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Metals Data Package 06/2007
Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSLO10 Water Samples Received: 6/14/07 & 6/15/07 A A rT A t f% f1 A T A PAC KAG E I -A I-Aus'w. I EInvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. SC40 11747 U2/A "US. l %Co ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 6/14/07 & 6/15/07 SDG NO.: TSLO10 I. NYS DEC SUMMARY FORMS II. SDG NARRATIVES_ III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY U2A "US, I%C. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SDG: TSL010 SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY Analytical Requirements Customer Sample Code Laboratory Sample Code ME we MW -BD 0706952-001 X f X MW -4D 0706952-002 X X j MW -4S 0706952-003 X X MW -5D 0706952-004 X X MW -5S 0706952-005 X X !r MW -6D 0706952-006 X X MW -6S 0706952-007 X XI; MW -8D ` 0706952-008 X X MW -8S 0706952-009 X X _ FB 061407 0706952-010 X X MW -1D 0706986-001 X�j X MW -1S 0706986-002 X X A^ MW -3D 0706986-003 X 1- X { MW -3S 0706986-004 _ --X -�-- X ~ CLPCon-CLP`{Please indicate year of AJP v 10M CES- -1�z1a' NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSLO10 INORGANIC ANALYSIS Laboratory Samp ID 1 Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0706952-001 IMW-BD WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 I 06/07 0706952-002 NIW-4D ( WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 I 06/07 0706952-003 MW -4S WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-004 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 114 -Jun -07 06/07 0706952-004DUP ;MW-5DD WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-004MS IMW-5DS I WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-005 IMW-5S WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-006 IMW-6D I WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-007 IMW-6S I WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-008 IMW-8D I WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-009 MW -8S I WATER CA,CD,FE,K,MG,MN,NA,PB, 114 -Jun -07 06/07 0706952-010 JFB 061407 I WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706986-001 MW -1D WATER I CA,CD,FE,K,MG,MN,NA,PB, 15 -Jun -07 06/07 0706986-002 MW -Is I WATER CA,CD,FE,K,MG,MN,NARB, 15 -Jun -07 I 06/07 0706986-003 MW -3D I WATER CA,CD,FE,K,MG,MN,NA,PB, 15 -Jun -07 06/07 0706986-004 MW -3S I WATER I CA,CD,FE,K,MG,MN,NA,PB, I 15 -Jun -07 06/07 TSLO10 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY INORGANIC ANALYSIS SDG : TSL010 t Laboratory Samp ID II ! Client Sample ID Matrix I I Tests DateRec I d at Lab Date Analyze 0706952-001 MW -BD Aqueous I SELECT WET CHEMISTRY ** 06/14/07 j 06/07 0706952-002 I MW -4D e Aqueous ( SELECT WET CHEMISTRY *" 06/14/07 06/07 0706952-003 MW -4S Aqueous I SELECT WET CHEMISTRY ** ! 06/14/07 I 06/07 0706952-004 MW -5D I Aqueous SELECT WET CHEMISTRY ** j 06/14/07 06/07 0706952-004DUP MW-5DDUP I Aqueous SELECT WET CHEMISTRY ** 06/14/07 06/07 0706952-004MS i MW-5DMS Aqueous SELECT WET CHEMISTRY ** 06/14/07 I 06/07 0706952-005 MW -5S Aqueous SELECT WET CHEMISTRY ** 06/14/07 I 06/07 0706952-006 MW -6D Aqueous SELECT WET CHEMISTRY ** 06/14/07 I 06/07 0706952-007 MW -6S I Aqueous SELECT WET CHEMISTRY ** 06/14/07 06/07 0706952-008 MW -8D Aqueous SELECT WET CHEMISTRY ** 06/14/07 06/07 0706952-009 i MW -8S Aqueous SELECT WET CHEMISTRY ** I 06/14/07 I 06/07 0706952-010 FB 061407 Field Blank SELECT WET CHEMISTRY ** 06/14/07 06/07 0706986-001 + MW -1D Aqueous SELECT WET CHEMISTRY ** 06/15/07 06/07 0706986-002 ( MW -IS Aqueous SELECT WET CHEMISTRY ** ! 06/15/07 ( 06/07 0706986-003 MW -3D Aqueous I SELECT WET CHEMISTRY ** ! 06/15/07 06/07 0706986-004 I MW -3S Aqueous I SELECT WET CHEMISTRY ** 1 06/15/07 j 06/07 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand ; Chloride; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable ; Sulfate ; Total Dissolved Solids; Total Organic Carbon ; U2A "US' INC. Ii. SDG NARRATIVES 0 0 UO Ey SDG NARRATIVE FOR METALS SAMPLE RECEIVED: 6/14/07 & 6/15/07 SDG#: TSLO10 For Sample: MW -BD MW -61) MW -1D MW -4D MW -6S MW -IS MW -4S MW -8D MW -3D MW -5D MS/MSD MW -8S MW -3S MW -5S FB 061407 Fourteen water samples were received by H2M Labs, Inc. for analysis of a select list of metals. Samples were prepared and analyzed using EPA methods 6010B with a TJA 61E Trace ICP Instrument. Sample MW -51) was utilized for QC analysis and reporting. • The sample spike recovery for manganese was above 125%. Since the sample result exceeded the spike concentration by more than four times, post spike analysis and data qualifiers were not required. • In the serial dilution analysis of the sample, %D for potassium exceeded the acceptance range, and all results for this analyte were flagged with the qualifier "E" on Forms 1 and 9. All other QC data and calibrations met the requirements of the method and no problems were encountered with sample analysis. Sample MW -3S was reanalyzed for manganese at a dilution to keep the concentration within the calibration range. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: June 21, 2007 Ursula Middel o Technical Manager o v� F-+ U2M "US, INCo For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLES RECEIVED: 6/15/07 SDG#: TSLO10 MW -BD MW -813 MW -4D MW -8S MW -4S FB 061407 MW -5D MW -1D MW -5S MW -1S MW -6D MW -3D MW -6S MW -3S Fourteen water samples were received by H2M Labs, Inc. on 6/15/07 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: Alkalinity Anions- chloride/sulfate/bromide Biochemical Oxygen Demand Chemical Oxygen Demand Hardness Ammonia Nitrate Phenols Total Dissolved Solids Total Kjeldahl Nitrogen Total Organic Carbon Sample was utilized for QC analysis and reporting. EPA 310.1 EPA 300.0 EPA 405.1 EPA 410.4 EPA 130.2 EPA 3501 EPA 353.2 EPA 420.1 EPA 160.1 EPA 351.2 EPA SW846 9060 Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: June 29, 2007 Vincent Stancampiano Vice President U2M "US. INC. III. CHAIN OF CUSTODY DOCUMENTATION .: 1H2 , 1 -AUS, INN re a r_a LI -11..... OA uer..11fn #JV 747A7.-AA7R U 4 U EXTERNAL CHAIN OF CUSTODY We -r. v.... ..—•-------.--- ------ -1--- - - Tel: (631) 694-3040 Fax. (631) 420-8436 CLIENT: H2M SDG NO: -FS L 0t0 PROJECT NAMEINUMBER S o c'77 -!Q Q) Z,g+ND F r L L_ X 007 Q� 91 -2 a o 7zX o ` CL NOTES: Project Contact Pia 7- c3 3 Phone Number. l 8 if k3 0 U 77ArE Pismuote # 0A/ S 6! �To7o / SAMPLERS: (signaturoyClient V iso DELIVERABLES:. Z G �° v 1. �r ANALYSIS REQUESTED TURNAROUND TIME: a 1 DA- Y ORGANIC INORG. . DATE TIME MATRIX FIELD I.D. (,3� 5z U LAB I.D. NO. REMARKS: Uffla 0: -6& S s S 1 1 3 1 1b' �0 5- o —MVV- M w-- - 5 D d4 1 3 3 `j' 3 0'�-o Q 9 /115 la,00 N! W- 4-S S a l I i 13 ce-I -� 3 !a 30 M W r- D 1#40 /W W- (vV-50 M W - o'er CQ Ct z- l M ►� - 8 S Cf'Iv u of 12 3 MW" SD D--�OCQGlb Oc`3 lq 12: LV 50 14Q Fg M W =- P13 a 1 13 C�`�fl C 15i b 161 F411 I . (s ) Date ('11410 Time IS�.t� Received try. (signature) Date �a�ltf (3� Time 1 15� LABORATORY USE ONLY DlsorepanclesBetween Sample Labels and COC Record? Y or N Explain: S$@motesvrere: 2, bi ecf_ °r Hand Delivered_ a hbimt mbient or chided, Temp 2 Ambient 3. Received in good condition: Y or N 4. Properly preserved: Y or N COC Taos was: t. Present on outer package: Y or N 2. Unhroken 3. COC onrd present 6 er complkage:ete upon sample receipt: YorN Relinquished by: (Signature) Dat Time Received by: (Signature) Date Time Relinquished by: (Signature) Data Time Rece2ved by. (Signature) Date Time Rellnqulshed by: (Signature) Date Time Received by: (Signature) Date Time 1'SLUI�APU - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY 12M LABS, INC. n Sample Receipt Checklist Client Name PCTSL Date and Time Receive 6/14/2007 3:15:00 PM Work Order Numbe 0706952 Received by CAM Checklist completed by �]� Reviewed by Signature T Date Initials 6ate Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes ❑d No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable W Chain of custody present? Yes ❑d No ❑ Chain of custody signed when relinquished and received? Yes E%0'1 No ❑ Chain of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes No ❑ Sample containers intact? Yes ❑d No ❑ Sufficient sample volume for indicated test? Yes W No ❑ II samples received within holding time? Yes ❑d No ❑ Container/Temp Blank temperature in compliance? Yes No ❑ Water - VOA vials have zero headspace? No VOA vials submitted ❑ Yes No Water - pH acceptable upon receipt? Yes No L7 Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section be Client contacted Date contacted: Contacted by: Regarding Comments: Corrective Action Person contacted WA FLAUSs INC* INTERNAL CHAIN OF CUSTODY CLIENT': L DELIVERABLES: k) �� TURN AROUND TVAE:_ D�S SDG #j--5 L © CASE #. - MATRIX: — pH CI SCK Y or N REMARKS: c) . — C SIGNATURE: 0 DA t E: 6 • j tf-OTTD.4F f RECEIVED BY: CLIENT ID H2M LAB * DATE BOTTLE N OF TESTS COLLECTED TYPE IBOTTLES.REQUESTED _ 0^�D -6 bLi o A S -5-0 „ . u u _ u }} u „ n n METALS P 0247 N O -.1 O H CLImn: SDG # :aL b I INTERNAL CHAIN OF CUSTODY METALS 02,45 SAMPLEPURPOSE RELINQUISHED SAMPLE BY' ,-ECEIVED BY gl Slow .. BOTTLE TYPE C.3 OF CHANGE OF CUSTODY INIT DATE TIME c-Li4a30 � 1 Zaj alae g 1C: S S slow slow ._ alai slow SIGw SIGN aIGN SIGN ' glow SIGN SIow SIGN - ' slab- SIGN SAO" SIGN SION SIGN SIGH SIGN 310H SIGN slow SIGN SIGN SIGN SIGH SIGH , 310N SIGN glow SIGN BION SIGN SIGN SIGN glow SIGN SIGN SIGN, SIGN SIGN METALS 02,45 INTERNAL CHAIN OF CUSTODY CLIENT�� 5L� DELIVERABLES: TURN AROUND TR E: `-1 S pH CHECK YofN SDG #: CASE #:_�— MATRIX: �— RECEIVED BY: PX' SIGNATURE: DATE:% YIP TA3E:L— BOTTLE BOF TESTS I12M LAB DATE It EQUFSTED CLIENT ID N COLLECTED TYPE BOTTLES R L� 1�T 3cYa—W as O —w, l r + r —(Y,.> L --co IL, Gie V-t� I llp-1-0-LS0, �s 3 TSG-9cxeorw WET CHEMISTRY P 0193 IH2A UAzu'vil) INCO -U� CLIMU.1 sDG INTERNAL CHAIN OF CUSTODY WET CHEMISTRY P 0194 Imp I'VI WET CHEMISTRY P 0194 lo -Al Isc- cl,:[ Em : - SDG 1: lsu 1 -rKTrPWpNAL CHAIN OF. CUSTODY WET CHEMISTRY p 0195 r__ f L I—IA13�� ' �C. 2 EXTERNAL CHAIN OF CUSTODY Z2.,I MIwf..fllw AIV 447L7_U17R .Tel. -(631) 694-3040 Fax: (639) 420-8436 CLIENT: T S (, H2M SDG NO: L_ \ C) PROJECT NAME/NUMBER S O LITH OL O 4 4 AQ F I LL, 2 00-7 0 Z .si co -1 '�, C Z Q y 10 �- Q� • :� NOTES: Project Contac! 3 6 0 Phone Number: O N PfdI%�METFP6 P!S/Quote# ENV soH7o7ol� EA SAMPLERS: (signatureYCllent V&- M Ll" DELIVERABLES: C —70 D c g Z c I F. U �► ANALYSIS REQUESTED TURNAROUND TIME: aZ I I) [ S ORGANIC INORG. . DATE- TIME MATRIX FIELD I.D. a m a � C2.)��� Z U LAB I.D. NO. REMARKS: Mw -- 8 t 3 I — oq,op M W 104OCe15(0 —ia--)3 1200 ID Reitnqul by: (Stgpature) ! Date 15 o Time 13%53 Received by: (Sipriature) Date b'19 �" Time 13 `.b'� LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y or N Explain, samwes w`7 1. SNpped_ or Hand Delivered_ AlrbW Z Ambient orcNl{adjemp 3. Received In good condition: Y or N 4. Property preserved: Y or N COC Tape urea: C 1. Present on outer package: Y or N Z Unbroken on outer package: Y or N 3. COC record present & complete upon sample receipt: YorN Relinquished by: (Signature) 1DaQ3 Time Received by: (Signature) Date Time Retinqulshed by, (Signature) Date Time Received by. (Signature) Date Time Retir,Wshed by. (Signature) Date Time Received by. (Signature) Date Time ORIGINAL YELLOW COPY -CLIENT PINK COPY - LABORATORY 12M LABS, INC. Sample Receipt Checklist Client Name PCTSL Date and Time Receive 6/15/2007 1:53.00 PM Work Order Numbe 0706986 Received by CAM ,� Checklist completed by6� 1 'd. b---- Reviewed by �s (AU [a j 'r Signature �Dale Initials i Dale r— Matrix: Carrier name Hand Delivered Shipping container/cooler in good condition? Yes No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable 91 Chain of custody present? Yes W No ❑ Chain of custody signed when relinquished and teceived? Yes 1VJ No ❑ Chain of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes No ❑ Sample containers intact? Yes No ❑ Sufficient sample volume for indicated test? Yes No ❑ II samples received within holding time? Yes No ❑ Container/Temp Blank temperature in compliance? Yes No ❑ Water - VOA vials have zero headspace? No VOA vials submitted Yes ❑ No ❑ Water - pH acceptable upon receipt? Yes No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section be Client contacted Contacted by: Comments: Corrective Action Date contacted: Regarding Person contacted 00 O O IH2A LA INC. INTERNAL CHAIN OF CUSTODY CLM4rTQ�DELIVERABLES: nAROUND TME:2k Sr, 4- CASE #: MATRIX: pH CHECK Y or N REMARKS: bclD RECEIVED BY: � -SIGNATURE: qAuAt:,,� . DATE:& -1 1# TRAE: Wr*3 CLIENT ID 112M LAB # DATE COLLECTED BOTTLE TYPE 0 OF BOTTLES TESTS REQUESTED Ot>tD (o GS 611) -cb�ls) -0,)-) o METALS P 0 253 U2A UAUSs INC. L SDG #: _F6 C) INTERNAL CHAIN OF CUSTODY DATE T330 SAMPLE RELINQUISHED BY SAMPLE _RECEIVED BY BOTTLE TYPE PURPOSE OF CHANGE OF CUSTODY INIT m.6-0 ... Q7� - .. 9 Sias a2 sI tT0 A��L()• z tI BION vXOV31 BION SION 8.109 slow BION Bioko Blow SIGN • BION SIGN -SION SIGN SION SIGN SION SIGN SION SIGN 51011 SIGN 310" SIGN SION SION SIGN SION Bioko SIGN SION SION 31011 SION SION SION Bioko SIGN SIGN SIGN SIGN SIGN 31 ON SIGN METALS P 02.54 I u2m, UA"9 INC, INTERNAL CHAIN OF CUSTODY - ? bpi"l- CLM4IbSH c -i- C�J�&.DELJVERABLES- TURN AROUND TWE SDG g.rlff� Q C) MATRIX: pHCHECK Y"N CASE 9: REMARKS:— ?c C) SIGNATURE: DATE., � RECEIVED BY: _-kV&T0AE-jX- Qprn� CLIENT ID H2M L, # OD I -0t) tell SAP- NA 17 1. IV I WET CHEMISTRY P 0205 CLIERT: SDG TM'PRRNAL CHAIN OF CUSTODY WET CHEMISTRY P o2o. (; lH2M "USS IMC. IV: ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY 1 st-o t D U2M "I3S-9 INCe METALS TABLE OF CONTENTS I. REPORTS II. QC SUMMARY III. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Lab Code: 10478 Case No SOW No.: ILM04.1 EPA Sample No. FB 061407 MW -1D MW -1S MW -4D MW -4S MW -5D MW-5DD MW-5DS MW -5S MW -6D MW_ GS MW -8D Were ICP interelement corrections applied? Were ICP backqround corrections applied? If yes -were raw data generated before application of background corrections? Comments: DATE REPORTED: JUNE 21, 2007 Contract: SAS No.: SDG No.: TSLO10 Lab Sample ID. 0706952-010 0706986-001 0706986-002 V IVV./VV-VV 0706952-003 V- ... -:L 0706952-004DUP 0706952-004MS 0706952-005 0706952-006 0706952-007 0706952-008 0706952-009 0706952-001 Yes/No YES Yes/No YES Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer -readable data submitted on diskette has been authorized by the Laboratory Manaqer or the Manaqer's designee, as verified by the followiAsiature, /�/j� �qp(.%I Scj, la / 7 I' CSL j Signature:� f �' Name • vi nr-ort Ctanra,.mi nay„ Date: / Title: COVER PAGE - IN ILM04.1 U2A isco REPORTS FOR METALS IH28t "U%s INC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L CASA No. Analyte 7440-43-9 1Cadmium Concentration i C Q^ 1. 1' B i `_ 1 EPA SAMPLE NO { 395001 1 INORGANIC ANALYSIS DATA SHEET -- -- - - I P 7439-92-1 ;Lead I 1.11 U MW -BD Lab Name: H2M LABS, INC. Contract: 17440-09-7 Potassium --j Lab Code: 10478 Case No. SAS No..: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-001 Level (low/med)• LOW Date Received: 6/14/2007 Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L CASA No. Analyte 7440-43-9 1Cadmium Concentration i C Q^ 1. 1' B i `_ M P ! 7440-70-2 Calcium { 395001 1 i P j7439 -89-6,I o _ 123, I P 7439-92-1 ;Lead I 1.11 U P i 74 39 4 agnesium r 7439-96-5 IManganese -i_- ( 173004 ! — _ _ 4580; P ; P i 17440-09-7 Potassium --j 452_0; B_; E --- i ( P .74440-23-5 Sodium 156001 i Color Before:_ COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 21, 2007 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1' U.S. EPA - CLP Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: nATR RRPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET -� MW -4D Lab Name: H2M_LABS, INC. Contract: i ---- Lab Code: 10478 Case No.. SAS No.: SDG No.:, TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-002 Level (low/med): LOW Date Received: 6/14/2007 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L R CAS No. 1 Analyte Concentration C Q ! M E B iT-_— P 17440-43-9 C ium ----0.45; 7440-70-2 7&a1cium 565001 i P —r— 7939-89-6 I 'Iron --------1— ; i - 94.91 B_i -- P 7439-92-1 (Lead ---; _ 1.11 U . ( P j 17439-95-4 !Magnesium j 20200; I~ j P 17439-9'6-5 iManganese — j -101001 j P ;7440-09-7 jPotassium 48200 j E +-----1. P 2 iSodun1 25000 P7 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: nATR RRPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): Color Before: COLORLESS_ Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR_ Comments: DATE REPORTED: JUNE 21,2007 a FORM I - IN UG/L Texture: Artifacts: ILM04.1 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET f---- - i MW -4S Lab Name: H2M LABS, INC. Contract: ? -.---I _ Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-003 Level (low/med): LOW Date Received: 6/14/2007 Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): Color Before: COLORLESS_ Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR_ Comments: DATE REPORTED: JUNE 21,2007 a FORM I - IN UG/L Texture: Artifacts: ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET _-- — ---- MW-5D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-004 Level (low/med): LOW Date Received: 6/14/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. i Analyte !Concentration C Q M 74-40-43--9 —,',Cadmium _0.16) U 11 P 7440-70-2 ICa�lciu_m 991001 1 _ 1 P 7439-89 Iron 93. 41 B 1 1 P I 87439-92-1 `Lead 2.31 B 1 PTI 7439-95-4 _ !Magnesium` — 58100; _ I P `7439_-96 -5 Manganese ! 118001 _ P _ 17440_-09-7 Potassium _ 1210001 ? E --- _ i_P ;7440-23-5 Sodium ----- _ T_ —.