSPHORUS1 TOTAL (AS P) SAMPLE MEASUREMENT *#*#** ##*##* ####*# ###*#* Q1J 19) 7� CT 00665 U 0 0 SEE COMMENTS BELOW **#* MG/.L PERMIT REQUIREMENT ' REPQRT 0*1LY. AX WICED 114ONTH RAS .1HOSPHORUS1 TOTAL (AS P) SAMPLE MEASUREMENT G1 ( 19) .� U(ta � �a IWM ,J0665 W 0 0 SEE COMMENTS BELOW *#*# MG/L PERMIT REQUIREMENT REPORT DAILY f!X WICEi MONTH RA$ '-HLOROPHYLL A SAMPLE MEASUREMENT /"71/ ( 28) ;�I 30 6406 132230 T 0 0 IiFE COMMENTS 9ELOW ### #### UGJL PERMIT REQUIREMENT; ######; -*#*### ###### #*#*## REPORT DAILY; MX: WICEJ MONTH RAB "4ITROGENI AMMONIA/ ;TOTAL (AS NH3) SAMPLE MEASUREMENT 19) ;34726 U 0 0 -iEE COMMENTS 3ELOW ### MGJL PERMIT REQUIREMENT REPORTMICE DAILY NX MONTH RAS �ITROGEN� AMMONIA* COTAL (AS NH3) SAMPLE MEASUREMENT Q 1 / a�0 AB !34726 W 0 0 ''sEE COMMENTS BELOW #* #*# MGJL PERMIT REQUIREMENT *1K?B*## ** # # **##*# I **##** REPORT DAILY'MX NWICE MONTH I, -RA B SAMPLE MEASUREMENT PERMIT REQUIREMENT` SAMPLE j MEASUREMENT PERMIT REQUIREMENT< " NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE /8 U.S.C. 1 1001 AND 33 U.S.C. 1, 1319. 1Ar/r/ess mdsr dI w sbtures m.y inekde fsrss yo ro s 70,000 sndor/rlsain/sn%IIA/IAT/M/MHolbstwsn6monthssnd6yssrsl ATIAI,IC TELEPHONE DATE L. /� $ f- Cao �,� 477-077/� 13 197 SIGNATURE PRINgPAL EXECUTIVE OFFICER AUTHORIZED AGENT YPEOO PRINTED . AAAA ASA/TC ALM GVO/ ALIATIAAI AG AAIV tl- AREA CODE NUMBER YEAR MO DAY -ONITORING LOCATION "Tn I1401CATES TOPy "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM, EE PERMIT FOR ADDITIONAL NOTESp COMMENTS ANE REQUIREMENTS. -PA Form 3320-1 (08-95) Previous editio- s - � be used. (REPLACES EPA FORM T -d(1 'A'HIc4 */ N 'F 'jSF ? I — 00009/973917-1436 3�^ 4. ,'ERMITTEENAMEIAD•S/lrMbiecrGry NAME.MARICULTURE TECHNOLOGIES, INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VTT11 L CAPORUS50. PRESIDENT NATIONAL POLLUTANT DIS E ELIMINATION SYSTEM /NPDESI Form Approve DISCHARGE M RING REPORT OMR) 2-fs 17-19 ROTATING WQM OFF NNS UMBER DI02R M (SUBR 01) PProval eYgras 3i-88 PERMIT NSCHARGE NUMBER F - FINAL MONITORING PERIOD MINOR YEAR I MO I DAY I I YEAR I MO DAY EFFLUE FROM To *** NO DISCHARGE 120.211 122-231 (24-251 126.271 (28-291 /30.31/ NOTE: Read (nsttuctions before completing this form. PARAMETER' 13 Card Onlo QUANTITY OR LOADING 14 Card On4l QUANTITY OR CONCEN[TRATION NO. FREQUENCY SAMPLE 132-371 146-5 (54-61 138-461 46-6 64-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS i 2 -es 164-681 (69-701 TEMPERATUREI NATER SAMPLE MEASUREMENT ****** ****** #*#*** **#*##c �!�• 04) a DEG. CENTIGRADE PERMIT > ##*1« **#** #*## *, REPt1RT WIC£/ "RAB , ?0010 T 0 O *#*#*# *#* SEE COMMENTS BELOW REQUIREMENT: **** DAILY SIX;' DEG.0 MONTH ITEMPERATURE� WATER SAMPLE MEASUREMENT ****** ****#* *#*##* *#*#*# aQ10 ( 04) n o�/3Q %= G. CENTIGRADE PERMIT # ### *##### ###### REPORT NICE/ RAS :0410 U 0 0 #**##* #** 3EE COMMENTS BELOW REQUIREMENT ###* DAILY MX DEG.0 MONTH FEMPERATURE1 WATER SAMPLE MEASUREMENT ##*#*Ile **#*## *#*### *#*##* n ©� / ( 04) Cif :) 2EG. CENTIGRADE pS PERMIT ##*## #*#**# *#**** REPORT 'WICE/61RAB :0010 W 0 0 **#*#* ### I�Ec COMMENTS BELOQ REQUIREMENT *#,�# 'dIL MX- D DEG.0 MONTH .XYGENg DISSOLVED, SAMPLE MEASUREMENT #**#Ile##*### ####*# ###*## ( 19) (DO) PERMIT REPORT **##** #i1>hR## WILE/ RAB 10300 T 0 0 �tE COMMENTS BLOW REQUIREMENT ### DAILY MN MG/L MONTH ?XYGEN* DISSOLVED't' SAMPLE MEASUREMENT // fjI 4.7 4 #*#### ****#* ( 19) #3Q GA.48 (DO) 10300 U 0 0 **## * * PERMIT **###*' REPORT #**##* **** WICE RAB COMMENTS, BELOW REQUIREMENT *#* DAILY MN MG/L MONTH _)EE _?XYGEN! DISSOLVED SAMPLE##**** MEASUREMENT ***#** 4,7 ****#ar ***#** ( 19 ) Al—k (DO) 61096 !40300 W 0 O #***** ** PERMIT. ***#*# REPORT. #*#***' *#**** WICE RAB ;EE COMMENTS SLOW REQUIREMENT ### DAILY MN MG/L MONTH 'H SAMPLE 3 �+ aS' 12 n�^ ��Q 6� MEASUREMENT D /� }0400 T 0 0 *##*## ## PERMIT *#**** 6.0 #*#** 9.0 WIC AB EE COMMENTS 3ELOW REQUIREMENT ##* MINIMUM MAX UM SU MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE 01101 DUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT SUBMITTING FALSE , L PENALTIES FOR INFORMATION, INCLUDING TME POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. S 1001 AND 33 V.S.C. f 1318. /Ax.i/8er ursYr Ihasa mertas may krehde Paras t9s ro t 70,000 endoffwkmwnknpsmwwwuelberw~6Morhsanwr d6ye:l ` ,I� �� / b `� Z 3 971 SIGNATURE F PRINCIPAL EXECUTIVE OFFICER RAUTHORIZEDAGENT TYP OR PRINTED AREA CODE NUMBER YEAR i MO DAY NOMMEN I S ANU CArLA111A 11UN yr mrr T v IULA I I V rv0 IrTererence .n aaacnrrrants nerel NITORING LOCATION "T" INDICATFS TOPI "U" INOICATLS MIODLEI "W" INDICATES BOTTOM. r- PERMIT F9R ADDITIONAL NnTESI CfjMMENTS A"i REQUIREME- wS. -PA Form 3320-1 (06-95) Previous editio - tie used (REPLACES FPA FOPM T-10'""�7^u .•.' �!^- RE ';SE^ I - _ - r - 9n1117/97gg17-1436 L t .f c.NMiI ILL NAMLiA44—.-i.,.,.;. ui NAM MARK TURF TECHNOLOGIES, ADDmss MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY INC 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NAI;ONAL POLLUTANT DlSjdjkIIpL LLIMiNAT10N SYSTEM /NPDES) DISCH2 R6GE M RING REPORT DMR9) PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY I I YEAR I MO DAY FROM TO Ma21) 122-231 r24 -25J 126-27/ 128-29/ 1303f1 Form Approve ROTATING WQM OFFSTpWW I�S (SU$R 01) PProval�e r4 -3 -98 F — FINAL MINOR EFFLUE _ ### NO DISCHARGE NOTE: Reed kwouadons before completing this form. PARAMETER /3? -37/1>< (3 Gid OnJ J QUANTITY OR LOADING 46- 154-611 /4 Card Only) QUANTITY OR CONCENTRATION (38-45) /46-53 /54-6/ NO. EX 2 Bs FREQUENCY SAMPLE OF ANALYSIS TYPE 164-66) 169-701 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS ,H SAMPLE MEASUREMENT *#*#** #***## h ��(!� ###*## �tO3 t12) 130 mob J0400 U 0 0 SEE COMMENTS BELOW ### #### SU PERMIT REQUIREMENT #*#*#?R ####*# 6.0 M NIM M #*#### 911 s© MAX ## , WICE/ RAS M �'H SAMPLE MEASUREMENT ###### #####* i ###### �• 10 , ( 12) i? kn4s /r3D J0400 W G 0 5EE COMMENTS BELOW ### #### SU PERMIT REQUIREMENT ###### # K##�k# 6 .0 MINIMUM *#### r3s0 14AXI14#S1M WICE/ RAB MONTH iSALINITY SAMPLE MEASUREMENT ####** **###* *####* *#*##* � - 10 ( 32) Q 6kAg )0480 T 0 0 3EE COMMENTS BELOW #### PPTH PERMIT REQUIREMENT REP€3RT aAlliMX' "WICE/;RAS MONTH 13ALINITY SAMPLE MEASUREMENT ##*##* **#*#* #**#** ##** 3Qa O 32) 100480 U D 0 .SEE COMMENTS BELOW #***###* *##* PPTH PERMIT REQUIREMENT ###### REPORT QAILY MX WICE/ RA8 MONTH SALINITY SAMPLE MEASUREMENT *#*#*# *#*##* ##*#*# ##*### ���Q ( 32) a A6 30480 W O O ;SEE COMMENTS BELOW *## *#*# PPTH PERMIT####*' REQu�REMENT< *#**## *###* ####** REPORT {DAILY' ,MX 1iICE/ RAB MONTH ♦ITROGEN� TOTAL (AS N) SAMPLE MEASUREMENT **#*## ****## *#*#*# ##*#*# t 19) �4 ')0600 U 0 0 IEE. COMMENTS BELOW ### #### MG/L PERMIT REQUIREMENTi ####:' : *####k #*#### ##### REPORT QAILY MX' WICE/ RAB MONTH , 4ITROGEN1, TOTAL (AS N) SAMPLE MEASUREMENT �2 / ( 19 of/3t? 4RAS 30600 W O 0 PERMIT REPORT V I TC, R AB SEE COMMENTS BELOW REQUIREMENT: #### DAILY MX MG/L MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER r.LFY 'LIAR INFORMATION SM SUBMITTED HEREIN; AND ON QTHERBPERSONALLY NDQ MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. IAMAWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND WIPIYSONMENT. SEE 18 U.S.C. ! 1001 AND 33 U.S.C. f 1318. 1pw-hiss www *am writes may k*dU& Anes to let 10,000 anAormorirwnielenGvnawetMtwom6monthsrW6y.sem) ArrnwrQ /n -t -_---- -.-..--L----.- �_--' i Vii• TE LEPHONE DATE 1 /Zr �C <l� _17 �l47 ' ^- y SIONA PRINgPAL EXECUTIVE OFFICE AUTHORIZEOAQENT JYM OR ...n Eva A11 Ar1A\I AC ALry 114^4 ALOE NUMBER YEAR MO DAY MONITORING LOCATION "T" INDICATES TOPV "U" INDICATES MIDDLE, "W" INDICATES BOTTOM. .Ec PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS. :PA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) PAGE OF 0001 `_i/97t�927-1436 2 , IAM I ILL IVH Nl � .1 I.0 d J-I'�,,:. , J--.,, "AME MARK*URE TECHNOLOGIES, INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NAI IUNAL PULLUTANT DIS - Ut CLI ff INA IIQN SYSTEM INPOES'/ F.,m ANI,'Uve DISCHARGE M RING REPORT OM9/ ROTATING W QM O FF SPN�t�D S (SUBR 01) Approvein 5- 98 PERMIT NUMBER DISCHARGE NUMBER F — FINAL MONITORING PERIOD MINOR YEAR I I DAY I R I MO I DAY EFFLUE _ FROM TO *#* NO DISCHARGE 120-21! 122-231 126-25! 126-27! 12e-291 !30311 NOTE: Read kwoucdorn before completing this form. PARAMETER 132-37/�>< (3 Card Only/ QUANTITY OR LOADING 166- 54-61 /6 Card Only) QUANTITY OR CONCENTRATION !36-45/ (46-5w f54-611 NO. EX FREQUENCY SAMPLE OF ANALTYPE 164-68M/) 169-7p AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS PHOSPHORUS? TOTAL (AS P) SAMPLE MEASUREMENT ****** *##*** ***#** **#*** (� ,�I�r / n ( 19) n 00665 U 0 0 SEE COMMENTS BELOW #�Ir*# MG/L PERMIT REQUIREMENT REPORT QAILY' Mx MONTH WILE/ RAB PHOSPHORUS, TOTAL (AS P) SAMPLE MEASUREMENT ##*##* ##*##* #**#** #*#*** ,30 ( 19) R� •)0665 W O 0 #** PERMIT #**##* **###* *****# **#### REPORT WILE/ RAS SEE COMMENTS BELOW REQUIREMENT #*** DAILY XX MG/L MONTH CHLOROPHYLL A SAMPLE MEASUREMENT ****** ****** ***#** ***#** h-740 ( 2g) dl 8 j32230 T 0 0 *** PERMIT####*# 1k#**** ###### #**##sr REM RT ` WICE/ RAS SEE COMMENTS BELOW REQUIREMENT` ##* DAILYMX> UG/L MONTH vITROGEN, AMMONIA! NOTAL (AS NH3) SAMPLE MEASUREMENT *####* ****** #*#*** **#*** D/ A9.0-4 ( 19) A60 moo 14726 U 0 O PERMIT REPORT TWICE/R"SEE COMMENTS BELOW REQUIREMENT #0-r# DAILY MX MG/L MONTHf !'JITROGENj AMMONIA! 'TOTAL (AS NH3) SAMPLE MEASUREMENT #*###* ###*## *####* **##*# GIDS t 19) aP/��,QAB 34726 W 0 0 PERMIT REPORT WICE% RA$ ?SEE COMMENTS BELOW REQUIREMENT *** DAILY MX MG/L MONTH SAMPLE MEASUREMENT PERMIT REQUIREMENT' SAMPLE MEASUREMENT PERMIT i REQUIREMENT I NAMERITLE PRINCIPAL EXECUTIVE OFFICER ! AM� AIARDVWVI H THE PENALTY NFORMA ONTSHAVE MHT ESD PERSONALLY EXAMINED BIASED ON MY INQUIRY OF THOSE INOMDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE IS U.S.C. 1 1001 AND 33 end or n w 1319. imrirr /inpr o/ betwoon 6 mars dis whNude fines 4o to S f 0,000 rets/ - SICiNA F PRINCIPAL EXECUTNE OFFICER AUTHORIZED AGENT TELEPHONE DATE , —I ' O TYPED NUMBER COMB YEAR I MO I DAY 9NITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE, PWM INDICATES BOTTOM. cE PERMIT FOR ADDITIONAL NOTES, COMMENTS ANO REQUIREMENTS. =PA Form 3320-1 (08-954 Previous editio-s tie used. (REPLACES EPA FORM T-40 1VIHICH N = N^ ?E ' etre1 00019/9700-17-1435 - 3°c PLHMITTEE NAMUAA Sil.cbe.iaarl,n . NAM' MARIURE TECHNOLOGIES, INC ADOREss MARICULTURE TECH 14ET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSStl_ PRF-STnFNT NATIONAL POLLUTANT DI GE ELIMINATION SYSTEM (NPOES) DISCH2AR/BE MWORING REPORT DMR3) PERMIT NUMBER DISCMAME NUMBER MONITORING PERIOD YEAR I MO DAY I YEAR I MO DAY FROM V f 1 08 1 011 TO 12&211 122..231 121-261 126.271 PIA -101 ,nwi Form Approv ROTATING MQM UFFSi° �PS (SUER 01) pprove( e� ip, 98 F - FINAL 1G� MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read knirucdons before eomoletino due form. PARAMETER 132-371 /3 Gird Only) QUANTITY OR LOADING 46-5 154-61 (4 Card Only) QUANTITY OR CONCENTRATION 136-45/(46431 54-61 NO. w2.6.11 FREQUENCY OF ANALYSIS (64-68) SAMPLE TYPE 16-701 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS TEMPERATURE, WATER DEG, CENTIGRADE SAMPLE MEASUREMENT #*#**# **##** #****# *#**** J',pc ( 04) a/ j dA0G9 00010 T 0 0 SEE COMMENTS BE ***>!c#>!c ##* *#* DEG*CF PERMIT REQUIREMENT: *3R*#* ##*#*# ##*##* REPORTWICEI1 6AILY< MX MONTH RAS TEMPERATURES NATER