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Metals Data Package 12/2007
Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSLO12 Water Samples Received: 12/5/07 & 12/6/07 METALS DATA PACKAGE DECEMBER 2007 VIA I -AUS, I SC. Environmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 12/5/07 & 12/6/07 SDG NO.: TSLO12 1. NYS DEC SUMMARY FORMS II. SDG NARRATIVES III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY I. NYS DEC SUMMARY FORMS NEW.YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION Snr;• TCI nl,> SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY Anal tical Requirements Customer Sample Code Laboratory Sample Code ME we MW -1D 0713771-001 X 1 X MW -1S_ _ 0713771-002 X MW4D MW -4S _ MW -5D MW -5S _ MW -8D ^� 0713771-003 0713771-004 0713771-005 0713771-006 0713771-007 T X X� X X J X j X X X i X_ f X v MW -8S 0713771-008 X X FB 120507 0713771-009 X X MW -3D 0713817-001 X I X MW -3S 0713817-002 X X MW -6D 0713817-003 _ X I X MW -6S 0713817-00_4 X X MB -BD 0713817-005 w X —�— X M N O CLP, on -C �'(Please indicate year of "��p protocol) NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSL012 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0713771-001 MWAD WATER CA,CD,FE,K;MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-002 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-003 MW -4D WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-004 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Deo -07 12/07 0713771-005 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-006 MW -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-007 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-007DUP IMW-8DD WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-007MS MW-8DS WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-008 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-009 FB 120507 WATER CA,CD,FE;K,MG,MN,NA,PB, 05 -Deo -07 12/07 0713817-001 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 0713817-002 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 -12/07 0713817-003 MW -6D WATER I CA,CD,FE,K,MG,MN,NARB, 06 -Dec -07 12/07 0713817-004 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 0713817-005 MB -BD WATER I CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 TSLO12 A4 Laboratory Samp ID Tclient Sample ID Matrix Tests DateRecd at Lab Date Analyze 0713771-001 MW -11) Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-002 MW -1S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-003 MW4D Groundwater 'SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-004 MW -4S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07. 0713771-005 MW -51) Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-006 MW -5S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-007 MW -8D Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-007DUP MW-8DDUP Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-007MS MW-8DMS Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-008 MW -8S Groundwater SELECT WET CHEMISTRY *" 12/05/07 12/07 07.13771-009 FB 120507 Field Blank SELECT WET CHEMISTRY ** 12/05/07 12/07 0713817-001 MW -3D Groundwater SELECT WET CHEMISTRY ** 12/06/07 12/07 0713817-002 MW -3S Groundwater SELECT WET.CHEMISTRY ** 12/06/07 12/07. 0713817-003 MW -6D Groundwater SELECT WET CHEMISTRY '* 12/06/07 12/07 0713817-004 MW -6S Groundwater SELECT WET CHEMISTRY ** 12/06/07 12/07 '0713817-005 MB -BD Groundwater SELECT WET CHEMISTRY * 12/06/07 12/07 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand; Chloride; Hardness (As CaCO3) ; Nitrate as N; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable ; Sulfate ; Total' Dissolved Solids; Total Organic Carbon ; N h i II. SDG NARRATIVES i N O H SDG NARRATIVE FOR METALS SAMPLE RECEIVED: 12/5/07 & 12/6/07 SDG#: TSLO12 For Sample: MW -1D MW -8S MW -IS FB 120507 MW -41) MW -3D MW -4S MW -3S MW -5D MW -6D MW -5S MW -6S MW -8D MB -BD Fourteen water samples were received by H2M Labs, Inc. on 12/5/07 and 12/6/07 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA 61E Trace ICP Instrument. Sample MW -8D was utilized for QC analysis and reporting. Iron spike analysis did not recover within 75-125%. Since the sample value was greater than four times the spike concentration, post spikes and data qualifiers were not required. No problems were,noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: December 21, 2007 Vient Stancampiano V.fce President SDG NARRATIVE, FOR WET CHEMISTRY SAMPLE RECEIVED: 12/5/07 & 12//6/07 , SDG#: TSL012 For Samples: MW -41) MW -8S MW -4S FB 120507 MW -51) MW -1D MW -5S MW -1S MW -6D MW -31) MW -6S MW -3S MW -81) MW -BD Fourteen water samples were received by H2M Labs, Inc. on 12/5/07 and 12/6/07 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: Alkalinity Anions: Chloride/Sulfate/Bromide Biochemical Oxygen Demand Chemical Oxygen Demand Total Hardness Ammonia EPA 310.1 Nitrate EPA 353.2 EPA 300.0 Phenols EPA 420.1 EPA 405.1-_ Total Dissolved Solids - EPA 160:1 EPA 410.4. Total Kjeldahl Nitrogen EPA 351.2 EPA 130.2 Total Organic Carbon EPA 9060 EPA 350.1 Sample MW -81) was utilized for QC analysis and reporting. Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: January 2, 2008 c* $c Lrthent Stancampiano ice President III. CHAIN OF CUSTODY DOCUMENTATION I NC, 24#g EXTERNAL CHAIN OF CUSTODY 575 Broad Hollow Rd, Melville, NY 11 747-W76 _ Tel: (631) 694-3040 Fax: (631) 420-8436 CLIENT: H2MI SDG NO: PROJECT NAMEINUMBER 14- NOTES: Project Confect S o v 7HoLO (4-1v d 1=1 LL a W� 1 M PART 3 6 0 C b 11/cr Z Phone Number: 007 Q Z z R auT/lU SAMPLERS: (signatureyClient X/ / Zf f} }" �I'% 7�1i5 PIS/Quote# E/U V DELIVERABLES: 6S— 70 D g ANALYSIS REQUESTED TURNAROUND TIME: a I D,+Y.S-,ORGANIC INORG.. _ t- 2 DATE_ TIME MATRI FIELD I.D. > U LAB I.D. N0. REMARKS: .y o Io30 G W- 9 -St I 3 iCoQ MW- SD a 31319 3 1 1 -COP- AIS IM 6P 1136 MW �{ S $ a ► 3 l -0�-f laota' N1 W = 40 1 t I I- 1/330 . InW — 1S 15t•d0 - ! Q - C.�l 1200 g aw .8 Fr'el gig k Relinquished sJDate Time Reeeive by: (Sip-' ro) Date Time LABORATORY USE ONLY )a)si� 4�,�Q Dlsorepancles Between � vrere: 1. Shipped_ or Hand Delhrered, AIN110 Relkqulshed by: (Signature) DafeTime Received by: (Signature) Date Time Sample labels and 2. Ambient or chilled, Temp COC Record? Y or N 3. Ibeeeived in good condition: Y of N 4• Pivpedy per: Y or N Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Explain: 1. Present on outer package: Y or N Relinquished.by: (Signature) Date Time Recehrod by (SigWk") Date Time 2. unbroken on outer package: Y or N 3. COC record present & complete upon sample recelpt: YorN T §ffl� 9CM - ORIGINAL YELLOW COPY - CLIENT PINK COPY -LABORATORY: t Sample Receipt Checklist Client Name PCTSL Date and Time Receive 12/5/2007 3:40:00 PM ` Work Order Numbe 0713771 Received by CAM Checklist completed by 1 �- �� �.� t� Reviewed by Signature bate Initials Date Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes RJ No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable Chain of custody present? Yes No ❑ Chain of custody signed when relinquished and received? Yes No ❑ Chain of custody agrees with sample labels? Yes 0 No ❑ Samples in proper container/bottle? Yes (] No ❑ Sample containers intact? Yes © No ❑ Sufficient sample volume for indicated test? Yes 0 No ❑ tll samples received within holding time? Yes No ❑ Container/Temp Blank temperature in compliance? Yes 0 No ❑ Water - VOA vials have zero headspace? No VOA vials submitted Yes ❑ No ❑ Water -pH acceptable upon receipt? Yes ❑O No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section be — — — — — — — — — — — — — — — — — — — — — — -- — — — — — — — — — — — — — — — — — — — — — - - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - Client contacted Date contacted: Person contacted Contacted by: Regarding Comments: Corrective Action p I CLIENT ID 112M LAB # DATE COLLECTED BOTTLE TYPE N OF BOTTLES TESTS REQUESTED t n gD r2 METALS P 0247 CUSTODY INTERNAL CHAIN OF .P .0249 F2A UA"� INTERNAL CHAIN OF CUSTODY CLMWr:2DELIVERABLES: b�.--MTURN AROUND TUAE: c: n CASE A- MATR'X: pH CHECK Y or )SAL qT9vM7 IS P RECEWMBY: SIGNATURE (1-N lDATE--t--)-. -- WET CHEMISTRY -,,"go ®�I�e u I ; :- 1 v 1:x:.1 _i WET CHEMISTRY -,,"go C . LIENT pco L. SUG STODY OF Cla WET CHEMISTRY P 0110 i .PS9 INN 249-- 575 Broad Hollow Rd, Melville, NY 41747-5076 Tel: (631) 694-3040 Fax: (631) 420-8436 CLIENT: . PROJECT NAME/NUMBER So�TyoL/J' iA1Vd FILL. 8 ?007 Q s SAMPLERS: (signatursyClient m V (r H Phone Number: RABLES: 70-b o g ANALY ORGANIC JQUND TIME:I DAYS x l*s4 REMARKS:.'= ; , TIME MATRIX velm FIELD I.D. w - 3 s Mvd - 3Z M - 6 s W - b q o9.3o P!S/Quote # GNV 1000 1030 1100 M n� by: b by: (Signature) I uaw I . T�Vtgft�F,RP%- ORIGINAL EXTERNAL CHAIN OF CUSTODY H2M SDG NO: NOTES: Project Contact J or4\ o M 1°at0T 3 t- O YELLOW COPY - CLIENT Phone Number: INORG. , g Z U ocJTf/il x l*s4 REMARKS:.'= ; , , � 7 Rs P!S/Quote # GNV O , oOH70701 � YELLOW COPY - CLIENT I ,c INORG. , g Z U LAB I.D. NO. REMARKS:.'= ; , LABORATORY USE ONLY Discrepancies Between were_ 1 ' 3Npped—or Hand Deiivered,,,_Alrbin# ; Sample Labels and 2 Ambient or chilled, Temp COC Record? Y or N 3. Received in good condition: Y or N, Explain: 4. Properly preserved: Y or N Tom was: 1. Present on outer package: Y or N I Unbroken on outer packago: ' Y or N 3. COC record present ,& complete upon Semple receipt: YorN az PINK COPY - LABORATORY I 2M LABS, INC. Sample Receipt Checklist Client Name PCTSL Date and Time Receive 12/6/20071:16:00 PM Work Order Nunibe 07.1381 Received by CAM Checklist completed by SIL Reviewed by Signature Dale Initials Date Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes ❑d No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable W Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable ❑� Chain of custody present? Yes 0 No ❑ Chain of custody signed when relinquished and received? Yes No ❑ Chain of custody agrees with sample labels? Yes ❑ No ❑ Samples in proper containerlbottle? Yes 0 No ❑ Sample containers intact? Yes 0 No ❑ ufficient sample volume for indicated test? Yes No ❑ II samples received within holding time? Yes ❑ No ❑ Container/Temp Blank temperature in compliance? Yes No ❑ Water - VOA vials have zero headspace? No VOA vials submitted Yes ❑ No ❑ Water - pH acceptable upon receipt? Yes O No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section be --------------------------------------------- - — — — — — — — — — — — — — — — — — — — — — — — — — — ---------------- Client -------------Client contacted Date contacted: Person contacted Contacted by: Regarding Comments: Corrective Action U2A t-AUSs INC' INTERNAL CHAIN OF CUSTODY CLlwr:T0;]S _DELIVERABLES: S TURN AROUND TIME SDG 9: CASE 'MATRIX: pH CHECK Y or N REMARKS: RECEIVED BY:t —SIGNA711RE:01 �0 CLIENT ID 112M LAB # DATE COLLECTED BOTTLE TYPE 0 OF BOTTLES[tj TESTS -REQUESTED oro j::) 1-00(o t METALS o2'74 SI ON SIGN SIGN SIGN SIGN SION SIGN SION SION METALS N O IP 0275 E-� WET CHEMISTRY 'SUO 0-13.9 .J I I 7 7 WET CHEMISTRY P 0140.' IV.- ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY ^isLo i- H2M LABS, 1NC. METALS TABLE OF CONTENTS 1. REPORTS II. QC SUMMARY III. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 SOW No.: ILM04.1 EPA Sample No. Lab Sample ID. FB 120507 0713771-009 MB -BD 0713817-005 MW -1D 0713771-001 MW -1S 0713771-002 MW -3D 0713817-001 MW -3S 0713817-002 MW -4D 0713771-003 MW -4S 0713771-004 MW -5D 0713771-005 MW -5S 0713771-006 MW -6D MW -6S 10713817-003 0713817-004 MW- 8DS MW -8S Were ICP interelement corrections applied? Were ICP backqround corrections applied? If yes -were raw data generated before application of background corrections? Comments: Date Reported: 12/17/07 0713771-007DUP 0713771-007MS 0713771-008 Yes/No YES i Yes/No YES I - Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions de 'led above. Release of the data contained in this hardcopy data package and in 'Reacputer-readable data submitted on diskette has been authorized., by• Laboratory Manaqer or the Manaqer's desiqnee, as verified by the follownW'�,I�iate Signature• Name: Vincent Stancampiano Date: Title: Vice President �J4 COVER PAGE - IN ILM04.1 H2M LABS, 1NC. 1. REPORTS FOR METALS H2M LAB:S., 1NC . k j QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers i E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 I i W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. - Duplicate analysis is not within control limits. ' C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL.. M Method Qualifiers P - Analyzed by ICP. M - Analyzed.by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. i C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. N NR- Analyte not Required. �' U.S: EPA -ICLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET ` MW -1D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.:' SDG No.: TSLO12 Matrix (soil/water); WATER Lab Sample IDr 0713771-001 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.80 BI P 7440-70-2 Calcium 20300 P 7439-89-6 Iron 449 P 7439-92-1 Lead 2.5 BI P 7439-95-4 Magnesium 8450 P 7439-96-5 Manganese 157 P 7440-09-7 Potassium 3560 B P 7440-23-5 Sodium 14700 P _ f Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water).: WATER MW -1S SAS No.: SDG No.: TSLO12 Lab Sample ID: 0713771-002 Level (low/med):_ LOW Date Received: 12/5/2007 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U i P 7440-70-2 Calcium 9000 P 7439-89-6 Iron 2430 P 7439-92-1 Lead 1.4 U P 7439-95-4 IMagnesium 5870 P 7439-96-5 IManganese 114, p- 7440-09-7 7440-09 7 Potassium 26101 B I P 7440-23-5 Sodium 380001 ( { P Color Before: COLORLESS Clarity Before: CLEAR Texture:.' Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -4D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713771-003 Level (low/med):_ .. LOW Date Received: :12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS'No. Analyte lConcentration C Q I M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 163000 P 7439-89-6 lIron 396 P 7439-92-1 ILead 1.4 U P 7439-95-4 Magnesium 71500 P 7439-96-5 Manganese 3620 P 7440-09-7 Potassium 78700 P 1440-23-5 Sodium 242000 P Color Before: COLORLESS Clarity Before: CLEAR Texture. Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID Level (low/med): LOW Date Received Solids: 0.0 EPA SAMPLE NO MW -4S SDG No.: TSLO12 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS'No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P j 7440-70-2 Calcium 49800 P 7439-89-6 Iron 930 P 7439-92-1 Lead 2.1 5 I P 7439-95-4 Magnesium 22700 P 7439-96-5 Manganese 11100 P 7440-09-7 Potassium 48600 P 7440-23-5 Sodium 189001 P 12%5/2007 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date ed: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -5D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: .0.713771-005 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration CI Q i M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 102000 P 7439-89-6 Iron 67.6 B P 7439-92-1 ILead 1.4 U P 7439-95=4 Magnesium 48200 P 7439-96-5 Manganese 11400 P 7.440-09-7 .Potassium 117000 P 7440-23-5 Sodium 247000 ( P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -5S Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713771-006 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte iConcentration C 4 i M ( 7440-43-9 Cadmium 0.32 U' P 7440-70-2 Calcium 14000 P 7439-89-6 Iron 68.0 B P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 9.500 P 7439-96-5 Manganese 2890 It P 7440-09-7 Potassium 6290 P 7440-23-5 ISodium 11900--T P I � Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: W Comments: �--i Date Reported: 12/17/07 N O FORM I - IN ILM04:1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -8D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG, No. : TSLO12 Matrix (soil/water): WATER Lab Sample ID:. 0713771-007 Level (low/med):.: LOW Date Received: 12/5/2007 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L . CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 68700 P 7439-89-6 Iron 8910 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 34500 P 7439-96-5 Manganese 1400 P 7440-09-7 Potassium 81300 1 P 7440-23-5 Sodium 80900 P Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: Date Reported: 12/17/07 1. L GLiLt Texture:' Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1• EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER MW -8S SAS No.: SDG No.: TSLO12 Lab Sample ID: 0713771-008 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q ( M 7440-43-9 Cadmium 0.32 U1 P 7440-70-2 Calcium 37700 P 7439-89-6 Iron 24900 P 7439-92-1 Lead 1.41 Uj P 7439-95-4 Magnesium j 15800 P 7439-96-5 Manganese 152 P 7440-09-7 Potassium 54600 P 7440-23-5 Sodium 31500 I P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET FB 120507 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713771-009 Level (low/med):. LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 95.9 B P 7439-89-6 Iron 28.4 B j P 7439-92-1 ILead 1.4 U P 7439-95-4 Magnesium 15.5 U P 7439-96-5 Manganese 0.39 U P 7440-09-7 Potassium 87.5 B, P 7440-23-5 Sodium 62.91 B P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/17/07 Texture: Artifacts: FORM I - IN ILM04.1 .U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -3D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG -No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713817-001 Level (low/me d): LOW Date Received: 12/6/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 39100 P 7439-89-6 Iron 6870 P 7439-92-1 ILead 1.4 U P 7439-95-4 Magnesium 33400 i P 7439=96-5 Manganese 3670 P 7440=09-7 Potassium 127000 P 7440-23-5 Sodium 195000 P I Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After:: COLORLESS Clarity After: CLEAR Artifacts: Comments : Date Reported: 12/17/07 FORM I - IN ILM04.1 d' i N O V" U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -3S Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713817-002 Level (low/med)::. ... LOW Date Received: 12/6/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium , 0.34 B P 7440-70-2 Calcium 43700 ) P 7439-89-6 Iron ( 43500 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 24800 P 7439-96-5 Manganese 15900 P 7440=09-7 Potassium 38900 P 7440-23-5 Sodium 54400 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Retorted: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -6D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID:- 0713817-003 Level (low/med)..:•... LOW Date Received:. 