— _ . -- -_ 24500,0; —(- ---_, P� Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: DATE REPORTED: JUNE 21, 2007 Texture: Artifacts: FORM I IN ILM04.1- U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET —__ -1 MW -5S i i Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-005 Level (low/med): LOW Date Received: 6/14/2007 Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 21, 2007 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 O O Cn H U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID Level (low/med): LOW Date Received Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L }CAS No. 1 Analyte 1Concentration FC Q M— 7440-43-9 lCadmium0.20i B _� P_ 17440-70-2 Calcium _« 41j 01 P j JP 17439-89-6 !Iron— I-- 114; I -----1.1 17439-92-1 iLead_ U! P 7439-95-4 _- jMagnesium '— 180001 i_ P `7439-96-5 ;Manganese 4_760' _ i P� iPotassium ! B j E T P� X7440_-_09-7 171440-23-5 ;Sodium _ _4580 161001' i P EPA SAMPLE NO MW -$D SDG No.: TSLO10 0706952-006 6/14/2007 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR ` Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration { C Q 1 EPA SAMPLE NO --^_ Cadmium INORGANIC ANALYSIS DATA SHEET X7440-70-2 --i_ ;Calcium_ _T 144001 i_-_— I P j MW -6S i Lab Name: H2M LABS, INC. Contract: -_j (Lead s Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-007 Level (low/med)• LOW Date Received: 6/14/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration { C Q M -L440-43-9 --^_ Cadmium 0.16; U — —,-P X7440-70-2 --i_ ;Calcium_ _T 144001 i_-_— I P j 7439-89-6 ;;Iron ^_ 1531 i P i 7439-92-1 (Lead s 1.1F UT P ;7439-95-4 _ ;Magnesium 1— B j P - !7439-96-5 'Manganese I v _3730 _1330] j P 7440-09-7 !Potassium I_ — _6560; _` E ; Pu; 17440-23-5 !Sodium- i— 4610; B ! PY j Color Before: COLORLESS Clarity Before: CLEAR Texture: _ Color After: COLORLESS- Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE FORM I - IN - ILM04.1 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L 1 EPA SAMPLE NO CAS No. INORGANIC ANALYSIS DATA SHEET ------, E7440-43-9 !Cadmium - _ U 1 ! MW -8D Lab Name: H2M LABS, INC. Contract: P 17439-89-6 jIron Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-008 Level (low/med): LOW Date Received: 6/14/2007 % Solids: 0.0 -439-96-5 17440-09-7 `gan.se_ !Potassium847001 Concentration Units (ug/L or mg/kg dry weight): UG/L Color Before:_ COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 CAS No. Analyte (Concentration C -0.16; E7440-43-9 !Cadmium - _ U 1 1 P 7440-70-2 jCalcium 72700;'_-- P 17439-89-6 jIron - _ 89401 74397.92-1 (Lead U i--_' — 17939-95-4 !Magnesium 385001 P-( - — — --- 1600 - P -439-96-5 17440-09-7 `gan.se_ !Potassium847001 - --- E i P — —i--- 17440-23-5 !Sodium --r ..:----- - -4 - - -- --- 82700; - ! P Color Before:_ COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP Comments: M DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET - MW -85 j Lab Name: H2M LABS, INC. Contract: --� Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706952-009 Level (low/med): LOW Date Received: 6/14/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. M� i Analyte l Concentration I C Q 7440-43-9 GCadmium--_-.i 0.91; B j P__) 7440-70-2 jCalcium �- 603001 ! i P 7439-89-6 Tirol �- -- 49000; j P { 7439-92-1 ;Lead_- I 1.1! U X7439-95-4 Nagnesium _- 20400 P i X7439-96-5 ;Manganese 918 E P ;7440-09-7 !Potassium ( 396001 E P 1 ;7440-23-5 ES odium �-378001 i Color Before: COLORLESS Clarity Before: CLEAR - Texture: Color After: COLORLESS Clarity After: CLEAR - Artifacts: — Comments: M DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. 1 Analyte r —T ; Concentration C j Q I M I 7490-43-9 Cadmium 0.16iU P 7440-70-2 aC1 lcium ---�—� 46.41 B ; r P 7430- 9-89-6 iIron 1 22.9. B P�� ILae d— 1. 1 U j j P I }743�7_439-92-1 IMagnesium 7.71 U P� 7439-96-5 !Manganese _ 0.79,B! P 7440-09-7 !Potassium 80.6; B! E P 17440-23-5 4S odium i 89.71 B 1 I P Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 21, 2 EPA SAMPLE NO FB 061407 S SDG No.: TSL010 6/14/2007 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L !Concentration C Q 1 EPA SAMPLE NO Analyte INORGANIC ANALYSIS DATA SHEET 17440-43-9 (Cadmium 0.16E U ; f P i j MW -1D ` Lab Name: H2M LABS, INC. Contract: 7439-89-6 11ron— Lab Code: 10478 Case No. SAS No.: SDG No. :• TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706986-001 Level (low/med): LOW Date Received: 6/15/2007 % Solids: 0.0 7440-09-7 Potassium Concentration Units (ug/L or mg/kg dry weight): UG/L Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 !Concentration C Q M CAS No. Analyte 17440-43-9 (Cadmium 0.16E U ; f P i 7440-70-2 Calcium 227001 P 7439-89-6 11ron— 2_2_2j I j P I 7439-92-1 ILead _ —_ --_ 1.11 U _ G P I 7439-95-4 IMagnesium 104001—r i P i 7439-96-5 _ IManganese 7.1 B I P 7440-09-7 Potassium 1360 E P 7440-23-5 ISodiurn 20100 1 P I Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte ± Concentration C j Q--� M 7440-43-9 Cadmium_ 0.501 B i� 7440-70-2 Calcium--- 9090 _ P j — 7439-89-6 Iron 23701 1- P^i 2.8 B r 7439-92-1 1Lead I P 7439-95-4 Magnesium_ 1 7150 _ I 7439-96-5 IManganese 82.31 i P 7440-09-7 Potassium 1 23901 B E P 17440-23-5 _ iSo' diem _ i — 51200 1— ; P EPA SAMPLE NO I MW -1S SDG No.: TSLO10 6/15/2007 Color Before:_ COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE. REPORTED: JUNE 21, 2007 FORM I - IN ILM04.1 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. j Analyte (Concentration C� Q I M 7440-43-9 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET 62100; j P 7439-89-6;Iron �743�9-922-�1_;Lead �; MW -3D Lab Name: H2M LABS, INC. Contract: P P 774440-09-7 Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Matrix (soil/water): WATER Lab Sample ID: 0706986-003 Level (low/med): LOW Date Received: 6/15/2007 o Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. j Analyte (Concentration C� Q I M 7440-43-9 iCadmium 0.16; U 7440-70-2 [Calcium 62100; j P 7439-89-6;Iron �743�9-922-�1_;Lead �; 6650; I l.lj P .7443+ —9--95--44 jj-Magnesium j 7439( 96-5 IManganese I 330001 { _ 39301 j P P 774440-09-7 jPotassium� i 131000] E i P 74401 23-5 :Sodium j _ zls000j i P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: nAT7 RRPnRTED: JUNE 21, 2007 Texture: Artifacts: FORM I - IN ILM04.1 ro WR 07 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L — jconcentrationlC� M ASNo. F 1 EPA SAMPLE NO 7440-43-9 INORGANIC ANALYSIS DATA SHEET Calcium I 50700 P ! 224 00 P� 7439-89-6 � MW -3S Lab Name: H2M LABS, INC. Contract: 1.1TU i P 743_9-95-4 Magnesium Lab Code: 10478 Case No. SAS No.: SDG No.: TSL010 Matrix (soil/water): WATER Lab Sample ID: 0706986-004 Level (low/med): LOW Date Received: 6/15/2007 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L — jconcentrationlC� M ASNo. F Analyte 4 7440-43-9 �Cadmi�um^ —� 1.0 B I P 7440-70-2 Calcium I 50700 P ! 224 00 P� 7439-89-6 IronI 7439-92-1 Lead. 1.1TU i P 743_9-95-4 Magnesium 263001 ! P I 7439-96-5 Man anese 195001 I j P { ;7440-09-7 Potassium 386001 1 E P i 7440-23-5 sodium �_ 558001 I P Color Before: COLORLESS Clarity Before: CLEAR— Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 21, 2007 — —V' - --- -- -- FORM I - IN ILM04.1 U2M "US9 l%Co II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA.AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE'SAMPLE RECOVERY :F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H.' LABORATORY CONTROL SAMPLE 1. STANDARD ADDITION RESULTS J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT-CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O O FORM II (Part 1) - IN ILM04.1 H Initial Calibration I Continuing Calibration Analyte True Found %R(1) i True Found %R(1) Found %R(1) II M! Cadmium Calcium ! 2500.0 ! 2488.98 1._ 50000.0 47889.32 T 99.6 95.8 2_500.0 :, 50000.0! 24i7--737^96.7 46747.53 _i 93 5 2402.68 i ^d6825.64 96.1 P 93.7 P Iron 50000.01 48761.67 97.5 ;50000.0 47361.95 1 94.7 -T---- 46971.53-} 93.9 P Lead 500.0 1 532.88 ; 106.6 L500.0519_83 j- 103_6 ; 520.84_ i 104.2 i P Magnesium um 50000.01 51436_.34 1 102.9 150000 .0,1 50449.71 100.9 j 50238.28 100.5 j P � ,Manganese y 2500.0 ! .53 !199.1 2 74 6 0 { 2500 j 2409.42 96.4 ! 240_8.49 96.3 P Potassium �80000.0� 83964.26 105.0 X80000.0; 82227.90 102.8 81874.64 102.3_; P 1 ...--:------t-- Sodium ;8.0000.0 83051.53 j 103.8 180000.0----i-----; 81424.20 101.8 ( 80976.87 ! 101.2 !! P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O O FORM II (Part 1) - IN ILM04.1 H U.S. EPA - CLP 2A. INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial CalibrationContinuingCalibration Analyte I True Found %R(1) True Found %R(1) Found %R(1) �� M1 ICadmium _� �j _ 2500.0 2456.11 ; 98.2 12472.72 98.9_ T P -j !Calcium ;50000.0 46859.64 ': 93_7 48698.25 , 97.4 s P 150000.0; 47326.33 94.7 ; 48443.09 ! 96.9 P Lead ' _ 500_0 I 513.61-102_7 547.39 _ 109.5_; Pi Magnesium _ 15O000 0 49808.52 i 99.6 52_325.27 104.7 ` P -- -- ---- 96 2 z 2497.40 99.9 P Manganese i _E- T T_ 2500 0 , `2404.78 _ _ (Po�tas�sium- I i ; 80000 0i 81111.26 -10 84627.90 105.8 � P ga' dium 80000 01 80600.29 100.8 i 82332.03 102.9 ; P { ------ (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N O O FORM II (Part 1) - IN ILM04.1 Fes-+ U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10,478 Case No. SAS No.: SDG No.: TSLO10 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration j Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) l M Iron 2500.01 2589.30_! 103.6 12500.0! 2595.08 103.8 12460.11 i 98_4 P _ Sodium 2500.0 2660.44 X106.4 - ' 2500.0 _—__ i 2674.41 107.0 2505.08 _�- -- -- 100.2 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N O O FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(l) ii M y�— LI ron ' 2500.0 'r — 2611.03 104.4 25-79.141 03.2 P j (ISodium i -- -- - ' 2500.0 2636.05 1 105. 412726. 81 -109.1 P { _ (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (Part 1) - IN ILM04.1 V) U.S. EPA - CLP 2B I CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. AA CRDL Standard Source: Contract: 1 SAS No.: ICP CRDL Standard Source: MV Labs/High Purity Concentration Units: ug/L SDG No. TSLO10 FORM II (Part 2) - INJ ILM04.1 CRDL Standard for AA J CRDL StandEird for ICP Initial i Final I Analyte 1 True Found %R True Found %R Found %R Cadmium 10.01 10.14 I 161. 41 10.891 10 8. 9; Lead 6.01 6.71' 111.9 5.861 97.61 Manganese 29.631 99.41 38.371 127.91 J - FORM II (Part 2) - INJ ILM04.1 U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL010 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L FORM III - IN Initial Calib. ; Continuing Calibration i Prepa- I Blank i Blank (ug/L) jj ration jE C M j Analyte (ug/L) C 1 C 2--C 3— C i Blank ICadmium ICalc — 0 U 3 j B, 0. _0.2j U — — — 8 0 2�I U - 51.0 B t-_�-66.6001 0 180' B i P -- r— ; B ' P i u iCalcium -59.0; B 1 -� �___-_ -33.0 B ; -7 1 B ; _-61.0 --� -21Oi B i ; B G ; -17 900; B_ P fIron j_ 22.0; B _ 1.4 B ; . -1.7 . B ; _-10.0 —1.1' U�-- -1.7 1 B 1 0811 U i P iLead — -- 58.0 B �- -31.0 ' B! -59.01B ' -57.0 -B -_52.7001 B ( P I magnesium Manganese 0.2�j B _._ _ ; B� 0.11 U _0.3 0.129 U r P -�^ Potassium - — 38.3 B -- i0.2 . 369 B j 45.2! B! 56. 5 B _ _ 31.7OOi B;? P !Sodium— —1 7.1' B 1 10.4 B 20.41 B 1 33.3 i B t; 4.789.-B P i FORM III - IN U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg); UG/L —_.__.__; I :Initial- ---- ; i I I Calib. Continuing Calibration i Prepa- Blank Blank (ug/L) ration i Analyte ; (ug/L) C 1 1 C 2 C 3 C Blank C i M Cadmium---- v-_.- j 0. 4 B - - ---- - r P Calcium �— -40.0 Iron -. --� -15.0 i B: i ! P I fLead - -_ 1 1-� i ;Magnesium_ _ -46.0 B _ i �r — i? i CManganese I _ - - -- ----- — - - jPotassium' j - I i-- 47". 4 B --- _r-- I - - i - P 1 Sodium _ i - -- --- i—r---- ! 15. 9 I B --- -- _! - ! —T� i, p — --- - -�-- i - — �- FORM III - IN U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 104.78 Case No. SAS No.: SDG No.: TSLO10 ICP ID Number: TJA6IEA ICS Source: MV Labs/High Purity Concentration Units: ug/L True Ji Initial Found Sol. Sol. - Sol. Sol. Analyte ! A AB ii A AB %R Final Found Sol. Sol. A AB %R !Aluminum 500000 5000067 - 499721 524802.61 105.0;-489275 511677.01 _ 102.1 !Cadm_ium 1000 1031.21 103.11`_ 1021 91 102.21 _; Calcium 500000 _ 500000 ; 503772 532568.8: 5i 503292 532104.61 106.4 Iron i 200000 200000 —202701 213761.6, _106 106.91 199785 20_9678 9 ': 11a3._9� 104.8; 114:4; Lead !Magnesium ! 1 500000 j 1000 ! I 500000 ; 513663 j 1133.21 537723.1` —� 113 31 - 107.5; 508737 5_34093.3 106.8; Langanese 500 ii 534.1 _ 106.8; _— _j 527.0 _ _105_41. FORM IV.- IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No. Concentration Units (ug/L or mg/kg dry weight) EPA SAMPLE NO MW-5DS SDG No.: TSLO10 Level (low/med): LOW UG/L Comments: FORM V (Part 1) - IN ILM04.1 00 N O O Control i j i Limit Spiked Sample Sample Spike { j f Analyte %R Result (SSR) C' Result (SR) C1 Added (SA) j $R i Q j M !Cadmium i 75-125 i 52.4600 ; 1 0.1643_ U! 50.001 104.9 X P i 1Iro _ ' 75-125 i i 1121. 4100 ! 2659= _ 93.3700 { B') 1000.00 102.8 P 4.7 �L-ead an anese i 75-125 - ' -23 12939 9900 ; 11812.4294 0B i 500.00 2205.5 P _ _ '- - --- Comments: FORM V (Part 1) - IN ILM04.1 00 N O O Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES ;--^ MW -5D Contract: SAS No.: SDG No.: TSLO10 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L f Analyte Control Limit Sample (S) C I Duplicate (D) C' RPD Q M (Cadmium I 0 1643 U _ � 0.1643! U' - ? ' P -i-- 5 •: P iCalcium 99051 7100 I ! 104737.8600' I 61 , Iron __ 1100.0000 i _- 93.3700 B� 80. 5100 B 14.8; ! ; P Lead - _3.0000-i -_ ---2 3294 j B -- _ 1.0807! U� _ 200.01 P P Ma nesium I i 58059 4300 Ir _61230.4800; 12462.5500; ; 5.3 5_4�T-`P IMan�nese Potassium �I ! ' _11812.4900; 121080.8900 ' _ 12653_7.8100!_' I 4 4 I_ i P i Sodium - I i245273. 6300 I--- 256535.5200' !-�--4 5! P! FORM VI - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSLO10 Aqueous (ug/L) I Solid (mg/kg) Analyte 1 True Found oR True Found C Limits oR Cadmium 2500.01 2369. 86, 94.8; Calcium 1, 005 005 00.0; 45818.331 91. 61 'Iron ! 50000.01 44860.06{_89.7 L -- 0 518_.74; 103.71-----� — —�— --- --- —�l Ma ne ium _ 50000.01 49184.88! 98 4 Mananese 2360.87 94 4 Potassium a _2.500.0! 80.000.0' 80583.03 - 100.7! Sodium - 1 80000.0! 79846 67� 99.8 FORM VII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No.: Concentration Units: ug/L SDG No.: TSLO10 EPA Sample ; 0 ADD; 1 ADD i 2 ADD 3 ADD Final No. iP'ni ABS j CON ABS CON ABS ' CON ABS i Conc. FORM VIII - IN r iQ ILM04.1 U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Lab Name: H2M LAB'S, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Concentration Units: ug/L MW -5D I _ SDG No.: TSLO10 Level (low/med): LOW I 'j Serial ;Differ- ! j Initial Sample I( Dilution Analyte I + Result (I) C. i Result (S) C j I ence IQ f M Cadmium - 0. 16 U 1 0. 821 U i I - -_ P i Calcium — _ 99051.711—i _ 103456. 151 i -�? 4 - 4i I ! ` ^� P ` iIron i 93.377 B i t _ T 16.75. B ; �� ` 5. 40 U 82.1 100.0i�—_� P _ P Lead 2. 33! B ! i _ Magnesium Manganese- ^_ _ 58059.43_; , !_ 11812.4 91 I '-r _ 60116.30; , 12672.15 _7.31 ~_ 3 5 3 P I P Potassium 1210 2.6:E' P 18 1 (Sodium i 295273 63 1250359.751 —, ; - --2 1, P - .`.----- i- FORM IX - IN- ILM04.1 Lab Name: H2M LABS, Lab Code: 10478 ICP ID Number: Flame AA ID Number: Furnace AA ID Number: Comments: U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) NC. Contract: Case No. SAS No.: SDG No.: TSLO10 TJA6IEA Date: 3/19/20.07 i Analyte Wave- length Back- I (nm) aground! CRDL ; (ug/L) IDL (ug/L) M ;Cadmium 226.501 i 5.01 `5000.01 0.2! ICPum _': 6.21 P _317.931 90i 100. O 1. 9 P 1 rIron ;259. }Lead !_t220.35; iMagnesium j 279.08L 3.0 5000.01 1_1! P ~ —7.7 P [Manganese 1 257.61! 15.0; 0.11 PP Potassium �- 766.491 5000.0;---^11.41 P ;Sodium 1 _ 588.901_ T 5000_.0 3.11 P FORM X - IN ILM04.1 O O 4 W T' PoHgi OOTi 6L6'0- 10000000'0 0000000,0 ;0000000' 0 0000000'0 1000_0000'0 0000000'_0 10.000000'0 0000000'0 X0000000'0 0000000'0_±0000000'0 006806b'0 ;0000000'0 0000000 ,0 ;000000_0" 0_ 0000000' 0_;000_0000' 0 0000000'0 10000000'0 000000010 ;0000000'0 ZLbS000'0-`0000000'0 _0000000'0 i0000000'0 00ST09S' 0- 10000000_' 0 OOLLOhb'O 10000000'0 0000000'0 100,00000'0 0000000'0 +0_000000'0 0000000'0 10000000'0 0000000'0 10000000'0 0000000'0 `0000000'0 0000000'0 i 0000000'0 0000000,0 00000.00'0 0000000'0 ';:0000000'0 000000.0'0 jD000000'0 000000_0'_0.;000.0000' 0 0000000'0 ;0000000'0 0000000.0 10000000'0 0000000'0 10.000000'0 OOPTLTO'0-i0000000'0 00 fDW NI - ( T IEVd ) IX WU03 06L£b£0'0-_ ;0_000000'0 0000000'0 ;0000000'0 0_000000'0 __;0000000'0 0000000'0 10000000'0 0000000'0_ 10000000'0_ 0000000'0 0000000'_0 00000_00'0 _+0000000'0 00000_00'0 ;0000000'0 0000000'00000000'0 0000000'0 ^;0000000'0 0000000'0 -10000000'0 00_0000.0'0 100000D0'0 0000000'0 10000000'0 009S80T'O ;00_00000'0 FO0TT_6 60 .0 __10000000 ' 0 ;0000000'0 ;0000000'0 ;0000000'0 10000000'0 iZOb0000'0- '0000_000'0 L9000000.0 10000000'0 10000000'0 10000000'0 0000000'0 ;0000000'0 !VL£T000'O 10000000'0 96S£000.0- 10000000'0 !000000.0`0;0000000'0 ;0000000'0 10000000'0 10000000'0 10000000'0 ;0000000'0 10000000'0 !0000000' 0 _ !000000_0' 0 0 00 0000'0 10000000'0 a3 eO 0000000'0_ 0000000,0 0000000'0 _0_000000'0 0000000'0 000_0000'0__ 000000_0'0 000_0_000_' 0 0000000,0 0000000'0 0000000'0 SS£T000'0= 0000000'0_ OOOL09�'O 0000£bZ'0 0000000'0 0000000'0 0000000'0 10000000'0 ;0000000'0 `0000000_0_ ZS00000'0- ;0000000'0 ?0000000'-0 '0000000"0 10000_000'0 ;0000000_' 0 110_0_00000'0 ;0000000"0 :Jog sao4oe3 UOT40aaaoD-4uauiaTa1a4ul TK LL' LOb_ 00'689 £Z'0££ LO'8ZE 9I'88Z- £0'961_ £0'96T 6b'99L 09'TEZ £0'Z0Z T9'LSZ 80'6LZ S£'OZZ SE' 0ZZ - 6b'TLZ I66'6SZ [SL ' bZ£ 8ZZ IZ9L9Z j£6' LTE lOS'9ZZ 189'6bZ b0'ET£ ILS6 6 b0'68T b8'90Z 68''90Z jZZ'80£ ( uiu ) ggbuaT -aaeM : SWGUMOD uinTTTugs MnTquoags wnzpog wnrpoS — aanT?S uoozTTS wnzuaTaS an-TuaTaS wnisSegoa G pe pp uoal - -Tadd-0 �Tp 3 wnTwoag3 umzoTe3 uinTllIpeo uozoe m.TT a@O —uinT-T20 aqA L00Z/TZ/S0 :aac�unN QI d0I OTO'IS,L :'oN OQS :'oN SKZIN :-ON aSeo 8LbOT :apoo 4e'I :goe'aquo.D 'ONI 'SgK2 WZH :auiuN qez (X,I` VGNNK) S2i0ZZii3 NOIJZ)a2IWD ZN3W3gS'd3lNI dOI KTT aqD - Ka3 'S'D I U.S. EPA - CLP 11A ICF INTERELEMENT CORRECTION FACTORS (ANNUALLY) t Lab Name: H2M LABS, INC. Contrac • Comments: FORM XI (PART 1) - IN ILM04.1 kn M O O Wave- `+ Interelement . Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSLO10 ICP ID Number: TJA61EA Date: 05/21/2007 Comments: FORM XI (PART 1) - IN ILM04.1 kn M O O Wave- `+ Interelement Correction Factors for: j I length Analyte i (nm) i Al Ca Fe M g Co Tin 189.99 0._0000000) .00001 -0.00021801 0.0000000 0.0000000 0000000 _ Titanium 334.94j�` 292.401 0.0000000;, 0.0_000000; 0.0000000; 0.0000000' 0.0000000 0.0000000, 0.00000.00 0.0000000 0 0.0000000 iVanadium Enc ; 0_00000001 0.00000 Or 0.00009111 0.0000000; 0.0000001 1 _213.86;]_ Comments: FORM XI (PART 1) - IN ILM04.1 kn M O O I'vOHgI Ni - (z Z2iKd) IX Hdoi l : squaunuo0 OOLT9ZT'T- 10000000'0 -- i001LIZL"o- :0000000'0 — 0002761'0 +98'061 ' urn?TTpus lun?quoz:Si -- 0000000' 0 10000000' 0 ;0000000 0 — 0000000 0 ;0000000.6 _ LL'LOb 1� OL 0 68S 0000000 ,0 00_00000 " 0 10000000 0 0000000 0 100000001' 0� _ -n?pos 0000000'0 10000000'0 10000000'0 0000000 0 10000000_0 'EZ'0££ umrpoSl zanTTS 0000000,0 '0000000'0 000b99T'O ,00000.00 0 0000000'0 _' L0'8Z£ 191'882 j uO°?T?S1 0000000'0_;0000000'0 10000000'0 0000000'0 10809600"0_-_ ! uzn?ua S, ~OOT6SZZ'0 10000000'0 OOLOSTS•0_ 100000000 ;0000000.0 £0961 I gun?ua1a� 0000000' 0 000'0 0000000.0 —�-- -- 0000000 0 - 10000000.0 1£0'962 iun rsseToa —; 0000000'0 ,0000000•'0 10000000"0 ;0000000'0 1 0000000'0 {j--- 6b'99L I — _ -0000000'0 1 158£000'0-100000_00 ;00000_00"0 i0000000 0 0 10000000'0 10000000'0 ;0000000'0 x0000000.0 109'1£2 ;0000000'0 j1£0'ZOZ Tai[°TIS j>unua--------------------- P aue i asuey� 0000000'0 1000o000'0� 10000000'0 10000000'0 ;T9'LSZ 0000000'0 00000000 80Zb00-0 0000000"0_ _;0000000'0 ;0000000'0 ;80'6LZ ;- nzsau eW 1 P 0000000.0 '•0008£££"0 10000000'0 ;0000000 0_ 10000000"0 _S£�OZZ — —_- - _ 009LT8T' o- i009HZ T' 0 0 _ !0000000,0-10000000' 0 !S£' OZZ _ pe w, 1 Z6zs000'0 10000-000'0 _10000000' ;0000000'0 0000000 0 100000000 1 ;�b_1LZ—I _ uozl 0000000 0 o0000On•n onnnnoo-o 10000000 0 _� _ —'000000_0 '0000000'0 �— --- — ib6'6SZ — —.-- i uO�I 0000000,0 _ 10000000' 0 _ _ 10000000,0 0 *0 io00o000 " 0 0000000.0 9C• Z£ 1Z9'8ZZ 1 z�Oo ! :ITeq°o 0000000'0 000o000'o i0000000,o 10000000 S 0£000'0 10000000"0 ;0000000'0 X0000000 0 '0000000"0 iZ9"L9Z uzn?uiozu0; 0000000"0 ;000OOoo'0 10000000'0 10000000 0 10000000 _0 *0 �I FIFE SOS 1 »? Teo umTWP123 0 000 0 I£18T00o'o 0000000'0 !0000000 10000000"0 9ZZ 1 10000000"0 !0000000'0 1,0000000 0 `o000000'0 1 189'6bZ uOZOg �.Z:ObZ000'0- I T89Zo00'0 10000000"0 10000000"O 10000000 0 ;0000000'0 60'£2£ uzn? -1 ; TT ucnzzegj 0000000'0 000 0000.0 !0000000"0 '0000000 0 ;0000000'0—;I1b'86b 1 - 0000000'0 10000000'0 ;0000000"0_ 10000000'0_ 1000£LS9'0 'L b0'681 �uouz?�u� 1 00909V -'S- i000b6LZ`T- 10000000'0 10000000.0 _ '0009S£6 L..v8'90Z_ i —�ouz?�uFtl 0000000'0 ;0000000'0 !000000_0'0_ 11 000000'0!';0008vL£'9 ii 8'90Z 1 OOSZLTO"0 10000000_0_IOSZ6I000- - — 10000000'0 — ,0000000"0 — — 122'80£ ; wnu?uznT�1 _ n -- -zN uW no ao (amu) 1 a4ATeuKI j p�.buaT i i zoo s.z0q02,3 uo?40aaaOD quauiaTaza4ul { i -aaeM 1 LOoZ/TZ/S0 :a-JeQ VHT9vfl :.zaquinN QI doI 01011SJ, : °N oQS :'°N SVdN :-ON aseo 8LDOT :ap°o qe7 :q°ezquoo "DNI 'Sg'dq WZH :awes qe7 (XggvoNNH) sEol3VZ NoIsosdwo ZNgldg` ESINl doI SIT azo - Vd2 'S'D r� U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSLO10 ICP ID Number: TJA6IEA Date: 05/21/2007 Comments: FORM XI (PART 2) - IN ILM04.1 i1� Wave- ( Interelement Correction Factors for: ; j length i ! Analyte (nm) ! Cr Cu Mn Ni V ;Tin -- 189.99 I ----.. 0.0000000; 0.0000000_ 0.00.00000! — _, --— 0.0000000! 0.0000000 ;Titanium , 334.94 1 0.0000000 0.000_0000; 0.0000000; 0.00000001 0.0000000—j !Vanadium ( 292.40! 0:0000000; 0.0000000; 0.00000001 0.0000000! 0.0000000 J (Zinc213.86 0.0000000` ----- 0.00090461 - O.000O0001 0.00392701 0.0000000 — Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO10 ICP ID Number: TJA6IEA Date: 05/22/2007 Comments: 00 M O O ILM04.1 FORM XII - IN Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP., 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSLO10 EPA Sample E No. ! Preparation Weight Date (gram) y i Volume (mL) FB 061407 —i— 50 Lc w_ _06/19/2_007 ! 06/19/200750 -f Mw -1D -' 0.6/19/2007 50 iM is _-�_ _�- 06/19/2007 _- --- 7_ 50 I E 3D 06/19/2007 1 Mw -3S _!_ 0_6_/19!200'7 —! i 50 Mw -4s 007 06/19/2007 1 _ 06/19/2007k --- 50 - —} 50 ' S0 - �Mw-SDD jM SDs --- i - 06/19/2007 { — ---06/19/2007 `--- -- ; 50 — 50 i _ ------i- Mw -5s ---- — _ 06/19/2_007 j 50 'Mw -6D �M 6S 1 06/19/2007 06/19/2007 _ 50_ _ J 50 Mw -8D 06/19/2007 50 I -_T Mw 8s - ----i _ 06/19/2007 _i 50 Mw -BD _— 06/19/2007 _ ; 50 PW 106/19/2007 50 FORM XIII - I14 ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA61EA Start Date: 06/20/2007 FPA U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSLO10 06/20/2007 Analytes Sample D/F No. Time i% R AiS A B LBI C C C!CiC! FIP E 11 1 iA,R!O!U1EjB LIB S A E DI M M K SjA!NjT VIZ C 1 1 1 1 i I GIN G I E GIA L: N N. I 104 1.00 084 ixi x x ix x XIX x Is 1.00 6851 x X1 xi S 1.00 1.00 0857 0902 - --------- x 1.00 09,16 j 0923 i i I i 1XI T Ix x! ix 77- -X X, icv 1.00 1.00 0928 j 0933 1 X;x i x licv 1.00 0940 1 x x : 1ICB 'CRI 1.00 0948 1 Xix �x x i X x,x! x 1XI 1XI 1.00 ICSA 1.00 IICSAB1.00 0955 1.029 j 1037 X x x 1 xix "L -- t-----I--=--�j x x x x x 1 x x Xi jCCv 1.00 0 4 5 !xx 1 1 x 'Ix x X� X ix F CCB 1.00 1.00 T- 1052 1 1100 X x1x PBW ILCSW 1.00 1.00 1107 ills X x x x ix1xix X, X X x x X, -D x x Mw B 1.00 IMW-4D 1.00 1123 1130 x x x X ;x X x x x IX; x IMW-49 1.00 1.00 j 1138 1145 ;X;Xi XjX xxx x X1 x X x x x MW -5D 1.66 1153 1 -Co --t- x X!x x x x L x MW--5DS 1.00 12 x x x x j x i x x x MW-5DL 1 5.00 1208 x x 1 x x x x x x x x 1MW-5s I 1.00 1 1215 X x x x x X ccv 1.00 1 1223 x ixx x x x jCCv CCB 1.00 1.00 i 1250 C 1258 x x x X x x x MW -6D 1.00 1 1305 x x 1x X T -x X�X, iMW-6S 1.00 1313 Xx I WX x x x x MW -8D 1.00 1320 , x x X 1 x :x X X :-I� IMN-as FB 061407 1.00 1.00 1328 1336 1 x x 1 1 x XT, I x xix x x XX ix X1 x! X -F 1.00 1-343 X- xlxlxlxl -,jx 1 '1 1XI FORM XIV - IN 1LMU4.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA61EA Start Date: 06/20/2007 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSLO10 06/20/2007 FORM XIV - IN ILM04.1 Analytes Sample D/F Time R 1 A S 1 A BIB5CICICCICF PIM IM!HN'K' b'A N T,V:Z,Ic ,l No. ILTS A11DIAIRIO UE BIGIN'G E I GIA Ll jNjNj Mw -is 1.00 1351 X x x x x x x x MW -3D 1.00 X x i x x . . . . . . . �71 ix; T -i MW -3S lzzzzzz 1.00 50.00 i 14-6-6 1418 X x x x x x CCv 1.00 1427 1 X x I x x x x ccv 1.00 1435 --L-A x CCB 1.00 ------ 1442 lxix x I x x xx i xi zzzzzz 1.00 1450 . . ....... . �CRI 2.00 1.00 1506 1514 X , x x Ix_7 1 1521 1 X I x X x x x1x IICSA ICSAB _1'.00 1.00 1529 X X. X ix x X.. —i 1CCv 1. 00' !:Dj 6 X 1x X X X iC'cvt !CCB 1.00 1.00 1544 1552 X 1 X;xl xixi x X! x! x IV FORM XIV - IN ILM04.1 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY INORGANIC ANALYSIS SDG: TSL010 Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab I Date Analyzed 0706952-001 MW -BD WATER I CA,CD,FE,K,MG,MN,NA,PB, 1 14 -Jun -07 06/07 07069527002 MW -4D I WATER CA,CD,FE,K,MG,MN,NA,PB, 114 -Jun -07 06/07 0706952-003 IMW-4S WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 I 06/07 0706952-004 1MW-5D I WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 06/07 0706952-004DU1' MW-5DD 1 WATER CA,CD,FE,K,MG,MN,NA,PB, 114 -Jun -07 06/07 0706952-004MS !MW-5DS IMW-5S WATER CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 T 06/07 0706952-005 1 WATER I CA,CD,FE,K,MG,MN,NA,PB, I 14 -Jun -07 06/07 0706952-006 0706952-007 IMW-6D f MW -6S WATER i WATER CA,CD,FE,K,MG,MN,NA,PB, I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 I 14 -Jun -07 I 06/07 06/07 0706952-008 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 114 -Jun -07 I 06/07 0706952-009 IMW-8S WATER I CA,CD,FE,K,MG,MN,NA,PB, 14 -Jun -07 I 06/07 0706952-010 1FB 061407 WATER I CA,CD,FE,K,MG,MN,NA,PB, I 14 -Jun -07 I 06/07 0706986-001 MW -1D j WATER CA,CD,FE,K,MG,MN,NA,PB, I 15 -Jun -07 1 06/07 0706986-002 MW -15 I WATER CA,CD,FE,K,MG,MN,NA,PB, 115 -Jun -07 I 06/07 0706986-003 ;MW -3D I WATER CA,CD,FE,K,MG,MN,NA,PB, 115 -Jun -07 OG/07 0706986-004 1MW-3S WATER CA,CD,FE,K,MG,MN,NA,PB, 115 -Jun -07 I 06/07 TSLO10 M42 U28t I% C® III. RAW DATA FOR METALS A. ICP DATA P 0014 CLIENT 1 SLOIc-�)'wµs,Oot - DATE SuuC a0,2000q ANALYST .TASK: (''L?1 RESULT FILE: i # ; SAMPLE NOTES # SAMPLE NOTES 1 ZCV 26:OaoU9SZ- tyA0 (6S ! S 2 7CVl_ 27:o\o.� 3 i 1 -CA ! 28:OloLdq$(P-Gb,-.),! i 4 291 I , 5 '! Icsx, i i 30 c! 1n1 ^ 3 { , _ , r i 6 !-LS1F:-ij i i 31, 7 CGV N ! i 32 ,' 010 - t^• 0029 ER 8 Cf -VLA i 33! CC -\)3 i ! i 9`! CC61 ! - i 34! Ccy1-3 i 10l I'dar- o�\�jq� !`)aW 'TSl oto i 35 ! co�,s • ! i II ! Lts p�tJg� i L.i.6W 36lQgo-4 011.1-OP0fd )& wW- uL2-pbo'f61^ Rc%'vti-P.i�„� i Z2i(�'fO�o �G^(O�11 k, -a, 1 37107100bG-ooLtk�i r%t.W-�J i r i , 13.. + i 14� Od3l� N1W—yS. ! 391 mc5i3-r- ! ! 15 i CoLtu 40 ! S.CSAfbr- ! ! L 1611 wP 41 ! CGV ! 171 µ. i 421 Cc -\)Q' ! i i 18i SO 43! ! i 19 4-4'1 ! ! 201, a ! i 451, ! i' 21' CCULD ' 46'. `i 22 ! c.Gis 2 - i ; 47, ' ' 23i ! µWb i 48 i. ! ' 24'' ppl ! 141-(o'S 49 ! ! P 0014 Standardization Rpt. P' od: CLP1 Standard: StdBLANK F Time: 06/20/07 08:44:04 18.05 Elem Ag Al As1890 Avge -.00406 .0133 -.00260 SDev .00007 .0020 .00086 %RSD 1.6405 14.94 32.942 #1 -.00398 .0155 -.00162 #2 -.00411 .0129 -.00303 #3 -.00408 .0116 -.00316 Elem Cd Avge -.0036 SDev .0007 %RSD 18.05 #1 -.0033 #2 -.0044 #3 -.0032 Elem Mg Avge .0084 SDev .0044 %RSD 52.41 42.41 .0134 .0004 .0069 ff� .0050 Elem 2203/2 Avge .00080 SDev .00267 %RSD 335.31 #1 .00138 #2 -.00212 #3 .00312 Elem Sr Avge .0003 SDev .0001 %RSD 19.27 #1 .0002 #2 .0002 #3 .0003 Co Cr .0002 .0008 .0001 .0001 44.86 5.934 .0001 .0008 .0002 .0007 .0001 .0007 Mn Mo .0007 .0002 .0003 .0002 42.41 68.05 .0004 .0001 .0010 .0002 .0007 .0004 2068/1 2068/2 .01024 .01043 .00477 .00488 46.625 46.801 .01572 .01419 .00801 .01219 .00699 .00491 Ti T11908 .0004 -.00541 .0001 .00195 26.33 36.122 .0003 -.00331 .0005 -.00718 .0003 -.00575 06/20/07 08:51:30 AM B 0008 .0002 29.87 .0006 .0011 .0008 Cu .0062 .0003 4.005 .0059 .0063 .0064 Na -.0221 .0023 10.50 -.0248 -.0208 -.0208 1960/1 -.01075 .00232 21.597 -.00820 -.01273 -.01132 v .0000 .0001 687.7 0001 .0000 -.0001 Ba .0001 .0000 26.33 .0001 .0001 .0001 Fe .0001 .0000 30.59 .0002 .0001 .0001 Na .4414 .0148 3.348 .4243 .4499 .4499 1960/2 .00125 .00082 65,.828 .00055 .00216 .00104 Zn .0049 .0005 9.307 .0044 .0052 .0051 Be -.0005 .0000 4.592 -.0005 -.0005 -.0005 Fe .1961 .0949 48.36 .3014 .1697 .1173 Ni .0004 .0001 40.96 .0004 .0005 .0002 Si .0511 .0021 4.155 .0487 .0521 .-0526 page 1 Ca .0134 .0035 26.22 .0174 .0121 .0107 K .0121 .0007 5.649 .0113 .0127 .0122 2203/1 .02374 .00648 27.305 .02396 .03011 .01715 Sn .0071 .0028 39.02 .0076 .0041 .0097 Standardization Rpt. 06/20/0708:57:28 AM page 1 r od: CLP1 Standard: StdAGSBH F Time: 06/20/07 08:51:36 Elem Ag 2068/1 2068/2 Avge .81362 3.1659 1.9330 SDev .00590 .0280 .0126 %RSD .72537 .88600 .6538.1 #1 .81761 3.1614 1.9446 #2 .81640 3.1960 1.9348 #3 .80684 3.1404 1.9195 Standardization Rpt. 06/20/07 09:02:39 AM page 1 N Dd: CLP1 Standard: StdICSH Rui, Time: 06/20/07 08:57:34 Elem Al Ca Fe Avge 33.27 48.16 .5891- SDev .20 .15 .0037 %RSD .5989 .3204 .6210 #1 33.46 48.23 .5925 #2 33.29 48.26 .5895 #3 33.06 47.98 .5853 Mg 70.37 .20 .2902 70.19 70.59 70.32 O O E-+ Standardization Rpt. 06/20/07 09:08:38 AM K )d: CLP1 Standard: StdFURNH mime: 06/20/07 09:02:45 Elem As1890 2203/1 2203/2 1960/1 1960/2 T11908 Avge 1.2022 3.0357 1.5210 .91008 .65826 .93612 SDev .0104 .0370 .0054 .00754 .00183 .00442 %RSD .86406 1.2187 .35518 .82802 .27734 .47195 #1 1.2037 3.0777 1.5149 .91704 .65653 .93362 #2 1.1912 3.0080 1.5249 .90208 .65810 .93352 #3 1.2118 3.0212 1.5233 .91112 .66017 .94122 page 1 Standardization Rpt. 06/20/07 09:23:26 AM page 1 N od: CLP1 Standard: StdMULTH Time: 06/20/07 09:16:47 Elem B Ba Be Cd Co Cr Cu Avge 1.733 5.533 6.882 53.62 1.901 2.376 1.559 SDev .012 .069 .043 .83 .017 .016 .011 %RSD .6829 1.253 .6184 1.545 .9144 .6572 .6861 #1 1.726 5.594 6.871 54.39 1.885 2.380 1.559 ##2 1.747 5.548 6.928 53.73 1.920 2.390 1.570 #3 1.726 5.458 6.845 52.74 1.900 2.359 1.548 Elem Mn Mo Ni Si Sn Sr Ti Avge 16.77 2.060 1.844 1.309 9.1.38 10.07 1.502 SDev .11 .023 .032 .008 .163 .07 .034 %RSD .6277 1.122 1.710 .6280 1.779 .7000 2.236 #1 16.79 2.078 1.876 1.311 8.954 10.10 1.539 #2 16.86 2.068 1.844 1.316 9.262 10.13 1.495 ##3 16.65 2.034 _ 1.813 1.300 9.198 9.995 1.473 Elem v Zn Avge 1.159 4.943 SDev .007 .030 %RSD .6172 .5979 1.157 4.937 1.166 4.975 #3 1.152 4.916 Standardization Rpt: M >d: CLP1 Standard: StdFENAL R _'ime: 06/20/07 09:23:32 Elem Fe Na Avge 40.60 35.64 SDev .36 .46 %RSD .8772 1.289 #1 40.19 35.12 #2 40.81 35.97 #3 40.81 35.83 06/20/07 09:28:38 AM page 1 Standardization Rpt. N, Dd: CLP1 Standard: StdNAKH Ru rime: 06/20/07 09:28:44 Elem K Na Avge 7.553 2.020 SDev .028 .001 %RSD .3676 .0465 #1 7.525 2.021 #2 7.555 2.020 #3 7.580 2.020 06/20/07 09:33:03 AM page 1 0 O H Standardization Report 06/20/07 09:33:03 AM page 1 N od:,. CLP1 Slope = Conc (SIR) /IR Element Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGSBH StdBLANK 2445.97 9.91975 06/20/07 09:28:44 Al 308.215 StdICSH StdBLANK 15.0338 -.200662 06/20/07 09:28:44 As1890 189.042 StdFURNH StdBLANK 829.996 2.16014 06/20/07 09:28:44 B 249.678 StdMULTH StdBLANK 2.88658 -.002368 06/20/07 09:28:44 Ba 493.409 StdMULTH StdBLANK .903672 -.000086 06/20/07 09:28:44 Be 313.042 StdMULTH StdBLANK .726696 .000346 06/20/07 09:28:44 Ca 317.933 StdICSH StdBLANK 1.19652 -.010764 06/20/07 09:28:44 Cd 226.502 StdMULTH StdBLANK .093253 .000339 06/20/07 09:28:44 Co 228.616 StdMULTH StdBLANK 2.62983 -.000431 06/20/07 09:28:44 Cr 267.716 StdMULTH StdBLANK 2.10566 -.001631 06/20/07 09:28:44 Cu 324.754 StdMULTH StdBLANK 3.22022 -.019950 06/20/07 09:28:44 Fe 271.441 StdICSH StdBLANK 1.02370 -.000070 06/20/07 09:28:44 Fe 259.940 StdFENAL StdBLANK .123746 -.024272 06/20/07 09:28:44 K 766.491 StdNAKH StdBLANK 1.06020 -.006063 06/20/07 09:28:44 Mg 279.079 StdICSH StdBLANK .890154 -.006893 06/20/07 09:28:44 Mn 257.610 StdMULTH StdBLANK .298044 -.000213 06/20/07 09:28:44 Mo 202.030 StdMULTH StdBLANK 2.43461 -.000604 06/20/07 09:28:44 Na 330.232 StdNAKH StdBLANK .987199 -.006743 06/20/07 09:28:44 Na 588.995 StdFENAL StdBLANK .142040 -.062692 06/20/07 09:28:44 Ni 231.604 StdMULTH StdBLANK 2.71178 -.000959 06/20/07 09:28:44 2203/1 220.351 StdFURNH StdBLANK 332.015 -7.88273 06/20/07 09:28:44 2203/2 220.352 StdFURNH StdBLANK 657.794 -.523262 06/20/07 09:28:44 2068/1 206.831 StdAGSBH StdBLANK 633.775 -6.49062 06/20/07 09:28:44 /2 206.832 StdAGSBH StdBLANK 1040.28 -10.8516 06/20/07 09:28:44 /1 196.021 StdFURNH StdBLANK 1085.97 11.6760 06/20/07 09:28:44 1960/2 196.022 StdFURNH StdBLANK 1522.04 -1.90225 06/20/07 09:28:44 Si 288.158 StdMULTH StdBLANK 3.94006 -.201507 06/20/07 09:28:44 Sn 189.989 StdMULTH StdBLANK .547615 -.003909 06/20/07 09:28:44 Sr 421.552 StdMULTH StdBLANK .496336 -.000135 06/20/07 09:28:44 Ti 334.941 StdMULTH StdBLANK 3.32973 -.001272 06/20/07 09:28:44 T11908 190.864 StdFURNH StdBLANK 1062.10 5.74647 06/20/07 09:28:44 v 292.402 StdMULTH StdBLANK 4.31580 -.000053 06/20/07 09:28:44 Zn 213:856 StdMULTH StdBLANK 1.01744 -.004979 06/20/07 09:28:44 Pb2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Sb2068 206.838 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Se1960 196.026 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Standardization Readback Report 06/20/07 09:33:03 AM M )d: CLP1 Element Wavelength Standard Ag 3.28.068 StdBLANK StdAGSBH Element Wavelength Standard Al 308.215 StdBLANK StdICSH Element Wavelength Standard As1890 189.042 StdBLANK S't dFURNH Element Wavelength Standard B 249.678 StdBLANK StdMULTH Element Wavelength Standard Ba 493.409 StdBLANK StdMULTH E ent Wavelength Standard Be 313.042 StdBLANK StdMULTH Element Wavelength Standard Ca 317.933. StdBLANK StdICSH Element Wavelength Standard Cd 226.502 StdBLANK StdMULTH Element Wavelength Standard Co 228.616 StdBLANK StdMULTH Element Wavelength Standard Cr 267.716 StdBLANK StdMULTH Element Wavelength Standard C 324.754 StdBLANK - StdMULTH Known Concentration .000000'' 2000.00 Known Concentration .000000 500.000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .005266 57.6118 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration -.000000 500.000 Measured Concentration .000000 1000.00 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00113 Measured Signal .013397 48.1584 Measured Concentration .000000 5.00051 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00161 Measured Concentration .000000 5.00000 page 1 Residual Concentration .000000 -.000122 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 -.001134 Residual Signal -.008131 9.45341 Residual Concentration -.000000 -.000510 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.001608 M Residual o Concentration -.000000 a .000000 Standardization Readback Report Eicui2nt Wavelength Standard Fe 271.441 StdBLANK StdICSH Element Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard K 766.491 StdBLANK StdNAKH Element Wavelength Standard Mg 279.079 StdBLANK StdICSH Element Wavelength Standard Mn 257.610 StdBLANK StdMULTH ]ient Wavelength Standard T 202.030 StdBLANK StdMULTH Element Wavelength Standard Na 330.232 StdBLANK StdNAKH Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTH Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNH Element Wavelength Standard 093/2 220.352 StdBLANK StdFURNH 06/20/07 09:33:03 AM Known Measured Signal Signal .000055 .000122 .602976 .589087 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Signal Signal .006759 .012094 8.00205 7.55341 Known Measured Signal Signal .000584 .008400 62.6316 70.3681 Known Measured Concentration Concentration .000000 .000000 5.00000 4.99715 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.01559 