OEG* CENTIGRADE SAMPLE MEASUREMENT �EJ,J ( O4) al30 ecAB 00010 U 0 0 SEE COMMENTS 3E LOW ##* DEG. C PERMIT REQUIREMENT,; REPORT SAI L'MX ttltiCEl MONTH RAtI TEMPERATURE, NATER DEG, CENTIGRADE SAMPLE MEASUREMENT �b,� 04) Al 10010 w 0 0 SEE COMMENTS BELOW *#* DEG. C PERMIT REQUIREMENT' REPORT DAILY-, MX : WILE/ MONTH RAS OXYGENt DISSOLVED ( 7007 ) SAMPLE*#**** MEASUREMENT #*#*## 17,6 *###*# ****## ( 19) a%�p 4' �� 0300 T 0 0 SEE COMMENTS BELOW **###* ** **# MG/L PERMIT REQUIREMENT ***##*> REPORT DAILY MN #**** **** NICE/ MONTH RAB OXYGEN, DISSOLVED (OO) SAMPLE MEASUREMENT **##*# #*#*#* `� �p F J #*##�t* ##**** ( 19) / b03OO U 0 0 'EE COMMENTS BELOW **#*** *# #** MG/L PERMIT REQUIREMENT; *#*# "* REPORT DAILY MN ****** ******I ifICE/ MONTH RAB OXYGEN, DISSOLVED (DO) SAMPLE MEASUREMENT #*#*** ###**# *##*** **#*** ( 19) Q 30300 W O 0 SEE COMMENTS BELOW ##**** ## MG/L PERMIT REQUIREMENT **###* REPORT DAILY MN *##### *##** —TWICE /GRAB MONTH SALINITY SAMPLE MEASUREMENT *#**Ilok ###### ###### ###### 32 a/3D 30480 T U 0 SEE COMMENTS BELOW ###**# *# ### PPTH PERMIT****** REQUIREMENT: *###** **#*** REPORT DAI Y MX WICE MONTH RAB NAME/TTTLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN: AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SIabwTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF RIVE AND IMPRISONMENT. SEE 18 U.S.C. S 1001 AND 33 U.S.C. f 13111. O%rAg es ands► VWw sorures nvy inckde Alves up to S 10,000 and or mslrirwn lrr piisarrrwrt ol6erwNn 6.nonrhsand 6 ye«a / TELEPHONE DATE "f Sl6A417-1777 ` ! Q 9 SN'aNA OF PRINCIPAL EXECUTIVE OFflCEq R AUTHORIZED AGENT - PRINTED ,. CODE NUMBER YEAR MO ' DAY 'ONITORING LOCATION "T" INOICATES TOP, "U" IN€7ICATES MIDDLE ARID -W- INDICATFS BOTTOM. =E PERMIT FOR ADOITIDMNAL igOTFSj COMMENTS AND RE,�UIREMENTS. =PA Form 3320-1 (08-95) Previous editin-s -,Pv he used. (REPLACES EPA FORM T -AO WHIr,u u n N^- �-F 'iSE- -" - X0129/ 37,3417-1436 - Z r� I PERMI*AME!ADDRESS-7..c"Fanbn NAME MARICULTIU F TECH,;; _:_ [ St I;vL ADDRESS MARICULTURE TECH N -T ? -N PO BOX 451 GREENPORT tiY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSS0. PRESIDENT NATIONAL&TANT DISCHARGE ELIMINATION SYSTEM (NPDESI DISCHARGE MONITORING REPORT /OMR/ (2-16) (17-191 t PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO T DAY YEAR I MO I DAY FROM .971 081 011 TO 1 971 081 31 (2421) 122-231 124251 (26-271 (28-291 (30-31) FoApproved. ROTATING WQM OFF j"r"` (SUBR 01) PP ove�nXW1 5 F — FINA L MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read instructions before completing this form. PARAMETER /3 Card Only) QUANTITY OR LOADING (4 Card Only) QUANTITY OR CONCENTRATION NO FREQUENCY SAMPIi 132-371L?< 116531 154-611 /38-451 (46-53) 154-611 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS sz s ANALYSIS (64-68) (69-701 SALINITY SAMPLE ,II Sc**** **#**# ****** *#**** ( 32) 6012.4! MEASUREMENT V-0 3D 00480 U 0 0 PERMIT REPORT: -,-. MICE Rha SEE COMMENTS BELOW REQUIREMENT **** - A 7i` PPTH M SALINITY SAMPLE *#*### ##**** ***#** ****** �J�O ( 32) h A MEASUREMENT OrD f7i 004.80 M 0 0 ##* PERMIT *****# ** #** ** # ****** REPO_RT, rWIG IF/ R1lB SEE COMMENTS BELOW REQUIREMENT *### DAILY MX PPTH _` i(I(WT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT _ SAMPLE MEASUREMENT PERMIT REQUIREMENT F71-1 NAM8ITnU PrAVC#AL EXECUTIVE OFFICER I CERTIFY AMI FAMILIAR VWT THE OF LAW THAT I HAVE PERSONALLY EXAMINED Alp AM FAMILIAR VMTH 711E B/fORMATION >EUBMITTEO HERESi; AND BA.4fD ON MY SIQUWV OF THOSE , DO MDUALS: IMMEDIATELY RESPOWN LE FOR /vo- TELEPHONE DATE OBTAINING THE WFOIMIATION, 1 BELIEVE THE SUBMITTED WFC MMTRMI IS CEO 'CEO TRUE. ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT FENALTIES FOR SUBMITTING FALSE INF~TION, WCLUDNIGAVON ` 0 t THE POSSIBILRY OF FBIE AND IMPRISONN9lT. SEE 10 U.S.C. 11 1001 AND SS .Umar Imodma"iFIriwrnwlt.F� I mpoem mind&yens/s�arlf0.000 FRINdFAL EXECUTIVE67 OFFICER AUTHORIZEDAWIT 1 %7 J A, PRIlaw CAREA NUMBER YEAR MO DAY MONITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W" INDICATES 3OTTOMe SEE PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS. EPA Fam 3520-1 IM961 Provibus editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00030/970917-1436 PAGE 7OF r'ERMITTEENAME)AD90ncbd.Pwcd,n ,,,•,m, ,; ff.mp NAS MARICU TURE TECHNOLOGIES, INC ADDRESS MARICULTURE TECH NET PSN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTNs VTTD L CAPORUSSd. PRESIDENT NATIONAL POLLUTANT DIS E ELIMINATION SYSTEM (NPDES) Form Approv DISCHARGE M RING REPORT OMR) -� 17-19 ROTATING WQM OFF NNS 04R M (SUBR 01) pprovalerpiw PERMIT NUMBER DISCHMGE NUMBER F — FINAL 1 L �4 MONITORING PERIOD MINOR YEAR I MO DAY YEAR I MO I DAY INTERM _ FROM Vfl 031 011TO I Yll ot5l *** NO DISCHARGE (20-21) 122.231 124-251 126271 128-291 130.311 NOTE: Read kwfttcdaw before complodny this form. PARAMETER" 132-371 /3 Card OnM QUANTITY OR LOADING 46-5 51-61 (S Card Only/ QUANTITY OR CONCENTRATION /38-4b/ I66 6I-61 NO. EX :�3 FREQUENCY of ANALYSIS 164-6er SAMPLE TYPE (69-701 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS FEMPERATURE1 MATER :EGe CENTIGRADE SAMPLE****** MEASUREMENT ****** ****## *#*### �j plQ+ p% ( 04) o'� /.� 5. jJ0010 T 0 0 ISEE COMMENTS BELOW PERMIT REQUIREMENT 1Ir#1jr>1r REPORT DA LY. MX' DEGoCI 'WICE/111, MONTH RAB IFEMPERATURE, NATER JEG. CENTIGRADE SAMPLE***#* MEASUREMENT0 *#*** *#***# ***### a�d � ( 04) a'2/ �A8 )0010 U 0 0 PERMIT REPORT NICE/ RAB !SEE COMMENTS BELOW REQUIREMENT: *** DAILY MX- DEG.0 MONTH IENPERATUREi WATER .=EGe CENTIGRADE SAMPLE MEASUREMENT 04) PERMIT ****#* ###*## ####*# REPORT TWICE/ GRAB 10710 W 0 0 #*##* ## SEE COMMENTS BELOW REQUIREMENT'. ##�k DAILY MX DEGeCF MONTH ;XYGENT DISSOLVED' (DO) SAMPLE MEASUREMENT *#�k*## #> *### ##**## �t##### ( 19) a fes^ /7v 'J0300 T 0 0 0-R**##Ik *# PERMIT Ik### REPORT _lEE COMMENTS BELOW REQUIREMENT' **# DAILY MN MG/L MONTH :XYGENj DISSOLVED ( DQ) SAMPLE MEASUREMENT ****** *#*****#*** *****# t 19) All cwpg )0300 U 0 0 PERMIT REPORT WICE/ FLAB .SEE COMMENTS BELOW REQUIREMENT: **# DAILY MN MG/L MONTH ',JXYGEN, DISSOLVED (DO) SAMPLE MEASUREMENT #**### **#* ****** **#*#IIr t 19) 1)0300 W 0 O ##klk## *# PERMIT **#*## REPORT ****#* ****## MICE RAB 'SEE COMMENTS BELOW REQUIREMENT **# DAILY MN MG/L MONTH I_iALINITY SAMPLE MEASUREMENT *##*** ##$1Ir#* #**### #*#### 49/. D 32 p? 10480 T 0 0. #1ir*### ** PERMIT ###### ###### *##### REPORT W ,. EE COMMENTS BELOW REQUIREMENT: #* OAI MX PPTH MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT 1 HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; ANO BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C, f 131 s. Ift—was www Nwsw saemrs nwy inchme Firms up to S 10,000 and or.nr,rkmmkr is mW orarween6Monrna«aeyowls.) _ e TELEPHONE DATE CEO 47 } ( 0 /1 t„/� SIGNA OF PRINCIPAL EXECUTIVE OFFI OR AUTHORIZED AGENT PED PRINTED AREA CODE NUMBER YEAR j MO DAY :.VMMCnI1.7 MIYV cnr cnnnrava� yr nrr vrvcn ,v,.v pay. v0- encu ox vaaaa....nv...... NITORING LOCATION "T" INDICATES TQPI "U" INDICATES MIDDLE AND "W" INDICATES 30TTOM. .EE PERMIT FOR AUDITIO%AL NOTES, COMMENTS AN": REQUIREMENTS0 -PA Form 3320-1 (08-95) Previous e(iitm-s -qv be used. (REPLACE`; EP4 FC)PM T -an u' N ­IE USI-. 10037/°7,,`317-14 3 6 0 r I PERMIT PANT PERM ITT9A ME/ADDRESS 7-1-d. F—hn ��— . .- -.v NATIONAL DISCHARGE ELIMINATION SYSTEM (NPDES) Folopproved. NAME ag2IC:!LTU�t- TcC� _L _ s=3 � I�' C DISCHARGE MONITORING REPORT (DMR) (2-161 117-19) ROTATING , D WQA OFFIRWILD 5- ADDRESS MARICULT±URE TECH, I _� $NSR O1) PProva�nacPlr� & PO BOX 461 PERMIT NUMBER DISCHARGE NUMBER F — FINAL GREENPORT NY 11944MONITORING MINOR FACILITY PERIOD MEASUREMENT YEAR MO DAY YEDAY I NTE RH AR MO _ LOCATION FROM V11 U81 01 TO *** NO DISCHARGE ATTN: VITO L CAPORU S01 PRESIDENT 120-211 122-231 124-25i (26-27/ 128-29) 130-31) NOTE: Read instructions before completing this form. PARAMETER (3 Card oMy) QUANTITY OR LOADING M Csrd On)y/ QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE (32-371 REQUIREMENT ' (46 (54-61) (38-45) (46-53 (54-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS I - ANALYSIS Z Y THE POS IUTY (q� AM IMPpgONMENT. SEE 18 U.B.C. 1 1001 AND �Q 33 U.S.C. 1 1319. Inrwws salty omw ,rnss �•r rlrA,e. nlNs IV a r1oaoo .�Ispnr.�wrt+srNunlrrwlcs/aaw.rr sTandrand INGNA OF PRINCIPAL EXECUTIVE 2 sa 164-s81 169-70) SALINITY SAMPLE s yra/ OFFICE OR AUTHORIZED AGENT CAREA OpE NUMBER YEAR MO DAY COMIAVM AND EXPLANATION OF ANY VIOLATIONS /Rs/wwwo aN atmchmsnts here) MONITORING LOCATION •T" INDICATES TOP, "U" INDICATES MIDDLE AND nW- INDICATES BOTTOM. SEE PERMIT FOR ADDITIONAL NOTES9 COMMENTS AND REQUIREMENTS. 3�i 7 MEASUREMENT ,�Q. QA� 004$0 U 0 0 #** PERMITPORT: #*ik* ###�k## **### #####Ile•�/ iIIC GRAB SEE COMMENTS BELOW REQUIREMENT ##*# PPTHmmn SALINITY SAMPLE ##;### #*##4c4c *##### ###### ( 32) MEASUREMENT, PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT: r REQUIREMENT ' NAMERffLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDO PENIALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMIUAII %JH THE NFORMATION SUBMITTED HEREIN: AND BASED ON MY INOURY OF THOU INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE I - OBTAINING' THE NF6IMNATIOK i SEUEW THE SUBMITTED INFORMATION IS TRUE. ACCUMTE AND COO�LETE. t AM AWME THAT THERE ARE SIGNIFICANT PH�TIEB FOR W M604 FALSE INFORMATION; BICLUDBNG Z Y THE POS IUTY (q� AM IMPpgONMENT. SEE 18 U.B.C. 1 1001 AND �Q 33 U.S.C. 1 1319. Inrwws salty omw ,rnss �•r rlrA,e. nlNs IV a r1oaoo .�Ispnr.�wrt+srNunlrrwlcs/aaw.rr sTandrand INGNA OF PRINCIPAL EXECUTIVE 6 J OR I s yra/ OFFICE OR AUTHORIZED AGENT CAREA OpE NUMBER YEAR MO DAY COMIAVM AND EXPLANATION OF ANY VIOLATIONS /Rs/wwwo aN atmchmsnts here) MONITORING LOCATION •T" INDICATES TOP, "U" INDICATES MIDDLE AND nW- INDICATES BOTTOM. SEE PERMIT FOR ADDITIONAL NOTES9 COMMENTS AND REQUIREMENTS. EPA Form 3320-1 (00-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00038/970917-1436 PAGE O 7 „LRMITTEENAMLIASd—Jud,F—h, i,"f—w) ”^"'E. MARIC.TURE TECHNOLOGIESV ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT N YINC 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO, PRESIDENT NATIONAL POLLUTANTDI GE ELIMINATION SYSTEM /NPOESI DISCHARGE ORING REPORT DMR91 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD Y AR I I DAY I I YEAR I MO I DA FROM V f I U111 I U11 I TO 120.211 122-231 (24-26) (26-271 128-291 (34311 Form Approvift ROTATING WQM OFFS " (SUER 01) pprova( eir,>� 5- 98 F — FINAL 1G�� MINOR EFFLUE *** NO DISCHARGE NOTE: Read instructions before completing this form. PARAMETER r3 card only! QUANTITY OR LOADING 14 Card OnM/ QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE 132-371�>< (46-63) 5661 3h3 -IS 6661 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 4sNALYSISj A 16666814-680 (69-7p TEMPERATURE, WATER SAMPLE MEASUREMENT ###*## ###### ##11csjolc# ##tic##111 ( 04) a/� 8 ,)EG. CENTIGRADE p4D/� 00010 T 0 0 **** ##* PERMIT ##**Sas ***#*# ****## JEPQ#tT iiIGEI"RAS SEE COMMENTS BELOW REQUIREMENT **#* DAILY Mit' DEG.0 MONTH TEMPERATURE, WATER SAMPLE ###### #***** ***### **#*** / { 04) 'EG. CENTIGRADE MEASUREMENT a%/30 4gjejo!3 ?0010 U 0 0 *#**** *#* PERMIT # **** ***#** *#*#** REPORT WICE/ RA8 SEE COMMENTS BELOW REQUIREMENT' **# DAILY'' MX DEG.0 ' MONTH FEMPERATURE9 WATER SAMPLE ####*# *##*## *##*** ***##* ( 04) JEG* CENTIGRADE MEASUREMENT aQ. p� X0010 W 0 0 ****## **# PERMIT * *#*# ###*** **##*# REPORT TWICE/ GRAB �3EE COMMENTS BELOW REQUIREMENT: #*## DAILY MX DEG.0 MONTH IXYGEN? DISSOLVED SAMPLE #*#*** **#*#* �� 8 *****# *****# ( 19) (DO) MEASUREMENT !:!0300 T 0 0 **#### ** PERMIT #**#** REPORT WIGE/ RAB 13EE COMMENTS BELOW REQUIREMENT #** DAILY MN MG/L MONTH ,.sXYGENj DISSOLVEIT= SAMPLE h i (DO) MEASUREMENT (O / p( 6404S ':")0300 U 0 0 *#**** ** PERMIT #**#># REPORT *##*** *#***#' WICE RAS -'-EE COMMENTS BELOW REQUIREMENT ##* DAILY MN MG/L MONTH 7XYGEN, DISSOLVED SAMPLE #**#** ##*### **##*# *##*** 19 n ^ 1 (OD) MEASUREMENT �i I /? Cr � W 0 0 ****# *# PERMIT *##*7a# REPORT *#**#* ***#** WICE -,R —AB I30300 SEE COMMENTS BELOW REQUIREMENT- *** DAILY MN MG/L MONTH SALINITY SAMPLE *#*#** ***#** *###*# *##### 3 MEASUREMENT L pro 29 �j g 30460 T 0 0 ###** *# -V PERMIT #*#*# ##*#** *#*#*#. REPORT i`JEE COMMENTS 3ELOM REQUIREMENT. #*# DAILY MX PPTH MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONS18LE FOR - TELEPHONE DATE OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS C� TRUEAND COMPLETE. I AM THAT THEE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSEAWARE INFORMATION. INCLUDING `7� g 6 97 Q f THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. S 1001 AND 33 U.S.C..i 1310. IFsiwJCbi wl*r 4"0" "Outs msy k -A,* Hess up m S 70,000 sndwrnuimsnhpriaanwrto/Mewssn6marMS&dsY&AMI SIONA OF PRINCWAL EXECUTIVE OFFICE gAUTHORIZEDAGENT S(�p y %7���� ! J PED PRINTED CODE NUMBER YEAR MO I DAY IONITORING LOCATION "T" INDICATES TOP? "U* INDICATES NICOLE AND "W" INDICATES BOTTOM. :EE PERMIT FOR ADDITI9:44AL NOTES, COMMENTS AND REQUIREMENTS, 'PA Form 3320-1 f08-95) Previous er it-- -i `+P used. (REPLACES EPA FORM T-dn 1-1cu ." 