12/6/2007 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration Ci Q I M � 7440-43-9 Cadmium 0.321 UI P 7440-70-2 Calcium 408001 1 P 7439-89-6 Iron 126 P 7439-92-1 ILead 1.4 U P 7439-95-4 IMagnesium 17500 ( P 7439-96-5 IManganese 3930 ! P 7440-09-7 jPotassium 4210 B P 7440-23-5 ISodium 13600_j_ P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med).; LOW Solids: 0.0 MW -6S SAS No.: SDG No.: TSLO12 Lab Sample ID: 0713817-004 Date Received: 12/6/2007 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 17900 P 7439-89-6 Iron 473 P 7439-92-1 Lead 1.41 U F P 7439-95-4 Magnesium 4780 B, P 7439-96-5 Manganese 1930 i P 7440-09-7 lPotassium 8520 P 7440-23-5 Sodium 2900 BI P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 r— N. O r4 U.S. EPA'- CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MB -BB Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG" No.: TSL012 Matrix (soil/water): WATER Lab Sample ID: 0713817-005 Level (low/med): LOW Date Received: 12/6/2007 Solids.: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 {Calcium 43100 P 7439-89-6 Iron 109 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 18600 P 7439-96-5 Manganese 3990 P 7440-09-7 Potassium 4340 B P 7440-23-5 Sodium 13900 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments Date Reported: 12/17/07 FORM I - IN ILM04.1 H2M LABS., INC. II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) I' I True Continuing Calibration Found %R(1) Found %R(1) M Cadmium 2500.0 2445.59 97.8 2500.0 2439.50 97.6 2439.69 97.6 P Calcium X50000.0 49302.48 98.6 50000.01 49151.71 98.3 49150.85 98.3 P Iron 150000.0 49528.93 99.1 50000.01 49435.22 98.9 49433.77 98.9 P Lead 1 500.0 490.67 98.2 500.0 489.61 97.9 488.07 97.6 P Magnesium 50000.0 50967.15 101.9 50000.0 50895.00 101.8 ,50638.78 101.3 P Manganese 2500.0 2486.73 99.5 2500.0 2475.75 99.0 2473.93 99.0 P Potassium 80000.0 85121.15 106.4 80000.0 84926.17 106.2 84877.48 106.1 P Sodium 80000.0 83491.35 104.9 180000.0 83216.32 104.0 82972.82 103.7 P c i (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O f 1 N j O FORM II (Part 1) - IN ILM04.1 CC/i U.S. EPA - CLP 2A INITIAL AND CONTIN ING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte ( Initial Calibration ' True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) I i M Cadmium 2500.0 2449.05 98.0 2435.88 97.4 P Calcium X50000.0 48888.88 97.8 48523.76 97.0 P Iron 50000.0 49426.73 98.9 49180.43 98.4 P Lead 1 500.0 484.56 96.9 481.26• 96.3 P Magnesium 150000.050514.76 101.0 50276.27 100.6 P Manganese 2500.0 2467.19 98.7 2455.74 98.2 P Potassium 80000.0 85923.92 107.4 86077.93 107.6 P Sodium 180000.0 83604.53 104.5 83728.88 104.7 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N O FORM II (Part 1) - IN ILM04.1 C/) U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code:. 1047.8 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration ' True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Cadmium 2500.0 2456.48 98.3 P Calcium 50000.0 48991.41 98.0 P Iron 50000.0 49584.25 99.2 P Lead 500.0 487.04 97.4 P Magnesium 150000.0 50796.92 101.6 P Manganese 2500.0 2471.68 98.9 P Potassium 180000.0 85973.25 107.5 P Sodium 180000.01 83681.09 104.6 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs./High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Analyte True Found %R(1) Continuing Calibration True Found %R(1) Found %R(1) I M Iron 2500.0 2564.19 102.6 2506-:0-1 2571.70 102.9 2501.90 100.1 P Sodium 2500.0 2591.50 103.7 2500.0 2575.16 103.0 j 2589.27 103.6 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (Part 1) - IN ILM04 . 1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS,' INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs/High Purity, Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M' Iron 2500.0 2498.61 99.9 2501.46 100.1 P Sodium 2500.0 2605.88 104.2 2663.39 106.5 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 ' N N ,-r O FORM II (Part 1) - IN ILM04.1 �j U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration. Analyte True Found %R(1) I True Found %R(l) Found %R(1) M Iron2500.0 2533.59 101.3 1 P Sodium 2500.0 2616.23 104.6 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide"85-115 FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AA CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purity Concentration Units: ug/L SDG No.: TSLO12 .Analyte CRDL Standard for AA CRDL Standard Initial True Found %R True Found %R for ICP Final Found %R Cadmium 10.0 10.061 100.61 10.051 100.5 Lead 6.01 4.581 76.3 3 , 571 59.6 Manganese 30.0 30.051 100.21 30.08 100.3 FORM II (Part 2) - IN ILM04.1 U:S. EPA -,CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: ..SDG No.: TSLO12 Preparation Blank Matrix (soil/water): WATER Preparation Blahk'Concentration Units (ug/L or mg/kg): UG/L Analyte Initial Calib. Blank. (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 C Prepa- ration Blank C M Cadmium 0.3 U1 0.3 1 U 1 0.3 U 1 0.3 1 U 0.324 U P Calcium 16.0 U 16.0 1 U 1 16.0 ul 16.0 1 U 15.966 U Iron 29.2 U 24.2 U 24.2 U 24.2 U 24.215 ULead Vp 1.4 U 1.4�U 1.4 U 1.9 U 1.380 U Magnesium 15.5 U 15.5 U 15.5 U 15.5 U 15.480 U P Manganese 0.4 U 0.4 U 0.4 U 0.4 U 0.570 B P Potassium 39.0 B 51.3 B 44.2 B 42.2 B 44.700 B P Sodium 16.3 U 16.3 U 17.1 B 28.2 B 16.339 U P FORM III - IN U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: `SDG No.: TSLO12 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Analyte Initial Calib. Blank (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 Prepa- ration C Blank C M Cadmium 0.3 Ul 0.31 U 11P Calcium 16.0 U 16.1 B P Iron 24.2 U1 24. 2'U1 1P Lead -1.4 B -2.4 B 11P Magnesium 15.5 U1 16.0 B 1P Manganese 0.4 U1 0.4 U P Potassium 49.8 B 39.6 B P Sodium 54.2 B 25.7 B P FORM III - IN U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS; INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 ICP ID Number: TJA6IEA ICS Source: MV Labs/High Purity Concentration Units: ug/L Analyte True Sol. Sol. A AB Initial Found Sol. Sol. A AB oR Final Found Sol. Sol. A AB I i %R Aluminum 500000 500000 499682 497173.8 99.4 503910 1 .50174 4. 01 100.3 Cadmium 1000 939.8 94.0 948.71 94.9 Calcium 500000 500000 509954 508945.3 101.81 506948 508122.01 101.6 Iron 200000 200000 202422 202007.6 101.01 202762 203016.0 101.5 Lead 1000 1 976.6 97.71 976.3 97.6 Magnesium 500000 500000 503112 1 501503.2 100.31 500438 501159.6 100.2 Manganese 500T,485.2 97.01 481.9 96.4 FORM IV - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U:S. EPA _ tLP I 5A SPIKE SAMPLE RECOVERY Contract: SAS No. EPA SAMPLE NO MW-8DS SDG No.:TSL012 Level (low/med):LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit %R Spiked Sample Result (SSR) C Sample Result (SR) C Spike Added (SA) %R Q M Cadmium 75-125 48.2300 0.3235 U 50.00 96.5 P Iron 10282.9200 8907.9700 1000.00 137.5 P Lead 75-125 19.2907 1.3800 U 20.00 96.5 P Manganese 75-125 1946.9700 1404.8000 500.00 108.4 P Comments: FORM V (Part 1) - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES MW -8D ` Contract: SAS No.: SDG No.: TSLO12 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG%L Control Analyte Limit Sample (S) C Duplicate (D) C RPD I Q M Cadmium 0.3235;U 0.3235 U P Calcium 68669.9600 71210.4200 1 3.6 P Iron 8907.9700 9241.1800 3.7 P Lead 1.3800 U 1 1.3800 U P Magnesium 34497.9800 35831.5500 3.8 P Manganese 1404.8000 1453.2900 3.4 P Potassium 81279.0800 83697.77001 2.91 P Sodium 80863.2100 83210.0800 2.91 P FORM VI - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSLO12 Analyte Aqueous (ug/L) I True Found Solid (mg/kg) %R True Found C Limits %R Cadmium 2500.01 2329.041 93.2 Calcium 50000.0 46734.811 93.5 Iron 50000.0 47328.811 94.7 Lead 500.0 474.201 94.8 Magnesium 50000.0 47937.611 95.9 Man anese 2500.0 2370.991 94.8 Potassium 1 80000-01 82393.921 103.0 Sodium 80000.01 81606.00 102.0 FORM VII - IN ILM04.1 I Lab Name: H2M LABS, INC. Lab Code: 10478 Case No U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No:: Concentration Units: ug/L SDG No.: TSL012 EPA Sample 0 ADD 1 ADD 2 ADD 3 ADD Final No. An ABS CON ABS CON ABS CON ABS Conc. r Q FORM VIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA --CLP 9 ICP SERIAL DILUTIONS Contract: SAS No.: Concentration Units: ug/L i MW -8D SDG No.: TSLO12 Level (low/med): LOW Analyte Initial Sample Result (I) C Serial Dilution Result (S) C % Differ - ence Q M Cadmium 0.32 U 1.60 U P Calcium 68669.96 73166.60 6.51 P Iron 8907.97 9335.45 4.811 P Lead 1.401 U 6.90 U I P Magnesium 34497.481 1 1 36593.65 6.1 P Manganese 1404.80 1501.55 6.9 P Potassium 81279.08 74546.25 8.3 P Sodium 80863.21 84665.05F 4.7 P FORM IX - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: 82M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: TJA6IEA Flame AA ID Number: Furnace AA ID Number: Comments: Contract: SAS No.: Date: 9/26/2007 SDG No.: TSL012 Analyte Wave- length Back- (nm) ground CRDL (ug/L) IDL (ug/L) M Cadmium 226.50 5.0 0.3 P Calcium 317.93 5000.0 16.0 P Iron 259.90 100.0. 24.21 P Lead 220.351 3.0 1.4 P Magnesium 279.081 5000.0 15.51 P Manganese 257.61 15.0 0.4 P Potassium 766.49 5000.0 14.3 P Sodium I 588.90 5000.0 16.3 P FORM X - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSLO12 ICP ID Number: TJA61EA Date: 08/22/2007 Analyte Wave- length (nm) Interelement Al Ca Correction Factors for: Fe Mg Co Aluminum 308.22 1 0.0000000 0.0000000 0.0000000 0.0000000 -0.0169820 AntimonV 206.84 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Antimony 206.84 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Arsenic 189.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Barium 493.41 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Boron 249.68 1 0.00000001 0.0000000 -0.0003810 0.00000001 0.0000000 Cadmium 226.50 0.00000001 0.0000000 0.00.01260 0.00000001 0.0000000 Calcium 317.93 1 0.0000000 , 0.0000000 0.0000000 0.00000.00 Chromium 267.62 0.00000001 0.0000000 0.0000000 10.00000001 0.00000001 0.0000000 1 Cobalt 228.62 0.0000000 0.0000000 0.0000000 0.00000001 0.0000000 Copper 324.75 0.000.0000 0.0000000 0.0000000 0.0000000 -0.0005274 Iron 259.99 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 271.44 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Lead 220.35 -0.28988901 0.0000000 0.0449130 0.0000000 0.3383700 Lead 220.35 0.59129701 0.00000001 0.1104100 0.0000000 0.0000000 Magnesium 279.08 0.000000or 0.0000000 0.0000000 0.0000000 0..0000000 Manganese 257.61 -0.0000196 0.0000000 0.0000000 0.0000000 -0.0005878 Mol bdenuml 202.03 0.0000000; 0.00000001 0.0000000 0.00000001 0.0000000 Nickel 231.60 0.00000001 0.0000000) 0.0000000 0.0000000 0.0000000 1 !Potassium 1 766.49 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 'Selenium 196.03 0.00000001 0.00000001_ -0.02521001 0.00000001 0.3501500 Selenium !Silicon 196.031 1 288.161 0.00000001 0.0000000 0.0000000 0.0000000 0-00000001 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 1 Silver 328.071 0.0000000; 0.0000000 0.00000001 0.0000000 0.0000000 Sodium 330.23 1 0.00000001 0.0000000 0.000000010.0000000 0.0000000 Sodium 589.00-1 0.0000000! 0.0000000 0.00000001 0.00000001 0.0000000 1 (Strontium 407.77 1 0.00000001 0.00000001 0.0000000 0.0000000 0.0000000 .Thallium 190.86 I 0.00000001 0.0000000 -0.3087590 0.000000'0;-0.9867100 Comments: FORM XI (PART 1) - IN ILM04.1 M N O U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: ICP ID Number: TJA6IEA Contract: NRAS No.: SDG No.: TSLO12 Date: 08/22/2007 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Tin 189.99 0.0000000 0.0000000 -0.0002025 0.00000001 0.0000000 Titanium 334.94 0.0000000 0.00000001 0.0000000 0.00000001 0.0000000 Vanadium 292.4'0 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Zinc 213.86F 0.0000000 0.00000001 0.0001536 0.00000001 0.0000000 Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSLO12 ICP ID Number: TJA6IEA Date: 08/22/2007 Analyte Wave- T length (nm) Interelement Cr Cu Correction Factors for: Mn Ni v Aluminum 30 , 8.221 0.00000ool 0.00000001 0.00000001 0.0000000 0.0141540 Antimony 206.84 7.18351801 0.00000001 0.0000000 0.0000000 0.0000000 Antimony 206.84 9.3517600 0.00000001 0.0000000 -1.3216900 -5.3461690 Arsenic 189.04 0.1835660 0.00000001 0.0000000 0.0000000 0.0000000 Barium 493.41 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0001975 Boron 249.68 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 0.00000001- 0.0000000 0.0000000 -0.0001533 0.0000000 Calcium 317.93 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Chromium 267.62 0.0000000 0.0000000 0.0000000 0.0002458 0.0003072 Cobalt 228.62 0.00000001 0.00000001 0.0000000 0.0000000 0.0000000 Copper 324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 259.94 0.0000000 0.0000000 0.0000000 0.0000000 0.00000.00 Iron Lead 271.441 1 220.351 1 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.11464301-0.1896630 0.0000000 Lead 220.35 0.0000000 o.o0000001 0.0000000 0.41006901 0.0000000 Magnesium Mancranese 279.08 257.61 0.00000001 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 0.00000001 0.00000001 0.0000000 0.0000000 Molybdenum 202.03 0.0000000 0.0000000 0.0000000 0.00000001 0.0000000 Nickel Potassium 1 231.60 766.491 0.0000000, 0.0000000 0.0000000, 0.0000000 0.0000000 0.0000000 0.0000000 0.00000001 0.0000000 0.0000000 'Selenium 196.03' 0.0000000 0.0000000 0.4041530; 0.0000000 0.1927530 Selenium !Silicon j 196.031 1 288.161 0.00000001 0.00000001 0.00000001 0.0000000 0.0000000 0.00000001 0.0000000 0.00000001 0.0000000 0.0000000 Silver 328.07 1 0.00000001 0.0000000 0.00000001 0.0000000 0.0000000 1 Sodium 330.23-T 0.00000001 0.0000000 0.0000C)OOl 0.00000001 0.000 0 Sodium 589.00. 0.0000000 0.00000001 0.00000001 0.00000001 0.0000000 Strontium 407.77 0.0000000; 0.000OOOOf 0.0000000 0.0000000 0.0000000 Thallium 190.861 1 0 0000000; 0.00000001 -0.7197950 0.0000000 -1.1386100 Comments: FORM XI (PART 2) - IN ILM04.1 00 M N O E--+ U.S. EPA' - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL012 ICP ID Number: TJA6IEA Date: 08/22/2007 Analyte Wave- length ' (nm) Interelement Cr Cu Correction Mn Factors for: Ni V Tin 189.99 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Titanium 334.94 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Vanadium 292.40 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Zinc 213.86 0.00000001 0.00095261 0.0017640 0.0045467 0.0000000 Comments: FORM XI (PART 2) -.IN ILM04.1 U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 ICP ID Number: TJA6IEA Date: 12/08/2007 Comments: Analyte Integ. Time (Sec.) Concentration (ug./L) M Cadmium 15.00 20000P Calcium 15.00 1000000 P Iron 15.00 250000P Lead 15.00 50000P magnesium 15.00 1000000P Manganese 15.00 20000P Potassium 15.00 300000P Sodium 15.001 750000P FORM XII - IN ILM04.1 O 7t N O Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL012 EPA Sample No. Preparation Weight Date (gram) Volume (mL) FB 120507 12/10/2007 50 LCSW 12/10/2007 50 MB -BD 12/10/2007 50 MW -1D 12/10/2007 50 Mw -is 12/10/2007 50 MW -3D 12/10/2007 50 MW -3S 12/10/2007 50 MW -4D 12/10/2007 50 MW -4S 12/10/2007 50 MW -5D 12/10/2007 50 MW -5S 12/10/2007 50 MW -6D 12/10/2007 50 Mw -6S 12/10/2007 50 MW -8D 12/10/2007 50 MW-8DD 12/10/2007 50 MW-8Ds 12/10/2007 50 MW -8s 12/10/2007 50 PBW 12/10/2007 50 f FORM XIII - IN ILM04.1 N O r4 C/) I Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 12/14/2007 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date:" SDG No.: TSLO12 .12/14/2007 EPA Sample No. D/F Time % R A S A L B S BIB C C C AI E D A R Analytes C CIF P MI M H 0 UjE B G{N G I I N K S A i I E GIA N T V Z C L N N SO 1.00 0843 X j X x I j x I x I X X1 I I X I I x j S 1.00 0851 1 11 S 1.0.0 0856 j X Ix I ix X S 1.00 0901 jX j S 1.00 0907 X X S' 1.00 0914 I X T X S 1.00 0919 X X ICv 1.00 0923 X X1 I X XX X Ix X ICv 1.00 0930 X X ICB 1.00 0938 r X X, i X X X X X X CRI 1.00 0945 X X X ICSA 1..00 0952 X X XI I Ix X �X X ICSAB 1.00 1000 X, j X X j X X I X X ccv 1.00 10,07 X X X XIX X j X1 X ccv 1.00 1014 X1 I X III CCs 1.00 1022 X X X X X X X X zzzzzz j 1.00 1029 j zzzzzz 1.00 1036 zzzzzz 1.00 1044 jzzzzZ 1. -00 -Ti 0 5 1 zZZZZz 1.00 1058 IZZZZzz 1.00 1106 4Ccv 1.00 1113 j j I I X Xj j XX x X X ccv 1.00 1120 i- - I (�j� i X j X j CCB 1.0.0 1128 j I X Xj XjXX X X X j Psw 1.00 j 1135 j i X X X i IX XjX X jX I i LCSW 1.00 1142 j j I X XI XjXIXjX X Xj-�-�-�j Mw -1D 1.00 11150 j ' I X•Xj XjX X X X jXI , ► , MW-ls 1.00 1157 j j �j_ XjXj I I IXjXjX X I jXj j X1 MW -4D I MW -4S j 1.00 1.00 j 1205 1220 j j j i j I j jXXj I jXlXj I IXjXjX XI IXTX x X IXI j ix I 1 X I iX j MW -5D IMW-5S I IMW-8D !Mw-8DD j 1.00 1.00 1.00 1.00 1228j_XjXI_i 1235-j 1242 1250 I j i i i iX Xi j jX XI ! jX Xi I IXIX XjX ( iXi I jX;X XX Xi I j X XX X� ;X' i j XIX x I jXj j �X fXj jXi ^l -j XI Yum XIV - IN N tet+ �N IC) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 12/14/2007. U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSLO12 12/14/2007 EPA Sample No. D/F Time I o R A S L�B A B B C S A�E D C C A R Analytes C C F P M M 0 U E B G N H N K S G I I E A N T V Z C G A L N N CCV 1.00 1 1257 j X x! X X I X I X 1XI I X CCV 1.00 1304 j XI I X CCB 1.00 1312 j X X X X X X X I X MW-8DS 1.00 1321 X X1 I X X .x X X I X MW-8DL 5.00 1328 X X I X X X X X I X MW -8s 1.00 1335 X X Ix X X X1 X X1 I FB 120507 1.00 1343 j X j X 1x X X X X X MW -3D 1.00 1350 I X X X XIX X X X MW -3S 1.00 1358 X X X X X X X X MW -6D 1.00 1405 j X X X X X X X X MW -6S 1.00 1 1412 1 IX X' I ix X X X Ix X MB -BD 1.00 1420 1 1 IX X1 I I X X X X X X zzzzzz 1.00 1427 CCV 1.00 1434 X X I X X X X I Ix X CCv 1.00 1442 XX CCB 1.00 1449 X X X X X X X X CRI 1.00 1456 i X X1 X j ICSA 1.00 1504 j X -FF X X i . X XIX X ICSAB 1.00 1511 ! x! I X x i X X X X _ CCv 1.00 1519 j I ix Xi X X XIX 1X� jX CCV 1.00 1526' iX 1 -x —x I X Ccs i 1.00 1 1533 i i I i �X X. jx,x ,x XI FORM XIV - IN ILM04.1 H2M LABS, INC. Ill. RAW DATA FOR METALS A. ICP DATA 7 N CLIENT 15�- 012 '1 R � DATE OG -C. 14,2= TASK: C IPI RESULT FILE: G\LMO1 ANALYST4��-� 27 , '�-t fl ��- go 1 3 PLC'S , , , 28 3 0 i000 1 4 ' C-Q.Z ; 29' A'C'V 1 t ' 6 , 1 � c 32 �0-►�311� `►o ��^,.'-�So rns 7 Gc.! 1 � � + 'SO g 33 r+d'i O Sfl ' ' , 9 ` GC- , , ii ! 10 ;�71'�1►2�1 005A , Z Z� Z �y SSOL 35 i roto mono -1 i , ' -cceA, 36,0`113$il-0010 11t , . , 12, 'C9p� i 37 i �a3Za i %y1W-3$ , , , 13 ;O'11y1i�-cGo1A i , 38 , Ck30 , 14 ; -Oo2A , ' , 15, Cc 16; V2 41 ;0-t 13x 3 �1-6 - CFP PA=M 171 t C�LZ ; L12! CcV �{ , 43: 44: C—Czc( 2o,L 21'0`I1�11-co S t-ALu-1O ; 46; -5A 22 23 -L)03D; (mow -HO 48; ,4; -0040, moo -LA 49. CC�i.