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HomeMy WebLinkAboutSample Data Summary Package 12/2007Analytical Data Package F®r TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL012 Water Samples Received: 12/5/07 & 12/6/07 SAMPLE DATA SUMMARY PACKAGE DECEMBER 2007 V I/" 1-/Akus� Is C'm Environmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 SAMPLE DATA SUMMARY PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 12/5/07 & 12/6/07 SDG NO.: TSLO12 1. NYS DEC SUMMARY FORMS. 2. CHAIN OF CUSTODY DOCUMENTATION 3. SDG NARRATIVES 4. SAMPLE REPORTS 4.1 METALS 4.2 WET CHEMISTRY 5. DUPLICATE SUMMARY RESULTS 5.1 METALS 5.2 WET CHEMISTRY 6. SPIKE SAMPLE RESULTS 6.1 METALS 6.2 WET CHEMISTRY 7. BLANK SUMMARY DATA AND RESULTS 7.1 METALS 7.2 WET CHEMISTRY 1. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL C ONSERVATION SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY Cr)(.- TCI n17 Anal tical Requirements Customer Sample Code Laboratory Sample Code ME we MW -1D Y�_-- - 0713771-001 X X MW-1S--`-�--- 0713771-002 --- X - iIVX� PJIW-4D 0713771-003 — X i X� X X MW -_4S — - 0713771-004 — MW -5D - _ 0713771-005 T X MW -5S 0713771-006 X �� MW -8D 0713771-007 X _ X Mw -8S - — 0713771-008 - X `X FB 120507 0713771-009 I X j MW -3D _ MW -3S --~-- -- --- MW -6D MW -6S - ----- 0713817-001 0713817-002 — 0713817-003 0713817-004------X X _—X — X_...- i X 1 X— ' X X IMB-BD 0713817-005 __.X__..I X CLP,on-CL (Please indicate year of protocol M CION O C/1 C� NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG : TSLO12 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0713771-001 MW -ID WATER CA,CD,FE,KMG,MN,NA,PB, 05 -Dec -07 12/07 0713771-002 IMW-1S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-003 MW -4D WATER CA,CD,FE,K;MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-004 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-005 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-006 lmw.5s WATER CA, CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-007 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-007DUP MW-8DD WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Deo -07 12/07 0713771-007MS MW-8DS WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713771-008 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07' 12/07 0713771-009 FB 120507 WATER CA,CD,FE,K,MG,MN,NA,PB, 05 -Dec -07 12/07 0713817-001 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 0713817-002 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 0713817-003 MW -6D WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 0713817-004 MW -6S WATER CA,CD,FE,K;MG,MN,NA,PB, 06 -Dec -07. 12/07 0713817-005 MB -BD WATER CA,CD,FE,K,MG,MN,NA,PB, 06 -Dec -07 12/07 I Laboratory Samp ID Client Sample IDI .-T- Matrix Tests DateRecd at Lab Date Analyze 0713771-001 MWAD Groundwater SELECT WET CHEMISTRY ** 1'2/05/07 12/07 0713771-002 MWAS'. Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-003 MW-4D Groundwater SELECT WET CHEMISTRY ** . 12/05/07 12/07 0713771-004 MW-4S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-005 MW-5D Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-006 MW-5S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-007 MW-8D Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-007DUP MW-8DDUP Groundwater SELECT WET CHEMISTRY 12/05/07 12/07 0713771-007MS MW-8DMS Groundwater SELECT WET CHEMISTRY 12/05/07 12/07 0713771-008 MW-8S Groundwater SELECT WET CHEMISTRY ** 12/05/07 12/07 0713771-009 FB 120507 Field Blank SELECT WET CHEMISTRY ** 12/05/07 12/07 0713817-001 MW-3D Groundwater SELECT WET CHEMISTRY ** 12/06/07 12/07 0713817-002 MW-3S Groundwater SELECT WET CHEMISTRY " 12/06/07 12/07. 0713817-003 MW-6D Groundwater SELECT WET CHEMISTRY ** I2/06/07 12/07 0713817-004 MW-6S Groundwater SELECT WET CHEMISTRY ** 12/06/07 12/07 0713817-005 MB-BD Groundwater SELECT WET CHEMISTRY ** 12/06/07 r 12/07 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand; Chloride; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable ; Sulfate; Total Dissolved Solids; Total Organic Carbon ; 2. CHAIN OF CUSTODY DOCUMENTATION A, ®� MAO WIG &Tie =.y.off Unlln.0 Off AAFAM11a- NV 447d7 .JW7R 21 0 EXTERNAL CHAIN OF CUSTODY E Tet: (631) 694-3040 Fax. (631) 420-8436 CLIENT: H2Ril SDG NO: (' PROJECT NAME/NUMBER So v7HOLO /V bPI LL 007 Q a s ~ N � d ° 1 m © i NOTES: Project Contact:' PAP -7 360 Phone Number: Ro�7 �/� X % $)sAo2S ,+" 06739 -AS P/S/Quote # 7 . SAMPLERS: (signatureyClient �/�EjvV DELIVERABLES: r S 70D _ ANALYSIS REQUESTED TURNAROUND TIME:DAYS -ORGANIC INORG.. DATE TIME MATRICk FIELD LD. V LAB I.D. NO. REMARKS: rZ © 00.30 • G w- g s a �► 3 CoQ w- g0a 4 3 3 3 -C MS 5p 1! 3a /Yl IN - 4 S $ oL 1 1 3 rzo.0 In W 40 12-30 M — 5's 1300 Mw,_ so _ 1330 -?7w — /_S IYoa '— 10 1:2001 BinBinq F .8 4rFeel Blot r� . Relinquished . s�nature Date Iz Ya7 Time / Recetve�by (stR+' uro) Date �s Time 1.��(Q LABORATORY USE ONLY DlsorepanclesBetv.m Sample Labels and COC Record? Y or N Expialn: Samoleswere: 1.ed or Hand t)eltvered_ Atrbin+R nblent or dulled, Temp 2. Z Ambi 3. Received in good condition: Y or N 4, Properly preserved: Y or N Teoe was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y'or N 3. COC record present b complete upon sample receipt: YorN Rei uished by: (Signature) Time Received by: (SigWM) Date Time Relinquished by: (Signature) Date Time Received by, (Signature) Date Time Relinquished by. (Signature) Date Time ReceW by: (Signature) Date Time TSLC 1 07PY - ORIGINAL YELLOW COPY - CLIENT PINK COPY -LABORATORY Client Name PCTSL Date and Time Receive 12/5/2007 3:40:00 PM ` Work Order Numbe 0713771 Received by CAM Checklist completed by—�� �.� �� Reviewed by Signature Date Initials D e Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes >/ No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ NotApplicable Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable ❑d Chain of custody present? Yes W No ❑ Chain of custody signed when relinquished and received? Yes No ❑ Chain. of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes O No ❑ Sample containers intact? Yes .