1 N-7 '�0�14I%�I^'>17-143Fi 1`^ PERMITTEEIOAME/ADDRESS a.Yr.d.F—d,n �—m NAME AARICULrURE TECH'. .�. ,�,_ ,� INC ADDRESS MAR ICULTURE TECH `ti -T P 7N I PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. 9RrslnFNT NATIONAL PWT DISCHARGE ELIMINATION SYSTEM (NPDES) DISCHARGE MONITORING REPORT (DMR) 12-161 (17-191 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY I I YEAR MO DAY FROM VTJ 081 TO 1 911 0131 Tr 120-21) 122-230 124-25J 126-27) [2a-29) 13D.21) Foreproved. ROTATING WQM OFFSMW-*"OWNS ( SI J B R 01) Approva j.2l j%tO5-31-9& F — FINAL L� MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read instructions before compistin9 this form. PARAMETER (32-371 13 Card Only/ QUANTITY OR LOADING 146-531 I54-611 (4 Card OnW QUANTITY OR CONCENTRATION 130--45) l46 -53l (54-611 NO. EX 2-63 FREQUENCY of ANALYSIS 164-68) SAMPLE TYPE 169-70) AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS SALINITY SAMPLE MEASUREMENT *#*�c>,c# #*#### **#*## ###**# 3� Q t 32)C7 a /yr'tl��, 00480 U 0 0 SEE COMMENTS BELOW ### PPTH PERMIT REQUIREMENT :R#*�K** #�k1k#�k�k *##* #1�1k�R## REPORT..'' DAILYAXi Int SALINITY SAMPLE MEASUREMENT **#* #***** ****** ****** ( 32) n 00480 W 0 O SEE COMMENTS BELOW Nc##* PPTH PERMIT REQUIREMENT REPORT.:,' IiAILYX< ICfI MONTH ARAB SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT'` kQUIREMENT NAAIIETTLE PRUNCUPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED MOWN; AND SAM ON MY INOUNIY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE WFORMATNMN, I BELIEVE THE SUBMITTED INFORMATION IS TRUE. ACCUMTE MW COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT PENAL FOR SUBMITTING FALSE INFORMATION. INCLUDING THE POSSIBILITY OF E AND IMPRISONMENT. SEE 10 U.S.C. f 1001 AND 33 U3 -C. 11316. ownfmw rndr tlra, ,oder, MAY kwk/ � MMS q a t 10,ono .es.+�r.nNarwe,..«rsalena.rrsrw,) BN1NA Of PRBYCIrAI EXECUTIVE DFFINR OR AUTHORIZED AGENT TELEPHONE DATE OM OR --,v , ^, ,` W - 1 77 D / 9 CODE"REA NUMBER YEAR MO DAY MONITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM. SEE PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS. EPA Form 3320-1 106-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00042/970917-1436 PAGE 2OF I EHMIT TEE NAMEIA5 (I—Ad, nd..mo NAME RI-';*TURE TECHNOLOGIES] INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VTTO L CAPnRUSSn. PRFSTnFNT NATIONAL POLLUTANT DI GE ELIMINATION SYSTEM (NPDES) DISCHARGE ORING REPORT 4fDM9I 26 06R PERMIT NUMBER IMSC14MOE NUMset MONITORNIIG PERIOD YEAR I bdO I DAY I 1YEAR O A FROM V r I I TOI Vfj U51 31 120-217 122.231 11A.191 va.»l r3t2*I rwk-vti Form Approv ROTATING WQM OFFS-pj/1 S (SUER 01) rovai r9I -88 F - FINAL MINOR EFFLUE _ #** NO DISCHARGE 1-1 **# : NOTE: Read inaVucdona boon comWetinn this form_ PARAMETER /32-37/ >< /3 Grd Onm QUANTITY OR LOADING 1465 54-61 14 Card OnW QUANTITY OR CONCENTRATION 38-46 465 54-61 NO. EX 2-631 FREQUENCY OF A/1 r6I-6816s� SAMPLE TYPE f69 -7a AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS TEMPERATUREI NATER DEG. CENTIGRADE SAMPLE MEASUREMENT #**#** ****#>Or #***## #####* a0-, (J ( 04) a/3OjQ6 00010 T 0 0 SEE COMMENTS BELOW **## DEG*C PERMIT REQUIREMENT` REPORT DAILY: HK WICE/ MONTH RA8 TEMPERATUREI RATER ")EG* CENTIGRADE SAMPLE MEASUREMENT ##*#** **#*** **#*## *#### aO�� ( O4) �/� .)0010 U 0 0 SEE COMMENTS BELOW #** #** DEG.0 PERMIT REQUIREMENT! *## * *** *# *****# ****#* REPORT DAILY < !1X WICE/ MONTH RAS TEMPERATUREI MATER JEG* CENTIGRADE SAMPLE MEASUREMENT ****** ****** ****#* **#,pk* A0140 ( 04) .)0010 W Q 0 SEE COMMENTS BEL(]W. *** ***# DEG*C PERMIT REQUIREMENT: **�k*##, *�k#*#* ****** ****** REPORT ' GAILY MX. HICE/ TMONTH RAB )XYGENt DISSOLVED-. SAMPLE MEASUREMENT *#**** #*##** fp I *#**#* ****** ( 19) 9 0300 T 0 0 SEE COMMENTS BEL ** *#** MG/L PERMIT REQUIREMENT ***** *#**** REPORT DAILY MN ****** ****** WICE/ MONTH RAB JXYGENI DISSOLVED; ( 00) SAMPLE MEASUREMENT ****** *#**** /pa 7 ****** ***#** ( 19) n/� p(��n Ag 10300 U 0 0 SEE COMMENTS BELOW #** MG/L PERMIT REQUIREMENT REPORT DAILY MN **#*** #** TWICE/GRAB MONTH JXYGENI DISSOLVED (DO) SAMPLE MEASUREMENT�8 ****** ****** ****** ****** If 19) 10300 0 O SEE COMMENTS BELOW ** *** MG/L PERMIT REQUIREMENT ****#* #***** REPORT DAILY MN ****** *#**** WILE/ MONTH RAB SALINITY SAMPLE MEASUREMENT ****** ****** ****** ****** 3a a ( 32) a 13fl 6006 10480 T 0 0PERMIT REPORT 1lICE R A 3 IEE COMMENTS BELOW REQUIREMENT: *** DATAY MX PPTH MONTH NAMErnTLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INGUIRY OF THOSE INDIMOUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 3314 U.S.C. i 1318. (P1MWeee uns➢r dloom sbK4tes rosy bxlude riot: up to 570,000 endwmax1fts" rr samnrrto/betwwn6monihsard6yeers) jiv TELEPHONE DATE YAt L. Wa8 I I _17 i U` + 9 StONA OF PRINC�AL EXECUTNE OFFICE OR AUTHORIZEOAOENT TYPED PRINTED AREA CODE NUMBER YEAR� MO 1 DAY `:7VITORING LOCATION "T" INDICATES TOP* "U" INDICAT=S MIDDLE Aq0 NWN INDICATES -"JTTOM* EE IPERMIT FOR ADDITI` -4AL NOTES? C,--,MMFNTS AND REQUIREMENTS, =PA Form 3320-1 108-951 Previous editing used. {REPLACES EPA POP" T-40 "'�I w � = •- �F '_1ST 00,04/ ?7 "; 17-143 PERMITTE2'ITAME/ADDRESS,7.k6.d .—Niru �.m.: . r NAME AARICIULT;1k—_z I,`jC ADDRESS' HARICULTURE TECH :tiJT PFN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDFNT NATIONAL PANT DISCHARGE ELIMINATION SYSTEM (NPDES) DISCHARGE MONITORING REPORT (DMR) (2-16) (17-19) PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY I IYEARIMODAY FROM TO 11 051 120-21) 122-231 f24 -25i 126-27) 128-2911 For proved. ROTATING KQM 0FFSjRW1 4;; (SUBR 01) PProv 1 L�r E F — FINAL MINOR EFFLUE _ *** NO DISCHARGE NOTE: Road inetfuc ions before completing this form. PARAMETER (32-37) (3 Card Only) QUANTITY OR LOADING (46-53) (54-61) (4 Card On/v) QUANTITY OR CONCENTRATION (36-45) 146-5 (56-611 NO. EX 2-6J FREQUENCY of ANALYSTS (64-68) SAMPLE TYPE 169-70) AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS>< SALINITY SAMPLE MEASUREMENT #####* #**#** ###s## ###*##( p, Q 32) 2/.v 00480 U 0 0 SEE COMMENTS BELOW ### #### PPTH PERMIT REQUIREMENT **# ## ## #ale #IIc*�kak# **#### REPGRT DA Y ft WCE/ PWNTH ;RAB SALINITY SAMPLE MEASUREMENT #####* *####* ###*## **#*## % �i Q ( 32) a 00480 N 0 O SEE COMMENTS BELOW #### PPTH PERMIT REQUIREMENT REPT: AI Y N . iICE� MONT RSB SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT NAME/TITLE PRINCIPAL EXECUTIVE OFFICER 1 CERTIFY UNDER PENALTY OF LAW THAT i HAVE PERSONALLY EXAMINED AND AM FAMILIAR VMTH THE INFORMATION SUBMITTED HEREIN, AND BASED ON MY INQUIRY OF THOSE OW-40UALS IMMEDIATELY RESPONSIBLE FOR OSTARING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE. ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SKINIRCANT PENALTIES FOR SUS&KTTING FALSE INFORMATION. INCLUDING THE Possas ITY W FINE AND umsONMENT. SEE to U.S.C. 1 1001 AND 33 U.S.C. 1 1318. M1mamw" rush Nbrar Samoa" nary kwkf* flay yr m 110,000 .oww�kno" irrnwu.isaw..w8 adwSFW5Yom&/ TELEPHONE DATE it l) SIGNATURE PRINIDWAL EXECUTNE OFFICER AUTHORIZED AGENT trym opt PRINTED CODE NUMBER YEAR MO DAY MONITORING LOCATION "T" INDICATES TOP, "UNI INDICATES MIDDLE AND "M/1 INDICATES 30TTOM. SEE PERMIT FOR ADDITIONAL NOTES? COMMENTS AND REQUIREMENTS. EPA Form 3320-1 108-951 Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00046/970917-1436 PAGE SOF PEHMIIILL NAML/ SSIb.r�,d/;s w,'•.m• afJ•.rnr/ NAME MARK LTURE TECHNOLOGIES9 INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANT DI GE ELIMINATION SYSTEM (NPDES) DISCHARGE GORING REPORTDMR( 2-1s 17-19 I P726 07R M PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY YEAR I MO DAY FROM TO 120.211 122-231 124-250 126.27) 128-291 /90.1/1 Form App ROTATING WQM OFF rov S 2 (SUER 01) pprovalllyi >�OSM-98 F - FINAL MINOR EFFLUE _ *** NO DISCHARGE I_I *** NOTE: Read iriam dorm before oompkting Osie form. PARAMETER /3 Gid Only/ QUANTITY OR LOADING /4 Card Only/ QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE 132-371 146-53) 5161 (38-4N 46 6 (54-611 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2-631 ANALYSIS 164-681 169-701 TEMPERATURE, MATER SAMPLE MEASUREMENT #*#*## ####1k# #,Icyc,Inlnk ###*## �d ( 04) a/� Q4 DEG* CENTIGRADE I 00010 T O 0 PERMIT ***** ***** *** ***#** ***## REPORT RASREQUIREMENY COMMENTS SELOM OE6 C MONTSEE TEMPERATURE, MATER SAMPLE *###*# *##### *#*#** �R##### t04)DCG. I CENTIGRADE MEASUREMENT 0?a'a 00010 U 0 0 PERMITREPORT uICE RAS 'EE COMMENTS BELOW REQUIREMENT ### DJEIL1f !4X DE6eC MONTH EMPERATURE9 MATER SAMPLE ##*### *##### *****# ###### ( 04) a�.,p 6t4& DEG, CENTIGRADE MEASUREMENT �Q�3 00410 w 0 0 PERMIT REPORT TWICE/ GRAB SEE COMMENTS BELOW REQUIREMENT ***, DAI Lf !IX DEG. C MONTH OXYGEN, DISSOLVED`-. SAMPLE *#*#*# ***##* ###*sc# ##*### ( 19) a/30 (DO) MEASUREMENT 0300 T 0 0 ### PERMIT' #�k#* *##*## REPORT *#*#** *##*** WICE/ RA$ SEE COMMENTS BELOW. REQUIREMENT *## DAILY MN MG/L TMONTH OXYGEN, DISSOLVED SAMPLE#*#*## MEASUREMENT *#*### /6-7 #*#*#* *#**## ( 19) (00) 0300 U 0 0 ## PERMIT **### *** #* REPORT ***** ## #* TWICE/ GRAB SEE COMMENTS BELOW REQUIREMENT #** DAILY MN MG/L MONTH OXYGEN, DISSOLVED SAMPLE *###** ***#** ****** ****** { 19) a/ (DO) MEASUREMENT �� AO 0300 W 0 0 ## PERMIT **###* ****** REPORT EE COMMENTS BELOW REQUIREMENT *## DAILY MN MG/L MONTH ALINITY SAMPLE #***#* ****** #**#** ##### t 32) 130 MEASUREMENT 3iaO 0450 T 0 0 ## PERMIT �k*#�k*Tk ik### * ###### #####* REPORT MICE/GRAB EE COMMENTS 3ELOM I REQUIREMENT##* DAI MX PPTH MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I GIIERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE OBTAINING THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE - ' SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDINGVA THE POSSIBILITY OF FINE AND IMPNSONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C. i 1318. (P&,wAiss Undw dkew so8rMes mry kwki& fins up to $10,000 and or/rwr!