Known Measured Signal Signal -.028601 -.022141 1.98779 2.02039 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.000 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 page 2 Residual Signal -.000067 .013889 Residual Concentration .000000 .000000 Residual Signal -.005335 .448644 Residual Signal -.007816 -7.73653 Residual Concentration -.000000 .002855 Residual Concentration .000000 -.015590 Residual Signal -.006459 -.032606 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000061 d - Residual Concentration o .000000 0 .000000 a F� Standardization Readback Report 06/20/07 09:33:03 AM E--,,,--nt Wavelength Standard 2068/1 206.831 StdBLANK StdAGSBH Element Wavelength Standard 2068/2 206.832 StdBLANK StdAGSBH Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNH Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNH Element Wavelength Standard Si 288.158 StdBLANK StdMULTH E int Wavelength Standard S 189.989 StdBLANK StdMULTH Element Wavelength Standard Sr 421.552 StdBLANK StdMULTH Element Wavelength Standard Ti 334.941 StdBLANK StdMULTH Element Wavelength Standard T11908 190.864 StdBLANK StdFURNH Element Wavelength Standard V 292.402 StdBLANK StdMULTH Element Wavelength Standard 7.n 213.856 StdBLANK StdMULTH Known Measured Concentration Concentration .000000 .000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 -.000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 1000.00 10.00.00 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.95659 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.02400 page 3 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 -.000061 Residual Concentration 000000 -.000061 Residual Concentration .000000 .043410 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration =.000000 .000000 Residual Concentration -.000000 -.000061 Residual Concentration -.000000 .000000 Residual `n Concentration 0 .000000 -.024004 C:) ri E-� Standardization Readback Report 06/20/07 09:33:03 AM E =_nt Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard 8b2068 206.838 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .0,00000 .000000 .000000 page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 O O c� E -i Analysis Report 06/20/07 09:40:35 AM page 1 1 [od: CLP1 Sample Name: ICV Operator: MAG 1,,,, Time: 06/20/07 09:33:09 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1005.5 48.74 526.06 2.526 2.549 2.516 47.89 SDev 3.0 .20 3.34 .018 .010 .017 .33 %RSD .30167 .4098 .63578 .7027 .3970 .6853 .6950 #1 1006.1 48.83 524,14 2.510 2.554 2.501 47.62 #2 1002.3 48.51 524.13 2.522 2.537 2.512 47.78 #3 1008.2 48.87 529.93 2.545 2.555 2.535 48.26 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.489 2.485 2.488 2.575 48.76 83.96 51.44 SDev .009 .024 .015 .011 .26 .34 .32 %RSD .3603 .9492 .6175 .4385 .5246 .4090 .6195 #1 2.494 2.463 2.478 2.568 48.66 84.11 51.15 2.479 2.483 2.481 2.569 48.57 83.57 51.37 2.494 2.510 2.506 2.588 49.05 84.21 51.78 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 -55.00 Low 2.250 2,.250 .2.250 2.250 45.00 72.0'0: 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.477 2.465 83.05 2_.502 574.68 512.02 984.84 SDev .014 .012 .43 .012 7.34 2.42 17.68 %RSD .5561 .4723 .5153 .4721 1.2780 .47231 1.7956 #1 2.467 2.458 82.69 2.513 566.93 509.23 965.53 #2 2.471 2.458 82.94 2.490 575.56 513.63 98.8.76 #3 2.492 2.478 83.52 2.504 581.54 513.18 1000.2 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 983.12 541.68 519.54 2.627 2.471 2.537 2.784 SDev 15.80 6.80 3.19 .017 .043 .012 .058 %RSD 1.6072 1.2553 .61463 .6451 1.722 .4764 2.066 965.41 533.84 517.69 2.613 2.429 2.531 2.850 988.16 545.94 523.23 2.621 2.470 2.529 2.744 #3 995.78 545.25 517.71 2.646 2.514 2.551 2.759 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/017 09:40:35 AM Low . Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 513.42 2.496 2.562 532.88 983.69 526.9'1 SDev 3.88 .016 .016 3.93 16.41 3.86 %RSD .75488 :6305 .6219 .73798 1.6686 .73349 #1 515.38 2.483 2.550: 528.45 965.45 523.06 #2 508.96 2.490 2.557 534.25 988.36 530.79 #3 515.93 2.513 2.580 535.95 997.27 526.88 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 00 O O H Analysis Report 06/20/07 09:48:06 AM page 1 M �d: CLP1 Sample Name: ICVL Operator: MAG R'_, Cime: 06/20/07 09:40:41 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.02047 -.0380 -.64169 0069 _0007 .0008 -.0588 SDev .04000 .0083 1.89180 .0010 .0002 .0002 .0033 %RSD 195.43 21.93 294.82 13.85 26.66 25.95 5.603 #1 -.05677 -.0288 1.1643 .0080 .0007 .0009 -.0607 #2 -.02705 -.0403 -.48034 .0064 .'0009 .0009 -.0550 #3 .02242 -.0449 -2.6090 .0063 .0005 .0006 -.0607 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm, ppm ppm ppm ppm Avge .0008 .0005 .0007 -.0002 2.589 .0635 -.0468 SDev .0003 .0001 .0004 .0006 .022 .0158 .0037 %RSD 31.09 25.28 60.44 432.4 .8601 24.84 7.984 #1 .0008 .0004 .0006 -.0008 2.572 .0495 -.0479 "'- .0010 .0006 .0013 .0005 2.582 .0806 -.0427 .0005 .0004 .0004 -.0002 2.614 .0603 -.0499 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Hiah 2.750 Low 2.250' Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0117 2.660 .0008 -.99968 -.08054 -2.9358 SDev .0003 .0044 .022 .0001 2.93062 1.70297 4.5442 %RSD 44.38 37.61 .8332 15.16 293.15 2114.4 154.78 #1 .0005 .0165 2.636 .0007 -4.3349 1.0513 2.3098 #2 .0009 .0108 2.666 .0008 1.1636 -2.0391 -5.4485 #3 .0004 .0079 2.679 .0009 .17225 .74615 -5.6687 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb PPM PPM PPM PPM Avge -.08173 3.1969 -1.5821 ..0177 :0012 .0007 .0009 SDev 2.82307 2.1240 3.5664 .0025 .0003 .0002 .0003 %RSD 3454.3 66.440 225.42 14.26 21.77 33.97 39.85 3.1633 1.2479 -5.4324 .0148 .0015 .0007 .0010 -1.4359 5.4608 -.92198 .0189 .0011 .0009 .0011 #3 -1.9726 2.8820 1.6081 .0195 .0011 .0004 .0005 Errors -NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 09:48:06 AM page 2 n L �j Zn Low Sb2068 Elem T1.1908 Units ppb Avge 2.6356 SDev 1.5224 %RSD 57.761 #1 1.0776 #2 2.7097 #3 4.1196 Errors NOCHECK High 328.85 Low .0018 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0012 .0027 -.38654' -1.0321 .00932 .0006 .0002 .82359 3.3941 2.8168 53.27 6.984 213.07 328.85 30225. .0018 .0028 -.74225 2.8791 -3.2078 .0010 .0029 -.97248 -2.7720 1.2035 .0006 .0025 .55512 -3.2034 2.0323 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/,07 09:55:38 AM page 1 Mr., ,d: CLP1 Sample Name: ICB Operator: MAG R'U.Ll "lime: 06/20/07 09:48:12 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.04317 -.0485 .06839 .0007 .0002 .0003 -.0587 SDev .32009 .0279 1.6863 .0040 .0000 .0000 .0022 %RSD 741.52 57.51 2465.7 590.4 24.76 .2215 3.766 #1 -.01-047 -.0273 1.6888 .0035 .0002 .0003 -.0587 ##2 -.37835 -.0381 -1.6769 .0024 .0002 .0003 -.0565 #3 .25932 -.0801 .19333 -.0039 .0001 .0003 -.0609 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm - ppm ppm Avge .0001 -.0001 -.0002 -.0014 -.0223 .0383 -.0583 SDev .0002 -.0003 .0004 .0009. .00.62 .0039 .0016 %RSD 242.6 293.3 240.0 63.69 27.81 10.20 2.6-96 #1 -.0000 .0002 -.0007 -.0016 -.0182 .0352 -.0566 .0003 -.0001 .0001 -.0.004 -.0.193 .0427 -.0587 -.0000 -.0004 .0000 -.0021 -:0295 .0370 -.0597 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0002 .0028 .0071 -.0001 .42036 -2.3025 -7.6151 SDev .0001 .0021 .0125 .0008 2.9193 2.1179 2.2431 %RSD 46.73. 76.79 .177.4 1228. 694.48 91.983 29.456 ##1 .0001 .0046 .0152 .0000 2.0270 -2.3713 -6.2733 ##2 .0003 .0032 .0133 .0007 2.1834 -.15102 -10.205 #3 .0003 .0005 -.0074 -.0010 -2.9494 -4.3852 -6.3673 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -7.7257 .62071 -.67101 .0071 -.0007 .0002 .0000 SDev 3.6667 1.6648 1.53252 .0060 .0013 .0000 .0003 %RSD 47.461 268.20 228.39 85.43 183.4 17.34 908.5 -10.171 2.5048 -.11031 .0096 -.0023 .0002 -.0001 2, -3.5097 -.65159 -2.4049 ".0114 .0000 .0003 .0004 #3 -9.4960 .00892 .50220 .0002 .0001 .0002 -.0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 09:55:38 AM =h Low Elem T11908 v Zn Pb2203 , Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.2124 .0004 -.0037 -1.3958 -7.6888 -.24085 SDev 1.5002 .0006 .0001 2.3059 1.7015 1.38471 %RSD 67.810 157.8 2.302 165.21 22:129 574.92 #1 .99783 .0010 -.0037 -.90665 .-8.8732 .76052 #2 1.7499 .0061 -.0036 .62638 -5.7391 -1.8211 #3 3.8894 -.0001 -.0038 L-3.9070 -8.4541 .33797 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 06/20/07 10:03:09 AM page 1 N Dd: CLP1 Sample Name: CRII Operator: MAG Ru,,: Time: 06/20/07 09:55:44 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 19.020 -.0155 17.064 .2052 .0000 .0106 -.0744 SDev .191 .0173 1.452 .0019 .0000 .0001 .0034 %RSD_ 1.0062 111.4 8.5069 .9123 231,.8 .5179 4.596 #1 18.851 .0044 17.971 .2031 .0000 .0105 -.0783 #2 18.979 -.0245 17.831 .2056 .0000 .0.106 -.0730 #3 19.228 -.0264 15.390 .2068 -.0000 .0106 -.0719 Errors LC Pass NOCHECK LC Pass NOCHECK NOCHECK LC Pass NOCHECK High 26.000 26.000 .0130 Low 14.000 14.000 .0070 Elem Cd Co Cr Cu Fe K� Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0101 .0974 .0197 .0454 -.0212 .0400 -.0603 SDev .0002 .0010 .0002 .0004 .0003 .00'65 .0036 %RSD 2.371 1.067 .9392 .8728 1.298 16.19 5.940 #1 .0101 .0963 .0195 .0450 -.0209 .0381 -.0602 .0104 .0974 .0197 .0457 -.0212 .0472 -.0567 .0099 .0983 .0199 .0456 -:0215 .0347 -.0639 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK NOCHECK NOCHECK HiQ_h .0130 .1300 .026.0 .0650 Low .0070 .0700 .0140 .0350 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0298 .0229 .1849 .0808 6.5031 6.8175 112.04 SDev .0001 .0002 .0025 .0011 3.5568 .3352 1.43 0 -.RSD .2591 .8042 1.375 1.376 54.694 4.9171 1.2748 #1 .0298 .0227 .1821 .0820 9.9087 7.2045 110.79 #2 .0299 .0231 .1856 .0801 2.8122 6.6289 111.73 #3 .0298 .0229 .1870 .0801 6.7884 6.6190 113.60 Errors LC Pass LC Pass NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0390 .0260 .1040 Low .0210. .0140 .0560 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb Ppm ppm Ppm ppm Avge 107.32 11.300 8.5650 .1570 .0765 .0524 .1974 1.34 1.942 1.9237 .0026 .0014 .0003 .0043 .SDev %RSD 1.2524 17.185 22.460 1.630 1.773 .6015 2.166 107.87 11.070 7.7170 .1540 .0751 .0520 .2023 105.79 9.4837 7.2109 .1585 .0764 .0525 .1954 #3 108.30 13.347 10.767 .1583 .0778 .0526 .1945 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Analysis Report 06/20/07 10:03:09 AM 1 .1040 Low .0560 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 20.762 .0978 .0407 6.7129 108.89 9.4759 SDev 1.246 .0012 .0004 1.3739 1.15 1.9.119 %RSD 6.0029 1.217 .9246 20.467 1.0554 20.176 #1 19.330 .0964 .0402 8.1052 108.84 8.8337 #2 21.599 .0981 .0409• 5.35.81 107.77 7.9678 #3 21.357 .0987 .0408 6.6756 110.07 11.626 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 30.000 .1300 .0520 9.0000 180.00 13.000 Low 10.000 .0700 .0280 3.0000 60.000 7.0000 page 2 Analysis Report 06/20/07 10:37:22 AM page 1 M A: CLP1 Sample Name: ICSAI Operator: MAG R___ Cime: 06/20/07 10:29:57 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb ppm Ppm ppm ppm Avge .50303 499.7 -.35405 -.0088 .0011 .0004 503.8 SDev .43393 3.3 2.35984 .0006 .0001 .0000 6.8 %RSD 8,6.265 .6656 666.53 7.207 10.44 4.684 1.350 #1 .04634 499.0 .57723 -.0091 .0012 .0004 499.0 #2 _55284 496.8 -3.0374 -.0093 .0010 .0004 500.8 #3 .90990 503.4 1.3980 -.0081 .0012 .0004 511.6 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe 'K Mg Units ppm ppm ppm ppm Ppm Ppm Ppm Avge .0042 .0035 -.0002 -.0085 202.7 .0345 513.7 SDev .0006 .0006 .0006 .0.011 2.0 .0149 5.7 %RSD 13.84 16.95 392.0 12.53 .9849 43.31 1.108 #1 .0037 .0037 .0003 -.0075 201.9 -.0412 509.3 .0029 -.0009 -.0097 201.2 ..0174, ,511.7 .0041 .0048 .0041 .0001 -.0084 205.0 .0449 520.1 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm Ppm ppm ppb Ppb ppb Avge ..0116 -.0039 .0175 .0037 -2.6452 -4.4540 .76027 SDev .0003 .0007 .0011 .0013 2.1016 3.0815 5.6786 %RSD 2.860 19.09 6.482 34.99 79.449 69.185 746.92 #1 .0115 -.0032 .0170 .0046 -4.0501 -7.5817 -.82221 #2 .0114 -.0046 .0167 .0022 -3.6563 -1.4208- 7.0622 #3 .0120 -.0039 .0188 .0044 -.22916, -4.3596 -3.9592 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.1322 -.99093 .96841 .0174 .0141 .0040 .0033 SDev 4.22'56 9.77475 1.5017 .0039 .0029 .0049 .0006 %RSD 373.23 986.42 155.07 22.70 20.15 123.9 18.39 -.78656 -11.115 2.3218 .0161 .0138 -.0017 .0034 -1.7936 -.25062 -.64720 .0142 .0115 .0063 .0026 #3 5.9766 8.3926 1.2307 .0218 .0171 .0074 .0038 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 10:37:22 AM page 2 -y--)�1 Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm Ppb -3.8515 ppb 1.0084 ppb .31596 Avge SDev -.42326 4.15700 .0050 .0005 -.0036 .0004 2.2494 1.7379 2.9725 %RSD 982.13 9.675 11.92 58.403 172.35 940.79 #1 -2.4084 .0048 -.0040 L-6.4055 -.79843 -2.1526 #2 -3.2155 .0056 -.0034 -2.1650 1.1554 -.51514 #3 4..3542 .0047 -.0033 -2.9840 2.6680 3.6156 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 O O C/1 H Analysis Report 06/20/07 10:44:54 AM page 1 N Dd: CLP1 Sample Name: ICSABI Operator: MAG Run Time: 06/20/07 10:37:28 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM Ppb ppm ppm PPM Ppm Avge 1142.0 524.8 1185.2 1.107 .5612 .5358 532.6 SDev 19.5 9.7 13.6 .014 .0108 .0077 8.3 %RSD 1.7113 1.845 1.1462 1.282 1.918 1.430 1.555 #1 1158.7 533.2 1190.9 1.118 .5703 .5419 539.7 #2 1147.0 527.0 1195.0 1.111 .5641 .5383 534.5 #3 1120.5 514.2 1169.7 1.091 .5493 .5272 523.5 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm PPM ppm 213.8 ppm .0506 ppm 537.7 Avge SDev 1.031 .018 .5178 .0064 .5243 .0078 .5965 .0105 4.0 .0070 7.0 %RSD 1.787 1.231 1.495 1.758 1.877 13.79 1.303 #1 1.049 .5224 .5311 H".6041 217.4 .0512 543.0 1.032 .5204 .5261 H.6007 214.5 .0434 540.4 1.012 .5105 .5158 .5845 209.4 .0573 529.8 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm PPM PPM ppm ppb Ppb- Ppb Avge 5341 1.064 .7749 1.034 1225.3 1087.2 -13.288 SDev .0078 015 .0092 .020 13.2 19.4 1.967 %RSD 1.463 1.447 1.181 1.952- 1.0750 1.7865 14.804 #1 .5.406 1.076 .7778 1.054- 1225.9 1104.7 -12.704 #2 .5362 1.069 .7823 1.035 1238.2 1090.4 -15.481 #3 .5254 1.047 .7647 1.013 1211.9 1066.3 -11.679 Errors LC Pass- NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High_ .6000 1.200 Low .4000 .8000 Elem. 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb ppm ppm ppm ppm Avge -10.977 1160.0 1120.9 .3943 1.099 .3330 1.190 SDev 3.143 20.9 24.4 .0083 .012 .0042 .035 %RSD 28.632 1.8014 2.1786 2.104 1.134 1.258 2.964 A -7.4226 1172.4 1142.8 .4015 1.103 .3341 1.229 tt2 -12.118 1171.7 1125.4 .3961 1.109 .3364 1.179 #3 -13.389 1135.9 1094.5 .3852 1.085 .3283 1.161 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 10:44:54 AM page 2 Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1087.7 .5389 1.127 1133.2 -11.746 1.133.9 SDev 20.2 .0081 .015 16.2 2.231 23.0 %RSD 1.8606 1.495 1.363 1.4255 18.995 2.0247 #1 1104.3 .5450 1.139 1145.1 -9.1813 1152.6 #2 1093.7 .5419 1.132 .1139.6 -13.238 1140.8 #3 1065.2 .5298 1.110 1114.8 -12.820 1108.3 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 Analysis Report 06/20/07 10:52:25 AM page 1 MDd: CLP1 Sample Name: CCV1 Operator: MAG R-.. rime: 06/20/07 10:45:00 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb PPM PPM PPM PPM Avge 983.94 47.52 519.29 2.467 2.483 2.455 46.75 SDev 13.63 .78 7.43 .028 .038 .033 .68 %RSD 1.3856 1.636 1.4311 1.127 1.529 1.332 1.451 #1 990.55 47.97 518.32 2.469 2.503 2.466 47.08 #2 993.00 47.98 527.16 2.493 2.507 2.480 47.20 #3 968.26 46.63 512.40 2.437 2.439 2.418 45.97 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm PPM. PPM PPM PPM Avge 2.418 2.423 2.420 2.516 47.36 82.23 50.45 SDev .042 .029 .034 .033 .77 .98 .69 %RSD 1.718 1.207 1.405- 1.297 1.621 1.195 1.364 #1 2.445 2.425 2.435 2.523 47.80 82.57 50.69 2.438 2.451 2.444 2.545 47.81 83.00 50.99 2.370 2.392 2.381 2.481 46.48 81.12 49.67 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.409 2.400 81.42 2.433 560.54 496.51 958.85 SDev .033 .030 - .88 .046 3.93 8.16 7.54 %RSD 1.373 1.265 1.084 1.872 .70080 1.6430 .78648 #1 2.423 2.413 81.57 2.465 557,.03 499..75 956.22 #2 2.434 2.422 82.23 2.453 564.78 502.55 967.35 #3 2.372 2.366 80.48 2.381 559.79 487.23 952.97 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb ppb PPM PPM ppm, PPM Avge 955.44 529.93 510.56 2.531 2.420 2.44 2.703 SDev 10.32- 6.11 4.02 .036 .025 .035 .070 %RSD 1.0797 1.1523 .78692 1.437 1.045 1.395 2.594 947.69 530.75 514.83 2.539 2.410 2.487 2.776 967.15 535.59 509.99 2.563 2.449 2.501 2.698 #3 951.48 523.46 506.85 2.492 2.401 2.435 2.636 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 10:52:25 AM page 2 Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 501.53 2.433 2.495 517.83 956.57 517.01 SDev 9.14 .033 .032 6.00 9.24 4.09 %RSD 1.8222 1.339 1.276 1.1592 .96639 .79061 $#1 508.60 2.445 2.505 518.82 950.53 520.13 ##2 504.78 2.458 2.520 523.28 967.21 518.52 ##3 491.21 2.396 2.459 511.39 951.97 512.38 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 .1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 Analysis Report - 06/20/07 10:59:57 AM N Dd: CLP1 Sample Name: CCVL1 Operator: MAG Rte... Time: 06/20/07 10:52:31 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.05562 .0260 2.5101 .0054 .0008 .0009 SDev .35279 .0423 1.5244 .0019 .0004 .0004 %RSD 634.24 162.4 60.731 35.79 48.12 42.42 #1 .13953 .0736 3.7846 .0076 .0012 .0013 #2 -.46287 .0118 2.9245 .0048 .0006 .0008 ##3 .15647 -.0073 .82136 .0039 .0005 .0006 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0008 .0004 .0007 .0000 2.595 .0564 SDev .0004 .0008 .0004 .0006 .082 .0135 %RSD 54.66 207.4 60.23 2930. 3.172 23.99 ##1 .0013 .0012 -.0011 .0007 2.689 .0720 .0006 .0001 .0003 -.0004 2.537 .0478 .0005 -.0002 .0006 -.0002 2.559 .0494 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb Avge .0006 .0116 2.674 .0005 2.9597 -2.7083 SDev .0003 .0054 .042 .0004 1.1841 .8009 %RSD 52.87 46.73 1.575 76.43 40.008 29.571 ##1 .0010 .0176, 2.723 .0003 1.6981 -2.3463 #2 .0005 .0102 2.646 .0009 3.1339 -2.1523 #3 .0004 .0071 2.655 .0002 4.0470 -3.6262 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb Ppm Ppm Ppm Avge -1.7283 1.8582 -.60311 -.0002 -.0001 .0007 SDev 6.5407 1.5961 2.82157 .0037 .0018 .0004 %R'SD 378.45 85.893 467.84 1556. 