� ; ' 25 ' r'Aw -gt� so C/) Standardization Rpt. I" -god: CLP1 Standard: StdBLANK ] Time: 12/14/07 08:43:42 .0013 Elem Ag Al As1890 Avge -.00459 .0097 -.00316 SDev .00006 .0003 .00208 %RSD 1.2571 2.724 66.013 #1 -.00465 .0094 -.00086 #2 -.00459 .0099 -.00493 #3 -.00454 .0097 -.00367 Elem Cd Co Cr Avge .0013 .0001 .0011 SDev .0006 .0002 .0001 %RSD 45.51 192.3 12.40 #1 .0008 -.0001 .0012 #2 .0012 .0003 .0011 #3 .0019 .0001 .0010 Elem Mg Mn Mo Avge .0011 .0018 .0003 SDev .0002 .0002 .0000 %RSD 16.18 12.71 6.804 #1 .0011 .0017 .0003 .0013 .0016 .0003 .0010 .0020 .0003 Elem 2203/2 2068/1 2068/2 Avge .00065 -.00378 .00102 SDev .00109 .00121 .00226 %RSD 166.71 32.024 221.82 #1 .00188 -.00300 .00135 #2 .00026 -.00316 .00309 #3 -.00019 -.00517 -.00139 Elem Sr Ti T11908 Avge .0002 .0007 -.00691 SDev .0001 .0001 .00098 %RSD 52.75 8.248 14.140 #1 .0002 .0006 -.00701 #2 .0001 .0007 -.00783 #3 .0003 .0007 -.00589 12/14/07 08:50:57 AM B .0013 .0001 7.760 .0012 .0014 .0012 Cu .0062 .0001 .8809 .0061 .0062 .0062 Na -.0309 .0018 5.920 -.0324 -.0315 -.0289 1960/1 -.01564 .00279 17.852 -.01763 -.01683 -.01245 v .0001 .0001 77.91 .0000 .0001 .0002 Ba .0008 .0001 10.19 .0007 .0008 .0007 Fe .0001 .0000 50.20 .0000 .0001 .0001 Na .5682 .0042 .7432 .5634 .5712 .5700 1960/2 .00438 .00149 34.057 .00533 .00516 .00266 Zn .0037 .0001 1.243 .0037 .0037 .0036 Be -.0005 .0000 4.317 -.0005 -.0005 -.0005 Fe .0388 .0204 52.54 .0622 .0286 .0255 Ni .0010 .0002 18.63 .0012 .0009 .0010 Si .0531 .0005 1.024 .0525 .0535 .0533 page 1 Ca .0055 .0001 .9848 .0055 .0055 .0056 K .0113 .0007 5.803 .0108 .0111 .0120 2203/1 .03555 .00565 15.895 .03380 .03099 .04187 Sn .0079 .0026 33.42 .0071 .0108 .0058 N O G7 N Standardization Rpt. 12/14/07 08:56:45 AM page 1 I Lod: CLP1 Standard: StdAGSDH I Time: 12/14/07 08:51:04 Elem Ag 2068/1 2068/2 Avge .85019 3.2235 1.9989 SDev .00430 .0191 .0238 %RSD 50619 .59346 1.1922 #1 .85197 3.2182 1.9991 #2 .84529 3.2076 1.9750 #3 .85333 3.2447 2.0226 rl- �t N O DO N Standardization Rpt. 12/14/07 09:01:45 AM page 1 T`-`'-Eod: CLP1 Standard: StdICSH ] Time: 12/14/07 08:56:51 Elem Al Ca Fe Avge 35.25 55.65 .6743 SDev .03 .03 .0006 %RSD .0903 .0602 .0895 #1 35.28 55.68 .6749 #2 35.22 55.63 .6737 #3 35.26 55.62 .6743 Mg 81.33 .09 .1080 81.43 81.27 81.28 1 00 N O C/� Standardization Rpt. 12/14/07 09:07:32 AM V `'-od: CLP1 Standard: StdFURNH R rime: 12/14/07 09:01:51 Elem As1890 2203/1 2203/2 1960/1 1960/2 T11908 Avge 1.3679 4.1154 1.7697 .99762 .71496 1.0699 SDev .0066 .0209 .0020 .00188 .00150 .0033 6RSD .48168 .50795 .11169 .18840 .21029 .30594 #1 1.3751 4.1392 1.7683 .99903 .71563 1.0727 #2 1.3622 4.0999 1.7688 •.99549 .71324 1.0707 #3 1.3664 4.1073 1.7719 .99834 .71601 1.0663 page 1 Standardization Rpt. 12/14/07 09:14:06 AM page 1 M- " od: CLP1 Standard: StdMULTH F Time: 12/14/07 09:07:38 Elem B Ba Be Cd Co Cr Cu Avge 1.888 5.933 7.967 62.41 2.167 2.732 1.665 SDev .004 .013 .011 - .05 .003 .003 .004 %RSD .2206 .2171 .1412 .0849 .1321 .0954 .2200 #1 1.884 5.923 7.955 62.35 2.164 2.729 1.662 #2 1.890 5.947 7.969 62.41 2.168 2.733 1.669 #3 1.891 5.928 7.977 62.46 2.170 2.734 1.665 Elem Mn Mo Ni Si Sn Sr Ti Avge 18.87. 2.278 2.095 1.533 10.21 11.16 2.319 SDev .02 .005 .002 .004 .02 .02 .003 %RSD .1222 .1988 .0898 .2818 .1502 .1860 .1322 #1 18.84 2.273 2.094 1.528 10.19 11.14 2.316 #2 18.88 2.280 2.094 1.534 10.21 11.18 2.322 #3 18.89 2.281 2.097 1.536 10.22 11.15 2.319 Elem v Zn Avge 1.321 5.263 SDev .002 .005 %RSD .1338 .1002 #1 1.319 5.257 1.323 5.265 1.322 5.268 Standardization Rpt. P"-"-od: CLP1 Standard: StdFENAL P Time: 12/14/07 09:14:12 Elem Fe Na Avge 47.58 39.51 SDev 1.50 .95 %RSD 3.144 2.410 #1 45.86 38.41 #2 48.52 40.03 #3 48.37 40.10 12/14/07 09:19:06 AM page 1 N O h Standardization Rpt. A" — od: CLP1 Standard: StdNAKH F Time: 12/14/07 09:19:13 Elem K Na Avge 7.843 2.159 SDev .004 .003 %RSD .0548 .12.04 #1 7.838 2.157 #2 7.843 2.162 #3 7.847 2.158 12/14/07 09:23:20 AM page 1 Standardization Report 12/14/07 09:23:20 AM page 1 P"-`'-.od: CLP1 Slope = Conc (SIR) /IR L.LCutent Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGSBH StdBLANK 2339.76 10.7478 12/14/07 09:19:13 Al 308.215 StdICSH StdBLANK 14.1876 -.136917 12/14/07 09:19:13 As1890 189.042 StdFURNH StdBLANK 729.381 2.30210 12/14/07 09:19:13 B 249.678 StdMULTH StdBLANK 2.64948 -.003317 12/14/07 09:19:13 Ba 493.409 StdMULTH StdBLANK .842906 -.000633 12/14/07 09:19:13 Be 313.042 StdMULTH StdBLANK .627663 .000322 12/14/07 09:19:13 Ca 317.933 StdICSH StdBLANK 1.03532 -.000462 12/14/07 09:19:13 Cd 226.502 StdMULTH StdBLANK .080107 -.000104 12/14/07 09:19:13 Co 228.616 StdMULTH StdBLANK 2.30703 -.000231 12/14/07 09:19:13 Cr 267.716 StdMULTH StdBLANK 1.83211 -.001995 12/14/07 09:19:13 Cu 324.754 StdMULTH StdBLANK 3.01183 -.018585 12/14/07 09:19:13 Fe 271.441 StdICSH StdBLANK .894239 -.000012 12/14/07 09:19:13 Fe 259.940 StdFENAL StdBLANK .105167 -.004076 12/14/07 09:19:13 K 766.491 StdNAKH StdBLANK 1.02093 -.004780 12/14/07 09:19:13 Mg 279.079 StdICSH StdBLANK .770138 -.000274 12/14/07 09:19:13 Mn 257.610 StdMULTH StdBLANK .264828 -.000471 12/14/07 09:19:13 Mo 202.030 StdMULTH StdBLANK 2.20187 -.000717 12/14/07 09:19:13 Na 330.232 StdNAKH StdBLANK .920741 -.000112 12/14/07 09:19:13 Na 588.995 StdFENAL StdBLANK .128387 -.072950 12/14/07 09:19:13 Ni 231.604 StdMULTH StdBLANK 2.38795 -.002450 12/14/07 09:19:13 2203/1 220.351 StdFURNH StdBLANK 245.104 -8.71400 12/14/07 09:19:13 2203/2 220.352 StdFURNH StdBLANK 565.284 -.367751 12/14/07 09:19:13 2068/1 206.831 StdAGSBH StdBLANK 619.713 2.34183 12/14/07 09:19:13 2068/2 206.832 StdAGSBH StdBLANK 1001.06 -1.01800 12/14/07 09:19:13 : /1 196.021 StdFURNH StdBLANK 986.918 15.4307 12/14/07 09:19:13 /2 196.022 StdFURNH StdBLANK 1407.30 -6.16695 12/14/07 09:19:13 Si 288.158 StdMULTH StdBLANK 3.34979 -.177858 12/14/07 09:19:13 Sn 189.989 StdMULTH StdBLANK .490182 -.003867 12/14/07 09:19:13 Sr 421.552 StdMULTH StdBLANK .448209 -.000084 12/14/07 09:19:13 Ti 334.941 StdMULTH StdBLANK 2.15690 -.001485 12/14/07 09:19:13 T11908 190.864 StdFURNH StdBLANK 928.676 6.41757 12/14/07 09:19:13 v 292.402 StdMULTH StdBLANK 3.78504 -.000379 12/14/07 09:19:13 Zn 213.856 StdMULTH StdBLANK .957551 -.003524 12/14/07 09:19:13 Pb2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Sb2068 206.838 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Se1960 196.026 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Standardization Readback Report 12/14/07 09:23:20 AM N od: CLP1 Element Wavelength Standard Ag 328.068 StdBLANK StdAGSBH Element Wavelength Standard Al 308.215 StdBLANK StdICSH Element Wavelength Standard As1890 189.042 StdBLANK StdFURNH Element Wavelength Standard B 249.678 StdBLANK StdMULTH Element Wavelength Standard Ba 493.409 StdBLANK StdMULTH nent Wavelength Standard 313.042 StdBLANK StdMULTH Element Wavelength Standard Ca 317.933 StdBLANK StdICSH Element Wavelength Standard Cd 226.502 StdBLANK StdMULTH Element_ Wavelength Standard Cc 228.616 StdBLANK StdMULTH Element Wavelength Standard Cr 267.716 StdBLANK StdMULTH Element Wavelength Standard r" 324.754 StdBLANK ` StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 500.000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .005266 57.6118 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration .000000 2000.00 Measured Concentration .000000 500.000 Measured Concentration .000000 1000.00 Measured Concentration -.000000 5.00000 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00099 Measured Signal .005532 55.6467 Measured Concentration -.000000 4.99917 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00276 Measured Concentration -.000000 4.99736 page 1 Residual . Concentration -.000000 .000122 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.000988 Residual Signal -.000267 1.96516 Residual Concentration .000000 .000830 Residual Concentration -.000000 .000000 Residual Concentration -.000000 7t -.002765 Residual N Concentration O .000000 r� .002635 Standardization Readback Report 12/14/07 09:23:20 AM ] ient Wavelength Standard �-e 271.441 StdBLANK StdICSH Element Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard K 766.491 StdBLANK StdNAKH Element Wavelength Standard Mg 279.079 StdBLANK StdICSH Element Wavelength Standard Mn 257.610 StdBLANK StdMULTH Element Wavelength Standard 202.030 StdBLANK StdMULTH Element Wavelength Standard Na 330.232 StdBLANK StdNAKH Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTH Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNH Element Wavelength Standard 2203/2 220.352 StdBLANK StdFURNH Known Signal . .00005'5 - .602976 Known Concentration .000000 5.00000 Known Signal .006759 8.00205 Known Signal .000584 62.6316 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal -.028601 1.98779 Known Concentration ..000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known_ Concentration .000000 1000.00 Measured Signal .000075 .674304 Measured Concentration .000000 5.00000 Measured Signal .011302 7.84267 Measured Signal .001114 81.3256 Measured Concentration .000000 4.99710 Measured Concentration -.000000 5.01559 Measured Signal -.030942 2.15902 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration .000000 1000.00 Measured Concentration -.000000 1000.00 page 2 Residual Signal -.000020 -.071328 Residual Concentration -.000000 .000000 Residual Signal -.004543 .159381 Residual Signal -.000530 -18.6940 Residual Concentration -.000000 002900 Residual Concentration .000000 -.015590 Residual Signal .002341 -.171232 Residual Concentration -.000000 -.000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 tt� Residual Concentration N .000000 O ..000000 h Standardization Readback Report 12/14/07 09:23:20 AM F ent Wavelength Standard 2000/1 206.831 StdBLANK StdAGSBH Element Wavelength Standard 2068/2 206.832 StdBLANK StdAGSBH Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNH Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNH Element Wavelength Standard Si 288.158 StdBLANK StdMULTH Element Wavelength Standard E' 189.989 StdBLANK StdMULTH Element Wavelength Standard Sr 421.552 StdBLANK StdMULTH Element Wavelength Standard Ti 334.941 StdBLANK StdMULTH Element Wavelength Standard T11908 190.864 StdBLANK StdFURNH Element Wavelength Standard V 292.402 StdBLANK StdMULTH Element Wavelength Standard Zn 213.856 StdBLANK StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000' 2000.00 Known Concentration .000000 1000.00 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration .000000 2000.00 Measured Concentration -.000000 1000.00 Measured Concentration .000000 1000.00 Measured Concentration -.000000 4.95659 Measured Concentration -.000000 5.00000 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration .000000 1000.00 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.03617 page 3 Residual Concentration .000000 .000000 j Residual ti Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual i Concentration -.000000 .000000 Residual Concentration .000000 .043410 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 i Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 �p Residual . Concentration N i .000000 C) j -.036167 N Standardization Readback Report 12/14/07 09:23:20 AM I ent Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard Sb2068 206.838 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .00.0000 .000000 .000000 .000000, page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Analysis Report 12/14/07 09:30:42 AM page 1 Dft-"-.od: CLP1 Sample Name: ICV Operator: CO F Time: 12/14/07 09:23:26 i C- -aent : Mode: CONC Corr. Factor: 1 f Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1039.7 49.49 502.61 2.508 2.555 2.511 49.30 SDev 4.5 .20 4.32 .008 .009 .010 .19 %RSD .43552 .4119 .85939 .3146 .3614 .3870 .3832 } #1 1038.9 49.41 498.57 2.505 2.553 2.508 49.25 I #2 1035.7 49.34 502.11 2.503 2.548 2.503 49.14 #3 1044.6 49.72 507.16 2.517 2.565 2.522 49.51 i Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 I Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.446 2.477 2.485 2.592 49.53 85.12 50.97 SDev .008 .010 .010 .011 .19 .35 .18 j %RSD .3318 .4126 .4048 .4249 .3839 .4105 .3626 i #1 2.446 2.473 2.482 2.587 49.49 85.00 50.91 #2 2.437 2.469 2.477 2.584 49.36 84.85 50.82 2.454 2.488 2.496 2.605 49.73 85.51 51.17 � Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.487 2.457 83.49 2.467 494.97 488.82 986.26 SDev .009 .010 .34 .009 2.43 .56 4.30 %RSD .3812 .4111 .4070 .3815 .49130 .11464 .43566 I #1 2.484 2.450 83.44 2.464 494.34 489.10 983.40 i I #2 2.479 2.452 83.18 2.459 492.92 488.18 984.18 #3 2.497 2.468 83.85 2.477 497.66 489.19 991.20 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm 00 Avge 991.13 502.29 500.17 2.324 2.444 2.'498 2.453 SDev 13.35 3.50 3.02 .010 .011 .010 .010 %RSD 1.3474 .69627 .60345 .4481 .4591 .3914 .3992 N O' #1 993.69 502.90 -498.75 2.319 2.439 2.495 2.450 976.68 498.52 498.12 2.317 2.436 2.490 2.445 1003.0 505.44 503.63 2.336 2.457 2.509 2.464 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 09:30:42 AM 4h --.v - Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb. ppb ppb Avge 500.84 2.491 2.568 490!87 989.51 500.87 SDev 3.29 .011 .011 1.13 9.97 3.06 %RSD .65639 .4381 .4340 .22955 1.0080 .61073 #1 497.75 2.489 2.565 490.84 990.26 500.13 #2 504.29 2.481 2.558 489.76 979.18 498.25 #3 500.49 2.503 2.580 492.01 999.08 504.23 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 12/14/07 09:38:03 AM page 1 m- -hod: CLP1 Sample Name: ICVL Operator: CO Time: 12/14/07 09:30:48 -.......lent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm. Avge .64122 .0163 2.3679 .0043 .0009 .0007 .0194 SDev .45250 .0042 .9932 .0012 .0002 .0002 .0034 %RSD 70.568 25.71 41.945 28.00 20.53 24.55 17.76 #1 1.0828 .0206 2.1086 .0056 .0011 .0009 .0233 #2 .66241 .0160 1.5300 .0042 .0007 .0006 .0167 #3 .17851 .0123 3.4650 .0032 .0008 .0007 .0182 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0007 .0004 -.0003 .0010 2.564 .0714 .0106 SDev .0002 .0002 .0002 .0004 .007 .0200 .0054 %RSD 28.89 44.60 70.00 46.47 .2571 27.98 50.97 #1 .0009 .0006 -.0001 .0011 2.572 .0754 .0128 #2 .0005 .0002 -.0005 .0005 2.560 .0498 .0045 .0006 .0005 -.0003 .0013 2.561 .0891 .0146 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0044 2.592 -.0000 -2.2431 -.03002 5.0554 SDev .0002 .0017 .012 .0005 4.5891 2.04033 2.6345 %RSD 39.29 37.43 .4705 1444. 204.59 6796.6 52.112 #1 .0007 .0063 2.605 .0002 -3.4766 2.1702 6.7406 #2 .0003 .0039 2.581 -.0006 -6.0895 -.40058 6.4061 #3 .0007 .0031 2.589 .0004 2.8367 -1.8597 2.0195 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 4.8673 4.4520 -1.8798 -.0033 -.0013 .0008 .0008 SDev 3.2965, 1.0350 2.7762 .0021 .0010 .0002 .0002 %RSD 67.726 23.2.47 147.69 63.59 78.23 30.88 22.10 #1 6.5703 3.6012 -1.4737 -.0015 -.0009 .0010 .0010 1.0677 4.1507 -4.8367 =.0027 -.0005 .0005 .0006 6.9639 5.6043 .67101 -.0056 -.0024 .0008 .0007 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 09:38:03 AM page 2 Ih Zn ----I Sb2068 Elem T11908 Units ppb Avge 89120 SDev .79658 %RSD 89.383 #1 .86886 #2 .1060.2 #3 1.6987 Errors NOCHECK High 38.953 Low .0011 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0010 .0029 -.76691 4.9300 .22876 .0002 .0001 1.35530 1.9204 2.0789 21.50 4.561 176.72 38.953 908.75 .0011 .0030 .28991 6.6271 .21631 .0012 .0027 -2.2949 2.8454 -1.8438 .0008 .0029 -..29571 5.3175 2.3138 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK N O Analysis Report 12/14/07 09:45:23 AM page 1 m -'-hod: CLP1 Sample Name: ICB Operator: CO Time: 12/14/07 09:38:08 -...nent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .14760 .0031 2.9072 .0012 .0002 .0002 .0022 SDev .47259 .0019 1.0756 .0008 .0001 .0000 .0008 %RSD 320.18 62.34 36.999 68.16 31.00 26.51 35.03 #1 -.26303 .0025 3.4556 .0015 .0002 .0002 .0031 #2 .66416 .0052 3.5982 .0019 .0002 .0001 .0017 #3 .04167 .0015 1.6679 .0003 .0001 .0001 .0017 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0001 -.0008 .0002 .0016 .0390 .0004 SDev .0000 .0003 .0003 .0002 .0008 .0080 .0006 %RSD 24.08 383.9 33.26 104.9 51.79 20.52 162.3 #1 .0002 -.0002 -.0009 .0004 .0024 .0311 .0003 #2 .0001 -.0003 -.0005 .0002 .0016 .0471 .0011 .0001 .0003 -.0011 -.0000 .0008 .0387 -.0002 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -..0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0000 .0014 .0147 -.0008 -.49772 -.27667 _51237 SDev .0001 .0003 .0022 .0006 1.36111 3.10205 3.6476 %RSD 669.5 20.39 14.82 75.2.1 273.47 1121.2 711.91 #1 -.0001 .0018 .0164 -.0007 -.35496 -3.7937 -3.3213 #2 .0001 .0012 .0155 -.0003 -1.9246 2.0698 3.9399 j #3 -.0000 .0014 .0123 -.0015 .78638 .89379 .91857 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK i i j High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm N Avge 3.4939 3.6980 -.71289 -.0114 -.0004 .0001 .0001 \10 SDev 2.7005 4.8369 .76653 .0013 .0006 .0001 .0001 %RSD 77.292 130.80 107.52 11.27 131.3 34.18 82.08 N O ##1 6.6013 8.9659 -.02105 -.0123 .0000 .0002 .0001 2.1648 2.6709 -.58071 -.0099 -.0003 1.7155 -.54283 -1.5369 -.0120 -.0010 .0002 .0001 .0002 .0001 H Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 09:45:23 AM [h Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .17838 -.0002 .0020 -.35021 2.5011 .75596 SDev 1.5231 .0002 .0000 1.99126 .9495 2.1003 %RSD 853.82 116.2 1.373 568.59 37.963 277.83 #1 -.88915 -.0002 .0020 -2.6485 3.2971 2.9716 #2 -.49821 .0001 .0020 .73978 2.7559 .50210 #3 1.9225 -.0004 .0020 .85810 1.4502 -1.2059 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 0 page 2 Analysis Report 12/14./07 09:52:44 AM page 1 --'zod: CLP1 Sample Name: CRI Operator: CO Time: 12/14/07 09:45:29 ��JU[Lnent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 20.566 .0096 22.493 .2079 -.0001 .0102 .0022 SDev .157 .0032 1.026 .0004 .0002 .0001 .0016 %RSD .76268 32.73 4.5625 .2055 143.4 .4942 74.06 #1 20.629 .0110 22.404 .2082 .0000 .0102 .0029 #2 20.682 .0118 23.561 .2074 -.0001 .0102 .0032 #3 20.388 .0060 21.515 .2081 -.0003 .0101 .0003 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0101 .0997 .0192 .0506 -.0008 .0440 -.0004 SDev .0002 .0005 .0004 .0006 .0010 .0199 .0040 %RSD 1.8.80 .5123 2.054 1.108 121.8 45.19 1056. 