/mmlmpisonmw/tofbetwom6//w//d/sand6yaws.) I SIGMA OF PRINCIPAL EXECUTIVE OFFICE RAUTHORIZEDAGENT 7-I 7-7 / eT S qj . TYPPRINTED ED CODE NUMBER ; YEAR MO I DA %.VMMCry 1 a (%FIV cnr a.nnn / /v/. yr r+— r r r ry0// O[l04/NlR!/W nwa/ MONITORING LOCATION "T" INDICATES TOP( "U" T'4 ICATES MIDDLE AND "WIN INDICATES 6OTTOM, SEE PERMIT FOR ADDITIE3NAL NOTES( CUMMFNTS A3` . REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions r -,ay be used. (REPLACES EPA FORM T -An WI,41ru u n v ?E USE^ I - -- �''OI`;49/?; X1917-1436 - Imo^ A YEHMII ILL NAMLii—i...... .. u. NAME I LTURE TECHNOLOGIES, INC ADDR>=SS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTat• VTTn t eADnD1iccn DDCCTnCWV NATIONAL YULLUTANT DI GE ELIMINATION SYSTEM (NPDES) Form Approve DISCHARGE ORING REPORT (DMR) 2-16 f7-19ROTATING WQM OFF Y022672 07R(SUBR 01) roVtll.atwtr 8 PERMIT NUMBER ascHARGE NUMBER F — FINAL l L 3 MONITORING PERIOD MINOR YEAR I MO I DAY 1, 1 YEAR I MO -1 DAY , EFFLUE _ FROM TO *** NO DISCHARGE roRen 199.771 Yei — NATE- Road Inatnl All 6af� eennaNatinn MS. f— PARAMETER _ 132-371 _ _t3 Cord OMW " QUANTITY OR LOADING ss 64-61 (s Cerd Only) QUANTITY OR CONCENTRATION (36-45) Ids 1 NO. EX 2;3 :REQUBfCY OF ANALYSIS (64-660 SAMPLE TYPE 169-7a AVERAGE MAXIMUM UNITS MINIMUM AVERAGE': MAXIMUM UNRS SALINITY SAMPLE MEASUREMENT ##*## ####*# ##*##* ###### ��• Q ( 32) /� �/� 00480 U 0 0 SEE COMMENTS BELOW *#Ik *# H PERMIT REQUIREMENT" #*###* ####*# ###### ###### REPORT ,PP rWICE/rwRA8 MON SALINITY SAMPLE###### MEASUREMENT ###### ###### ***#*# ` 3/ 1 { 32) ii 30e ," 00480 W U O SEE COMMENTS BELOW PPTH PERMIT REQUIREMENT **### ###*1t REPORT DAILY MA MICE MONT RAS SAMPLE MEASUREMENT PERMIT < REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT f(EQUIREMENT1. SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT, NAME/TITLE PRINCIPAL EXECUTIVE OFFICER ERnFY UNDER PI?IALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND TELEPHONE DATE FAMIUM WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE WMVIDUALS IMMEDIATELY RESPONSIBLE FOR - OBTAIN NO THE INFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCUMTE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND W"SONMENT. SEE 18 UAC. f 1001 AND 33" S% 7 -1 16 U.S.C. f 1318. 0% NM* WNW teaao s nwy hcbdr lies gw ro$7�A SIGNA PRINCIPAL EXECUTIVE OR PRINTED and or nwriswn inpuiswrrwrt of eatw"n 6 nwnda and 6 y az) OFFICER OR AUTHORIZED AGENT AREA NUMBER YEAR MO DAY COMMENTS AND EXPLANATION OF ANY VIOLATIONS !Reference aNsKechments here! MONITORING LOCATION 'IT" INDICATES TOPq "U" INDICATES MIDDLE AND "W" INDICATES 30TTOM, SEE PERMIT FOR ADOIT19NAL NOTES, COMMENTS AND REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00050/970917-1436 PAGE `OF YEHMIIILL NAME! ESS[I—Ad,i—hl, .,......,,,,...,,,.,�/,.•r NAME MARIC LTURE TECHNOLOGIES, ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY INC 11944 FACILITY LOCATION ATTM! VTTn i CAPIlRI1SSf1_ PRFCTIIFNT NATIONAL POLLUTANT 0 GE ELIMINATION SYSTEM (NPOES) DISCHARGE I�ORING REPORTDMR/ 2-16 1 ZI9 77A ORR PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY I YEAR I MO DAY FROM Vfl U01 011TO1 /20.211 112-231 19411.2si 124LI71 1910.JP01 I -In III Form Approv ROTATING WQM OFFS' S (SUBR 01) Approve, - -98 F - FINAL MINOR EFFLUE _ *** NO DISCHARGE NOTE: Road insvuc8Gn8 before, comol.tirw dlis form. PARAMETER (3 Gid O1Ny1 QUANTITY OR LOADING (4 Card Only) QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE 132-3�1 >< 146-5 /54-61 39-461 /46-5 54-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS jw2.a3j ANALYSIS (64-681 (69-701 TEMPERATURE, WATER SAMPLE MEASUREMENT ***#***##* #*#*## *##*#* ( 04) DEG. CENTIGRADE 00010 T 0 O #*# PERMIT *#*#*?k #*## ##***# #*###* REP£IRT 's WICE/ RA8 SEE COMMENTS BELOW REQUIREMENT ,S,b,�,« DAILY NX,OEG.0 MONTH TEMPERATUREt WATER SAMPLE NIC##*#* ##k�##* ###*## ###### n { 04) UEG. CENTIGRADE MEASUREMENT �JOrO/3D �g 0010 U 0 0 ### PERMIT #*** * ##* ** ####** ###*** REPORT TWICE/ GRAB SEE COMMENTS BELOW REQUIREMENT #*** DAILY MX DEG.0 MONTH TEMPERATURE, WATER SAMPLE MEASUREMENT #####* **#p�## *#*#** *#*##* aO/ ( 04) �/aq 0EG. CENTIGRADE 00010 W 0 1 PERMIT REPORT TWICE/ GRAB SEE COMMENTS BELOW REQUIREMENT #*# DAILY MX > DEG. C MONTH OXYGEN, DISSOLVEO:' SAMPLE ###*## *** ** Q ##s#*# s##*** ( 19) (DO) MEASUREMENT Ice 0300 T 0 0 PERMIT REPORT ###### #**##* TWICE/GRAS EE COMMENTS BELOWREQUIREMENT ### DAILY MN MG/L MONTH XYGEN9 DISSOLVEW- SAMPLE ###### ****** **###* ***#** ( 19) Q (DO) MEASUREMENT 00300 U 0 0 ** PERMIT **### #**##* REPORT ###### #**# WICE/ RAB `'EE COMMENTS BELOW REQUIREMENT *##* DAILY MN MG/L MONTH OXYGEN, DISSOLVED SAMPLE #####Nk *##*#* #*#*## #**#** ( 19) (DO) MEASUREMENT � / 46 alp &,P,46 0300 W 0 0 ** PERMIT *#*#** ***#** REPORT *#*#** *****# WICE/ RAB SEE COMMENTS BELOW REQUIREMENT ### DAILY MN MG/L MONTH -. SALINITY SAMPLE*#*#** #***** ##**## #**#** ( 32 MEASUREMENT _q,;,/Q o�I/� 'erlog 00480 T 0 0 # PERMIT ##**** ****#* *##*## #####* REPORT WICE RAB SEE COMMENTS BELOW I REQUIREMENT ### DA Y MX PPTH MONTH NAMETTITLE PRINCIPAL EXECUTIVE OFFICER I OERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIA ION WITH THE INFORMATSUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR IfTELEPHONE DATE OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SSO t CL CJ /�vs SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 33 U.S.C. i 1318. 1p&,%0 ss tardar Ness sbWtes may Inehde re yp toS 10,000 and or Manbavn bllprlaDlwwff of betw~ 6 Months 6 _ SI(3 OF PRINCIPAL EXECUTIVE OFFICE J 4 7 7-1777 JO ? 1-1 J tryPED PRINTED AREA and ysarsl R AUTHORIZED AGT EN CODE NUMBER YEAR MO DAY I.VMMC1� r a nav a.nr a.•-aasra a rva• v. r.r. , .,v�r� r r.+..v r•avw va.v w• oaaoa.•••••vr•w trot v/ MONITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM, SEE PERMIT FOR ADDITIO AL NOTESy COMMENTS ANV REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions -,av be used. (REPLACES EPA, FORM T -An tk'ylCw M± N - aE IJSF- X0'}53/?7!717-143F � 1` 14, PLHMIIILL NAME/SSdncrmhn<il... , . .p v NAf MARI LTURE TECHNOLOGIES, INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTNz VTTn U CAPORUSSn_ PRFSinFNT NATIONAL POLLUTANT DI GE ELIMINATION SYSTEM (NPDES) DISCH2AO ORING REPORT ID %)l 11100 PERMIT NUMBER I DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAYJ I YEAR I MO AY FROM 971 0 TO 1 (20.2fl 122-23) 124-25/ 12627) f28-291 0"fl Form Approvift ROTATING MQM OFFS..` (SUBR 01) rovaLel�Nr B F --FINAL lL3 MINOR EFFLUE _ ***-= NO DISCHARGE NOTE: Rud kweuelfons beton compMdnp this form. PARAMETER /12-3>I (3 card only) QUANTITY OR LOADING 46 50-e► 14 Card.Onlyl QUANTITY OR CONCENTRATION = s"F NO. EX 2.63 FREQUEFICY OF ANALYSIS SAMPLE l p AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS SALINITY SAMPLE MEASUREMENT #*#* #*#*#* **#*** ****** ( 32) 00480 U 0 0 PERMIT REPORT MICE/ rwRAB SEE COMMENTS BELOW REQUIREMENT **** DAILY 14K PP H SALINITY SAMPLE MEASUREMENT #�c#### ###### ##*### ##Ik*IR# / / ( 32) ­'Av Iseqs 00480 K O '0 ### PERMIT ####>totr ###### *##### #####* REPORT ,; MICE RAS SEE COMMENTS BELOW REQUIREMENT #yr## DAILY MX< PPTH MONT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT - REQUIREMENT NAMERTTLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AUMp FAMILIAR WTH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE 1 AM AWARE THAT THERE ARE PENALTY FOR SUIIMITTING FALSE INFORMATION, INCLUDING THE POSSIBIUTY OF FINE AND RAWSONMENT. SEE 18 U.S.C. § 1001 AND 13 U.S.C. 11 1918. 0%no n told► flow ri ifte nwy km*# b /Pus up to $WADI) and or merser n anp l xwmaw aMtworr 6 nwntlu &W 6 yers/ TELEPHONE DATE - _ CEOChSIGNIFICANT S' -t O l _T�_ a1pNA OF PigNCIPAI EXECUTIVE O OR AUTHORIZED AGENT + ArODE NUMBER YEAR MO I DAY comNItN 15 AMU CArL.ANA I NUN Ur AN T v IULA I IUlva IrTererence AN saeanmenrs nerel :4ONITORING LOCATION "T" INDICATES TOPI "U" INDICATES MIDDLE AND -Ww INDICATES BOTTOM, SEE PERMIT FOR ADDITIONAL NOTES1 COMMENTS ANO REQUIREMENTS. EPA Form 3320-1 (06-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00054/970917-1436 PAGE 2 O PERMITTEE NAMEESSu,,.r,af..,nq ,.,,.,,,'—di„g...nu NAS MARI LTURE TECHNJLJGIESt INC ADDRESS MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION ATTN: VITO L CAPORUSSO. PRESIDENT NATIONAL POLLUTANTGE ELIMINATION SYSTEM (NPDES) DISCHARGE ORING REPORT (DMRJ 2-16 f7 -f9 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY I I YEAR I MO DAY FROM 9 r I U51 Ul I TO (20.211 122-23J 124-261 (26-27) (28-290 130Ifl Form Approv ROTATING WQM OFFS;8 ( SUER O1) roveL ex�rp>� F — FINAL MINOR EFFLUE *** NO DISCHARGE NOTE: Reed InBtruadom before completing this form. PARAMETER (3 GM OnW QUANTITY OR LOADING (4 Cord Only) QUANTITY OR CONCENTRATION NO. FREauENCY SAMPLE (32-371 [><ANALYSIS 48-6 54-61 36-46/ 46-6 64-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2-69! (64-68) (69-700 TEMPERATURE, NATER SAMPLE ****** *****>ar *#***# #***** ( 04) DEG• CENTIGRADE MEASUREMENT PERMIT RE -PORT illCEf RAB 00010 T 0 0 SEE COMMENTS BELOW REQUIREMENT` **#* DAILY NX DEG•C - l40NTH TEMPERATURE, NATER SAMPLE MEASUREMENT **#### ##*##Ik **#*** ##*>tjc ( O4) DEG. CENTIGRADE PERMIT #**##?# ###*## ###*## REPORT —WICE/GRAS 00010 U 0 0 *#*### *** SEE COMMENTS BELOW REQUIREMENT #*# DAILY MX OEG.0 MONTH TEMPERATURE_-, NATER SAMPLE ****** ****** ****** ****** ( 04) DEG. CENTI'G3RADE MEASUREMENT 4;�Oe 49 PERMIT ##*### ****#* ***#** REPORT WICE/ RA8 0010 W 0 0 ##*### * SEE COMMENTS BELOW REQUIREMENT ### DAILY MR: DEG•C MONTH OXYGEN, DISSOLVED SAMPLE MEASUREMENT **#* ****#* 1p/ B **##** **#*#* ( 19) /g, (DO) PERMIT #*#*# REPORT ##*### ***### ' TWICE /GRAS . 0300 T 0 0 ** #* #* EE COMMENTS BELOW REQUIREMENT *#* DAILY MN MG/L MONTH OXYGEN, DISSOLVED SAMPLE *####* **#*#* **#### #**#** ( 19) (30) MEASUREMENT • �� " 00300 U 0 0 #####* # PERMIT *### REPORT #* *## ##sem** TWICE /GRAS EE COMMENTS 3ELOW REQUIREMENT ##* UAiLY MN MG/L }ltil+tTH XYGEN, DISSOLVED SAMPLE ###*#* *#*#** 00, ###### *#***# ( 19) �+� 6e-46 (DQ) MEASUREMENT • 0300 N 0 0 **##** ** PERMIT ***#** REPORT ##*#** *#*#** WICE/ RAS EE COMMENTS BELOW REQUIREMENT' **# DAILY MN MG/L MONTH ALINITY SAMPLE *#*#** ****** ****** ***### ( 32) MEASUREMENT 33,10 48 00484 T 0 0 PERMIT REPORT 1 WICE RAB BEE COMMENTS BELOW REQUIREMENT *** DAILY MX PPTH MONTH NAME/TITLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAYV THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INGUIRY OF THOSE e101NOUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE i DATE OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED.INFORMATION Is i TRUE, ACCURATE AND COMPLETE.I AM AWARE THAT THERE ARE - Of PreS t SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBIUTY OF FINE AND IMPRISONMENT. SEE 1 B U.S.C. ! 1001 AND 33 U.S.C. 3 I. /AvM6ss W,&, euas a0rt " e y include rest up to S 10,000 and ormsxlrrNsnAnp.isareoltolDstwssn6nwnehssnd6 ywnl _ I -77 ,,ll U SIGNA OF PRINCIPAL EXECUTNE OFFICE OR AUTHORIZED AGENT PED OR TED C pE NUMBER YEAR 1 MO I DAY COMMENTS ANLL tAMANA I IVN yr ANT V IULA I IUN.7 Irrerarence se arrecnmenrs neral MONITORING LOCATION "T" INDICATES TOPI "U" INDICATES MIDDLE AND "W" INDICATES BOTTOM. SEE PERMIT FOR ADDITIOvAL NOTES, COMMENTS AN, KE UIREMENTS. EPA Form 3320-1 (06-95) Previous editio,s .