-No ❑ Sufficient sample volume for indicated test? Yes No ❑ tll samples received within holding time? Yes © No ❑ Oontainerlfemp Blank temperature in compliance? Yes 0 No ❑ Water- VOA vials have zero headspace? No VOA vials submitted Yes ❑ No ❑ Water- pH acceptable upon receipt? Yes ❑ No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section be --------------------------------------------- --------------------------------------------- Client contacted Date contacted: Person contacted Contacted by: Regarding Comments: Corrective Action 00 N O Cn N INTERNAL CH -AIN OF CUSTODY CLIEI�Tf:. C DELIVERABLES: V�� - AROUND T& E:a S SDGCASE#: MATRIX: pH CHECK Y or N Tr[]CASlIRKS: RAVED BY- C /1 SIGNATURE: DATE: ca(sf rA'.Tw: /6: L/ O r. f CLIENT ID H2M LAD N DATE COLLECTED BOTTLE 'TYPEBOTTLES N OF TESTS - REQUESTED _s koc _csD _. _s lil- 41, „ n ' n METALS P 0247 N O E-� IH2A UAUS,� ISCO CLIENT.,sm INTERNAL CHAIN OF CUSTODY i x%J . DATE TIME SAMPL E.. REDSi5¢ii ]t BY Sn';P3,E R IVED BY BOTTLE TYPE PURPOSE OF CHANGE OF CUSTODY INIT HIGw , 9I0 �� _ 1-tli S (li 12 io to=� HI slow H=� Dl( . - •IGN 91019 . BION SION slow SIGN slow slow .. sION SIGN ' slow SION SIGN SIGN Slow SIGN , slow SIGN sIONSIGN SION G slow 'BION - SIGN BION SIGN SIO" SION SIGN SIGN SION SION SIow SIGN SION SIGN 9I0 SIGN ION SIGN SIGN SIGN SION SIGN I METALS 0249 IH 2A UAUSs INC. INTERNAL CHAIN OF CUSTODY r7l� CLIENT -y -- DELIVERABLES- e UN AROUND SDG 4--�A LN -a CASE 9: MATRIX: PH CHECK Y RENURKS: RECEIVED BY: SIGNATURE: WET CHEMISTRY I� WET CHEMISTRY POOL CLIENT #'— SDG if -21y �� DATE TIME A INC 11b I —SM POOL CLIENT #'— SDG if -21y �� WET CHEMISTRY c DATE TIME 1 11b I —SM L-lq-"u7 1513 /F _ A WET CHEMISTRY c /F _ IN esm �A, "ll WET CHEMISTRY c A� iso 1 c. a.r u..R.ttt.. UV 44TAT_rnTR 2 4 EXTERNAL CHAIN OF CUSTODY Tel. (631) 694-3040Fax: (631) 420-8436 CLIENT: HM SDG NO: AM PROJECT NE/NUMBER So 6/%-9 0 L / v d F l L 200% Q o. -� LU Q g a.. ori) t• .� NOTES: Project Contact P/tIqT 3 6 0CL Phone Number. Ro(i-TIME x 14S4 1916,49' ' Al. jg'.T5RS PIS/Quote # ; GA/V s OH"T0701 C -A. SAMPLERS: (signatureyClient V DELIVERABLES: S 70-b ANALYSIS REQUESTED TURNARQUND TIME: DAYS �I bA Y S ORGANIC INORG. , DATE TIME IMATRIXFIELD I.D. U LAB I.D. NO. REMARKS: 09.30 M W - 3.0 /000 nrnvv-6s ,030 w_- 60 //00 /v1 . d DV 0�kkerrlFe Relinquished (S tore) Date 1-46/0 Time 13110 Received by: (Signature) Date ID CQ Time 13.1 LABORATORY USE ONLY Discrepancies Between1. Sample Labels and COC Record? Y or N Explain: or Ha 2 Aunbnt or chillednd Delivered— AUbHM , Temp - 3. Roceived in good common: Y or N . 4. Pnperly preserved: Y 00 Teoe was: t. Present on outer package: Y or N 2 Unbroken on outer package: Y or N 3. COC record present 6 complete upon sample receipt: Y orN Relinquished by: (S�ture) a Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by: (Signature) Date nme Relinquished by (Signature) Date Tlme Received by (Sipnaturo) Date Time WHITE COPY - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY TSLO12 S13 Client Name PCTSL Date and Time Receive 12/6/2007 1:16:00 PM Work Order Ntimbe 071381 Received by CAM Checklist completed by Reviewed by Signature Dale Initials Dale Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes W No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable❑ Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable Chain of custody present? Yes 0 No ❑ Chain of custody signed when relinquished and received? Yes No ❑ Chain of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes No ❑ Sample containers intact? Yes ❑d No ❑ sufficient sample volume for indicated test? Yes W No ❑ 11 samples received within holding time? Yes No ❑ Container(remp Blank temperature in compliance? Yes ❑� No ❑ Water - VOA vials have zero headspace? No VOA vials submitted Yes ❑ No ❑ Water- pH acceptable upon receipt? Yes ❑d No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed.in the comments section be — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - Client contacted Contacted by: Comments: Corrective Action Date contacted: Regarding Person contacted CLIENT ID 112M LAD N DAVE COLLECTED BOTTLE TYPE it OF BOTTLES TESTS REQUESTED t 1 o ro 4a e�lcoJc Z� "(0 W �� SSD 11 1 q 11 - It IY k a n . METALS ®2'74 cn N O N 8s0]I _ SIGN - SIGN 'Fti L� , alcor SI SI ON. slow slow 31cm u i1/ p%!i ... 5foft S .. .. slow slow BIGa .Blom slow SIGN slow SIGN 3IOit 3I ON SIGN SIGN SION SIGN SIGN SIGN r� N O METALS P 02'715 ILAUS9 INC INTERNAL -CHAIN OF DELIVERABLES: 4 CLmip. lz�-, L SDG -9: _rq CASF, 9: MATR REMARKS: RECEIVED BY:Def):flSIGNATURE: .- - -. r PJ USTODY, URN AROUND TWE X: pH CHECK -y as N, CLIENT ID 112M LAB val5bll -60t DATE COLLECTED1 igLl. J a BO , Ty?E 1E�F 0 OF BOTTLES nQuFSTED Cw. _G C- al WET CHEMISTRY cMMT: pC L sDa � a INTERNAL CHAIN.OF CUSTODY WET CHEMISTRY 00 N O F� oil 7 til/%�riG�//,�Mal; WE -- f WET CHEMISTRY P 0140 00 N O F� P 0140 3. SDG NARRATIVES MW-1D MW -8S MW -1S FB 120507 MW -4D MW -3D MW -4S MW -3S MW -5D MW -6D MW -5S MW -6S MW -8D MB -BD Fourteen water samples were received by H2M Labs, Inc. on 12/5/07 and 12/6/07 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA 61E Trace ICP Instrument. Sample MW78D was utilized for QC analysis and reporting. Iron spike analysis did not recover within 75-125%. Since the sample value was greater than four times the spike concentration, post spikes and data qualifiers were not required. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: December 21, 2007 Vincent Stancampiano Vice President Fourteen water samples were received by H2M Labs, Inc. on 12/5/07 and 12/6/07 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: Alkalinity EPA 310.1 Anions: Chloride/Sulfate/Bromide EPA 300.0 _ Biochemical Oxygen Demand EPA 405.1 Chemical Oxygen Demand EPA 410.4 Total Hardness EPA 130.2 SDG NARRATIVE FOR WET CHEMISTRY 17 . EPA 350.1 SAMPLE RECEIVED: 1215/07 & 12//6/07' SDG#: TSLO12 . For Samples: ,. MW-46 MW-8S MW-4S FB 120507- MW-51) MW-1D I MW-5S MW-1S MW-61) MW-31) MW-6S MW-3S MW-8D MW-BD Fourteen water samples were received by H2M Labs, Inc. on 12/5/07 and 12/6/07 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: Alkalinity EPA 310.1 Anions: Chloride/Sulfate/Bromide EPA 300.0 _ Biochemical Oxygen Demand EPA 405.1 Chemical Oxygen Demand EPA 410.4 Total Hardness EPA 130.2 Ammonia EPA 350.1 Sample MW -8D was utilized for QC analysis and reporting. Nitrate EPA 353.2 . Phenols EPA 420.1 Total Dissolved Solids . - _ _. EPA 160.1. Total Kjeldahl Nitrogen EPA 351.2 Total Organic Carbon EPA 9060 Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: January 2, 2008 r Vincent Stancampiano Vice President 4. SAMPLE REPORTS 4.1 METALS 4.2 WET CHEMISTRY QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An . explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N Matrix spike sample recovery not within control limits. S The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. . M (Method) Qualifiers P - Analyzed by ICP. M - Analjrzed.by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric .Method. NR- Analyte not Required. Concentration Units (ug/L or mg/kg -dry weight): UG/L CAS No. Analyte U.S. EPA - •CLP,. . M 7440-43-9 Cadmium 1 B EPA SAMPLE NO 7440-70-2 Calcium INORGANIC ANALYSIS DATA SHEET P 7439-89-6 Iron 449 P 7439-92-1 MW -1D Lab Name: H2M LABS, INC.. P 7439-95-4 Magnesium 8450 Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Potassium Lab Sample ID: 0713771-001 Level (low/med):. LOW Sodium Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg -dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.80 B P 7440-70-2 Calcium 20300 P 7439-89-6 Iron 449 P 7439-92-1 Lead 2.5 B I P 7439-95-4 Magnesium 8450 P 7439-96-5 Manganese 157 P 7440-09-7 Potassium 3560 B P 7490-23-5 Sodium 14700 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 1 of 9 Laboratory Manager U2A "US IfelC. 