41 .0101 .0999 .0193 .0503 .0003 .0441 .0012 #2 .0103 .1002 .0195 .0512 -.0010 .0639 .0026 #3 .0099 .0992 .0187 .0502 -.0017 .0241 -.0050 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb {e .0301 .0214 .0135 .0791 2.6671 5.5322 119.77 �v .0003 .0008 .0023 .0009 2.6630 .7321 3.86 %RSD 1.014 3.844 17.05 1.119 99.846 13.233 3.2224 #1 .0301 .0214 .0158 .0780 5.7407 4.7911 117.06 #2 .0303 .0223 .0137 .0796 1.0505 6.2549 124.19 #3 .0297 .0206 .0112 .0796 1.2102 5.5505 118.05 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 118.86 13.048 8.7295 .1540 .0795 .0530 .1997 SDev 2.80 1.760 .3562 .0022 .0012 .0001 .0003 %RSD 2.3563 13.490 4.0809 1.425 1.558 .2147 .1579 #1 119.37 14.806 8.7978 .1529 .0809 .0530 .1995 #2 115.84 11.286 8.3441 .1565 .0791 .0532 .2001 #3 121.37 13.052 9.0467 .1525 .0785 .0529 .1996 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 20.164 .0994 .0446 4.5781 119.16 10.168 SDev 1.994 .0006 .0001 .5035 .95 .760 %RSD 9.8875 .6425 .2550 10.997 .80118 7.4759 41 21.043 .0988 .0447 5.1074 118.60 10.799 #2 17.882 .1001 .0447 4.5219 118.62 9.3238 #3 21.568 .0992 .0445 4.1052 120.26 10.380 Analysis Report -" iod: CLP1 Sample Name: ICSA Time: 12/14/07 09:52:50 ppm k;ornrnent : ppm .0045 Mode: CONC Corr. Factor: 1 510.0 Elem Ag Al As1890 Units ppb ppm ppb Avge .63538 499.7 6.0712 SDev .16537 .7 3.5808 %RSD 26.026 .1428 58.980 #1 .61484 500.1 9.1167 #2 .81006 498.9 2.1265 #3 .48124 500.0 6.9705 Errors LC Pass LC Pass NOCHECK High 10.000 600.0 400.0 Low -10.000 400.0 K Elem Cd Cc Cr Units ppm ppm ppm Avge .0007 .0019 .0012 SDev .0001 .0002 .0004 %RSD 20.64 12.69 34.52 #1 .0009 .0018 .0012 #2 .0006 .0022 .0015 202.3 .0007 .0017 .0007 Errors LC Pass NOCHECK LC Pass High .0050 LC Pass .0100 Low -.0050 -.0100 Elem Mn Mo Na Units ppm ppm ppm Avge -.0048 -.0054 .0091 SDev .0003 .0008 .0007 %RSD 6.583 14.37 7.259 41 -.0046 -.0052 .0085 42 -.0051 -.0047 .0098 #3 -.0046 -.0062 .0092 _ Errors LC Pass NOCHECK NOCHECK High .0-150 .0030 -18.690 Low -.0150 .0025 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 11.627 12.286 -6.1540 SDev 5.387 4.520 5.6371 %RSD 46.332 .36.791 91.600 411 7.6438 7.3597 .04064 ppm 9.4803 13.255 --7.5203 - 17.756 16.243 -10.982 Errors NOCHECK NOCHECK NOCHECK 12/14/07 10:00:03 AM page 1 Operator: CO B Ba Be Ca ppm ppm ppm ppm .0045 .0013 .0002 510.0 .0006 .0001 .0000 .1 12.23 7.555 16.999 .0175 .0051 .0013 .0002 510.1 .0041 .0014 .0002 509.9 .0043 .0012 .0002 509.9 NOCHECK LC Pass LC Pass LC Pass .2000 .0050 600.0 -.2000 -.0050 400.0 Cu Fe K Mg ppm ppm ppm ppm .0053 202.4 .0332 503.1 .0002 .1 .0067 .5 3.469 .0738 20.36 .0895 .0052 202.6 .0324 503.5 .0055 202.3 .0403 502.6 .0052 202.4 .0268 503.2 NOCHECK LC Pass NOCHECK LC Pass 240.0 600.0 160.0 400.0 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0021 -19.587 5.3704 3.9373 .0012 1.249 1.1895 3.5109 58.27 6.3765 22.149 89.172 i .0007 -21.013 4.0583 7.6467 i .0030 -18.690 5.6745 3.4993 .0025 -19.057 6.3782 .66588 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti ppm ppm ppm ppm -.0065 -.0065 -.0304 .0135 .0031 .0017 .0009 .0001 48.60 26.50 3.059 .5374 N O -.0043 -.0047 -.0298 .0134 -.0050 -.0081 -.0315 .0135 -.0101 -.0066 -.0300 .0135 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 10:00:03 AM fh .U�vv Elem T11908 v Zn - Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.65755 .0045 =.0091 -2.9402 9.0661 -.01358 SDev 1.77817 .0003 .0002 1.1821 2.5982 2.25557 %RSD 270.42 6.733 2.024 40.205 28.658 16604. #1 -2.1692 .0042 -.0089 -4.2904 7.6448 2.4779 #2 -1.1051 .0048 -.0092 -2.4388 7.4887 -.60222 #3 1.3016 .0045 -.0092 -2.091.5 12.065 -1.9165 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 Analysis Report 12/14/07 10:07:22 AM page 1 P- od: CLP1 Sample Name: ICSAB Operator: CO F Time: 12/14/07 10:00:09 Comment: - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1107.7 497.2 1017.7 1.033 .5249 .4992 508.9 SDev 4.1 1.3 9.3 .004 .0018 .0016 1.7 %RSD .36643 .2711 .91000 .4361 .3362 .3262 .3386 #1 1105.4 496.6 1020.5 1.030 .5238 .4995 509.7 #2 1112.3 498.7 1025.2 1.038 .5270 .5007 510.2 #3 1105.2 496.2 1007.4 1.030 .5240 .4975 507.0 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .9398 .4783 .4861 .5651 202.0 .0292 501.5 SDev .0041 .0021 .0012 .0023 .7 .0124 1.6 %RSD .4374 .4302 .2472 .4057 .3481 42.64 .3209 #1 .9422 .4792 .4869 .5638 202.0 .0432 501.6 42 .9422 .4798 .4868 .5678 202.7 .0195 503.0 .9351 .4760 .4848 .5638 201.3 .0248 499.8 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .4852 .9719 .0398 .9530 968.67 980.59 -5.0059 SDev .0013 .0053 .0006 .0029 4.87 6.78 5.4459 0 -.RSD .2663 .5402 1.473 .2996 .50242 .69108 108.79 #1 .4857 .9721 .0405 .9545 965.09 982.79 .33778 #2 .4862 .9771 .0394 .9549 966.72 985.99 -4.8071 #3 .4838 .9666 .0395 .9497 974.21 972.98 -10.549 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm -ppm ppm ppm Avge -.03448 1005.2 999.52 1.029 .9730 .5108 1.024 SDev 3.66684 4.4 3.32 .005 .0067 .0015 .003 %RSD 10635. .43508 .33199 .4525 .6872 .2926 .2618 -41 -2.1469 1002.3 1003.1 1.028 .9767 .5118 1.023 4.1996 1003.1 998.82 1.034 .9770 .5115 1.027 „ -2.1562 1010.2 996.62 1.025 .9653 .5091 1.021 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 10:07:22 AM [h .Uu W - Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 972.05 .5011 1.046 976.62 -1.6899 1001.4 SDev 6.56 .0013 .003 3.10 3.0923 1.3 %RSD .67532 .2500 .3149 .31728 182.98 .13169 #1 970.74 .5011 1.046 976.90 -1.3194 1002.8 #2 979.17 .5023 1.050 979.57 1.2004 1000.3 #3 966.24 .4998 1.043 973.39 -4.950.8 1001.2 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 Analysis Report 12/14/07 10:14:42 AM page 1 --hod: CLP1 Sample Name: CCV1 Operator: CO Time: 12/14/07 10:07:28 --..,.nent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1044.6 49.37 502.49 2.504 2.543 2.503 49.15 SDev .8 .05 1.85 .005 .003 .003 .06 %RSD .07247 .1045 .36862 .2122 .1357 .1221 .1215 #1 1044.7 49.36 502.10 2.498 2.539 2.499 49.09 #2 1043.8 49.43 500.87 2.506 2.546 2.503 49.15 #3 1045.3 49.33 504.51 2.508 2.542 2.505 49.21 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.440 2.462 2.476 2.579 49.44 84.93 50'.90 SDev .004 .004 .004 .003 .08 .11 .00 %RSD .1797 .1543 .1413 .1327 .1579 .1351 .0031 #1 2.435 2.458 2.472 2.576 49.37 84.84 50.90 #2 2.440 2.461 2.475 2.583 49.41 85.06 50.89 2.444 2.466 2.479 2.578 49.52 84.88 50.90 terrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.476 2.439 83.22 2.459 493.02 487.91 982.62 SDev .003 .007 .09 .001 2.01 1.28 6.16 %RSD .1340 .2854 .1075 .0549 .40695 .26322 .62728 ##1 2.472 2.431 83.15 2.458 494.66 487.13 978.96 #2 2.477 2.441 83.18 2.459 493.62 489.39 989.73 43 2.479 2.444 83.32 2.460 490.78 487.20 979.15 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb -ppb ppb ppm ppm ppm ppm Avge 993.27 509.50 501.36 2.306 2,422 2.487 2.446 SDev 1.38 2.41 1.68 .003 .001 .003 .003 0-.RSD .13891 .47389 .33489 .1404 .0499 .1227 .1047 #1 991.80 508.62 500.80 2.302 2.423 2.484 2.443 994.53 512.23 500.04 2.308 2.421 2.490 2.448 993.49 507.64 503.25 2.307 2.422 2.487 2.447 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK N O Analysis Report 12/14/07 10:14:42 AM gh =_w Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 498.20 2.482 2.562 489.61 989.72 504.07 SDev 2.37 .004 .002 1.20 2.84 .65 %RSD .47567 .1675 .0899 .24585 .28722 .12967 #1 495.70 2.477 2.559 489.64 987.52 503.41 #2 498.51 2.484 2.562 490.80 992.93 504.10 #3 500.41 2.485 2.564 488.39 988.72 504.71 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 12/14/07 10:22:02 AM page 1 P'-`'zod: CLP1 Sample Name: CCVL1 Operator: CO Time: 12/14/07 10:14:48 L-J««<ient : - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .35318 .0596 2.0461 .0033 .0009 .0008 .0595 I SDev .64344 .0182 1.3184 .0010 .0003 .0003 .0216 %RSD 182.19 30.51 64.436 30.00 31.33 34.31 36.36 j #1 .80431 .0725 2.2191 .0040 .0011 .0010 .0776 I ,#2 .63886 .0674 3.2695 .0037 .0010 .0008 .0652 f #3 -.38364 .0388 .64973 .0022 .0006 .0005 .0355 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0007 .0006 .0001 .0008 2.572 .0642 .0557 SDev .0003 .0004 .0003 .0006 .012 .0106 .0195 %RSD 34.96 64.40 389.9 78.90 .4535 16.49 34.91 #1 .0010 .0006 .0001 .0013 2.580 .0734 .0712 #2 .0007 .0010 .0003 .0010 2.577 .0665 .0621 .0005 .0002 -.0002 .0001 2.558 .0526 .0339 I Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0052 2.575 -.0009 -1.3739 -1.8175 2.5572 SDev .0003 .0023 .015 .0007 1.9066 .7111 .8235 %RSD 41.68 43.65 .5862 75.24 138.77 39.123 32.202 #1 .0008 .0078 2.589 -.0002 -3.2722 -11.9950 3.4986 I #2 .0007 .0045 2.577 -.0010 -1.3903 -2.4231 2.2025 #3 .0003 .0034 2.559 -.0015 .54083 -1.0345 1.9706 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 I Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm ,--� Avge 3.2976 5.3302 .51422 -.0096 -.0003- .0008 .0008 SDev 4.4652 1.6259 2.3088 .0015 .0007 .0003 .0004 %RSD 135.40 30.503 448.99 15.19 208.1 36.25 47.16 N O #1 5.5907 4.1856 3.1246 -.0083 -.0005 .0010 .0011 6.1504 7.1913 -1.2601 -.0093 .0004 .0009- .0010 -1.8481 4.6137 -.32186 -.0112 -.0010 .0004 .0004 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 10:22:02 AM h Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.1140 .0009 .0035 -1.6697 3.0511 2.1180 SDev 2.3125 .0003 .0004 1.0189 3.1417 1.1835 %RSD 109.39 27.55 11.25 61.019 102.97 55.878 #1 -.54546 .0011 .0038 -2.4202 4.8941 3.4779 #2 3.6517 .0011 .0036 -2.0791 4.8358 1.5543 #3 3.2357 .0006 .0030 -.50986 -.57648 1.3217 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low page 2 Analysis Report 12/14/07 10:29:21 AM page 1 N'-`'-od: CLPl Sample Name: CCB1 Operator: CO R Time: 12/14/07 10:22:07 C. MLtLant : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.07963 .0143 2.2338 .0007 .0002 .0001 .0090 SDev .03115 .0011 1.5741 .0001 .0001 .0000 .0012 %RSD 3.9.114 7.373 70.471 18.03 51.10 18.90 12.82 #1 -.05048 .0139 2.9368 .0007 .0002 .0002 .0094 #2 -.11245 .0135 .43061 .0006 .0001 .0001 .0077 #3 -.07596 .0155 3.3339 .0008 .0003 .0001 .0100 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0002 -.0005 .0003 .0053 .0513 .0118 SDev .0001 .0004 .0004 .0003 .0010 .0156 .0040 %RSD 70.86 248.7 80.05 76.67 18.78 30.31 34.21 #1 .0001 -.0002 -.0005 .0002 .0065 .0476 .0130 ##2 .0000 .0001 -.0010 .0002 .0045 .0380 .0073 .0001 .0007 -.0001 .0006 .0050 .0684 .0151 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0000 .0008 .0144 -.0009 -2.5400 -.14706 -.10982 SDev .0002 .0005 .0020 .0004 2.4295 .97070 1.27508 %RSD 389.9 65.95 13.99 42.21 95.650 660.05 1161.1 #1 -.0000 .0005 .0165 -.0005 -3.9832 .57628 1.3158 #2 -.0001 .0004 .0125 -.0009 -3.9017 .23277 -.50400 43 .0003 .0014 .0142 -.0012 .26497 -1.2502 -1.1413 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti t Units ppb ppb ppb ppm ppm ppm ppm cn Avge 1.0515 4.0759 -1.3582 -.0147 -.0008 SDev 2.4635 .3603 .9997 .0046 .0016 .0002 .0001 .0003 .0002 oRSD 234.30 8.8410 73.601 31.35 205.8 29.72 75.18 c`1 #1 -1.7715 4.4174 -1.4821 -.0166 .0011 .0002 .0003 2.7665 3.6993 -2.2901 -.0181 -.0014 .0001 .0001 C/) 2.1593 4.1111 -.30237 -.0095 -.0020 .0002 .0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 10:29:21 AM page 2 gh Zn __9 Sb2068 El em T11908 Units ppb Avge -1.7021 SDev .6942 %RSD 40.785 #1 -1.9057 #2 -2.2717 #3 -.92886 Errors LC Pass High 10.000 Low -10.000 v Zn Pb2203 Sb2068 Se.1960 ppm ppm ppb ppb ppb .0001 .0040 -.94383 .66479 .45139 .0001 .0002 .19917 1.2580 .73198 275.9 4.533 21.103 189.23 162.16 .0002 .0042 -.94195 -.74339 .4.8.246 -.0001 .0039 -1.1439 1.6775 -.29563 .0001 .0039 -.74560 1.0603 1.1673 LC Pass LC Pass LC Pass LC Pass LC Pass .0500 .0200 3.0000 60.000 5.0000 -.0500 -.0200 -3.0000 -60.000 -5.0000 Analysis Report 12/14/07 10:36:41 AM page 1. P- hod: CL21 Sample Name: 0714124-003A Operator: CO ] Time: 12/14/07 10:29:27 C-...ient : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .38276 .0229 3.2914 .0252 .0017 -.0000 .0073 SDev .19006 .0066 2.4561 .0022 .0008 .0000 .0056 %RSD 49.656 28.73 74.622 8.586 43.65 7.117 76.10 #1 .16969 .0219 1.2752 .0271 .0025 -.0000 .0137 #2 .53483 .0300 2.5721 .0257 .0016 -.0000 .0052 #3 .44378 .0169 6.0268 .0229 .0010 -.0000 .0031 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0000 -.0002 .0007 .0050 .0694 .0051 SDev .0000 .0007 .0016 .0004 .0027 .0314 .0027 %RSD 19.20 3064. 977.7 51.32 52.89 45.17 52.06 #1 -.0001 -.0008 -.0013 .0004 .0037 .0351 .0027 #2 -.0001 .0005 -.0008 .0007 .0033 .0765 .0047 ##3 -.0001 .0004 .0017 .0011 .0081 .0966 .0080 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb [e -.0001 .0054 14.03 -.0011 -4.6213 -.68218 .17845 v .0004 .0027 .62 .0011 1.8381 1.67735 3.4080 6xSD 483.8 49.40 4.422 104.0 39.774 245.88 1909.8 #1 -.0005 .0074 13.31 -.0024 -5.7538 .66488 3.0372 #2 -.0001 .0063 14.43 -.0008 -5.6096 -.15048 1.0911 #3 .0004 .0024 14.34 -.0002 -2.5005 -2.5609 -3.5929 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.9250 10.352 -2.0681 11.14 .0003 .0001 .0023 SDev 1.8325 2.303 1.2836 .23 .0028 .0001 .0002 %RSD 46.689 22.246 62.068 2.060 872.0 111.6 10.16 #1 5.7060 8.4460 -.84751 11.26 -.0029 -.0000 .0024 #2 4.0242 9.6989 -1.9502 11.27 .0017 .0001 .0026 #3 2.0449 12.911 -3.4067 10.87 .0022 .0002 .0021 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.0105 -.0001 .0064 -1.9938 2.6774 2.0677 SDev .4329 .0006 .0028 .5346 2.3469 .1630 %RSD 42.841 617.4 43.70 26.812 87.653 7.8841 #1 .80783 -.0005 .0094 -1.4725 4.8173 2.2473 #2 1.5076 .0006 .0059 -1.9683 3.0475 1.9289 #3 .71616 -.0004 .0039 -2.5407 .16753 2.0270 Analysis Report 12/14/07 10:44:00 AM page 1 V-�'-,:od: CLP1 Sample Name: 0714124-002A Operator: CO Time: 12/14/07 10:36:46 (_....tent: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .07054 .0112 2.7436 .3380 .0011 -.0000 .0051 SDev .50020 .0043 .5532 .0010 .0001 .0000 .0032 -RSD 709.12 38.61 20.164 .3034 13.46 35.16 64.03 #1 .64748 .0146 2.7364 .3372 .0012 -.0000 .0088 #2 -.19425 .0126 2.1940 .3392 .0012 -.0000 .0033 #3 -.24161 .0063 3.3003 .3377 .0010 -.0000 .0031 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0001 -.0007 .0017 .0004 .0734 .0068 SDev .0001 .0006 .0004 .0009 .0012 .0179 .0056 %RSD 225.7 531.2 52.98 53.65 296.6 24.31 81.59 #1 .0001 .0008 -.0003 .0026 .0000 .0933 .0127 #2 -.0000 -.0002 -.0010 .0016 .0017 .0588 .0060 #3 -.0002 -.0002 -.0010 .0008 -.0005 .0682 .0017 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e -.0001 .0038 22.65 -.0007 -3.6798 .05562 -2.0131 v .0002 .0015 .22 .0005 1.1127 .73728 1.0516 6x,bD 203.5 40.80 .9618 75.26 30.237 1325.7 52.239 #1 .0001 .0050 22.41 -.0012 -4.1599 .81446 -1.4605 #2 -.0002 .0044 22.84 -.0001 -4.4718 -.65803 -1.3529 #3 -.0002 .0021 22.69 -.0008 -2.4077 .01041 -3.2258 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.7094 7.8719 -.19367 17.06 .0024 .0001 .0037 SDev 1.1925 1.5434 2.97887 .09 .0015 .0001 .0004 %RSD 69.764 19.607 1538.1 .5428 63.43 156.5 9.731 41 1.4056 6.3220 2.9457 17.15 .0016 .0002 .0041 #2 .69813 7.8851 -2.9807 17.05 .0041 -.0000 .0035 #3 3.0244 9.4088 -.54597 16.97 .0014 .0000 .0035 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.3473 -.0003 .0047 -1.1882 .46983 2.4922 SDev 4.5014 .0008 .0007 .6411 .46426 1.7329 %RSD 334.10 241.5 14.61 53.953 98.816 69.532 #1 2.2717 .0003 .0054 -.84193 .45118 4.0700 #2 5.3148 -.0001 .0049 -1.9280 .01516 .63759 #3 -3.5445 -.0012 .0040 -.79474 .94313 2.7690 N O E -q Analysis Report 12/14/07 10:51:19 AM page 1 M -+-hod: CLP1 Sample Name: 0714124-003A Operator: CO ] Time: 12/14/07 10:44:06 (._..... lent : Mode: CONC' Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .00280 .0097 1.6996 .0238 .001.0 -.0001 .0002 SDev .33472 .0026 .6420 .0008 .0002 .0000 .0012 %RSD 11943. 26.18 37.773 3.287 23.98 45.32 547.3 #1 -.37155 .0118 2.2748 .0237 .0012 -.0001 .0016 #2 .10672 .0105 1.8168 .0246 .0010 -.0001 -.0002 #3 .27324 .0069 1.0070 .0231 .0007 -.0000 -.0008 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 -.0001 -.0012 .0005 -.0021 .0628 -.0006 SDev .0001 .0004 .0002 .0003 .0005 .0030 .0020 %RSD 1207. 