2901. 53.15 5.8225 3.6638 1.5207 .0040 .0020 .0011 -5.6464 1.2754 .47466 -.0032 -.0014 .0006 #3 -5.3609 .63546 -3.8047 -.0015 -.0008 .0004 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK page 1 Ca ppm .0096 .0388 405.5 .0532 -.0030 -.0214 NOCHECK Mg ppm .0228 .0416 181.9 .0701 .0063 -.0079 NOCHECK 2068/1 ppb -2.4146 4.7267 195.75 1.9836 -1.8149 7.412.5 NOCHECK Ti ppm .0010 .0006 56.93 .0016 .0007 .0006 NOCHECK knalysis Report 06/20/07 10:59:57 AM page 2 niyil Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM ppb ,ppb Ppb Avge 1.0872 .0012 .0024 -.82077 -1.9568 .21652 SDev 1.4251 .0006 .0005 .37311 5.6919 2.3251 %RSD 131.08 55.10 21.62 45.458 290.88 1073.9 #1 1.02,09 .0017 .0030 -.99942 4.5442 2.2344 #2 2.5442 .0013 .0022 -:39192 -4.3705 .74131 #3 -.30363 .0005 .0020 -1.0710 -6.0441 -2.3261 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Analysis Report 06/20/07 11:07:29 AM page 1 M! Dd: CLP1 Sample Name: CCB1 Operator: MAG Ruii Time: 06/20/07 11:00:03 Comment: Mode: CONC Corr. Factor: 1 Eleni Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm Ppm -.0327 Avge -.38601 -.0203 .33672 1.7712 .0026 .0003 .0001 .0003 .0001 .0151 SDev %RSD .28216 73.097 .0235 115.8 526.03 .0009 36.59 56.66 43.27 46.21, #1 -.17241 .0037 2.0596 .0036 .0004 .0005 -.0171 #2 -.70588 -.0212 -1.4792 .0017 .0002 .0003 -.0337 #3 -.27975 -.0434 .42981 .0024 .0001 .0002 -.0472 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm _ -.0001 ppm -.0008 Ppm -.0071 Ppm .0369 Ppm -.0310 Avge SDev .0003 .0001 .0003 .0003. .0004 .0087 .0012 .0136 %RSD .0000 11.80 438.3 366.7 53.50 121.7 3.142 43.83 #1 .0004 -.0002 -.0002 --.000.9 .0019 .0367 -.0173 .0003 .0002 -.0003 -.0080 .0382 -.0312 .0003 .0003 .0001 -.0003 -.0012 -.0153 .0359 -.0445 'Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Mo Na Ni 2203/1 2203/2 2068/1 Eleni Units Mn ppm ppm ppm ppm ppb -1.2234 Ppb -1.8889 ppb -7.4861 Avge .0002 .0027 .0104 .0004 .0006 .2.1827 2.4591 3.2611 SDev %RSD .0001 49.76 .0009 34.96 .0068 65.01 155.9 178.41 130.19 43.562 #1 .0037 .0173 .0008 -.76703 -3.8753 -4.0233 #2 .0004 .0022 .0101 -.0.003 -3.5982 .86152 -7.9363 #3 .0003 .0001 .0021 .0038 .0006 .69500 -2.6528 -10.499 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm Ppm -.0001 ppm .0003 ppm .0000 Avge -7.2167 -.57253 -1.5.878 2.5387 -.0093 .0009 .0001 .0001 SDev 3.3362 46.228 4.18567 731.09 159.89 .0053 57.32 668.6 44.35 351.1 %RSD -8.6622 -2.2934 .43724 -.0093 .0007 .0004 .0001 -9.5862 -3.6235 -4.4359 -.0039 -.0000 .0002 -.0001 #3 -3.4015 4.1993 -.76465 -.0146 -.0010 .0002 .0000 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 11:07:29 AM page 2 nl.yil Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.6793 .0002 -.0036 -1.6672 -7.3064 -1.2497 SDev 1.4487 .0006 .0002 1.1140 1.6441 2.6150 %RSD 86.266 240.5 6.146 66.816 22.503 209.26 ##1 1.1509 .0006 -.0034 -2.8402 -7.1175 -.47206 $#2 .56899 -.0004 -..0036 -.62353 -9.0368 -4.1653 #3 3.3180 .0005 -.0038 -1.5380 -5.7648 .88834 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.00.00 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 0 �t O O E-� Analysis Report 06/20/07 11:15:00 AM page 1 N Dd: CLP1 Sample Name: MB -21391 Operator: MAG R,,. time: 06/20/07 11:07:35 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb Ppm Ppm ppm Ppm Avge -.28581 -.0481 -1.3288 .0008 -.0000 .0001 -.0667 SDev .53148 .0129 1.9323 .0004 .0001 .0001 .0033 %RSD 185.96 26.89 145.42 46.62 474.3 67.71 5.003 #1 .22934 -.0332 .43455 .0011 .0001 .0002 -.0628 #2 -.83224 -.0560 -3.3945 .0009 -.0001 .0001 -.0685 #3 -.25452 -.0552 -1.0265 .0004 -,0000 .0001 -.0687 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm Ppm Ppm Avge .0002 -.0003 -.0003 -.0009 -.0179 .0317 -.0527 SDev .0002 .0004 .0004 .0004 .0032 .0081 .0063 %RSD 128.7 135.3 140.6 52.09 17.97 25.53 11.95 #1 .0005 -.0001 .0002 -.00,13 -.0142 .0288 -.0455 -.0007 -.0005 -.0009 -.0195 .0254 -.0569 .0000 .0001 -.0000 -.0005 -.0004 -:0201 .0408 -.0558 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.005.0 -.05010 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0001 .0013 .0048 -.0006 1.8226 -.18890 -8.1603 SDev .0001 .0003 .0022 .0007 .5110 .74658 3.4555 %RSD 59.84 19.47 45.61 109.6 28.039 395.23 42.345 #1 .0001 .0010 .0073 -.0000 1.8508 =1.0450 -5.0506 #2 .0000 .0015 .0034 -.0005' 1.2981 .32694 -11.880 #3 .0001 .0013 .0037 -.0014 2.3190 .15136 -7.5500 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb ppm Ppm ppm ppm Avge -8.8315 -.24854 -.78127 -.0082 .0003 -.0000 -.0003 SDev .2391 1.77000 .65671 .0020 .0014 .0001 .0002 %RSD 2.7079 712.17 84.057 24.08 505.7 235.0 62.66 -8.8534 1.7929 -.17091 -.0100 -.0011 .0000 -.0001 -8.5822 -1.1834 -.69675 -.0083 .0017 -.0001 -.0003 _ #3 -9.0590 -1.3551 -1.4761 -.0061 .0002 -.0000 -.0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07. 11:15:00 AM Z Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.2781 .0003 .0011 .48102 -8.6080 -.60387 SDev 2.1090 .0003 .0001 .49898 1.0476 .98451 %RSD 165.01 102.5 5.517 103.73 12.171 163.03 #1 .28332 -.0001 .0012 -.08061 -7.5870 .48304 #2 -.14949 .0005 .0011 .65041 -9.6804 -.85879 #3 3.7004 .0005 .0011 .87326 -8.5564 -1.4358 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 O O E- Analysis Report MI )d: CLP1 Sample Name: LCS-21391 Run Time: 06/20/07 11:15:06 Comment: Mode: CONC Corr. Factor: 1 06/20/07 11:22:37 AM page 1 Operator: MAG Elem Ag Al As1890 B Units ppb ppm Ppb Ppm Avge 966.76 46.40 511.98 2.418 SDev 74.04 3.79 40.67 .177 %RSD 7.6587 8.161 7.9436 7.317 #1 1018.6 49.11 543.72 2.536 #2 999.69 48.03 526.08 2.504 #3 881.96 42.08 466.14 2.215 511.03 NOCHECK NOCHECK NOCHECK NOCHECK Errors High Low Elem Cd Co Cr Cu Units ppm PPM PPM PPM Avge 2.370 2.375 2.370 2.454 SDev .190 .177 .187 .193 %RSD 8.035 7.468 7.911 7.852 #1 2.509 2.490 2.499 2.585 2.448 2.153 Errors NOCHECK High Low Elem Mn Units ppm_ Avge 2.361 SDev .184 %RSD 7.809 #1 2.487 #2 2.446 #3 2.149 Errors NOCHECK High 79.85 Low 561.34 Elem 2068/2 Units ppb Avge 952.92 SDev 62.82 %RSD 6.5928 "1 992.94 ,2 985.32 #3 880.51 Errors NOCHECK 2.465 2.457 2.545 2.171 2.155 2.233 NOCHECK NOCHECK NOCHECK Ba PPM 2.429 .196 8.056 2.569 2.513 2.206 NOCHECK Fe PPM 44.86 3.66 8.165 47.45 46.46 40.67 NOCHECK Be PPM 2.403 .186 7.729 2.529 2.491 2.190 NOCHECK K ppm 80.S8 5.83 7.238 84.68 83.16 .73.91 NOCHECK Ca ppm 45.82 3.54 7.730 48.22 47.48 41.75 NOCHECK Mg PPM 49.18 3.76 7.653 51.71 50.98 44.86 NOCHECK Mo Na Ni 2203/1 2203/2 2068/1 PPM PPM PPM Ppb Ppb Ppb 2.358 79.85 2.386 561.34 497.48 958.32 5.26 .195 33.05 30.73 53.60 .184 7.801 6.592 8.169 5.8875 6.1775 5.5932 2.482 83.33 2.530 580.11 519.10 988.45 2.445 82.41 2.465 580.73 511.03 990.08 2.146 73.79 2.165 523.18 462.30 896.43 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 1960/1 1960/2 Si Sn Sr Ti ppb Ppb PPM PPM PPM PPM 523.99 508.01 2.463 2.388 2.420 2.704 33.72 29.09 .199 .172 .190 .255 6.4358 5.7256 8.082 7.210 7.843 9.413 546.45 530.25 2.599 2.492 2.551 2.916 540.30 518.67 2.556 2.483 2.508 2.775 485.21 475.09 2.234 2.189 2.203 2.422 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 11:22:37 AM page 2 ,h Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 492.87 2.382 2.464 518.74, 954.72 513.33 SDev 36.80 .185 .190 31.43 59.72 30.59 %RSD 7.4669 7.776 7.706 6.0593 6.2549 5.9587 #1 519.92 2.508 2.593 539.41 991.44 535.65 #2 507.73 2.470 2.553 534.24 986.91 525.88 #3 450.96 2.170 2.246 482.57 885.82 478.46 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low 00 0 O H knalysis Report 06/20/07 11:30:37 AM .14 )d: CLP1 Sample Name: 0706952-001D Operator: MAG 2__- rime: 06/20/07 11:23:12 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm Ppb PPM PPM PPM Avge -.21909 -.0107 1.6608 .0574 .0233 .0006 SDev .56537 .0129 1.0843 .0012 .0003 .0003 %RSD 258.05 121.0 65.289 2.031 1.278 40.74 #1_ .37656 .0037 2.5610 .0583 .0235 .0009 ##2 -.28553 -.0143 .45706 .0579 .0234 .0006 #3 -.74831 -.0215 1.9644 .0561 .0230 .0004 Elem Cd Co Cr Cu Fe K Units ppm ppm PPM PPM PPM PPM Avge .0011 .0129 .0015 .0014 .1230 4.519 SDev .0005 .0007 .0006. .0003 .0053 _ .005 %RSD 47.39 5.521 37.65 20.88 4.284 .1053 ##1 .0016 .0136 .0021 .0011 .1284 4.515 ##2 .0009 .0129 .0013 :.0016 .1225 4.524 ##3 .0006 .0122 .0010 .0016 .1179 4.518 Elem Mn Mo Na Ni 2203/1 2203/2 is ppm ppm PPM PPM Ppb ppb e 4.579 .0092 15.59 .0130 .66446 -.56642 5uev .022 .0030 .18 .0016 1.3210 .52160 %RSD .4828 32.00 1.177 12.31 198.81 92.088 #1 4.555 .0125 15.38 .0139 1.4467 -.36107 #2 4.598 .0086 15.65 .0139 -.86076 -.17874 #3 4.585 .0066 15.74 .0111 1.4074 -1.1594 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb Ppb PPM PPM PPM Avge -4.8149 1.8240 -.28108 6.080 -.0003 .1539 SDev 1.6759 3.8296 1.76870 .040 .0008 .0011 %RSD 34.805 209.95 629.24 .6631 236.6 .7078 #1 -3.7832 3.2830 -1.0807 6.034 -.0004 .1526 #2 -6.7486 4.7097 1.7462 6.110 .0005 .1547 #3 -3.9131 -2.5206 -1.5088 6.095 -.0011 .1543 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .92654 .0010 .0058 -.15645 -4.7515 .41991 SDev 1.1824 .0005 .0004 .34791 1.4904 2.2898 %RSD 127.61 52.42 7.663 222.37 31.367 545.29 #1 .90143 .0015 .0062 .24100 -3.2363 .37239 42 -.24311 .0010 .0058 -.40577 -6.2158 2.7331 2.1213 .0005 .0053 -.30459 -4.8023 -1.8457 page 1 Ca PPM 39.53 .20 .5139 39.31 39.71 39.57 Mg PPM 17.32 .11 .6241 17.20 17.40 17.37 2068/1 ppb -4.6244 2.2671 49.024 -2.1412 -5.1486 -6.5835 Ti PPM .0014 .0004 29.51 .0018 .0013 .0010 Analysis Report 06/20/07 11:38:09 AM page 1 d: CLP1 Sample Name: 0706952-002D Operator: MAG R Time: 06/20/07 11:30:43 Comment : ' Lk) Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.23665 -.0141 1.7925 .1623 .1356 .0001 56.49 SDev .16814 .0085 1.7450 .0007 .0005 .0001 .07 %RSD 71.052 60.44 97.352 .4134 .3854 67.86 .1298 #1 -.43042 -.0057 2.2786 .1619 .1362 .0002 56.46 #2 -.15044 -.0138 3.2429 .1631 .1354 .0001 56.57 #3 -.12910 -.0227 -.14404 .1619 .1353 .0001 56.43 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0005 .0024 .0026 .0047 .0944 48.23 20.17 SDev .0003 .0003 .0002 0004 .0015 .09 .02 %RSD 69.92 .11.51 .8.162 9.302 1.581 .1878 .1087 #1 .0008 .0027 .0028 .0044 .0957 48.34 20.15 #2 .0004 .0022 .0026 .0052 .0949 48.17 20.19 #3 .0002 .0023 .0024 .0045 .0928 48.19 20.18 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 ppm ppm ppm ppm ppb ppb ppb lts e 10.13 .0024 25.00 .0124 1.7830 -2.3830 -8.6667 ev .01 .0011 .12 .0008 1.1316 1.7118 2.0802 %RSD .0960 47.68 .4856 6.731 63.465 71.833 24.002 #1 10.13 .0035 24.86 .0130 1.0895 -2.6371 -10.731 #2 10.14 .0023 25.03 .0114 3.0888 -.55840 -6.5709 #3 10.12 .0012 25.10 .0126 1.1707 -3.9536 -8.6983 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -9.9387 -.18150 .27155 4.698 -.0019 .1952 .0010 SDev 1.4S56 3.16550 1.2231 .007 .0019 .0004 .0001 %RSD 14.645 1744.1 450.40 .1409 98.55 .2245 13.26 #1 -8.4977 .25761 -.90732 4.701 -.0036 .1947 .0011 #2 -9.9100 -3.5436 1.5345 4.702 -.0023 .1953 .0009 #3 -11.408 2.7415 .18746 4.690 .0001 .1956 .0010 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.8930 .0003 .0170 -.99566 -9.5151 .12071 SDev 2.3531 .0002 .0001 1.49251 .8862 .81485 %RSD 124.31 59.22 .9035 149.90 9.3138 675.02 #1 -.17437 .0003 .0170 -1.3961 -9.2413 -.51935 #2 4.4537 .0005 .0171 .65622 -8.7980 -.15650 0 1.3997 .0001 .0168 -2.2471 _10.506 1.0380 Analysis Report 06/20/07 11:45:40 AM P od: CLP1 Sample Name: 0706952-003D Operator: MAG F_-__ Time: 06/20/07 11:38:15 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .07033 .0242. 1.3009 .7996 .2638 .0001 SDev .09453 .0058 .9123 .0203 .0064 .0000 %RSD 134.41 24.06 70.125 2.539 2.427 45.55 #1 .10151 .0281 2.3260 .7802 .2583 .0001 ##2 .14532 .0175 .99825 .7980 .2623 .0001 #3 -.03585 .0271 .57843 .8207 .2709 .0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 .0200 .0030 .0084 .6797 67.48 SDev .0001 .0009 .0008 ..0013 .0166 1.54 %RSD 71.15 4.722 27.76 15.35 2.440 2.281 ##1 .0000 .0190 .0020 .0069 .6645 66.18 #2 .0001 .0200 .0034 .0088 .6771 67.09 #3 .0002 .0209 .0035 .0094 .6974 69.18 Elem Mn Mo Na Ni 2203/1 2203/2 -- '. t s ppm ppm ppm ppm ppb ppb le 2.919 .0027 256.2 .0520 1.4969. .57885 Lev .0.68 .0003 5.5 .0019 .2041 .54285 %RSD 2.321 11.14 2.166 3._567 13.632 93.780 #1 2.859 .0025 251.2 .0502 1.3340 1.1110 #2 2.907 .0031 255.2 .0519 1.4309 .02593 #3 2.992 .0026 262.2 .0539 1.7258 .59960 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge -10.064 1.5059 -1.8006 10.53 -.0017 .8150 SDev 1.707 1.0772 .4217 .27 .0015 .0228 %RSD 16.959 71.535 23.422 2.559 91.91 .2.803 #1 -8.1299 2.5918 -1.7023 10.29 -.0030 .7944 #2 -10.703 .43760 -2.2628 10.49 -.0000 .8110 #3 -11.359 1.4882 -1.4367 10.82 -.0019 .8395 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.20418 .0007 .0086 .88466 -9.3483 -.69954 SDev .00326 .0005 .0003 ..35443 1.6602 .58289 %RSD 1.5959 71.10 3.318 40.065 17.759 83.324 #1 -.20377 .0005 .0084 1.1854 -7.4384 -.27234 #2 -.20762 .0012 .0086 .49388 -10.160 -1.3636 -.20114 .0003 .0089 .97472 -10.446 -.46272 page 1 Ca PPM 181.7 4.5 2.460 177.7 181.0 186.5 Mg PPM 79.75 1.98 2.486 77.90 79.51 81.85 2068/1 ppb -7.9149 1.6282 20.572 -6.0533 -9.0737 -8.6176 Ti PPM .0059 .0003 4.780 .0056 .0061 .0061 Analysis Report 06/20/07 11:53:12 AM page 1 M' )d: CLP1 Sample Name: 0706952-004D Operator: MAG Run rime: 06/20/07 11:45:46 Comment: R -W - J' Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb Ppm PPM Ppm Ppm Avge -.11296 -.0052 .10208 .5405 .1443 .0003 99.05 SDev .0159 1.0915 .0127 .0038 .0001 2.07 %RSD .55042 487.28 306.7 1069.2 2.348 2.659 18.48 2.093 #1 .12361 .0122 1.3491 .5410 .1459 .0003 99.35 #2 -.74212 -.0087 -.36355 .5530 .1471 .0003 101.0 $3 .27963 -.0191 -.67936 .5276 .1399 .0002 96.85 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM PPM 121.1 PPM 58.06 Avge SDev .0001 .0227 .0006 .0026 .0002 .0150 .0009 .0934 .0031 3.2 1.28 %RSD .0001 99.48 2.781 8.253 6.154 3.270 2.611 2.198 #1 -.0000 .0223 .0024 .0147 .0946 122.6 58.25 #2 .0002 .0234 .0027 .0160 .0956 123.2 59.23 $3 .0001 .0223 .0028 .0143 .0899 117.4 56.70 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 is ppm PPM PPM 245.3 PPM ppb Ppb Ppb -10.194 [e SDev 11.81 .0012 .0005 5.1 .0516 .0016 1.7826 199986 3.852 0 -.RSD .26 2.189 46.72 2.094 3.098 35.586 120.88 37.789 ##1 11.87 .0015 246.4 .0533 4.4099 .29475 -7.5447 #2 12.04 .0015 249.8 .0515 7.0140 .30436 -14.613 ##3 11.53 .0005 239.7 .0501 3.6033 2.3755 -8.4241 Elem 2068/2 1.960/1 1960/2 Si -Sn' Sr Ti Units ppb Ppb ppb PPM PPM PPM PPM Avge -8.1122 1.6381 -3.2456 6.435 -.0014 .6245 .0011 SDev 2.0006 2.2012 .8023 .158 .0014 .0140 2:242 .0001 4.950 %RSD 24.661 134.38 24.719 2.463 101.1 ##1 -10.192 -.66232 -2.3212 6.473 -.0020 .6258. .0012 #2 -6.2014 3.7246 -3.6555 6.570 .0002 .6378 .0012 43 -7.9433 1.8521 -3.7601 6.261 -.0024 .6099 .0011 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb Ppb Avge 2.1982 .0003 .0101 2.3295 -8.8054 -1.6193 SDev 2.3213 .0004 .0003 .5883 .6271 .3700 %RSD 105.60 111.8 3.419 25.253 7.1220 22.852 #1 -.29041 .0001 .0101 1.6652 -9.3103 -1.7688 un 4.3048 .0001 .0105 2.5388 -9.0024 -1.1979 2.5801 .0008 .0098 2.7844 -8.1034 -1.8912 N 00 0 O Ci E- knalysis Report 06/20/07 12:08:15 PM q .)d: CLP1 Sample Name: 0706952-004DMS Operator: MAG :Z,". "ime: 06/20/07 12:00:50 2omment : ► 4 - rJ, i�AS Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge 50.396 2.154 46.977 .5738 2.313 .0534 SDev .672 .036 1.689 .0022 .015 .0001 0 -.RSD 1.3343 1.678 3.5945 .3801 .6477 .1394 #1 51.159 2.195 45.331 .5713 2.328 .0533 #2 50.138 2.139 46.896 .5755 2.311 .0534 #3 49.890 2.128 48.705 .5744 2.299 .0534 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0525 .5498 .2131 .2985 1.121 127.4 SDev .0008 .0052 .0000 .000 .3 %RSD 1.6.15 .9383 .0174 _.0022 7382 .0437 .2012 #1 .0534 .5441 .2131 .2961 1.122 127.6 #2 .0523 .5511 .2131 .2991 1.121 127.1 #3 .0517 .5542 .2132 .3003 1.121 127.5 Elem Mn Mo Na Ni 2203/1 2203/2 is ppm ppm PPM PPM Ppb Ppb e 12.94 -.0009 259.0 .5839 27.304 21.249 SDev .01 .0002 .4 .0064 1.603 .211 %RSD .0848 19.10 .1443 1.089 5.8726 .99064 #1 12.94 -.0008 258.6 .5905 26.832 21.389 .#2 12.93 -.0011 259.2 .5833 25.990 21..352 #3 12.95 -.0008 259.3 .5779 29.091 21.007 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm 547.28 14.903 7.2814 6.790 -.0031 .6563 .Avge SDev 1.18 5.166 2.1902 .009 .0013 .0011 %RSD .21609 34.666 30.079 .1253 40.73 .1707 #1 546.88 12.452 5.1384 6.786 -.0017 .6559 #2 546.35 11.418 9.5158 6.785 -.0042 .6576 ##3 548.61 20.838 7.1899 6.800 -.0033 .6555 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb Ppb Avge 54.819 .5282 .5712 23.266 547.30 9.8193 SDev 1.866 .0020 .0020 .405 1.39 2.1000 %RSD 3.4032 .3865 .3498 1.7413 .25457 21.387 #1 53.636 .5259 .5691 23.202 546.98 7.5739 ##2 53.851 .5287 .5712 22.897 546.10 10.149 56.970 .5299 .5731 23.699 548.83 11.735 page 1 Ca PPM 104.6 .2 .1963 104.4 104.4 104.8 Mg PPM 61.37 .24 .3942 61.12 61.40 61.60 2068/1 ppb 547.34 1.84 .33627 547.18 545.59 549.26 Ti PPM .0016 .0002 13.44 .0014 .0015 .0018 Analysis Report 06/20/07 12:15:47 PM 'od: CLP1 Sample Name: 0706952-004DSD Operator: MAG Time: 06/20/07 12:08:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.22782 -.0522 .17153 .1142 .0304 .0001 SDev 1.03089 .0173 3..2252 .0045 .0017 .0000 %RSD 452.50 33.13 1880.2 3.905 5.555 22.51 #1 -.63531 -.0344 -2.3460 .1187 .0322 .0001 #2 .94453 -.0532 -.94625 .1142 .0303 .0001 #3 -.99269 -.0690 3.8069 .1098 .0288 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm PPM PPM Ppm Ppm Avge -.0002 .0045 .0010 .0045 .0034 21.16 SDev .0002 .0005 .0003. .0007.' .0018 .67 %RSD 106.3 11.23 30.40 15.09 52.67 3.164 #1 -.0001 .0045 _0009 .0048 .0046- 21.87 #2' -.0000 .0051 .0014 .0049 .0041 21.07 #3 -.0003 .0041 .0008 .0037 .