-ipv be used. (REPLACES EPA FORM T-40 Err!-IlCw v v^r 8-E '-jccn I _ -= - 40057/ 97'1917-1436 ` 1 r^ PERMITTEE NAME/ADDRESS Rnd d. Fardiry �a . i. -rr. NAME MARICULTURE TECH`V L06 -IFS, INC ADDRESS MARICULTURE TECH NFT P!I:N 1 PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION OTTN: VTTn 1 rAPnRI1tSf1_ PRF,�TnFlI • NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPDES) DISCHARGE MONITORING REPORT (DMR) (2-161 17-19) �• PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MO I DAY YEAR I MO I DAY FROM 971 031 011 TO 081 31 (2421) 122-231 124-251 (26-27) 128-29) (301-311 n LJ Form Approved. ROTATING WQM OFFS�� (SUBR O1) PProvaLeXWrp 8 F — FINAL lL�'i MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read instructions before completing this form. PARAMETER (3 Cord Only/ QUANTITY OR LOADING 14 Cord o/ry/ QUANTITY OR CONCENTRATION FREQUENCY SAMPLE 132-371 (46 -SM (54-61) (38-45) (46.53 (64-61/ EX E OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS 2 ss ANALYsIs 164 68) f69-701 SALINITY SAMPLE MEASUREMENT #****# ****** *#**** #** �J ( 32) r� 00480 U O 0 PERMIT #lEPiI#'i. > WICK R8 SEE COMMENTS BELOW REQUIREMENT **** PPTH M SALINITY SAMPLE MEASUREMENT **## ****** ****** ***** ` ( 32) 00480 W 0 0 ### PERMIT 1*## ###*1R *##kik ####?her REPORT ICE R$ SEE COMMENTS BELOW .REQUIREMENT #*** DAILY JqX PPTH MONT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT i PERMIT i REQUIREMENT i SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT i PERMIT I REQUIREMENT 1 SAMPLE MEASUREMENT PERMIT REQUIREMENT' NAMERITLE PRINCIPAL EXECUTIVE OFFICER 1 CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE MFOIIMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE WDMDUALS IMMEDIATELY RESPONSIBLE FOR TELEPHONE DATE OBTAINING THE NFORMATION, I BELIEVE THE SUBMITTED INFORMATION IS TRUE. ACCURATE AND COMPLETE. 1 AM AWARE THAT THERE ARE SIGNIFICANT POMTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING a -722 f10NA NRINq►Al EXECUTIVE OFFlCE Oft AUTHORIZED AGENT THE POSSIBILITY OF FINE AND IMPRISONMENT. EEE 1e U.S.C. l 1001 AND as U.S.C. f 1AL1B. /MrNMN I.rw Soft areWs mW Nw kt* flnm rV M $/0,000 anaa./n.IrrrwwlArllorwwrrffbMwow#aar"OW5ywa) TYM OR PRINT® CODE NUMeER YEAR MO DAY VV�Ga�10 I�aW i/a�iln/'a r ava� va ,�a� • . rv�,-, r rvry ,rr�,wwrv� wI �a NrurarrmrN //w �/ MONITORING LOCATION SIT" INDICATES TOPj -U- INDICATES MIDDLE AND "W" INDICATES 6OTTOM. SEE PERMIT FOR ADDITIONAL NOTES, COMMENTS AND REQUIREMENTS. EPA Form 3320-1 (08-951 Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00058/970917-1436 PAGE ?OF • 0 PERMITTEE NAMEiADDRESS17—hdeF—hlyN— ff.. NAME MA? I ULTU tE TECHNbL` GIES, I -NC ADDRESS MARICVLTURE TECH NFT PEN PO FOX 451 GREENFORT NY 11944 FACILITY LOCATION ATTN: VTTJ L CAPORUSSQ. PRESIDENT NATIONAL POLLUTANT DISCHARGE ELIMINATION SYSTEM (NPDES) DISCHARGE MONITORING REPORT (DMR) 12-161 117491 PERMIT NUMBER DISCHARGE NUMBER MONITORING PERIOD YEAR I MODAY YEAR MO DAY FROM TO 124211 122-231 (2425) 126-271 (28-291130-31) Form Approved. ROTATING WQM OFF p' #WtD�i s (SUSR 01) ai611� s F — FINAL MINOR EFFLUE _ *** NO DISCHARGE NOTE: Read instructions before completing this form. PARAMETER (32-37)>< I3 Card OnW QUANTITY OR LOADING 146-53/ 154-611 /4 Card Only/ QUANTITY OR CONCENTRATION I38-451 1453 15461/ NO. EX /62-63 FREQUENCY SAMPLE of ANALYSIS TYPE 164681 (69-701 AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS TEMPcRATUREV NATER EG* CENTIGRADE SAMPLE MEASUREMENT #**#** #**#*# ***#*# **#*** n v(�6 � t 0$) Al,--k)/Cl8 PERMIT *##*** **###* ****ale* XEPDR. I =: EIFI£E/ tAB 00010 T 0 0 *##*## #** SEE COMMENTS BELOW REQUIREMENT QA > KX. DEG.0 IMONTH TEMPERATURE, MATER Ge CENTIGRADE SAMPLE MEASUREMENT yc##### ##*### ####*# *****# 40'0 t 04) a�3p 6iP�06 PERMIT VICE/GRAB 0010 U 0 0 SEE COMMENTS BELOW REQUIREMENT #** DAI)t< DEG.0 MONTH TEMPERATURE, WATER DE -Ge CENTIGRADE SAMPLE MEASUREMENT ##ale### ###**# #*#### **#### � 4400 t 04) JJ a /3O &44151 0010 Eli 0 0 PERMIT REPt3RT MICE/ RAS EE COMMENTS BEL REQUIREMENT ##*# DAILY MX OEG•C MOUTH OXYGEN, DISSOLVED ( Dry) SAMPLE MEASUREMENT *##### *##### Q • D #***** ####** { 19) �. / %�gj 0300 T 0 0 ##*### ** PERMIT ***##* REPORT ##*#*# #**IRS* MICE/ RAH EE COMMENTS BELOW REQUIREMENT ### DAILY MN MG/L MONTH OXYGEN, DISSOLVED SAMPLE MEASUREMENT ###### ##*### d ##*#*# ##*### ( 19) a/ M8(00) 30 0300 U 0 0 PERMIT #####* ale##### *# REPORT *#**** *#**** —NICE/GRAB SEE COMMENTS BELOW REQUIREMENT ##* DAILY MN #4G/L MONTH XYGENt DISSOLVED 0 0) SAMPLE MEASUREMENT ###*## **#### �p r #**### ###### { 19) /� +<we, 0300 W 0 ! PLHMII ILL NAMLiA -J—r J. fu' ,,,. ...q NAME I TUBE TE.CHNOLUGIES, INC ADDREss MARICULTURE TECH NET PEN PO BOX 461 GREENPORT NY 11944 FACILITY LOCATION NATIONAL POLLUTANT 015 E ELIMINATION SYSTEM fNPDESI Form Approved gft DISCHARGE M4WING REPORT DMR) ?-t6) 17 -fol ROTATING WQM OFF52T" WO (SUBR 01) pprovrlLa7<ptr 8 PERMIT NUMBERJ DISCHARGE NUMBER F — FINAL l C� MONITORING PERIOD MINOR YEAR I MO I DAY I YEAR I MOAY EFFLUE _ FROM TO **# NO DISCHARGE A11M: VlIU L f-ArUKU bUl YKtSlUtN1 IZa2tl Izz-z31Ize-zsl 126271128-291 f3D-311 ^ 11&' 4rw4w" wsm''wqw"ew'wwUwwFwwwwW" rwm. PARAMETER f3 Card Only) QUANTITY OR LOADING /4 Card Only/ QUANTITY OR CONCENTRATION NO. FREQUENCY SAMPLE f3? -371 46 54-61 (38-45) 1d6 64-61 EX OF TYPE AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS z -e3 ANALYSIS /61-661 (69-70 SALINITY SAMPLE Q ( 32) MEASUREMENT MEASUREMENT V 3 a Q •� �jp� U O O iIERMIT00484 CE . SEE COMMENTS BELOW REQUIREMENT ****PPTH�;. SAMPLE SALINITY SAMPLE *###*# »c###** ###*** ##,«#*# 32) MEASUREMENT PERMIT ****Itxr ***i�* **ar*** *##** _ ` RE P.... IC£ RAN 00480 M 0 O *** SEE COMMENTS BELOW REQUIREMENT *#** AIL f III PPTH MOW0 SAMPLE MEASUREMENT MONITORING LOCATION "T" INDICATES TOP? N'U'N INDICATES MIDDLE AND "W- INDICATES BOTTOM, SEE PERMIT FOR ADDITIONAL NOTES9 COMMENTS AND REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00062/971917-1436 PAGE ZOF PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT ., REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT NAME/TITLE PRINCIPAL EXECUTIVE OFFICER IC RTIFY UNDER PENALTY OF LAW THAT 1 HAVE PERSONALLY EXAMINED AND FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN. AND BASED ON TELEPHONE DATE MY INQUIRY OF THOSE IiO1VIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING Q 'f THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. f 1001 AND 33 U.S.C. f 1315. P%wN" rwdw View sawfts Hwy Awkide ffmw rP to 610,000 PED OR PRIIIITED and or marsm n aarw~ 6 nwna6i and B y..z► . /� 7 _/ 7� / SIGNATURE PRINCIrAI EXECUTIVE OFFICER OR AUTHORIZED AGENT CODE NUMBER YEAR MO DAY COMMENTS AND EXPLANATION OF ANY VIOLATIONS /Reference aM ettechments here/ MONITORING LOCATION "T" INDICATES TOP? N'U'N INDICATES MIDDLE AND "W- INDICATES BOTTOM, SEE PERMIT FOR ADDITIONAL NOTES9 COMMENTS AND REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00062/971917-1436 PAGE ZOF PERMITTEE NAMEIA•SSll—AkFYubp nn.,,J L,gnmq NAME MARICULTURE TECHNULUGIES, INC ADDRESS MARICULTURE TECH NET PEN PO 6OX 461 GREENPORT NY 11944 FACILITY LOCATION ATTUH_ VTTn L CAPf]R115S[l_ PRFSTDFNT NATIONAL POLLUTANT DI E ELIMINATION SYSTEM ,,NPDESI DISCHARGE M ORING REPORT DM9l PERMIT NUMBER I DISCHARGE NUMBER MONITORING PERIOD YEAR O I DAY I I YEAR I MO DAY FROM 9fl U81 01LITO 120-211 122431 124-221 126.271 128-291 130311 Form Approvaq ROTATING WQM OFFS�L-e�p1rp %.m (SUBR 01) PProv 1 C�9 8 F - FINAL MINOR EFFLUE _ #** NO DISCHARGE NOTE: Road inatruadorls beton oonwloting this form. PARAMETER 132-371 (3 Gard Onyl QUANTITY OR LOADING 146-5 (54-61 (4 Card Only/ QUANTITY OR CONCENTRATION 138-451 146-63 64-61 NO. EX 2�s FREQUENCY OF µ4_Y813 164-68i SAMPLE TYPE 160-70- AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNITS TEMPERATURE, WATER DEG. CENTIGRADE SAMPLE MEASUREMENT ****** *#**** ****#* ****** nn t 04) a PERMIT REPORT WICEy RA$ 00010 T O O SEE COMMENTS BELOW REQUIREMENT **** DAILY NX DEG.0 MOUTH TEMPERATUREI HATER OEG. CENTIGRADE SAMPLE MEASUREMENT ****# *********** ****** p?Qi� t O4) -/o pd 6-4A9 PERMIT REPORT 'TWICE/ GRAS ' 0010 U 0 0 EE COMMENTS BELOW REQUIREMENT *** DAILY HX DEG.0 MONTH EMPERATURE9 WATER DEG. CENTIGRADE SAMPLE****** MEASUREMENT ****** **#*** *****s �/ AI9.3 t 04) /3v Gil�g PERMIT REPORT WICEj RAB 0010 W 0 O SEE COMMENTS BELOW REQUIREMENT *** DAILY MX DEG.0 MONTH XYGENT DISSOLVED (DO) SAMPLE MEASUREMENT *##*## #*rk##* L f Cf *#*#** #*##*# t 19) a` / 3,0 �JQ PERMIT REPORT TWICE/ GRAS 0300 T 0 0 SEE COMMENTS BELOW REQUIREMENT Ik** DAILY MN MG/L MONTH XYGENI, DISSOLVED- (DO) SAMPLE MEASUREMENT *#### *##*** .r 6 ****** ***#** t 19) a1W o6kA8 00300 U 0 0 PERMIT REPORT #**### **** WICE/ RA$ SEE COMMENTS BELOW REQUIREMENT *�k* _ DAILY MN MONTH OXYGEN, DISSOLVED SAMPLE MEASUREMENT **#i1#* **##** ` 110 *#***# #***�t*)(DO) rG 0300 W O 0 *###*# ** PERMIT **rk*## REPORT ****** **#*#* MICE RAS `EE COMMENTS. BELOW REQUIREMENT. _ ##* DAILY MN MONTH SALINITY SAMPLE ***##* *#tk*tk* #tk**#* ***#**MEASUREMENT ��/ 2X640 ��NQ 0480 T 0 0 ****** ** PERMIT ***** ****** ****** REPORT WICE RAB EE COMMENTS BELOW REQUIREMENT *##I DAI Y MX PPTH MONTH NAMWITLE PRINCIPAL EXECUTIVE OFFICER I BERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR WITH THE INFORMATION SUBMITTED HEREIN; AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BELIEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. i AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMITTING FALSE INFORMATION, INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. 1 1001 AND 331477-/777SIfiNA U.S.C. 1 1318. (Pen/Lbt wisbr Dow sarrurts msy kwAA* rwws up to S 10,000 and nwx wnhrpiworrwrd Kofbtrween6monrnsa5yeam) _ _ F PRINCIPAL EXECUTIVE OFFICE RAUTHORIZEDAGENT TELEPHONE DATE - - tP—nc—l-c OR COQ NUMBER YEAR MO I OA COMMENTS AND EXPLANATION OF ANY VIOLA 1 IUN5 ifrererence bur e[facnments nerel MONITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "W• INDICATES BOTTOM, SEL PERMIT FOR ADDITIONAL :MOTES, COMMENTS AN0 REQUIREMENTS. EPA Form 3320-1 (08-95) Previous editio,s -iav be used. (REPLACES EPA FORM T-40 NrHlr;w v N'�- PE USED I -� e 00065/971917-1435 1�� PERMITTEE NAME/AAS d8a6wb fruuy %o.. NAME . MARICULTURE TECHNOLOGIES, INC ADDRESS MARICULTURE Tr_CH NET PEN PO BOX 461 GREENPORT NY 11444 FACILITY LOCATION NATIONAL POLLUTANT q ELIMINATION SYSTEM NPDES) Form Approved DISCfj� HA M G REPORT o 9/ ROTATING WQM OFF (SUBR 01) PProveq><gr8 PERMIT NUMBER DISCAARGE NUMBER F — FINAL G MONITORING PERIOD MINOR YEAR IMOI DAY I YEAR I MO- EFFLUE FROM q 0 01 To 0 ***-NO DISCHARGE A T T N: V I I U L twAPUKLIS509 N R E S I D E N I 120-211 122-ZM 124-251 (26-27/ 126-29/ 130.311 w r c: Man wwuuaumw Palms cvmPwnny ars corm. PARAMETER 132-37) >< 13 Cud 01W) QUANTITY OR LOADING . 