575 Broad Hollow Road, MdAe W 11747 LABORATORY RESULTS (631) 6943040: FAX (631) 42(18436 NYSDOH ID# 10478 ,. Sample Information .' Town of Southold Landfili Lab No. :. 0713771-001 .:,. ;Type :.Groundwater, Origin Attn To Original Client ID. : MW -ID. Collected :1215/2007 2:00:00 PM Received :12/512007 3:40:00 PM Collected By VG Copies To :Original CC. -. Parameter(s) Results Qualifier D.F. -Units Method Number Analyzed Alkalinity, Total (As CaCO3) 33.2 2 mg/L E310.1 12/13/2007 946 AM Chloride 19.0 2 mg/L E300.0 12/19/2007 4:11 PM Sulfate 52.1 2 mg/L E300.0 12/19/2007 4:11 PM Bromide < 0.5 1 mg/L E300.0 12/14/2007 4:37 PM_ BiochemicalOxygen Demand < 2 1 mg/L E405.1 12/06/20071:20 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/20/20071:47 PM Hardness (As CaCO3) 105 5 mg/L El 30.2 12/11/2007 2:34 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12128/200711:29 AM Nitrate as N 2.28 5 mg/L E353.2 12/17/200712:05 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/200711:20 AM Total Dissolved Solids 176 1 mg/L E160.1 12/10/2007 3:11 PM Nitrogen, Kjeldahl, Total 0.19 1 mg/L------ - E351.2 ° ` 121201200710:18 AM - Total Organic Carbon 2.3 1 mg/L SW9060 12/07/2007 8:27 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 1 of 9 Laboratory Manager CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0,.32 U P 7440-70-2 Calcium 9000 U.S. EPA - CLP 7439-89-6 Iron I EPA SAMPLE NO P INORGANIC ANALYSIS DATA SHEET U I P 7439-95-4 Magnesium 5870P MW -1S 7439-96-5 Lab Name: H2M LABS, INC. P 7440-09-7 Potassium Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 . Matrix (soil/water): WATER Lab Sample ID: 0713771-002 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0_0 j Concentration Units (ug/L or mg/kg dry { weight): UG/L j CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0,.32 U P 7440-70-2 Calcium 9000 P 7439-89-6 Iron 2430 P 7439-92-1 Lead 1.4 U I P 7439-95-4 Magnesium 5870P 7439-96-5 Manganese 114 P 7440-09-7 Potassium 2610 B P 7440-23-5 Sodium 38000 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR ,Comments: Date Reported: 12/17/07 Texture: Artifacts: FORM I - IN . ILM04.1 575 Broad Hollm Road, MelvBe NY 11747 ' LABORATORY RESULTS (631)694-3040. FAX (631)4205436 NYSDOHID#10478 Town of Southold Landfill Lab No. 0713771-002 Attn To Original Client ID.: MW -1S Collected :12/5/20071:30:00 PM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Chloride Sulfate Bromide Biochemical Oxygen Demand Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Total Dissolved Solids Nitrogen, IQeldahl, Total Total Organic Carbon Results Qualifier D.F.. Units 9.3 1 mg/L 59.2 2 mg/L 22.6 2 mg/L < 0.5 1 mg/L < 2 1 mg/L <10 1 mg/L 52.0 4 mg/L < 0.10 1 mg/L 3.24 5 mg/L < 5.0 1 Ng/L 179 1 mg/L 0.18 1 mg/L < 1.0 1 mg/L Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 2 of 9 Method Number Analyzed E310.1 12/13/2007 9:54 AM E300.0 12/19/2007 4:25 PM E300.0 12/19/2007 4:25 PM E300.0 12/1412007 4:51 PM E405.1 12106/20071:25 PM E410.4 12/20120071:48 PM E130.2 12/11/2007 2:36 PM E350.1 12/28/200711:30 AM E353.2 12/17/2007 12:06 PM E420.1 12/20/200711.30 AM E160.1 12/10/2007 3:13 PM E351.2 12/20/200710:19 AM SW9060 12/07/2007 8:58 PM Q,„ n /4 Laboratory Manager Lab Name: H2M LABS, INC. Lab Code: 10.478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: .0713771-003 Level (low/med)•. LOW Date Received: :12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS'No. Analyte Concentration C Q M 7440-43-9 jCadmium 0.32 U P 7440-70-2 Calcium 163000 P 7439-89-6 Iron 396 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 71500 P 7439-96-5 Manganese 3620 P 7440-09-7 Potassium 787001 P 7440-23-5 ISodium 242000 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/17/07 FORM I - IN Texture: Artifacts: ILM04.1 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor . . Date Reported; - Page 3 of 9 Laboratory Mas -cri U28* "US, INC® 575Broad Hollow Road, MdWe NY 11747 LABORATORY•RESULTS (631)6943040. FAX (631)42M436 NYSDOHID#10478 SampleJnforrnot ,t Town of Southold Landfill .Lab No. 07137717003 . Type :.,Grounds+ .? Origin:, Attn To : Original Client ID.: MW-40 Collected :12/5/2007 12:00:00 PM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original cc . Parameter(s) Results Qualifier D.F.. Units. Method Number Alkalinity, Total (As CaCO3) 766 20 mg/L E310.1 I2 Chloride 339 16 mg/L E300.0 Sulfate 87.5 10 mg/L E300.0 12: Bromide 2.5 1 mg/L E300.0 '2;14!2(.;:;:" . "_: r;:;. Biochemical Oxygen Demand < 2 1 mg/L E405.1 Chemical Oxygen Demand 53.5 1 mg/L E410.4 I2 2f.12 Hardness (As CaCO3) 760 20 mg/L E130.2 Nitrogen, Ammonia (AS N) 25.0 - 20 mg/l. E350.1 - '1177,7 r (' !'�' 3 i Flit%; Nitrate asN <0.10 1 mg/L E353.2. F'P' Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 2:2•'.;: .:i::r ', = ,, ::? Total Dissolved Solids 1280 4 mg/L E160.1 127 ::"';r :!? I z P Nitrogen, Kjeldahl, Total 37.9 20 mg/L­­­ Total Organic Carbon Total 27.4 1 mg/L SW9060 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor . . Date Reported; - Page 3 of 9 Laboratory Mas -cri U.S. EPA - CLP E INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. �...-. Lab Code: 10478 Case No. SAS No.: SDG No.' Matrix (soil/water): WATER Lab Sample ID: 07137 Level (low/med): LOW Date Received: 12/ ;'21 ,i: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 49800 P 7439-89-6 Iron 930 P 7439-92-1 Lead 2.1'B I P 7439-95-4 Magnesium 22700 P 7439-96-5 'Manganese 11100 P 7440-09-7 Potassium 48600 P 7440-23-5 Sodium 18900 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN Qualifiers: E - Value above quantitation range 0 - Results for Dilution D.F- = Dilution Factor .. Date Reported Page 4 of 9 1,4 Laboratory Manag&., -Z A 575BroadFidlow Road, Melyile NY 11747,' LABORATORY RESULTS (M.1 FAX-'(631)42MW WSDOHID#10478- Sample Informatit..."I'-, Town of Southold Landfill LabNo. 0713771-004 Type G to u n d -.v a, i :.Original Attin To Origin: Client ID. MW -4S Collected :12/5/200711:30:00 AM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original cc Parameter(s) Results Qualifier D.F. Units Method Number &�a.lvzec Alkalinity, Total (As CaCO3) 203 10 mg/L E310.1 12 113 f (.1 G - :U. Chloride 26.0 2 mg/L E300.0 12.j1 'C*!� :: Sulfate 50.3 2 mg/L E306.0 121I9I200-: -'1*92 P-�,4 Bromide < 0.5 1 mg/L E300.0 12114120,07 PM Biochemical Oxygen Demand <2 1 mg/L E405.1 4 2.' 35 P, Chemical Oxygen Demand 13.0 1 mgIL E410.4 12 Hardness (As CaCO3) 240 20 mg/L E130.2 12,.'t!!-20,.*.'.' Nitrogen, Ammonia (As N) 0.31 1 mg/L E350.1 12!28i -,G(;-;, I Nitrate as N 9.34 10 mg/L E353.2 7! 2007 -2,* iO-'3 c!? Phenolics, Total Recoverable < 5.0 1 VOL E420.1 12i201*(07 Total Dissolved Solids 401 1 mg/L E160.1 Nitrogen, Kjeldahl, Total 3.78-- 20 mg/L E351.2 Total Organic Carbon 13.2, 1 mg/L SW9060 Qualifiers: E - Value above quantitation range 0 - Results for Dilution D.F- = Dilution Factor .. Date Reported Page 4 of 9 1,4 Laboratory Manag&., Lab Name: H2M LABS, INC. MW -5D Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water)• WATER Lab Sample ID: 0713771-005 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 102000 P 7439-89-6 Iron 67.6 B P 7439-92-1 ILead 1.4 U I P 7439-95-4 Magnesium 46200 P 7439-96-5 Manganese 11400 P 7440-09-7 .Potassium 117000 P 7440-23-5 Sodium 247000 P -71 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 U2A4 ILAU,�'!!I. 575 Broad Hollow Road, Mdvie NY 11747 LABORATORY RESULTS (631) 6943040. FAX (631)4205436 WSDOH ID# 10478 Sample lnfoM'12 01*'.. Town of Southold Landfill Lab No. 0713771-00.5 % Type: Groundwate" - Attn To Original Origin: Client ID.: MW -5D Collected :12f5/2007 1:00:00 PM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original CC Parameter(s) Results Qualifier D.F. Units Method Number Anaii_; d Alkalinity, Total (As CaCO3) 715 20 mg1L E310.1 Chloride 340 10 mg/L E300.0 2,, Sulfate 46.4 5 mg/L E300.0 1211 Bromide 1.4 1 mg/L E300.0 Biochemical Oxygen Demand < 2 1 mg/L E405.1 Chemical Oxygen Demand 71.3 1 mg[L E410.4 21'2;-,t.'2t_',i.!*' Hardness (As CaCO3) 480 20 mg1L E130.2 12il Nitrogen, Ammonia (As N) 39.7 50 mgIL E350.1 Nitrate as N <0.10 1 mg/L E353.2 2"17 Phenolics, Total Recoverable <5.0 1 pg/L E420.1 2i20; 2 n 07- 12.0i:- PN' Total Dissolved Solids 1090 4 mg/L E160-1 Nitrogen, Kjeldahl, Total 62.9 50- mg/L' E351.2 !:OA Total Organic Carbon 25.5 1 mg/L SW9060 12/07/2607 10 -: i: -1 Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 5 of 9 C*0 Laboratorj Maonaljt� U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS,DATA SHEET MW -5S Lab Name: H2M LABS, INC. Lab Code:_ 10478 Case No. SAS No.: SDG No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: 0713771-006 Level (low/med): LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units'(ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 14000 P 7439-89-6 Iron 68.6 B P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 9500 P 7439-96-5 Manganese 2890 P 7440-09-7 Potassium 6290 P 7440-23-5 ISodium 11900 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/17/07 Texture: Artifacts: FORM I - IN ILM04.1 ..4' U2A1 INC, 575 Broad Hdbw (631)6943040 FAX (631)4W843611747 WSDOHID#10478 LABORATORY RESULTS Sample Information... .Town of Southold Landfill' Lab No. 0713771-006 Type: Groundwater Attn To Original Origin: Client ID:: MW -5S Collected :1215/200712:30:00 PM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Chloride Sulfate Bromide Biochemical Oxygen Demand Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) _Nitrate as N Phenolics, Total Recoverable Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon . Results Qualifier D.F. Units Method Number Analyzed 38.5 1 mg/L E310.1 12/13/2007 10:26 AM 15.6 1 mg/L E300.0 12/19/2007 5:32 PM 37.0 1 mg/L E300.0 12/19/2007 532 PM < 0.5 1 mg/L E300.0 12/14/2007 5:45 PM < 2 1 mg/L E405.1 12/06/2007 1:45 PM 13.0 1 mg/L E410.4 12/20/2007 1:52 PM 96.0 4 mg/L El 30.2 12/11/2007 2:44 PM 0.18 1 mg/L E350.1 12/28/200711:35 AM 1.76 5 mg/L E353.2 12/17/200712:11 PM < 5.0 1 Pg/L E420.1 12/20/2007 12:10 PM 147 1 mg/L E160.1 12/10/2007 3:21 PM 0.40 1 mg/L E351.2 12/20/200710:22 AM 3.8 1 mg/L SW9060 12/07/200711:04 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor r)nt,, Rennrteri • . Page 6 of 9 t W-1 Laboratory Manager % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. - U.S. EPA.- CLP 7440-43-9. lCadmium 0.32 U P 7440-70-2 lCalcium 68700 P 'INORGANIC ANALYSIS DATA SHEET. F.,. Lab Name: H2M LABS, INC. Lead 1.4 U �•- Lab Code: 10478 Case No. SAS No.: SDG.Nc3.. Matrix (soil/water): WATER P Lab Sample ID: 0713;71 Level (low/med) • LOW 7440-23-5 Date Received: . 121.`-./.= % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9. lCadmium 0.32 U P 7440-70-2 lCalcium 68700 P 7439-89-6 Iron 8910 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 34500 P 7439-96-5 manganese 1400 P 7440-09-7 Potassium 81300 P 7440-23-5 Sodium 80900 P Color Before:. COLORLESS Clarity Before: CLEAR Texture:' Calor After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN Laboratovy .L Y a e, ` 575 Broad Hollow Road, Mdvile iVY.11747 LABORATORY RESULTS (631)6943040. FAX (631)420-8436 NYSDOHID#10478 °i I Sample In#0rr;a+ Town -of Southold Landfill Lab No :. 0713771-007..; Type : Gror.r�evs ' Origin: Attn To Original " Client ID.: MW -8D Collected :12/5/2007 11:00:00 AM Received :1215/2007 3:40:00 PM Collected By VG i Copies To ;Original I CC C Parameter(s) Results Qualifier DD=F. Units Method Number A; va,;' Alkalinity, Total (As CaCO3) 438 20 m6/1- E310.1' 12t^ 3: 2i:; . _= iV" -' I' Chloride 126 5 mg/L E300.0 : ,,.�,:, : _;.,..�..z,: • � Sulfate 81.8 5 mg/L E300.0 Bromide 0.9 1 mg/L E300.0 Biochemical. Oxygen Demand < 2 1 mg/L E405.1 - Chemical Oxygen Demand 58.6 1 mg/L E410.4 :2 .M.;: z:::.: :. " •. Hardness (As CaCO3) 380 20 mg/L E130.2 Nitrogen, Ammonia (As N) 30.0 50 mg/L E350.1 Nitrate as N < 0.10 1 mg/L E353.2 Phenolics, Total Recoverable < 5.0 1 ug/L E420.1 Total Dissolved Solids 678 2 mg/L E160-1 Nitrogen, Kjeldahl, Total 43.0 50 mg/L E351.2 -! 't r;'C) _" a `2:2 A E Total Organic Carbon 18.7 1 mg/L SW9060 36:.. Laboratovy 1, EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -8S Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No..: SDG No.: TSLO12 Matrix (soil/water):. WATER Lab Sample ID: 0713771-008 Level (low/med)• LOW Date Received: 12/5/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 744.0-.70-2 .Calcium 37700 P 7439-89-6 Iron 24900 P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 15800 P 7439-96-5 Manganese 152 P 7440-09-7 Potassium 54600 P 7440-23-5 Sodium 31500 P Color Before: COLORLESS Clarity Before: CLEAR Texture:_ Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Repor ed: 12/17/07 FORM I - IN ILM04.1 00 M N O F-+ Sample Information. Town of Southold Landfill Lab No. : 0713771-008 Type: Gro'undwat.--- Attn To Original Origin: ClientlD. : MW -8S Collected :12/5/2007 10:30:00 AM Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original CC Parameter(s) Results Qualifier D.F. Units Method Number Ana!{- Alkalinity, Total (As CaCO3) 253 20 mg/L E310.1 Chloride 43.6 5 mg/L E300.0 12: 1 Sulfate 66.8 5 mg/L E300.0 Bromide < 0.5 1 mg/L E300.0 1 2.! 14 20,07 LD Biochemical Oxygen Demand < 2 1 mg/L E405.1 t 2 J 0 17`1 r 'L::1,: Chemical Oxygen Demand' 38.3 1 mg/L E410.4 Hardness (As CaCO3) 176 4 mg/L E130-2 12:' 7 Nitrogen, Ammonia (As N) 25.0 10 mg/L E350.1 12V. ' �2;`-,C' Nitrate as N <0.10 1 mg/L E353.2 II 2;J 1-`2 (*.-',*;' -4*.' : Phenolics, Total Recoverable < 5.0 1 PgIL E420.1 E212,0/2,3()7 Total Dissolved Solids 378 2 mg/L E160.1 111 ,,7 '3: P.N,, Nitrogen, Kjeldahl Total 46.2 20 mg/L E351.2 '1 2, on Total Organic Carbon 11.1 1 mg/L SW9060 12f06Y2`.-`,lI*,' !Il :1A'! Qualifiers: E -ValUG 2130ve quantitation range D - Results for Dilution D.F. = Dilution Factor . Date Reported: Page 8 of 9 Laboratory ?4-inagei Lab Code: 10478 Case No. SAS No.: SDG Matrix (soil/water): WATER Lab Sample ID: 01137.,..- Level (low/med):. LOW Date Received: 12;'x_2 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 95.9 B P 7439-89-6 Iron 28.4 B P 7439-92-1 Lead 1.4 U P 7439-95-4 Magnesium 15.5 U P 7439-96-5 Manganese 0.39 U P 7440-09-7 Potassium 87.5 B P 744.0-23-5 sodium 62.9 B P` Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments; Date Reported: 12/17/07 FORM I - IN O G� N O F-+ U2AILA IJ INCQ !j 5756roadHollow Road, Melville NY 11747, LABORATORY RESULTS ._ (631)6943040. FAX (631)4208436 NYSDOHID#10478 Sample tnfo"rm' a , Town of Southold Landfill Lab No. 0713771-009 Type: Field Btau4 `" - I Origin: Attn To Original Client ID.: FB 120607 I Collected :12/5/2007 12:00:00 PM j Received :12/5/2007 3:40:00 PM Collected By VG Copies To :Original I CG Parameter(s) Results Qualifier D.F.. Units Method Number Anal:'� : Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 12"! ":2C::,': Chloride < 2.0 1 mg/L E300.0 Sulfate < 5.0 1 mg/L E300.0 Bromide < 0.5 1 mg/L E300.0 +2•`+L2!?;t: ' ♦?': Biochemical Oxygen Demand < 2 1 mg/L E405.1 ? . ;� ,?r:". Chemical Oxygen Demand < 10 1 mg/L E410.4 Hardness (As CaCO3) < 5.0 1 mg/L El 30.2 Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350A :2,28;;'0:: . - ?. Aii -.. Nitrate as N < 0.10 1 mg/L E353.2 12r17;2.1r : _ 15 Phenolics, Total Recoverable < 5.0 1 Ifg/L E420.1 Total Dissolved Solids <10 1 mg/L E160-1 12;" ' :: )t, ` Nitrogen, lCeldahl, Total <0.10 1 mg/L E351.2 Total Organic Carbon < 1.0 1 mg/L SW9060 I i i i I I i I i i w i i Qualifiers: E -Value above quantitation range D - Results for Dilution l + D.F_ = Dilution Factor I Laboratory iv1ai'!a ,.:- Date Reported Page 9 of 9 I 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW 3D Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG •No.: TSLO12 Matrix (soil/water): WATER Lab Sample ID: '0713817-001 Level (low/med):. LOW Date Received: 12/6%2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2. calcium 39100 P 7439-89-6 Iron 6870 P 7439-92-1 jLead 1.4 U P 7439-95-4 Imagnesium 33400 P 7439=96=5 Manganese 3670 P 7440=09-7 Potassium 127000 P 7440-23-5 Sodium 195000 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color Afte.r.:...COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN ILM04.1 Attn To Original Origin: Client ID.: MW -3D Collected :12/6/2007 9:30:00 AM Received :1216/2007 1:16:00 PM Collected By VG Copies To :Original CC Parameter(s) Results Qualifier D.F. Units Method Number Air altizt- Alkalinity, Total (As CaCO3) 839 20 mg/L E310.1 1.21 13 Chloride 233 10, mg/L E300-0 Sulfate 34.3 1 mg/L E300.0 Bromide 1.1 1 mg/L E300.0 Biochemical Oxygen Demand < 2 1 mg/L E405.1 Chemical Oxygen Demand 124 1 mg/L E410.4 Hardness (As CaCO3) 460 20 mg/L E130.2 Nitrogen,, Ammonia (As N) 81.0 50 mg/L E350-1 2 C Nitrate as �N < 0A0 I mg/L E353.2 0 ':'•'' Phenolics, Total Recoverable < 6.0 1 pg/L E420.1 Total Dissolved Solids 928 4 mg/L E160.1 Nitrogen, Kjeldahl, Total 122 100 mg/L E351.2 12.;2GI2,,K�7 AN' Total Organic Carbon 30.8 1 mg/L SW9060 AM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F_ = Dilubon Factor Date Reported Page 1 of 5 1.4 Laboratory Nlanjut-, CAS No. Analyte Concentration C Q M 7440-43-9 U.S. EPA - CLP P 7440-70-2 1 EPA 'SAMPLE NO P INORGANIC ANALYSIS DATA SHEET P 7439-92-1 Lead 1.4 U I P 7439-95-4 MW -3S 24800 Lab Name: H2M LABS, INC.` Manganese 15900 P 7440=09-7 Potassium Lab Coded 10478 Case No. SAS No.: SDG No.: TSLO12 . i Matrix (soil/water): WATER Lab Sample ID: 0713817-002 Level (low/medy:,-,- LOW Date Received: 12'/6/2007 % Solids: 0.0 i Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.34 B P 7440-70-2 Calcium 43700 P 7439-89-6. Iron 43500 P 7439-92-1 Lead 1.4 U I P 7439-95-4 Magnesium 24800 P 7439-96-5 Manganese 15900 P 7440=09-7 Potassium 38900 P 7440-23-5 Sodium "` 54400 P Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: CLEAR Texture: CLEAR Artifacts: Comments: d Date Reported: 12/17/07 N O H FORM I - IN ILM04.1 24 .. .4 575 Broad Hollow Road, M&Ie W 11747 LABORATORY RESULTS (631)6943040. FAX (631),420-84M WSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. :0713817-002 Type Groundwater - Attn To Original Origin: Client ID.: MW-3S Collected :12/6/2007 9:00:00 AM Received :12/6/2007 1:16:00 PM Collected By VG Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 313 20 mg/L E310.1 121131200712:58 PM Chloride 74.9 2 mg/L E300.0 12/19/2007 7:48 PM Sulfate 37.9 2 mg/L E300.0 12/19/2007 7:48 PM Bromide < 0.5 1 mg/L E300.0 12/14/2007 7:47 PM Biochemical Oxygen Demand 3 1 mg/L E405.1 12/07/2007 10:05 AM Chemical Oxygen Demand 66.2 1 mg/L E410.4 12/20/2007 1:59 PM Hardness (As CaCO3) 260 20 mg/L E130.2 12/11/2007 2:58 PM Nitrogen, Ammonia (As N) 17.0 10 mg/L E350.1 12/28/200711:48 AM Nitrate as N < 0.10 1 mg/L E353.2 121171200712:22 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/20071:20 PM Total Dissolved Solids 452 2 mg/L E160.1 12/10/2007 3:35 PM Nitrogen, Kjeldahl, Total 26.0 20 mg/L E351.2 12120/200710:28 AM Total Organic Carbon 1.1 1 mg/L SW9060 12/08/2007 3:48 AM Qualifiers: E -Value above quantitation range D - Results for Dilution .. . D.F. = Dilution Factor Date Reported Page 2 of 5 Laboratory Manager W) d - C/) N r-1 Cl F--1 J r Analyte Concentration C Q M 7440-43-9 U.S. EPA -.CLP 0.32 U P 7440-70-2 Calcium 40800 P 7439-89-6 INORGANIC ANALYSIS DATA SHEET j Lab Name: H2M LABS, INC. Lead 1.4 Lab Code: 10478 Case No. SAS No.: SDG idc: . Matrix (soil/water): WATER P Lab Sample ID: 071: Level (low/med)-: .LOW Date Received: 12/ a Solids: 0.0 4210 I P Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 40800 P 7439-89-6 Iron 126 P 7439-92-1 Lead 1.4 U1 I P 7439-95-4 Magnesium 17500 P 7439-96-5 Manganese 3930 P 7440-09-7 Potassium 4210 B P F441-2-3-5 Sodium 13600 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/17/07 FORM I - IN. Attn To Original Client ID.: MW -6D Collected . :12/6/2007 10:30:00 AM Received - :12/6/2007 1:16:00 PM Collected By VG Copies To :Original CC Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 22.8 1 mg/L E310.1 12/13/20071:06 PM Chloride 34.3 5 mg/L E300.0 12/19/2007 8:01 PM Sulfate 101 5 mg/L E300.0 12/19/2007 8:01 PM Bromide < 0.5 1 mg/L E300.0 12/14/2007 8:00 PM Biochemical Oxygen. Demand < 2 1 mg/L E405.1 12/07/2007 10:10 AM Chemical Oxygen Demand <10 1 mg/L E410.4 12/20/2007 2:00 PM Hardness (As CaCO3) 184 4 mg/L E130.2 12/11/2007 3:00 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/28/200712:00 PM Nitrate as N 9.78 10 mg/L E353.2 12/17/2007 12:23 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/20071:30 PM Total Dissolved Solids 319 1 mg/L E160.1 12/10/2007 3:37 PM Nitrogen, Kjeldahl, Total 0.14 1 mg/L E351.2 12120/200710:28 AM Total Organic Carbon 12.2 1 mg/L SW9060 12/08/2007 4:20 AM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 3 of 5 f� Laboratory Manager Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium :.. U. S. EPA = CLP. P 7440-70-2 Calcium 17900 P 7439-89-6 Iron 473 INORGANIC ANALYSIS DATA SHEET Lead 1.4 Lab Name: H2M LABS, INC. 7439-95-4 Magnesium 4780 L.. Lab Code: 10478 Case No. SAS No.: SDG N-- Matrix (soil/water): WATER Potassium Lab Sample ID: 071.381 -,- P Level (low/med)•:,. LOW 2900 Date Received: 12:i , ,.• Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight) CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 17900 P 7439-89-6 Iron 473 P 7439-92-1 Lead 1.4 U1 P 7439-95-4 Magnesium 4780 B' P 7439-96-5 Manganese 1930 P 7440-09-7 Potassium 8520 P 7440-23-5 Sodium 2900 B P UG/L Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifact-. Comments: Date Reported: 12/17/07 FORM I - IN U_2AA AUSSINIC 575 Broad Hollow Road, Mdvie NY 11747 (631)694-.FAX(631)42M436 WSDOHID#10478 LABORATORY RESULTS � Sample lnformai'(---',,. Town of Southold Landfill Lab No. 0713817-004 Type: Groundwaif' Attn To : Original Client ID.: MW -6S Collected :12/6/200710:00:00 AM Received :1216/2007 1:16:00 PM Collected By VG Copies To :Original cc Origin-. Parameter(s) Results Qualifier D.F. Units Method Number Anwv-�.t:!,.' Alkalinity, Total (As CaCO3) 58.2 4 mg/L E310.1 121�: ,' Chloride 5.6 1 mg/L E300.0 121', Sulfate 7.1 1 mg/L E300.0 1211? %:';"t Bromide < 0.5 1 mg/L E300.0 Biochemical Oxygen Demand < 2 1 mg/L E405.1 Chemical Oxygen Demand 23-1 1 mg/L E4110.4 12 j, Hardness (As CaCO3) 72.0 4 mg/L El 30.2 Nitrogen, Ammonia (As N) < 0.10 1 mgIL E350.1 Nitrate as N 1.20 5 mg[L E353.2 12:" Phenolics, Total Recoverable <5.0 1 Pg/L E420.1 Total Dissolved Solids 117 1 mgIL E160.1 Nitrogen, Kjeldahl, Total 0.63 1 mg/L E351,2 Total Organic Carbon, 7.2 1 mg/L SW9060 Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported Page 4 of 5 Laboratory iljlanag:�; V) Fq 1 INORGANIC ANALYSIS DATA 'SHEET I. Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SAS No.: SDG N:. Matrix (soil/water): WATER Lab Sample ID: 0713,= Level (low/med) : LOW Date Received: 121/ 6 2 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.32 U P 7440-70-2 Calcium 43100 P 7439-89-6 Iron 109 P 7439-92-1 Lead 1.4 U I P 7439-95-4 Magnesium 18600 P 7439-96-5 Manganese 3990 P 7440-09-7 Potassium 4340 B P 7440-23-5 Sodium 13900 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/17/07 FORM I - IN Texture: Artifacts: Qualifiers: E -Value above quantitation range -, 1A-_ D - Results for Dilution D.F. = Dilution Factor Date Reported : Laboratory Page 5 of 5 ;n . v „575Broad Hoflow Road; MdW W,11747 LABORATORY RESULTS.. - m(631)fi943090.FAX (631)42U436NYSDOHID#10478 I Sample lnforma ` Town of Southold Landfill .. Lab No 0713817-005 • _t. .. - t - - Type:. Ground Origin,': I Attn To. Original Client ID.: MB -BD Collected :12/6/2007 11:00:00 AM I Received -12/6/2067 1:16:00 PM Collected By VG 'Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number -Alkalinity, Total (As CaCO3) 23.4 1 mg/L E310.1 12;:,;.' Chloride 34.0 5 mg/L E300.0 Sulfate 99.4 5 mg/L E300.0 12r: t., Bromide <0.5 1 mg/L E300.0 2'� a,;;,?::•:` ..i r; I Biochemical Oxygen Demand <2 1 mg/L E405.1 Chemical Oxygen Demand <10 1 mg/L E410.4 11 r21 .-i'i Hardness (As CaCO31 176 4 mg/L' E130.2 Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12 2c:20_' Nitrate as N 9.21 10 mg/L E353.2 .12PII Phenolics, Total Recoverable < 5.0 " 1 pg/L E420.1 2! i Total Dissolved Solids 309 1 mg/L E160.1 Nitrogen, Kjeldahl, Total.... :. .. _ 0.14 _. , .-.. A ,._. mg/L, E351.2 ; Total Organic Carbon 1.5 1 mg/L , SW9060 Qualifiers: E -Value above quantitation range -, 1A-_ D - Results for Dilution D.F. = Dilution Factor Date Reported : Laboratory Page 5 of 5 5. DUPLICATE SAMPLE RESULTS 5.1 METALS 5.2 WET CHEMISTRY Concentration Units (ug/L or mg/kg dry weight): UG%L Control Analyte Limit Sample (S) C M� RPD Q M Cadmium 0.3235 U 0.3235 U P Calcium 68669.9600 71210.4200 3.6 U.S. EPA.- CLP - . 9241.1800 6 EPA SAMPLE NO Lead 1.3800 Ul DUPLICATES P Ma nesium 34497.4800 1 35831.5500 3.8 P MW -8D 1404.8000 Lab Name: H2M LABS, INC. Contract: Potassium 81279.0800 83697.7700 2.9 Lab Code: 10478 Case No. SAS No.:. SDG No.: TSLO12 I Matrix (soil/water): WATER Level (low/med): LOW % Solids for Sample: 0.0 % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG%L Control Analyte Limit Sample (S) C Duplicate (D) C RPD Q M Cadmium 0.3235 U 0.3235 U P Calcium 68669.9600 71210.4200 3.6 P Iron 8907.9700 9241.1800 3.7 P Lead 1.3800 Ul 1.3800 U P Ma nesium 34497.4800 1 35831.5500 3.8 P Manganese 1404.8000 1453.2900 3.4 P Potassium 81279.0800 83697.7700 2.9 P Sodium 80863.2100 83210.0800 2.9 P M 0/) N O FORM VI - IN ILM04.1 H2M LABS, INC. Date: 31 -Dec -0 QC SUMMARY REPORT SDG: TSLO12 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analvte Result Units Amount Result %REC Limits Value %RPD UCL mb-121307 mb-121307 Alkalinity, Total (As CaCO3) < 1 mg/L MB -120707 Ics-121307 Ics-121307 Alkalinity, Total (As CaCO3) 21.7 mg/L 25 < 1 87 80 120 0713771-007aMS MW-8DMS Alkalinity, Total (As CaCO3) 919 mg/L 500 438 96 75 125 0713771-007aDUP MW-8DDUP Alkalinity, Total (As CaCO3) 445 mg/L 1438 1.6 20 MB -120607 MB -120607 Biochemical Oxygen Demand <2 mg/L LCS-120607 LCS-120607 Biochemical Oxygen Demand 184 mg/L 200 < 2 92 80 120 0713771-007ADUP MW-8DDUP Biochemical Oxygen Demand < 2 mg/L < 2 20 MB -121407 MB -121407 Bromide <0.5 mgIL MB -120707 MB -120707 jBiochemical Oxygen Demand <2 mg/L 0713771-007AMS MW 8DMS Bromide 1.9 mg/L 1 0.9 102 75 125 LCS-120707 ILCS-120707 jBlochemicai Oxygen Demand 1 174 mg/L 1 200 1 < 2 1 87 180 1120 _ 58.6 4.4 20 .: 1IDDLI MB -120607 MB -120607 Biochemical Oxygen Demand <2 mg/L LCS-120607 LCS-120607 Biochemical Oxygen Demand 184 mg/L 200 < 2 92 80 120 0713771-007ADUP MW-8DDUP Biochemical Oxygen Demand < 2 mg/L < 2 20 MB -121407 MB -121407 Bromide <0.5 mgIL LCS-121407 LCS-121407 Bromide 2.4 mg/L 2.5 < 0.5 96 90 110 0713771-007AMS MW 8DMS Bromide 1.9 mg/L 1 0.9 102 75 125 0713771-007ADUP MW 8DDUP Bromide 0.9 mg/L 10.9 0 20 MB -122007 MS -122007 Chemical Oxygen Demand <10 mg/L LCS122007 LCS122007 Chemical Oxygen Demand 973 mg/L 1000 < 10 97 80 120 0713771-007BMS MW-8DMS Chemical Oxygen Demand 1050 ( mg/L 1000 58.6 99 75 125 0713771-0076DUP _ MW-8DDUP �— Chemical Oxygen Demand 56.1 Tmg/L _ 58.6 4.4 20 MB -121907 __.._._— Nil 12190-F Chloride t c 2 mgtl T I..0 - 43i!'%' _t" -1219(77' GhlUricle 9 ;l ? 0 % 92 1 90� 1'Zi } ._v. 07 13 r 1n S _.... - -...,. yi!%: °U(14 ,-_ -. Ca CEt 5 • s!; �i . ..,. = F' .: 1IDDLI TSLO12 S54 QC SUMMARY REPORT SDG: TSL012 Spike Sample Recovery RPDRer %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121107 MB -121107 Hardness (As CaCO3) < 5 mg/L LCS-121107 LCS-121107 Hardness (As CaCO3) 1020 mg/L 1000 < 5 102 80 120 0713771-007Cms MW-BDMS Hardness (As CaCO3) 2440 mg/L 2000 380 103 75 125 0713771-007Cdup MW-BDDUP Hardness (As CaCO3) 420 mg/L 380 10 20 MB -121707 MB -121707 Nitrate as N < 0.1 mg/L LCS-121707 LCS-121707 Nitrate as N 1.14 mg/L 1.13 <0.1 1 101 80 11201 0713771-007BMS MW-BDMS Nitrate as N 0.52 mg/L 0.5 < 0.1 1 104 1 75 11251 0713771-007BDUP MW-8DDUP Nitrate as N < 0.1 mg/L I I < 0.1 20 mb-24238 mb-24238 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS-24238 LCS-24238 Nitrogen, Ammonia (As N) 1.12 mg/L 1 < 0.1 112 80 120 0713771-007BMS MW-8DMS Nitrogen, Ammonia (As N) 35.8 mg/L 5 30.0 117 75 125 0713771-007BDUP MW-8DDUP Nitrogen, Ammonia (As N) 30.0 mg/L 30.0 0 20 MBI -24152 MB1-24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L MB -24152 MB -24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS1-24152 LCS1-24152 Nitrogen, Kjeldahl, Total 3.91 mg/L 4 < 0.1 98 80 120 LCS-24152 LCS-24152 Nitrogen, Kjeldahl, Total 3.87 mg/L 4 < 0.1 97 80 120 0713771-007BMS MW-8DMS Nitrogen, Kjeldahl, Total 46.8 mg/L 4 43,0 95 75 125 0713771-007BDUP MW-8DDUP INitrogen, Kjeldahl, Total 43.0 mg/L 43.0 0 20 MB -24205 MB -24205 Phenolics, Total Recoverable < 5 LCS-24205 t rr007MAS iLCS-2.4205 VvDMS Phenolics, Total Recoverable PhanolcTotal Recoverable 129.2 ! un/L30- < _-9-7 . : . 8-0- 120 _- -_ - - - +i tL "9f 75 125 19.? o �20C TSLO12 S55 QC SUMMARY REPORT SDG: TSLO12 " Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121907 MB -121907 Sulfate < 5 mg/L LCS-12.1907 LCS-121907 Sulfate 9.0 mg/L 10 < 5 90 90 110 0713771-007Ams MW-8DMS Sulfate 129 mg/L 50 81.8 94 75 125 0713771-007Adup MW-8DDUP Sulfate 81.9 mg/L 81.8 0.12 20 MB -121007 MB -121007 Total Dissolved Solids <10 mg/L LCS-121007 LCS-121007 Total Dissolved Solids 292 mg/L 300 <10 97 80 120 0713771-007AMS MW-8DMS Total Dissolved Solids 1270 mg/L 600 678 99 75 125 0713771-007ADUP MW-8DDUP Total Dissolved Solids 674 mg/L 678 0.59 20 v MB -120707 MB -120707 Total Organic Carbon < 1 mg/L LCS-120707 LCS-120707 Total Organic Carbon 27.6 mg/L 25 <1 110 80 120 0713771-007EMS MW-8DMS Total Organic Carbon 28.5 mg/L 10 18.7 98 75 125 0713771-007EDUP MW 8DDUP Total Organic Carbon 19.0 mg/L 18.7 1.1 20 TSLO12 S56 6. SPIKE SAMPLE RESULTS 6.1 METALS 6.2 WET CHEMISTRY U.S. EPA - CLP 5A EPA SAMPLE NO SPIKE .SAMPLE RECOVERY . MW-8DS Lab Name: H2M LABS,- INC. Contract: Lab Code: - 10478 Case No. SAS No.: SDG No.:TSL012 Matrix (soil/water): WATER Level (low/med):LOW +) % Solids for Sample: 0.0 ! Concentration Units (ug/L or mg/kg dry weight).: UG/L { Analyte Control Limit %R Spiked Sample Result (SSR) C Sample Result (SR) Spike C Added (SA) %R Q M Cadmium 75-125 48.2300 0.3235 U 50.00 96.5 P Iron 10282.9200 8907.9700 1000.00 1 137.5 P Lead 75-125 19.2907 1.3800 U 20.00 96.5 P, Manganese 75-125 1946.9700 1404.8000 500.00 108.4 P Comments: FORM V (Part 1) - IN ILM04.1 00 N O C4 H2M LABS, INC. Date: 31 -Dec -07 QC SUMMARY REPORT SDG: TSLO12 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID• Analyte Result Units Amount Result %REG Limits Value %RPD UCL mb-121307 mb-121307 Alkalinity, Total (As CaCO3) < 1 mglL Ics-121307 Ics-121307 Alkalinity, Total (As CaCO3) 21.7 mg/L 25 < 1 87 80 120 0713771-007aMS MW-8DMS Alkalinity, Total (As CaCO3) 919 mglL 500 438 96 75 125 0713771-007aDUP MW-8DDUP Alkalinity, Total (As CaCO3) 445 mg/L 438 1.6 20 MB -120607 MB 120607 BiochemicalOxygen Demand <2 mg/L MB -120707 MB -120707 jBiochemical Oxygen Demand <2 mg/L 0713771-007ADUP MW-8DDUP Biochemical Oxygen Demand <2 mg/L —<2— 77:W 0713771-007ADUP LCS-120707 ILCS-120707 jBiochemical Oxygen Demand 174 mg/L 200 < 2 1 87 180 1120 MB -120607 MB 120607 BiochemicalOxygen Demand <2 mg/L LCS-120607 LCS-120607 Biochemical Oxygen Demand 184 mg/L 1 200 <2 92 80 120 0713771-007ADUP MW-8DDUP Biochemical Oxygen Demand <2 mg/L —<2— 77:W MB -121407 MB 121407 Bromide <0.5 mg/L LCS-121407 LCS-121407 Bromide 2.4 mg/L 2.5 < 0.5 96 90 110 0713771-007AMS MW-8DMS Bromide 1.9 mg/L 1 0.9 102 75 125 0713771-007ADUP MW-8DDUP Bromide 0.9 mg/L 0.9 0 20 MB -122007 MB -122007 Chemical Oxygen Demand <10 mg/L LCS122007 LCS122007 Chemical Oxygen Demand 973 mg/L 1000 <10 97 80 120 0713771-007BMS MW-8DMS Chemical Oxygen Demand 1050 mg/L. 1000 58.6 99 75 125 0713771-007BDUP MW-8DDUP Chemical Oxygen Demand 56.1 mg/L 58.6 4.4 20 MB -121907 MB -121907 Chloride <2 mg/L LCS-121907 LCS-121907 Chloride 9.2 mg/L 10 < 2 92 90 110 0713771-007Ams MW-8DMS Chloride 171 mg/L 50 126 89 75 125 0713771-007Adup MW-8DDUP Chloride 126 mg/L 126 0 20 TSLO12 S59 QC SUMMARY REPORT SDG: TSL012 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121707 MB -121107 MB -121107 Hardness (As CaCO3) < 5 mg/L LCS-121707 Nitrate as N LCS-121107 LCS-121107 Hardness (As CaCO3) 1020 mg/L 1000 < 5 102 80 120 d20 0.52 mg/L 0.5 < 0.1 104 75 125 0713771-007Cms MW-8DMS Hardness (As CaCO3) 2440 mg/L 2000 380 103 75 125 Nitrogen, Kjeldahl, Total 3.87 0713771-007Cdup MW-8DDUP Hardness (As CaCO3) 420 mg/L 380 10 46.8 MB -121707 MB -121707 Nitrate as N < 0.1 mg/L LCS-121707 LCS-121707 Nitrate as N 1.14 mg/L 1.13 < 0.1 101 80 120 0713771-007BMS MW-8DMS Nitrate as N 0.52 mg/L 0.5 < 0.1 104 75 125 0713771-007BDUP MW-8DDUP Nitrate as N < 0.1 mg/L < 0.1 20 mb-24238 mb-24238 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS-24238 LCS-24238 Nitrogen, Ammonia (As N) 1.12 mg/L 1 < 0.1 112 80 120 0713771-007BMS MW-8DMS Nitrogen, Ammonia (As N) 35.8 mg/L 5 30.0 117 75 125 0713771-007BDUP MW-8DDUP Nitrogen, Ammonia (As N) 30.0 mg/L 30.0 0 20 MBl-24152 MB1-24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS-24205 MB -24152 MB -24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L MW-SDMS LCS1-24152 LCS1-24152 Nitrogen, Kjeldahl, Total 3.91 mg/L 4 < 0.1 98 80 120 LCS-24152 LCS-24152 Nitrogen, Kjeldahl, Total 3.87 mg/L 4 • < 0.1 97 80 120 0713771-007BMS MW-8DMS Nitrogen, Kjeldahl, Total 46.8 mg/L 4 43.0 95 75 125 0713771-007BDUP MW-8DDUP INitrogen, Kjeldahl, Total 43.0 mg/L I 1 1 43.0 0 20 MB -24205 MB -24205 Phenolics, Total Recoverable < 5 ug/L LCS-24205 LCS-24205 Phenolics,Total Recoverable 29.2 ug/l.30 <5 97 80 120 0713771-007BMS MW-SDMS Phenolics, Total Recoverable 19.2 ug/L 20 <5 96 75 125 0713771-007Bdup MW-8DDUP Phenolics, Total Recoverable <5 ug/L <5 20 TSLO12 S60 I SDG: TSLO12 Total Dissolved Solids <10 mg/L LCS-121007 LCS-121007 QC SUMMARY REPORT Sample ID: Client Sample ID: Analyte Result Units Spike Amount Sample Result Recovery RPDRef %RPD %REC Limits Value %RPD UCL MW-8DDUP Sulfate 81.9 mg/L 81.8 0.12 20 MB -121907 MB -121907 Sulfate <5 mg/L LCS-121907 LCS-121907 Sulfate 9.0 mg/L MB -121007 MB -121007 Total Dissolved Solids <10 mg/L LCS-121007 LCS-121007 Total Dissolved Solids 292 10 < 5 90 90 110 0713771-007Ams MW-8DMS Sulfate 129 mg/L 50 81.8 94 75 125 0713771-007Adup MW-8DDUP Sulfate 81.9 mg/L 81.8 0.12 20 MB -121007 MB -121007 Total Dissolved Solids <10 mg/L LCS-121007 LCS-121007 Total Dissolved Solids 292 mg/L 300 <10 97 80 120 0713771-007AMS MW-8DMS Total Dissolved Solids 1270 mg/L 600 678 99 75 125 0713771-007ADUP MW-8DDUP Total Dissolved Solids 674 mg/L 678 0,59 20 MB -120707 MB 120707 Total Organic Carbon < 1 mg/L LCS-120707 LCS-120707 Total Organic Carbon 27.6 mg/L 25 <1 110 80 120 0713771-007EMS MW-8DMS Total Organic Carbon 28.5 mg/L 10 18.7 98 75 125 I 0713771-007EDUP MW-8DDUP Total Organic Carbon 19.0 mg/L 1 1 18.7 1.1 20 TSLO12 S61 7. BLANK SUMMARY DATA AND RESULTS 7.1 METALS 7.2 WET CHEMISTRY Analyte Initial Cal,ib. Blank. (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 C Prepa- ration Blank C M Cadmium 0.3 U 0.3 U1 0.3 U1 0.3 U 0.324 U P Calcium 16.0 U --16.0 U 16.0 U 16.0 U 15.966 U P Iron 24.2 U 24.2 U 24.2 U 24.2 U 24.215 U P Lead 1.4 U 1.4 U 1.4 U 1.4 U 1.380 U P Magnesium 15.5 U 15.5 U 15.5 U 15.5 U 15.480 U P Manganese 0.4 U 0.4 U 0.4 U 0.4 U 0.570 B P Potassium 39.0 B 51.3 B 44.2,B 42.2 B 44.700 B P Sodium 16.3 U 16.3 U 17.11 B 28.2 B 16.339 U P .. M C/) N r ---q _ O FORM III - IN ILM04.1 Lab Name: H2M LABS, INC.- Contract: Lab Code: 10478• Case No. SAS No..: -SDG No.: TSLO12 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Analyte Initial Calib. Blank (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 Prepa- ration C Blank C M Cadmium L 0.3 U1 0.3 U1 P Calcium 16.0 U :16.1 BI P. Iron 24.2 U 24.2 Ul P Lead -1.4 B -2.4 Bi P Magnesium 15.5 U 16.0 B P Manganese 0.4 U 0.4 U P Potassium 44.8 B 39.6 B P Sodium 54.2 B 25.7 B P FORM III - IN ILM04.1 d' 110 CIO N O C/) H2M LABS, INC Date: 31 -Dec -07 QC SUMMARY REPORT SDG: TSLO12 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID• Analyte Result Units Amount Result %REC Limits Value %RPD UCL mb-121307 mb-121307 Alkalinity, Total (As CaCO3) < 1 mg/L Ics-121307 Ics-121307 Alkalinity, Total (As CaCO3) 21.7 mg/L 25 < 1 87 80 120, 0713771-007aMS MW-8DMS Alkalinity, Total (As CaCO3) 919 mg/L 500 438 96 75 125 0713771-007aDUP MW-81DDUP Alkalinity, Total (As CaCO3) 445 mg/L 438 1.6 20 MB -120707 MS -120707 jBlochemical Oxygen Demand <2 mg/L LCS-120707 ILCS-120707 jBiochemical Oxygen Demand 174 mg/L 1 200 1 <2 1 87 180 11201 MB -120607 MB -120607 jBiochemiical Oxygen Demand < 2 mg/L LCS-120607 LCS-120607 Biochemical Oxygen Demand 184 mg/L 200 < 2 92 80 120 0713771-007ADUP MW-8DDUP jBiochemical Oxygen Demand < 2 mg/L 1 <2 20 MB -121407 MS -121407 Bromide < 0.5 mg/L LCS-121407 LCS-121407 Bromide 2.4 mg/L 2.5 < 0.5 96 90 110 0713771-007AMS MW-8DMS Bromide 1.9 mg/L 1 0.9 102 75 125 0713771-007ADUP MW-80DUP Bromide 0.9 mg/L 0.9 0 20 MB -122007 MB -122007 Chemical Oxygen Demand <10 mg/L LCS122007 LCS122007 Chemical Oxygen Demand 973 mg1L 1000 < 10 97 80 120 0713771-007BMS MW-8DMS Chemical Oxygen Demand 1050 mg/L 1000 58.6 99 75 125 0713771-007BDUP MW-8DDUP Chemical Oxygen Demand 56.1 mg/L. 5$.6 4.4 20 1 7 7 I < 2 tYttj/l. . �..£{r. LU:>>.^?1qn • t_{ J-121901 Chiwide 3.2 d-1 !;i - <292 - ' .:.':)`'• G.f -i7.; ., r„-,•:• ... 101,Nt.,+ c :, F. .. -t ;, i ;;tGii: 75 TSLO12 S65 QC SUMMARY REPORT SDG: TSL012 Spike Sample Recovery RPDRef %RPD Sample ID• Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121107 MB -121107 Hardness (As CaCO3) <5 mgIL LCS-121107 LCS-121107 Hardness (As CaCO3) 1020 mg/L 1000 < 5 102 80 120 0713771-007Cms MW-8DMS Hardness (As CaCO3) 2440 mg/L 2000 380 103 75 125 0713771-007Cdup MW-8DDUP Hardness (As CaCO3) 420 mg/L 380 10 20 MB -121707 MS -121707 Nitrate as N < 0.1 mg/L LCS-121707 LCS-121707 Nitrate as N 1.14 mg/L 1.13 < 0.1 101 80 120 0713771-007BMS MW-8DMS Nitrate as N 0.52 mg/L 0.5 < 0.1 104 75 125 0713771-007BDUP MW-81DDUP Nitrate as N < 0.1 mg/L < 0.1 20 mb-24238 mb-24238 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS-24705 LCS-24238 LCS-24238 Nitrogen, Ammonia (As N) 1.12 mg/L 1 < 0.1 112 80 120 0713771-007BMS MW-8DMS Nitrogen, Ammonia (As N) 35.8 mg/L 5 30.0 117 75 125 0713771-007BDUP MW-8DDUP Nitrogen, Ammonia (As N) 30.0 mg/L 30.0 0 20 MBI -24152 MBI -24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS-24705 MB -24152 MB -24152 Nitrogen, Kjeldahl, Total < 0.1 mg/L Pd1N1-BDf�/f LCS1-24152 LCSI-24152 Nitrogen, Kjeldahl, Total 3.91 mg/L 4 <0.1 98 80 120 LCS-24152 LCS-24152 Nitrogen, Kjeldahl, Total 3.87 mg/L 4 < 0.1 97 80 120 0713771-007BMS MW-8DMS Nitrogen, Kjeldahl, Total 46.8 mg/L 4 43,0 95 75 125 0713771-007BC MW-8DDUP INitrogen, Kjeldahl, Total 43.0 mgtL 43.0 0 20 MB -•24205 SMB -24205 lPhenolics, Total Recoverable Total Recoverable ( <5 1 ug/t_ 29.2 i ugit 30 <5 97— 80 120 LCS-24705 LCS-24205 Phenolics. �_ --— _... Oi'1'>7'' -OOic IVi• Pd1N1-BDf�/f _ _�. -- -- - - ----- -- — - - — Phe olics. Total RQcove.rable 19.?. 7 ug,'L i i.. I 20~' ' 6 96 i 75 1125!20 (1, +3; +-[.rU: �.+uc, 1 idJ-£•,L'fi1UF- i : + +P. e:no(ic >. Total Recoverable �,1�L.. 5. TSLO12 S66 f�• QC SUMMARY REPORT SDG: TSL012 Spike Sample Recovery RPDRef %RPD Sample ID• Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121907 MB -121907 Sulfate < 5 mg/L LCS-121907 LCS-121907 Sulfate 9.0 mg/L 70 <5 90 90 110 0713771-007Ams MW-8DMS Sulfate 129 mg/L 50 81.8 94 75 125 0713771-007Adup MW-8DDUP Sulfate 81.9 mg/L 81.8 0.12 20 MB -121007 MB -121007 Total Dissolved Solids <10 mg/L LCS-121007 LCS-121007 Total Dissolved Solids 292 mg/L 300 < 10 97 80 120 0713771-007AMS MW-8DMS Total Dissolved Solids 1270 mg/L 60D 678 99 75 125 0713771-007ADUP MW-8DDUP Total Dissolved Solids 674 mg/L 678 0.59 20 MB -120707 MB -120707 Total Organic Carbon < 1 mgn- LCS-120707 LCS-120707 Total Organic Carbon 27.6 mg/L 25 < 1 110 80 120 0713771-007EMS MW-8DMS Total Organic Carbon 28.5 mg/L 10 18.7 98 75 125 0713771-007EDUP MW-8DDUP Total Organic Carbon 19.0 mg/L 18.7 1.1 20 TSLO12 S67 1< .._-............. ........ - ............._-__- - - - lk( t 3 TSLO12 S67 1< .._-............. ........ - ............._-__- - - -