-0013 20..54 Elem Mn Mo Na Ni 2203/1 2203/2 Lts ppm PPM PPM PPM Ppb Ppb 4e 2.534 .0002 50.07 .0112 .52056 -.68585 5llev .095 .0003 1.47 .0011 3.4339 .26958 %RSD 3.736 163.8 2.926 9.567 659.66 39.306 #1 2.629 .0000 51.50 .0113 4.4850 -.93439 #2 2,534 .0005 50.14 .0122 -1.5256 -.39927 #3 2.440. -.0000 48.5.8 .0101 -1.39.78 -.72387 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm. Avge -7.4425 -1.7262 .73554 1.335 -.0006 .1269 SDev 2.8426 2.0398 .78971 .054 .0006 .0045 %RSD 38.194 118.16 107.37 4.018 106.5 3.579 #1 -6.2554 -.65897 1.5347 1.389 -.0011 .1314 #2 -10.686 -4.0782 -.04440 1.335 .0001 .1268 #3 -5.3858 -.44150 .71633 1.282 -.0007 .1223 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.36393 .0006 .0027 -.28403 -7.4646 -.08423 SDev 1.32532 .0007 .0004 1.00350 1.9392 1.15336 %RSD 364.17 112.5 13.64 353.31 25.979 1369.3 #1 1.0709 .0001 .0030 .87035 -7.8689 .80420 #2 -1.5422 .0014 .0027 -.77424 -9.1698 -1.3877 -.62052 .0003 .0023 -.94820 -5.3551 .33078 page 1 Ca ppm 20.69 .76 3.691 21.44 20.72 19.92 Mg ppm 12.02 .44 3.650 12.46 12.03, 11.58 2068/1 ppb -7.5089 3.1388 41.801 -11.101 -6.1325 -5.2934 Ti ppm .0002 .0001 21.04 .0002 .0003 .0002 W) 00 0 0 DO H ' Analysis Report 06/20/07 12:23:19 PM page 1 MI, >d: CLP1 Sample Name: 0706952-005D Operator: MAG Run Time: 06/20/07 12.:15:53 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM ppb PPM PPM PPM PPM 16.79 Avge -.36244 .0198 -1.1274 2.2277 .0345 .0878 .0009 .0001 .0000 .30 SDev %RSD .41857 115.49 .0070 35.30 197.60 .0011 3.071 1.057 7.513 1.769 #1, -.20472 .0252 -3.6063 .0337 .0867 .0001 16.46 #2 -.83695 .0119 -.48257 .0342 .0883 .0000 16.87 #3 -.04563 .0225 .70680 .0357 .0884 .0000 17.03 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM PPM 6.242 PPM 12.42 Avge SDev .0004 .003-8 .0001 .0104 .0003 .0063 .2306 .0043 .060 .20 %RSD .0001 40.30 2.945 2,.606 _.0009 14.41 1.866 .9558 1.599 #1 .0005 .0039 .0101 .0053 -.2263 6.176 12.20 #2 .0002 .0038 .0105 .0068 .2307 6.291 12.49 43 .0003 .0037 .0107 .0069 .2349 6.259 12.57 wl "mMn Mo Na Ni 2203/1 2203/2 2068/1 its Ppm PPM PPM 16.10 PPM ppb 1.3164 ppb 1.3100 ppb -8.4364 ge SDev 2.539 .0007 -0006 .25 .0149 .0005 1.8234 1.6962 1.7992 %RSD .041 1.602 81.49 1.571 3.587 138.51 129.48 21.326 #1 2.493 .0002 15.80 .0143 1.5614 -.44524 -6.7296 #2 2.552 .0007 16.26 .0153 -.61712 2.9403 -8.2640 #3 2.571 .0014 16.23 .0151 3.0049 1.4350 -10.315 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb PPM PPM PPM PPM Avge -8.5526 1.5684 -2.3159 7.046 -.0020 .1030 .0023 SDev 2.7603 .1024 .8510 .115 .0023 .0017 .0002 10.62 %RSD 32.274 6.5301 36.748 1.638 115.0 1.638. #1 -9.2152 1.5200 -1.7358 6.915 -.0046 .1010 .0021 #2 -10.921 1.6861 -1.9190 7.091 -.0003 .1038 .0025 #3 -5.5213 1.4993 -3.2928 7.132 -.0011 .1041 .0023 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM ppb ppb ppb Avge 2.8413 .0008 .0167 1.3122 -8.5139 -1.0224 SDev 1.2250 .0003 .0003 .9486 1.4634 .5852 %RSD 43.114 34.00 1.677 72.292 17.188 57.243 #1 4.2485 .001.0 .0164 .22307 -8.3874 -.65162 "2 2.2617 .0008 .0168 1.7558 -10.036 -.71849 3 2.0136 .0005 .0170 1.9579 -7.1178 -1.6971 Analysis Report 06/20/07 12:30:50 PM page 1 N od: CLP1 Sample Name: CCV2 Operator: MAG Run Time: 06/20/07 12:23:25 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 975.35 46.99 516.95 2.466 2.458 2.460 46.83 SDev 1.29 .09 4.85 .009 .003 010 .18 %RSD .13194 .2002 .93730 .3585 .1416 .3894 .3799 #1 975.85 47.09 511.77 2.456 2.462 2.450 46.64 #2 973.89 46.91 517.71 2.470 2.455 2.462 46.83 #3 976.31 46.96 521.37 2.472 2.457 2.469 47.00 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.403 2.445 2.417 2.505 46.97 81.87 50.24 SDev .004 .015 .007 .002 .06 .24 .15 %RSD .1603 .6294 .2726 .0900 .1364 .2881 .2959 #1 2.405 2.428 2.411 2.503 46.91 82.13 50.08 2.398 2.447 2.417 2.506 46.96 81.67 50.25 2.405 2.459 2.424 2.507 41.04 81.83 50.-38 Errors_ LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.408 2.379 80.98 2.409 573.81 494.39 963.15 SDev .007 .007 .05 .006 4.59 4.29 13.63 %RSD .2798 .3147 .0623 .2428 .80006 .86791 1.4156 #1 2.402 2.371 81.03 2.412 569.43 489.72 947.53 #2 2.409 2.378 80.93 2.403 573.42 495.27 969.26 #3 2.415 2.386 80.97 2.414 578.59 498.17 972.66 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 960.57 533.62 509.76 2.528 2.467 2.461 2.790 SDev 8.69 2.68 4.18 .010 .019 .003 .040 %RSD .90487 .50229 .81904 .3902 .7618 .1408 1.424 955.24 530.86 506.11 2.520 2.445 2.458 2.836 n- 955.87 536.21 508.86 2.525 2.473 2.461 2.763 #3 970.60 533.79 514.32 2.539 2.481 2.465 2.772 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK r- 00 0 0 Cn F- %nalysis Report 06/20/07 12:30:50 PM page 2 high Low Elem T11508 v Zn Pb2203 Sb2068 Se1960 Units ppb Ppm PPM Ppb ppb ppb Avge 493.26 2.433 2.495 520.84 961.43 517.71 SDev 1.55 .007 .007 4.36 9.36 3.23 %RSD .31342 .2972 .2633 .83681 .97318 .62404 #1 495.03 2.426 2.488 516.27 952.67 514.35 #2 492.53 2.434 2.497 521.30 960.33 517.97 #3 492.21 2.440 2.501 524.95 971.29 520.80 Errors LC Pass LC Pass LC Pass LC Pass LCPass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 00 00 O O H Analysis Report D� od: CLP1 Sample Name: CCVL2 Run Time: 06/20/07 12:50:56 Comment: Mode: CONC Corr. Factor: 1 Elem Ag, Al As1890 Units ppb ppm ppb Avge -.28650 -.0352 -3.5012 SDev .47336 .0134 .8027. %RSD 165.22 38.03 22.927 #1 -.15189 -.0198 -3.6463 ##2 -.81258 -.0427 -4.2214 $#3 .10499 -.0432 -2.6358 Errors NOCHECK NOCHECK NOCHECK High Low Elem Cd - Co Cr Units ppm ppm ppm Avge -.0001 -.0000 -.0000 SDev .0003 .0002 .0004 %RSD 222.8 2068. 1537. #1 -.0005 -.0002 -.0005 -.0000 .0001 .0001 .0001 .0001 .0003 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn - Mo ppm 00. .0002 .030 1&.62 NOCHECK ppb Na ppm 2.505 1.184 .0011 2.471 .0011 2.524 .0014 2.521 ppb LC Pass 1960/1 1960/2 2.0209 -2.3964 1.1.587 2.6362 57.337 110.01 3.3312 -.44188 1.1311 -5.3946 -1.3526 Errors NOCHECK NOCHECK NOCHECK 06/20/07 12:58:21 PM page 1 Operator: MAG B ppm .0007 .0003 42.07 .0003 .0008 .0008 NOCHECK Cu ppm -.0031 .0006 20.01. -.0038 -.0027 -.0027 NOCHECK Ni ppm -.0004 0006 138.1 0000 -.0011 -.0002 NOCHECK Ba ppm .0001 ..0000 59.64 .0000 .000.1 .0001 NOCHECK Fe ppm 2.460 .010 .41b9 2.450 2.470 2.460 LC Pass 2.750 2.250 22.03/1 ppb -.62655 2.15355 343.71 1.3163 -.25382 -2.9421 NOCHECK Be ppm .0004 .00'00 8.153 .0004 .0004 .0004 NOCHECK K ppm .0439 .0126 28.59 .0296 .0530 .0491 NOCHECK 2203/2 ppb -.38189 .15982 41.849 -.36186 -.23303 -:55078 NOCHECK Ca ppm -.0701 .0039 5.498 -.0745 -.0681 -.0676 NOCHECK Mg ppm -.0588 .0040 6.876 -.0625 -.0545 -.0596 NOCHECK 2068/1 ppb -10.076 2.009 19.942 -9.4242 -12.330 -8.4736 NOCHECK Si Sn Sr Ti ppm ppm ppm ppm -.0081 .0002 .0001 -.0001 ..0032 .0010 .0001 .0001 39.43 543.9 100.2 70.59 -.0114 .0003 -.0000 -.0002 -.0080 -.0008 .0001 -.0001 -.0050 .0011 .000.1 -.0001 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report =a Low 06/20/07 12:58:21 PM page 2 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.7489 .0006 -.0024 -.46332 -9.3124 -.92540 SDev 2.0331 .0003 .0001 .79591 .9063 2.07471 %RSD 116.25 45.76 2.610 171.78 9.7325 224.20 #1 4.0875 .0003 -.0023 .19701 -8.5435 .81455 #2 .40117 .0008 -.0024 -.23991 -9.0819 -3.2215 #3 .75819 .0006 -.0023 -1.3471 -10.312 -.36925 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Analysis Report 06/20/07 01:05:51 PM page 1 N od: CLPl Sample Name: CCB2 Operator: MAG Ru„ Time: 06/20/07 12:58:27 Comment: Mode: CONC Corr. Factor: 1 Elem * Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb ppm Ppm ppm ppm Avge -.06768 -.0342 -2.8117 .0013 .0000 .0004 -.0610 SDev. .51386 .0146 1.5919 .0004 .0000 .0000 .0038 %RSD 759.21 42.73 56.619 29.55 411.1 7.722 6.257 #1 -.23597 -.0176 -3.4399 .0009 -.0000 .0004 -.0654 #2 .50922 -.0398 -3.9936 .0016 .0001 .0004 -.0588 #3 -.47629 -.0451 -1.0015 .0014 -.0000 .0003 -.0588 Errors LC Pass LC Pass LC Pass LC Pass LC Passe LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units_ ppm ppm ppm ppm ppm ppm ppm Avge -.0001 -.0000 .0001 -.0029 -.0213 .0452 -.0588 SDev .0001 1.0003 .0001 .0004 .0006 .0091 .0007 %RSD 78.96. 741.9 158.7 14.25 2.770 20.03 1.135 #1 -.0000 .0002 -.0000 -.0034 -.0213 .0362 -.0590 -.0002 -.0004 .0001 -.0027 -.0207 .0543 -.0593 -.0001 .0001 .0001 -.0026 -.0219 .0451 -.0580 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000- 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb' ppb ppb Avge .0001 .0010 .0204 -.0001 -1.2148 -.29306 -9.1419 SDev .0001 .0008 .0015 .0008 1.4276 2.36.368 2.8682 %RSD 142.3 82.08 7.169 1390. 117.51 806.55 31.374 #1 -.0000 .0019 .0213 .0008 .42740 .41976 --11.677 #2 .0001 .0009 .0212 -.0002 -1.9125 1.6322 -6.0285 #3 .0001 .01003 .0187 -.0007 -2.1594 -2.9311 -9.7207 Errors LC Pass NOCHECK 'LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400. Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb ppb ppm ppm ppm ppm Avge -8.4228 1.7886 -2.7118 -.0105 -.0020 .0001 -.0003 SDev .5505 2.3328 3.0271 .0025 .0015 .0000 .0001 %RSD 6.5362 130.42 111.63 23.65 76.74 23.48 26.63 -8.3180 4.4783 -4.5151 -.0131 -.0017 .0001 -.0003 -9.0182 .3.1604 -4.4032 -.0081 -.0006 .0001 -.0003 #3 -7.9322 .57156 .78300 -.0105 -.0036 .0001 -.0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis'Report 06/20/07 01:05:51 PM Low Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.3464 .0003 -.0041 -.59997 -8.6622 -1.2131 SDev 3.5391- .0008 .0001 1.79632 .7164 1.7920 %RSD 150.83 257.6 1.647 299.40 8.2709 147.72 #1 5.7809 -.0001 -.0040 .42235 -9.4364 -1.5203 #2 2.5471 .0012 -.0040 .45185 -8.0226 -2.8317 #3 -1.2888 -.0002 -.0042 -246741 -8.5278 .71259 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.0.00 5.0000 Low -10.000 -.0500 -.02.00 -3.0000 -60.000 -5.0000 page 2 knalysis Report 06/20/07 01:13:22 PM page 1 ala �d: CLP1 Sample Name: 0706952-006D Operator: MAG Zun Time: 06/20/07 13:05:57 omment : ' W -(O" lode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.64232 -.0601 -1.8441 .0522 .0237 .0001 41.41 SDev .26831 .0467 1.1534 .0050 .0001 .0000 .12 %RSD 41.772 77.64 62.549 9.520 .2604 11.56 .2916 #1 -.39561 -.0224 -1.5043 .0552 .0238 .0001 41.52 #2 -.60338 -.0457 -.89870 .0549 .0236 .0001 41.28 #3 -.92797 -.1123 -3.1292 .0465 .0237 .0002 41.43 Elem. Cd Co Cr Cu Fe K Mg Units ppm ppm PPM PPM PPM PPM PPM Avge .0002 .0123 .0003 .0009 .'1139 4.580 18.05 SDev .0005 .0005 .0010 .0016 .0074 .034 .03 %RSD 234.7 4.220 362.1 170.9 6.514 .7425 .1840 #1 -.0003 .0120 -.0007 -.0006 .1192 4.545 18.03 #2 .0003 .0120 .0002 .0009 .1170 4.583 18.03 #3. .0006 .0129 .0013 .0025 .1054 4.6.12 18.09 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 is ppm PPM PPM PPM Ppb Ppb Ppb e 4.760 -.0013 16.06 .0124 -1.8347 -.69722 -11.060 SDev .011 .0024 .22 .0010 2.0156 .91419 2.353 %RSD .2322 184..7 1.350 8.502 109.86. 131.12 21.276 #1 4.770 -.0005 15.82 -.0112 -4.1601 .21878 -8.6304 #2 4.749 .0006 16.14 .0129 -.75724 -.70085 -11.221 #3 4.762 -.0039 16.23 .0131 -.58687 -1.6096 -13.328 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm PPM ppm ppm Avge -7.5273 -.03476 -4.4198 6.314 -.0028 .1623 .0005 SDev 4.6320 5.43559 1.8861 .007 .0020 .0001 .0004 %RSD 61.536 15638. 42.674 .1156 70.37 .0953 95.32 #1 -11.232 -6.1132 -6.5283 6.317 -.0051 .1621 -.0000 #2 -2.3340 1.6497 -2.8932 6.306 -.0020 .1624 .0006 #3 -9.0159 4.3592 -3.8378 6.320 -.0014 .1623 .0008 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm Ppm ppb ppb ppb Avge -.13181 .0003 .0085 -1.0759 -8.7036 -2.9595 SDev 4.29280 .0002 .0002 .3090 2.9537 2.9740 %RSD 32.56.8 58.96 2.231 28.719 33.937 100.49 #1 -4.0105 .0003 .0083 -1.2393 -10.366 -6.3900 u^ 4.4806 .0001 .0086 -.71955 -5.2933 -1.3804 -.86551 .0005 .0087 -1.2689 -10.452 -1.1082 page 1 Ca ppm 14.41 .02 .1094 14.42 14.41 14.39 Mg ppm 3.730 .002 .0632 3.728 3.733 3.730 2068/1 ppb -9.4610 1.3910 14.703 -9.0009 -8.3584 -11.024 Ti ppm .0033 .0002 4.781 .0035 .0032 .0032 06/20/07 01:20:53 PM analysis Report A( d: CLP1 Sample Name: 0706952-007D Operator: MAG Run Time: 06/20/07 13:13:28 Comment: Rw .- (a Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb Ppm ppb ppm PPM ..0395 ppm .0001 Avge SDev -.56551 .0062 .0151 .38859 .80318 .0797 .0002 .0002 .0000 %RSD .23471 41.504 244.3 206.69 .2270 .5692 18.99 #1 -.46766 .0235 -.0373.3 .0797 .0397 .0001 #2 -.39556 -.0010 -.11192 .0795 .0395 .0001 #3 -.83331 -.0040 1.3150 .0799 .0393 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm PPM PPM .1526 PPM 6.556 Avge SDev -.0000 .0030 -.0001 .0028 .0001 .0096 .0002 .0007 .016 %RSD .0002 1020. 2..328 4.884 2.267 .4541 .2511 #1 .0002 .0030 .0029 .0094 .1534 6.559 #2 -.0002 .0031 .0027 .0096 .1520 6.570 #3 -.000.2 .0030 .0029 .0098 .1526 6.538 L''Qm Mn Mo Na Ni 2203/1 2203/2 its ppm PPM PPM 4.607 PPM .0091 Ppb -1.4385 Ppb -.52887 _ge SDev 1.330 .0007 .0004 .045 .0006 3.5686 .46322 %RSD .003 .2173 50.61 .9715 6.732 248.07 87.586 #1 1.332 .0006 4.558 .0089 -.92166 .00037 #2 1.330 .0012 4.646 .0098 -5.2374 -.86056 ##3 1.326 .0005 4.616 .0086 1.8435 -.72644 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb Ppb -2.1954 Ppb -.38820 PPM 5.310 PPM -.0007 PPM .0430 Avge SDev -10.773 1.395 2.1872 2.33480 .013 .0001 .0001 %RSD 12.946 99.628 601.44 .2402 19.81 .2013 #1 -12.140 -4.0637 -2.8252 5.308 -.000.8 .0430 #2 -10.827 -.2.7329 1.8289 5.323 -.0009 .0431 #3 -9.3523 :21049 -.16829 5.298 -.0006 .0429 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM Ppb -.83171 Ppb -10.336 ppb -.98999 Avge 1.2020 2.1545 .0005 .0127 .0002 1.30546 .659 1.95443 SDev %RSD 179.24 .0000 .3181 1.450 156.96 6.3723 197.42 #1 3.2746 .0005 .0129 -.30659 -11.095 -3.2376 '2 1.3575 .0005 .0125 -2.3180 -10.005 .30978 3 -1.0260 .0005 .0127 .12942 -9.9089 -.04215 page 1 Ca ppm 14.41 .02 .1094 14.42 14.41 14.39 Mg ppm 3.730 .002 .0632 3.728 3.733 3.730 2068/1 ppb -9.4610 1.3910 14.703 -9.0009 -8.3584 -11.024 Ti ppm .0033 .0002 4.781 .0035 .0032 .0032 Analysis Report 06/20/07 01:28:24 PM P "od: CLP1 Sample Name: 0706952-008D Operator: MAG Rug. Time: 06/20/07 13:20:59 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb Ppm PPM PPM Avge -.30557 -.0589 2.1151 .4574 .083.3 .0000 SDev .14308 .0066 .5137 .0018 .0006 .0000 %RSD 46.824 11.24 24.289 .3919 .7747 49.03 ##1 -.46596 -.0514 1.8703 .4592 .0840 .0001 #2 -.25969 -.0613 1.7696 .4576 .0832 .0000 #3 -.19105 -.0640 2.7055 .4556 .0827 .0000 Elem Cd Cc Cr Cu Fe. K Units ppm ppm ppm ppm ppm ppm Avge .0000 .0077 .0009 .0030 8.939 84.72 SDev .0002 .0001 .0005 .0002 .037 .75 %RSD 387.8 1.827 58.40 5.939 .4108 .8867 #1 -.0001 .0078 .0014 .0028 8.971 85.45 #2 .0002 .0075 .0003 .0.029 8.948 84.76 #3 -.0001 .0078 .0010 .0032 8.899 83.95 Elem Mn. Mo Na Ni 2203/1 22'03/2 its- ppm Ppm PPM PPM ppb ppb 3e 1.596 .0005 82.74 .0095 -1.1143 .36314 SDev .008 .0009 .44 .0.006 1.2764 .82586 %RSD .4724 190.3 .5361 6.305 114.55 227.42 #1 1.603 -.0003 83.13 .0089 -1.2899 .07204 #2 1.597 .0015 82.83 .0101- -2.2938 1.2951 #3 1.588 .00.03 82.25 .0095 .24079 -.27775 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb PPM PPM PPM Avge -8.1962. 2.9942 -.88813 12.32 -.0006 .4633 SDev 2.9761 2.9790 3.92089 .06 .001.1 .0019 0-oRSD 36.311 99.495 441.48 .5046 172.4 .4122 ##1 -4.8833 4.9682 2.5230 12.38 -.0004 .4644 #2 -10.643 4.4468 -5.1.718 12.34 -.0018 .4645 #3 -9.0617 -.43254 -.01557 12.26 .0003 .4611 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Unites ppb PPM PPM ppb ppb ppb Avge .9'0620 .0009 .0071 -.12876 -8.3189 .40468 SDev 2.0786 .0003 .0001 .24163 1.6777 2.6968 %RSD. 229.38 28.82 2.147 187.66 20.167 666.40 #1 2.4604 .0010 .0072 -.38139 -6.3985 3.3372 R? -1.4549 .0012 .0071 .10012 -9.0585 -1.9688 t 1.7131 .0006 .0069 -.10500 -9.49.97 -.15438 . page 1 Ca ppm 72.73 .30 .4119 72.99 72.79 72.40 Mg PPM 38.47 .14 .3739 38.58 38.52 38.31 2068/1 ppb -8.5649 2.3692 27.662 -9.4338 -5.8839 -10.377 Ti ppm .0007 .0001 10.68 .0007 .0006 .0007 06/20/07 01:35:55 PM page 1 gnalysis Report 1)d: CLP1 Sample Name: 0706952-009D Operator: MAG Run lime: 06/2.0/07 13:28:30 -$ S Comment :� Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca ppm Units ppb ppm ppb 3.5344 ppm .2556 ppm .2647 ppm .0001 60.25 Avge SDev -.10943 .44081 -.0494 .0078 3.0068 .0003 .0014 .0000 .08 %RSD 402.82 15.72 85.072 .1247 .5192 29.17 .1315 #1 .27014 -.0408 .20150 .2553 .2663 .0000 60.26 60.17 #2 -.59291 -.0517 6.0432 4.3586 .2559 .2643 .2637 .0001 .0001 60.32 #3 -.00553 -.0558 .2557 Elem Cd Co Cr Cu Fe PPM K ppm Mg ppm Units ppm ppm ppm ppm .0004 49.00 39.56 35 20.01 Avge SDev .0009 .0001 .0030 .0001 .0039 .0002 ..0003 .16 .19 %RSD 12.06 4.133 4.722 77.11 .3165 .4867 .0538 #1 .0008 .0029 .0039 .0001 49.18 39.77 39.54 20.36 20.34 #2 .0009 .0029 .0037 .0003 48.88 48.95 39.38 20.36 #3 .0010 .0031 .0040 .0007 Na Ni 2203/1 2203/2 2068/1 Elem Mn Mo Ppb Ppb Ppb Lts ppm ppm PPM 37.81 ppm .0046 -4.6606 -1.7396 -8.8007 3e .4183 -.0002 .15 .0010 3.0509 1.6249 1.4680 SDev %RSD .0008 .1862 .0012 558.0 .3948 22.92 65.463 93.405 16.681 #1 .4192 -.0009 37.66 .0034 -8.1652 -1.4596 -7.7467 -8.1778 #2 .4177 .0012 37.96 .0051 -2.5979 -3.2185 -.27291 -3.4863 -10.477 #3 .4180 -.0009 37.80 .0052 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb ppm 9.251 PPM PP m .2953 ppm .0009 Avge -8.8357 - 3.1918 -.05416 .0035 .0002 01 042 SDev 4.3734 16.197 4054506 .015 .1624 70 033 .0750 152S %RSD 49.497 #1 -12.744 3.3850 .96130 9.268 .0015 .2952 .0010 #2 -4.1120 3.5843 -2.5736 9.240 9.245 .0063 .2956 .2953 .0009 .0008 #3 -9.6512 2.6060 .1.4499 .0028 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb - ppm ppm PP b -2.7121 ppb -8.8240 ppb 1.0268 Avge 2.4309 .0021 .0225 1.4496 2.9649 1.3426 SDev 2.2745 .0003 12.85 .0001 .3981 53.449 33.601 130.76 %R'SD 93.566 #1 3.8689 .0024 .0225 -3.6924 -11.080 1.7684 u� -.1.9137 .0021 .0226 -1.0470 -5.4658 -9.9263 -.52303 1.8349 3 3.6153 .0019 .0225 -3.3970 Analysis Report 06/20/07 01:43:26 PM N Dd: CLP1 Sample Name: 0706952-010D Operator: MAG Rte.. Time: 06/20/07 13:36:01 Comment: r (�j 0(0 ii 10T Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb PPM ppb Ppm PPM PPM Avge -.33780 -.0493 -.50847 .0013 .0002 .0002 SDev .37025 .0042 2.80056 .0008 .0001 .0001 %RSD 109.61 8.491 550.79 61.53 47.32 67.48 #1 -.09395 -.0504 2.5929 .0019 .0003 .0001 #2 -.15560 -.0528 -2.8524 .0014 .0002 .0001 #3 -.76385 -.0446 -1.2659 .0004 .0001 .0003 Elem Cd Co Cr Cu Fe K Units ppm PPM Ppm PPM PPM Ppm Avge -.0000 -.0006 .0010 -.0005 .0224 .0806 SDev .0001 .0002 .0002 .0006 .0170 .0100 0 -.RSD 1527. 