368.4 19.46 49.01 23.22 4.786 322.0 #1 -.0000 -.0005 -.0013 .0007 -.0019 .0631 .0011 #2 -.0001 .0004 -.0010 .0002 -.0018 .0656 -_0001 #3 .0001 -.0002 -.0015 .0006 -.0027 .0596 -.0029 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units - ppm ppm ppm ppm ppb ppb ppb e -.0003 .0009 14.11 -..0014 -2.2311 -1.9123 -1.4902 v .0000 .0003 .62 .0002 1.5383 .6366 2.7541 or,,)D 12.54 34.57 4.408 14.64 68.947 33.290 184.82 #1 -.0003 .0007 13.39 -.0015 -.46348 -2.6450 -4.6138 #2 -.0003 .0013 14.49 -.0011 -2.9636 -1.5976 -.44579 #3 -.0003 .0008 14.45 -.0015 -3.2663 -1.4944 .58896 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.31052 7.9157 -3.2916 10.84 -.0028 -.0000 .0020 SDev .89336 2.2716 1.1467 .10 .0007 .0000 .0003 %RSD 287.70 28.698 34.836 .9280 25.86 174.9 15.14 #1 .16183 10.480 -4.2030 10.95 -.0033 .0000 .0022 #2 .24752 7.1106 -2.0041 10.77 -.0019 -.0000 .0021 #3 -1.3409 6.1562 -3.6677 10.78 -.0030 -.0000 .0016 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.9483 .0000 .0031 -2.0184 -.70331 .44044 SDev 2.2173 .0001 .0008 .0880 .72256 .74483 %RSD 113.81 319.1 26.94 4.3603 102.74 169.11 #1 4.2443 -.0001 .0040 -1.9185 -1.4284 .68654 N #2 1.7814 .0000 .0029 -2.0524 .01668 1.0311 O #3 -.18081 .0002 .0024 -2.0844 -.69822 -.39630 N Analysis Report 12/14/07 10:58:39 AM page 1 P"od: CLP1 Sample Name: 0714160-001A Operator: CO F Time: 12/14/07 10:51:25 C.kJI<«<<ent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.22407 .0247 5.4300 .0042 .0126 -.0000 5.464 SDev .30491 .0034 .8216 .0005 .0004 .0000 .035 %RSD 136.08 13.91 15.131 11.27 3.468 46.56 .6433 #1 -.42608 .0270 5.5156 .0038 .0124 -.0000 5.431 #2 .12667 .0265 6.2055 .0047 .0123 -.0000 5.501 #3 -.37280 .0208 4.5690 .0043 .0131 -.0000 5.460 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0003 -.0002 -.0011 .0068 .0361 .6038 1.190 SDev .0001 .0003 .0000 .0003 .0012 .0141 .010 %RSD 34.77 156.8 3.316 3.764 3.425 2.335 .8444 #1 -.0002 -.0001 -.0011 .0070 .0371 .5965 1.186 #2 -.0003. .0000 -.0012 .0070 .0365 .6201 1.201 #3 -.0004 -.0005 -.0011 .0065 .0347 .5948 1.182 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .0225 .0001 7.744 -.0018 -.48385 -1.2641 -1.9294 v .0029 .0003 .117 .0008 1.20541 1.3299 .7473 %RSD 12.86 225.4 1.512 43.40 249.13 105.20 38.730 #1 .0211 -.0002 7.746 -.0023 .90649 -2.7306 -2.2864 #2 .0258 .0003 7.861 -.0021 -1.1223 -.13644 -2.4312 #3 .0205 .0004 7.627 -.0009 -1.2358 -.92523 -1.0706 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 2.4232 12.847 .60214 1.127 -.0027 .0151 .0016 SDev 1.3349 1.213 2.9546 .010 .0013 .0003 .0023 %RSD 55.088 9.4400 490.69 .9288 49.24 1.881 143.5 #1 3.9560 13.669 -2.3637 1.133 -.0031 .0150 -.0002 #2 1.7983 13.418 3.5454 1.134 -.0012 .0155 .0008 #3 1.5154 11.454 .62472 1.115 -.0038 .0150 0042 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.010,2 -.0.002 .0018 -1.0042 .97386 4.6798 SDev 1.1912 .0001 .0006 .5278 .79352 1.9676 %RSD 59.258 40.88 34.21 52.558 81.482 42.044 #1 .63809 -.0002 .0025 -1.5194 1.8773 2.9754 #2 2.6129 -.0002 .0014 -.46464 .38992 6.8330 41q 2.7797 -.0001 .0015 -1.0286 .65432 4.2310 Analysis Report 12/14/07 11:05:59 AM page 1 PA--'iod: CLP1 Sample Name: 0714160-002A Operator: CO ] Time: 12/14/07 10:58:45 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .27998 .0271 4.2167 .0042 .0121 -.0000 5.470 SDev .29947 .0031 1.5771 .0002 .0007 .0000 .115 %RSD 106.96 11.32 37.401 4.071 5.873 25.Oi 2.108 #1 .58625 .0276 3.0271 .0040 .0125 -.0000 5.477 #2 -.01220 .0238 3.6173 .0043 .0113 -.0000 5.351 #3 .26588 .0299 6.0056 .0043 .0125 -.0000 5.581 Eleni Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 -.0003 -.0014 .0040 .0649 .5997 1.182 SDev .0001 .0004 .0004 .0005 .0023 .0168 .020 %RSD 56.66 134.6 27.50 11.68 3.546 2.800 1.653 #1 -.0001 -.0003 -.0011 .0038 .0629 .5885 1.175 #2 -.0002 -.0007 -.0018 .0036 .0644 .5917 1.167 #3 -.0001 .0001 -.0012 .0045 .0674 .6190 1.204 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .01.92 .0002 7.846 -.0012 -2.8410 -1.2942 -.58026 v .0004 .0005 .082 .0005 1.6598 .7734 .47620 aR.SD 1.861 242.4 1.040 39.71 58.426 59.764 82.067 #1 .0190 .0001 7.752 -.0014 -4.7551 -1.0356 -.04424 #2 .0196 .0007 7.889 -.0007 -1.9689 -.68309 -.74207 #3 .0190 -.0002 7.898 -.0016 -1.7989 -2.1637 -.95448 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.1031 10.538 -1.0518 1.116 -.0022 .0150 -.0003 SDev 1.3185 2.005 .4254 .019 .0012 .0003 .0001. %RSD 119.53 19.030 40.440 1.718 53.61 1.696 27.78 41 -.34677 10.267 -.57299 1.104 - -.0009 .0149 -.0002 #2 -2.6256 12.665 -1.1966 1.107 -.0033 .0148 -.0004 #3 -.33687 8.6821 -1.3859 1.138 -.0025 .0153 -.0004 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .36452 .0003 .0030 -1.8092 -.92894 2.8076 SDev 2.3313 .0003 .0019 .6155 .93792 .7530 %RSD 639.56 108.0 65.78 34.020 100.97 26.819 41 -2.3263 .0000 .0052 -2.2741 -.24599 3.0367 #2 1.7781 .0002 .0016 -1.1112 -1.9983 3.4194 113 1.6418 .0006 -.0020 -2.0422 -.54249 1.9667 Analysis Report 12/14/07 11:13:19 AM page 1 --hod: CLP1 Sample Name: 0714160-003A Operator: CO Time: 12/14/07 11:06:05 .,,,,, ient : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .04772 .0282 4.7975 .0049 .0124 -.0000 5.490 SDev .31309 .0022 .3318 .0004 .0006 .0000 .070 %RSD 656.06 7.769 6.9158 7.965 5.176 36.49 1.278 #1 .15076 .0306 4.4144 .0053 .0129 -.0001 5.532 #2 .29631 .0263 4.9903 .0050 .0117 -.0000 5.409 #3 -.30390 .0277 4.9879 .0045 .0125 -.0000 5.528 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 -.0001 -.0013 .0009 .0517 .6034 1.187 SDev .0002 .0002 .0002 .0001 .0017 .0142 .007 %RSD 325.1 117.6 12.86 10.46 3.219 2.349 .5805 #1 .0001 .0000 -.0015 .0008 .0499 .5878 1.186 #2 -.0003 -.0001 -.0013 .0009 .0523 .6071 1.180 #3 .0000 -.0003 -.0012 .0009 .0531 .6154 1.194 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .0200 .0001 7.824 -.0012 -2.5024 -.38956 -1.3511 v .0035 .0006 .050 .0007 2.4900 1.94901 3.0914 %RSD 17.39 792.9 .6395 60.28 99.504 500.31 228.80 #1 .0171 -.0002 7.768 -.0020 -3.2100 .99720 1.7562 #2 .0191 -.0003 7.842 -.0010 -4.5622 .45209 -1.3833 #3 .0238 .0008 7.863 -.0006 .26479 -2.6180 -4.4262 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.1391 10.861 .68582 1.119 -'.0013 .0152 -.0003 SDev 1.5553 1.619 1.9274 .008 .0019 .0001 .0002 %RSD 136.54 14.906 281.03 .7192 147.2 .6639 60.67 #1 -.56113 11.688 2.4012 1.111 -.0018 .0151 -.0005 #2 1.4881 8.9953 -1.3998 1.119 -.0028 .0151 -.0001 #3 2.4902 11.899 1.0561 1.127 .0008 .0153 -.0004 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.8947 -.0000 -.0001 -1.0931 .30987 4.0741 SDev 1.9715 .0003 .0009 .6363 .19268 1.7911 %RSD 104.06 9027. 763.3 58.213 62.182 43.963 #1 3.3141 .0002 .0009 -.40371 .21058 5.4937 #2 -.35640 .0002 -.0008 -1.2176 .53195 2.0618 #3 2.7264 -.0004 -.0005 -1.6579 .18709 4.6668 O 00 N O Analysis Report 12/14/07 11:20:40 AM page 1 M od: CLP1 Sample Name: CCV2 ime: 12/14/07 11:13:25 82.97 Co Hent: 001 .008 .13 Mode: CONC Corr. Factor: 1 .3158 Elem Ag Al As1890 Units ppb ppm ppb Avge 1046.0 49.26 500.35 SDev .9 .03 3.03 %RSD .081850 .0533 .60590 #1 1045.2 49.25 496.85 #2 1045.8 49.29 502.01 #3 1047.0 49.25 502.18 Elem Cd Cc Cr Units ppm ppm ppm Avge 2.440 2.456 2.472 SDev .002 .003 .003 %RSD 0633 .1188 .1224 #1 2.438 2.454 2.468 #2 2.441 2.457 2.473 #3 2.440 2.459 2.474 Elem Mn Mo Na Units ppm ppm ppm B PPM 2.506 .003 1150 2.503 2.509 2.506 Cu ppm 2.566 .003 .1000 2.567 2.567 2.563 Ni ppm 2.458 .001 .0410 2.457 2.459 2.457 Si PPM 2.295 .002 .0928 2.293 2.297 2.295 Pb2203 ppb 488.07 1.46 .29881 486.57 488.16 489.49 Ba Ppm 2.529 .002 .0827 2.531 2.530 2.527 Fe PPM 49.43 .06 .1201 49.37 49.44 49.49 2203/1 ppb 489.59 2.02 .41160 487.35 491.27 490.13 Sn PPM 2.410 .004 .1736 2.406 2.414 2.409 Sb2068 ppb 982.54 5.80 .59029 976.87 982.29 988.47 Operator: CO Be ppm 2.504 .003 .1157 2.500 2.506 2.504 K PPM 84.88 .12 .1458 84.87 85.00 84.76 2203/2 ppb 487.32 1.61 .33068 486.19 486.61 489.16 Sr PPM 2.478 .002 .0750 2.479 2.478 2.476 Se1960 ppb 507.91 1.31 .25717 507.60 509.34 506.78 Ca PPM 49.15 .09 .1834 49.05 49.20 49.20 Mg PPM 50.64 .07 .1395 50.56 50.68 50.67 2068/1 ppb 974.62 11.79 1.2098 961.37 978.51 983.97 Ti Ppm 2.439 .001 .0472 2.439 2.440 2.438 2.474 2.436 82.97 ec 001 .008 .13 %RSD .0598 .3158 .1607 #1 2.472 2.428 82.92 #2 2.475 2.440 82.88 #3 2.474 2.442 83.13 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 986.50 513.58 505.08 SDev 3.65 2.59 3.21 %RSD .37023 .50418 .63509 #1 984.61 513.19 504.82 #2 984.18 511.21 508.41 #3 990.71 516.34 502.01 Elem T11908 V Zn Units ppb ppm ppm Avge 496.68 2.474 2.564 SDev 1.78 .002 .003 %RSD .35923 .0730 .1267 #1 494.94 2.472 2.561 #2 496.58 2.475 2.567 #3 0 498.51 2.475 2.564 B PPM 2.506 .003 1150 2.503 2.509 2.506 Cu ppm 2.566 .003 .1000 2.567 2.567 2.563 Ni ppm 2.458 .001 .0410 2.457 2.459 2.457 Si PPM 2.295 .002 .0928 2.293 2.297 2.295 Pb2203 ppb 488.07 1.46 .29881 486.57 488.16 489.49 Ba Ppm 2.529 .002 .0827 2.531 2.530 2.527 Fe PPM 49.43 .06 .1201 49.37 49.44 49.49 2203/1 ppb 489.59 2.02 .41160 487.35 491.27 490.13 Sn PPM 2.410 .004 .1736 2.406 2.414 2.409 Sb2068 ppb 982.54 5.80 .59029 976.87 982.29 988.47 Operator: CO Be ppm 2.504 .003 .1157 2.500 2.506 2.504 K PPM 84.88 .12 .1458 84.87 85.00 84.76 2203/2 ppb 487.32 1.61 .33068 486.19 486.61 489.16 Sr PPM 2.478 .002 .0750 2.479 2.478 2.476 Se1960 ppb 507.91 1.31 .25717 507.60 509.34 506.78 Ca PPM 49.15 .09 .1834 49.05 49.20 49.20 Mg PPM 50.64 .07 .1395 50.56 50.68 50.67 2068/1 ppb 974.62 11.79 1.2098 961.37 978.51 983.97 Ti Ppm 2.439 .001 .0472 2.439 2.440 2.438 Analysis Report 12/14/07 11:28:00 AM page 1 Y--'-od: CLP1 Sample Name: CCVL2 Operator: CO F Time: 12/14/07 11:20:46 CUMCL,ent : - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .12218 .0230 1.9710 .0037 .0009 .0008 .0221 SDev .41.043 .0094 1.7900 .0014 .0004 .0003 .0082 %RSD 335.94 41.04 90.818 37.68 42.91 43.53 36.94 #1 .59488 .0313 3.9392 .0053 .0012 .0011 .0294 #2 -.08474 .0249 1.5334 .0032 .0010 .0009 .0238 #3 -.14362 .0127 .44033 .0026 .0005 .0004 .0133 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0007 .0003 -.0004 .0041 2.502 .0602 .0131 SDev .0004 .0002 .0002 .0002 .008 .0079 .0080 %RSD 57.88 62.58 60.23 4.516 .3080 13.06 60.97 #1 .0012 .0005 -.0004 .0043 2.505 .0684 .0195 #2 .0007 .0002 -.0002 .0041 2.507 .0597 .0158 #3 .0003 .0002 -.0007 .0039 2.493 .0527 .0041 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb __ .0009 .0045 2.589 -.0001 -.50799 -1.0492 4.7073 s .0004 .0028 .013 .0006 .93372 .2795 4.6361 %RSD 44.86 62.97 .4918 391.1 183.81 26.640 98.488 #1 .0013 .0076 2.599 -.0006 -1.2168 -1.2584 9.1871 #2 .0010 .0039 2.594 .0005 .54999 -.73175 5.0054 #3 .0005 .0020 2.575 -.0004 -.85715 -1.1574 -.07067 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.8183 7.0844 -2.2958 .0022 -.0010 .0010 .0007 SDev .6395 .8547 1.2634 .0021 .0023 .0004 .0004 %RSD 16.750 12.065 55.031 93.93 228.3 36.98 60.86 #1 4.3769 7.9985 -.90253 .0041 -.0028 .0013 .0010 #2 3.9572 6.9493 -2.6179 .0027 -.0020 .0011, .0009 #3 3.1207 6.3052 -3.3670 -.0001 .0016 .0006 .0002 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.5407 .0004 .0145 -.86886 4.1144 .82784 SDev .5780 .0003 .0005 .49735 1.9674 1.1265 %RSD 22.750 68.89 3.458 57.242 47.818 136.08 #1 2.3160 .0008 .0149 -1.2444 5.9788 2.0616 #2 2.1088 .0003 .0146 -.30482 4.3063 .56806 -#3 3.1973 .0002 .0139 -1.0573 2.0580 -.14611 Analysis Report 12/14/07 11:35:20 AM page 1 M -'' )d: CLP1 Sample Name: CCB2 Operator: CO R Cime: 12/14/07 11:28:06 CUI[h[Lent : - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .24294 .0101 1.9504 .0005 .0001 .0001 .0028 SDev .34886 .0023 .5824., .0007 .0000 .0000 .0010 %RSD 143.60 22.97 29.860 129.2 23.50 19.86 33.85 #1 -.10352 .0082 2.6072 .0006 .0001 .0002 .0035 #2 .23820 .0127 1.4971 .0012 .0001 .0002 .0033 #3 .59415 .0094 1.7469 -.0002 .0002 .0001 .0017 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0002 -.0007 .0000 .0020 .0442 -.0008 SDev .0001 .0003 .0000 .0002 .0011 .0080 .0020 %RSD 173.1 131.5 .1275 985.0 54.11 18.22 268.7 #1 -.0001 -.0004 -.0007 -.0000 .0025 .0390 -.0002 #2 .0001 -.0004 -.0007 -.0001 .0026 .0401 -.0030 #3 .0002 .0001 -.0007 .0002 .0007 .0534 .0009 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb .0001 .0010 .0171 -.0008 -.65804 -1.3038 1.0514 r .0000 .0006 .0023 .0009 2.02883 .7008 .0723 %RSD 44.40 61.06 13.30 118.8 308.32 53.749 6.8752 #1 .0000 .0015 .0179 -.0005 -.63034 -2.0848 1.0511 #2 .0001 .0010. .0188 -.0018 1.3568 -.72982 1.1238 #3 .0001 .0004 .0145 .0000 -2.7006 -1.0969 .97925 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .99306 1.3863 -1.7401 -.0200 -.0014 .0001 .0001 SDev 1.1437 3.0554 2.4616 .0016 .0005 .0000 .0002 %RSD 115.17 220.40 141.46 7.816 33.51 13.36 132.8 #1 1.6131 1.8871 -2.3151 -.0186 -.0010 .0002 -.0000 #2 1.6928 4.1604 -3.8634 -.0198 -.0014 .0001 .0001 #3 -.32676 -1.8886 .95808 -.0217 -.0019 .0002 .0003 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 3.0151 .0001 .0003 -1.0887 1.0125 -.69899 SDev 2.6424 .0006 .0001 .9127 .7841 .62945 %RSD 87.639 574.4 18.45 83.838 77.444 90.051 ##1 1.4402 -.0002 .0003 -1.6004 1.4260 -.91570 #2 6.0657 .0008 .0004 -.03490 1.5034 -1.1915 :R3 1.5393 -.0002 .0003 -1.6308 .10818 .01019 Analysis Report 12/14/07 11:42:40 AM page 1 Y -'od: CLP1 Sample Name: MB -23971 Operator: CO F Time: 12/14/07 11:35:2.6 Comment: Mode: CONC Corr. Factor: 1CWL Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.05199 .0086 .00813 .0001 -.0004 .0000 .0124 SDev .41841 .0020 1.8983 .0002 .0001 .0000 .0011 %RSD 804.75 22.92 23361. 289.8 24.65 174.0 8.690 #1 .43039 .0092 2.0525 .0000 -.0003 .0001 .0133 #2 -.26985 .0102 -.32929 .0003 -.0004 .0000 .0127 #3 -.31652 .0064 -1.6988 -.0001 -.0005 -.0000 .0112 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0002 -.0002 .0001 .0002 .0157 .0447 .0011 SDev .0001 .0004 .0004 .0002 .0003 .0186 .0041 %RSD 47.15 173.8 295.3 92.13 1.702 41.56 358.5 #1 -,0003 .0002 .0004 .0003 .0159 .0510 .0030 #2 -.0003 -..0003 .0004 .0003 .0159 .0593 .0040 -.0001 -.0006 -.0003 -.0000 .0154 .0238 -.0035 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 22.03/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0004 .0074 -.0006 3.4364 -.34017 -1:3899 SDev .0001 .0004 .0022 .0007 1.9011 .95061 1.9302 %RSD 26.27 119.7 29.78 108.6 55.322 279.45 138.87 #1 .0007 .0005 .0094 -.0002 3.0478 -.19585 .59435 #2 .0006 -.0001 .0078 -.0003 5.5019 -1.3547 -3.2612 #3 .0004 .0007 .0051 -.0014 1:7597 .53003 -1.5030 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm �t Avge 2.2904 -1.9323 .01042 -.0226 -.0013 .0000 .001700 SDev 4:1022 2.5124 1.3695 .0009 .0021 .0001 .0002 %RSD 179.10 130.02 13140. 4.013 161.5 187.0 12.72 N 2.2139 -4.7532 1.5901 -.0220 .0008 .0001 .0019 6.4303 .06487 -.71584 -.0222 -.0034 .0001 .0017 -1.7730 -1.1086 -.84302 -.0236 -.0013 -.0000 .0015 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 11:42:40 AM h Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -2.2892 .0000 .0025 .91752 1.0649 -.63646 SDev 1.3774 .0003 .0001 .02925 2.4995 .25758 %RSD 60.170 6805. 5.048 3.1879 234.72 40.470 #1 -3.1067 -.0001 .0026 .88434 1..6746 -.52215 #2 -.69891 .0003 .0026 .92862 3.2031 -.45582 #3 -3.0621 -.0002 .0024 .93960 -1.6831 -.93141 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 12/14/07 11:50:00 AM M-1-1-od: CLP1 Sample Name: LCS-23971 Operator: CO F Time: 12/14/07 11:42:46 C-......ent : f Mode: CONC Corr. Factor: 1 l� CCCj Eleni Ag Al As1890 B Units ppb ppm ppb ppm Avge 1019.7 47.11 475.05 2.380 SDev 6.3 .31 3.69 .018 %RSD .61937 .6639 .77717 .7442 #1 1015.9 46.89 472.72 2.367 #2 1016.3 46.98 473.13 2.373 #3 1027.0 47.47 479.31 2.400 Errors LC Pass LC Pass LC Pass LC Pass High 1200.0 60.00 600.00 3.000 Low 800.00 40.00 400.00 2.000 Eleni Cd Co Cr Cu Units ppm ppm ppm ppm Avge 2.329 2.343 2.363 2.538 SDev .015 .015 .016 .016 %RSD .6487 .6344 .6576 .6455 #1 2.318 2.333 2.352 2.528 #2 2.322 2.336 2.355 2.528 2.346 2.360 2.381 2.557 terrors LC Pass LC Pass LC Pass LC Pass High 3.000 3.000 3.000 3.000 Low 2.000 2.000 2.000 2.000 Elem Mn Mo Na Ni Units ppm ppm ppm ppm Avge 2.371 2.383 81.61 2.331 SDev .015 .017 .38 .017 %RSD .6243 .7237 .4674 .7124 #1 2.361 2.373 81.29 2.320 #2 2.364 2.372 81.50 2.322 #3 2.388 2.403 82.03 2.350 Errors LC Pass NOCHECK LC Pass LC Pass High 3.000 96.00 3.000 Low 2.000 64.00 2.000 Eleni 2068/2 1960/1 1960/2 Si Units ppb ppb ppb ppm Avge 939.79 455.60 462.89 2.750 SDev 3.30 1.96 6.75 .023 %RSD .35130 .43083 1.4590 .8310 #1 942.27 453.35 459.74 2.733 936.05 456.98 458.29 2.741 941.07 456.46 470.64 2.776 Errors NOCHECK NOCHECK Ba ppm 2.465 .016 .6305 2.456 2.455 2.483 LC Pass 3.000 2.000 Fe ppm 47.33 .32 .6867 47.12 47.16 47.70 LC Pass 60.00 40.00 2203/1 ppb 481.66 1.82 .37752 480.83 480.41 483.75 NOCHECK Sn ppm 2.332 .020 .8525 2.317 2.325 2.355 NOCHECK NOCHECK NOCHECK Be ppm 2.367 .015 .6546 2.358 2.359 2.385 LC Pass 3.000 2.000 K ppm 82.39 .54 .6578 81.96 82.22 83.00 LC Pass 96.00 64.00 2203/2 ppb 470.47 5.43 1.1537 466.90 467.79 476.72 NOCHECK Sr PPM 2.407 .014 .5985 2.399 2.399 2.424 NOCHECK page 1 Ca PPM 46.73 .30 6479 46.52 46.60 47.08 LC Pass 60.00 40.00 Mg ppm 47.94 .31 .6439 47.74 47.78 48.29 LC Pass 60.00 40.00 2068/1 ppb 924.34 8.25 .8.9266 919.88 919.27 933.86 NOCHECK Ti PPM 2.385 .015 .6476 2.376 2.376 2.403 NOCHECK Analysis Report 12/14/07 11:50:00 AM page 2 h Elem T11908 v Zn Pb2203 Sb2.068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 477.36 2.389 2.445 474.20 934.65 460.46 SDev 5.72 .015 .016 4.22 4.11 4.73 0 -.RSD 1.1989 .6075 .6597 .88904 .43923 1.0269 #1 473.65 2.379 2.434 471.54 934.81 457.61 #2 474.48 2.382 2.437 472.00 930.46 457.85 #3 483.95 2.406 2.463 479.06 938.67 465.92 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 600.00 3.000 3.000 600.00 1200.0 600.00 Low 400.00 2.000 2.000 400.00 800.00 400.00 t- oo N Analysis Report 12/14/07 11:57:19 AM page 1 M-�'�od: CLP1 Sample Name: 0713771-001D Operator: CO R Time: 12/14/07 11:50:06 C..,......�nt : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm PPM ppm Avge .03566 .3546 .01068 .0198 .0380 .0007 20.34 SDev .61842 .0072 .32667 .0014 .0003 .0003 .01 %RSD 1734.4 2.024 3058.8 7.253 . .7568 39.83 .0502 #1 .31758 .3609 -.36629 .0215 .0383 .0010 20.33 #2 .46288 .3560 .21066 .0191 .0380 .0007 20.35 ##3 -.67349 .3468 .18767 .0189 .0377 .0004 20.33 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0008 .0014 .0026 .0037 .4486 3.559 8.455 SDev .0004 .0002 .0003 .0004 .0067 .007 .010 %RSD 50.08 16.36 9.475 11.99 1.494 .1935 .1179 #1 .0012 .0013 .0029 .0042 .4553 3.551 8.466 ##2 .0008 .0017 .0026 .0034 .4487 3.562 8.452 ##3 .0004 .0014 .0024 .0034 .4419 3.564 8.447 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb .15,73 .0044 14.68 .0035 6.7073 .46843 .53470 r .0003 .0020 .02 .0006 1.6936 2.8763 1.1548 6x6D .1744 45.01 .1481 17.05 25.251 614.03 215.98 #1 .1575 .0062 14.67 .0034 6.2005 -.48938 1.3402 #2 .1574 .0047 14.68 .0029 5.3249 3.7014 1.0523 #3 .1570 .0023 14.71 .0041 8.5965 -1.8068 -.78837 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 2.5653 -1.3559 .73951 6.910 .0014 .0888 .0233 SDev 2.5917 2.2805 3.1559 .005 .0007 .0003 .0002 %RSD 101.03 168.19 426.76 .0689 47.19 .3312 .8452 #1 5.1783 1.0510 .32105 6.915 .0009 .0891 .0235 #2 2.5222 -3.4844 -2.1863 6.907 .0021 .0887 .0232 #3 -.00452 -1.6342 4.0838 6.907 .0012 .0885 .0231 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.55008 .0018 .2191 2.5461 1.8892 .04179 SDev 1.52792 .0006 .0005 1.4694 2.0866 2.4414 %RSD 277.76 32.24 .2368 57.711 110.45 5841.5 #1 -.91312 .0024 .2196 1.7385 3.9002 .56.417 #2 -1.8638 .0018 .2191 4.2422 2.0327 -2.6185 #3 1.1267 .0012 .2186 1.6577 -.26550 2.1797 00 00 N O Analysis Report 12/14/07 12:05:17 PM page 1 M-`'-od: CLP1 Sample Name: 07137717002D Operator: CO F Time: 12/14/07 11:57:25 C�«««ent : I -A l� Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.18478 .9083 1.7704 .0262 .0753 .0001 8.996 SDev .17305 .0030 .3672 .0005 .0001 .0000 .026 %RSD 93.652 .3322 20.740 1.815 .1011 18.58 .2864 #1 -.10963 .9116 1.8614 .0259 .0754 .0002 9.022 #2 -.06201 .9075 1.3662 .0267 .0752 .0001 8.971 #3 -.38271 .9057 2.0834 .0258 .0753 .0001 8.995 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0015 .1330 .0061 2.431 2.606 5.871 SDev .0002 .0002 .0006 .0003 .005 .011 .016 %RSD 78.05 15.30 .4621 5.678 .1912 .4209 .2729 #1 .0001 .0017 .1338 .0064 2.436 2.610 5.887 #2 .0003 .0013 .1327 .0057 2.426 2.593 5.855 #3 .0005 .0014 .1326 .0062 2.431 2.613 5.872 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .1136 .0029 38.02 .0123 5.5979 -.82180 -.54580 v .0004 .0004 .11 .0011 1.4519 1.44883 1.34772 %RSD .3715 14.77 .2888 8.713 25.935 176.30 246.93 #1 .1140 .0033 38.15 .0117 5.1565 .74035 -1.7763 #2 .1132 .0024 37.96 .0117 4.4180 -1.0843 .89452 #3 .1136 .0030 37.96 .0135 7.2192 -2.1214 -.75559 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 2.0584 -.49326 .76580 5.177 -.0008 .0590 .0532 SDev .9256 4.25186 1.2244 .009 .0019 .0001 .0001 %RSD 44.965 861.99 159.88 .1710 246.7 .1944 .2264 #1 3.0473 .72972 -.22529 5.186 -.0004 .0592 .0533 #2 1.2129 -5.2226 .38818 5.169 -.0028 .0589 .0531 #3 1.9151 3.0131 2.1345 5.175 .0009 .0590 .0532 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.8628 .0026 .0332 1.3161 1.1912 .34657 SDev .4365 .0004 .0000 .7844 .2201 1.9660 %RSD 23.434 17.00 .0924 59.597 18.477 567.27 #1 -2.1666 .0031 .0332 2.2111. 