46 54 -61 (4 Cud Only/ QUANTITY OR CONCENTRATION 1319 -ss/ r ss-sf NO. EX 2 �OU94C' OF r6I-68/ ANA 6WYSI SAMPLE TYPE (69-70V AVERAGE MAXIMUM UNITS MINIMUM AVERAGE MAXIMUM UNIT SALINITY SAMPLE MEASUREMENT #***## *#*#** *#**## #### Q J3.d/3►O ( 32) 00480 U O 0 SEE COMMENTS BELONMONT *### PERMIT RENT; QUIREME <:REPOtT iiIGEA$ ` SALINITY SAMPLE MEASUREMENT 33• 32) 00460 k 0 0 SEE COMMENTS BELow PPTH PERMIT REQUIREMENT' REPIDATWICE AIL. MX ROUT RIIB�j SAMPLE MEASUREMENT PERMIT REQUIREMENT' •� SAMPLE MEASUREMENT PERMIT REQUIREMENT' SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT REQUIREMENT SAMPLE MEASUREMENT PERMIT .REQUIREMENT.:- NAME/i1TLE PRINCIPAL EXECUTIVE OFFICER I CERTIFY UNDER PENALTY OF LAW THAT I HAVE PERSONALLY EXAMINED AND AM FAMILIAR UMTH THE INFORMATION SUBMITTED HEREIN. AND BASED ON MY INQUIRY OF THOSE INDIVIDUALS IMMEDIATELY RESPONSIBLE FOR OBTAINING THE INFORMATION, 1 BEUEVE THE SUBMITTED INFORMATION IS TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES FOR SUBMIrnNG FALSE INFORMATION. INCLUDING THE POSSIBILITY OF FINE AND IMPRISONMENT. SEE 18 U.S.C. f 1001 AND 33 U.S.C. f 1318. �Mn1lehe Un4br thea( sa sifts may iiclub Ow w to $ f0,000 and ormnrb+wan�eruarrwrte/eerw«nsnwetrwands ytr:l TELEPHONE DATE f V_ ,r res �r CEQ 4DAY SH3NATURE SAL EXECUTIVE OFFICER AUTHORIZED AGENT PRINTED AREA NUMBER IYEAR MO COMMENTS AND EXPLANATION OF ANY VIOLATIONS (Reference a# attachments here) MONITORING LOCATION "T" INDICATES TOP, "U" INDICATES MIDDLE AND "N" INDICATES 1OTTOM. SEE PERMIT FOR ADDITZONAL NOTES, COMMENTS AND REWIREMENTS. EPA Form 3320-1 (08-95) Previous editions may be used. (REPLACES EPA FORM T-40 WHICH MAY NOT BE USED.) 00066l970917-1436 PAGE 2 0F _ = GURICN F GERE LABORATORIES, INC. September 5, 1997 Dr. Merle Wiggin Peconic Associates, Inc. One Bootleg Alley . P.O. Box 672 Greenport, NY 11944 Re: Lab Data Report File: 6626.001.517 Dear Dr. Wiggin: Please find enclosed the results of laboratory analysis on samples received 08/21/97. If you have any questions concerning these results, -please do not hesitate to contact us. Very truly yours, • O'BRIEN & GERE LABORATORIES, INC. Monika Santucci Supervisor MS/vpm Enclosure U O'SRIEN G GERE LASOSATORIES. INC. an O'Brien & Gere Company 5000 Brittonfield Parkway ! P.O. Box 4942 / Syracuse, NY 13221 / (315) 437-0200 FAX (315) 463-7554 O'Brien & Gere Laboratories,Inc. Client: Peconic Associates, Inc. Project: Maricultum Technologies - Net Pen Prcj. Desc: S.E. Plum Island Analytical Results Wet Chemistry Job No.: 6626.001.517 Certification NY No.: 10155 Sample: F8633 Collected: 08/20/97 Matrix: Water Samp. Description: 1F - Bottom Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .05 op/L L31107061A 09/02/97 090297Y21 Nitrite i nitrate 4.01 sip/L L11107041A 08/28/97 082897Y23 nitrogen nitrogen Total Kjeldahl nitrogen .5 mp/L EPA 351.2 08/27/97 08/29/97 08279721 Total phosphorus .1 sip/L EPA 365.4 08/27/97 08/27/97 08279721 Notes: F8634 Collected: 08/20/97 Matrix: Water •Sample: Samp. Description: 1F - Middle Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .02 np/L L31107061A 09/03/97 0903971421 Nitrite i nitrate <.01 sip/L L11107041A 08/28/97 08289723 nitrogen Total Kietdahl nitrogen .6 mg/L EPA 351.2 08/27/97 08/29/97 08279721 Total phosphorus 4.05 mo/L EPA 365.4 08/27/97 08/27/97 082797Y21 Notes: • J -Estimated value Authorized: mp�..0 JK9&,e~ Date: September 4,1997 Monika Santucci 5000 Brittonfield Parkway / Suite 300, Boz 4942 / Syracuse, NY 13221 / (315) 437-0200 O'Brien & Gere Laboratories,Inc. Client: Peconic Associates, Inc. Project: Maricultum Technologies - Net Pen Proj. Desc: S.E. Plum Island Analytical Results Wet Chemistry Job No.: 6626.001.517 Certification NY No.: 10155 Sample: F8635 Result Units Method Collected: 08/20/97 Matrix: Water Samp. Description: 3F - Bottom .12 sip/L L31107061A Received: 08/21/97 11:00 0902971121 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .08 ne/L L31107061A 09/02/97 0902971121 Nitrite i nitrate <.01 mg/L L11107041A 08/28/97 08289823 nitrogen <.05 sg/L EPA 365.4 08/27/97 08/27/97 0827971121 Total KJeldahl nitrogen .6 ng/L EPA 351.2 08/27/97 08/29/97 0827976121 Total phosphorus <.05 mg/L EPA 365.4 08/27/97 08/27/97 082797621 Notes: Sample: F8636 • Samp. Description: 3F - Middle Collected: 08/20/97 Matrix: Water Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .12 sip/L L31107061A 09/02/97 0902971121 Nitrite i nitrate <.01 mg/L L11107041A 08/28/97 08289823 nitrogen Total KJeldahl nitrogen .7 sg/L EPA 351.2 08/27/97 08/29/97 08279821 Total phosphorus <.05 sg/L EPA 365.4 08/27/97 08/27/97 0827971121 Notes: • J -Estimated value Authorized: • Date: September 4,1997 Monika Santucci 5000 Brittonfield Parkway / Suite 300, Box 4942 / Syracuse, NY 13221 / (315) 437-0200 O'Brien & Gere Laboratories,lnc. Client: Peconic Associates, Inc. Project: Mariculture Technologies - Net Pen Prof. Dew: S.E. Plum Island Sample: F8637 Samp. Description: 1R - Bottom Analytical Results Wet Chemistry Job No.: 6626.001.517 Certification NY No.: 10155 Collected: 08/20/97 Matrix: Water Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed CC Batch Note Ammonia nitrogen .1 ag/L L31107061A 09/02/97 090297W21 Nitrite i nitrate <.01 mg/L L11107041A 08/28/97 082897W23 nitrogen Total Kjeldahl nitrogen .5 mg/L EPA 351.2 08/27/97 08/29/97 082797W21 Total phosphorus <.05 p/L EPA 365.4 08/27/97 08/27/97 082797W21 Notes: •Sample: F8638 Samp. Description: 1R - Middle Collected: 08/20/97 Matrix: Water Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .04 mg/L L31107061A 09/03/97 090397W21 Nitrite i nitrate .01 mg/L L11107041A 08/28/97 082897W23 nitrogen Total Kjeldahl nitrogen .5 mg/L EPA 351.2 08/27/97 08/29/97 082797W21 Total phosphorus .06 mg/L EPA 365.4 08/27/97 08/27/97 082797W21 Notes: • J -Estimated value Authorized: T xr.Ar Date: September 4,1997 Monika Santucci 5000 Brittonfield Parkway / Suite 300, Box 4942 / Syracuse, NY 13221 / (315) 437-0200 O'Brien & Gere Laboratories,lnc. Analytical Results Wet Chemistry Client: Peconic Associates, Inc. Job No.: 6626.001.517 Project: Mariculture Technologies - Net Pen Certification NY No.: 10155 Prof. Desc: S.E. Plum Island Sample: F8639 Collected: 08/20/97 Matrix: Water Samp. Description: 2R - Bottom Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed GC Batch Note Ammonia nitrogen .05 mg/L L31107061A 09/02/97 090297W21 Nitrite i nitrate <.01 mg/L L11107041A 08/28/97 082897H23 nitrogen Total Kjetdmhl nitrogen .7 mg/L EPA 351.2 08/27/97 08/29/97 082797Y21 Total phosphorus <.05 mp/L EPA 365.4 08/27/97 08/27/97 08279721 Notes: Sample: F8640 • Samp. Description: 2R - Middle Collected: 08/20/97 Matrix: Water Received: 08/21/97 11:00 Parameter Result Units Method Prepared Analyzed OC Batch Note Ammonia nitrogen .02 mg/L L31107061A 09/03/97 09039721 Nitrite i nitrate <.01 mg/L L11107041A 08/28/97 08289723 nitrogen Total Kjeldaht nitrogen .7 mg/L r EPA 351.2 08/27/97 08/29/97 082797W21 Total phosphorus <.05 mg/L EPA 365.4 08/27/97 08/27/97 082797W21 Notes: • J -Estimated value Authorized: Date: September 4,1997 Monika Santucci 5000 Brittonfield Parkway / Suite 300, Box 4942 / Syracuse, NY 13221 / (315) 437-0200 • • CHAIN OF CUSTODY RECORD CTORICN 6 GCRC L.AeORATORIES, INC SURVEY: t7fAXiev&mw SiA V447M LOCATION: s,,,r„ sive ep P,w is..w,o 14*4 =s..+•v t„y SAMPLED BY: EQ�c 1✓,►a,,•�t ORGANIZATION: G'�'7flzo,j Eru�r�sz.,.s Assac,,�.rs Cc STATION NUMBER SAMPLE LOCATION DAT E MLLFLM TIME COUMEQ SAMPLE VATAIX COMP. OR GRAB NO. OF GMUMRS ANALYSIS REQUIRED 1 F �r ijo rr,,�, ,r►,ofl�r �: J i=to w G T r P N� , /✓ Na No Ilk AO' 3 F ZC' — ZR Bo Tom'^ 9` j!r 1 24 l - Relinc fished B ' / AT 17toki3� TIME Recewrc By: GA•= TIME Relinquished By. a, TE TIVE Recz%-ec By. >11?.: 1tM Relinquished. By: DATE TI;.4E feck.,ved by Lab 0 METHOD OF SHIPMENT: O'DRIEN 6 GERE LADORATORIES. INC. an O'Brien A Gere Company 5000 Brittonfield Parkway / P.O. Box 4942 / Syracuse, NY 13221 / (315) 437-0200 FAX (315) 463-7554 ,. _ coA L I L_ J, -045 618 4890341 568489014"l 5167N I023-9795-4 r IF e4f,,� CO- e- L4 t516 477-1777 MCRICULTRIAL 5000 81_14n#Cs_,old i.,I:A._I, 1'. "'. U."PC 127 STERLING 57IN to, c u -V Q_ Ft SlAd ZAP crl,ileA GREENPURT NY 1 1 9 4 4 ii:ii6ib�ii-tt)fxitir4iinN.nt F EXAddfassillorgI Jll yij,, OA 11110;13 1 1) slaw IIPRequireA wt W-.,; ZZ El. I . u, I I Nw'.k:1 1.1, 1' 11"I 1'll...'. .=UP -22-97 MON 1!5 � 2 S T I RL- I "a COMPUTER P 0 1 • UBRIEN G GORE L.AGC7RATCMIL!S. INC SgMmber 1S, 1997 Dr. Mede Wiggin Pecaeic As9ociates, Ina. One Bootleg Alley P.O. Box 672 Grar47or% NY 11944 Re: Lab Data Report File: 6626.001.517 Dear Dr. Wiggin: Plena find enclnsed the results of laboratory analysis on samples received 08128197. 1f yuu true any quccdom concerning these results, please do not hesitate to =1 ct us. • Vey truly yours, O' BRIEN a GERE LABORATORIES, INC. I�,L. * 11� Monika Santucci Supervisor MSlvpm • CGRIEN Fi GEME LAOCRATOMMM INC. an O'8 W & Gera Company Soon SManNO Parkway / PO. Box 4942 / Syracuse. NY 13221 I (315) 437-02M FAX (315) 463-7554 SEP -22-1997 16:11 5164770198 97% P.01 SUR -22-907 MON 15:!53 STIRLING COMPUTER P-02 O'Brien & Gere Laboratorles,bc. Chest: pecooie Anocista. lac. pmjwe mmim"m Teebsoloem - Nat Pas pith. Den: S.& plum wwd Analytical Results Wet Chemistry Job Na: 6626.001.517 CatiBcadw NY No.: 10155 Sompim P9176 tesutt units .03 WWL Method L31107MIA Collocsed: Oa/27/97 08:00 Mt U&. Watee Samp. Dssc:iptom: IF Bottom .01 em/t 011070M1A !received: OMAM 09:43 Paramour Awmnfe n1too9w+ 1towit units .09 MIVL at"d L3110706tA PM -rod An.tvted oe htdr Not. 09/03/9T 09039TU21 Nitrite i nitrate 4.01 MIA 1,11107041A 09/10/47 091097t/22 nttrooen .06 00A EPA 365.4 09/03!97 09/04/97 090397183 Total Kloidlpt nttr0gon .5 soft EPA 351.2 09/03/97 09/08/97 090397k23 Tetat ommoomm .2 VWL EPA 363.4 09/03/97 09/04/97 090397183 Notes: • Sample: F9177 Samp. Desmptson: IF Middle Collected: 08!27/97 08:10 Matrix: Water Received: 08/28/97 09:45 Pwwwter Amm►fe nit. "a+ tesutt units .03 WWL Method L31107MIA P=red Anotyzed OC Botch Not* 09/03!97 0903971421 Nitrite i nitrate .01 em/t 011070M1A 09/10/97 091097V22 of tro". Tout t:Jotdwt nftr"w .3 mrs/t VA 351.2 09/03/97 09/08/97 0903971+25 Teeat phosphons .06 00A EPA 365.4 09/03!97 09/04/97 090397183 Nota: J-Eatiamood vale. Authorised: Js--iwi e., 0 Date: September 12,1997 Monih Saatucci 3000 anooaSold Pa*wsy / Suite 300, Box 4942 / Syracuse, NY 13121 / (315) 437-M SEP -22-1997 16:11 5164770198 P.02 SUP -22-97 MON 1!5:5:5 STIRLING COMPUTER P. Oz O'Brien & Gere Laboratories,Inc. CHUM FMOWe Anodaoee, loc. hojeat Asara T6411 6411- Net Pao Prot. Dwain S.L ft m bland Analytical Results Wet Chemistry Job No.: 6626.001.117 C r iSaitiaa NY No.: 10133 Sae ow F9176 Collected: 08/27/97 09:10 Maui= Wow lamp. Deaeripbm 3F Bottom i Awkied: 08/28!9'; 09:65 [araMer 01"Vit Unita .10 aQ/L `iiatbw L3110MIA MMred Analvzad X Batch Meta 09/03/47 09039821 Mamie nfta a" Nitrite i nitrate .01 ae/L 1,1119MIA 09/10/47 091097= ni t. a". 