36.20 16.51 117.2 75.78 12.42 #1 -.0001 -.0009 .0010 .0001 .0404 .0917 #2 .0001 -.0005 .0012 -.0005 .0203 .0778 #3 .0000 -.0004 .0009 -.0011 .0066 .0723 Elem Mn Mo Na Ni 2203/1 2203/2 ppm Ppm Ppm Ppm Ppb Ppb _ts je .0008 .0002 .0897 .0016 1.6322 -1.3690 SDev .0002 .0003 .0172 .0008 1.8480 .5648 %RSD 23.63 116.9 19.21 49.00 113.22 41.258 #1 .0010 .0001 .1084 .0025 .65858 -.80019 #2 .0008 .0001 .0862 .0011 .47450 -1.3771 #3 .0006 .0006 .0745 .0012 3.7634 -1.9298 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb Ppm Ppm ppm Avge -8.8726 -.57711 -2.3075 .0176 -.0003 .0001 SDev 2.6527 1.53084 1.3306 .0022 .0001 .0001 %RSD 29.897 265.26 57.664 12.22 41.92 75.27 #1 -11.192 1.1293 -.86401 .0197 -.0004 .0002 #2 -9.4453 -1.8299 -3.4850 .0177 -.0002 .0001 #3 -5.9804 -1.0306 -2.5733 .0154 -.0003 .0000 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb Ppm Ppm Ppb Ppb Ppb Avge 2.9336 .0002 .0089 -.36955 -9.8038 -1.7312 SDev 1.1333 .0003 .0001 .36643 1.5794 1.3961 %RSD 38.631 149.0 .6974 99.157 16.110 80.640 #1 3.7159 .0005 .0088 -.31434 -11.415 -.20026 #2 1.6339 -.0001 .0089 -.76045 -9.7390 -2.9339 3.4508 .0001 .0089 -.03385 -8.2579 -2.0596 page 1 Ca ppm .0464 .0200 43.16 .0672 .0448 .0272 Mg PPM -.0430 .0097 22.60 -.0329 -.0438 -.0523 2068/1 ppb -11.669 1.257 10.774 -11.860 -10.327 -12.820 Ti ppm -.0002 .0001 49.17 -.0001 -.0002 -.0002 Analysis Report 06/20/07 01:50:58 PM page 1 M; )d: CLP1 Sample Name: 0706986-001D Operator: MAG R.-__ Time: 06/20/07 13:43:32 Comment: R -i Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .08830 .0615 -.79041 .0138 .0282 .0004 22.69 SDev .16590 .0127 .61590 .0003 .0003 .0000 .32 %RSD 187.88 20.71 77.921 2.45.9 1.087 4.762 1.425 #1 .11209 .0762 -.07970 .0136 .0281 .0003 22.50 #2 .24102 .0533 -1.1235 .0136 .0279 .0003 22.49 #3 -.08821 .0551 -1.1680 .0142 .0285 .0004 23.06 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm PPM Ppm Ppm PPM Avge -.0001 .0001 .0019 -.0018 .2222 1.360 10.43 SDev .0001 .0004 .0005 .0004 .0024 .009 _ .15 %RSD 71.71 625.3 23.94 19.43 1.081 .6466 1.452 #1 -.0000 -.0003 .0014 -.0022 .2227 1.353 10.33 #2 -.0002 .00.04 .0021 -.0015 .2196 1.356 10.35 #3 -.0002 .0001 .0022 -.0018 .2243 1.370 10.60 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 - is ppm Ppm PPM PPM ppb Ppb - ppb e .0071 .0010 20.09 .0014 -.39263 -.48679 -9.1724 bLev .0001 .0006 .41 .0005 .58617 1.12216 .6096 %RSD 1.928 54.11 2.019 34.57 149.29 230.52' 6.6457 #1 .0069 .0016 19.77 .0019 -.9.9494 07539 -8.4818 #2 .0072 .0005 19.95 ..0010 .17594 -1.7789 -9.6354 #3 .0071 .0009 2'0.55 .0013 -.35891 .24316 -9.4001 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -10.405 2.5735 -3.5213 9.057 -,0004 .0917 .0053 SDev .7381.2663 1.1133 .127 .0035 .0017 .0005 %RSD 7.0895 49.205 31.617 1.408 883.8 1.855 9.108 #1 -9.8284 1.5510 -4.8042 8.999 .0011 .0903 .0049 #2 -11.236 3.9899 -2.8075 8.969 .0021 .0912 .0052 ##3 -10.150 2.1797 -2.9523 9.203 -.0045 .0936 .0059 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 47319 .0012 .0943 -.45532 -9.9944 -1.4917 SDev .96871 .0003 .0014 .60449 .6666 1.0933 %RSD 204.72 23.05 1.435 132.76 6.6695 73.293 #1 1.2411 .0010 .0933 -.28091 -9.3800 -2.6879 #2 .79360 .0011 .0937 -1.1278 -10.703 -.54396 -.61514 .0015 .0958 .04279 -9.9002 -1.2433 Analysis Report 06/20/07 01:58:29 PM N od: CLP1 Sample Name: 0706986-002D Operator: MAG R--_ Time: 06/20/07 13:51:04 Comment: Kw -L S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm IPPb ppm ppm ppm Avge .09846 .7427 -1.8107 .0233 .0907 .0005 SDev .27578 .0333 .7094 .0005 .0010 .0001 %RSD 280.10 4.484 39.176 1.967 1.142 13.40 #1 -.03624 .7788 -2_3099 .0231 .0917 .0006 #2 .41571 .7362 -.99871 .0239 .0908 .0005 #3 -.08409 .7132 -2.1236 .0231 .0896 .0005 Elem Cd Co Cr Cu Fe K Units ppm ppm Ppm PPM ppm ppm Avge .0005 .0008 .2425 .0179 2.368 2,.394 SDev .0003 .0001 .0007 .0006 .016 .022 _ %RSD 64.03 7.627 .2832 3.456 .6742 .9083 #1.0003 .0007 .2424 .0172 2.373 2.413 #2_ .0004 .0008 .2432 .0180 2.381 2.398 #3 .0009 .0008 .2418 .0184 2.350 2.370 Elem Mn Mo Na Ni 2203/1 2203/2 .ts ppm ppm ppm ppm Ppb Ppb je .0823 .0020 51.22 .0087 3.6836 2.3251 SDev .0004 .0001 .27 .0005 3.6319 .3724 %RSD .5076 4.275 .5305 5.437 98.596 16.017 #1 .0824 .0020 51.14 .0084 4.8014 2.0963 #2 .0826 .0019 51.53 .0092 -.37579 2.7548 #3 .0818 .0021 51.00 .0084 6.6253 2.1242 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb Ppb ppm ppm Ppm Avge -10.146 3.0299 -3.3614 6.072 -.0004 .0691 SDev 2.238 3.5425 .6363 .043 .0014 .0004 %RSD 22.058 116.92 18.929 .7035 327.4 .6527 #1 -9.5567 6.1480 -3.5623- 6.092 -.0020 .0690 #2 -8.2616 -.82205 -3.8729. 6.100 .0002 .0697 #3 -12.620 .3.7636 -2.6489 6.022 .0005 .0688 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm Ppm ppb ppb ppb Avge .85562 .0033 .0659 2.7776 -9.5325 -1.2331- SDev 1.0679 .0002 .0004 .9741 1.8870 1.4093 %RSD 124.81 6.053 .5798 35.071 19.796 114.29 #1 1.5012 .0030 .0657 2.9972 -9.0202 -.32880 #U2 1_4427 .0034 .0664 1.7124 -7.9545 -2.8569 -.37705 .0034 .0657 3.6231 -11.623 -.51349 page 1 Ca PPM 9.086 .056 .6151 9.084 9.142 9.030 Mg ppm 7.148 .033 .4573 7.140 7.184 7.120 2068/l ppb -8.3036 1.1846 14.266 -7.9457 -7.3392 -9.6259 Ti ppm .0462 .0012 2.527 .0476 .0456 .0455 Analysis Report 06/20/07 02:06:00 PM page 1 M )d: CLP1 Sample Name: 0706986-003D Operator: MAG R,. mime: 06/20/07 13:58:35 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb ppm PPM ppm Ppm Avge -.50264 -.0593 4.5028 .9911 .2053 .0001 62.11 SDev .0129 .3418 .0058 .0009 .0000 .12 %RSD .17711 35.237 21.76 7.5914 .5878 .4224 19.90 .1993 #1 -.37006 -.0459 4.4418 .9844 .2063 .0001 61.97 #2 -.70379 -.0603 4.1956 .9944 .2050 .0001 62:20 #3 -.43408 -.0717 4.8710 .9945 .2047 .0001 62.17 Elem Cd Cc Cr Cu Fe K Mg Units ppm PPM ppm ppm PPM 6.654 PPM 131.5 Ppm 33.04 Avge SDev .0000 .0317 .0003 .0022 .0000 .0062 .0006 .013 .4 .15 %RSD .0001 625.4 .8930 1.760 10.24 .1897 .2811 .4411 #1 .0001 .0320 .0022 .0058 6.639 131.9 32.87 #2 -.0001 .0314 .0023 .0059 6.663 131.2 33.11 #3 -.0000 .0316 .0022 .0069 6.658 131.4 33.14 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm 218.0 ppm Ppb .92904 Ppb -2.1854 Ppb -9.1557 ge SDev 3.928 .0009 .0006 .2 .0521 .0011 4.8348 1.4580 3.4281 %RSD .006 .1634 70.36 .0828 2.091 520.41 66.712 37.442 #1 3.920 .0015 217.8 .0527 6.1951 -3.8404 -11.959 #2 3.932 .0002 218.1 .0527 -3.3091 -1.0906 -10.175 #3 3.931 .0009 218.0 .0508 -.09887 -1.6253 -5.3336 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb PPM 8.768 ppm -.0016 ppm .4365 ppm .0004 Avge SDev -7.0736 1.7303 3.6553 2.7126 -.32246 2.40905 .024 .0009 .0008 0005 %RSD 24.461 74.211 747.08 .2690 55.72 .1776 118.4 #1 -5.8737 6.6920 -.40756 8.740 -.0025 .4356 .0005 #2 -6.2901 1.4721 2.1280 8.783 -.0007 .4371 -.0001 #3 -9.0571 2.8017 -2.6878 8.779 -.0016 .4367 .0009 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM ppm -Ppb Ppb Ppb Avge 1.8991 .0009 .0104 -1.1482 -7.7669 1.0022 SDev 1.9208 .0002 .0001 .6660 .1640 1.6126 %RSD 101.14 17.85 .8206 57.997 2.1109 160.92 #1 1.8413 .0008 .0104 -.49850 -7.8999 1.9566 :R2 .0.011 .0105 -1.8293 -7.5838 1.9096 .00794 3.8482 .0009 .0103 -1.1169 -7.8172 -.85977 page 1 Ca PPM 50.72 .10 .1.969 50.77 50.60 50.77 Mg ppm 26.26 .04 .1485 26.23 26.25 26.31 2068/1 ppb -8.1332 1.8433 22.664 -6.0070 -9.2819 -9.1106 Ti ppm .0043 .0001 1.535 .0044 .0042 .0043 06/20/07 02:13:31 PM Analysis Report M' Dd: CLP1 Sample Name: 0706986-004D Operator: MAG R-_= Time: 06/20/07 14:06:06 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb Ppm ppb Ppm Ppm PPM Avge -.43951 .0486 1.8823 .2577 .1815 .0001 SDev .50482 .0128 1.6819 .0009 .0006 .0000 %RSD 114.86 26.29 89.354 .3579 .3272 36.67 #1 -.12888 .0628 3.1298 .2580 .1822 .0001 #2 -1.0220 .0450 -.03048 .2566 .1811 .0001 ##3 -.16765 .0380 2.5475 .2584 .1812 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm PPM Ppm .0049 ppm 42.24 PPM 38.63 Avge SDev .0010 .0277 .0001 .0032 .0002 .0003 .21 .07 %RSD .0001 11.59 .4954 4.980 5.792 .4893 .1756 ##1 .0010 .0276 .0031 .0047 42.48 38.56 #2 .0009 .0277 .0031 .0047 42.11 38.70 #3 .0011 .0279 .0034 .0052 42.13 38.63 Elem Mn Mo Na Ni 2203/1 2203/2. its ppm ppm PPM 55.79 ppm .0117 Ppb -.46317 Ppb -4.9629 4e 20.14 -.0008 .28 .0004 1.64343 2.1518 oLzv %RSD .03 .1677 .0003 32.19 .4948 3.162 354.82 43.357 ##1 20.15 -.0005 55.50 .0114 -2.3036 -3.8066 #2 20.10 -.0009 56.05 .0116 .85771 -3.6365 #3 20.17 -.0010 55.83 .0121 .05637 -7.4456 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb Ppb ppm PPM PPM Avge -5.3630 6.4273 -4.7969 8.057 .0017 .4031 SDev 1.0546 1.6942 2.1312 .009 .0016 .0006 0 -.RSD 19.664 26.360 44.429 .1067 90.97 .1518 #1 -4.7608 6.7008 -3.6392 8.049 .0006 .4024 ##2 -4.7475 7.9682 -3.4950 8.056 .0011 .4033 ##3 -6.5807 4..6130 -7.2564 8.066 .0035 .4036 Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm PPM Ppb -3.4644 Ppb -6.2855 ppb -1.0592 Avge 3.1078 2.6474 .0015 .0054 .0000 1.4104 1.1240 1.9611 SDev %RSD 85.187 .0004 29.99 .3320 40.712 17.882 185.15 #1 3.7455 .0019 .0054 -3.3060 -5.1758 -.19603 #_#2 .0010 .0054 -2.1399 -6.2574 .32222 .19974 5.3781 .0015 .0054 -4.9474 -7.4232 -3.3039 page 1 Ca PPM 50.72 .10 .1.969 50.77 50.60 50.77 Mg ppm 26.26 .04 .1485 26.23 26.25 26.31 2068/1 ppb -8.1332 1.8433 22.664 -6.0070 -9.2819 -9.1106 Ti ppm .0043 .0001 1.535 .0044 .0042 .0043 Analysis Report 06/20/07 02:26:17 PM page 1 P od: CLP1 Sample Name: 0707014-002A Operator: MAG 1,-.. Time: 06/20/07 14:18:52 1 V.; W - �� lio �^ i?(�c} -16S- L� ct �a �P�', c.L� Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb Ppm Ppm Ppm PPM Avge- .45183 .0280 4.2045 -.0020 .0012 .0001 .0214 SDev .19068 .0067 1.6750 .0006 .0000 .0000 .0032 %RSD 42.202 24.01 39.840 28.52 3.346 15.99 14.78 #1 .67187 .0358 6.0437 -.0019 .0012 .0001 .0232 #2 .34883 .0249 3.8033 -.0016 .0011 .0001 .0233 #3 .33480 .0234 2.7665 -.0027 .0012 .0001 .0178 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM PPM PPM Avge .0003 .0245 .0602 .2082 218.1 .0790 .0255 SDev .0005 .0002 0005 .2 .0011 .0027 %RSD 174.5 _.0004 1.574 .2655 .2272 .0951 1.438 10.59 #1 -.0003 .0243 .0601 .2086 218.4 .0788 .0264 #2 .0007 .0242 .0604 .2077 218.1 .0802 .0276 #3 .0005 .0249 .0601 .2083 218.0 .0779 .0225 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 .ts ppm ppm PPM PPM Ppb Ppb Ppb je 1.647 .0131 .0875 .0949 -18.686 -4.9185 -2.4955 SDev .001 .0008 .0072 .0008 2.565 1.0974 2.5567 %RSD .0398 6.351 8.227 .8582 13.726 22.312 102.45 #1 1.647 .0133 .0937 .0957 -15.741 -6.0858 -2.7720 #2 1.648 .0137 .0892 .0940 -19.890 -3.9078 .18819 #3 1.647 .0121 .0796 .0950 -20.428 -4.7621 -4.9028 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb PPM PPM PPM PPM Avge -1.9937 .31784 1.0108 .2745 .0334 .0005 .0027 SDev 1.6706 1.6172 1,8495 .0018 .0013 .0001 .0002 %RSD 83.795 508.81 172.72 .6417 3.972 11.49 7.716 #1 -.22047 -.53075 -1.0256 .2739 .0321 .0006 .0029 #2 -3.5381 2.1827 1.7664 .2765 .0347 .0006 .0026 #3 -2.2225 -.69841 2.4716 .2731 .0333 .0005 .0025 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm Ppm ppb ppb ppb Avge 10.620 .0221 -.0162 -9.5030 -2.1608 .82007 SDev 1.309 .0002 .0004 .4134 1.0293 1.4761 %RSD 12.330 .8009 2.321 4.3504 47.633 180.00 #1 9.7602 .0222 -.0166 -9.3008 -1.0701 -.86083 2. 9.9729 .0222 -.0159 -9.2296 -2.2973 1.9050 12.127 .0219 -.0161 -9.9786 -3.1150 1.4160 Analysis Report 06/20/07 02:35:06 PM page 1 Md: CLP1 Sample Name: CCV3 Operator: MAG Ru Time: 06/20/07 14:27:41 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 969.88 47.10 509.52 2.433 2.467 2.453 46.86 SDev 8.18 .39 3.53 .027 .022 .026 .49 %RSD .84387 .8337 .69251 1.123 .8730 1.063 1.044 #1 964.78 46.88 505.55 2.407 2.455 2.433 46.52 #2 965:55 46.86 510.70 2.430 2.454 2.444 46.64 #3 979.32 47.55 512.30 2.462 2.492 2.483 47.42 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm 2.425 ppm 2.417 ppm 2.468 ppm 47.33 ppm 81.11 ppm 49.81 Avge SDev 2.456 .030 .023 .026 .42 .69 .55 %RSD .019 .7882 1.225 .9474 1.059 .8976 .8568 1.102 #1 2.455 2.399 2.402 2.446 47.11 80.71 49.37 2.437 2.420 2.407 2.461 47.05 80.71 49.63 2.476 2.457 2.444 2.497 47.82 81.91 50.42 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm 80.60 ppm 2.471 ppb 546.86 ppb 497.00 ppb 959.02 Avge 2.405 2.401 .024 5.00 2.35 13.67 SDev %RSD .023 .9731 .030 1.257 .92 1.136 .9600 .91365 .47202 1.4249 #1 2.389 2.383 79.76 2:469 543.18 497.82 945.08 #2 2.394 2.384 80.46 2.449 544.86 494.36 959.58 #3 2.432 2.436 81.58 2.496 552.55 498.83 972.39 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2:750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb Ppm ppm ppm ppm Avge 947.07 522.98 502.68 2.497 2.417 2.445 2.506 SDev 19.15 7.33 3.55 .033 .034 .026 .079 0-oRSD 2.0220 1.4024 .70536 1.306 1.389 1.061 3.137 935.81 517.00 504.47 2.472 2.383 2.424 2.596 936.22 520.77 498.60 2.486 2.419 2.437 2.464 #3 969.18 531.16 504.98 2.534 2.450 2.474 2.456 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 02:35:06 PM Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 497.54 2.412 2.484 513.61 951.05 509.44 SDev 4.53 .024 .026 2.83 16.82 3.92 %RSD .90978 1.013 1.061 .55192 1.7689 .76948 #1 495.33 2.392 2.463 512.92 938.90 508.64 ##2 494.55 2.405 2.476 511.18 944.00 505.98 #3 502.75 2.440 2.513 516.72 970.25 513.70 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 -2.250 450.00 900.00 450.00 page 2 Analysis Report 06/20/07 02:42:37 PM page 1 P od: CLP1 Sample Name: CCVL3 Operator: MAG Time: 06/20/07 14:35:12 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm Ppm Ppm Avge .33869 -.0196 -.59016 .0056 .0006 .0009 -.0610 SDev .24428 .0152 1.28327 .0012 .0001 .0001 .0013 %RSD 72.124 77.68 217.44 21.14 19.63 12.32 2.140 #1 .59038 -.0027 -1.8721 .0066 .0007 .0010 -.0623 #2 .10256 -.0239 .69441 .0060 .0005 .0009 -.0597 #3 .32314 -.0322 -.59279 .0043 .0005 .0008 -.0611 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm PPM -.0027 Ppm 2.611 Ppm .0631 Ppm -.0485 Avge SDev .0006 .0002 .0005 .0005. .0003 .0002 .0003 .004 .0090 .0043 %RSD 32.40 109.3 61.31 12.99 .1592 14.21 8.872 #1 .0008 .0010 .0006 -.0028 2.616 .0702 -.0437 "- -.0000 .0001 -.0029 2.609 .0530 -.0520 .0006 .0004 .0004 .0003 -.0023 2.608 .0662 -.0499 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm 2.636 ppm -.0005 ppb -.91142 ppb -.32197 ppb -6.7294 Avge SDev .0006 .0098 .0047 .033 .0003 1.68681 2.39716 1.6624. %RSD .0002 32.08 47.99 1.258 77.58 185.08 744.52 24.704 #1 .0008 .0149 2.598 -.0003 .91435 -2.9309 -6.9955 #2 .0005 .0088 2.659 -.0002 -1.2367 .18163 -8.2428 #3 .0004 .0057 2.651 -.0008 -2.4119 1.7834 -4.9500 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb ppm PPM Ppm Ppm Avge -4.5030 1.9116 -1.2693 .0020 .0007 .0005 .0002 SDev 1.6060 .4508 3.1168 .0022 .0017 .0001 .0005 %RSD 35.666 23.582 245.55 105.2 246.4 21.53 264.8 -3.2122 1-.8171 1.8862 .0002 .0020 .0006 .0007 -6-.3015 1.5155 -4.3459 .0015 .0012 .0005 -.0003 #3 -3.9953 2.4021 -1.3483 .0044 -.0012 .0004 .0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 02:42:37 PM page 2 V Zn Low Sb2068 Elem T11908 Units ppb Avge 3.7066 SDev 1.6944 %RSD 45.714 ##1 5.2937 ##2 1.9221 #3 3.9040 Errors NOCHECK High 28.173 Low .0017 V Zn Pb2203 Sb2068 Se1960 PPM PPM Ppb ppb Ppb .0012 .0014 -.51818 -5.2444 -.21009 .0004 .0001 1.03730 1.4775 2.13079 35.70 5.459 200.18 28.173 1014.2 .0017 .0015 -1.6504 -4.4720 1.8632 .0008 .0014 -.29060 -6.9480 -2.3941 .0012 .0013 .38643 -4.3132 -.09941 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 02:50:09 PM page 1 M )d: CLP1 Sample Name: CCB3 Operator: MAG Ruii rime: 06/20/07 14:42:44 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb Ppm ppm Ppm Ppm Avge -.01616 -.0349 .41213 .0022 .0002 .0005 -.0513 SDev .28951 .0274 .89230 .0006 .0001 .0002 .0040 %RSD 1791.8 78.73 216.51 27.77 47.87 40.08 7.798 #1 .07996 -.0041 .83845 .0019 .0004 .0007 -.0554 #2 -.34150 -.0436 1.0113 .0019 .0001 .0004 -.0510 #3 .21307 -.0568 -.61336 .0029 .0002 .0003 -.0474 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.200.0 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units_ ppm ppm Ppm Ppm Ppm Ppm Ppm Avge -.0000 -.0001 -.0002 -.0007 .-.0102 .0565 -.0565 SDev .0002 .0008 .0003 .0014 .0030 .0117 .0046 %RSD 2166. 1227. 207.4 201.7 29.17 20.77 8.094 #1 .0002 .0005 .0002 -.0019 -.0069 .0609 -.0513 -.0002 -.0010 -.0004 -.0012 -.0110 .0432 -.0599 .0001 .0003 -.0003 .0009 -.0127 .0654 -.0583 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0003 .0029 .0333 .0001 -2.5922 -1.2180 -9.1783 SDev .0001 .0010 .0023 .0015 2.4272 1.0856 1.2884 %RSD 50.87 34.00 7.015 1072. 93.636 89.133 14.038 #1 .0004 .0038 .0356 .0015 -.65895 .02722 -10.633 #2 .0001 .0031 .0334 -.0014 -1.8015 -1.9657 -8.7218 #3 .0003 .0018- .0310 .0003 -5.3162 -1.7153 -8.1803 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -8.0462 .82338 -4.3028 .0058 -.0006 .0003 -.0000 SDev 1.7878 2.9042 2.4923 .0038 .0005 .0001 .0001 %RSD 22.219 352.71 5.7.923 64.95 82.02 26.01 809.8 -6.2323 4.1669 -7.0048 .0027 -.0006 .0004 .0001 -8.0996 -.62482 -2.0938 .0101 -.0012 .0002 -.0002 #3 -9.8066 -1.07-19 -3.8097 .0047 -.0002 .0002 -.0000 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK r - C) 0 0 Cn Ei knalysis Report 06/20/07 02:50:09 PM 1 _ Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .56867 .0002 -.0036 -1.6755 -8.4231 -2.5958 SDev 1.5227 .0001 .0002 1.3718 .7901 .8798 %RSD 267.77 55.29 6.514 81.873 9.3806 33.894 #1 2.2286 .0001 -.0034 -.20123 -7.6976 -3.2846 #2 -.76352 .0001 -.0036 -1.9110 -8.3068 -1.6047 #3 .24097 .0003 -.0038 -2.9144 -9.2650 -2.8980 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 knalysis Report 06/20/07 02:57:40 PM 4 A: CLP1 Sample Name: 0707014-001APDS Operator: MAG Z- Time: 06/20/07 14:50:15 3omment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 3 Ba Be Units ppb PPM Ppb PPM PPM PPM Avge 18.703 2.465 18.486 .5762 .0122 .0110 SDev .172 .042. 1.336 .0047 .0002 .0001 %RSD .92104 1.702 7.2249 .8136 1.754 1.158 #1 18.845 2.510 19.327 .5814 .0125 .0111 ##2 18.753 2.457 19.185 .5751 .0122 .0109 ##3 18.512 2.427 16.946 .5722 .0121 .0108 Elem Cd Co Cr Cu Fe K Units ppm PPM PPM PPM PPM PPM Avge .0110 .1121 .0482 .3784 .9241 .2264 SDev .0004 .0007 .0005 .0028 .0108 .0003 %RSD 3.906 .6017 1.097 .7360 1.171 .1424 #1 .0114 .1128 .0485 .3815 .9358 .2262 #2 .0106 .1122 .0485 .3773 .9222 .2263 #3 .0109 .1114 .0476 .3763 .9144 .2268 Elem Mn Mo Na - Ni 2203/1 2203/2 is ppm PPM PPM PPM Ppb Ppb ;e .0530 .0020 .3514 .1226 31.835 21.122 SDev .0006 .0006 .0022 .0015 3.383 .939 %RSD 1.057 32.12 .6335 1.188 10.625 4.4458 #1 .0536 .0026 .3527 .1226 28.882 20.475 #2 .0530 .0019 .3526 .1241 35.525 20.691 #3 .0525 .0014 .3488 .1212 31.097 22.199 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb Ppb - ppb PPM PPM PPM Avge 131.37 3.4986 11.412 1.130 .0527 .0386 SDev 1.67 2.0932 .345 .011 .0014 .0004 %RSD 1.2749 59.832 3.0192 .9465 2.618 1.012 #1 132.23 3.1152 11.184 1.139 .0543 .0391 #2 132.44 1.6235 11.809 1.132 .0518 .0385 #3 129.44 5.7570 11.244 1.118 .0521 .0383 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm Ppb ppb Ppb Avge 18.564 .1109 .2039 24.689 129.58 8.7770 SDev .984 .0016 .0022 1.247 .68 .5555 %RSD 5.3013 1.403 1.062 5.0515 .52675 6.3290 #1 17.490 .1123 .2061 23.275 129.52 8.4973 ;U2. 18.780 .1111 .2038 25.631 130.29 8.4170 19.422 .1092 .2018 25.162 128.93 9.4168 page 1 Ca PPM 4.850 .043 .8868 4.895 4.844 4.810 Mg PPM .1895 .0022 1.149 .1908 .1908 .1870 2068/1 ppb 126.00 1.91 1.5150 124.09 125.99 127.91 Ti PPM .1103 .0025 2.294 .1131 .1098 .1081 O O O E- 06/20/07 03:14:18 PM page 1 analysis Report v! )d: CLP1 Sample Name: 0706986-004D Operator: MAG R- Time: 06/20/07 15:06:53 Rr1.A Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm ppm -.0001 ppm 23.98 Avge -.27875 -.0167 1.2569 1.2115 .1211 .0056 .0854 .0038 .0000 1.09 SDev %RSD .14457 51.864 .0053 31.92 96.390 4.602 4.471 6.744 4,549 #1 -.11539 -.0112 1.8705 .1148 .0814 -.0001 22.82 24.14 #2 -.39019 -.0171 2.0387 .1229 .0858 -.0001 -.0001 24.99 #3 -.33066 -.0218 -.13866 .1256 .0890 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm ppm ppm 20.87 ppm 17.17 ppm 12.37 Avge SDev .0002 .0124 .0005, .0008 .0002 .0030 .0009 .62 .87 .58 %RSD .0003_ 155.8 4.271 19.61 30.21 2.968 5.078 4.720 #1 -.0001 .0117 .0008 .0020 20.37 16.27 17.24 11.75 12.44 #2 .0002 .0127 .0010 .0034 21.56 20.68 18.00 12.91 #3 .0005 .0126 .0006 .0037 Mo Na Ni 2203/1 2203/2 2068/1 Elem .ts Mn ppm ppm Ppm Ppm ppb -2.3774 ppb -1.8634 ppb -6.8736 le 9.743 .0001 26.33 1.17 .0049 .0006 3.4124 1.8339 1.0814 SDev %RSD .432 4.436 .0001 107.5 4.451 11.58 143.54 98.417 15.732 #1 9.287 .0003 25.07 .0049 -5.9856 -.96040 -5.9664 #2 9.795 .0002 26.54 .0055 .79788 -3.9737 -8.0702 $3 10.15 -.0000 27.39 .0044 -1.9444 -.65609 -6.5843 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb Ppm 3.803 Ppm Ppm .1873 ppm .0019 Avge -7.5207 1.3216 4.0825 -.82071 1.10951 .181 .0005 .0023 .0088 .0001 SDev %RSD 2.6734 35.547 308.91 135.19 4.764 433.7 4.690 6.438 #1 -4.6509 -.55818 .20686 3.612 .0021 .1780 .0019 #2 -7.9705 6.0054 -1.9971 3.824 .0016 .1884 .0020 .0018 #3 -9.9407 -1.4824 -.67185 3.973 -.0021 .1954 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb Ppm Ppm -.0019 ppb -2.0345 Ppb -7.3052 ppb -.10730 Avge .37545 1.1804 .0009 .0002 .8316 1.9626 .80637 SDev %RSD 314.38 .0004 50.98 8.178 40.876 26.865 751.54 #1 .0005 -.0021 -2.6337 -5.0889 -.04790 419 ..59756 1.4290 .0008 -.0019 -2.3847 -8.0036 .66774 -.90018 .0013 -.0018 -1.0850 -8.8230 -.94173 O O O E- Analysis Report 06/20/07 03:21:49 PM page 1 h od: CLP1 Sample Name: ORIF Operator: MAG R-__ Time: 06/20/07 15:14:24 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 19.898 -.0498 20.100 .2283 .0000 .0114 -.0535 SDev .295 .0118 1.333 .0004 .0000 .0001 .0017 %RSD 1.4811 23.65 6.6295 .1824 126.6 .8221 3.097 #1 20.180 -.0366 18.642 .2285 .0001 .0115 -.0550 #2 19.922 -.0591 20.403 .2286 .0000 .0115 -.0517 #3 19.592 -.0537 21.255 .2278 -.0000 .0113 -.0538 Errors LC Pass NOCHECK LC Pass NOCHECK NOCHECK LC Pass NOCHECK High 26.000 26.000 .0130 Low 14.000 14.000 .0070 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm PPM Ppm Ppm. Ppm PPM Avge .0109 .1109 .0217 .0567 .0045 .0649 -.0542 SDev .0002 .0003 .0001 .0003 .0019 .0024 .0028 %RSD 1.890 .2872 .4202 .5668 42.55 3.745 5.116 #1 .0111 .1111 .0217 .0567 .0066 .0644 -.0513 .1111 .0216 .0570 .0040 .0676 -.0544 .0110 .0107 .1105 .0218 .0564 .0029 .0628 -.0569 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0130 .1300 .0260 .0650 Low .0070 .0700 .0140 .0350 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0384 .0228 .2406 .0887 6.8262 5.3747 123.99 SDev .0008 .0006 .0026 .0006 .8826 2.9203 1.36 %RSD 2.014 2.750 1.087 .6497 12.929 54.334 1.0986 #1 .0388 .0230 .2433 .0893 5.8947 7.2369 124.58 #2 .0388 .0221 .2403 .0885 7.6499 6.8782 124.97 #3 .0375 .0232 .2381 .0882 6.9340 2.0090 122.44 Errors LC Pass LC Pass NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High •.0390 .0260 .1040 Low .0210 .0140 .0560 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb PPM PPM PPM PPM Avge 122.50 6.8295 7.9042 .1819 .0894 .0581 .2594 SDev 1.32 3.5969 1.1333 .0128 .0020 .0003 .0072 %RSD 1.0748 52.668 14.338 7.054 2.235 .5573 2.792 122.79 9.6435 8.6253 .1875 .0871 .0583 .2676 121.06 2.7769 8.4894 .1672 .0908 .0583 .2569 #3 123.64 8.0680 6.5979 .1909 .0902 .0577 .2538 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Analysis Report 06/20/07 03:21:.49 PM .1040 Low 0560 Elem T11908 v Zn Pb2203 Sb2068 Se1960- - Units ppb ppm ppm ppb ppb ppb Avge 23.164 .1100 .0455 5.8582 123.00 7.5463 SDev 1.575 .0011 .0004 1.9208 .56 1.2533 %RSD 6.7994 1.032 .8695 32.789 .45230 16.608 ##1 24.961 .1109 .0456 6.7901 123.39 8.9644 ##2 22.021 .1104 .0459 7.1353 122.36 L6.5872 ##3 22.511 .1087 .0451 3.6492 123.24 7.0874 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 30.000 .1300 .0520 9.0000 180.00 13.000 Low 10.000 .0700 .0280 3.0000 60.000 7.0000 page 2 Analysis Report 06/20/07 03:29:21 PM page 1 N od: CLP1 Sample Name: ICSAF Operator: MAG R- Time: 06/20/07 15:21:56 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm Ppm Ppm Avge .04634 489.3 -.63309 -.0060 .0018 .0003 503.3 SDev .21134 11.0 2.61991 .0004 .0001 .0000 12.0 %RSD 456.05 2.257 413.83 7.442 7.226 10.67 2.390 #1 .10639 501.7 1.1847 -.0058 .0020 .0003 516.7 #2 -.18853 485.7 -3.6362 -.0057 .0018 .0003 499.9 #3 .22116 480.5 .55217 -.0065 .0018 .0003 493.3 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm -.0001 ppm -.0040 Ppm 199.8 ppm .0389 Ppm 508.7 Avge SDev .0039 .0004 .0034 .0005 .0005 .0017 5.0 .0088 9.2 - %RSD 10.65 14.74 361.2 43.19 2.505 22.66 1.801 #1 .0034 .0039 .0004 -.0020 205.4 .0488 519.0 .0029 -.0003 -.0046 198.3 .0363 506.0 .0040 .0042 .0033 -.0005 -.0053 195.7 .0317 501.3 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm Ppm -.0045 ppm ppm .0028 ppb 6.5510 Ppb -10.318 ppb 3.2204 Avge SDev .0106 .0011 .0358 .0062 .0005 2.2890 2.534 5.4530 %RSD .0005 4.982 24.92 17.39 18.76 34.942 24.561 169.33 #1 .0107 -.0048 .0425 .0022 8.5844 -13.239 -.33275 #2 .0101 -.0033 .0348 .00.29 6.9967 -8.7000 9.4989 #3 .0112 -.0055 .0302 .0033 4.0719 -9.0155 .49514 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ' ppb Ppb ppm ppm Ppm ppm Avge -.25365 3.6959 .32676 .0257 .0084 -.0093 .0031 SDev 2.01996 3.9187 .36249 .0028 .0017 .0033 .0004 %RSD 796.37 106.03 110.93 10.84 20.51 35.72 11.80 -.60350 3.7240 .01932 .0289 .0068 -.0126 .0035 -2.0758 -.23682 .23449 .0241 .0082 -.0094 .0028 ##3 1.9184 7.6004 .72646 .0241 .0102 -.0059 .0029 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK knalysis Report 06/20/07 03:29:21 PM ---1 -1 Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm Ppm ppb Ppb Ppb Avge -2.3599 .0048 -.0020 -4.7005 .90323 1.4487 SDev 7.6593 .0005 .0001 1.2499 1.2381 1.4787 %RSD -324.56 9.557 7.463 26.590 137.08 102.07 #1 -6.6875 .0043 -.0021 -5.9714 -.51334 1.2530 42 -6.8758 .0051 -.0021 -3.4728 1.7786 .07755 #3 6.4837 .0050 -.0018 -4.6572 1.4444 3.0155 Errors LC Pass- LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 Analysis Report 06/20/07 03:36:53 PM page 1 M id: CLP1 Sample Name: ICSABF Operator: MAG R-___ Cime: 06/20/07 15:29:27 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm ppm Ppm 532.1 Avge 1116.6 511.7 1180.6 1.103 .5485 .5335 .0071 7.9 SDev %RSD 16.4 1.4662 8.1 1.592 19.1 1.6155 .012 1.056 .0090 1.642 1.328 1.483 ##1 1128.4 518.0 1194.0 1.110 .5558 .5382 537.4 #2 1123.6 514.5 1189.2 1.109 .5512 .5369 535.9 #3 1097.9 502.5 1158.8 1.089 .5384 .5253 523.0 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm ppm PPM 209.7 ppm .0412 PPM 534.1 Avge 1.022 .5205 .5189 .0068 .5885 .0069 3.7 .0051 5.8 SDev %RSD .020 2.002 .0056 1.077 1.308 1.169 1.778 12.44 1.077 ##1 1.041 .5231 .5233 .5920 212.7 .0466 537.5 "- 1.025 .5244 .5222 .5929 210.8 .0404 537.3 1.0000 .5141 .5111 .5806 205.5 .0365 527.5 Errors LC Pass LC Pass LC Pass LC Pass 'LC Pass NOCHECK LC Pass 600.0 High 1.200 .6000 .6000 .6000 240.0 400.0 Low .8000 .4000 .4000 .4000 160.0 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm ppm ppm ppm Ppb Ppb 1079.5 ppb -10.125 Avge .5270 1.048 .7855 1.020 1272.9 12.0 13.4 1.626 SDev .0074 .016 1.557 .0069 .022 2.126 .94443 1.2394 16.062 %RSD 1.399 .8793 #1 1.060 .7856 1.039 1266.8 1088.2 -11.308 #2 .5319 1.055 .7924 1.024 1286.8 1086.2 -10.796 #3 .5306 .5185 1.030 .7786 .9965 1265.2 1064.1 -8.2702 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb ppm Ppm 1.116 PPM PPM 1.278 Avge -16.894 1150.1 1116.6 .3860 .3128 .018 SDev 2.550 13.3 1.1543 17.4 1.5565 .0089 2.301 .011 .9502 .0058 1.855 1.402 %RSD 15.096 -14.927 1152.7 1121.4 .3911 1.117 .3160 1.295 -19.775 1161.8 1131.1 .3911 1.126 .3163 1.281 #3 -15.980 1135.7 1097.4 .3757 1.105 .3061 1.259 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 03:36:53 PM .L J. �'dIZ Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm Ppm Ppb ppb ppb Avge 1068.5 .5346 1.117 1143.9 -14.640 1127.8 SDev 17.1 .0075 .014 11.4 1.864 16.0 %RSD 1.5971 1.399 1.227 .99912 12.735 1.4192 #1 1080.3 .5397 1.126 1147.7 -13.722 1131.8 #2 1076.2 .5381 1.124 1153.0 -16.785 1141.3 #3 1048.9 .5260 1.101 1131.1 -13.413 1110.1 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 O O Analysis Report 06/20/07 03:44:25 PM page 1 P od: CLP1 Sample Name: CCV4 Operator: MAG I---- Time: 06/20/07 15:36:59 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1004.0 48.34 534.16 2.564 2.526 2.553 48.70 SDev 18.0 .91 16.63 .052 .046 .045 .86 %RSD 1.7960 1.885 3.1142 2.035 1.825 1.768 1.770 #1 985.67 47.43 515.01 2.511 2.479 2.508 47.85 #2 1004.7 48.33 542.38. 2.565 2.527 2.554 48.67 #3 1021.7 49.25 545.08 2.615 2.571 2.598 49.57 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.473 2.551 2.506 2.586 48.44 84.63 52.33 SDev .032 .051 .048 .058 .78 1.76 1.04 %RSD 1.309 2.004 1.903 2.234 1.601 2.082 1.991 #1 2.442 2.499 2.457 2.525 47.69 82.83 51.26 2.469 2.552 2.507 2.591 48.40 84.69 52.38 2.507 2.601 2.552 2.640 49.24 86.36 53.34 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.497 2.452 82.33 2.477 600.94 520.65 1009.5 SDev .047 .047 2.51 .039 21.01 3.89 16.6 %RSD 1.866 1.905 3.054 1.559 3.4959 .74761 1.6485 ##1 2.450 2.406 79.56 2.439 577.06 517.89 992.99 ##2 2.499 2.450 82.98 2.475 609.20 518.97 1009.3 #3 2.543 2.499 84.46 2.516 616.57 525.10 1026.3 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb ppm Ppm PPM PPM Avge 997.24 544.26 523.37 2.620 2.592 2.542 3.009 SDev 24.20 14.76 15.13 .053 .062 .050 .032 %RSD 2.4265 2.7122 2.8914 2.041 2.410 1.980 1.068 972.64 527.84 5.05.89 2.567 -2.526 2.490 2.982 998.08 548.51 531.82 2.621 2.598 2.546 3.001 #3 1021.0 556.43 532.38 2.674 2.651 2.590 3.045 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 03:44:25 PM h Low Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 509.62 2.525 2.588 547.39 .1001.3 530.32 SDev 8.85 .046 .047 9.10 21.7 14.90 %RSD 1.7360 1.810 1.824 1.6615 2.1649 2.8103 #1 500.44 2.479 2.540 537.59 979.41 513.20 $#2 510.33 2.525 2.589 549.02 1001.8 537.38 43 518.09 2.570 2.634 H555.56 1022.8 540.39 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report M )d: CLP1 Sample Name: CCVL4 R Cime: 06/20/07 15:44:31 ppm Comment: PPM .0061 .0007 Mode: CONC Corr. Factor: 1 .0017 Elem Ag Al As1890 Units ppb ppm ppb Avge -.35356 -.0222 .14221 SDev .19943 .0144 1.6293 %RSD 56.406 64.95 1145.7 ##1 -.31137 -.0059 -.13213 ##2 -.57071 -.0273 -1.3325 ##3 -.17860 -.0333 1.8913 Errors NOCHECK NOCHECK NOCHECK High .0115 .0133 5.659 Low 19.81 226.6 .0020 Elem Cd Co Cr Units ppm ppm* ppm Avge .0012 .0005 .0006 SDev .0004 .0001 .0003 %RSD 33.61 25.40 39.00 #1 .0016 .0006 .0009 '- .0010 .0004 .0005 ppb .0009 .0004 .0005 Errors NOCHECK NOCHECK NOCHECK High .95707 3.4246 47.28 Low 194.77 67.530 .0014 .0014 Elem Mn -1.3171 .0005 1.9057 -1.3532 -5.8723 .0010 -2.0031 .53863 -8.0243 -1.9441 -1.3004 ##3 -4.2022 Errors NOCHECK Mo ppm .0104 .0046 44.66 .0155 .0091 .0065 NOCHECK 1960/1 ppb 2.7682 1.2666 45.756 4.0846 2.6618 1.5582 NOCHECK Na ppm 2.727 .032 1.184 H2.750 2.740 2.690 LC Pass High 2.750 Low 2.250 1960/2 ppb 1.7383 2.1758 125.16 3.7839 -.54763 1.9787 NOCHECK 06/20/07 03:51:56 PM page 1 Operator: MAG B Ba Be Ca ppm ppm ppm PPM .0061 .0007 .0008 -.0004 .0017 .0001 .0002 .0130 27.67 19.85 26.23 2948. :0079 .0009 .0010 .0142 .0058 .0006 .0007 -.0052 .0046 .0006 .0006 -.0104 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg ppm ppm ppm ppm .0019 2.579 .0581 .0059 .0001 .039 .0115 .0133 5.659 1.494 19.81 226.6 .0020 2.617 .0708 .0208 .0018 2.580 .0485 .0016 .0019 2.540 .0549 -.0048 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 220.3/2 2068/1 ppm ppb ppb - ppb .0009 -1.2602 -.49139 -5.0712 .0004 2.8675 .95707 3.4246 47.28 227.55 194.77 67.530 .0014 .0014 -3.6831 -.65959 -1.3171 .0005 1.9057 -1.3532 -5.8723 .0010 -2.0031 .53863 -8.0243 NOCHECK NOCHECK NOCHECK NOCHECK Si Sn Sr Ti ppm ppm ppm ppm .0076 .0003 .0007 .0012 .0011 .0025 .0002 .0004 14.28 761.8 25.53 36.53 .0078 .0032 .0009 .0017 .0086 -.0011 .0006 .0010 .006.5 -.0011 .0006 .0009 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 03:51:56 PM page 2 _ 1 Zn Low Sb2068 Elem T11908 Units ppb Avge 1.0201 SDev 1.2797 %RSD 125.45 #1 1.3087 #2 2.1308 #3 -.37922 Errors NOCHECK High 57.519 Low .0012 V Zn Pb2203 Sb2068 Se1960 Ppm PPM Ppb Ppb Ppb .0013 .0024 -.74732 -3.3443 2.0813 .0002 .0003 .79615 1.9236 1.6946 15.59 12.50 106.53 57.519 81.419 .0012 .0027 -1.6664 -1.7352 3.8841 .0012 .0023 -.26792 -2.8228 .52109 .0015 .0021 -.30769 -5.4749 1.8387 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 06/20/07 03:59:28 PM page 1 V od: CLP1 Sample Name: CCB4 Operator: MAG F, Time: 06/20/07 15:52:03 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb ppm ppm ppm ppm Avge -.52482 -.0617 -.39649 .0027 .0003 .0001 -.0400 SDev .17900 .0032 2.13839 .0006 .0001 .0000 .0014 %RSD 34.106 5.246 539.33 22.37 25.80 27.98 3.577 #1 -.62101 -.0580 -1.3822 .0029 .0003 .0002 -.0407 #2 -.31830 -.0630 -1.8642 .0032 .0002 .0001 -.0384 #3 -.63515 -.0641 2.0570 .0021 .0002 .0001 -.0410 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd 'Co Cr Cu Fe K Mg Units ppm- ppm -.0000 ppm -.0001 ppm .0016 ppm -.0147 Ppm .0474 ppm -.0461 Avge SDev .0004 .0000 .0004 .0002 .0003 .0009 .0102 .0007 %RSD 5.742 1115. 291.0 22.06 6.010 21.57 1.449 #1 .0004 .0001 .0001 .0015 -.0142 .0564 -.0456 - -.0004 -.0001 .0013 -.0141 .0363 -.0459 .0004 .0004 .0002 -.0002 .0020 -.0157 .0496 -.0469 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm -.0004 ppb 1.0082 ppb -1.1431 ppb -8.6187 Avge SDev .0003 .0028 .0007 .0159 .0014 .0005 2.1559 1.1269 1.3278 %RSD .0001 30.42 25.94 8.752 116.7 213.84 98.575 15.406 #1 .0004 .0035 .0167 .0001 2.9188 -2.4419 -8.8321 #2 .0003 .0026 .0168 -.0004 -1.3292 -.42545 -7.1971 #3 .0002 .0021 .0143 -.0010 1.4351 -.56204 -9.8269 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr 'Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -5.8053 .31362 1.0638 .0046 -.0010 .0002 .0003 SDev 3.0506 3.1995 1..0748 .0021 .0009 .0000 .0002 %RSD 52.548 1020.2 101.03 45.93 83.46 18.95 71.98 -3.0502 3.3057 1.0619 .0029 -.0001 .0003 .0005 -9.0837 .69433 -.01003 .0070 -.0013 .0002 .0001 43 -5.2819 -3.0592 2.1395 .0040 -.0017 .0002 .0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK- NOCHECK NOCHECK NOCHECK knalysis Report 06/20/07 03:59:28 PM Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm Ppb ppb ppb Avge .75113 .0001 -.0036 -.42670 -6.7421 .81397 SDev 2.9933 .0006 .0001 .46009 1.7405 .86665 %RSD 398.50 492.5 1.413 107.82 25.816 106.47 #1 -2.2690 -.0006 -.0037 -.65678 -4.9756 1.8091 #2 3.7167 .0005 -.0036 -.72637 -8.4554 .22453 #3 .80565 .0005 -.0036 .10304 -6.7954 .40834 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 v2M l us3 Isco IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING- ANALYST SIGNATURE PAGE 1H2M Labs, Inc. CLP Digestion Log o� Client: PGS Analyst Si nature: SDG #: fish I C7 Date: 1 q O QQ Time StartedlEnded: Matrix. Method: Zn 1 p A Sample ID # -�J LAS -5b SS Ub A Description t Comments: d N PH: •Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. O 'Description of texture: fine, medium, coarse. - O `.Description of clarity: clear, cloudy, opaque. `Description of artifacts: yes or no and describe C!� O:/QCBOOKS(CLPDigestionlog iyy Nis mm t Comments: d N PH: •Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. O 'Description of texture: fine, medium, coarse. - O `.Description of clarity: clear, cloudy, opaque. `Description of artifacts: yes or no and describe C!� O:/QCBOOKS(CLPDigestionlog iyy U2M "US, INC. SDG NO.: i Sl-oi SCAN: LE7zVU.S This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature: Date: Tuf-llz .Reviewed By Signature: Date: - 1 22 l G`7