1.4411 .09276 #2 -2.0593 .0025 .0332 .74811 1.1069 -1.4802 *-4 -1.3626 .0022 .0.332 .98917 1.0258 2.4271 Analysis Report 12/14/07.12:12:40 PM page 1 ad: CLP1 Sample Name: 0713771-003D Operator: CO Time: 12/14/07 12:05:23 Co ment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1.0787 .0291 1.2541 .7460 .2124 .0001 163.3 SDev .2139 .0023 .8221 .0022 .0006 .0000 .4 %RSD 19.828 7.881 65.557 .2936 .3017 1.301 .2422 #1 .91454 .0308 .55835 .7485 .2131 .0001 163.7 #2 1.3205 .0300 1.0425 .7446 .2118 .0001 163.0 #3 1.0009 .0265 2.1613 .7448 .2123 .0001 163.1 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0184 .0007 .0073 .3962 78.66 71.54 SDev .0.001 .0003 .0003 .0004 .0012 .11 .19 %RSD 74.78 1.404 39.34 5.723 .3052 .1381 .2685 #1 -.0000 .0185 .0008 .0072 .3976 78.77 71.75 #2 -.0002 .0181 .0004 .0069 .3955 78.55 71.38 #3 -.0001 .0185 .0009 .0077 .3956 78.65 71.48 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb 3.621 .0013 241.7 .0473 1.6958 .00389 .63621 0e v .009 .0003 .4 .0003 2.2056 1.2115 2.5609 %RSD .2624 25.15 .1465 .6662 130.07 31159. 402.53 #1 3.632 .0014 242.0 .0476 1.9266 -.50154 -.92383 #2 3.613 .0015 241.3 .0474 -.61617 1.3863 3.5918 #3 3.619 .0009 241.8 .0470 3.7770 -.87308 -.75931 Elem. 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.93331 -.89550 1.5654 9.157 -.0002 .7265 .0033 SDev 2.43273 2.•01147 1.4867 .023 .0010 .0018 .0001 -'.RSD 260.65 224.62 94.968 .2555 462.7 .2533 4.238 #1 1.5236 -1.2165 1.4296 9.183 -.0002 .7286 .0033 #2 -.98234 -2.7272 .15134 9.138 -.0012 .7251 .0032 #3 -3.3412 1.2572 3.1154 9.149 .0008 .7258 .0034 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.60607 .0002 -.0004 .56737 -.41065 .74597 SDev 1.37606 .0002 .0001 .22647 1.79525 1.6607 %RSD 227.05 107.3 28.09 39.915 437.17 222.63 #1 .62666 .0001 -.0004 .30711 .70858 .54850 #2 -2.0907 .0003 -.0005 .71954 .54084 -.80721 4* -.35418 .0001 -.0003 .67546 -2.4814 2.4966 Analysis Report 12/14/07 12:28:09 PM page 1 M- -hod: CLP1 Sample Name: 0713771-004D Operator: CO F Time: 12/14/07 12:20:55 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1.9719 .3377 -.29145 .1396 .1212 .0001 49.82 SDev .0922 .0012 1.85974 .,0011 .0005 .0000 .23 %RSD 4.6763 .3514 638.09 .7825 .4304 39.88 .4547 #1 1.8671 .3391 .67863 .1408 .1218 .0001 50.06 #2 2.0080 .3368 .88268 .1395 .1210 .0001 49.78 #3 2.0406 .3372 -2.4357 .1386 .1208 .0000 49.62 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0031 .0085 .0058 .9297 48.58 22.67 SDev .0001 .0002 .0001 .0004 .0041 .28 .10 %RSD 95.73 5.607 1.660 7.078 .4455 .5712 .4497 #.1 .0001 .0029 .0085 .0062 .9343 48.90 22.79 #2 .0003 .,0032 .0085 .0059 .9284 48.46 22.65 #3 .0000 .0031 .0083 .0054 .9263 48.39 22.59 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb - e 11.12 -.0000 18.85 .0114 3.9135 1.2263 .52930 v .05 .0002 .12 .0010 .3245 .4621 1.8976 6vcoD .4663 355.4 .6250 8.763 8.2912 37.685 358.50 #1 11.17 .0001 18.99 .0119 4.1281 .85297 -.77991 #2 11.10 -.0002 18.81 .0120 4.0721 1.0827 -.33766 #3 11.07 -.0001 18.76 .0102 3.5402 1.7431 2.7055 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.63511 -.85369 3.4518 4.351 -.0001 .1380 .0220 SDev 2.45390 2.18344 4.4224 .022 .0015 .0009 .0002 %RSD 386.38 255.76 128.12 .5134 1501. .6741 .8428 #1 -.15822 1.6665 8.2390 4.376 -.0018 .1391 .0221 #2 -3.2924 -2.0504 -.48104 4.344 .0009 .1374 .0221 #3 1.5453 -2.1771 2.5973 4.333 .0007 .1375 .0218 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.7264 .0011 -.0118 2.1212 -.24732 2.0181 SDev 1.8759 .0003 .0000 .2024 2.12254 3.6340 %RSD 108.66 27.54 .1382 9.5431 858.22 180.07 ##1 -.23102 .0014 -.0118 1.9437 -.36520 6.0504 #2 -1.1169 .0012 -.0118 2.0783 -2.3085 -1.0036 #3 -3.8312 .0008 -.0118 2.3416 1.9317 1.0075 Analysis Report 12/14/07 12:35:29 PM page 1 M -')d: CLP1 Sample Name: 0713771-005D Operator: CO R Pime: 12/14/07 12:28:15 Comment:- Mode: CONC Corr. Factor: 1 r Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 2.1019 .0195 -1.1775 .5201 .1755 .0000 102.0 SDev .2039 .0031 1.3759 .0036 .0010 .0000 .6 %RSD 9.6993 16.08 116.85 .6959 .5919 82.33 .6003 #1 1.9309 .0195 -.47453 .5184 .1751 .0000 101.9 #2 2.0472 .0163 -2.7629 .5177 .1748 .0000 101.4 #3 2.3275 .0226 -.29518 .5243 .1767 .0001 102.6 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0203 .0016 .0140 .0676 117.5 48.22 SDev .0001 .0004 .0002 .0003 .0007 .8 .30 %RSD 124.3 1.976 10.93 2.439 1.057 .6654 .6176 #1 .0000 .0205 .0018 .0139 .0679 117.1 48.20 42 -.0002 .0198 .0015 .0138 .0668 116.9 47.94 #3 -.0001 .0205 .0016 .0144 .0681 118.4 48.53 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ,e 11.38 .0003 247.2 .0540 3.7442 .12898 -1.1593 v .07 .0002 1.6 .0005 2.7984 1.3113 2.6579 %RSD .5814 54.77 .6431 .8983 74.739 1016.7 229.28 #1 11.37 .0001 246.7 .0543 6.8835 -1.1396 -4.1852 #2 11.32 .0005 246.0 .0535 2.8376 1.4792 .79772 #3 11.45 .0004 249.0 .0543 1.5116 .04732 -.09028 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.18908 .73925 2.9842 6.118 -.0012 .6261 .0030 SDev 1.44727 .91246 2.2208 .039 .0001 .0037 .0001 %RSD 765.43 123.43 74.419 .6438 8.214 .5856 4.768 #1 1.2170 .98697 .42181 6.106 -.0012 .6254 .0029 #2 -1.6743 -.27148 4.3529 6.086 -.0013 .6229 .0029 #3 -.10996 1.5023 4.1778 6.162 -.0012 .6301 .0031 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .43860 .0000 -.0066 1.3329 -.51211 2.2366 SDev 1.3073 .0004 .0000 .7193 .37871 1.4285 %RSD 298.05 6277. .5977 53.962 73.950 63.867 #1 1.1138 -.0001 -.0066 1.5322 -.58189 .61001 #2 -1.0682 -.0004 -.0066 1.9316 -.85107 2.8130 fl -I 1.2702 .0005 -.0065 .53504 -.10336 3.2868 Analysis Report 12/14/07 12:42:49 PM page 1 M-^*-'-,od: CLP1 Sample Name: 0713771-006D Operator: CO R Cime: 12/14/07 12:35.35 C. ....... �nt : , _ �J S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B - Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .55266 .0558 .92750 .0498 .0735 .0001. 14.01 SDev .22257 .0060 1.0740 .0018 .0024 .0000 .47 %RSD 40.273 10.70 115.79 3.683 3.249 16.51 3.368 #1 .66744 .0583 .56493 .0509 .0748 .0001 14.28 #2 .29613 .0602 2.1358 .0508 .0750 .0001 14.30 #3 .69442 .0490 .08176 .0477 .0708 .0001 13.47 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0011 .0030 .0024 .0680 6.287 9.497 SDev .0001 .0006 .0005 .0009 .0027 .214 .315 %RSD 128.6 47.54 17.06 37.85 4.019 3.402 3..321 #1 .0002 .0017 .0032 .0030 .0695 6.424 9.671 #2 .0001 .0012 .0033 .0029 .0696 6.397 9.686 #3 -.0000 .0006 .0024 .0014 .0648 6.041 9.133 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb 2.890 .0000 11.90 .0105 3.5356 -.13119 -1.3706 r .095 .0002 .38 .0006 1.5028 .97108 1.8432 6xbD 3.287 1247. 3.199 5.8.64 42.504 740.20 134.48 #1 2.943 .0001 12.13 .0103 2.2508 .89643 .61766 #2 2.947 -.0002 12.11 .0112 3.1680 -.25643 -3.0224 #3 2.781 .0002 11.46 .0100 5.1881 -1.0336 -1.7071 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm - ppm ppm ppm Avge -.15253- -.80908 2.2383 6.096 -.0000 .0786 .0031 SDev 2.17940 1.51656 4.4723 .194 .0001 .0027 .0001 %RSD 1428.9 187.44 199.81 3.188 1082. 3.443 3.018 #1 1.6451 -1.3482 6.7570 6.201 -.0001 .0802 .0032 #2 .47383 .90339 2.1439 6.215 .0001 .0800 .0031 #3 -2.5765 -1.9824 -2.1861 5.872 -.0000 .0754 .0031 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .50740 .0001 .0033 1.0899 -.55812 1.2235 SDev 1.9259 .0003 .0002 .2360 1.79865 3.1192 %RSD 379.57 315.3. 4.919 21.655 322.27 254.93 #1 .91700 .0003 - 0034 1.3475 1.3030 4.0580 #2 -1.5904 .0002 .0033 .88400 -.69038 1.7309 #3 2.1955 -.0002 .0031 1.0383 -2.2870 -2.1182 Analysis Report 12/14/07 12:50:09 PM page 1 N ' :)d: CLP1 Sample Name: 0713771-007D Operator: CO R Time: 12/14/07 12:42:55 Comment: - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .01800 .0242 3.9043 .4091 .0813 .0001 68.67 SDev .65214 .0044 1.9355 .0013 .0002 .0000 .26 0 -.RSD 3622.5 18.07 49.573 .3285 .2124 15.70 .3823 #1 .33994 .0272 5.9346 .4096 .0814 .0001 68.78 #2 .44657 .0261 3.6981 .4102 .0815 .0001 68.86 #3 -.73251 .0192 2.0802 .4076 .0812 .0001 68.37 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0002 .0072 .0007 .0022 8.908 81.28 34.50 SDev .0002 .0005 .0006 .0005 .023 .19 .07 %RSD 129.5 7.221 83.56 22.58 .2579 .2349 .2113 #1 -.0002 .0075 .0010 .0026 8.912 81.06 34.50 #2 .0001 .0075 .0010 .0025 8.929 81.42 34.57 #3 -.0004 .0066 .0000 .0016 8.883 81.35 34.42 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e 1.405 .0008 80.86 .0079 2.8020 -.59205 .11950 v ..004 .0006 .22 .0005 1.0568 .25355 1.1745 %RSD .3181 71.84 .2701 6.676 37.716 42.825 982.83 #1 1.406 .0008 80.65 .0084 2.4107 -.45814 1.4532 #2 1.408 .0013 81.08 .0074 1.9966 -.88448 -.33466 #3 1.400 .0002 80.86 .0077 3.9986 -.43353 -.76008 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.1374 -2.6150 .40901 10.34 -.0009 .4164 .0024 SDev 1.8716 1.9991 1.9766 .02 .0010 .0007 .0002 %RSD 164.54 76.446 483.26 .1639 120.3 .1763 8.095 #1 -.14980 -2.2510 -.17441 10.33 .0003 .4159 .0025 #2 .27772 -.82298 -1.2102 10.35 -.0012 .4172 .0026 #3 3.2844 -4.7711 2.6116 10.32 -.0017 .4160 .0022 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -2.0192 .0005 .0026 .53825 79849 -.59797 SDev 1.8031 .0006 .0001 .48502 .99864 .65940 0 -.RSD 89.298 102.1 3.859 90.112 125.07 110.27 #1 -3.1177 .0009 .0027 .49727 .38402 -.86591 #2 .06175 .0008 .0027 .07501 .07384 -1.0812. -? -3.0015 -.0001 .0025 1.0425 1.9376 .15323 Analysis Report 12/14/07 12:57:29 PM page 1 P,-`'-od: CLP1 Sample Name: 0713771-007DDUP Operator: CO I Time: 12/14/07 12:50:15 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .38260 .0318 3.0682 .4215 .0839 .0001 71.21 SDev .44991 .0024 1.2092 .0006 .0001 .0000 .09 %RSD 117.59 7.412 39.413 .1300 .1726 28.39 .1319 #1 .80197 .0307 2.8279 .4212 .0839 .0001 71.31 #2 -.09264 .0345 4.3795 .4221 .0839 .0001 71.12 #3 .43846 .0303 1.9971 .4211 .0841 .0001 71.20 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0003 .0072 .0009 .0019 9.241 83.70 35.83 SDev .0002 .0004 .0006 .0004 .007 .12 .04 %RSD 65.98 6.083 59.69 18.39 .0801 .1460 .1189 #1 -.0004 .0072 .0011 .0016 9.249 83.69 35.88 #2 -.0003 .0068 .0003 .0019 9.235 83.58 35.79 #3 -.0001 _0077 .0013 .0023 9.240 83.83 35.83 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb je 1.453 .0010 83.21 .0082 1.6146 -.98524 .88755 :v .001 .0005 .25 .0006 1.9193 1.59662 1.8407 %RSD .0909 47.84 .3026 6.970 118.87 162.05 207.39 #1 1.455 .0013 83.22 .0080 .37143 -.81553 .62739 #2 1.452 .0013 82.95 .0077 .64725 .51975 2.8445 #3 1.453 .0005 83.45 .0088 3.8251 -2.6599 -.80923 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .01475 2.1701 .35213 10.89 -.0017 .4295 .0021 SDev 1.8530 .7294 1.1397 .01 .0004 .0004 .0003 %RSD 12559. 33.611 323.65 .1057 26.82 .1024 13.94 #1 -1.3301 1..4015 1.6312 10.90 -.0014 .4293 .0022 #2 -.75403 2.2561 -.55526 10.88 -.0014 .4292 .0018 #3 2.1284 2.8527 -.01960 10.89 -.0022 .4300 .0024 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .74197 .0005 .0039 -.11941 .30543 -.95755 SDev 2.1886 .0003 .0001 .59173 .92207 .58717 %RSD 294.97 59.48 1.789 495.53 301.89 61.320 #1 .68081 .0005 .0039 -.42020 -.67820 1.5548 #2 -1.4154 .0002 .0038 .56229 .44432 .38098 #� 2.9605 .0008 .0039 -.50033 1.1502 .93691 .I Analysis Report 12/14/07 01:04:49 PM page 1 r M-`'Dd: CLP1 Sample Name: CCV3 Operator: CO R Cime: 12/14/07 12:57:35 ' I Mode: CONC Corr. Factor: 1 i Elem Ag Al As1890 B Ba Be Ca j Units ppb ppm ppb ppm ppm ppm ppm Avge 1057.2 49.82 503.38 2.504 2.553 2.492 48.89 SDev 1.8 .05 2.14 .002 .004 .004 .06 %RSD .17364 .0929 .42566 .0913 .1664 .1415 .1150 t F #1 1055.3 49.76 503.58 2.501 2.548 2.490 48.87 I #2 1058.9 49.84 501.15 2.504 2.556 2.496 48.95 #3 1057.4 49.84 505.42 2.506 2.556 2.490 48.85 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low_ 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg I i Units ppm ppm ppm ppm ppm ppm ppm i Avge 2.449 2.439 2.464 2.575 49.43 85.92 50.51 SDev .003 .003 .003 .005 .04 .04 .06 %RSD .1087 .1180 .1137 .1777 .0775 .0424 .1227 t ##1 2.448 2.439 2.462 .2.570 49.42 85.90 50.48 #2 2.452 2.443 2.467 2.577 49.39 85.97 50.59 2.447 2.437 2.464 2.578 49.47 85.91 50.48 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.467 2.449 83.60 2.477 483.28 485.20 975.96 SDev .002 .007 .09 .003 3.20 3.01 5.69 %RSD .1001 .2962 .1066 .1399 .66144 .62015 .58262 .#1 2.465 2.440 83.60 2.473 484.52 486.48 969.39 #2 2.470 2.451 83.70 2.480 485.67 487.35 979.18 #3 2.467 2.454 83.52 2.478 479.65 481.76 979.30 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 993.80 513.69 507.03 2.322 2.386 2.479 2.447 SDev 2.09 4.31 4.05 .003 .006 .003 .003 %RSD .20997 .83835 .79808 .1493 .2579 .1154 .1360 N O #1 995.42 516.28 506.12 2.324 2.386 2.476 2.443 991.45 516.08 511.46 2.325 2.392 2.481 2.450 994.54 508.72 503.52 2.318 2.380 2.481 2.44.8 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 01:04:49 PM h Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 499.56 2.469 2.565 484.56 987.86 509.25 SDev 2.46 .003 .002 3.07 1.42 3.88 0-oRSD .49310 .1407 .0904 .63377 .14422 .76153 #1 497.16 2.465 2.563 485.83 986.75 509.50 #2 499.44 2.470 2.567 486.79 987.36 512.99 #3 502.08 2.471 2.563 481.06 989.47 505.25 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 12/14/07 01:12:10 PM page 1 M-`'-Dd: CLP1 Sample Name: CCVL3 Operator: CO R Pime: 12/14_/07 13:04:56 CUIUMe'nt : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .46237 .0378 1.9749 .0026 .0008 .0008 .0200 SDev .56136 .0048 .7508 .0006 .0002 .0002 .0063 %RSD 121.41 12.7-31 38.015 23.78 27.67 24.80 31.53 #1 .39457 .0427 2.7512 .0033 .0010 .0009 .0268 #2 -.06201 .0377 1.2526 .0023 .0007 .0007 .0187 #3 1.0546 .0331 1.9211 .0022 .0006 .0006 .0144 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0002 -.0004 .0035 2.499 .0632 .0129 SDev .0003 .0001 .0001 .0006 .049 .0095 .0026 oRSD 42.61 40.85 14.63 16.26 1.953 15.10 20.22 #1 .0009 .0001 -.0004 .0040 2.545 .0736 .0139 #2 .0005 .0003 -.0004 .0035 2.504 .0611 .0149 .0004 .0003 -.0005 .0029 2.448 .0548 .0099 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 i Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0007 .0052 2.606 -.0012 -1.6848 1.0321 3.8883 j SDev .0003 .0023 .054 .0005 2.2235 .9338 1.2948 %RSD 34.80 45.04 2.065 46.51 131.98 90.471 33.300 41 .0010 .0078 2.658 -.0017 -1.682.7 2.0744 5.2325 i #2 .0007 .0045 2.610 -.0006 .53771 .74994 2.6493 #3 .0005 .0032 2.550 -.0011 -3.9094 .27197 3.7830 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti i Units ppb ppb ppb ppm ppm ppm ppm 00 Avge 3.2925 6.2435 -.79852 .0134 -.0012 .0009 .0008 SDev 2.4423 1.6778 1.10171 .0053 .0016 .0002 .0004 %RSD 74.177 26.873 137.97 39.19 127.4 27.39 43.69 N O ftl 4.8780 5.0893 -.04804 .0173 -.0005 .0011 .0012 4.5196 8.1682 -2.0633 .0155 -.0030 3 .48002 5.4729 -.28418 .0074 -.0002 .0008 .0007 .0009 .0004 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 01:12:10 PM page 2 01 Elem T11908 Units ppb Avge 1.9021 SDev 2.6623 %RSD 139.97 #1 1.2909 #2 4.8170 #3 -.40141 Errors NOCHECK High .0005 Low 1.0830 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0005 .0111 .12746 3.4910 1.5465 .0005 .0005 1.0830 1.7439 .1762 103:2 4.791 849.72 49.954 11.392 .0008 .0117 .82337 4.9961 1.6627 -.0001 .0109 .67935 3.8969 1.3438 .0008 .0106 -1.1203 1.5799 1.6330 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report r4-"iod: CLP1 Sample Name: CCB3 I Time: 12/14/07 13:12:16 Be (_._tent: PPM ppm Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .38082 .0256 1.9048 SDev .32647 .0011 1.4075 %RSD 85.728 4.156 73.892 #1 .72503 .0244 2.3299 #2 .34184 .0260 .33373 #3 .07559 .0265 3.0507 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge .0002 -.0001 -.0006 SDev .0001 .0004 .0003.. %RSD 83.40 309.6 53.04 #1 .0002 -.0003 -.0009 #2 .0000 .0003 -.0008 .0448 .0003 -.0003 -.0003 Errors LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem. Mn Mo Na Units ppm ppm ppm Avge .0001 .0008 .0282 SDev .0001 .0005 .0017 %RSD 124.5 62.65 6.122 #1 .0002 .0015 .0301 #2 -.0000 .0005 .0278. #3 .0001 .0005 .0267 Errors LC Pass NOCHECK LC Pass High .0150 -.03831 5.000 Low -.0150 -.0011 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge .59752 6.1718 -2.4451 SDev 2.5300 3.6768 1.7434 %RSD 423.42 59.574 71.301 #1 -.97370 7.5742 -.83204 Sn 3.5161 2.0002 -4.2946 ppm -.74982 8.9411 -2.2085 Errors NOCHECK NOCHECK NOCHECK 12/14/07 01:19:30 PM page 1 Operator: CO B Ba- Be Ca PPM ppm ppm ppm ..0002 .0002 .0002 .0010 0009 .0000 .0000 .0015 526.0 9.476 11.40 150.2 .0001 .0002 .0003 .0028 .0011 .0002 .0002 .0001 -.0007 .0002 .0002 .0001 LC Pass LC Pass LC Pass LC Pass .2000 .2000 .0050 .2000 -_2000 -.2000 -.0050 -.2000 Cu Fe K Mg ppm ppm ppm ppm -.0008 .0030 .0423 .0020 .0001 .0010 .0036 .0007 10.16 34.46 8.604 33.15 -.0009 .0040 .0448 .0014 -.0008 .0029 .0381 .0019 -.0007 .0020 .0439 .0027 LC Pass LC Pass LC Pass LC Pass .0250 .1000 5.000 .2000 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb -.0007 -.13800 -.44311 -1.1988 .0004 .80080 3.80162 .5021 49.91 580.29 857.93 41.884 -.0007 -.03831 3.6246 -1.6928 -.0011 -.9.8397 -3.9061 -.68902 -.0004 .60828 -1.0479 -1.2144 LC Pass NOCHECK NOCHECK NOCHECK .0400 j -.0400 Si Sn Sr Ti O ppm ppm ppm ppm O -.0122 .0002 .0002 .0001 .0018 .0014 .0000 .0001 15.15 708.6 15.89. 36.52 N O -.0116 .0017 .0002 .0002 -.0107 -.0006 .0001 .0001 -.0142 -.0006 .0002 .000.2 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 01:19:30 PM 'h Elem T11908 v Zn Pb2203_ Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .90731 -.0000 .0016 -.34143 -.00060 .42440 SDev 2.2737 .0003 .0002 2.67233 1.83936 2.2832 %RSD 250.60 768.9 12.33 782.68 306050. 