1,11107041A 04/10/97 041097M nitrooan Totat KjeldM/ not rM w .3 ais/L DA 351.2 09/03/97 04/08197 0903973 Total phoapdory .06 +e/L PA 365.46 09/03/97 04/06/97 0903971123 Noma: Sample: F9i79 Collected: 08/21/97 W.13 Matrix: Water Saeap. Dercripaa+a: 3F Middle Received: 08/28/97 09:45 • Psra ter Imit units aathodPranOnd ALMlvzed Qc "Itch Mote Aaiwfa nitroew .04 XWL L3110MIA 09/03/97 0403971;21 Mltrite 4 nitrate 4.01 p/L 1,11107041A 04/10/97 041097M nitrooan Tout Kjeldahl ni traw .3 "A EPA 351.2 04/03/97 04/0!1/97 0903971;23 Total pw"Morue .06 man iPA 365.4 04/03/97 09/04/97 09MAJ23 Noiea: J-Ed.mated valve Dara: Sepromber 12.1997 MOWU Saatucci • 5000 Brincafield Par rmq / Sake 300, Dan 4942 / Syraclma. NY 13221 / (31S) 437-02W SEP -22-1997 16:12 5164770198 9511: P.03 SUP — 2 2— 9 T M O N O'Brien & Gere Laboratories,inc. 1 z - M4 ST I Rl_ I NG COMPUTER Analytical Results Wet Chemistry COMM Pecooio Associates. lana. Project: Maticutt m Techooi*w - Net Pen. Praj. Deet" S.B. Plain Wood M No.: 6=.001.517 Ca dncwm NY No.: 10155 Semple: P9130 C U=teri: OGMI97 09:37 Matic: Water Same. Daaipb aw tit Bouont • Samp. Description: I R Middle Received: 08/28/99 09:43 Psremster __, Result - g to nitroge tenth 1Ntbw lreoarad Anatyzod 91 Batch Note 09/03/97 0903971 W/L L31107061A nitrite i altreto .02 a0/L L11107041A 09/10/97 0910971122 nitrogen 090397121 nitrite i nitrate .02 q/L Total Kleldsht nitr02'M+ .4 WWI. QA 351.2 09/03/97 09/08/97 0903471123 Totat phosoorw .08 OWL EPA 365.4 04/03/97 09/04/97 0903971+23 Notal: Semple: P9t81 Collected: 08/27/97 09:42 Matrix: Water • Samp. Description: I R Middle Received: 08/28/97 09:45 larae�tor Resutt units Method orioerod Analyzed QC Batch Not Amnle nitrogen .06 XWL L31107061A 99/03/97 090397121 nitrite i nitrate .02 q/L L1110MIA 09/10/97 091097122 nitrogen Total Kj•tdoh+ Mtrogon .2 OWL EPA 351.2 09/03/97 09/08/97 090397N23 Total ohosow-wr .011 q/L EPA 369.4 0!/03/97 04/04/97 0903971123 • f -Estimated value Autltotixed• rujw Joaut.0p.."A Date: September 12,1997 Monika Santucci 5000 BrittoatieW Pathway / Suite 300, Bos 4942 / Syrscuwe NY 13221 / (315) 437-0200 SEP -22-1997 16:12 5164?70198 P.04 SUP -22—S7 M O N O'Brien & Gere Laboratoriesjnc. 1!5 :!5!!S ST I RL I NG COMPUTER P - 03 Cliaft Pecoaia Aasaddse, leo. Project: Matievftm TaebsoloSim - Net Poo Prof. Dean S.B. Plum k aad Analytical Results Wet Chemistry Job No.: 6626.601.317 Ceotificatim NY No.: 10135 Samplx P9182 teaatt Unice Nothad CADadaoi: 08/27/97 10:32 Matrix: Wow Same. Damariptioa: 2R Boom L3110MIA 09/03/97 090397W21 RaWveda 0612LW 09:45 Parameter aeault units flethed Preoered Anlned OC fetch Note 090397NL1 PAMMi* nftr"M .02#4/4 L311WMIA 09/03/97 Nitrite a nftrese m.01 *WL 0110MIA 09/10/" 09109TWU nttragen Total tjoideht nfb Ww .3 wWL VA 331.2 09/03/97 09/03/97 090397183 Total phoephorue .06 owt DA 365.4 09/03/9T 09/04/97 090397123 Notes: Samples P9183 • Samp. Descripboo: 2R Middle Collected: 06/27/97 10:37 Matrix: Water Received: 06128/97 09:45 Paramter teaatt Unice Nothad f rated Anetned QC Batch Note Ammonia nitrogen 6.01 WWL L3110MIA 09/03/97 090397W21 Nitrite i nitrate .01 We/L L11107041A 09/10/97 0910971122 nitrogen Total KleldmM nitrogen .4 mg/t TEPA 351.2 09/03/97 09/04/97 090397Y23 Total phoaptfons .08 OWL EPA ?65.4 09/03/97 09/04/97 0903971123 Nalmm • f -Estimated value Autbotim&- AJA a ..j Dale: September 12,1997 Moviia Swmmmi 3000 Btittaofield Parkway / 3uito 300, Box 4942 / Syracw% NY 13221 / (3 15) 437-0200 SEP -22-1997 16:13 5164770198 P SUP -22-97 MON 1!5--!5!5 S T I R L I N G COMPUTER P. 0 6 CHAIN OF CUSTODY RECORD CO3 1 13RIEN F GERE I.ApOfaATCRIES. INC • t5r, 3/ SURVEY /l,Te,a k aa.s v f i '�c�.ah►C! . S•K . LOCATION kw wn:rc 19UPt A.N.• Ss.wndw, NY SAMPLED BY: Ed:lt, w.-wrfx ORGANIZATION: swrm ttuMeER ` 10N Dart MUM TIME CX= SMt U MAM WW OR ON Iia of CNN= �- RMAW f /F 6. rra.t I1t.u��t 7 bos. •/♦ 1N C I �•r /� rN N �o /c,.i 3 f M•�u�t :if i ie orv,•+ 14-37 �-- / a Ova p4,e' f t � , A�rgm ited drDa of -if -7 TIME %Med cy. # v r � 09E V0F I Aernpwsned t3v WE TIME Rawwd 9y: -�...�� ' t1�fE FtME 144kn 11l w Rt j 0AM Tl*iiY FIMi`_ :Y COMMENTS: (t 04,t METHOD OF SHIPMENT: • 0lBr-LEN & GGRC- LAGOAATOMICS. ►NC. an O'erfen & Gera Company 5000 8ntt nosid Parkway; P0. Bos 48+2 / Syrwuse. NY 13221 / (315) 437-M FAX (315) 483.7554 r -. .SEP -22-1997 16:14 5164770198 95% P.06 z l � RECIPIENT'S COPY AIRB/LL ►MCMI 4109036116 ours !l N" CAU AOri-2Js sm IOU FFF nudnni Hwar�l 4109x36116•, r �9 6 s mm C(I Rt I LD Qi 1 RI a� IM 11 Taw r 1. p lsu rat � p +cool lint � p �.��. ....•... � VOW H! • �M � � ; 1 1 1 6tlRtl�Qlt�l011S 6r�... „ ri V �_ � _ se�...c �r r•r• ...... • ••.�r.�ra- 1 w.t^w r •itr 1. w n nrt I n :....�. erna amen - •�- i • I i � I � � i mm C(I Rt I LD Qi 1 RI a� IOW Tq A.O..i10 , � eE r Elvrcr.e Ms.M. R.:1i1 J:i tfr w 1 VOW H! �i,ba i mm C(I Rt I LD Qi 1 RI a� 0 Ul GCOI EST LABORATORIES, INC. ENVIRONMENTAL TESTING NA Y 51622 4 7 FAX 516 422 5770 377 SHEFFIELD AVE. • . B B LON, N.Y. 11703 () -577 • LAB NO.C973500/1 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*. Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 1F—Bottom, 8:15 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.3 Nitrogen, total as N mg/L 0.3 cc: REMARKS: * South side of Plum Island. DIRECTO 0 0 GCO■EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE • N BABYLON N Y 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973500/2 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 1F—Middle, 8:20 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.7 Nitrogen, total as N mg/L 0.7 cc: REMARKS: * South side of Plum Island. DIRECTO GCO■EST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 * (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973500/3 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 - ATTN: Robert Link 0 40 SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 3F—Bottom, 8:55 am ANALYTTCAI. PARAMF.TF.RS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 1.0 Nitrogen, total as N mg/L 1.0 cc: REMARKS: * South side of Plum Island. DIRECTO GOOIEST LABORATORIES, INC. db 0 1� ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (51 6) 422-5770 LAB NO.C973500/4 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 3F -Middle, 9:00 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc: REMARKS: * South side of Plum Island. DIRECTO 0 0 GCO■EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973500/5 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*. Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample. 1R -Bottom. 10:25 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.6 Nitrogen, total as N mg/L 0.6 cc: REMARKS: * South side of Plum Island. X111 --/,•T TnJr . nIn- ^ DIRECTOR 0 CO EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. ON. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973500/6 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, IR—Middle, 10:30 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.4 Nitrogen, total as N mg/L 0.4 cc: REMARKS: * South side of Plum Island. ,,,,,.,.,.,, -- J, . DIRECTOR CO EST LABORATORIES, INC. ENVIRONMENTAL TESTING 0 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 0 LAB NO.C973500/7 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 2R—Bottom, 9:35 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.7 Nitrogen, total as N mg/L 0.7 cc: REMARKS: * South side of Plum Island. DIRECTO CO EST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422.5770 LAB NO.C973500/8 09/04/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link L� SOURCE OF SAMPLE: Sea Water off Plum Island*, Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/20/97 RECEIVED:08/20/97 SAMPLE: Water sample, 2R—Middle, 9:40 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.6 Nitrogen, total as N mg/L 0.6 cc: REMARKS: * South side of Plum Island. rn= 22141 NYSDOH TDyk 1 n1?n DIRECTO �'O EST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/2 09/12/97 0 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 A71'N : Robert Link, SOURCE OF SAMPLE: Sea Water off Plum Island-, Job *CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewater sample, 1F—Middle, 8:10 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.03 Ammonia as N mg/L <0.05 Nitrate as N mg/L <-0.05 Tot. Kjeldahl N. mg/l. 0.4 Nitrogen, total as N mg//L 0.4 C C : REMARKS: South side of Plum Island. • �I DIRECTOR V , COEST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/3 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street. P.O. Box 461 Greenport, NY 11944 ATTN : Robert Link • • SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewater sample, 3F—Bottom, 9:10 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.03 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc: REMARKS: * South side of Plum Island. DIRECTO= i 0 —% e %*-0%0EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777• FAX (516) 422-5770 LAB NO.C973625/4 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATrh : Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08%27/97 RECEIVED:08/27/97 SAMPLE: Vastewater sample, 3F—Middle, 9:15 am ANALYTICAL PARA:`tETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L <0.02 Ammonia as N mg/L <0.05 Nitrate as N ILg/L <0.CS Tot. Kjeldahl K. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc: REMARKS: * South side of Plum Island. tt Ilk, f I, l i DIRECTOr: . . f 0 0 0 rieCO■EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/5 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN : Hobert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewaten sample, 1R—Bottom, 9:37 am ANALYTICAL PARAMETERS Phosphorous as P mg/L Ammonia as N mg/L Nitrate as h mg/L Tot. Kjeldal,l N. mg/L Nitrogen, total as N mg/L cc: <O.02 <0.05 <0.05 0.6 0.6 ANALYTICAL PARAMETERS REMARKS: * South side of Pluir, Island. I DIRECTOR f�11 i 1 , IC GCO/EST LABORATORIES, INC. ENVIRONMENTAL TESTING 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/6 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, ICY 11944 ATTS: Robert Link SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SASMPLE: Wastewaters sample, IR—Middle, 9:42.am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.04 Ammonia as N mg/L <O.US Nitrate a.s N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc: REI-LA.RKS: ^ South side of Plum Island. DIRCTO:: CO EST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. a N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/7 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link 0 SOURCE OF SAMPLE: Sea Fater off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewate?.sample, 2R—Bottoin, 10:32 am ' ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.04 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl N. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc REI-iARKS: Sout!-k side. of Plum Island. 1 ( DIRECTOR EMTESTLABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 • (516) 422-5777 • FAX (516) 422-5770 LAB NO.C973625/8 09/12/97 Mariculture Technologies, Incorporated 127 Sterling Street, P.O. Box 461 Greenport, NY 11944 ATTN: Robert Link 0 SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Camercn DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewater -,sample. 2R—Middle, 10:37 am ANALYTICAL PARA -METERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.04 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.05 Tot. Kjeldahl S. mg/L 0.5 Nitrogen, total as N mg/L 0.5 cc. RE:Q.RKS: * South side of Plum Island. DIRECTOR CO EST LABORATORIES, INC. ENVIRONMENTAL TESTING • 377 SHEFFIELD AVE. • N. BABYLON, N.Y. 11703 (516) 422-5777 a FAX (516) 422-5770 LAB NO.C973625/1 09/12/97 ji, Mariculture Technologies, Incorporated127 Sterling Street, P.O. Box 461p7 Greenport, NY 11944 ATT: : Robert Link 1.-- SOURCE OF SAMPLE: Sea Water off Plum Island*, Job #CE204 COLLECTED BY: Cameron DATE COL'D:08/27/97 RECEIVED:08/27/97 SAMPLE: Wastewater sample, 1F—Bottom, 8:00 am ANALYTICAL PARAMETERS ANALYTICAL PARAMETERS Phosphorous as P mg/L 0.04 Ammonia as N mg/L <0.05 Nitrate as N mg/L <0.03 Tot. Kjeldahl N. mg/L 0.6 Nitrogen, total as N mg/L 0.6 cc: RE?:ARKS: * South side of Plum.. Island. !' GI°ECTGr. C:OSPER ENVIRONMENTAL SERVICES, INC. e3 CAW -OWN Rollo CSS BOwEM A. NEW YORK t 1710-2003 • s t 0-563-OWS" Fine: s 16-503-2900 E Man.: CosPEwQwowl,awcr.,%rr.Ncr September 19, 1997 CHLOROPHYLL SHAMES FOR MARICULTURE TECH NOLOGEES: POB 461,127 Sterling St. Greenport, NY 11944 Sample Due Site ug Chlorophyll a per liter 6/19/97 2R Top 1.92 6/19/97 1R 1.92 6/19/97 3F Top 2.16 6/19/97 IF Top 2.63 7/2/97 1F Top 5.25 7/2/97 IR Top 4.79 712/97 3F Top 4.02 • 7/2197 2R Top 4.94 7/30/97 1R Top 2.16 7/30/97 1F Top 1.83 7/30/97 2R Top 2.47 7/30/97 3F Top 2.32 8!20/97 IF Top 1.28 8/20197 2R Top 1.10 8/20/97 1R Top 1.01 8/20/97 3F Top 1.47 8/27/97 IR Top 1.74 8127/97 2R Top 1.79 8/27/97 IF Top 1.65 8/27/97 3F Top 1.60 9116/97 IR Top 2.16 9/16197 3F Top 1.69 9/16/97 IF Top 2.63 9/16197 2R Top 2.78 SEP -19-1997 1322 5165632999 P.01 0 OCT— 2-97 THU 3'58 PM EcoTest Labs, Inc. FAX K0. 516 422 5770 P. 1 ECOTEST LABORATORIES. INCORPORATED 377 SHEFR&D AVENUE • NORTH BABYLON, NY 11703 51642244 FAX 516422-5770 0 DATE: 10 /0P%7 FROM: STELLA VOLPE FAX NO.: (516) 422-5770 RE: Ewa . Mort CVA )&Ak TO: NAME: &• C 6)Qjv♦ _. COMPANY. Om*-oLI nw,% FAX NO.: _ IA=22 ' NUMBER OF PAGES (INCLUDING COVERSHEET): .5__ NOTE: IF YOU HAVE ANY QUESTIONS OR HAVE NOT RECEIVED THIS CLEARLY OR COMPLETELY PLEASE CALL ME AT (516) 422-5777. FAXCOVEREW OCT -02-1997 16:07 516 422 5770 92% P.01 OCT- 2-97 THU 3:59 PM EcoTest Labs, Inc. FAX NO. 516 422 5770 P. 2 . NITROGEN, KJELDAHL, TOTAL Method 351.3 (Colorimetric; Titrimetric; Potentiometric) STORET NO. 00625 I. Scope and Application 1.1 This method covers the determination of total Kjeldahl nitrogen in drinking, surface and saline waters, domestic and industrial wastes. The procedure converts nitrogen components of biological origin such as amino acids, proteins and peptides to ammonia, but may not convert the nitrogenous compounds of some industrial wastes such as amines, nitro compounds, hydrazones, oximes, semicarbazones and some refractory tertiary amines. 1.2 Three alternatives are listed for the determination of ammonia after distillation: the titrimetric method which is applicable to concentrations above 1 mg N/liter; the Nesslerization method which is applicable to concentrations below 1 mg NAiter; and the potentiometric method applicable to the range 0.05 to 1400 mg/ 1. 1.3 This method is described for macro and micro glassware systems. 2. Definitions 2.1 Total Kjeldahl nitrogen is defined as the sum of free -ammonia and organic nitrogen compounds which are converted to ammonium sulfate (NH,)2S0„ under the conditions of digestion described below. S2.2 Organic Kjeldahl nitrogen is defined as the difference obtained by subtracting the free - ammonia value (Method 350.2, Nitrogen, Ammonia, this manual) from the total Kjeldahl nitrogen value. This may be determined directly by removal of ammonia before digestion. 3. 3.1 The sample is heated in the presence of cone. sulfuric acid, K=SO, and HgSO, and evaporated until SO3 fumes are obtained and the solution becomes colorless or pale yellow. The residue is cooled, diluted, and is treated and made alkaline with a hydroxide- thiosulfate solution. The ammonia is distilled and determined after distillation by Nesslerization, titration or potentiometry. 4. Sample Handling and Preservation 4.1 Samples may be preserved by addition of 2 ml of cone. HZSO, per liter and stored at 40C. Even when preserved in this manner, conversion of organic nitrogen to ammonia may occur. Preserved samples should be analyzed as soon as possible. 5. Interference 5.1 High nitrate concentrations (IOX or more than the TKN level) result in low TKN values. The reaction between nitrate and ammonia can be prevented by the use of an anion exchange resin (chloride form) to remove the nitrate prior to the TKN analysis. Approved for NPDES Issued 1971 Editorial revision 1974 and 1978 • 351.3-1 OCT -02-1997 1608 516 422 5770 92% P.02 OCT— 2-97 THU 4:00 PM EcoTest Labs, IDC. FAX NO. 516 422 5770 P. 3 • , - NITROGEN, NITRATE-NITTRITE Method 353,2 (Colorimetric, Automated, Cadmium Reduction) STORET NO. Total 00630 I. Scope and Application 1.1 This method pertains to the determination of nitrite singly, or nitrite and nitrate combined in surface and saline waters, and domestic and industrial wastes. The applicable range of this method is 0.05 to 10.0 mg/1 nitrate -nitrite nitrogen. The range may be extended with sample dilution. tmrma-ry of Method 2.1 A filtered sample is passed through a column containing granulated copper -cadmium to reduce nitrate to nitrite. The nitrite (that originally present plus reduced nitrate) is determined by diazotizing with sulfanilamide and coupling with N -(I -naphthyl) - ethylenediamine dihydrochloride to form a highly colored szo dye which is measured colorimetrically. Separate, rather than combined nitratc-nitrite, values are readily obtained by carrying out the procedure first with, and then without, the Cu -Cd reduction step. 3. Sample Handling and Preservation 3.1 Analysis should be made as soon as possible. If analysis can be made within 24 hours. the sample should be preserved by refrigeration at 4'C. When samples must be stored for • more than 24 hours, they should be preserved with sulfuric acid (2 ml conc. H2SO, per liter) and refrigeration. Caution: Samples for reduction column must not be preserved with mercuric chloride. 4. Interferences 4.1 Build up of suspended matter in the reduction column will restrict sample flow. Since nitrate -nitrogen is found in a soluble state, the sample may be pre -filtered. 4.2 Low results might be obtained for samples that contain high concentrations of iron, copper or other metals. EDTA is added to the samples to eliminate this interference. 4.3 Samples that contain large concentrations of oil and grease will coat the surface of the cadmium. This interference is eliminated by pre -extracting the sample with an organic solvent. 5. Apparatus 5.1 Technicon AutoAnalyzer (AAI or AAII) consisting of the following components: 5. 1.1 Sampler. 5.1.2 Manifold (AAI) or analytical cartridge (AAII). 5.1.3 Proportioning Pump 5.1.4 Colorimeter equipped with a 15 mm or 50 mm tubular flow cell and 540 nm fi?te;s. 5.1.5 Recorder. Approved for NPDES and SDWA Issued 1971 Editorial revision 1974 and 1978 • 353.2-1 OCT -02-1997 1609 516 422 5770 92% P.03 OCT- 2-97 THU 4:00 PM Ec,,Test Labs, Inc. FAX NO. 516 422 5770 • NITROGEN, AMMONIA • Method 350.3 (Potentiometric, Ion Selective Electrode) P. 4 STORET NO. Total 00610 Dissolved 00608 1. Scope and Application 1.1 This method is applicable to the measurement of ammonia -nitrogen in drinking, surface and saline waters, domestic and industrial wastes. 1.2 This method covers the range from 0.03 to 1400 mg NH3—N/1. Color and turbidity have no effect on the measurements, thus, distillation may not be necessary. 7 Saim-mary of Method 2.1 The ammonia is determined potentiometrically using an ion selective ammonia electrode and a pH meter having an expanded millivolt scale or a specific ion meter. 2.2 The ammonia electrode uses a hydrophobic gas -permeable membrane to separate the sample solution from an ammonium chloride internal solution. Ammonia in the sample diffuses through the membrane and alters the pH of the internal solution, which is sensed by a pH electrode. The constant level of chloride in the internal solution is sensed by a chloride selective ion electrode which acts as the reference electrode. 3. Sample Handling and Preservation 3.1 Samples may be preserved with 2 ml of conc. H2SO, per liter and stored at 4°C. 4. Interference& 4.1 Volatile amines act as a positive interference. 4.2 Mercury interferes by forming a strong complex with ammonia. Thus the samples cannot be preserved with mercuric chloride. 5. Apparatus 5.1 Electrometer (pH meter) with expanded mV scale or a specific ion meter. 5.2 Ammonia selective electrode, such as Orion Model 95-10 or EIL Model $002-2. 3.3 Magnetic stirrer, thermally insulated, and Teflon -coated stirring bar. 6. Reagents 6.1 Distilled water. Special precautions must be taken to insure that the distilled water is free of ammonia. This is accomplished by passing distilled water through an ion exchange column containing a strongly acidic cation exchange resin mixed with a strongly basic anion exchange resin. 6.2 Sodium hydroxide, ION: Dissolve 400 g of sodium hydroxide in 800 ml of distilled water. Cool and dilute to 1 liter with distilled water (6.1). 6.3 Ammonium chloride, stock solution: 1.0 ml = 1.0 mg NH3--N• Dissolve 3.819 g NH.CI in water and bring to volume in a 1 liter volumetric flask using distilled water (6.1). Issued 1974 Approved for NPDES following preliminary distillation (Niethod 950.2) OCT -02-199? 1609 350.3-1 516 422 5770 92% 0 • OCT- 2-97 THU 4:01 PM EcoTzst Labs, Inc. FAX N0. Sir 422 7770 PHOSPHORUS, ALL FORMS Method 365.3 (Colorimetric, Ascorbic Acid, Two Reagent) P. 5 STORET NO. See Section 4 Scope and Application 1.1 These methods cover the determination of specified forms of phosphorus in drinking, surface and saline waters, domestic and industrial wastes. 1.2. The methods are based on reactions that are specific for the orthophosphate ion. Thus, depending on the prescribed pretreatment of the sample, the various forms may be determined. 1.2.1 Except for in-depth and detailed studies, the most commonly measured forms are phosphorus and dissolved phosphorus, and orthophosphate and dissolved orthophosphate. Hydrolyzable phosphorus is normally found only in sewage -type samples and insoluble forms of phosphorus are determined by calculation. 1.3 The methods are usable in the 0.01 to 1.2 mg P/1 range. 2. Summary of Method .... 2.1 Ammonium molybdate and antimony potassium tartrate react in an acid medium with dilute solutions of phosphorus to form an antimony-phospho-molybdate complex. This complex is reduced to an intensely blue -colored complex by ascorbic acid. The color is proportional to the phosphorus concentration. 2.2 Only orthophosphate forms a blue color in this test. Polyphosphates (and some organic phosphorus compounds) may be converted to the orthophosphate form by sulfuric -acid - hydrolysis. Organic phosphorus compounds may be converted to the orthophosphate form by persulfate digestion. 3. Sample Handling and Preservation 3.1 If benthic deposits are present in the area being sampled, great care should be taken not to include these deposits. 3.2 Sample containers may be of plastic material, such as cubitainers, or of Pyrex glass. 3.3 If the analysis cannot be performed the day of collection, the sample should be preserved by the addition of 2 ml cone. H2SO. per liter and refrigeration at 4'C. 4. Definitions and Storet Numbers 4.1 Total Phosphorus (P) -- all of the phosphorus present in the sample, regardless of form, as measured by the persulfate digestion procedure. (00665) 4.1.1 Total Orthophosphate (P, ortho) -- inorganic phosphorus ((PO4)-j in the sample as measured by the direct colorimetric analysis procedure. (70507) 4.1.2 Total Hydrolyzable Phosphorus (P, hydro) - phosphorus in the sample as measured by the sulfuric acid hydrolysis procedure, and minus pre -determined orthophosphates. This hydrolyzable phosphorus includes polyphosphorus. ((P2OjA, (P,O,o),, etc,] plus some organic phosphorus. (00669) Approved for NPDES Issued 1978 OCT -02-1997 16:10 365.3-1 516 422 5770 95% P. 05