537.98 #1 -1.5374 -.0002 .0015 2.4050 -1.2131 1.9673 #2 1.3008 .0003 .0014 -2.9330 2.1158 -2.1984 #3 2.9586 -.0002 .0018 -.49629 -.90449 1.5043 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 12/14/07 01:28:30 PM page 1 Y-`'-Dd: CLP1 Sample Name: 0713771-007DMS Operator: CO R Time: 12/14/07 13:21:15 C�««<<znt : - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 50.332 2.037 42.882 .4234 2.137 .0491 71.38 SDev .555 .002 1.136 .0010 ..001 .0000 .02 %RSD 1.1023 .0972 2.6489 .2427 .0400 .0549 .0223 #1 50.036 2.036 42.098 .4230 2.137 .0491 71.36 #2 50.972 2.037 44.184 .4245 2.138 .0491 71.39 #3 49.988 2.039 42.363 .4226 2.137 .0491 71.39 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0482 .4907 .1971 .2656 10.28 84.39 35.94 SDev .0001 .0007 .0001 .0004 .00 .17 .03 %RSD .2274 .1438 .0424 .1562 .0424 .2006 .0935 #1 .0483 .4909 .1971 .2653 10.28 84.22 35.93 #2 .0481 .4913 .1972 .2661 10.29 84.40 35.98 #3 .0483 .4899 .1971 .2656 10.28 84.56- 35.92 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb 1.947 -.0006 83.72 .4994 21.274 18.301 501.98 v .001 .0001 .15 .0008 2.123 .465 1.64 %RSD .0361 21.61 .1798 .1517 9.9798 2.5431 .32715 #1 1.947 -.0005 83.62 .4990 20.822 18.826 500.46 #2 1.948 -.0006 83.90 .5002 19.414 17.940 503.72 #3 1.947 -.0007 83.65 .4988 23.587 18.136 501.75 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb - ppm ppm ppm ppm Avge 510.10 11.766 10.561 10.93 -.0009 .4316 .0023 SDev 2.83 3.290 .930 .01. .0021 .0003 .0002 %RSD 55509 27.957 8.8075 .0771 228.6 .0630 9.734 #1 508.00 15.390 10.214 10.92 -.0003 ..4319 .0021 ##2 513.32 8.9674 11.615 10.94 -.0033 .4315 .0026 #3 508.99 10.942 9.8544 10.93 .0008 .4314 .0022 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 47.185 .4935 .5261 19.291 507.40 10.962 - SDev .496 .0008 .0005 .780 2.42 .883 %RSD 1.0518 .1510 .0889 4.0414 .47788 8.0545 #1 46.613 .4926 .5257 19.490 505.49 11.937 #2 47.441 .4940 .5266 18.431 510.13 10.733 #3 47.501 .4939 .5260 19.951 506.58 10.216 Analysis Report 12/14/07 01:35:51 PM page 1 M-" od: CLP1 Sample Name: 0713771-007DSD Operator: CO R rime: 12/14/07 13:28:36 C -....ant : Mode: CONC Corr. Factor: 1 Kkw - Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .32512 .0287 2.1909 .0862 .0180 .0001 14.63 SDev 61761 .0022 1.7327 .0004 .0004 .0000 .03 %RSD 189.96 7.534 79.089 .5214 2.233 12.22 .2293 #1 .31963 .0310 1.0130 .0867 .0184 .0001 14.65 #2 -.28972 .0285 1.3791 .0859 .0181 .0001 14.59 #3 .94545 .0267 4.1805 .0859 .0176 .0001 14.66 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0017 -.0005 -.0001 1.867 14.91 7.319 SDev .0002 .0001 .0004 .0006 .003 .01 .009 %RSD 166.9 8.170 75.90 492.1 .1419 .0978 .1221 #1 .0001 .0018 -.0002 .0005 1.869 14.92 7.319 #2 -.0003 .0016 -.0009 -.0007 1.864 14.92 7.310 #3 -.0001 .0015 -.0004 -.0002 1.868 14.89 7.328 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb .3003 .0003 16.93 .0012 -.18997 -1.2751 .45275 7 .0005 .0003 .03 .0003 2.01944 1.2032 1.7344 6XSD .1617 98.65 .1674 29.34 1063.0 94.364 383.07 #1 .3007 .0001 16.91 .0016 1.4332 -.51587 -1.5346 #2 .2998 .0006 16.96 .0010 .44826 -2.6624 1.2321 #3 .3005 .0001 16.93 .0009 -2.4514 -.64701 1.6607 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.0087 4.3899 -2.3816 2.241 -.0022 .0849 .0006 SDev 1.1129 1.5449 3.5491 .002 .0015 .0001 .0001 %RSD 36.991 35.191 149.02 .1105 64.65 .0900 8.976 #1 2.4833 6.1033 -3.4093 2.242 -.0039 .0850 .0006 #2 4.2870 3.9629 -5.3034 2.238 -.0015 .0849 .0005 #3 2.2557 3.1034 1.5680 2.243 -.0013 .0849 .0006 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.2158 .0002 .0027 -.91367 2.1576 -.12666 SDev .3572 .0007 .0002 .92622 1.0657 2.15081 %RSD 16.118 424.1 7.811 101.37 49.394 1698.1 #1 2.6190 .0002 .0029 .13326 1.1454 -.24161 #2 2.0896 -.0005 .0025 -1.6265 3.2698 -2.2177 #3 1.9389 .0008 .0028 -1.2478 2.0576 2.0793 Analysis Report 12/14/07 01:43:12 PM page 1 I" ''od: CLP1 Sample Name: 0713771-008D Operator: CO ] Time: 12/14/07 13:35:57 cuutment : Mode: CONC Corr. Factor: 1�J - SS Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.05484 .8427 5.3152 .2798 .1556 .0002 37.74 SDev .20800 .0036 .4081 .0005 .0001 .0000 .08 %RSD 379.29 .4251 7.6784 .1744 .0879 7.548 .2230 #1 -.18749 .8468 4.8441 .2802 .1558 .0002 37.81 #2 .18488 .8401 5.5384 .2793 .1555 .0002 37.77 #3 -.16191 .8413 5.5630 .2799 .1555 .0002 37.65 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0019 .0036 .0072 24.94 54.63 15.80 SDev .0001 .0001 .0001 .0002 .05 .13 .02 %RSD 115.6 5.230 3.001 2.879 .1861 .2303 .1154 #1 -.0000 .0019 .0036 .0073 24.97 54.77 15.81 #2 -.0000 .0021 .0038 .0072 24.97 54.54 15.81 #3 -.0002 .0019 .0035 .0069 24.89 54.57 15.78 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .1517 .0003 31.45 .0028 6.1342 -2.2845 -.51086 w .0005 .0002 .19 .0002 .2643 .9339 .16110 %RSD .3476 83.52 .5886 8.397 4.3080 40.880 31.535 #1 .1522 .0004 31.65 .0030 6.4232 -1.4915 -.60670 #2 .1518 .0000 31.29 .0026 6.0746 -3.3139 -.32487 #3 .15.12 .0003 31.42 .0028 5.9048 -2.0480 -.60102 j Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.1861 1.2698 -3.0090 8.484 -.0020 .2061 .0436 SDev 3.6420 1.6654 1.4745 .004 .0015 .0001 .0002 %RSD 307.06 131.15 49.002 .0421 73.15 .0403 .3846 #1 -4.7639 2.5375 -4.7113 8.488 -.0036 .2060 .0438 #2 2.5169 -.61637 -2.1827 8.484 -.0006 .2060 .0435 #3 -1.3112 1.8884 -2.1330 8.481 -.0020 .2061 .0435 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.3651 .0043 .0099 .51905 -.96119 -1.5841 SDev 1.0834 .0004 .0001 .66951 2.47701 .7548 O %RSD 79.363 10.33 .5275 128.99 257.70 47.646 #1 -1.6358 .0047 .0099 1.1442 -3.3795 -2.2974 #2 -2.2874 .0038 .0099 -.18741 1.5706 -1.6611 O -.17203 .0044 .0100 .60038 -1.0747 -.79381 i Analysis Report 12/14/07 01:50:36 PM page 1 M 'od: CLP1 Sample Name: 0713771-009D . - Operator: CO F Time: 12/14/07 13:43:19 Comment: �- �, 1-?- C) 0-4 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.30144 .0335 -.17280 -.0005 -.0004 .0001 .0959 SDev .07723 .0007 1.47637 .0002 .0001 .0000 .0083 %RSD 25.619 2.190 854.39 45.93 31.45 18.90 8.677 #1 -.38890 .0343 -1.1419 -.0004 -.0002 .0001 .1045 ##2 -.24264 .0329 -.90287 -.0003 -.0004 .0001 .0955 #3 -.27278 .0334 1.5264 -.0007 -.0005 .0001 .0879 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0002 -.0006 -.0000 -.0006 .0284. .0875 .0083 SDev .0002 .0004 .0005 .0003 .0053 .0303 .0076 %RSD 67.40 78.27 1110. 54.31 18.61 34.59 90.53 #1 -.0001 -.0001 .0005 -.0002 .0341 .1221 .0165 #2 -.0004 -.0008 -.0005 -.0007 .0276 .0749 .0068 #3 -.0003 -.0008 -.0002 -.0009 .0236 .0656 0017 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e .0000 .0001 .0629 -.0006 1.9766 -.21571 -.35661 v .0002 .0004 .0080 .0003 1.2712 2.30105 1.70578 %RSD 579.8 262.9 12.72 51.99 64.313 1066.7 478.34 ##1 .0003 .0004 .0714 -.0003 3.0817 -2.8603 -1.3207 #2 -.0001 -.0003 .0617 -.0007 2.2607 1.3293 -1.3621 #3 -.0001 .0004 .0556 -.0009 .58736 .88382 1.6129 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb- ppb ppm ppm ppm ppm Avge -1.3832 -3.6859 1.0866 .0520 -.0011 .0001 .0017 SDev 1.1578 2.5209 2.7711 .0048 .0020 .0001 .0003 %RSD 83.707 68.394 255.03 9.253 191.2 127.8 14.85 ##1 -.18310 -5.4630 3.7467 .0567 .0012 .0002 .0020 #2 -2.4936 -4.7939 1.2965 .0521 -.0026 .0000 .0015 #3 -1.4730 -.80072 -1.7835 .0471 -.0018 .0000 .0017 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -2.3569 .0001 .0066 .51440 -1.0413 -.50262 SDev 2.0510 .0002 .0002 1.2822 .9332 1.08632 %RSD 87.021 111.2 2.497 249.26 89.614 216.13 ##1 -4.3531 .0001 .0064 -.88153 -.56188 .67993 #2 -.25509 .0003 .0067 1.6395 -2.1167 -.73159 4+q -2.4626 .0001 .0066 .78517 -.44533 -1.4562 Analysis Report 1.2/14/07 01:57:57 PM Method: CLP1 Sample Name: 0713817-001D Operator: CO F Time: 12/14/07 13:50:42 C ent: Mode: CONC Corr. Factor: 1 t�W Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .89092 .0442 4.8762 .8592 .1855 .0001 SDev .29783 .0075 .8508 .0325 .0075 .0000 %RSD 33.430 17.06 17.447 3.785 4.016 5.438 #1 .60485 .0503 4.7212 .8774 .1898 .0001 #2 .86863 .0465 5.7938 .8786 .1898 .0001 #3 1.1993 .0358 4.1136 .8217 .1769 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge -.0002 .0311 .0020 .0019 6.873 127.4 SDev .0001 .0014 .0002 .0009 .273 5.0 %RSD 24.28 4.640 11.66 47.78 3.979 3.896 ##1 -.0003 .0317 .0021 .0024 7.030 130.3 #2 -.0002 .0322 .0022 .0024 7.031 130.4 #3 -.0002 .0295 .0018 .0008 6.557 121.7 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb ---� 3.672 .0006 194.8 0444 3.0064 -1.4384 T .144 .0003 6.9 .0029 2.6415 1.0270 anaD 3.928 54.39 3.538 6.404 87.860 71.401 #1 3.755 .0009 199.0 .0468 4.2342 -1.2308 #2 3.756 .0003 198.5 .0453 4.8106 -2.5533 #3 3.506 .0006 186.8 .0413 -.02544 -.53097 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge 2.8353 -1.1034 2.6767 7.687 -.0029 .3116 SDev .9807 3.2314 .7669 .301 .0017 .0128 %RSD 34.591 292.85 28.650 3.916 57.39 4.107 #1 3.4572 -4.7454 3.1168 7.866 -.0046 .3192 #2 3.3439 .01475 1.7912 7.855 -.0012 .3188 #3 1.7047 1.4204 3.1221 7.339 -.0029 .2968 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .76694 .0006 .0003 .04184 1.7357 1.4179 SDev 2.2372 .0005 .0002 .49163 .8341 1.0456 %RSD 291.71 84.84 74.51 1175.1 48.054 73.742 #1 -.72175 .0005 .0004 .58908 2.4783 .49867 #2 3.3397 .0002 .0004 -.10104 1.8956 1.1997 #3 -.31713 .0012 .0000 -.36252 .83328 2.5554 page 1 Ca PPM 39.10 1.52 3.884 39.96 39.99 37.35 Mg ppm 33.37 1.30 3.909 34.11. 34.12 31.86 2068/1 Ppb -.46681 .85361 182.86 .51738 -1.0055 -.91228 Ti ppm .0026 .0001 4.802 .0027 .0027 .0025 Analysis Report 12/14/07 02:05:19 PM page 1 P^-~'-od: CLP1 Sample Name: 0713817-002D Operator: CO - rime: 12,/14/07 13:58:04 Com, -.ent w S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 3.1632 .4633 -.48586 .2422 .1893 .0002 43.66 SDev .1010 .0009 2.21489 .0005 .0001 .0000 .05 %RSD 3.1918 .200'1 455.87 .2135 .0576 15.79 .1144 #1 3.1657 .4639 2.0202 .2428 .1894 .0001 43.61 #2 3.0609 .4623 -2.1809 .2420 .1892 .0002 43.68 #3 3.2628 .4639 -1.2969 .2418 .1894 .0002 43.70 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0248 .0031 .0120 43.49 38.88 24.75 SDev .0001 .0002 .0004 .0003 .06 .06 .00 %RSD 32.74 .6686 12.18 2.705 .1266 .1499 .0164 #1 .0003 .0247 .0027 .0118 43.43 38.94 24.75 #2 .0005 .0250 .0034 .0124 43.51 38.89 24.76 #3 .0003 .0248 .0032 .0120 43.53 38.82 24.75 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e 15.89 -.0008 54.38 .0109 2.9330 -4.7343 2.9806 v .01 .0009 .08 .0004 .4921 1.4581 1.6440 %RSD .0833 107.6 .1431 3.961 16.778 30.800 55.157 #1 15.87 .0001 54.39 .0104 2.9693 -6.0778 1.2668 #2 15.89 -.0017 54.45 .0111 2.4238 -3.1837 4.5445 #3 15.90 -.0010 54.29 .0111 3.4060 -4.9414 3.1304 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.4973 -,79573 2.9958 7.230 -.0038 .3648 .0346 SDev .8463 .58884 2.8479 .007 .0022 .0004 .0001 %RSD 56.521 74.000 95.062 .0934 58.28 .0989 .1491 #1 1.6662 -.21657 2.4653 7.232 -.0055 .3652 .0346 ##2 2.2465 -.77681 6.0716 7.235 -.0047 .3647 .0347 #3 .57933 -1.3938 .45051 7.222 -.0013 .3646 .0346 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.2472 .0027 -.0162 -2.1810 1.9913 1.7332 SDev 1.1786 .0004 .0001 .8745 .8853 1.9823 %RSD 52.447 15.43 .5665 40.099 44.459 114.37 #1 1.2757 .0022 -.0163 -3.0650 1.5332 1.5722 #2 3.5583 .0030 -.0161 -1.3163 3.0118 3.7911 #3 1.9076 .0030 -.0161 -2.1616 1.4289 -.16365 Analysis Report 12/14/07 02:12:41 PM page 1 MPr_hod: CLP1 Sample Name: 0713817-003D Operator: CO R Cime: 12/14/07 14:05:25 C int: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .00136 .0333 1.3140 .0423 .0233 .0001 40.83 SDev .18428 .0035 .8950. .0002 .0001 .0000 .08 %RSD 13519. 10.62 68.109 .5380 .5524 .2977 .1909 #1 .17923 .0372 .64086 .0425 .0233 .0001 40.81 #2 -.18872 .0304 .97153 .0420 .0234 .0001 40.91 #3 .01358 .0322 2.3296 .0422 .0231 .0001 40.76 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0121 .0006 .0001 .1255 4.205 17.53 SDev .0000 .0000 .0000 .0004 .0078 .025 .04 %RSD 18.10 .3247 6.481 656.5 6.186 .5902 .2146 #1 .0001 .0120 .0006 .0005 .1334 4.216 17.51 #2 .0001 .0120 .0006 -.0000 .1254 4.223 17.57 #3 .0001 .0121 .0006 -.0003 .1178 4.177 17.50 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb I 3.926 .0003 13.57 .0120 3.2417 -.17032 -2.0976 .009 .0008 .05 .0004 .7333 .96932 1.5793 .2342 265.9 .3357 3.180 22.622 569.10 75.291 #1 3.926 .0010 13.57 .0124 2.9807 -.92103 -1.3445 #2 3.934 -.0006 13.62 .0119 4.0698 -.51394 -3.9126 #3 3.916 .0006 13.53 .0117 2.6746 .92399 -1.0358 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.7263 .59323 1.7207 5.841 -.0020 .1561 .0020 SDev .3471 1.9683 .8102 .012 .0006 .0004 .0001 %RSD 20.108 331.79 47.088 .1996 28.92 .2296 4.128 #1 1.9797 2.2677 2.1662 5.836 -.0013 .1560 .0020 #2 1.8685 -1.5749 .78545 5.854 -.0025 .1565 .0021 #3 1.3306 1.0869 2.2103 5.832 -.0021 .1558 .0020 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .07362 -.0005 -.0007 .96596 .45294 1.3453 SDev 1.8794 .0005 .0001 .56579 .47108 1.1796 %RSD 2552.7 97.41 12.48 58.573 104.00 87.684 #1 1.5567 -.0008 -.0007 .37833 .87272 2.2000 #2 .70413 .0001 -.0006 1.0125 -.05654 -.00050 #3 -2.0399 -.0007 -.0006 1.5070 .54264 1.8362 Analysis Report 12/14/07 02:20:02 PM page 1 t" 'tod: CLP1 Sample Name: 0713817-004D Operator: CO Time: 12/14/07 14:12:47 Lvuuilent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .50.900 .2522 .52497 .0502 .0378 .0001 17.88 SDev .35753 .0005 1.0390 .0003 .0001 .0000 .04 %RSD 70.241 .1895 197.92 .6027 .2766 12.26 .2007 #1 .25258 .2525 1.6916 .0503 .0378 .0001 17.84 #2 .35701 .2525 -.30089 .0505 .0377 .0001 17.87 #3 .91741 .2517 .18425 .0499 .0379 .0001 17.91 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 .0027 .0032 .0096 .4734 8.521 4.778 SDev .0001 .0006 .0001 .0002 .0002 .024 .010 %RSD 70.82 23.14 2.139 2.125 .0493 .2813 .2045 #1 -.0000 .0020 .0031 .0096 .4734 8.517 4.773 #2 -.0001 .0027 .0032 .0095 .4732 8.499 4.771 #3 -.0002 .0033 .0032 .0099 .4737 8.547 4.789 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb [e 1.934 -.0001 2.902 .0065 3.4906 -1.6011 -.22597 :v .001 .0003 .006 .0009 .6992 1.0069 2.67587 %RSD .0593 246.4 .2063 14.04 20.030 62.889 1184.2 #1 1.933 .0001 2.908 .0061 3.6901 -.43854 2.8388 #2 1.934 -.0000 2.899 .0058 2.7133 -2.1979 -1.4181 #3 1.935 -.0004 2.897 .0075 4.0683 -2.1668 -2.0986 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .83800 -.40308 1.6538 4.413 -.0011 .0477 .0123 SDev 5.1710 2.23721 .8673 .003 .0008 .0001 .0000 %RSD 617.07 555.03 52.439 .0666 69.85 .2527 .2994 #1 -4.7694 2.0927 1.0551 4.412 -.0016 .0477 .0122 #2 5.4184 -1.0734 1.2580 4.411 -.0015 .0478 .0123 #3 1.8650 -2.2285 2.6484 4.416 -.0002 .0476 .0123 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.0129 .0005 .0034 .09451 .48373 .96891 SDev 3.3154 .0006 .0001 .76632 2.6894 .46197 %RSD 327.33 119.0 2.075 810.87 555.97 47.679 #1. -1.0944 -.0001 .0033 .93638 -2.2359 1.4006 #2 -4.2868 .0005 .0034 -.56242 3.1419 .48169 R3 2.3426 .0011 .0034 -.09043 .54519 1.0244 Analysis Report 12/14/07 02:27:24 PM page 1 t"-`'-od: CLP1 Sample Name:-0713817-005D • Operator: CO I Time: 12/14/07 14:20:09 Mode: CONC Corr. Factor: 1 + Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .35186 .0366 -.33050 .0435 .0248 .0001 43.08 SDev .41499 .0013 1.74454 .0005 .0001 .0000 .04 %RSD 117.94 3.656 527.84 1.066 .2686 14.18 .0997 #1 .24356 .0377 -1.8883 .0430 .0248 .0001 43.04 #2 .00177 .0351 1.5544 .0439 .0247 .0001 43.12 #3 .81026 .0371 -.65762 .0436 .0248 .0001 43.08 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0131 .0008 .0012 .1086 4.340 1.8.64 SDev .0000 .0001 .0000 .0002 .0001 .008 .01 %RSD 13.03 1.105 4.278 14.85 .1107 .1775 .0564 #1 .0001 .0132 .0008 .0013 .1087 4.337 18.64 #2 .0001 .0133 .0009 .0010 .1085 4.335 18.65 #3 .0001 .0130 .0009 .0013 .1087 4.349 18.63 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb e 3.994 -.0008 13.92 .0133 3.2645 .17708 -1.6033 v .003 .0003 .01 .0004 2.4881 1.6032 .7516 %RSD .0857 36.03 .0488 2.785 76.217 905.33 46.876 #1 3.992 -.0006 13.92 .0129 2.2456 .71609 -1.4929 #2 3.998 -.0011 13.93 .0136 6.1003 -1.6261 -2.4040 #3 3.993 -.0006 13.92 .0135 1.4476 1.4413 -.91307 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.99557 -.01783 3.3091 6.313 -.0011 .1645 .0025 SDev 2.83637 2.94101 1.9492 .004 .0020 .0003 .0000 %RSD 284.90 16493. 58.904 .0582 182.2 .1965 1.726 41 1.7566 -3.3442 1.7038 6.311 -.0000 .1645 .0025 #2 -.83414 2.2378 5.4780 6.317 .0001 .1648 .0024 #3 -3.9092 1.0530 2.7455 6.310 -.0035 .1642 .0025 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.9231 -.0002 .0008 1.2053 -1.1979 2.2012 SDev 1.8955 .0006 .0001 .2489 1.7983 2.1881 %RSD 98.562 244.1 12.69 20.653 150.12 99.404 #1 -2.9808 -.0002 .0007 1.2255 .67457 .02287 #2 -3.0538 -.0008 .0008 .94685 -1.3569 4.3990 #3 .26517 .0003 .0009 1.4435 -2.9115 2.1819 Analysis Report 12/14/07 02:34:46 PM page 1 M-`'-Dd: CLP1 Sample Name: 0713303-001EPDS Operator: CO R Time: 12/14/07 14:27:31 CkJ«<I«znt : L Mode: CONC Corr Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge 1.4080 .1500 38.505 23.44 .8019 .0003 SDev .4620 .0042 1.125 .38 .0120 .0001 %RSD 32.815 2.805 2.9206 1.602 1.503 18.06 #1 .93844 .1499 39.485 23.63 .8084 .0003 #2 1.4236 .1542 37.277 23.69 .8093 .0003 #3 1.8621 .1458 38.752 23.01 .7880 .0002 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge -.0000 .0107 .0919 .0008 3.205 295:5 SDev .0001 .0006 .0019 .0004 .064 5.4 %RSD 267.2 5.817 2.046 50.63 2.010 1.832 #1 .0000 .0109 .0930 .0012 3.240 299.0 #2 .0000 .0112 .0929 .0009 3.245 298.3 #3 -.0002 .0100 .0897 .0004 3.131 289.3 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb e 1.123 -.0007 828.8 .0204 -2.6803 -1.0359 v .023 .0003 12.3 .0005 .9320 .7403 %RSD 2.045 37.75 1.479 2.605 34.774 71.462 #1 1.136 -.0005 835.9 .0207 -1.6874 -1.4318 #2 1.136 -.0010 835.7 .0208 -2.8169 -1.4941 #3 1.096 -.0006 814.6 .0198 -3.5364 -.18186 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge 1.1482 9.4142 3.2250 19.64 .0030 3.011 SDev 1.7362 3.1236 2.2604 ..34 .00.07 .051 %RSD 151.21 33.179 70.088 1.712 23.57 1.685 #1 3.0882 6.4119 5.6332 19.81 .0022 3.040 #2 .61632 12.646 2.8926 19.86 .0036 3.041 #3 -.25981 .9.1844 1.1493 19.25 .0032 2.953 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .00327 .1061 .0105 -1.5834 .58199 5.2861 SDev 1.6983 .0016 .0005 .3230 .79771 1.2713 %RSD 51903. 1.520 4.324 20.401 137.07 24.051 #1 -.96135 .1066 .0107 -1.5168 1.4948 5.8925 #2 -.99303 .1074 .0109 -1.9345 .01869 6.1406. :Rq 1.9642 .1043 .0100 -1.2988 .23248 3.8250 Ca ppm 161.7 3.7 2.276 163.8 163.8 157.4 Mg ppm 157.3 2.9 1.871 158.9 159.1 153.9 2068/1 ppb -.55230 1.55525 281.60 -1.6969 -1.1785 1.2184 Ti PPM .2423 .0044 1.813 .2447 .2450 .2373 Analysis Report 12/14/07 02:42:08 PM page 1 A°-'-'-od: CLP1 Sample Name: CCV4 Operator: CO F Time: 12/14/07 14:34:52 C.-......ent . Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 10.59.0 49.89 502.81 2.518 2.555 2.475 48.52 SDev .8 .05 2.55 .010 .003 .003 .08 %RSD 07674 .0905 ..50711 .3973 .1343 .1282 .1697 #1 1059.7 49.92 500.64 2.529 2.558 2.474 48.48 #2 1058.1 49.83 502.17 2.511 2.551 2.472 48.47 #3 1059.1 49.90 505.62 2.513 2.555 2.478 48.62 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.436 2.425 2.449 2.575 49.18 86.08 50.28 SDev .005 .003 .004 .005 .09 .18 .05 %RSD .1993 .1207 .1575 .2089 .1794 .2095 .1043 #1 2.433 2.423 2.447 2.581 49.15 86.11 50.30 #2 2.433 2.424 2.447 2.571 49.11 85.88 50.22 2.441 2.428 2.454 2.572 49.28 86.24 50.31 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.456 2.443 83.73 2.472 482.38 480.70 974.63 SDev .003 .008 .25 .007 1.22 3.81 3.97 %RSD .1205 .3253 .2973 .2668 .25286 .79245 .40707 #1 2.455 2.435 83.98 2.473 482.48 479.61 976.83 #2 2.453 2.442 83.49 2.464 481.11 477.57 970.05 #3 2.459 2.451 83.72 2.477 483.54 484.94 977.01 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 995.28 513.14 501.78 2.367 2.370 2.474 2.440 SDev 2.87 5.40 4.60 .015 .005 .003 .002 %RSD .28854 1.0528 .91740 .6424 .1929 .1218 .0893 #1 992.24 509.5.9 506.35 2.385 2.365 2.477 2.440 997.94 510.47 497.15 2.358 2.369 2.471 2.437 995.65 519.35 501.85 2.358 2.374 2.475 2.441 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK N N O Cn knalysis Report 12/14/07 02:42:08 PM l i Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 499.89 2.454 2.553 481.26 988.40 505.56 SDev 5.45 .003 .003 2.93 1.19 3.45 %RSD 1.0911 .1020 .1213 .60849 .1203.3 .68226 ##1 495.67 2.454 2.554 480.56 987.11 507.43 ##2 497.96 2.451 2.550 478.75 988.66 501.58 #3 506.05 2.456 2.556 484.48 989.44 507.68 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 12/14/07 02:49:30 PM page 1 P"-`'-,od: CLP1 Sample Name: CCVL4 Operator: CO ] Time: 12/14/07 14:42:14 C..<«<<+ent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .57826 .0424 1.8698 .0124 .0010 .0008 .0175 SDev :34980 .0072 1.1091 .0016 .0003 .0003 .0072 %RSD 60.491 17.00 59.315 13.07 32.79 30.13 41.24 #1 .92499 .0487 .59163 .0141 .0013 .0011 .0250 #2 .22548 .0438 2.5778 .0123 .0010 .0008 .0170 #3 .58432 .0346 2.4399 .0108 .0006 .0006 .0106 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0008 .0005 -.0001 .0031 2.501 .0768 .0179 SDev .0004 .0007 .0006 .0007 .010 .0196 .0080 oRSD 57.16 138.5 1013. 22.70 .3901 25.47 44.55 #1 .0013 .0013 .0006 .0039 2.512 .0991 .0267 #2 .0006 .0003 -.0002 .0025 2.499 .0683 .0158 .0004 -.0001 -.0005 .0029 2.493 .0629 .0112 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0007 .0046 2.663 -.0008 -2.0549 -1.0814 3.0129 SDev .0004 .0021 .014 .0003 .6206 1.7651 2.6511 %RSD 51.40 45.26 .5301 35.86 30.201 163.22 87.992 41 .0011 .0069 2.676 -.0010 -1.6681 -1.8799 6.0699 #2 .0006 .0044 2.665 -.0008 -1.7259 .94183 1.3434 #3 .0004 .0027 2.648 -.0005 -2.7708 -2.3062 1.6255 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.25.0 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.5992 4.7500 -.31690 .0340 -.0010 .0010 .0009 SDev 2.6627 1.8631 2.61082 .0048 .0024 .0003 .0004 %RSD 73.982 39.222 823.85 14.14 243.4 29.79 48.26 #1 6.5124 4.4813 -1.3765 .0379 .0017 .0014 .0015 1.2911 3.0359 -2.2313 .0354 -.0021 .0010 .0007 2.9940 6.7328 2.6571 .0286 -.0025 .0008 .0006 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 02:49:30 PM page 2 h LAW Zn Elem T11908, Units ppb Avge 1.0324 SDev .4823 %RSD 46.719 #1 1.1391 #2 .50562 #3 1.4524 Errors NOCHECK High 3.505 Low 77.470 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0013 .0113 -1.4055 3.4040 1.3704 .0003 .0004 1.3049 2.6371 2.3493 25.66 3.505 92.841 77.470 171.43 .0015 .0116 -1.8093 6.3651 .57417 .0015 .0114 .05355 1.3086 -.47731 .0009 .0108 -2.4608 2.5383 4.0144 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report t'-`'-.od: CLP1 Sample Name: CCB4 I Time: 12%14/07 14:49:36 Ca (-�««<ient : ppm ppm ppm Mode: CONC Corr. Factor: 1 .0002 Elem Ag Al As1890 Units ppb ppm ppb Avge .35615 .0275 1.2010 SDev .43285 .0035 .4633 %RSD 121.54 12.70 38.579 ##1 .85356 .0281 1.0354 #2 _06502 .0306 1.7243 #3 .14987 .0237 .84319 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge -.0000 -.0003 -.0010 SDev .0002 .0003 .0004 %RSD 1069. 117.4 45.11 ##1 .0002 .0000 -.0005 #2 -.0002 -.0002 -.0011 .2000 -.0001 -.0006 -.0013 Errors LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem Mn Mo Na Units ppm ppm ppm Avge .0000 .0006 .0542 SDev .0002 .0002 .0045 %RSD 1870. 35.60 8.337 #1 .0002 .0006 .0592 #2 -.0000 .0008 .0533 ##3 -.0001 .0004 .0503 Errors LC Pass NOCHECK LC Pass High .0150 ppm 5.000 Low -.0150 -.0002 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 1.1681 8.502.1 -.71324 SDev 2.1729 1.4880 1.17618 %RSD 186.02 17.501 164.91 #1 1.6312 9.4686 .52808 NOCHECK -1.1990 9.2490 -.85668 3.0722 6.7886 -1.8111 Errors NOCHECK NOCHECK NOCHECK 12/14/07 02:56:52 PM page 1 Operator: CO B Ba Be Ca ppm ppm ppm ppm .0059 .0001 .0002 .0009 .0006 .0001 .0001 .0017 9.955 97.62 35.33 185.6 .0066 .0003 .0003 .0029 .0055 .0001 .0002 .0004 .0057 .0000 .0002 -.0005 LC Pass LC Pass LC Pass LC Pass .2000 .2000 .0050 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K - Mg ppm ppm ppm ppm -.0013 .0030 .0448 .0026 .0003 .0018 .0141 .0027 24.79 60.95 31.53 103.2 -.0010 .0049 .0611 .0052 -.0015 .0030 .0380 .0029 -.0015 .0012 .0354 -.0002 LC Pass LC Pass LC Pass LC Pass .0250 .1000 5.000 .2000 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb -.0015 -2.4267 -.88645 .54050 .0007 .8029 .82791 1.6529 50.59 33.086 93.395 305.82 -.0006 -1.8333 -1.8329 2.4423 -.0016 -2:1064 -.52975 -.55020 -.0021 -3.3403 -.29669 -.27062 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si - Sn Sr Ti ppm ppm ppm ppm .0013 -.0002 .0001 .0001 .0029 .0016 .0001 .0002 225.0 690.5 87.59 150.2 .0046 .0010 .0003 .0003 -.0000 -.0020 .0001 .0002 -.0007 .0003 .0000 -.0001 NOCHECK NOCHECK ' NOCHECK NOCHECK Analysis Report 12/14/07 02:56:52 PM z Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .43604 .0000 .0009 -1.3993 .95917 2.3555 SDev 2.1378 .0005 .0000 .3967 1.6821 1.2335 %RSD 490.27 1034. 4.407 28.352 175.37. 52.366 #1 -1.7143 .0006 .0008 -1.8330 1.9013 3.5053 #2 .46131 -.0001 .0009 -1.0547 -.98290 2.5086 #3 2.5611 -.0004 .0009 -1.3101 1.9591 1.0526 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 12/14/07 03:04:14 PM page 1 M-1--"od: CLP1 Sample Name: CRI Operator: CO R Time: 12/14/07 14:56:58 C_........ E�nt . Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 20.877 .0296 22.619 .2130 -.0001 .0102 -.0014 SDev .325 .0033 1.655 .0048 .0000 .0002 .0014 %RSD 1.5551 11.19 7.3181 2.239 36.63 1.641 95.27 #1 21.221 .0325 23.576 .2181 -.0001 .0104 .0000 #2 20.836 .0304 23.574 .2087 =.0001 .0101 -.0016 #3 20.575 .0260 20.708 .2123 -.0002 .0102 -.0027 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0101 .0996 .0191 .0497 -.0012 .0503 -.0013 SDev .0001 .0021 .0006 .0012 .0007 .0057 .0027 %RSD .7872 2.069 3.270 2.335 56.24 11.43 207.7 #1 .0101 .1019 .0197 .0510 -.0006 .0555 -.0020 #2 .0100 .0979 .0185 .0487 -.0012 .0511 .0017 #3 .0101 .0989 .0190 .0496 -.0019 .0441 -.0037 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb .0301 .0222 .0483 .0805 2.3963 4.1614 117.63 s .0005 .0009 .0046 .0011 .8989 .5942 1.05 ax81) 1.656 4.281 9.493 1.333 37.513 14.279 .89270 #1 .0306 .0232 .0533 .0817 2.6901 3.4780 116.73 #2 .0297 .0220 .0474 .0796 3.1115 4.5557 117.39 #3 .0300 .0213 .0442 .0803 1.3872 4.4505 118.78 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 119.16 14.145 8.2589 .1667 .0776 .0533 .2015 SDev 4.90 .466 1.8150 .0053 .0017 .0009 .0034 %RSD 4.1117 3.2960 21.977 3.201 2.136 1.648 1.704 #1 124.61 14.678 10.015 .1728 .0793 .0542 .2051 #2 115.12 13.811 6.3905 .1628 .0760 .0524 .1983 #3 117.75 13.946 8.3709 .1645 .0776 .0531 .2011 Elem T11908 v Zn Pb2203 Sb2068 Se1960 " Units ppb ppm ppm ppb ppb ppb Avge 21.269 .0997 .0435 3.5737 118.65 10.219 SDev 2.348 .0015 .0010 .4472 3.09 1.353 %RSD 11.037 1.559 2.226 12.513 2.6061 13.242 #1 20.452 .1014 .0445 3.2157 121.99 11.568 #2 23.917 .0984 .0425 4.0749 115.88 8.8617 #3 19.440 .0993 .0435 3.4305 118.09 10.227 00 s r-+ N O H Analysis Report 12/14/07 03:11:36 PM page 1 V -'od: CLP1 Sample Name: ICSA Operator: CO F Time: 12/14/07 15:04:20 Cumment : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .65963 503.9 7.8682 .0055 .0014 .0003 506.9 SDev .27110 .5 .4979 .0005 .0000 .0000 1.4 %RSD 41.099 .0935 6.3278 8.349 1.683 5.086 .2699 #1 .97171 503.5 7.5471 .0060 .0014 .0003 505.5 #2 .48232 503.9 7.6158 .0053 .0014 .0003 507.0 #3 .52487 504.4 8.4417 .0052 .0014 .0003 508.3 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0000 _0018 .0013 .0039 202.8 .0264 500.4 SDev .0000 .0003 .0004 .0002 .7 .0118 1.2 %RSD 260.0 16.62 33.37 4.760 .3210 44.61 2379 #1 .0000 .0020 .0018 .0039 202.1 .0331 499.3 #2 -.0000 .0014 .0014 .0040 202.8 .0334 500.4 -.0000 .0019 .0009 .0037 203.4 .0128 501.7 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0080 -.0049 .0359 .0021 -22.754 11.124 6.3038 SDev .0003 .0011 .0011 .0010 2.660 .736 3.7846 %RSD 4.061 22.71 3.138 46.33 11.691 6.6164 60.037 #1 -.0076 -.0037 .0371 .0032 -25.723 11.712 10.619 ##2 -.0082 -.0060 .0358 .0013 -20.588 10.299 4.7459 #3 -.0082 -.0051 .0349 .0019 -21.950 11.362 3.5468 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 11.691 9.1709 -6.1661 -.0020 -.0092 -.0370 .0134 SDev 2.624 4.1354 2.5417 .0020 .0033 .0014 .0003 %RSD 22.445 45.092 41.221 98.17 35.65 3.746 1.894 41 13.930 11.963 -3.2834 -.0042 -.0123 -.0379 .0137 8.8037 11.130 -7.1299 -.0014 -.0058 -.0377 .0133 12.338 4.4201 -8.0849 -.0005 -.0093 .-.0354 .0132 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK ON N O F-+ Analysis Report 12/14/07 03:11:36 PM h LOW Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb , ppb ppb Avge .14537 .0039 -.0107 -.15695 9.8969 -1.0589 SDev 3.7434 .0005 .0001 .53241 2.7204 2.8572 %RSD 2575.2 11.87 .7359 339.23 27.487 269.84 ##1 3.5273 .0043 -.0108 -.75372 12.828 1.7936 #2 -3.8770 .003.9 -.0107 .01355 7.4525 -1.0495 #3 .78577 .0034 -.0108 .26933 9.4106 -3.9207 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 Analysis Report 12/14/07 03:18:57 PM page 1 N -od: CLP1 Sample Name: ICSAB Operator: CO F Time: 12/14/07 15:11:42 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb ppm Ppm Ppm ppm Avge 1118.6 501.7 1027.6 1.040 .5279 .4995 508.1 SDev 2.0 1.0 5.6 .003 .0013 .0004 .3 %RSD .17819 .2081 _54747 .3247 .2392 .0845 .0506 #1 1119.2 502.4 1031.9 1.040 .5285 .4999 508.4 #2 1120.2 502.3 1029.6 1.043 .5288 .4997 508.1 #3 1116.4 500.5 1021.2 1.037 .5265 .4991 507.9 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .9487 .4764 .4855 .5647 203.0 .0464 501.2 SDev .0010 .0003 .0006 .0017 .2 .0097 .5 %RSD .1076 .0680 .1178 .3077 .0850 20.97 .0994 #1 .9499 .4767 .4859 .5648 203.1 .0471 501.5 #2 .9481 .4761 .4857 .5664 203.1 .0363 501.4 .9481 .4763 .4848 .5630 202.8 .0557 500.6 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm Ppm ppm ppb Ppb Ppb Avge .4819 .9818 .0600 .9666 961.32 983.71 -2.8175 SDev .0007 .0016 .0020 .0020 5.23 4.10 5.7463 %RSD .1475 .1646 3.375 .2086 .54446 .41693 203.95 #1 .4822 .9799 .0619 .9680 963.80 988.00 -6.5139 #2 .4823 .9830 .0600 .9643 964.85 979.82 -5.7413 #3 .4810 .9824 .0579 .9676 955.31 983.32 3.8027 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm Ppm ppm ppm Avge -.17184 1025.2 1012.1 1.040 .9661 .5035 1.027 SDev .59996 16.3 6.3 .003 .0048 .0021 .002 %RSD 349.13 1.5891 .61953 .2726 .5012 .4199 .1946 ul -.85538 1038.2 1015.4 1.039 .9717 .5045 1.028 1030.5 1004.9 1.043 .9640 .5049 1.028 Tr- .26756 .07230 1006.9 1016.1 1.037 .9627 ..5010 1.024 Errors NOCHECK NOCHECK NOCHECK NOCHECK - NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 03:18:57 PM 1 Elem T11908 v Zn Pb2203, Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 979.10 .4995 1.051 976.26 -1.0528 1016.5 SDev 5.19 .0014 .001 3.22 2.1111 5.7 %RSD .52960 .2850 .0887 .32954 200.51 .55660 #1 973.82 .5004 1.052 979.94 -2.7397 1023.0 #2 984.18 .5002 1.051 974.84 -1.7333 1013.4 #3 979.29 .4978 1.050 973.99 1.3146 1013.0 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 Analysis Report 12/14/07 03:26:20 PM page 1 PR_"-od: CLP1 Sample Name: CCV5 Operator: CO F Time: 12/14/07 15:19:04 CU««<<ent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1063.3 49.89 504.58 2.519 2.560 2.499 48.99 SDev 6.1 .23 5.00 .019 .013 .016 .28 %RSD .57129 .4619 .99153 .7449 .5267 .6440 .5782 #1 1056.6 49.65 498.81 2.498 2.545 2.482 48.73 #2 1068.4 50.11 507.78 2.535 2.571 2.515 49.29 #3 1064.9 49.93 507.14 2.523 2.563 2.499 48.95 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.456 2.448 2.469 2.580 49.58 85.97 50.80 SDev .014 .014 .015 .015 .32 .37 .28 %RSD .5768 .5647 .6242 .5721 .6386 .4293 .5588 #1 2.443 2.434 2.454 2.564 49.28 85.58 50.52 #2 2.471 2.461 2.485 2.593 49.91 86.31 51.09 2.455 2.449 2.468 2.584 49.56 86.03 50.78 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.472 2.467 83.68 2.484 484.58 48.8.27 985.54 SDev .015 .016 .44 .012 6.20 4.68 8.55 %RSD .6088 .6536 .5209 .4936 1.2793 .95761 .86751 #1 2.456 2.449 83.22 2.471 478.13 484.09 975.98 #2 2.486 2.480 84.09 2.495 490.50 493.32 992.46 #3 2.473 2.472 83.74 2.488 485.11 487.40 988.17 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 999.51 518.35 506.80 2.326 2.404 2.482 2.452 SDev 12.34 6.70 3.76 .014 .020 .013 .014 %RSD 1.2348 1.2916 .74159 .6134 .8266 .5289 .5609 #� 985.33 510.97 502.78 2.311 2.382 2.468 2.437 1007.8 520.04 510.23 2.340 2.422 2.494 2.465 1005.4 524.03 507.38 2.326 2.406 2.485 2.453 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 03:26:20 PM h LV W Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 502.47 2.473 2.572 487.04 994.86 510.64 SDev 8.11 .015 .017 5.15 11.05 4.46 %RSD 1.6132 .6103 .6486 1.0570 1.1110 .87271 #1 494.83 2.457 2.555 482.11 982.22 505.51 #2 510.97 2.487 2.588 492.38 1002.7 513.50 #3 501.61 2.474 2.573 486.64 999.68 512.92 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 . 450.00 page 2 Analysis Report 12/14/07 03:33:41 PM page 1 m -shod: CLP1 Sample Name: CCVL5 Operator: CO Time: 12/14/07 15:26:26 -...nent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .53082 .0850 1.3422 .0058 .0009 .0009 .0574 SDev .15950 .0277 .8165 .0013 .0004 .0004 .0299 %RSD 30.047 32.57 60.834 21.72 44.48 42.09 52.04 #1 .37653 .1114 1.8004 .0066 .0014 .0013 .0884 #2 .69506 .0873 .39950 .0065 .0009 .0009 .0551 #3 .52088 .0562 1.8268 .0043 .0005 .0005 .0287 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0007 .0006 -.0002 .0034 2.534 .0631 .0580 SDev .0003 .0006 .0005 .0004 .016 .0183 .0301 %RSD 50.97 112.9 189.2 11.44 .6173 28.95 51.91 #1 .0010 .0011 .0002 .0035 2.544 .0800 .0893 #2 .0007 .0007 -.0003 .0036 2.541 .0654 .0553 .0003 -.0001 -.0007 .0029 2.516 .0437 .0293 terrors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0051 2.616 -.0007 -1.9141 -.52997 2.7255 SDev .0004 .0026 .012 .0006 1.4572 .15846 1.7348 %RSD 65.37 50.83 .4463 95.53 76.126 29.899 63.650 #1 .0010 .0080 2.627 -.0004 -1.2704 -.64733 4.7135 42 .0006 .0043 2.617 -.0002 -.88971 -.34972 1.5182 #3 .0002 .0030 2.604 -.0014 -3.5823 -.59286 1.9449 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.2069- 8.4139 -1.9270 .0148 -.0022 .0009 .0009 SDev 1.9993 2.1979 .6127 .0011 .0020 .0003 .0005 %RSD 165.65 26.122 31.797 7.165 90.55 37.80 56.76 #1 2.1552 7.0839 -1.3271 .0159 -.0012 .0013 .0013 2.5556 10.951 -1.9020 .0139 -.0009 .0009 .0010 -1.0900 7.2070. -2.5517 .0145 -.0045 .0006 .0003 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 03:33:41 PM h Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.0359 .0009 .0117 -.99082 1.7127 1.5166 SDev 2.0798 .0004 .0005 .54236 1.6023 .8408 %RSD 102.16 41.27 4.279 54.739 93.554 55.443 #1 3.6771 .0012 .0122 -.85472 3.0072 1.4738 #2 2.7337 .0011 .0115 -.52946 2.2102 2.3780 #3 -.30307 .0005 .0113 -1.5883 -.07935 .69797 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low page 2 Analysis Report 12/14/07 03:41:02 PM page 1 CLP1 Sample Name: CCB5 Operator: CO F, Time: 12/14/07 15:33:47 C.r...... ent : Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .65236 .0408 2.7743 .0022 .0006 .0003 .0161 SDev .33636 .0031 .8436 .0003 .0001 .0001 .0061 %RSD 51.561 7.671 30.409 11.40 18.60 20.71 37.64 #1 .42565 .0423 3.2099 .0020 .0007 .0003 .0214 #2 1.0388 .0429 3.3111 .0024 .0006 .0003 .0175 #3 .49259 .0372 1.8019 .0020 .0005 .0002 .0095 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0001 -.0008 -.0010 .0096 .0396 .0160 SDev .0002 .0004 .0003 .0001 .0028 .0056 .0054 %RSD 247.6 296.2 29.87 13.35 29.31 14.10 33.93 #1 -.0000 -.0001 -.0010 -.0009 .0117 .0405 .0186 #2 .0003 .0006 -.0006 -.0010 .0106 .0446 .0197 -.0000 -.0001 -.0009 -.0011 .0064 .0336 .0098 .brrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0000 .0015 .0257 -.0009 -2.5619 -2.3262 -.02556 SDev .0001 .0003 .0027 .0009 .6666 .1249 1.53721 %RSD 262.4 18.08 10.61 98.S5" 26.020 5.3708 6014.3 #1 .0001 .0015 .0288 -.0001 -1.8873 -2.2544 -1.7603 #2 .0000 .0018 .0249 -.0008 -2.5781 -2.4704 .51609 #3 -.0000 .0012 .0235 -.0019 -3.2203 -2.2537 1.1675 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.6043 6.1605 -1.8504 -.0121 .0007 .0002 .0001 SDev .7293 .5307 .6454 .0018 .0007 .0001 .0001 %RSD 20.234 8.6148 34.879 15.01 98.30 35.70 51.93 #1 3.4057 5.6439 -2.4525 -.0130 .0015 .0002 .0002 4.4123 6.1333 -1.1690 -.0132 .0001 .0002 .0001 2.9949 6.7043 -1.9296 -.0100 .0006 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 12/14/07 03:41:02 PM page 2 n LV W Zn Elem T11908 Units ppb Avge 1.9694 SDev .7522 %RSD 38.197 #1 1.2403 #2 2.7428 #3 1.9250 Errors LC Pass High 10.000 Low -10.000 v Zn Pb2203 Sb2068 Se1960 ppm ppm ppb ppb ppb .0001 .0011 -2.4046 2.3956 .81729 .0001 .0001 .2385 .7148 .52149 84.56 6.133 9.9200 29.837 63.808 .0002 .0012 -2.1321 1.6855 .24364 .0000 .0011 -2.5062 3.1149 1.2627 .0001 .0010 -2.5755 2.3864 .94551 LC Pass LC Pass LC Pass LC Pass LC Pass .0500 .0200 3.0000 60.000 5.0000 -.0500 -.0200 -3.0000 -60.000 -5.0000 00 N N O C/j H2M.LABS; . INC. IV. DOCUMENTATION FOR METALS A. DIGESTION. LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE H2M Labs, Inc_ CLP Digestion Lo ant: PCi'SL Analyst Signature:_ SDG #: -TS LC?i 2 Date: (21111&7 Matrix: CPA%xrd t..c. r Time Started/Ended: Method:_ 301bk Description Sample ID # Lab # Dig Type Initial VolMt Final Vol Spike Sol # Lot # Volume Before After Ivl� D%li'%%/ ; D H7L!%)� priR,�/�� w{oT��s[C/`r (C �) s 6DZD _y D 0o1110 —it's OOtft ^ C0S0 --S oaa — or, (�bA ala .3D t��'13i71?^ po1D -3S a2 r 6� 003D M$-�D olssb ` M[�-2391kill / t Comments: PH: 4Z 'Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. 'Description of texture: fine, medium, coarse. 'Description of clarity clear, cloudy, opaque. 'Description of artifacts: yes or no and describe OJWBOOKS%CLPDigestionlog O M N O H2M LABS, INC. Y SDG NO.: TSL c�iZ SCAN: /YI k P.\S This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. - Signature: Reviewed By Signatu Date: