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HomeMy WebLinkAboutMetals Data Package 12/2005Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL004 Water Samples Received: 12/8/05 MFToi S nATA PACKAGE 1 -*t I-Aus'w I Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. SU40 11747 \!i N2M "US, INC. ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 12/8/05 SDG NO.: TSI -004 I. NYS DEC SUMMARY FORMS II. SDG NARRATIVES III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY U2M "U%s I %C. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY SDG: TSL004 Anal ical Requirements M d - O O CLP on -C Please indicate year of protocol) AS P 13 to (9s H TCUTAL, HSL, Priority Pollutant, Customer Sample Code Laboratory Sample Code ME we MW -1D 0512218-001 X X MW -1S 0512218-002 X X MW -3D 0512218-003 X X MW -3S 0512218-004 X X MW -4D 0512218-005 X X MW -4S 0512218-006 X X MW -5D 0512218-007 X X MW -5S 0512218-008 X X MW -6D 0512218-009 X X MW -6S 0512218-010 X X MW -8D 0512218-011 X X MW -8S 0512218-012 X X EQPT BLANK 0512218-013 X X M d - O O CLP on -C Please indicate year of protocol) AS P 13 to (9s H TCUTAL, HSL, Priority Pollutant, NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG. TSI -004 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0512218-001 MW -1D WATER CA,CD,FE,K,MG,MN,NA,PB, 0512218-002 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-003 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-004 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-005 MW -4D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Deo -05 12/05 0512218-006 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-006DUP MW-4SD WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-006MS MW-4SS WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-007 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-008 MW -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-009 MW -6D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-010 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-011 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-012 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-013 EQPT BLANK WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 08 -Dec -05 12/05 TSL004 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSI -004 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Tests DateRecd at Lab Date Analyze 0512218-001 MW -ID Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-002' MW -1S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05. 0512218-003 MW -31) Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-004 MW -3S Groundwater SELECT WET CHEMISTRY ** 12/08/05 12/05 0512218-005 MW4D Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-006 MW4S Groundwater SELECT WET CHEMISTRY *' 12/08/05 12/05 0512218-006DUP MW-4SDUP Groundwater SELECT WET CHEMISTRY " 12/08/05 12/05 0512218-006MS MW-4SMS Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-007 MW -5D Groundwater SELECT WET CHEMISTRY " 12/08/05 12/05 . 0512218-008 MW -5S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-009 MW -6D Groundwater SELECT WET CHEMISTRY" 12/08/05 12105 0512218-010 MW -6S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-011 MW -8D Groundwater SELECT WET CHEMISTRY ** 12/08/05 12/05 0512218-012 MW -8S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-013 EQPT BLANK Blank SELECT WET CHEMISTRY " 12/08/05 12/05 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand; Chloride; Hardness (As CaCO3) ; Nitrate as N; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable; Sulfate ; Total Dissolved Solids ; Total Organic Carbon ; U2M LAOS, INC. I1. SDG NARRATIVES U2M "US, INC. For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 12/8/05 SDG#: TSL004 EQPT BLANK MW -5D MW -11) MW -5S MW -1S MW -6D MW -31) MW -6S MW -3S MW -8D MW -41) MW -8S MW -4S MS/MSD Thirteen water samples were received by H2M Labs inc. on 12/8/05 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument. Sample MW -4S was utilized for QC analysis and reporting. ICP serial dilution analysis did not reproduce within acceptance ranges for calcium. Calcium data was reported flagged "E" on forms 1 and 9. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the follgiong signature. Date Reported: December 30, 2005 v ********************* Vincent Stancampiano Vice President o:\qc\narr2005\tsl\metals\ts1004.doc U2M L Uss INC. For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLE RECEIVED: 12/8/05 SDG#: TSL004 EQPT BLANK MW -5D MW -1D MW -5S MW -IS MW -6D MW -3D MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S MS/MSD EPA420.1 Thirteen water samples were received by H2M Labs, Inc. on 12/8/05 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: PARAMETER METHOD # PARAMETER METHOD # Alkalinity EPA 310.1 Nitrate EPA 353.2 BOD EPA 405.1 Phenols EPA420.1 Bromide EPA 320.1 Sulfate EPA 9038 Chloride EPA325.2 TDS EPA 160.1 COD EPA 410.4 TKN EPA 351.2 Hardness EPA 130.2 TOC EPA 9060 Ammonia EPA 350.1 Sample MW -4S was utilized for duplicate and spike QC analysis and reporting. Biological oxygen demand (BOD) values for samples MW -3D, MW -4D, MW -6D and MW -6S were calculated using chemical oxygen demand (COD) values. Aliquots utilized for BOD analysis depleted the oxygen content. Results reported as estimated values. Several ammonia values slightly exceeded the total kjeldahl nitrogen (TKN) values. All differences were within ± the CRDL. Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: January 4, 2006 ************************* Vincent Stancampiano Vice President gc\narr2005\ts1\wet chem\ts1004.doc 00 d - O O U2M IL AU%s INC. III. CHAIN OF CUSTODY DOCUMENTATION v� r d- UZ .K (LAPS, INC. 575 Broad Hollow Rd, Melville, NY 11747-5076 .123-3 EXTERNAL CHAIN OF CUSTODY Tel: (516) 694-3040 Fax (516) 420-W6 PROJECT NAMEMUMBER SovTK01,0 uFnro Fll.L_ ,4#X 7- 36,0�ov'T7nr� CLIENT: C o aa E co fGTS -_ * .� h a L., O y � f O 4 1H2M SDG NO: NOTES: Project Contact: f30 8�� c �' Ic Phone Number: C. SO l48N- lk '1DS TaX � SAMPLERS: (signatureyClient Ham DELIVERABLES: 70 �� ® Z t- v 1 ANALYSIS REQUESTED TURNAROUND TIME: A DAY -5 ORGANIC INORG. DATE TIME MATRI FIELD I.D. �° ;� $ _ U LAB I.D. Normo REMARKS: I k � MVV - IS 3 I 1 I Q 1 - 1 MWID 1030 M w - 3S 1100 MW - 3D 7 - / Mw— 4S 3 M5/ MSD MW - L4D 8 4 1 1 , E 3 a 1- Relinquished by: (Signature) -.0001110 Date n Timeby: !1 X53/A Signatu at � ii LABORATORY USE ONLY ancies Between Sample Labels and COC Record? Y or N Explain: Samples were: 1. Shipped_ or Hand Delivered Airbilltl 2. Ambient or chilled SAMLf ?QtLLJ'r lam. wF1Tt 3. Received in good conditio : Y or N 4. Property preserved:r N 5. Samples returned to ab HB from collection. COC Tape was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y or N 3. COC record present d complete upon sample receipt; YorN Relinquished by: (Signature) Dale Time Received by: (Slgnatu ) 10afte Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by, (Signature) Date Time ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY 1-121 ILAUS, INC. 575 Broad Hollow Rd, Melville, NY 11747-5076 1233 EXTERNAL CHAIN OF CUSTODY Tel. (07 0) 6943040 Fax. (516) 420-8436 CLIENT: .. L H2M SDG NO. PROJECT NAMEMUMBER r yw` 00 J Q ;?00 o E a J � I,ct,qz�C J J NOTES: Project Contact: A,�' (nom n /� J'F � ��'�S Phone Number. SAMPLERS: (signatureyClient NaM DELIVERABLES: d c° z 3 o V �► ANALYSIS RE ESTED TURNAROUND TIME: O�L ^ 4� ORGANIC INORG. DATE TIME Aa MATRI � Vj FIELD I.D. � 5L MW- SD ' �- 3 ) Z v LAB I.D. NO. c5/ REMARKS: 121 M —150 1z IM MWZ-ilp 4/330 - MW - & W" �l Relinquished by: mign ) Date Time by: (S lure) DV Time LABORATORY USE ONLY Discrepancies Between Sampl@ Labels and COC Record? Y or N Explain: Samples were: 1. Shipped_ or Hand Delivered_ Airbill# 2. Ambient or chilled SR �9fl O �g 3. Received in good conditio Y or N a. Properly preserved: Y or N CoL.1 5. Samples returned to lab _ Hrs from collection. COC Tape was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y or N 3. COC record present b complete upon sample receipt: YorN Relinquished by: (Signature) Difte Time R to a ime Relinquished by: (Signature) Date Time Received by. (Signature) Date Time Relinquished by: (Signature) Date T CIT. L]L1A -ti 1 1 Time Recelwd b S Y (Signature) Date Time 1 cMR)f - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATnRY 7 r_CC11_ H2M LABS, INC. Client Name PCTSL Work Order Numbe Checklist completed b Matrix Sample Receipt Checklist Date and Time Receive 12/8/2005 11:53:00 AM Received by BGL Reviewed by � MCO 1 Indials ate Shipping container/cooler in good condition? Yes No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable 91 Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable d❑ Chain of custody present? Yes 0 No Chain of custody signed when relinquished and received? Yes © No ❑ Chain of custody agrees with sample labels? Yes © No ❑ Samples in proper container/bottle? Yes 66 No ❑ Sample containers intact? Yes ® No ❑ Sufficient sample volume for indicated test? Yes No ❑ .Iamples received within holding time? Yes © No ❑ Container/Temp Blank temperature in compliance? Yes No ❑ Water - VOA vials have zero headspace? No VOA vials submitted © Yes ❑ No CJ Water - pH acceptable upon receipt? Yes d❑ No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section b — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - Client contacted Contacted by: Comments: Date contacted: Regarding Person contacted L % _It, m� � t t I ©� _ Y ` dfla E7�R GMM X17— N't D tm rr� A{ii L Corrective Action N O 0 Nom►1AFS, INC. INTERNAL CHAIN OF CUSTODY CLIENT: DELIVERABLES: nn"ARMMT&M- SDG 11 CASE it: MATRIX: ltl(v x REMARKS: � NXM'W Br 'Z SIGNKJURE m4on ME1'AI,S =min HIM K -W, WHIEFEWFA HIM MEMI h- w,.. EMEMMI m 0 m WE I W.- HIM m lm�MMM khm1b, NAME HE a, �MMIM MEN 120mmi.EMINIME MEIN 0101 MW ME1'AI,S NWM UAUS, wc. CLIM: t J 3DO INTERNAL CHAIN OFCIISTODY METALS U2A tAIUS, mac. INTERNAL CHAIN OF CUSTODY CLIENT:! DELIVERABLES TURN AROUND TIINE:. SDG 0: CASE 0��_ MATRIX: pH CWCX. REMARKS: CryL 05 w✓ RECEIVED BY: SIGNATURE_ DATF--lAn6B61F-- WET CHEMISTRY 0 _. P 0163 lip INK iFe "Immmm���� immm OEM IMMEEKAM immomim immommom Immommom lmmmmmmm��� WET CHEMISTRY 0 _. P 0163 r OAFS, INC. INTERNAL. CHAIN OF. CUSTODY WET CHEMISTRY- _- P Oi64 d - CD 2M �,AI3S, jht*4jC4,- CLIE TT: SDO 1 • AQ q INTERNAL CHAIN OF. CUSTODY WET CHEMISTRY - U2M "U%s INC. IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY U2M "US. INC. i SLOo%j TABLE OF CONTENTS I. REPORTS II. QC SUMMARY 111. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 SOW No.: ILM04.1 EPA Sample No. Lab Sample ID. EQPT BLANK 0512218-013 MW -1D 0512218-001 MW -1S 0512218-002 MW -3D 0512218-003 MW -3S 0512218-004 MW -4D 0512218-005 MW -4S 0512218-006 MW-4SD- 0512218-006DUP MW-4SS 0512218-006MS MW -5D 0512218-007 MW -5S 0512218-008 MW -6D 0512218-009 MW -6S 0512218-010 MW -8D 0512218-011 MW -8S 0512218-012 Were ICP interelement corrections applied? Yes/No YES Were ICP backqround corrections applied? Yes/No YES If yes -were raw data generated before application of background corrections? Yes/No NO Comments: Date Reported: 12/19/05 I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditionsVature ove. Release of the data contained in this hardcopy data package and r -readable data submitted on diskette has been authorized bry Manaqer or the Manaqer's desiqnee, as verified by the followi Signature: 1 Name: Vincent Stancampiano "iIDate: \�1�'1� \ Title: Vice President COVER PAGE - IN ILM04.1 U2M "US, 1%C. REPORTS FOR METALS U2A LAUSo INC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. Lab Name: H2M LABS, INC. Lab Code: 10478 Case Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Contract: �. SAS No.: Lab Sample ID: Date Received: Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. i Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 626 B E P 7439-89-6 Iron 165 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 170 B P 7439-96-5 Manganese 3.3 B P 7440-09-7 Potassium 361 B P 7440-23-5 Sodium 21000 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/19/05 EPA SAMPLE NO MW -1D SDG No.: TSL004 0512218-001 12/8/2005 Texture: Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 MW -1S Contract: SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-002 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 444 B E P 7439-89-6 Iron 78.7 B P 7439-92-1 Lead 1.4 B P 7439-95-4 Magnesium 122 B P 7439-96-5 Manganese 1.8 B P 7440-09-7 Potassium 351 B P 7440-23-5 Sodium 21100 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/19/05 FORM I - IN Texture: Artifacts: ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case Matrix (soil/water): WATER Level (low/med): LOW Solids: 0.0 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -3D Contract: �. SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-003 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 988 B E P 7439-89-6 Iron 199 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 1170 B P 7439-96-5 IManganese 4.1 B P 7440-09-7 lPotassium 6610 P 7440-23-5 ISodium 23100 P Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: Date Reported: 12/19/05 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 O O N U.S. EPA = CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 618 B E P 7439-89-6 Iron 171 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 155 B P 7439-96-5 Manganese 2.8 B P 7440-09-7 Potassium _ 333 B P 7440-23-5 Sodium 20300 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/19/05 EPA SAMPLE NO MW -3S SDG No.: TSL004 12/8/2005 Texture: Artifacts: FORM I - IN ILM04.1 00 O O C4 F-+ U:S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P 7440-70-2 Calcium 1440 B E MW -4D Lab Name: H2M LABS, INC. Contract: P 7439-92-1 Lead Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-005 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Potassium 7630 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 1440 B E P 7439-89-6 Iron 222 P 7439-92-1 Lead 1.8 B P 7439-95-4 Magnesium 676 B P 7439-96-5 Manganese 11.6 B P 7440-09-7 Potassium 7630 P 7440-23-5 Sodium 24500 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/19/05 Texture: Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP . 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.58 B P 7440-70-2 Calcium 1320 B E P 7439-89-6 Iron 190 P 7439-92-1 Lead 2.3 B P 7439-95-4 Magnesium 601 B P 7439-96-5 Manganese 10.4 B P 7440-09-7 Potassium 6600 P 7440-23-5 Sodium 23100 P EPA SAMPLE NO MW -4S SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS. DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 SAS No.: Lab Sample ID: Date Received: Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 740 B E P 7439-89-6 Iron 241 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 187 B P 7439-96-5 Manganese 3.2 B P 7440-09-7 Potassium 3601 B I P 7440-23-5 Sodium 213001 P EPA SAMPLE NO MW -5D SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 752 B E P 7439-89-6 Iron 239 P 7439-92-1 Lead 1.4 B P 7439-95-4 Magnesium 187 B P 7439-96-5 Manganese 3.2 B P 7440-09-7 Potassium 362 B P 7440-23-5 Sodium 21200 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 12/19/05 EPA SAMPLE NO MW -5S SDG No.: TSL004 12/8/2005 Texture: Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 Contract: EPA SAMPLE NO MW -6D SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-009 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 17440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 1160 B E P 7439-89-6 Iron 228 P 7439-92-1 Lead 1.8 B P 7439-95-4 iMagnesium 464 _ B P 7439-96-5 Manganese 7. 1 P 7440-09-7 Potassium 5390 P 7440-23-5 Sodium 22600 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 Contract: SAS No.: Lab Sample ID: Date Received: Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 iCadmium 0.26 U P 7440-70-2 Calcium 847 B E P 7439-89-6 Iron 188 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 249 B P 7439-96-5 Manganese 3.9 B P 7440-09-7 Potassium 1600 B P 7440-23-5 Sodium 20900 P EPA SAMPLE NO MW -6S SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID Level (low/med): LOW Date Received % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 759'B E P 7439-89-6 Iron 242 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 187 B P 7439-96-5 Manganese 3.1 B P 7440-09-7 Potassium _ 348 B P 7440-23-5 Sodium 20500 P EPA SAMPLE NO MW -8D SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 N FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level .(low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 740 B E P 7439-89-6 Iron 244 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 183 B P 7439-96-5 Manganese 3.0 B P 7440-09-7 Potassium 336 B P 7440-23-5 Sodium _ 20800 P EPA SAMPLE NO MW -8S SDG No.: TSL004 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 EQPT BLANK Contract: SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-013 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 112 B E P 7439-89-6 Iron 5.8 B P 7439-92-1 Lead 1_3 U P 7439-95-4 Magnesium 5.2 U P 7439-96-5 Manganese 0.40 U P 7440-09-7 Potassium 63.4 B P 7440-23-5 Sodium 354 B P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 .FORM I - IN ILM04.1 u2M "uso 1NC. II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TS1,004 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration True Found %R(l) True Continuing Calibration Found %R(1) Found %R(1) M Cadmium 2500.0 2280.67 91.2 2500.0 2452.60 98.1 2421.09 96.8 P Calcium 50000.0 49826.35 99.7 50000.0 52588.56 105.2 51938.83 103.9 P Iron 50000.0 49335.83 98.7 50000.0 52174.73 104.3 51581.66 103.2 P Lead 500.0 483.58 96.7 500.0 510.27 102.1 501.38 100.3 P Magnesium 50000.01 50285.15 1 100.6 50000.0 53216.74 106.4 52283.00 104.6 P Manganese_ 2500.0 2286.68 91.5 2500.0 2455.25 98.2 2423.70 96.9 P Potassium 80000.0 .82136.95 102.7 80000.0 86854.62 108.6 86491.61 108.1 P Sodium 80000.0 79772.43 99.7 80000.0 83553.21 104.4 83153.12 103.9 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 CN d' FORM II (Part 1) - IN ILM04.1 O O i � U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract.:. Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Cadmium 2500.0 2429.62 97.2 2470.81 98.8 P Calcium_ 50000.0 52255.59 104.5 53118.06 106.2 P Iron 50000.0 51811.72 103.6 52641.04 105:3 P Lead 500.0 504.86 101.0 511.89 102.4 P _ Magnesium 50000.0 52610.27 105.2 53684.68 107.4 P Manganese _ 2500.0 1 2435.70 97.4 2474.29 99.0 P Potassium 180000.0 87311.76 109.1 88266.46 110.3 P Sodium 180000.01 83943.47 104.9 84638.75 105.8 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N d' FORM II (Part 1) - IN ILM04.1 O O H U.S. EPA - CLP 2A INITIAL AND CONTINUI.NG CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Analyte True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Iron 2500.0 2443.87 97.8 2500.0 2517.28 100.7 2565.42 102.6 P Sodium 2500.0 2531.98 1 101.3 2500.0 2592.62 103.7 2672.77 106.9 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TS1,004 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M Iron 2500.0 2520.73 100.8 2497.33 99.9 P Sodium 2500.0 2651.45 106.1 2634.03 105.4 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N FORM II (Part 1) - IN ILM04.1 O O F-+ U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AA CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purit Concentration Units: ug/L SDG No.: TSL004 Analyte CRDL Standard for AA CRDL Standard Initial True Found %R True Found %R for ICP Final Found %R Cadmium 10.0 9.81 98.1 10.05 100.5 Lead _ 6.0 6.19 103.1 6.54 109.0 Manganese 30.0 28.80 96.0 29.48 98.3 FORM II (Part 2) - IN ILM04.1 U.S. EPA - CLP. 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Analyte Initial Calib. Blank (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 C Prepa- ration Blank C M Cadmium 0.3 U 0.3 U 0.3 U 0.3 U 0.2621 U 11P Calcium 33.8 B 42.6 B 32.3 B 32.6 B 117.000 B P Iron 4.3 U 6.9 B 4.3 U 4.3 U 27.600 B P Lead 1.3 U 1.3 U 1.3 U 1.3 U 1.290 U P Magnesium 5.2 U 10.5 B 5.2 U 5.2 U 11.500 B P Manganese 0.4 U 0.4 U 0.4 U 0.4 U 0.410 B P Potassium 45.1 B 41.6 B 45.51 B 48.5 B 174.000 B P Sodium16.8 U _ 17.9 B 26.1 B 23.1 B 45.900 B P FORM III - IN d' N ILM04.1 O O V1 H U.S. EPA - CLP' 3 BLANKS. Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Analyte Initial Calib. Blank (ug/L) C Continuing Calibration Blank (ug/L) 1 C 2 C 3 Prepa- ration C Blank C M Cadmium 0.3 U P Calcium 51.0 B P Iron_ — -- 9.6 B P Lead _ 1.3 U P Magnesium _ 1_8.1 B P Manganese Potassium _ 0.4 U P 48.6 B P Sodium -- — 22.8 B -- P FORM III - IN N ILM04.1 V) U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA ICS Source: MV ,Labs/High Purity Concentration Units: ug/L True Initial Found Final Found Sol. Sol. Sol. Sol. Sol. Sol. Analyte A AB A AB %R A AB %R Aluminum 500000 Cadmium �— _500000_ 511179 495237.7 940.5 99.0 505283 94.0 496042.0 935.2 99.2 93.5 [Calcium — 500000 _10001 500000 512498 498709.4 99.7 504841 497860.0 99.6 Iron 200000 -� 200000 205975 199969.0 100.0 202343 198924.1 99.5 Lead _ 1 _1000 1019.5 101_.9 1013.6 101.4 Magnesium 500000 1500000 51442_5 499914.9 477.6 100.01 507651 95,51 498708.01 1 476.41 99.7 95.3 Manganese 500 FORM IV - IN ILM04.1 E"I Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO MW-4SS SDG No.: TSL004 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit %R Spiked Sample Result (SSR) C Sample Result (SR) C Spike Added (SA) %R Q M Cadmium 75-125 48.1200 0.5800 B 50.00 95.1 P Iron 75-125 1.164.5300 189.9200 1000.00 97.5 P Lead _ 75-125 22.1529 2.3099 B 20.00 99.2 P Manganese 75-125 492.7300 10.3900 B 500.00 96.5 P ------ -- - --- Comments: FORM V (Part 1) - IN Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES Mw -4s Contract: SAS No.: SDG No.: TSL004 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q M Cadmium 5.0000 0.5800 B 0.2616 U 200.0 P Calcium 5000.0000 1324.0900 B _ _ 1492.9500 B 12.0 P Iron 100.0000 189.9200 196.6500 3.5 1 P Lead Magnesium 3.0000 I 5000.0000 _ _ 2.3099 B, _ 1.8184 600.9300 B 639.6200 B11 B 1 23.8 6.2 1 P P Manganese 15.0000 10.3900 B _ 10.7700 B 3.6 P Potassium 5000.0000 6598.0000 7142.9200 7.9 P Sodium 5000.0000 23086.6800 24932.4500 7.7 P FORM VI - IN ILM04.1 00 N O O DO F-+ Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA _ CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSL004 Analyte Aqueous (ug/L) True Found %R Solid (mg/kg) True Found C Limits %R Cadmium 2500.0 2429.91 97.2 Calcium 50000.0 54107.11 108.2 _ Iron 50000.0 52681.79 105.4 Lead 500.0 504.32 100.9 Magnesium 108 .7 Manganese _5_0000.0 —54328.16 2500.0 2458.10 98.3 Potassium 80000.0 105.3 Sodium 80000.0 _84242.68 86266.48 107.8 FORM VII - IN Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No.: Concentration Units: ug/L SDG No.: TSL004 EPA Sample 0 ADD 1 ADD 2 ADD 3 ADD Final No. An ABS CON_ ABS CON ABS CON ABS i Conc. r Q — _ FORM VIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Contract: SAS No.: Concentration Units: ug/L MW -4S SDG No.: TSL004 Level (low/med): LOW Analyte .Initial Sample Result (I) C Serial Dilution Result (S) C Differ - i ence Q M Cadmium 0.58 B 1.30 U 100.0 P Calcium 1324.09 B 1537.65 B 16.1 E P Iron 189.92 197.20 B 3.8 P Lead 2.31 B 6.50 U 100.0 P Ma nesium 600.93 B 629.95 B 4.8 P Man anese 10.39 B 11.00 B 5.9 P Potassium _ 6598.006679.45 B 1.2 P Sodium 23086.68 23658.95 B2.5 P _ FORM IX - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 10/3/2005 Flame AA ID Number: Furnace AA ID Number: Comments: Analyte Wave- length Back- (nm) ground CRDL (ug/L) IDL (ug/L) M Cadmium 226.50 5.0 0.3 P Calcium 317.93 5000.0 4.7 P _ Iron _ jLead 259.90 100.0 _ 4.3 P _ _ 220.35 3.0 1.31 P Ma nesium 279.08 5000.0 5.2 P Manganese 257.61 15.0 _ _ 0.4 P Potassium 766.49 5000.0 19.6 P Sodium 588.90 5000.0 16.8 P FORM X - IN N M+ C 7t ILM04.1 p V1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Aluminum j 308.22 0.0000000 0.0000000 0.0000000 0.0000000 -0.0170000 Antimony 206.84 0.0000000 0.0000000 0.0274000 0.0000000 0.0000000 Antimony 206.84 0.0000000 0.0000000 0.0380000 0.0000000 0.0000000 Arsenic 189.041 0.0127000 0.0000000 -0.0100000 0.0000000 -0.2470000 Barium 493.41 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Boron 249.68 0.0000000 0.0000000 -0.0004000 0.0000000 0.0017000 Cadmium 226.50 0.0000000 0.0000000 0.0001000 0.0000000 0.0000000 Calcium 317.93 0.0003000 0.0000000 0.0002000 0.0000000 0.0000000 Chromium_ 267.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 jCobalt 228.62 _ 0.0000000 0.0000000 0.0000200 0.0000000 0.0000000 Copper _324.75 �259.94� 0.0000000 0.0000000 -0.0000400 0.0000000 -0.0004000 Iron _ _ 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 271.44 0.0000000 0.0000000 0.0000000 0.0000000 0.0920000 Lead 220.35 -0.2670000 0.0000000 0.0900000 0.0000000 0.0890000 Lead 220.35 0.4000000 0.0000000 0.2200000. 0.0000000 0.0900000 Ma nesium 279.08 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese 257.61 -0.0001200 0.0000000 0.0000400 0.0000000 -0.0002000 Molybdenum 202.03 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 -0.0004200 Potassium 766.49 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 -0.0063000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.0000000 0.0000000 0.3540000 Silicon 288.16 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Silver 328.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 330.23 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 589.00 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Strontium 1 407.77 0.00000001 0.00000001 0.0000000 0.0000000 0.0000000 Thallium 1 190.86 0.00000001 0.0000000 -0.3600000 0.0000000 -0.5800000 Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS,, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Tin 189.99 0.0000000 0.0000000 -0.0004000 0.0000000 0.0000000 Titanium 334.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000500 Vanadium 1 292.40 0.0000000 0.0000000 0.0000200 0.0000000 0.0000000 Zinc 213.86 0.0000000 0.0000000 0.0000250 0.0000000 0.0000000 Comments: F FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Cr Interelement Cu Correction Factors for: Mn Ni V Aluminum 308.22 0.0000000 0.0000000 -0.0012000 0.0000000 0.0000000 Antimony 206.84 7.1400000 0.0000000 -0.3830000 0.0000000 0.0000000 Antimony 206.84 8.8100000 0.0000000 0.2510000 -1.0900000 -6.3000000 Arsenic 189.04 0.2500000 0.0000000 -0.2010000 0.0000000 0.0000000 Barium 493.41 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Ber llium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0002000 Boron 249.68 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 _ Cadmium 226.50 0.0000400 0.0000000 0.0000000 -0.0001800 0.0000000 Calcium 317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0019000 Chromium 267.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0002960 Cobalt 228.62 0.0000000 0.0000000 0.0000000 0.0001700 0.0000000 Copper 324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000360 Iron 259.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 271.44 0.0000000 0.0000000 -0.0038000 0.0000000 0.0000000 Lead 220.35 0.0000000 0.0000000 0.0000000 0.1500000 -0.1900000 Lead 220.35 0.0000000 0.0000000 0.0000000 0.3000000 -0.0200000 Magnesium 279.08 -0.0001000 0.0000000 0.1400000 -0.0001000 0.0000000 Manganese 257.61 0.0000000 0.0000000 0.0000000, 0.0000000 -0.0001000 Mol bdenum 202.03 1 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Potassium 766.49 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.3250000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.4100000 0.0000000 0.0000000 Silicon 288.16 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Silver 328.07 0.0000000 0.0000000 0.1780000 0.0000000 -0.0433000 Sodium 330.23 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 589.00 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Strontium 1 407.77 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Thallium 1 190.86 0.1720000 0.0000000 -0.7417000 0.0000000 -0.9000000 Comments: FORM XI (PART 2) - IN ILM04.1 M O CD U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Cr Interelement Cu Correction Mn Factors for: Ni V Tin 189.99 -0.0001100 -0.0001000 0.0000000 0.0000000 0.0000000 Titanium 334.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Vanadium 292.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Zinc 213.86 0.0000000 0.0004000 0.0000000 0.0042000 0.0000000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 ICP ID Number: TJA6IEA Date: 11/12/2005 Comments: Analyte Integ. Time (Sec.) Concentration (ug/L) M Cadmium 15.00 20000P Calcium 15.00 1000000 P Iron 15.00 250000 P Lead 15.00 50000 P Magnesium 15.00 1000000 P Manganese 15.00 20000P Potassium 15.00 250000 P Sodium 15.00 500000P FORM XII - IN Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL004 F EPA Sample No. ---- — Preparation Weight Date (gram) Volume (mL) EQPT BLANK 12/12/2005 50 LcsW 12/12/2005 50 MW -1D 12/12/2005 50 Mw -1S 12/12/2005 50 Mw -3D 12/12/2005 50 _ Mw -3S 12/12/2005 50 MW -4D 12/12/2005 50 _ MW -4S 12/12/2005 50 MW-4SD 12/12/2005 50 MW-4SS 12/12/2005 50 _ MW -5D _ 12/12/2005 50 Mw -5S 12/12/2005 50 MW -6D 12/12/2005 50 Mw -6S 12/12/2005 50 _ MW -8D 12/12/2005 50 Mw -8S 12/12/2005 50 PBW 12/12/2005 50 FORM XIII - IN ILM04.1 00 M O O Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 12/14/2005 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL004 12/14/2005 .. Sample No. e Time e • ` so 1 ee 11412 SEEMS ee 1 142e ■ MEN ■EEO ■■■■■■■■■■■■■■ ee ■ ■©■■■©■©■■■■■■■■■■■ 1.00 ■■ ■■©■■■■ ■■■■■■■■ ■■■■■■■ 1.00 ■■■■ !No1.■■■■■■■■©■■■ 1.00 44 ee M ® ■■E ©■ ■■�■■■■■© ■©■■■ e e e e ■ ■■■■■©M9■■■■■©■■■ ee e: ■ ©©■■■©©©©■■©■■©■■■ e e ��■ ■ ■©■■■■■©■©■■■■■■■■■ ee p■■■■©©■■. ©©BEEN■■■■■■■ 11 a ©© ©©©■■■■■■■■■■ 11m ■©©■■■©©©E■©EE©E■E■ 11 .■■ . ■ ■©■9■E■E■■©■■E■ ■■©©©©■■©■■©■■■ 1.00 ®�■■■■© ■■ 1-.-00 . e e © © ©©■■ E■©E■E■ IN■■©©..■©�©©■■�■■©■. ee—.....©©.■.©©©©..©..©.... �■ e1—.....©©...©©©©■.©..©.... ee _FINE .....©©...©©©©..©..©■... e e —.....®®...©©©®..©..©.... ee a .©©...©©©©.■©..©.... e1� ■■■■©©■ ■©©©©■E©■■©■■■■ CCv CCB ■■■■ INN©■ IHMMMEEEMMMEMEM©©©■■©■■©■■■■ MW -4D 1.00 11 ■ ■©©■■■©©©©■■©■■©■■■c 1.00 FORM XIV - IN ILM04.1 � V) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 12/14/2005 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL004 EPA Sample No. D/F Time % R Analytes A S L B A B B C C C C C F P M M H N K S A E D A R 0 U E B G N G I S A N T V' Z C E G A L N N MW -8S1.00 1821 X X X X X X X X EQPT BLANK _ 1.00 1829 X X X X X X X X CCv 1.00 1836 X X X X X X X X CCv 1.00 1 1843 _ X X _ CCs 1.00 1851 _ X X X X X X X X X X X CRI 1.00 1858 ICSA 1.00 1906 X X X X X X X ICSAs_ 1.00 1913 X X X X X X X CCv 1.00_ 1921 X X X X X X X X CCv 1.00 1928 X _ X _ _ _ CCs 1.00 1936 X X _ _ X X X X X X FORM XIV - IN ILM04.1 1H2M "US. INC. III. RAW DATA FOR METALS A. ICP DATA H2M LAOS, SIC. JCLIENT -TSLOO DATE 12liLilog ITASK: CLp + RESULT FILE: - 'C\21�o� ANALYS7:� TFACC 61 L G 1 ; # SAMPLE NOTES # SAMPLE NOTES ' 1 ju 26, 05k-tZA6- 001% f1 -1W 6D ; 2 27: oiv " Mu? 6S i i i 3Cf� i 28: —4 C Q.\\ ; 29: DiL F P Uv- fd S ; 1 6 C.SA(�) 31 ; C'Cw3 I7 C LV 1 ; 32: Cc\j 1-3 8 CC V[ 33; Cc(33 ; 9: CC;&1 34, 10; 11 ; LLS - ISL -0 6 1-c-sw 36; , •' 1 i 12,' D5 1 ZZ1J"L)O6C i RO-LtS 37 i CG11'i 13: QDb C -OLP 38� Cvl 14 ; opb&6: 39 ; C(6Li 15 ;S� SD 40' 16,' Oo + Iii. W - l b 41: 1 j 17 ; noz.0 I M k1 1 S 14 2; l 18: µms- I 43: 19: W 44: ' 1 20; CGv2 , r ; 45' r ' 21' CGVLL 46' Nr 22: cC-62. 47' , 2-3: C) 221 't?U$�; i Cl I 24; 00 49. :.25: OO9,I �1iil -�J S 50 ; I :�andardization Rpt. 12/14/05 02:20:10 PM page 1 '-thod: CLP1 Standard: StdBLANK in Time: 12/14/05 14:12:49 �1( Ag Al As1890 B Ba Be Ca Wge -.00451 .0049 .00047 .0013 .0002 -.0012 .0058 3Dev .00008 .0001 .00130 .0000 .0000 .0000 .0001 ''RSD 1.7584 2.310 276.52 2.097 17.51 1.918 1.444 #1 -.00458 .0050 -.00009 .0013 .0002 -.0012 .0058 #2 -.00453 .0048 .00196 .0013 .0002 -.0012 .0059 #3 -.00442 .0050 -.00046 ..0012 .0001 -.0013 .0058 31em Cd Co Cr Cu Fe Fe K kvge -.0007 -.0000 .0004 .0030 .0000 .0171 .0066 3Dev .0008 .0001 .0001 .0000 .0000 .0035 .0.005 'sRSD 102.5 336.5 16.44 1.385 .2566 20.65 7.036 11 -.0009 -.0000 .0004 .0030 .0000 .0150 .0069 #2 .0001 .0001 .0005 .0029 .0000 .0151 .0069 #3 -.0014 -.0001 .0004 .0030 .0000 .0212 .0061 ;lem Mg Mn Mo Na Na Ni 2203/1 �vge .0005 .0007 .0004 -.0210 .5523 .0005 .01344 3Dev .0002 .0003 .0001 .0015 .0075 .0002 .00549 sRSD 33.96 37.13 34.43 7.390 1.357 34.63 40.859 kl .0006 .0009 .0006 -.0197 .5476 .0006 .01893 k2 .0007 .0007 .0005 -.0205 .5485 .0003 .01344 13 .0003 .0004 .0003 -.0227 .5610 .0006 .00795 ,lem 2203/2 2068/1 2068/2 1960/1 1960/2 Si Sn ivge -.00162 -.00325 .00105 -.00685 .00197 .1399 .0059 ;Dev .00265 .00528 .00101 .00224 .00111 .0003 .0036 :RSD 163.02 162.40 95.574 32.730 56.361 .2227 60.54 `•1 -.00463 -.00928 .00111 -.00440 .00188 .1402 .0077 `2 -.00056 -.00100 .00002 -.00736 .00091 .1397 .0081 =3 .00033 .00053 .00203 -.00879 .00313 .1397 .0018 ;1 em Sr Ti T11908 v Zn ,vge .0014 .0004 -.00488 .0000 .0020 .Dev .0001 .0000 .00104 .0000 .0000 RSD 10.37 8.079 21.241 43.03 2.248 1 .0014 .0004 -.00368 .0000 .0020 2 .0016 .0005 -.00553 .0000 .0020 3 .0013 .0004 -.00543 .0000 .0019 tandardization Rpt. ethod: CLP1 Standard: StdAGSBH un Time: 12/14/05 14:20:17 E. Ag 2068/1 2068/2 Avge .71718 2.8757 1.8785 SDev .00135 .0129 .0107 %RSD .18850 .44823 .56829 #1 .71565 2.8610 1.8698 #2 .71821 2.8849 1.8904 43 .71767 2.8813 1.8753 12/14/05 02:26:03 PM page 1 tandardization Rpt. ethod: CLP1 Standard: StdICSH un Time: 12/14/05 14:26:09 E7 Al Ca Fe Avge 30.58 52.93 .6195 SDev .05 .05 .0004 %RSD .1553 .0861 .0694 12/14/05 02:31:09 PM page 1 Mg 71.30 .03 .0461 #1 30.63 52.95 .6200 71.32 #2 30.53 52.96 .6194 71.26 #3 30.58 52.87 .6192 71.32 tandardization Rpt. 12/14/05 02:37:02 PM ethod: CLP1 Standard: StdFURNH un Time: 12/14/05 14:31:15 E1___.' As1890 2203/1 2203/2 1960/1 1960/2 T11908 Avge 1.2019 4.1314 1.7242 .84375 .61470 .99383 SDev .0066 .0187 .0056 .00323 .00294 .00454 %RSD .55206 .45294 .32655 .38317 .47789 .45661 #1 1.1965 4.1360 1.7187 .84372 .61137 .98867 #2 1.1999 4.1108 1.7239 .84053 .61582 .99566 #3 1.2093 4.1473 1.7300 .84700 .61692 .99718 page 1 tandardization Rpt. ethod: CLP1 Standard: StdMULTH un Time: 12/14/05 14:37:08 E1 B Ba Be Avge 1.741 5.147 7.045 SDev .005 .015 .012 %RSD .2713 .2829 .1659 41 1.746 5.160 7.057 92 1.740 5.150 7.042 43 1.737 5.131 7.034 Elem Mn Mo Ni kvge 18.06 1.952 2.090 SDev .04 .003 .004 %RSD .2127 .1748 .1694 41 18.10 1.956 2.094 42 18.05 1.950 2.090 43 18.02 1.951 2.087 Elem v Zn lkvge 1.287 4.765 SDev .003 .011 %RSD .2660 .2404 41 1.290 4.778 k#; 1.287 4.761 1.283 4.756 12/14/05 02:43:42 PM page 1 Cd Co Cr Cu 65.00 2.071 2.640 1.455 .08 .004 .006 .006 .1219 .2035 .2233 .4280 65.09 2.075 2.646 1.461 64.96 2.070 2.638 .1.454 64.94 2.067 2.635 1.449 Si Sn Sr Ti 2.473 .10.27 10.22 2.107 .006 .02 .03 .005 .2391 .2237 .3204 .2306 2.479 10.30 10.25 2.111 2.471 10.27 10.22 2.108 2.468 10.25 10.18 2.102 ,tandardization Rpt. fethod: CLP1 Standard: StdFENAL .un Time: 12/14/05 14:43:48 E1 Fe Na Avge 42.24 44.99 SDev .30 .47 %RSD .7123 1.055 ##1 42.12 44.75 ##2 42.03 44.68 ##3 42.59 45.53 12/14/05 02:48:48 PM page 1 tandardization Rpt. ethod: CLP1 Standard: StdNAKH un Time: 12/14/05 14:48:55 E__ K Na Avge 8.961 2.182 SDev .354 .092 %RSD 3.952 4.217 #1 9.160 2.232 #2 9.170 2.238 #3 8.552 2.076 12/14/05 02:53:07 PM page 1 tandardization Report 12/14/05 02:53:08 PM page 1 .ethod: CLP1 Slope = Conc(SIR)/IR 1 it Wavelen High std Low std Slope Y -intercept Date Standardized g 328.068 StdAGSBH StdBLANK 2771.29 12.4971 12/14/05 02:48:55 .1 308.215 StdICSH StdBLANK 16.3533 -.080806 12/14/05 02:48:55 .s1890 189.042 StdFURNH StdBLANK 832.340 -.392773 12/14/05 02:48:55 249.678 StdMULTH StdBLANK 2.87846 -.003604 12/14/05 02:48:55 a 493.409 StdMULTH StdBLANK .971446 -.000153 12/14/05 02:48:55 e 313.042 StdMULTH StdBLANK .709780 .000876 12/14/05 02:48:55 a 317.933 StdICSH StdBLANK .924135 .002390 12/14/.05 02:48:55 d 226.502 StdMULTH StdBLANK .076917 .000.057 12/14/05 02:48:55 0 228.616 StdMULTH StdBLANK 2.41458 .000059 12/14/05 02:48:55 r 267.716 StdMULTH StdBLANK 1.89487 -.000783 12/14/05 02:48:55 u 324.754 StdMULTH StdBLANK 3.44372 -.010277 12/14/05 02:48:55 e 271.441 StdICSH StdBLANK .973272 .000019 12/14/05 02:48:55 e 259.940 StdFENAL StdBLANK .118409 -.002027 12/14/05 02:48:55 766.491 StdNAKH StdBLANK .892928 .000844 12/14/05 02:48:55 g 279.079 StdICSH StdBLANK .878417 .000115 12/14/05 02:48:55 n 257.610 StdMULTH StdBLANK .276897 -.000183 12/14/05 02:48:55 0 202.030 StdMULTH StdBLANK 2.56168 -.001152 12/14/05 02:48:55 a 330.232 StdNAKH StdBLANK .915314 -.009419 12/14/05 02:48:55 a 588.995 StdFENAL StdBLANK .112524 -.062151 12/14/05 02:48:55 i 231.604 StdMULTH StdBLANK 2.39137 -.001222 12/14/05 02:48:55 203/1 220.351 StdFURNH StdBLANK 242.840 -3.26378 12/14/05 02:48:55 203/2 220.352 StdFURNH StdBLANK 579.432 .940158 12/14/05 02:48:55 068/1 206.831 StdAGSBH StdBLANK 694.697 2.25873 12/14/05 02:48:55 068/2 206.832 StdAGSBH StdBLANK 1065.29 -1.12190 12/14/05 02:48:55 s 1 196.021 StdFURNH StdBLANK 1175.64 8.05337 12/14/05 02:48:55 5 2 196.022 StdFURNH StdBLANK 1632.04 -3.21676 12/14/05 02:48:55 i 288.158 StdMULTH StdBLANK 2.12076 -.296631 12/14/05 02:48:55 n 189.989 StdMULTH StdBLANK .486896 -.002859 12/14/05 02:48:55 r 421.552 StdMULTH StdBLANK .489520 -.000687 12/14/05 02:48:55 i 334.941 StdMULTH StdBLANK 2.37350 -.001038 12/14/05 02:48:55 11908 190.864 StdFURNH StdBLANK 1001.29 4.88629 12/14/05 02:48:55 292.402 StdMULTH StdBLANK 3.88596 -.000094 12/14/05 02:48:55 n 213.856 StdMULTH StdBLANK 1.04974 -.002048 12/14/05 02:48:55 b2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED b2068 206.838 NONE NONE 1.00000 .000000 *NOT STANDARDIZED e1960 196.026 NONE NONE 1.00000 .000000 *NOT STANDARDIZED tandardization Readback Report 12/14/05 02:53:08 PM E�thod: CLP1 IE t Wavelength Standard 9 328.068 StdBLANK StdAGSBH lement Wavelength Standard 1 308.215 StdBLANK StdICSH Lement Wavelength Standard 1890 189.042 StdBLANK StdFURNH Lement Wavelength Standard 249.678 StdBLANK StdMULTH Lement Wavelength Standard 493.409 StdBLANK StdMULTH E it Wavelength Standard 313.042 StdBLANK StdMULTH ement Wavelength Standard i 317.933 StdBLANK StdICSH .ement Wavelength Standard I 226.502 StdBLANK StdMULTH .ement Wavelength Standard 228.616 StdBLANK StdMULTH ement Wavelength Standard 267.716 StdBLANK StdMULTH Pm,-nt Wavelength Standard 324.754 StdBLANK StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 500.000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .007782 48.9123 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration .000000 2000.00 Measured Concentration .000000 500.000 Measured Concentration .000000 1000.00 Measured Concentration -.000000 5.00840 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00095 Measured Signal .005834 52.9251 Measured Concentration .000000 4.99930 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00108 Measured Concentration .000000 4.99875 page 1 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.008400 Residual Concentration .000000 .000000 Residual Concentration .000000 -.000950 Residual Signal .001948 -4.01276 Residual Concentration -.000000 .000700 Residual Concentration .000000 .000000 Residual Concentration .000000 -.001080 Residual kn Concentration -.000000 4- .001245 07 H tandardization Readback Report 12/14/05 02:53:08 PM lement Wavelength Standard e 271.441 StdBLANK StdICSH lement Wavelength Standard e 259.940 StdBLANK StdFENAL lement Wavelength Standard 766.491 StdBLANK StdNAKH lement Wavelength Standard 3 279.079 StdBLANK StdICSH Lement Wavelength Standard Z 257.610 StdBLANK StdMULTH lement Wavelength Standard 202.030 StdBLANK StdMULTH ement Wavelength Standard 330.232 StdBLANK StdNAKH _ement Wavelength Standard 588.995 StdBLANK StdFENAL ement Wavelength Standard 231.604 StdBLANK StdMULTH ement Wavelength Standard 03/1 220.351 StdBLANK StdFURNH ement Wavelength Standard 03/2 220.352 StdBLANK StdFURNH Known Signal .000055 .602976 Known Concentration .000000 5.00000 Known Signal .006759 8.'00205 Known Signal .000584 62.6316 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal -.028601 1.98779 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 1000.00 Measured Signal .000036 .619516 Measured Concentration -.000000 5.00000 Measured Signal .006624 8.96064 Measured Signal .000535 71.3004 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00000 Measured Signal -.020957 2.18199 Measured Concentration -.000000 5.00000 Measured Concentration .000000 4.99790 Measured Concentration .000000 1000.00 Measured Concentration -.000000 1000.00 page 2 Residual Signal .000018 -.016539 Residual Concentration .000000 .000000 Residual Signal .000135 -.958586 Residual Signal .000050 -8.66878 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Signal -.007644 -.194202 Residual Concentration .000000 .000000 Residual Concentration -.000000 .002100 Residual Concentration -.000000 .000000 Residual N Concentration .000000 .000000 d - O O tandardization Readback Report 12/14/05 02:53:08 PM lement Wavelength Standard 06 206.831 StdBLANK StdAGSBH lement Wavelength Standard 068/2 206.832 StdBLANK StdAGSBH lement Wavelength Standard 960/1 196.021 StdBLANK StdFURNH lement Wavelength Standard 960/2 196.022 StdBLANK StdFURNH lement Wavelength Standard i 288.158 StdBLANK StdMULTH Lement Wavelength Standard 189.989 StdBLANK StdMULTH Lement Wavelength Standard r 421.552 StdBLANK StdMULTH Lement Wavelength Standard L 334.941 StdBLANK StdMULTH Lement Wavelength Standard _1908 190.864 StdBLANK StdFURNH ement Wavelength Standard 292.402 StdBLANK StdMULTH .ement Wavelength Standard t 213.856 StdBLANK StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 2000.00 Known Concentration _.000000 1000.00 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration -.000000 2000.00 Measured Concentration -.000000 1000.00 Measured Concentration .000000 1000.00 Measured Concentration -.000000 4.94713 Measured Concentration -.000000 4.99870 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration .000000 1000.00 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 page 3 Residual Concentration .000000 -.000122 Residual Concentration .000000 .000122 Residual Concentration .000000 -.000061 Residual Concentration -.000000 .000000 Residual Concentration .000000 ..052870 Residual Concentration .000000 .001300 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual M Concentration � .000000 .000000 d - O O Cn E-4 ;tandardization Readback Report 12/14/05 02:53:08 PM Known Measured ;lenient Wavelength Standard Concentration Concentration 'b: i 220.353 NONE .000000 .000000 NONE .000000 .000000 Known Measured ;lement Wavelength Standard Concentration Concentration b2068 206.838 NONE .000000 .000000 NONE .000000 .000000 Known Measured lement Wavelength Standard Concentration Concentration e1960 196.026 NONE .000000 .000000 NONE .000000 .000000 page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 nalysis Report 12/14/05 03:00:34 PM page 1 ethod: CLP1 Sample Name: ICV Operator: CO un Time: 12/14/05 14:53:14 on t: TSL004 oc CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm Avge 961.74 49.70 493.46 L2.116 2.324 2.324 49.83 3Dev 1.01 .16 .77 .003 .002 .005 .08 `RSD .10495 .3175 .15539 .1511 .0817 .2348 .1639 l 962.90 49.54 492.76 L2.116 2.325 2.329 49.88 42 961.11 49.71 493.33 L2.113 2.322 2.318 49.73 43 961.20 49.85 494.28 L2.120 2.325 2.323 49.87 Errors LC Pass LC Pass LC Pass LC Low LC Pass LC Pass LC Pass sigh 1100.0 55.00 550.00 -2.750 2.750 2.750 55.00 'low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 ?1 em Cd Co Cr Cu Fe K- Mg Inits ppm ppm ppm ppm ppm ppm ppm vge 2.281 2.298 2.289 2.338 49.34 82.14 50.29 '>Dev .004 .004 .004 .003 .11 .44 .08 ;RSD .1870 .1869 .1796 .1369 .2203 .5300 .1493 !1 2.285 2.301 2.292 2.335 49.43 81.65 50.32 1-2 2.276 2.293 2.284 2.337 49.22 82.29 50.20 _ 2.281 2.299 2.290 2.342 49.36 82.47 50.33 :rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 'igh 2.750 2.750 2.750 2.750 55.00 88.00 55.00 ow 2.250 2.250 2.250 2.250 45.00 72.00 45.00 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 -nits ppm ppm ppm ppm ppb ppb ppb .vge 2.287 2.363 79.77 2.275 493.76 478.49 939.28 Dev .004 .002 .55 .004 3.30 3.42 3.85 RSD .1606 .0724 .6873 .1766 .66773 .71475 .41042 1 2.290 2.364 79.21 2.280 497.04 482.27 943.67 2 2.283 2.361 79.81 2.272 490.45 475.60 936.44 3 2.288 2.364 80.30 2.274 493.79 477.61 937.73 rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK igh 2.750 88.00 2.75.0 ow 2.250 72.00 2.250 lem 2068/2 1960/1 1960/2 Si Sn Sr Ti nits ppb ppb ppb ppm ppm ppm ppm vge 935.31 497.08 497.51 1.086 2.312 2.326 2.331 Dev 4.52 2.98 2.25 .007 .006 .002 .003 IZSD .48312 .59875 .45281 .5994 .2391 .0704 .1273 1 938.14 495.84 498.55 1.081 2.315 2.327 2.333 - 930.10 494.93 494.93 1.084 2.305 2.324 2.328 3 937.69 500.48 499.06 1.094 2.314 2.327 2.332 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK O CD H .nalysis Report 12/14/05 03:00:34 PM Hiah LC Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 482.30 2.308 2.394 483.58 936.63 497.37 j SDev 1.70 .003 .004 3.36 3.99 2.31 %RSD .35225 .1089 .1565 .69458 .42647 .46534 ##1 483.79 2.310 2.397 487.19 939.98 497.65 #2 482.66 2.306 2.390 480.55 932.21 494.93 #3 480.45 2.310 2.396 483.00 937.70 499.53 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 zalysis Report 12/14/05 03:08:01 PM page 1 =_thod: CLP1 Sample Name: ICVL Operator: CO in Time: 12/14/05 15:00:41 Dm TSL004 A 'ONC Corr. Factor: 1 ?lem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm ),vge .22118 .0168 -.02815 .0045 .0006 .0006 .0441 3Dev .23006 .0060 1.44761 .0014 .0002 .0002 .0051 '.RSD 104.01 35.56 5142.5 31.09 34.72 39.33 11.47 41 .46631 .0233 1.3085 .0060 .0008 .0008 .0497 42 .18727 .0155 -1.5657 .0039 .0006 .0005 .0429 #3 .00996 .0116 .17277 .0034 .0004 .0004 .0398 errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Sigh -jow ;lem CdCo Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge .0006 .0008 .0004 .0014 2.444 .0660 .0113 3Dev .0001 .0001 .0001 .0005 .029 .0133 .0048 '5RSD 24.77 20.17 18.06 35.48 1.175 20.22 42.54 #1 .0008 .0008 .0005 .0019 2.477 .0814 .0166 12 .0006 .0008 .0003 .0011 2.429 .0584 .0097 13 .0005 .0006 .0005 .0011 2.425 .0582 .0075 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK sigh 2.750 pow 2.250 ?lemMn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb �vge .0004 .0031 2.532 -.0004 .84250 .45990 3.1593 3Dev .0002 .0020 .040 .0003 1.7758 1.1309 2.5052 sRSD 47.81 62.70 1.588 60.32 210.78 245.89 79.295 kl .0006 .0054 2.571 -.0003 -.66316 1.3239 5.6465 k2 .0003 .0022 2.533 -.0007 2.8009 -.82005 3.1950 k3 .0002 .0018 2.491 -.0002 .38976 .87590 .63649 ;rrors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK sigh 2.750 -jow 2.250 ;lem 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm' ppm ppm ppm ivge 1.8554 1.1320 .15789 -.1781 .0012 -.0000 .0004 ;Dev 2.1163 1.7532 1.2936 .0032 .0013 .0002 .0003 ;RSD 114.06 154.88 819.28 1.791 101.8 640.7 79.70 k] 4.1448 -.21974 .11892 -.1745 .0027 .0002 .0007 E� 1.4509 .50278 1.4705 -.1790 .0009 -.0001 .0002 E3 -.02943 3.1130 -1.1158 -.1806 .0002 -.0002 .0002 :rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 03:08:01 PM page 2 Hiah Zn Lo; Sb2068 Elem T11908 Units ppb Avge 1.9522 SDev .6727 %RSD 34.458 #1 2.2252 #2 1.1859- .1859#3 43 2.4454 Errors NOCHECK High 97.721 Low .0010 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0007 .0005 .58734 2.2896 .48228 .0003 .0003 .17649 2.2374 .59424 40.90 56.88 30.049 97.721 123.22 .0010 .0009 .66222 4.6449 .00617 .0007 .0004 .38576 2.0317 1.1482 .0004 .0003 .71405 .19234 .29242 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 O O N nalysis Report 12/.14/05 03:15:27 PM page 1 ethod: CLP1 Sample Name: ICB Operator: CO un Time: 12/14/05 15:08:07 om t: TSL004 od L'ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .25502 .0050 .36945 -.0001 .0002 .0002 .0338 SDev .26971 .0026 .28456 .0005 .0000 .0000 .0008 °s RSD 105.76 52.10 77.022 586.2 12.57 15.92 2.483 k1 .06270 .0057 .43716 -.0001 .0002 .0002 .0331 42 .56331 .0073 .05714 .0004 .0002 .0002 .0347 �3 .13904 .0022 .61405 -.0006 .0002 .0001 .0335 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass ligh 10.000 .2000 10.000 .2000 .2000 .0050 .2000 mow -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg 7nits ppm ppm ppm ppm ppm ppm ppm Wge .0002 .0003 .0001 .0008 .0032 .0451 .0048 3Dev .0001 .0002 .0001 .0002 .0007 .0036 .0019 '5RSD 38.01 67.02 83.03 24.46 22.44 8.006 39.52 f1 .0001 .0004 .0001 .0009 .0032 .0451 .0042 k2 .0003 .0004 .0001 .0008 .0038 .0488 .0068 k3 .0002 .0001 .0000 .0005 .0024 .0415 .0032 ;rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Iigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 Jow -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 a em Mn Mo Na Ni 2203/1 2203/2 2068/1 rnits ppm ppm ppm ppm ppb ppb ppb .vge .0002 .0001 .0110 -.0000 .59873 .25162 .48106 ;Dev .0001 .0007 .0030 .0009 .91798 .24649 1.1598 -RSD 36.84 748.9 27.39 2286. 153.32 97.961 241.09 1 .0002 .0006 .0113 .0010 .52971 -.00836 -.85716 2 .0002 .0003 .0138 -.0004 -.28280 .48194 1.1943 3 .0001 -.0006 .0078 -.0006 1.5493 .28128 1.1060 rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK igh .0150 5.000 .0400 ow -.0150 -5.000 -.0400 lem 2068/2 1960/1 1960/2 Si Sn Sr Ti nits ppb ppb ppb ppm ppm ppm ppm vge 1.5188 .72308 .56479 -.0989 -.0017 -.0004 .0000 Dev 2.1271 .63296 2.1591 .0023 .0006 .0000 .0001 RSD 140.05 87.538 382.29 2.307 32.23 8.382 827.1 1 .03434 .03593 2.7983 -.0965 -.0011 -.0004 .0000 .56635 .85098 -1.5113 -.0990 -.0022 -.0004 .0001 3 3.9557 1.2823 .40738 -.1011 -.0019 -.0005 -.0001 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK ON d' O O H nalysis Report 12/14/05 03:15:27 PM High Lc Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .23251 .0002 .0005 .36724 1.1732 .61750 SDev 1.7699 .0000 .0001 .29262 1.6705 1.3034 %RSD 761.22 20.10 18.32 79.680 142.39 211.08 41 .85847 .0002 .0004 .17086 -.26251 1.8784 #2 1.6044 .0002 .0005 .22732 .77549 -.72467 43 -1.7653 .0003 .0006 .70356 3.0067 .69875 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Nigh 10.000 .0500 .0200 3.0000 60.000 5.0000 r,ow -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 nalysis Report ethod: CLP1 Sample Name: CRII un Time: 12/14/05 15:15:33 OT [t: TSL004 oc CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge 19.387 .0108 20.527 SDev .312 .0014 1.099 %RSD 1.6091 12.60 5.3556 41 19.031 .0093 21.614 42 19.517 .0118 19.416 43 19.612 .0114 20.550 Elem Cd Co Cr Jnits ppm ppm ppm Wge .0098 .0969 .0193 SDev .0001 .0003 .0003 oRSD 1.488 .3558 1.492 #1 .0098 .0966 .0191 12 .0100 .0973 .0196 #3 .0097 .0968 .0192 slem Mn Mo Na Jnits ppm ppm ppm .0288 .0198 .0104 3I .0001 .0002 .0011 ''RSD .4561 .9341 10.86 f1 .0287 .0198 .0114 k2 .0290 .0200 .0106 k3 .0287 .0197 .0092 'slem 2068/2 1960/1 1960/2 Jnits ppb ppb ppb ►vge 122.44 11.909 9.2153 ;Dev .84 1.349 1.4524 ;RSD .68729 11.332 15.761 :1 121.47 10.381 8.8519 :2 122.94 12.407 10.815 :3 122.92 12.938 7.9791 ;lem T11908 V Zn snits ppb ppm ppm .vge 21.246 .0970 .0436 Dev 1.030 .0002 .0001 RSD 4.8475 .1679 .1176 1 21.452 .0969 .0437 2 20.128 .0972 .0436 _ 22.157 .0969 .0436 12/14/05 03:22:53 PM Operator: CO B Ba Be PPM ppm ppm .1845 -.0000 .0100 .0006 .0000 .0000 .3185 730.3 .2532 .1838 -.0000 .0100 .1847 .0000 .0101 .1850 -.0000 .0100 Cu PPM .0491 .0000 .0540 .0490 .0491 .0491 Ni PPM .0769 .0003 .3450 .0766 .0771 .0768 Si PPM -.0072 .0005 6.919 -.0074 -.0075 -.0066 Pb2203 ppb 6.1881 .8459 13.670 5.4637 5.9828 7.1178 Fe PPM .0027 .0002 8.018 .0028 .0028 .0025 2203/1 ppb 5.4270 1.8294 33.710 6.1111 3.3541 6.8158 Sn PPM .0836 .0008 .9650 .0834 .0845 .0829 Sb2068 ppb 122.21 1.19 .97594 120.84 123.01 122.77 K PPM .0275 .0085 30.81 .0210 .0370 .0244 2203/2 ppb 6.5680 1.2364 18.824 5.1404 7.2951 7.2684 Sr PPM -.0006 .0000 7.480 -.0006 -.0006 -.0007 Se1960 ppb 10.112 1.076 10.642 9.3611 11.345 9.6305 page 1 Ca PPM .0291 .0005 1.838 .0294 .0293 .0285 Mg PPM -.0029 .0041 142.4 -.0044 .0018 -.0061 2068/1 ppb 121.74 1.91 1.5665 119.57 123.15 122.49 Ti PPM -.0005 .0001 15.89 -.0005 -.0004 -.0005 nalysis Report 12/14/05 03:30:19 PM page•1 ethod: CLP1 Sample Name: ICSAI Operator: CO un Time: 12/14/05 15:22:59 Dm --: TSL004 :)d' 'ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm 4,vge .89996 511.2 -4.2045 .0269 .0011 .0002 512.5 7Dev .25802 1.7 1.3826 .0003 .0000 .0000 1.5 %RSD 28.670 .3347 32.885 1.285 1.297 .6642 .2941 41 1.1241 509.2 -5.3181 .0265' .0011 .0002 511.5 42 .95782 512.2 -4.6385 .0272 .0011 .0002 514.2 43 .61792 512.2 -2.6569 _0270 .0011 .0002 511.8 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass Sigh 10.000 600.0 .2000 .0050 600.0 low -10.000 400.0 -.2000 -_0050 400.0 ?lem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm %vge .0011 -.0005 .0034 .0002 206.0 .0327 514.4 3Dev .0001 _0001 .0002 .0001 .5 .0040 1.2 -RSD 9.169 22.67 5.776 55.91 .2414 12.27 .2320 #1 .0011 -.0006 .0036 .0001 205.7 .0335 513.4 #2 .0012 -.0004 .0033 .0003 206.5 .0363 515.7 #3 .0010 -.0005 .0032 .0001 205.7 .0284 514.2 ;r_Luj-s LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass Sigh .0050 .0100 240.0 600.0 -jow -.0050 -.0100 160.0 400.0 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 ]nits ppm ppm ppm ppm ppb ppb ppb �vge -.0062 -.0050 .0367 .0020 35.988 -20.009 2.0807 3Dev _0003 .0003 .0009 .0005 .768 .584 4.9284 '5RSD 5.303 7.026 2.340 26.01 2.1335 2.9181 236.87 k1 -.0060 -.0049 .0371 .0014 36.753 -19.369 4.1616 k2 -.0066 -.0046 .0374 .0024 35.217 -20.512 5.6273 D -.0060 -.0053 .0358 .0023 35.995 -20.147 -3.5469 ;rrors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK sigh .0150 .0400 .Jow -.0150 -.0400 ,lem 2068/2 1960/1 1960/2 Si Sn Sr Ti ]nits ppb ppb ppb ppm ppm ppm ppm ►vge -4.7694 .85706 -3.9159 -.0050 .0402 -.3099 .0023 ;Dev 2.1408 2.4828 2.2182 .0015 .0023 .0013 .0001 ,RSD 44.885 289.69 56.645 31.01 5.780 .4145 3.485 -5.6322 3.3502 -1.4114 -.0060 .0426 -.3084 .0022 `-� -2.3319 -1.6154 -4.7033 -.0032 .0402 -.3108 _0024 `3 -6.3442 .83638 -5.6329 -.0057 .0379 -.3104 .0023 ;rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK malysis Report 12/14/05 03:30:19 PM High Lc Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge L-18.899 .0001 -.0097 -1.3621 -2.4883 -2.3265 SDev .971 .0003 .0002 .6416. 2.8674 2.1679 %RSD 5.1399 301.8 2.441 47.104 115.23 93.182 #1 L-18.470 -.0001 -.0095 -.68045 -2.3708 .17419 #2 L-18.216 -.0001 -.0096 -1.9543 .31851 -3.6750 #3 L-20.011 .0004 -.0100 -1.4516 -5.4127 -3.4786 Errors LC Low LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 inalysis Report 12/14/05 03:37:45 PM page 1 Iethod: CLP1 Sample Name: ICSABI Operator: CO 'un Time: 12/14/05 15:30:25 .on t: TSL004 [oc CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1090.4 495.2 1059.7 9038 .5172 .5019 498.7 SDev 1.9 1.2 2.6 .0022 .0011 .0008 .9 %RSD .17380 .2449 .24692 .2434 .2065 .1555 .1802 ill #1 1091.9 496.6 1061.9 .9045 .5184 .5013 497.8 #2 1091.0 494.9 1060.3 .9056 .5171 .5027 499.6 #3 1088.3 494.2 1056.8 .9013 .5162 .5016 498.7 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm tivge .9405 .4698 .4878 .5269 200.0 .0774 499.9 SDev .0017 .0007 .0009 .0014 .3 .0081 .6 'RSD .1829 .1428 .1955 .2722 .1531 10.49 .1135 41 .9392 .4694 .4871 .5284 199.7 .0681 499.7 $2 .9424 .4706 .4889 .5268 200.3 .0827 500.6 43 .9397 .4695 .4875 .5256 199.8 .0815 499.5 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass sigh 1.200 .6000 .6000 .6000 240.0 600.0 .,ow .8000 .4000 .4000 .4000 160.0 400.0 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 7nits ppm ppm ppm ppm ppb ppb ppb ivge .4776 .9830 .0286 .9276 1070.3 994.14 -8.0651 >Dev .0005 .0026 .0006 .0014 3.8 1.88 3.8762 ;RSD .1008 .2681 2.201 .1487 .35909 .18953 48.062 `1 .4778 .9803 .0279 .9269 1066.6 991.96 -7.3406 2 .4779 .9855 .0288 .9292 1074.3 995.20 -12.252 =3 .4770 .9831 .0291 .9268 1070.0 995.24 -4.6022 ,rrors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK :igh .6000 1.200 ow .4000 .8000 lem 2068/2 1960/1 1960/2 Si Sn Sr Ti nits ppb ppb ppb ppm ppm ppm ppm vge -7.1736 1038.7 1032.3 .5041 1.026 -.3076 .0017 Dev 1.6449 1.3 4.3 .0020 .006 .0012 .0001 RSD 22.931 .12565 .41423 .3999 .5559 .3994 2.845 1 -6.6480 1040.1 1027.5 .5064 1.025 -.3062 .0017 2 -5.8557 1037.5 1033.5 .5027 1.032 -.3078 .0017 3 -9.0171 1038.5 1035.8 .5032 1.021 -.3087 .0018 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 03:37:45 PM Lc Elem T11908 v Zn Pb2203 Sb2068 Sel960 Jnits ppb ppm ppm ppb ppb ppb .kvge 981.83 .4909 1.042 1019.5 -7.4705 1034.4 3Dev 2.53 .0007 .001 2.4 .5576 2.5 6RSD .25748 .1384 .0859 .23787 7.4635 .24314 41 984.55 .4906 1.042 1016.8 -6.8786 1031.7 42 981.36 .4917 1.043 1021.5 -7.9858 1034.8 ff3 979.56 .4904 1.041 1020.1 -7.5469 1036.7 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass Sigh 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 .nalysis Report 12/14/05 03:45:11 PM page 1 .ethod: CLP1 Sample Name: CCV1 Operator: CO .un Time: 12/14/05 15:37:51 'or it: TSL0 04 .ot_ _ CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1009.8 52.25 516.51 2.392 2.481 2.482 52.59 SDev 42.8 2.22 21.44 .101 .108 .107 2.23 %RSD 4.2367 4.252 4.1517 4.228 4.365 4.303 4.235 ##1 1035.2 53.66 528.58 2.451 2.545 2.540 53.83 ##2 1033.8 53.41 529.20 2.451 2.543 2.547 53.92 #3 960.42 49.69 491.75 2.276 2.356 2.359 50.02 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.453 2.465 2.458 2.490 52.17 86.85 53.22 SDev .103 .105 .106 .110 2.32 3.42 2.28 %RSD 4.216 4.239 4.332 4.428 4.456 3.943 4.279 91 2.507 2.522 2.517 2.558 53.43 H89.20 54.51 42 2.517 2.528 2.522 2.550 53.60 H88..44 54.55 k#. 2.333 2.344 2.335 2.363 49.49 82.92 50.59 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Ljow 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 7nits ppm ppm ppm ppm ppb ppb ppb ),vge 2.455 2.501 83.55 2.446 521.95 504.45 1004.2 SDev .106 .107 3.01 .104 20.55 16.73 30.3 'RSD 4.299 4.286 3.604 4.265 3.9363 3.3169 3.0191 #1 2.514 2.560 85.40 2.503 531.35 513.35 1021.9 #2 2.519 2.565 85.19 2.509 536.11 514.85 1021.5 #3 2.333 2.377 80.08 2.325 498.38 485.14 969.21 3rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK sigh 2.750 88.00 2.750 -low 2.250 72.00 2.250 ;lem 2068/2 1960/1 1960/2 Si Sn Sr Ti 7nits ppb ppb ppb ppm ppm ppm ppm wge 995.63 519.16 519.04 1.847 2.451 2.486 2.465 )Dev 40.33 20.62 16.09 .083 .102 .109 .109 -RSD 4.0509 3.9711 3.1007 4.470 4.156 4.379 4.419 k 1017.5 530.57 527.66 1.893 2.506 2.550 2.527 k� 1020.3 531.56 528.99 1.896 2.515 2.547 2.528 k3 949.09 495.37 500.47 1.751 2.334 2.360 2.339 :rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK analysis Report 12/14/05 03:45:11 PM High Lr Elem T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 505.07 2.475 2.570 510.27 998.49 519.08 SDev 21.52 .108 .111 17.99 36.99 17.60 %RSD 4.2609 4.361 4.322 3.5258 3.7047 3.3905 #1 516.71 2.536 2.632 519.34 1019.0 528.63 #2 518.26 2.539 2.637 521.93 1020.7 529.84 #3 480.23 2.351 2.442 489.55 955.79 498.77 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 .nalysis Report ethod: CLP1 Sample Name: CCVL1 un Time: 12/14/05 15:45:18 Orr, t : TSL004 od :70NC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .80683 .0505 .01882 SDev .16345 .0167 .53916 %RSD 20.258 33.17 2865.2 #1 .89182 .0679 .30964 #2 .91027 .0489 -.60331 #3 .61839 .0346 .35012 Errors NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem Cd Co Cr Units ppm ppm ppm kvge .0007 .0008 .0006 SDev .0002 .0002 .0001 %RSD 34.16 25.51 23.39 41 .0010 .0010 .0006 42 .0006 .0006 .0004 �3 .0005 .0007 .0007 3r.Lu.Ls NOCHECK NOCHECK NOCHECK -sigh mow 31em Mn Mo Na Jnits ppm ppm ppm kvge .0003 .0030 2.593 SDev .0001 .0019 .027 'sRSD 42.94 62.94 1.026 f1 .0005 .0052 2.614 f2 .0002 .0021 2.601 k3 .0003 .0017 2.563 'srrors NOCHECK NOCHECK LC Pass sigh 2.750 Jow 2.250 :lem 2068/2 1960/1 1960/2 [nits ppb ppb ppb ,vge .03730 1.5449 1.0056 ;Dev 1.3381 1.2580 1.2339 :RSD 3587.4 81.430 122.71 1 1.5817 2.9595 1.6816 2 -.69407 .55192 1.7537 3 -.77576 1.1231 -.41864 ;rrors NOCHECK NOCHECK NOCHECK 12/14/05 03:52:38 PM Operator: CO page 1 B Ba Be Ca PPM ppm ppm ppm .0152 .0006 .0005 .0743 .0016 .0002 .0002 .0187 10.48 34.04 39.76 25.18 .0169 .0008 .0007 .0950 .0150 .0005 .0005 .0691 .0137 .0004 .0003 .0587 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg PPM ppm ppm ppm .0014 2.517 .0600 .0401 .0003 .016 .0079 .0166 22.50 .6330 13.22 41.45 .0017 2.527 .0675 .0593 .0011 2.526 .051.7 .0316 .0013 2.499 .0607 .0295 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 2203/2 2068/1 PPM ppb ppb ppb -.0005 -.10449 -.21052 -.37652 .0007 .77998 .24827 .20257 136.9 746.43 117.93 53.800 .0003 .44607 .03787 -.34604 -.0008 -.99706 -.45866 -.19092 -.0009 .23750 -.21076 -.59261 NOCHECK' NOCHECK NOCHECK NOCHECK Si Sn Sr Ti PPM ppm ppm ppm -.1164 .0014 -.0001 .0004 .0022 .0003 .0001 .0001 1.859 24.17 97.58 27.63 -.1142 .0018 .0000 .0005 -.1164 .0013 -.0002 .0003 -.1186 .0011 -.0002 .0004 NOCHECK NOCHECK NOCHECK NOCHECK 00 O O C/) H .nalysis Report 12'/14/05 03:52:38 PM page 2 Hiah - Zn Lr Sb2068 Elem T11908 Units ppb Avge 3.6735 SDev 1.2943 %RSD 35.234 ##1 4.2055 ##2 2.1980 ##3 4.6171 Errors NOCHECK High 901.45 Low .0008 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0007 .0029 -.17518 -.10048 1.1852 .0001 .0002 .41765 .90582 1.0167 14.86 6.088 238.42 901.45 85.787 .0008 .0031 .17384 .93980 2.1072 .0006 .0028 -.63791 -.52650 1.3535 .0007 .0027 -.06146 -.71475 .09477 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 04:00:05 PM page 1 ethod: CLP1 Sample Name: CCB1 Operator: CO un Time: 12/14/05 15:52:45 on t: TSL004 oc CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm hvge .48591 .0174 -.60762 -.0012 .0001 .0001 .0426 SDev .10310 .0038 .69529 .0003 .0001 .0001 .0046 %RSD 21.218 21.85 114.43 23.02 52.54 31.64 10.86 41 .60477 .0217 -.93182 -.0013 .0001 .0002 .0478 42 .43232 .0160 .19057 =.0009 .0000 .0001 .0412 43 .42064 .0145 -1.0816 -.0014 .0002 .0001 .0389 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge .0002 .0000 -.0002 .0008 .0069 .0416 .0105 SDev .0000 .0001 .0002 .0002 .0024 .0039 .0032 6"RSD 21.03 354.0 109.7 28.49 34.37 9.415 30.30 41 .0002 -.0000 -.0003 .0009 .0096 .0400 .0141 42 .0002 -.0000 -.0003 .0005 .0061 .0388 .0093 4: .0003 .0001 .0001 .0009 .0050 .0461 .0081 errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 -jow -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 .lem Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb kvge .0001 .0003 .0175 -.0010 -.82299 .43458 .58819 SDev .0000 .0003 .0040 .0004 .54390 .97661 1.0240 'RSD 65.54 122.8 22.84 40.54 66.088 224.72 174.10 11 .0001 .0006 .0218 -.0008 -.19592 .06521 .59456 #2 .0000 .0000 .0165 -.0014 -1.1064 1.5420 -.43903 #3 .0001 .0001 .0140 -.0007 -1.1666 -.30347 1.6090 3rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK sigh .0150 5.000 .0400 -jow -.0150 -5.000 -.0400 ;lem 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm ppm ppm ppm Wge -.32053 -1.2040 .15143 -.2239 -.0004 -.0005 -.0002 SDev .41051 1.2748 1.5777 .0017 .0006 .0000 .0001 >RSD 128.07 105.89 1041.9 .7698 147.7 6.458 70.65 k -.44899 .24562 -1.5565 -.2219 -.0003 -.0005 -.0001 k� .13885 -1.7069 .45622 -.2246 -.0011 -.0005 -.0003 k3 -.65146 -2.1507 1.5545 -.2252 .0001 -.0005 -.0001 ,rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK analysis Report 12/14/05 04:00:05 PM Hiah L, Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .79313 .0004 .0029 .01585 -.01791 -.29991 SDev .97930 .0001 .0001 .62633 .10598 .63930 .RSD 123.47 34.81 4.084 3952.6 591.74 213.17 #1 .24052 .0005 .0030 -.02171 -.10147 -.95636 #2 .21503 .0006 .0030 .66011 -.05357 -.26407 #3 1.9238 .0003 .0028 -.59087 .10130 .32072 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 r` tt O O DO H analysis Report 12/14/05 04:07:32 PM page 1 Iethod: CLP1 Sample Name: MB -15608 Operator: CO ,-un Time: 12/14/05 16:00:12 '01 it: TSL004 !o( CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .33001 .0173 -.55410 -.0013 .0007 .0001 .1173 SDev .46673 .0019 .39465 .0002 .0001 .0000 .0022 %RSD 141.43 11.18 71.224 19.14 8.065 30.23 1.914 #1 .09267 .0195 -.10164 -.0012 .0007 .0001 .1197 #2 .86771 .0160 -.73327 -.0011 .0007 .0001 .1153 #3 .02964 .0163 -.82738 -.0016 .0006 .0001 .1170 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm zkvge .0001 .0002 .0004 .0013 .0276 .1736 .0115 SDev .0001 .0004 .0002 .0005 .0009 .0087 .0035 ''RSD 62.82 170.6 46.64 35.82 3.174 4.996 30.37 $1 .0001 .0003 .0004 .0018 .0286 .1820 .0153 $2 .0002 .0006 .0005 .0012 .0269 .1743 .0109 #= .0000 -.0002 .0002 .0009 .0274 .1646 .0084 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 meow -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 31em Mn Mo Na Ni 2203/1 2203/2 2068/1 7nits ppm ppm ppm ppm ppb ppb ppb �vge .0004 .0002 .0459 .0003 1.0681 .71754 .09861 )Dev .0001 .0003 .0030 .0002 .5661 .70613 .50045 ;RSD 24.48 144.0 6.445 65.35 52.999 98.410 507.51 `1 .0005 -.0001 .0493 .0005 1.5217 .01044 .61514 :2 .0005 .0003 .0450 .0001 1.2491 1.4227 .06472 :3 .0003 .0003 .0436 .0003 .43369 .71949 -.38403 ;rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK Agh .0150 5.000 .0400 low -.0150 -5.000 -.0400 lem 2068/2 1960/1 1960/2 Si Sn Sr Ti nits ppb ppb ppb ppm ppm ppm ppm vge -.41100 -1.6577 .50897 -.1409 -.0011 -.0004 .0007 Dev .71837 2.5750 .58428 .0024 .0003 .0001 .0001 RSD 174.79 155.33 114.80 1.734 29.69 15.93 16.62 1 .21341 -4.2090 .90158 -.1391 -.0007 -.0003 .0007 2 -.25030 .94043 .78781 -.1437 -.0013 -.0004 .0008 3 -1.1961 -1.7046 -.16250 -.1400 -.0013 -.0004 .0006 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK malysis Report 12/14/05 04:07:32 PM Hiah Lo Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.0532 .0004 .0150 .83436 -.24128 -.21253 SDev .9322 .0001 .0002 .46282 .64184 .91247 oRSD 88.508 32.70 1.239 55.469 266.01 429.33 #1 2.1288 .0005 .0153 .51376 .34720 -.80024 #2 .55072 .0003 .0149 1.3649 -.14538 .83865 #3 .48009 .0003 .0150 .62439 -.92567 -.67601 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 analysis Report 9ethod: CLP1 Sample Name: LCS-15608 :un Time: 12/14/05 16:07:38 'or it: TSL004 Io( CONC Corr. Factor: 1 12/14/05 04:14:58 PM Operator: CO Elem Ag Al As1890 B Units ppb ppm ppb ppm Avge 1018.5 54.21 504.69 2.724 SDev 3.4 .32 2.17 .011 %RSD .32909 .5889 .43049 .4107 41 1018.9 54.32 505.89 2.721 #2 1021.6 54.46 505.99 2.736 #3 1014.9 53.85 502.18 2.714 Errors LC Pass LC Pass LC Pass LC Pass High 1200.0 60.00 60.0.00 3.000 Low 800.00 40.00 400..00 2.000 Elem Cd Co Cr Cu Units ppm ppm ppm ,ppm Avge 2.430 2.459 2.460 2.538 SDev .007 .009 .010 .014 .RSD .3070 .3512 .4022 .5370 41 2.425 2.455 2.455 2.542 42 2.438 2.469 2.472 2.548 1' 2.427 2.453 2.454 2.522 Errors LC Pass LC Pass LC Pass LC Pass sigh 3.000 3.000 3.000 3.000 mow 2.000 2.000 2.000 2.000 s l em Mn Mo Na Ni Inits ppm ppm ppm ppm Wge 2.458 2.539 86.27 2.433 SDev .009 .010 .66 .007 ;RSD .3692 .4105 .7658 .2856 El 2.454 2.535 86.70 2.429 `-2 2.469 2.551 86.59 2.441 13 2.452 2.531 85.51 2.429 ;rrors LC Pass NOCHECK LC Pass LC Pass !igh 3.000 96.00 3.000 pow 2.000 64.00 2.000 '1 em 2068/2 1960/1 1960/2 Si nits ppb ppb ppb ppm .vge 989.26 488.96 490.07 4.511 Dev 2.00 2.37 1.24 .025 RSD .20177 .48534 .25249 .5462 987.00 486.32 491.31 4.486 _ 989.99 489.66 490.04 4.536 3 990.79 490.91 488.84 4.512 rrors NOCHECK NOCHECK NOCHECK NOCHECK Ba ppm 2.504 .011 .4425 2.505 2.515 2.493 LC Pass 3.000 2.000 Fe PPM 52.68 .19 .3579 52.59 52.90 52.56 LC Pass 60.00 40.00 2203/1 ppb 518.99 .57 .10905 518.39 519.51 519.05 NOCHECK Sn PPM 2.473 .009 .3728 2.470 2.483 2.465 NOCHECK Be PPM 2.504 .009 .3651 2.499 2.515 2.500 LC Pass 3.000 2.000 K• ppm 84.24 .55 .6533 84.56 84.56 83.61 LC Pass 96.00 64.00 2203/2 ppb 497.00 1.90 .38141 495.81 499.18 496.01 NOCHECK Sr ppm 2.504 .011 .4361 2.503 2.515 2.493 NOCHECK page 1 Ca PPM 54.11 .20 .3676 53.99 54.34 53.99 LC Pass 60.00 40.00 Mg PPM 54.33 .20 .3648 54.28 54.55 54.16 LC Pass 60.00 40.00 2068/1 ppb 993.51 3.55 .35750 990.44 997.40 992.70 NOCHECK Ti PPM 2.516 .011 .4235 2.513 2.528 2.507 NOCHECK nalysis Report 12/14/05 04:14:58 PM High Lc Elem T11908 v Zn Pb2203 Sb2068 Se1960 Jnits ppb ppm ppm ppb ppb ppb kvge 498.65 2.483 2.540 504.32 990.68 489.70 3)Dev 3.43 .009 .009 1.43 2.25 .20 .RSD .68756 .3796 .3518 .28280 .22729 .04033 41 494.94 2.480 2.537 503.33 988.15 489.65 42 501.71 2.494 2.550 505.95 9.92.46 489.92 43 499.29 2.475 2.533 503.68 991.43 489.53 3rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass -sigh 600.00 3.000 3.000 600.00 1200.0 600.00 -jow 400.00 2.000 2.000 400.00 800.00 400.00 page 2 ,nalysis Report 12/14/05 04:22:24 PM page 1 [ethod: CLP1 Sample Name: 0512218-006E Operator: CO .un Time: 12/14/05 16:15:04 'or 'it: TSL004 �,j C ' S [oc _ _ CONC Corr. Factor: 1 �W Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .11658 .0688 2.3252 .0064 .0013 .0005 1.324 SDev .12000 .0029 1.0137 .0008 .0001 .0001 .007 %RSD 102.93 4.209 43.595 11.97 7.646 23.62 .5640 #1 -.02190 .0713 3.2653 .0073 .0015 .0007 1.333 #2 .18156 .0694 2.4591 .0058 .0013 .0005 1.321 #3 .19008 .0656 1.2512 .0062 .0013 .0004 1.319 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm . ppm ppm ppm Avge .0006 .0014 .0007 .0439 .1899 6.598 .6009 SDev .0001 .0001 .0001 .0001 .0031 .041 .0034 %RSD 18.75 5.263 14.24 .2896 1.622 .6145 .5636 41 .0007 .0014 .0008 .0441 .1931 6.618 .6048 42 .0005 .0014 .0006 .0439 .1898 6.624 .5988 43 .0005 .0015 .0008 .0438 .1869 6.551 .5992 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb k` .0104 .0020 23.09 .0016 3.8183 1.5568 2.1115 3I .0001 .0007 .18 .0003 1.0456 1.0098 1.3401 '.RSD .9604 36.63 .7976 15.71 27.385 64.865 63.468 11 .0105 .0029 23.17 .0017 3.2551 1.6204 .62967 42 .0103 .0017 23.22 .0013 3.1749 2.5333 2.4662 13 .0103 .0015 22.88 .0017 5.0248 .51668 3.2385 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm ppm ppm ppm kvge .49241 2.1988 5.8051 1.206 -.0003 .0016 .0013 SDev 1.1258 1.0266 2.1494 .014 .0003 .0001 .0001 RSD 228.63 46.690 37.027 1.187 .98.14 6.730 7.050 f1 1.2268 3.1051 5.0728 1.220 -.0006 .0017 .0013 f2 -.80372 1.0839 4.1176 1.205 -.0005 .0016 .0012 f3 1.0542 2.4076 8.2250 1.192 .0000 .0015 .0013 ?,lem T11908 v Zn Pb2203 Sb2068 Se1960 Jnits ppb ppm ppm ppb ppb ppb ivge -.63272 .0007 .0196 2.3099 1.0316 4.6042 >Dev 1.22817 .0002 .0003 .3856 .7482 1.5984 ;RSD 194.11 22.79 1.597 16.693 72.529 34.717 1 -.43553 .0008 .0200 2.1648 1.0280 4.4175 .48493 .0005 .0195 2.7470 .28518 3.1074 -1.9476 .0008 .0194 2.0179 1.7815 6.2878 ,nalysis Report 12/14/05 04:29:50 PM lethod: CLP1 Sample Name: 0512218-006EDUP Cr Operator: CO :un Time: 12/14/05 16:22:30 Avge .0001 .0012 .0004 'on t : TSL0 04 .0004 .0003 %RSD 109.6 35.69 loc CONC Corr. Factor: 1 (v� .0017 .0006 42 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .27525 .0673 3.7967 .0057 .0010 .0001 SDev .59567 .0024 .4307 .0005 .0001 .0000 %RSD 216.41 3.521 11.344 8.113 7.049 37.60 #1 .91475 .0694 4.2311 .0059 .0010 .0001 #2 .17483 .0679 3.3697 .0061 .0009 .0001 #3 -.26383 .0648 3.7893 .0052 .0009 .0001 Elem Cd Co Cr Units ppm ppm ppm Avge .0001 .0012 .0004 SDev .0001 .0004 .0003 %RSD 109.6 35.69 86.30 #1 .0002 .0017 .0006 42 .0000 .0008 .0000 43 .0000 .0012 .0004 Elem Mn Mo Na Units ppm ppm ppm Ikti .0108 .0003 24.93 SI .0001 .0002 .07 6k5li 1.336 66.86 .2748 .0109 .0106 .0108 2068/2 ppb .96655 1.4548 150.52 .03272 .22412 2.6428 T11908 ppb -2.0242 .6834 33.763 .0003 .0001 .0005 1960/1 ppb 3.1939 1.5257 47.771 1.5316 3.5195 4.5305 v PPM .0002 .0003 167.6 24.97 24.98 24.85 1960/2 ppb 5.5091 1.5223 27.633 7.0992 4.0651 5.3629 Zn PPM .0279 .0002 .6570 -1.2480 .0006 .0281 -2.2891 .0000 .0279 -2.5355 -.0000 .0277 Cu PPM .0473 .0004 .8330 .0477 .0473 .0469 Ni PPM .0016 .0003 15.78 .0019 .0016 .0014 Si PPM 1.306 .009 .6687 1.314 1.307 1.297 Pb2203 ppb 1.8184 .2443 13.437 1.9855 1.9318 1.5380 Fe PPM .1967 .0018 .9234 .1984 .1967 .1948 2203/1 ppb 3.0517 .7197 23.585 2.9847 3.8026 2.3678 Sn PPM .0002 .0007 355.5 -.0004 -.0000 .0010 Sb2068 ppb 1.3391 1.2490 93.271 .64865 .58782 2.7810 K PPM 7.143 .016 .2268 7.155 7.149 7.124 2203/2 ppb 1.2027 .2539 21.110 1.4866 .99768 1.1236 Sr PPM .0014 .0001 4.004 .0015 .0014 .0014 Se1960 ppb 4.7381 .7444 15.712 5.2452 3.8835 5.0857 page 1 Ca PPM 1.493 .008 .5401 1.501 1.493 1.485 Mg PPM .6396 .0050 .7879 .6453 .6378 .6357 2068/1 ppb 2.0854 .8883 42.596 1.8824 1.3162 3.0577 Ti. PPM .0008 .0001 18.20 X10• BeM: O O V1 N y r C 0 J 00 E9S'ET DL'86D, OS6'TZ EOZS' Z08il" T7f,8'Lb :# 9LT'LT OF "POS TEO'ZZ ELZS' S98il' tCZ'LP c;# 9Z0'9T Z8, COS 8L:V'ZZ Z8ZS' TL8f,' OTZ'LP It Zf,8'IT TtET9" fi£8Z'T E£Z8 LE6L' 9TLSL' QS2iIC, 9T78 80'£ 68Z' £fl00' 6E00' 6SU AaQc, 88S, ST 6Z'ZOS EST'ZZ ESZS' 9tl8tl' 6ZD,'L6 a6AF qdd qdd qdd wdd Ladd qdd s q T ur 096TGS 890ZQS EOZZgd uZ A 806TT,L waT-e 9000' OT00' LZ00'- OtZ'I SLE'ST ZE£6'6 8T'86t, E# 8000' TT00' E000' ESZ'T fZ8'LT LL8'ST TL'fOS Z# S000' OT00' DIZ00'- L9Z'I P69'9T L89'tT 89'ZOS It TL'SZ 9T0'S 0' 90T 6LO'T TZLE"L L6Z'EZ 88S99' QS2I° 2000' T000' LT00' bTO' 9ZZ'T SbT'E PE"E AaQE 9000' TT00' 9TOO'- ESZ'T TE9'9T 66t,'ET 98'TOS a6A� wdd Ladd uidd wdd qdd qdd qdd S q T ur T1 as us TS Z/096T T/096T Z/8902 waT, L8' 66t, T06' ZZ DItlo OZ S89t,' LZ' EZ E000' - 8L8b' E# 6D'£0S Tb8'OZ ST:'tlZ I9LP' LE"EZ Z000'- OS6D,' Z# IT 90S EIiZ'ZZ 6T76' ZZ 6ELf,' b8"EZ b000'- PS6b' I EO£Z9' EE8L't, S668'6 TSZ8' ZOE'I ZS'6E 8£98' (ISE ° ET'E ZSO'I bZZ"Z 6E00' T£' 1000' E600' ZS 9T'EOS S66'TZ 69f,' ZZ 8ZLIi" 6t,'EZ E000'- LZ6b' 2� qdd qdd qdd wdd wdd wdd wdd S -1 -Fur T/8902 Z/EOZZ T/EOZZ TN aN ow uw waTE 606S' 8L9'9 £ST'T E88Z' LE6T' S9Lf,' 8LtO' E# Sf09' LTL'9 69T'T LT6Z' OL6T' LE8Ii' T78t'0' Zfl 866S' ZT8'9 TLT'T OP6Z' 896T' SE8I' T8t0' Tfi PST'T tZO'T ZDIS8' DT86' tOt,6' DiSS8' 8829" QS2ic 6900' 690' OTO' 6200' 8T00" Ttl00' E000" AaQS t,86S' SEL'9 S9T'T £T6Z' 8S6T' ZTSIi" T8D0' a6A-� wdd wdd wdd wdd wdd wdd wdd SgTur; FDW x a3 n0 aD 00 PJ waTS 9EE'T T78Ii0' OE6'T 6£00' 198' It, TOT' Z: 099'DID, E# 9S£'T Z6t0' ZS6'T Stl00' ME'tD, LTT'Z 68U H, Z# 9SE'T Z6t0' £96'T ST700' E80'ED, 6PT'Z ZLrv'bt, I# T9S8' 96L8' 1,998'. SS6'L 06£6'Z 6DT'I L91T£' GSH% ZTO' X000' LTO' £000' L9Z'T tlZO' 6ET' AaQS 61,E'T 68t0' 6t,6'I E600' ETT'£Ii ZZT'Z LOS 'b� abAV Ladd wdd wdd wdd qdd wdd qdd SgTun ag 12g g 068TSV TV 6`d waTg Svc S �7' M I : aOg0a3 • aaOD ONO, po vOOrIS,Z : - wo 9S=6Z=9T SO/bT/ZT :awes un O0 :aolpaod0 SWH900-8TZZTSO :awpN aTdwps TdrID :poLpa I a62d Wd LT: LE: b0 SO/PT/ZT gaoda21 sisAlpu nalysis Report 12/14/05 04:44:44 PM ethod: CLP1 Sample Name: 0512218-006ESD Operator: CO un Time: 12/14/05 16:37:23 om, t: TSL004 KVJ - 9 S SD 51�z od' --ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .18925 .0180 -.60333 -.0004 .0008 -.0000 SDev .59885 .0035 .44336 :0004 .0002 .0000 %RSD 316.43 19.38 73.486 119.4 21.65 2284. 91 .86458 .0210 -:25455 .0001 .0010 .0000 42 -.27712 .0142 -1.1023 -.0007 .0008 -.0000 43 -.01971 .0190 -.45317 -.0005 .0007 -.0000 Elem Cd Co Cr Cu Fe K Jnits ppm ppm ppm ppm. ppm ppm %vge .0001 .0003 -.0001 .0097 .0394 1.336 SDev .0001 .0001 .0004 .0004 .0008 .007 .RSD 98.95 42.18 273.0 4.189 2.146 .5077 11 .0002 .0004 -.0001 .0101 .0403 1.343 #2 .0001 .0001 -.0006 .0093 .0386 1.330 13 .0000 .0003 .0002 .0099 .0395 1.335 -Ilem Mn Mo Na Ni 2203/1 2203/2 Jnits ppm ppm ppm ppm ppb ppb kv .0022 -.0004 4.732 .0002 .87328 -.03814 3L .0001 .0002 .011 .0001 1.3479 1.22870 '5RSD 6.283 47.60 .2253 29.81 154.35 3221.2 fl .0023 -.0003 4.742 .0003 -.60127 1.3740 k2 .0021 -.0006 4.733 .0002 1.1791 -.86291 k3 .0022 -.0004 4.721 .0002 2.0420 -.62552 ?lem 2068/2 1960/1 1960/2 Si Sn Sr Jnits ppb ppb ppb ppm ppm ppm �vge .16693 -1.2140 1.1180 .1109 -.0013 -.0003 >Dev 59997 .5969 1.3875 .0021 .0015 .0001 ;RSD 359.42 49.168 124.11 1.899 116.5 23.05 E1 .84150 -1.0183 -.18295 .1133 -.0031 -.0002 `-2 -.03366 -.73946 .95856 .1092 -.0004 -.0003 `-3 -.30705 -1.8841 2.5783 .1102 I -.0005 -.0003 :l em T11908 v Zn Pb2203 Sb2068 Se1960 (nits ppb ppm ppm ppb ppb ppb ,v9e -.00682 .0005 .0062 .26541 .58423 .34145 ;Dev .86332 .0003 .0001 .44958 .43235 .77801 RSD 12657. 75.60 1.348 169.39 74.005 227.86 1 .88186 .0008 .0063 .71627 1.0818 -.46112 2 -.84232 .0002 .0062 -.18287 .29993 .39313 -.06000 .0003 .0061 .26283 .37097 1.0923 page 1 Ca PPM .3075 .0022 .7094 .3099 .3056 .3072 Mg PPM .1260 .0041 3.283 .1294 .1214 .1272 2068/1 ppb 1.4200 .4001 28.176 1.5630 .96806 1.7290 Ti PPM .0000 .0001 345.9 .0001 -.0000 .0000 O O 07 H nalysis Report .0313 12/14/05 04:52:10 PM ethod: CLP1 Sample Name: 0512218-001E .0270 Operator: CO un ' me: 12/14/05 16:44:50 .0012 .0005 .0574 om t: TSL004 .0000 1 W 1 ILA .0001 .0002 od=: C.ONC Corr. Factor: 1 6.501 6.335 25.28 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm hvge .24622 .0298 .61889 .0019 .0007 -.0000 SDev .45212 .0024 1.3709 .0001 .0001 .0000 %RSD 183.62 8.182 221.51 4.976 13.46 125.0 41 -.14462 .0313 42 .74138 .0311 43 .14190 .0270 page 1 Ca PPM .6263 .0003 .0442 1.8089 .0019 .0008 .0000 .6264 .92793 .0019 .0007 -.0000 .6264 -.88012 .0018 .0006 -.0000 .6259 Cd Co Cr Cu Fe K PPM ppm ppm ppm ppm ppm .0001 .0012 .0005 .0574 .1651 .3614 .0000 .0001 .0001 .0002 .0007 .0052 6.501 6.335 25.28 .3854 .4162 1.434 .0001 .0012 .0006 .0576 .1654 .3589 .0001 .0013 .0007 .0574 .1655 .3674 .0001 .0012 .0004 .0571 .1643 .3580 Mn Mo Na Ni 2203/1 2203/2 PPM ppm ppm ppm ppb ppb .0033 -.0004 21.03 .0010 1.6309 1.0569 .0001 .0004 .14 .0002 1.3693 1.1261 1.782 114.5 .6566 23.21 83.959 106.54 .0034 -.0007 21.16 .0008 3.1269 -.02443 .0034 .0001 20.88 .0012 .43979 2.2229 .0033 -.0007 21.05 .0009 1.3260 .97235 2068/2 1960/1 1960/2 Si Sn Sr ppb ppb ppb ppm ppm ppm .90286 3.8554 -.54704 1.281 -.0010 .0006 .70823 2.2562 1.13848 .004 .0008 .0000 78.443 58.520 208.12 .3424 80.42 .6377 1.3719 5.9798 -1.7116 1.286 -.0014 .0006 1.2486 1.4873 .56347 1.278 -.0001 .0006 .08817 4.0991 -.49302 1.278 -.0015 .0006 T11908 v Zn Pb2203 Sb2068 Se1960 ppb ppm ppm ppb ppb ppb 2.1631 .0003 .0176 1.2481 .32209 .91898 .7827 .0002 .0000 .3316 1.1167 .10206 36.183 62.30 .0339 26.569 346.70 11.106 1.8822 .0001 .0176 1.0250 .37348 .84966 3.0475 .0005 .0176 1.6292 1.4122 .87111 1.5596 .0004 .0176 1.0902 -.81940 1.0362 Mg PPM .1701 .0014 .7969 .1703 .1713 .1686 2068/1 ppb -.84124 2.29176 272.43 -1.6263 1.7399 -2.6373 Ti PPM .0002 .0000 14.86 .0002 .0002 .0001 nalysis Report 12/14/05 04:59:37 PM page 1 ethod: CLP1 Sample Name: 0512218-002E Operator: CO un Time: 12/14/05 16:52:17 on t: TSL004 i , oL-_ CONC Corr. Factor: 1 M Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .33300 .0285 -.61256 .0027. .0004 -.0000 .4445 SDev .24275 .0015 1.09335 .0003 .0000 .0000 .0012 %RSD 72.897 5.389 178.49 9.620 9.260 17.80 .2657 ##1 .55690 .0272 -.12590 .0030 .0004 -.0000 .4454 ##2 .07501 ..0281 .15297 .0026 .0004 -.0000 .4431 #3. .36711 .0302 -1.8647 .0025 .0003 -.0000 .4449 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0000 .0006 .0001 .1039 .0787 .3512 .1215 SDev .0001 .0002 .0003 .0004 .0001 .0066 .0006 %RSD 5635. 32.35 341.6 .3851 .0840 1.883 .5066 #1 .0000 .0008 .0004 .1041 .0787 .3588 .1222 42 .0000 .0004 -.0001 .1034 .0788 .3484 .1212 43 -.0001 .0006 -.0001 .1041 .0787 .3465 .1211 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb A' .0018 -.0002 21.10 .0001 1.8057 1.1910 2.6347 S: .0001 .0002 .07 .0002 2.4026 1.1349 .7522 %RSD 3.908 100.6 .3529 224.2 133.06 95.296 28.550 #1 .0019 -.0001 21.18 .0001 .54671 .86796 3.4022 42 .0018 -.0001 21.04 .0003 4.5762 .25255 1.8988 43 .0017 -.0004 21.07 -.0001 .29418 2.4524 2.6030 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.5244 -4.0268 .79865 1.206 -.0008 .0001 .0006 SDev 1.5491 3.3772 .76409 .003 .0014 .0000 .0001 %RSD 101.62 83.867 95.672 .2848 177.5 25.84 10.17 41 1.3636 -3.9257 1.3735 1.209 .0003 .0001 .0007 42 3.1476 -.70132 1.0909 1.203 -.0003 .0001 .0006 #3 .06203 -7.4534 -.06843 1.205 -.0023 .0001 .0006 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.0447 .0004 .0170 1.3957 1.8941 -.80822 SDev .7284 .0000 .0001 .5500 .9208 1.55344 oRSD 69.724 9.641 .6395 39.409 48.612 192.21 41 1.8455 .0005 .0171 .76106 2.0425 -.39114 #' .86690 .0004 .0171 1.6924 2.7318 .49411 # .42165 .0005 .0169 1.7338 .90820 -2.5276 00 O O DO N nalysis Report 12/14/05 05:07:04 PM ethod: CLP1 Sample Name: 0512218-003E un Time: 12/14/05 16:59:44 om `..: TSL004 Ca PPM 3' od --"ONC Corr. Factor: 1 .0000 Elem Ag Al As1890 B Units ppb ppm ppb ppm Avge .09955 .0309 3.1949 .0053 SDev .47079 .0024 .6206 .0004 %RSD 472.91 7.822 19.423 7.740 #1 .51079 .0336 3.9100 .0057 42 -.41397 .0296 2.7976 .0049 43 .20183 .0293 2.8772 .0054 Elem Cd Co Cr Cu Units ppm ppm ppm ppm kvge .0001 .0010 .0004 .0313 SDev .0001 .0000 .0001 .0003 6RSD 124.3 4.123 31.20 .8161 41 .0000 .0011 .0003 .0315 42 .0000 .0010 .0006 .0314 43 .0001 .0010 .0005 .0310 Mn PPM .0041 .0001 1.737 .0040 .0041 .0042 2068/2 ppb -.92408 .93774 101.48 -2.0024 -.30006 -.46973 T11908 ppb .39942 .67380 168.69 Mo PPM -.0006 .0002 34.07 -.0003 -.0006 -.0007 1960/1 ppb 3.6392 1.5216 41.811 2.0715 5.1100 3.7362 v PPM .0002 .0004 148.7 Na PPM 23.07 .2ti .8505 23.16 23.19 22.84 1960/2 ppb 2.5438 .7078 27.825 3.0944 1.7454 2.7917 Zn PPM .0192 .0001 .3604 -.27863 .0004 .0192 .40801 -.0002 .0192 1.0689 .0005 .0191 Ni PPM .0009 .0006 63.10 .0005 .0016 .0007 Si PPM 1.380 .010 .7313 1.388 1.384 1.369 Pb2203 ppb .79025 .29091 36.812 1.1261 .62873 .61594 Operator: CO page 1 Ba Be Ca PPM ppm ppm .0007 -.0000 .9879 .0000 .0000 .0036 6.358 5.865 .3650 .0006 -.0000 .9908 .0007 -.0000 .9890 .0007 -.0000 .9838 Fe PPM .1985 .0009 .4581 .1994 .1987 .1976 2203/1 ppb .28360 .83248 293.54 -.26674 1.2413 -.12377 Sn PPM -.0024 .0015 62.43 -.0040 -.0018 -.0013 Sb2068 ppb -.05924 .45290 764.50 -.32241 -.31903 .46372 K PPM 6.610 .046 .6953 6.622 6.649 6.559 2203/2 ppb 1.0431 .7510 71.996 Mg PPM 1.166 .003 .2605 1.169 1.166 1.163 2068/1 ppb 1.6730 1.7935 107.20 1.8214 3.0427 .32279 -.35708 .98513 2.3334 Sr Ti PPM ppm .0010 -.0001 .0000 .0000 2.283 72.18 .0010 -.0001 .0010 -.0000 .0011 -.0000 Se1960 ppb 2.9086 .1801 6.1920 2.7538 2.8658 3.1063 N 00 O O F-+ nalysis Report 12/14/05 05:14:30 PM page 1 =thod: CLP1 Sample Name: 0512218-004E Operator: CO in Time: 12/14/05 17:07:10 DMI, TSL004� ado 'ONC Corr. Factor: 1 7 J Tem Ag Al As1890 B Ba Be Ca hits ppb ppm ppb ppm ppm ppm ppm kvge .24486 .0349 .33985 .0013 .0005 -.0000 .6181 3Dev .29405 .0052 .70127 .0004 .0001 .0000 .0041 '6RSD 120.09 14.79 206.35 29.61 10.37 97.89 .6618 #1 -.08163 .0290 .34261 .0009 .0005 -.0000 .6148 #2 .48882 .0379 -.36280 .0013 .0005 -.0000 .6169 13 .32740 .0379 1.0397 .0017 .0006 -.0000 .6227 ,lem Cd Co Cr Cu Fe K Mg 7nits ppm ppm ppm ppm ppm ppm ppm vge .0001 .0010 .0001 .0506 .1710 .3330 .1551 'Dev .0001 .0003 .0002 .0006 .0019 .0073 .0036 sRSD 264.5 26.32 236.9 1.119 1.126 2.203 2.343 fi .0002 .0010 .0001 .0502 .1690 .3361 .1539 k2 .0001 .0008 -.0001 .0503 .1712 .3246 .1522 k3 -.0001 .0013 .0003 .0512 .1728 .3382 .1592 'lem Mn Mo Na Ni 2203/1 2203/2 2068/1 snits ppm ppm ppm ppm ppb ppb ppb LvI .0028 -.0004 20.31 .0008 -.17940 1.3505 1.4687 D .0001 .0002 .10 .0003 2.03379 1.5068 .9014 :RSD 4.426 54.19 .4799 34.96 1133.7 111.58 61.372 :1 .0028 -.0005 20.24 .0007 1.6891 -.29732 .61762 2 .0027 -.0005 20.27 .0011 -2.3457 2.6582 2.4131 :3 .0029 -.0001 20.42 .0006 .11837 1.6906 1.3754 lem 206.8/2 1960/1 1960/2 Si Sn Sr Ti nits ppb ppb ppb ppm ppm ppm ppm .vge .27949 .09846 .00619 1.277 -.0019 .0007 .0001 Dev .64066 1.0869 .34207 .010 .0006 .0000 .0001 RSD 229.23 1103.9 5528.1 .8162 32.39 6.048 162.9 1 .98534 .75898 .26990 1.267 -.0026 .0006 .0001 2 -.26520 -1.1560 .12899 1.277 -.0016 .0006 -.0001 3 .11833 .69244 -.38033 1.287 -.0015 .0007 .0002 lem T11908 v Zn Pb2203 Sb2068 Se1960 nits ppb ppm ppm ppb ppb ppb vge .57760 .0003 .0156 .84110 .67552 .03693 Dev .21562 .0001 .0003 .42217 .16838 .36952 RSD 37.329 28.83 1.618 50.192 24.926 1000.7 1 .81935 .0003 .0154 .36423 .86291 .43278 2 .40518 .0003 .0156 .99196 .62670 -.29891 3% 50828 .0002 .0159 1.1671 .53694 -.02310 M 00 O O COO F-+ nalysis Report 12/14/05 05:21:57 PM page 1 ethodr CLP1 Sample Name: CCV2 Operator: CO ur. Time: 12/14/05 17:14:37 on t: TSL004 od- CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1001.0 52.07 508.71 2.360 2.462 2.449 51.94 SDev 8.2 .43 4.80 .017 .019 .014 .29 %RSD .81980 .8235 .94451 .7333 .7781 .5799 .5581 #1 1007.2 52.33 510.25 2.371 2.479 2.459 52.08 #2 1004.2 52.30 512.55 2.368 2.467 2.454 52.13 43 991.71 51.57 503.32 2.340 2.442 2.432 51.61 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge 2.421 2.427 2.428 2.465 51.58 86.49 52.28 Mev .012 .0.14 .015 .023 .34 .75 .32 %RSD .5019 .5833 .6215 .9145 .6544 .8620 .6115 41 2.428 2.436 2.437 2.483 51.81 86.84 52.46 42 2.429 2.434 2.436 2.471 51.74 87.00 52.48 $= 2.407 2.411 2.410 2.439 51.19 85.64 51.91 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh 2.750 2.750 2.750 2.750 55.00 88.00 55.00 mow 2.250 2.250 2.250 2.250 45.00 72.00 45.00 31em Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb 3vge 2.424 2.468 83.15 2.420 511.02 496.57 992.39 3Dev .015 .017 .75 .012 1.49 3.15 10.37 RSD .6218 .6737 .9014 .4834 .29246 .63371 1.0453 f1 2.434 2.478 83.37 2.426 512.50 499.94 1003.8 f2 2.430 2.477 83.77 2.426 511.05 496.07 989.72 k3 2.406 2.449 82.32 2.406 509.52 493.71 983.61 ;rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK sigh 2.750 88.00 2.750 Jow 2.250 72.00 2.250 ;lem 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm ppm ppm ppm ivge 982.58 514.60 510.72 1.842 2.414 2.466 2.441 >Dev 7.74 1.04 2.93 .009 .014 .019 .016 Izt ;RSD .78759 .20163 .57439 .5009 .5646 .7726 .6683 E1 990.05 515.67 513.34 1.843 2.423 2.483 2.453 12 983.10 514.52 511.27 1.852 2.421 2.471 2.447 13 974.60 513.60 507.55 1.833 2.398 2.445 2.422 :rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 05:21:57 PM Hinh Lc Elem T11908 v Zn Pb2203' Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 499.93 2.445 2.537 501.38 985.85 512.01 SDev 4.09 .017 .017 2.59 8.53 2.29 %RSD .81875 .6881 .6793 .51696 .86566 .44810 #1 502.56 2.457 2.550 504.12 994.64 514.12 #2 502.02 2.451 2.543 501.06 985.30 512.35 ##3 495.22 2.426 2.517 498.97 977.60 509.57 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 in 00 �t O O cn H nalysis Report 12/14/05 05:29:24 PM page 1 ethod: CLP1 Sample Name: CCVL2 Operator: CO un Time: 12/14/05 17:22:04 DH t: TSL004 Dd_. CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm kvge .63443 .0249 -.75894 .0153 .0005 .0005 .0448 3Dev .51335 .0032 1.52561 .0009 .0002 .0002 .0042 .RSD 80.916 12.95 201.02 5.620 39.76 31.09 9.281 �1 .50917 .0285 .03603 .0162 .0008 .0007 .0495 12 1.1988 .0240 -2.5179 .0149 .0004 .0005 .0427 �3 .19529 .0222 .20501 .0147 .0005 .0004 .0420 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK -sigh JOw 7lem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge .0006 .0004 .0003 .0010 2.565 .0596 .0099 'Dev .0003 .0008 .0006 .0006 .003 .0192 .0066 'lRSD 53.19 229.2 217.0 57.26 .1189 32.17 67.22 #1 .0010 .0009 .0006 .0016 2.569 .0722 .0153 f2 .0003 -.0006 -.0004 .0004 2.563 .0376 .0025 f: .0006 .0009 .0005 .0012 2.564 .0691 .0118 'rrors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK sigh 2.750 -low 2.250 'sl em Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb ►vge .0003 .0025 2.673 -.0002 -1.1262 .55156 1.4336 ;Dev .0003 .0011 .023 .0005 3.7984 1.9481 3.5864 ;RSD 130.6 44.96 .8672 297.1 337.26 353.20 250.16 1-1 .0005 .0035 2.699 .0000 -1.6503 1.4065 .85741 2 -.0001 .0026 2.654 -.0008 -4.6354 1.9260 5.2733 3 .0004 .0013 2.665 .0002 2.9070 -1.6778 -1.8297 :rrors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK [igh 2.750 low 2.250 :lem 2068/2 1960/1 1960/2 Si Sn Sr Ti [nits ppb ppb ppb ppm ppm ppm ppm .vge .08951 .43682 1.5089 -.1030 -.0005 -.0001 .0004 Dev 1.8836 5.2043 1.8392 .0023 .0009 .0002 .0003 RSD 2104.4 1191.4 121.89 2.197 171.4 312.0 89.68 .64787 .91018 1.5897 -.1007 -.0003 .0002 .0007 -2.0102 -4.9880 -.36941 -.1031 -.0015 -.0002 .0000 3 1.6308 5.3883 3.3062 -.1053 .0002 -.0001 .0004 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 110 00 d - O O C/) F-+ nalysis Report 12/14/05 05:29:24 PM page 2 High Zn Lc Sb2068 Elem T11908 Units ppb Avge 2.7835 SDev 1.0383 %RSD 37.302 #1 3.8146 #2 1.7382 93 2.7975 Errors NOCHECK High 29.698 Low .0008 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0009 .0035 -.00711 .53713 1.1519 .0003 .0002 .34694 .15951 2.9592 33.44 6.027 4879.5 29.698 256.90 .0008 .0038 .38864 .71766 1.3634 .0013 .0034 -.25892 .41523 -1.9074 .0007 .0035 -.15105 .47849 3.9996 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 05:36:51 PM page 1 ethod: CLP1 Sample Name: CCB2 Operator: CO un Time: 12/14/05 17:29:31 om L: TSL004 od --ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .12637 .0081 -.28306 -.0019 .0001 .0001 .0323 SDev .22432 .0014 .93268 .0004 .0001 .0001 .0012 oRSD 177.51 17.77 329.50 19.99 51.08 53.25 3.671 #1 .38280 .0091 -.16627 -.0019 .0002 .0002 .0336 #2 .02979 .0088 -1.2686 -.0015 .0001 .0001 .0319 #3 -.03349 .0064 .58572 -.0022 .0001 .0001 .0313 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm , ppm _. ppm ppm ppm ppm Avge .0002 .0001 -.0001 .0005 .0032 .0455 .0025 SDev .0001 .0002 .0002 .0001 .0014 .0022 .0020 6RSD 43.65 107.8 403.1 22.54 43.81 4.742 78.11 41 .0003 .0003 -.0`0'0-2 .0006 .0047 .0443 .0035 42 .0002 .0000 .0002 .0005 .0027 .0480 .0038 �3 .0001 .0001 - ..0G.0.1 .0004 .0021 .0443 .0003 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Clem Mn Mo Na Ni 2203/1 2203/2 2068/1 snits ppm ppm ppm. ppm ppb ppb ppb Wge .0001 -.0000 .0261 -.0002 -.49268 .57422 .28066 SDev .0001 .0001 .0052 .0002 1.70611 1.3646 1.8352 'RSD 73.21 369.7 19.90 122.4 346.29 237.64 653.89 41 .0002 .0001 .0317 .0001 -2.4617' 1.9925 2.2763 #2 .0001 -.0002 .0254 -.0004 .54749 -.72932 -1.3344 #3 .0000 -.0000 .0213 -.0003 .43613 .45943 -.09993 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK sigh .0150 5.000 .0400 mow -.0150 -5.000 -.0400 slem 2068/2 1960/1 1960/2 Si Sn Sr Ti 7nits ppb ppb ppb ppm ppm ppm ppm kvge .61125 1.6068 -.87194 -.2189 -.0000 -.0005 -.0001 SDev 1.4312 2.6099 1.29388 .0013 .0008 .0000 .0000 '),RSD 234.15 162.42 148.39 .5733 1754. 9.414 32.77 f1 .27138 1.3352 -1.6775 -.2180 .0001 -.0004 -.0001 k2 2.1818 4.3419 -1.5589 -.2182 .0006 -.0005 -.0001 k3 -.61946 -.85660 .62053 -.2203 -.0009 -.0005 -.0002 ;rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 00 O O H nalysis Report 12/14/05 05:36:51 PM Elem T11908 v Zn Pb2203 Sb2068 Se1960 Jnits ppb ppm ppm ppb ppb ppb 3vge .84199 .0002 .0021 .21898 .50118 -.04650 3Dev .84866 .0002 .0002 .45392 .82145 .56105 '6RSD 100.79 138.3 8.223 207.29 163.90 1206.5 41 1.0559 .0003 .0023- .50932 .93904 -.67424 12 1.5632 -.0001 .0020 -.30410 1.0109 .40607 43 -.09315 .0003 .0020 .45171 -.44644 .12867 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh 10.000 .0500 .0200 3.0000 60.000 5.0000 1,ow -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 .nalysis Report 12/14/05 05:44:17 PM iethod: CLP1 Sample Name: 0512218-005E Operator: CO .un Time: 12/14/05 17:36:57 ,or it: TSL004 ,� AA NI :o( CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .69795 .0701 3.2924 .0046 .0012 .0001 SDev .70726 .0069 .3881 .0006 .0000 .0000 %RSD 101.33 9.791 11.787 12.89 2.858 30.95 ##1 1.4417 .0780 3.5295 .0053 .0012 .0001 #2 .61811 .0670 3.5031 .0044 .0011 .0001 #3 .03399 .0654 2.8445 .0042 .0012 .0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0002 .0.012 .0003 .0360 .2221 7.626 SDev .0001 .0003 .0002 .0001 .0024 .'026 %RSD 81.07 23.01 57.96 .2546 1.063 .3429 41 .0000 .0014 .0004 .0360 .2248 7.646 42 .0003 .0012 .0004 .0360 .2205 7.597 43 .0002 .0009 .0001 .0359 .2209 7.637 E,lem Mn Mo Na Ni 2203/1 2203/2 Jnits ppm ppm ppm ppm ppb ppb k, .0116 -.0001 24.48 .0020 .04487 2.6591 31 .0001 .0005 .07 .0003 .71038 .3507 'RSD 1.266 598.6 .2801 15.90 1583.2 13.190 #1 .0117 .0004 24.51 .0023 -.75857 3.0638 #2 .0116 -.0001 24.41 .0019 .30342 2.4700 #3 .0114 -.0005 24.54 .0017 .58976 2.4434 71 em 2068/2 1960/1 1960/2 Si Sn Sr 7nits ppb ppb ppb ppm ppm ppm 3vge .13491 4.1747 6.2608 1.296 -.0015 .0012 SDev .54535 1.3059 1.3769 .008 .0010 .0000 '5RSD 404.24 31.281 21.993 .5950 63.83 2.457 f1 .43541 3.1418 4.6732 1.305 -.0007 .0012 k2 -.49459 3.7396 6.9798 1.290 -.0026 .0012 k3 .46390 5.6425 7.1294 1.294 -.0013 .0012 'slem T11908 V Zn Pb2203 Sb2068 Se1960 hits ppb ppm ppm ppb ppb ppb ivge -.63434 .0004 .0145 1.7886 1.3652 5.5661 )Dev .53808 .0001 .0001 .0389 .4351 1.269.1 ;RSD 84.826 34.00 .9668 2.1733 31.871 22.800 =1 -.11475 .0006 .0147 1.7910 1.8649 4.1633 :? -1.1892 .0003 .0145 1.7486 1.0698 5.9008 -.59908 .0004 .0144 1.8262 1.1611 6.6343 page 1 Ca PPM 1.437 .011 .7618 1.449 1.428 1.433 Mg PPM .6761 .0057 .8507 .6826 .6717 .6739 2068/1 ppb 3.8295 1.1325 29.574 4.7281 4.2032 2.5574 Ti PPM .0006 .0001 20.29 .0007 .0007 .0005 nalysis Report 12/14/05 05:51:44 PM ethod: CLP1 Sample Name: 0512218-007E PPM Operator: CO Up `ime: 12/14/05 17:44:24 21.35 .0001 .0006 .07 DIT 't: TSL004 .3134 �n � W -5D JO.:.. = CONC Corr. Factor: 1 r Elem Ag Al As1890 B Ba Be Jnits ppb ppm ppb ppm ppm ppm kvge .22772 .0325 -.88773 .0016 .0006 .0000 Mev .19530 .0047 .66483 .0002 .0000 .0000 ''vRSD 85.761 14.63 74.891 13.81 6.350 74.36 '1 .39709 .0272 -.22580 .0014 .0007 .0000 12 .01410 .0338 -1.5554 .0015 .0006 .0000 13 .27197 .0364 -.88197 .0018 .0006 .0000 Cd PPM. .0001 .0001 61.08 .0001 .0000 .0001 Co PPM .0010 .0001 14.51 .0010 .0008 .0011 Cr PPM .0004 .0001 26.90 .0006 .0003 .0004 Mn Mo Na PPM ppm ppm .0032 -.0002 21.35 .0001 .0006 .07 1.402 270.8 .3134 .0032 .0032 .0032 2068/2 ppb -.51269 1.77733 346.67 .98593 -.04771 -2.4763 T11908 ppb .74814 .73060 97.655 1.0267 1.2985 -.08076 -.0007 -.0003 .0004 1960/1 ppb -1.9851 1.5301 77.078 -3..2248 -.27507 -2.4555 v PPM .0004 .0001 38.69 .0005 .0003 .0003 21.38 21.27 21.39 1960/2 ppb .56518 2.2011 389.46 -1.2286 -.09733 3.0215 Zn PPM .0165 .0001 .4593 .0164 .0165 .0166 Cu PPM .0324 .0001 .4746 .0324 .0322 .0325 Ni PPM .0014 .0004 30.68 .0009 .0017 .0016 Si PPM 1.363 .003 .2412 1.360 1.363 1.367 Pb2203 ppb 1.2504 .5895 47.141 1.7201 .58894 1.4422 Fe PPM .2414 .0013 .5228 .2399 .2423 .2419 2203/1 ppb 2.3324 .8339 35.753 3.2267 2.1945 1.5761 K PPM .3603 .0048 1.329 .3650 .3554 .3605 2203/2 ppb .71010 .82474 116.14 .96784 -.21273 1.3752 page 1 Ca PPM .7400 .0018 .2460 .7380 .7406 .7415 Mg PPM .1873 .0005 .2801 .1877 .1867 .1876 2068/1 ppb .72457 1.8422 254.24 -.00506 -.64103 2.8198 Sn Sr Ti PPM ppm ppm -.0006 .0009 .0006 .0011 .0000 .0001 196.7 2.040 17.28 -.0014 -.0011 .0007 Sb2068 ppb -.10066 .69568 691.10 .65595 -.24527 -.71268 Se1960 ppb -.28407 1.54944 545.44 -1.8933 -.15652 1.1977 aalysis Report 12/14/05 05:59:11 PM page 1 ethod: CLP1 Sample Name: 0512218-008E Operator: CO .in 'r4me: 12/14/05 17:51:51 DMI ; : TSL004 �� Ddt.. -'ONC Corr. Factor: 1 Clem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm %vge .30832 .0304 -1.2738 .0018 .0006 .0000 .7523 3Dev .22501 .0014 .2477 .0001 .0001 .0000 .0011 '.RSD 72.979 4.549 19.445 4.227 7.676 2118. .1463 11 .14552 .0290 -.99302 .0017 .0006 .0000 .7511 12 .56508 .0317 -1.3669 .0018 .0005 -.0000 .7527 13 .21437 .0304 -1.4614 .0017 .0006 .0000 .7532 Clem Cd Co CrCu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge .0002 .0011 .0002 .0286 .2388 .3622 .1867 3Dev .0001 .0001 .0002 .0001 .0008 .0019 .0007 DIRSD 52.05 8.583 77.17 .2318 .3328 .5337 .3964 .0003 .0001 .0002 Mn PPM .0032 .0001 1.582 .0032 .0032 .0032 2068/2 ppb -.52581 3.09515 588.65 2.6443 -3.5401 -.68160 T11908 ppb .08163 .67009 820.88 -.67623 .32544 .59568 .0011 .0010 .0011 Mo PPM -.0005 .0001 20.00 -.0004 -.0005 -.0005 1960/1 ppb -2.3713 1.7460 73.630 -3.6219 -3.1157 -.37650 v PPM .0001 .0003 240.6 -.0002 .0003 .0003 .0002 .0001 .0005 Na PPM 21.24 .07 .3284 21.24 21.31 21.17 1960/2 ppb -.20603 1.89648 920.50 -.09629 1.6332 -2.1550 Zn PPM .0190 .0001 .3405 .0189 .0190 .0190 .0287 .0286 .0287 Ni PPM .0012 .0006 47.20 .0007 .0018 .0011 Si PPM 1.353 .004 .2658 1.352 1.357 1.351 Pb2203 ppb 1.4070 .4545 32.301 1.5672 1.7597 .89412 .2380 .2396 .2387 2203/1 ppb 2.0353 1.5032 73.856 .52650 3.5328 2.0466 Sn PPM -.0015 .0007 44.15 -.0021 -.0016 -.0008 Sb2068 ppb -.16052 2.09046 1302.3 1.9099. -2.2704 -.12105 .3617 .3607 .3644 2203/2 ppb 1.0932 .9041 82.706 2.0867 .87430 .31862 Sr PPM .0009 .0000 3.141 .0009 .0009 .0010 Se1960 ppb -.92708 .86028 92.794 -1.2703 .05183 -1.5628 .1866 .1875 .1861 2068/1 ppb .57110 .38204 66.896 .43895 .27268 1.0017 Ti PPM .0007 .0000 3.855 .0007 .0007 .0008 aalysis Report 12/14/05 06:06:38 PM page 1 =thod: CLP1 Sample Name: 0512218-009E Operator: CO .in "me: 12/14/05 17:59:18 DMI. :: TSL004 12ONC Corr. Factor: (Aw-& Ddc . 1 Elem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm ),vge .37016 .0643 1.7752 .0033 .0009 .0000 1.162 3Dev .54772 .0042 .7021 .0003 .0000 .0000 .005 6RSD 147.97 6.472 39.551 7.839 3.211 53.28 .4057 #1 .90433 .0615 .98581 .0031 .0008 .0000 1.158 #2 -.19017 .0622 2.0098 .0032 .0009 .0000 1.161 #3 .39630 .0691 2.3299 .0036 .0009 .0000 1.167 ;lemCd Co Cr Cu Fe K Mg 7nits ppm ppm ppm ppm ppm ppm ppm vge .0000 .0009 .0004 .0429 .2278 5.394 .4640 'Dev .0001 .0003 .0001 .0003 .0012 .007 .0029 >RSD 253.5 32.78 44.09 .7412 .5231 .1261 .6364 k1 .0001 .0007 .0004 .0426 .2268 5.387 .4629 k2 -.0000 .0007 .0005 .0432 .2274 5.400 .4618 k3 .0000 .0012 .0002 .0431 .2291 5.394 .4674 :lem Mn Mo Na Ni 2203/1 2203/2 2068/1 hits ppm ppm ppm ppm ppb ppb ppb ,v .0078 -.0004 22.64 .0011 1.6927 1.9059 1.2007 ;D .0001 .0003 .05 .0003 1.2697 .8841 1.2916 :RSD .9070 64.44 .2052 25.87 75.013 46.387 107.57 :1 .0077 -.0007 22.60 .0013 .75612 1.4108 1.9660 .2 .0078 -.0005 22.69 .0008 3.1379 1.3803 -.29052 3 .0078 -.0001 22.65 .0011 1.1841 2.9266 1.9267 ;lem 2068/2 1960/1 1960/2 Si Sn Sr Ti "nits ppb ppb ppb ppm ppm ppm ppm .vge -.23575 -2.5811 3.7863 1.288 -.0011 .0011 .0012 Dev 2.63635 2.0538 .3564 .006 .0009 .0000 .0000 RSD 1118.3 79.573 9.4142 .4837 80.81 3.703 2.720 1 1.0023 -2.3575 3.3747 1.282 -.0014 .0010 .0012 2 1.5537 -.64815 3.9899 1.287 -.0018 .0011 .0012 3 -3.2632 -4.7375 3.9942 1.294 -.0001 .0011 .0012 lem T11908 v Zn Pb2203 Sb2068 Se1960 nits ppb ppm ppm ppb ppb ppb vge -.12196 .0005 .0231 1.8349 .24260 1.6660 Dev .87748 .0003 .0002 .5878 1.5513 .7012 RSD 719.48 54.80 .7630 32.032 639.46 42.091 1 -1.1347 .0007 .0230 1.1928 1.3232 1.4659 2 .41281 .0002 .0231 1.9656 .93958 2.4455 3 .35597 .0005 .0233 2.3464 -1.5350 1.0865 nalysis Report 12/14/05 06:14:05 PM ethod: CLP1 Sample Name: 0512218-010E Operator: CO up 'Time: 12/14/05 18:06:45 on t: TSL004 oe__ CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .13820 .0454 .17118 .0015 .0006 -.0000 SDev .17237 .0006 .25007 .0002 .0000 .0000 0RSD 124.72 1.379 146.09 12.58 4.300 70.02 41 -.05245 .0453 .04938 .0016 .0007 -.0000 42 .28304 .0448 .00535 .0013 .0007 -.0000 43 .18402 .0461 .45881 .0016 .0006 -.0000 3lem Cd Co Cr Cu Fe K Jnits ppm ppm ppm . ppm ppm ppm kvge .0001 .0009 .0000 .0614 .1875 1.596 SDev .0001 .0001 .0002 .0004 .0006 .010 'RSD 120.6 14.37 798.1 .6874 .2953 .6157 #1 .0002 .0009 -.0001 .0618 .1881 1.606 t2 .0002 .0008 .0003 .0614 .1875 1.597 f3 -.0000 .0010 -.0000 .0609 .1870 1.586 ,lem Mn Mo Na Ni 2203/1 2203/2 Tnits ppm ppm ppm ppm ppb ppb �v .0039 -.0006 20.91 .0011 .71509 .89335 3L .0001 .0004 .14 .0002 .43843 .10218 ;RSD 1.506 65.77 .6911 15.57 61.311 11.438 =1 .0040 -.0002 21.07 .0010 .42623 .93061 =2 .0040 -.0010 20.88 .0013 1.2196 .97168 :3 .0039 -.0005 20.79 .0010 .49946 .77777 ;lem 2068/2 1960/1 1960/2 Si Sn Sr rnits ppb ppb ppb ppm ppm ppm .vge -.35373 -1.5064 1.1960 1.260 -.0014 .0009 Dev .11257 .4115 2.4038 .006 .0001 .0000 RSD 31.824 27.319 200.99 .5077 7.391 2.749 1 -.45870 -1.1680 3.9701 1.266 -.0015 .0009 2 -.23485 -1.9645 -.27169 1.260 -.0013 .0009 3 -.36765 -1.3867 -.11048 1.253 -.0015 .0009 lem T11908 v Zn Pb2203 Sb2068 Se1960 nits ppb ppm ppm ppb ppb ppb vge .05009 .0003 .0215 .83401 -.22403 .29607 Dev .40769 .0002 .0001 .19463 .28871 1.7066 RSD 813.87 64.60 .3712 23.337 128.87 576.42 1 -.42024 .0001 .0215 .76267 -.02627 2.2591 2 .30271 .0005 .0216 1.0542 -.09049 -.83541 3 .26781 .0002 .0214 .68511 -.55534 -.53545 page 1 Ca PPM .8465 .0038 .4441 .8493 .8481 .8422 Mg PPM .2488 .0033 1.310 .2497 .2516 .2452 2068/1 ppb .03574 .89678 2509.2 .83988 .19867 -.93134 Ti PPM .0002 .0001 24.34 .0002 .0003 .0002 nalysis Report 12/14/05 06:21:32 PM page 1 athod: CLP1 Sample Name: 0512218-011E ppm Operator: CO .0182 in Time: 12/14/05 18:14:12 83.84 1.534 DIT 't: TSL0 04 14 vj, Jc CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm kvge .20022 .0354 -.05502 .0016 .0007 -.0000 .7587 3Dev .57622 .0016 .46551 .0001 .0000 .0000 .0092 MSD 287.79 4.628 846.05 7.943 6.134 22.62 1.206 41 .30607 .0337 .33379 .0015 .0007 -.0000 .7686 42 -.42158 .0355 .07201 .0015 .0007 -.0000 .7568 �3 .71618 .0369 -.57086 .0017 .0007 -.0000 .7506 31em Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm kvge .0001 .0012 .0004 .0324 .2421 .3480 .1866 3Dev .0001 .0001 .0001 .0007 .0029 .0086 .0027 oRSD 56.33 7.887 29.67 2.023 1.203 2.486 1.475 .0001 .0012 .0006 .0331 .0000 .0013 .0003 .0324 .0001 .0011 .0004 .0318 Mn PPM .0031 .0001 1.638 .0031 .0030 .0030 2068/2 ppb -.92514 2.41517 261.06 -.50637 1.2533 -3.5223 T11908 ppb .54804 .78871 143.91 Mo PPM -.0004 .0004 103.2 -.0007 .0000 -.0005 1960/1 ppb -.26972 1.12674 417.74 .69422 .00504 -1.5084 Na PPM 20.51 .22 1.096 20.75 20.49 20.30 1960/2 ppb -1.1530 1.2502 108.43 .25313 -1.5729 -2.1392 v Zn PPM ppm .0003 .0182 .0003 .0003 83.84 1.534 Ni PPM .0012 .0003 22.73 .0010 .0012 .0015 Si PPM 1.315 .020 1.500 1.335 1.313 1.296 Pb2203 ppb 1.2117 .8013 66.129 .68559 .0001 .0184 .74683 -.30039 .0003 .0183 .75135 1.2589 .0007 .0179 2.1370 .2452 .2417 .2394 2203/1 ppb 1.7276 .7037 40.732 2.2650 1.9867 .93111 Sn PPM -.0006 .0006 93.13 -.0007 -.0000 -.0012 Sb2068 ppb -.35395 1.79871 508.18 .12737 1.1551 -2.3444 .3568 .3477 .3395 2203/2 ppb .95405 1.5474 162.20 -.01124 .13449 2.7389 Sr PPM .0009 .0001 6.078 .0010 .0009 .0009 Se1960 ppb -.85884 1.17597 136.92 .40001 -1.0474 -1.9291 .1891 .1871 .1837 2068/1 ppb .79009 .70607 89.366 1.3967 .95853 .01503 Ti PPM .0006 .0001 20.07 .0007 .0005 .0005 7alysis Report 12/14/05 06:28:59 PM page 1 �thod: CLP1 Sample Name: 0512218-012E Operator: CO .in Tome: 12/14/05 18:21:39 )MI : TSL004 )i k/, OS ,)d(-. -'ONC Corr. Factor: 1 ;sem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm kvge .22481 .0297 -1.2379 .0008 .0006 -.0000 .7405 3Dev .27948 .0033 1.6177 .0004 .0000 .0000 .0016 '5RSD 124.32 11.03 130.68 57.44 4.744 54.57 .2110 #1 .54718 .0307 -.04695 .0013 .0006 -.0000 .7409 #2 .05061 .0260 -3.0796 .0004 .0005 -.0000 .7388 #3 .07664 .0322 -.58710 .0007 .0006 -.0000 .7418 3lem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm w9e .0000 .0009 .0002 .0379 .2439 .3363 .1833 3Dev .0001 .0003 .0002 .0001 .0008 .0067 .0029 iRSD 580.6 37.41 119.8 .1329 .3341 1.994 1.609 kl .0001 .0011 .0003 .0379 .2442 .3424 .1850 k2 -.0001 .0005 -.0001 .0380 .2430 .3291 .1799 k3 .0000 .0011 .0002 .0379 .2446 .3374 .1850 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb �v .0030 -.0004 20.79 .0012 1.5556 .75130 1.4465 >E .0001 .0005 .05 .0001 2.2917 .53817 1.4673 ;RSD 4.318 117.0 .2383 13.19 147.33 71.631 101.44 !1 .0031 .0001 20.75 .0012 2.8468 .53860 1.7704 12 .0029 -.0007 20.84 .0013 -1.0905 1.3633 2.7247 `3 .0031 -.0006 20.76 .0010 2.9104 .35199 -.15566 :1 em 2068/2 1960/1 1960/2 Si Sn Sr Ti snits ppb ppb ppb ppm ppm ppm ppm ,vge .57146 -.28954 .96873 1.329 -.0010 .0009 .0004 ;Dev 1.2159 2.24410 1.1471 .003 .0016 .0001 .0001 ;RSD 212.78 775.07 118.41 .2570 160.9 5.420 22.91 =1 .14389 1.3226 -.33225 1.325 .0008 .0010 .0005 2 -.37293 -2.8525 1.4038 1.331 -.0017 .0009 .0003 3 1.9434 .66138 1.8346 1.331 -.0021 .0009 .0004 :lem T11908 v Zn Pb2203 Sb2068 Se1960 [nits ppb ppm ppm ppb ppb ppb ,vge .61250 .0003 .0163 1.0192 .86286 .54973 :Dev .70025 .0001 .0001 .4128 .33074 .78309 RSD 114.33 49.11 .3916 40.503 38.331 142.45 1 1.2592 .0005 .0163 1.3073 .68552 .21880 -.13117 .0003 .0162 .54628 .65861 -.01357 .70943 .0002 .0162 1.2040 1.2444 1.4439 zalysis Report 12/14/05 06:36:26 PM page 1 =thod: CLP1 Sample Name: 0512218-013E Operator: CO in Time: 12/14/05 18:29:06 :)m1 .: TSL004 fav, 3dc . .:ONC Corr. Factor: 1 Clem Ag Al As1890 B Ba Be Ca 7nits ppb ppm ppb ppm ppm ppm ppm �vge .21151 .0100 -.94970 -.0022 .0004 -.0000 .1125 3Dev .34735 .0009 1.13896 .0000 .0000 .0000 .0004 ''RSD 164.22 9.015 119.93 .2295 5.146 51.81 .3374 11 .52989 .0090 .05828 -.0021 .0003 -.0000 .1122 #2 -.15893 .0103 -.72212 -.0022 .0004 -.0000 .1124 #3 .26357 .0107 -2.1853 -.0022 .0004 -.0000 .1129 ?lem Cd Co Cr Cu Fe K Mg 7nits ppm ppm ppm ppm ppm ppm ppm lvge .0000 .0000 .0001 .0007 .0058 .0634 .0025 3Dev .0001 .0001 .0001 .0000 .0001 .0023 .0023 >RSD 193.3 312.3 63.97 4.281 2.601 3.648 92.44 11 .0000 .0001 .0001 .0007 .0056 .0614 -.0002 k2 -.0000 .0001 .0001 .0006 .0059 .0628 .0039 k3 .0001 -.0001 .0000 .0007 .0058 .0659 .0039 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 hits ppm ppm ppm ppm ppb ppb ppb lv .0000 -.0008 .3543 -.0008 .67935 1.0617 .09565 ;D .0001 .0003 .0081 .0005 3.1626 1.3045 1.8610 ;RSD 136.8 33.94 2.291 62.51 465.53 122.87 1945.6 11 -.0000 -.0005 .3632 -.0008 2.3400 .60642 .30464 �2 .0001 -.0010 .3523 -.0013 2.6657 .04580 -1.8610 `-3 .0000 -.0007 .3473 -.0003 -2.9677 2.5327 1.8434 :l em 2068/2 1960/1 1960/2 Si Sn Sr Ti tnits ppb ppb ppb ppm ppm ppm ppm ,vge -1.1515 -.27743 .21986 -.1430 -.0018 -.0005 .0003 ;Dev .0619 1.32141 1.7263 .0008 .0010 .0000 .0000 ;RSD 5.3742 476.30 785.19 .5319 56.71 3.411 12.66 :1 -1.1772 .53007 .79362 -.1424 -.0022 -.0005 .0003 :2 -1.1964 .44000 -1.7203 -.1428 -.0025 -.0005 .0003 :3 -1.0809 -1.8024 1.5862 -.1438 -.0006 -.0005 .0004 :lem T11908 v Zn Pb2203 Sb2068 Se1960 [nits ppb ppm ppm ppb ppb ppb .vge -.32227 .0001 .0109 .93442 -.73619 .05427 Dev 1.43153 .0004 .0001 .24169 .65688 .92216 RSD 444.21 321.4 .4629 25.865 89.227 1699.2 1 -1.1184 -.0000 .0109 1.1838 -.68372 .70586 2 -1.1788 -.0002 .0109 .91831 -1.4177 -1.0009 3' 1.3304 .0005 .0108 .70119 -.10712 .45784 ialysis Report 12/14/05 06:43:53 PM page 1 �thod: CLP1 Sample Name: CCV3 Operator: CO in `----ie: 12/14/05 18:36:33 )MV : TSL004 )de: �-'ONC Corr. Factor: 1 ;lem Ag Al As1890 B Ba Be Ca 7nits ppb ppm ppb ppm ppm ppm ppm �vge 1006.3 52.41 511.36 2.379 2.475 2.462 52.26 3Dev 14.7 .70 8.00 .034 .035 .040 .83 '5RSD 1.4603 1.338 1.5646 1.425 1.416 1.630 1.598 fl 1011.4 52.58 515.38 2.390 2.491 2.481 52.60 f2 1017.7 53.02 516.55 2.406 2.500 2.489 52.87 f3 989.72 51.64 502.14 2.341 2.435 2.416 51.30 ;rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass iigh 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 .low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 ;lem Cd Co Cr Cu Fe K Mg Tnits ppm ppm ppm ppm ppm ppm ppm ivge 2.430 2.446 2.440 2.479 51.81 87.31 52.61 3Dev .041 .039 .039 .034 .88 1.03 .83 ;RSD 1.704 1.587 1.582 1.389 1.701 1.180 1.582 kl 2.450 2.463 2.457 2.492 52.19 87.36 52.95 k2 2.457 2.474 2.467 2.505 52.44 H88.32 53.22 k3 2.382 2.402 2.396 2.440 50.80 86.26 51.66 =ors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass iigh 2.750 2.750 2.750 2.750 55.00 88.00 55.00 low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 Tnits ppm ppm ppm ppm ppb ppb ppb ivge 2.436 2.485 83.94 2.426 519.62 497.48 999.40 3Dev .038 .040 .89 .041 5.54 9.69 19.35 ;RSD 1.542 1.615 1.060 1.701 1.0662 1.9475 1.9366 E1 2.452 2.500 83.93 2.448 522.22 502.16 1009.7 E2 2.463 2.516 84.84 2.452 523.38 503.95 1011.4 E3 2.393 2.440 83.06 2.379 513.26 486.34 977.07 rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK [igh 2.750 88.00 2.750 ,ow 2.250 72.00 2.250 :lem 2068/2 1960/1 1960/2 Si Sn Sr Ti hits ppb ppb ppb ppm ppm ppm ppm xge 991.03 514.61 511.26 1.867 2.442 2.481 2.449 ;Dev 13.71 3.73 8.31 .024 .039 .034 .037 ;RSD 1.3837 .72450 1.6261 1.276 1.602 1.380 1.506 994.31 517.16 516.01 1.866 2.458 2.495 2.466 `-2 1002.8 516.34 516.11 1.892 2.470 2.505 2.474 `3 975.98 510.33 501.66 1.844 2.397 2.442 2.407 :rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 O� d' O Cn ialysis Report 12/14/05 06:43:53 PM iiah io" slem T11908 v Zn Pb2203 Sb2068 Se1960 7nits ppb . ppm ppm ppb ppb ppb wge 499.50 2.456 2.553 504.86 993.82 512.37 3Dev 6.92 .037 .040 8.31 15.45 6.78 5RSD 1.3859 1.518 1.551 1.6455 .1.5549 1.3233 f1 500.93 2.472 2.571 508.84 999.44 516.39 k2 505.60 2.483 2.580 510.42 1005.7 516.19 f3 491.98 2.413 2.508 495.31 976.34 504.55 ;rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass sigh 550.00 2.750 2.750 550.00 1100.0 550.00 jow 450.00 2.250 2.250 450.00 900.00 450.00 page 2 alysis Report 12/14/05 06:51:20 PM page 1 thod: CLP1 Sample Name: CCVL3 Operator: CO n e: 12/14/05 18:43:59 mn : TSL004 de: CONC Corr. Factor: 1 lem Ag Al As1890 B Ba Be Ca nits ppb PPM ppb PPM PPM Ppm .0005 Ppm .0433 .vge .35166 .0201 .09755 .57240 .0144 .0013 .0005 .0001 .0001 0030 .. :Dev -RSD .27305 77.646 .0040 20.13 586.80 8.944 25.17 27.08 .903 6903 :1 .0246 -.06235 .0158 .0007 .0006 .0464 =2 .39072 .0188 -.37791 .0143 .0005 .0005 .0432 ``-3 .06118 .60308 .0168 .73289 .0132 .0004 .0004 .0404 ;rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK sigh pow ;lem Cd Co Cr Cu Fe K Mg 7nits ppm PPM PPM PPM PPM 2.521 PPM .0594 PPm .0112 �vge .0006 0002 .0006 .0003 .0001 .0008 .0002 .004 .0059 .0040 SDev ;RSD 32.97 .0002 30.58 31.63 21.08 .1588 9.891 35.40 #1 .0008 .0004 .0010 2.525 .0659 .0157 $; .0008 .0007 .0004 .0002 .0007 2.518 .0545 .0090 $; .0004 .0005 .0003 .0007 2.518 .0579 .0088 ?rrors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK 2.750 Sigh 2.250 -jOw Mo Na Ni 2203/1 2203/2 2068/1 Clem Jnits Mn ppm PPM PPM PPM ppb ppb ppb •88725 4,vge .0003 .0025 2.651 .0001 -.70524 1.07399 .26512 .86596 1.2532 SDev .0002 .0017 65.11 .019 .0003 191.3 152.29 326.64 141.25 %RSD 57.76 .7155 41 .0005 ...0044 2.669 -.0001 -1.2772 -.42470 1.1863 #2 .0002 .0018 2.654 .0005 .53368 -1.3722 1.2369 -.01688 -.48843 1.9639 #3 .0002 .0014 2.631 .0000 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb PPM PPM PPM -.0001 PPM .0004 Avge -1.0198 1.7761 -.90130 -.1025 .0010 06 01 SDev 223924 091 4446350 2.5416 62002 200002 30054 %RSD 65 .2413 -1.6546 2.1946 -.62435 -.0995 .0017 .0001 .0005 #2 -.32767 1.7173 -.71680 -.1035 .0009 -.0001 -.0002 .0003 .0003 #3 -1.0771 1.4165 -1.3628 -.1044 .0005 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Errors NOCHECK ialysis Report 12/14/05 06:51:20 PM sigh jo Clem T11908 v Zn Pb2203 Sb2068 Se1960 7nits ppb ppm ppm ppb ppb ppb wge 2.8196 .0006 .0027 -.05798 -.38474 -.00972 3Dev .6597 .0001 .0001 .92647 .32207 .38634 '')RSD 23.395 19.48 5.415 1598.0 83.711 3974.4 f1 2.1562 .0008 .0028 -.70854 -.70857 .31436 f2 2.8272 .0006 .0027 1.0028 -.38119 .09374 f3 3.4754 .0006 .0025 -.46817 -.06446 -.43726 ;rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK sigh Jow page 2 lalysis Report 12/14/05 06:58:48 PM page 1 �thod: CLP1 Sample Name: CCB3 Operator: CO 1n ''' ^le : 12/14/05 18:51:27 )MI : TSL004 )d(--. -'ONC Corr. Factor: 1 lem Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm ppm ppm ppm Wge .12364 .0047 -.40283 -.0020 .0002 .0001 .0326 3Dev .16001 .0017 .20421 .0002 .0001 .0001 .0019 '5RSD 129.42 35.44 50.693 9.842 43.39 55.02 5.794 fl -.05572 0062 -.58729 -.0019 .0002 .0002 .0348 f2 .25176 .0029 -.18339 -.0023 .0001 .0001 .0318 f3 .17486 .0049 -.43780 -.0019 .0001 .0001 .0313 ;rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass sigh 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Jow -10.000 -.2000 -10.000 -.2000 -.2000 -.0.050 -.2000 ilem Cd Co Cr Cu Fe K Mg 7nits ppm ppm ppm ppm ppm ppm ppm wge .0003 .0002 -.0001 .0004 .0039 .0485 .0030 3Dev .0001 .0002 .0001 .0001 .0016 .0055 .0021 ;RSD 29.72 74.88 125.4 30.07 41.31 11.34 70.70 k1 .0003 .0001 .0000 .0005 .0056 .0532 .0054 k2 .0003 .0002 -.0001 .0003 .0034 .0424 .0015 k3 .0002 .0004 -.0001 .0003 .0025 .0499 .0021 ;rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass sigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 ,ow -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 ;lem Mn Mo Na Ni 2203/1 2203/2 2068/1 hits ppm ppm ppm ppm ppb ppb ppb kvge .0002 -.0002 .0231 -.0004 1.0166 .63158 -1.2504 >Dev .0001 .0004 .0064 .0002 1.0840 1.5194 .7822 -RSD 45.34 158.7 27.71 48.87 106.63 240.58 62.556 41 .0002 -.0001 .0301 -.0002 .01589 2.0446 -1.8729 E2 .0001 .0000 .0217 -.0006 .86571 .82575 -.37240 `3 .0002 -.0007 .0176 -.0005 2.1682 -.97562 -1.5060 :rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK [igh .0150 5.000 .0400 ,ow -.0150 -5.000 -.0400 'lem 2068/2 1960/1 1960/2 Si Sn Sr Ti ►nits ppb ppb ppb ppm ppm ppm ppm ,vge .01598 3.2098 .09597 -.2182 -.0015 -.0004 -.0001 :Dev .86014 2.6493 1.4208 .0010 .0008 .0001 .0001 ;RSD 5381.4 82.538 1480.4 .4610 54.90 18.08 154.8 =7 .98469 1.3115 -1.4274 -.2172 -.0006 -.0003 .0000 :2 -.27848 6.2365 .33029 -.2182 -.0018 -.0005 -.0002 :3 -.6582.5 2.0814 1.3850 -.2192 -.0022 -.0005 -.0001 ;rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK N O O O C/ N nalysis Report Hinh Lo Elem T11908 Units ppb kvge 1.5905 SDev .7550 %RSD 47.471 91 1.1446 #2 1.1646 #3 2.4623 Errors LC Pass :sigh 10.000 Low -10.000 v ppm .0001 .0001 60.54 .0002 .0000 .0001 LC Pass .0500 -.0500 Zn ppm .0020 .0001 4.382 .0021 .0019 .0019 LC Pass .0200 -.0200 12/14/05 06:58:48 PM page 2 Pb2203 ppb .75982 .65251 85.878 1.3691 .83909 .07129 LC Pass 3.0000 -3.0000 Sb2068 ppb -.40.571 .49387 121.73 .03313 -.30974 -.94053 LC Pass 60.000 -60.000 Sel960 ppb 1.1329 1.4673 129.52 -.51532 2.2971 1.6169 LC Pass 5.0000 -5.0000 PS8'TT SZ'EZT 96SL'S 6f, P0' 9860' ZEil'OZ 9T76" OT 6Z'ZZT 60ZE'L TStO' 0660' L9E'TZ Ezfi' OT t E:' ZZT 6DES' 9 8tltl0' 1,660' ZE6' OZ TI OSES'9 OSTfIb' 6E6'TT 98LZ' TE9E' 6L£Z'Z QSH5 VZL' PS' 908L' T000' fl000' 89D,' naQf i,LO'TT £9'ZZT S8ES'9 6VVO ' 0660' 016'OZ GSAJ qdd qdd qdd wdd wdd qdd s-ITul 096TaS 890ZQS EOZZgd uZ A 806TIl wal, 9260 9000'- PE80' ZLf,O' - V88'TT £6L'TT 86' UT E# 9260' 5000'- LZ80' 8S60'- 6TL8'6 860'ET 86'OZT Z# SZ60' 9000'- 8280' 8LP0'- 808'OT ItS9'6 96'TZT T# LZLO' 900'6 6E6fi' 08T'Z P9LZ'6 660 'ST OOZE'T QS2I= T000' T000" fl000' OT00' L00'T 6£L'T T9'T naQC, 9260' 9000'- 0£80' 69P0'- SS8'OT STS'TT PT'ZZT aSnF wdd wdd wdd wdd qdd qdd qdd sgTur TZ zS us TS Z/096T T/096T Z/890z waTE 6L'TZT T7L8L'S 8EOL'S P6LO' Z8T0' OOzO' D,6Z0' E# Z6'tZT 6TLE'8 6STZ'S L8L0' zOZO' 6610' 9620' Z# OT'%ZT TtET'8 9TEE'£ LSLO' bozo' 86T0' S6ZO' T# 8TTE'T EZZ'6T OLE -9Z Zb6b' 9ZE'9 9EZT7 086Z' QS23° Z9'T SM, *T 9ZSZ'•T tl000' ZT00' T000' T000' IE 09'EZT TTEb'L EOSL'T7 68L0' 96TO' 66TO' S6ZO' Lf qdd qdd qdd wdd wdd wdd wdd SgTur T/8902 Z/£ozz T/Eozz TN PN ON uW waT�: TZ00'- z8E0' P000" S6t0' D,6T0' TG60" 6600' E# OT00' T8T70" 6000' 66D0' S6T0' 8660' ZOTO' z 6000' tl6t0' 8000' 66t0' £6T0' L660' TOTO' Tt 'ZDIEE LP'TT 66'6£ 666E' Oz9t' L6SE' 8ET'T QSH9$ LT00' OS00' £000' z000' T000' .D1000' T000' naQE T000'- SED10 L000' L6V0' 6610' S660' TOTO' abn% wdd wdd wdd wdd wdd wdd wdd S:tTur bW ?I ad n0 z0 of PO waTS 0620' ZOTO' 0000' 8E8T' fiib0'Oz 8600' 6ZZ'OZ E:h LOCO ' ZOTO' T000' OS8T' OSt,*TZ 6ETO' OSz'Oz Z$ 60£0' FOTO' 0000' SE8T' LOL'OZ 80T0' LEE'OZ Tfl 0Zt" E 8EOZ' Z' TET 98Tt,' SMU E 86'8T T8E8Z' QSdit OT00' 0000' 0000' 8000' EOL' zZ00' 8S0' AaQS ZO£0' ZOTO' 0000' Tf,8T' tEL'OZ STTO' ZLZ'OZ a6A-V wad wdd wdd wad qdd wdd qdd slTur �O ag eS S 068TSV TV 6V waTS T :.zogaed -aaOD ONO2 ' ^oc bS:8S:8T SO/bT/ZT OJ :jogezad0 aiHD :owpN aTdweS Td'IO :POgIG T abed Wd ST:90:LO SO/VT/ZT liodag sTsATeu nalysis Report 12/14/05 07:13:43 PM page 1 ethod: CLP1 Sample Name: ICSAF Operator: CO ur Tame: 12/14/05 19:06:22 OT it: TSL004 o(.- . CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .59041 505.3 -1.5891 .0264 .0011 .0002 504.8 SDev .17151 .9 3.9429 .0006 .0000 .0000 .6 %RSD 29.049 .1835 248.12 2.177 3.508 11.17 .1248 ##1 .63946 504.2 -.81351 .0260 .0010 .0002 504.1 #2 .39972 505.8 1.9084 .0261 .0011 .0002 505.2 #3 .73204 505.8 -5.8622 .0271 .0011 .0002 505.3 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd . Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm kvge .0011 -.0005 .0036 -.0002 202.3 .0383 507.7 SDev .0000 .0002 .0001 .0001 .3 .0047 .8 oRSD 4.076 47.95 3.717 57.74 .1683 12.19 .1507 41 .0010 -.0007 .0035 -.0003 202.0 .0329 506.8 �2 .0011 -.0002 .0037 -.0001 202.4 .0407 507.9 �# .0011 -.0005 .0035 -.0002 202.7 .0412 508.3 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass :sigh .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 31em Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb kvge -.0052 -.0053 .0424 .0027 35.111 -19.945 3.0998 3Dev .0003 .0005 .0005 .0004 2.526 2.724 3.1682 sRSD 5.326 9.608 1.085 14.93 7.1953 13.655 102.21 11 -.0053 -.0057 .0420 .0025 32.389 -17.852 5.1452 #2 -.0049 -.0054 .0424 .0024 37.381 -23.025 -.54962 #3 -.0054 -.0047 .0429 .0032 35.563 -18.959 4.7039 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK Sigh .0150 .0400 meow -.0150 -.0400 31em 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm ppm ppm ppm kvge 1.2460 .45640 -2.1871 -.0130 .0397 -.3060 .0023 3Dev 1.9059 2.3580 2.6918 .0008 .0020 .0009 .0001 5RSD 152.96 516.64 123.08' 6.159 5.056 .3101 4.018 I .59888 1.1679 -3.8209 -.0123 .0378 -.3059 .0023 #� 3.3913 2.3767 .91972 -.0130 .0418 -.3051 .0024 #3 -.25210 -2.1754 -3.6600 -.0139 .0396 -.3070 .0023 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 07:13:43 PM wLcHi -I- Lc Elem T11908 v Zn Pb2203. Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge L-16.565 -.0005 -.0102 -1.6116 1.8633 -1.3068 SDev 2.044 .0003 .0001 1.1353 .4031 2.4017 .RSD 12.341 68.39 .8027 70.448 21.635 183.78 #1 L-18.906 -.0001 -.0101 -1.1219 2.1128 -2.1596 42 L-15.130 -.0007 -.0101 -2.9096 2.0790 1.4049 43 L-15.659 -.0006 -.0103 -.80329 1.3983 -3.1656 Errors LC Low LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 nalysis Report 12/14/05 07:21:10 PM page 1 ethod: CLP1 Sample Name: ICSABF Operator: CO un 'P4,ne: 12/14/05 19:13:49 om t: TSL004 od- --ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1086.3 496.0 1056.4 .8984 .5153 .4993 497.9 SDev 8.1 3.8 7.2 .0074 .0036 .0041 5.1 %RSD .74292 .7616 .68609 .8241 .7023 .8128 1.018 #1 1077.0 491.7 1048.1 .8903 .5112 .4947 492.1 #2 1090.2 498.5 1059.7 .9000 .5174 .5009 499.9 #3 1091.7 497.9 1061.4 .9049 .5174 .5023 501.6 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .9352 .4677 .4854 .5230 198.9 .0798 498.7 SDev .0086 .0039 .0043 .0032 1.9 .0052 3.9 %RSD .9215 .8405 .8942 .6062 .9505 6.518 .7760 41 .9255 .4632 .4805 .5194 196.8 .0741 494.3 #2 .9382 .4697 .4872 .5249 199.7 .0811 500.3 4- .9419 .4703 .4886 .5248 200.3 .0843 501.5 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb 4,vge .4764 .9803 .0336 .9219 1070.2 985.32 -10.813 SDev .0036 .0078 .0005 .0093 6.5 14.39 1.882 '.RSD .7596 .7919 1.571 1.013 .61057 1.4604 17.406 41 .4723 .97.16 .0330 .9113 1062.7 970.48 -11.380 12 .4782 .9827 .0338 .9254 1072.9 986.28 -12.347 �43 .4788 .9866 .0340 .9290 1074.9 999.21 -8.7129 3rrors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK Sigh .6000 1.200 -jow .4000 .8000 3lem 2068/2 1960/1 1960/2 Si Sn Sr Ti Jnits ppb ppb ppb ppm ppm ppm ppm 3vge -4.0352 1033.0 1021.4 .4993 1.027 -.3052 .0017 SDev 2.0266 8.5 11.1 .0073 .012 .0022 .0001 sRSD 50.224 .82156 1.0838 1.453 1.123 .7258 8.362 #: -4.2940 1023.6 1011.2 .4909 1.013 -.3029 .0016 #� -1.8916 1040.1 1019.8 .5041 1.034 -.3052 .0018 #3 -5.9200 1035.4 1033.2 .5028 1.032 -.3073 .0018 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK .nalysis Report 12/14/05 07:21:10 PM Hiah Lc Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 980.52 .4.886 1.038 1013.6 -6.2923 1025.3 SDev 9.61 .0039 .008 11.7 .8020 9.3 %RSD .97984 .8006 .7738 1.1534 12.745 .91182 #1 969.54 .4842 1.029 1001.2 --6.6536 1015.3 #2 987.42 .4901 1.042 1015.1 -5.3732 1026.6 #3 984.59 .4915 1.044 1024.4 -6.8500 1033.9 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 .nalysis Report 12/14/05 07:28:38 PM page 1 fethod: CLP1 Sample Name: CCV4 Operator: CO :un Ti.me: 12/14/05 19:21:17 'ot Lt: TSL004 loc-__ CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1018.4 52.91 517.67 2.418 2.502 2.500 53.12 SDev .7 .07 1.60 .004 .003 .003 .03 %RSD .06627 .1404 .30904 .1574 .1031 .1124 .0490 #1 1017.8 52.97 516.27 2.414 2.499 2.497 53.13 #2 1019.1 52.95 517.33 2.422 2.504 2.500 53.09 #3 1018.2 52.83 519.41 2.418 2.502 2.503 53.14 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu- Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm kvge 2.471 2.487 2.479 2.502 52.64 H88.27 53.68 SDev .003 .002 .002 .003 .03 .22 .03 %RSD .1138 .0734 .0831 .1193 .0492 .2549 .0505 f#1 2.468 2.485 2.477 2.501 52.62 H88.40 53.72 42 2.471 2.487 2.479 2.505 52.63 H88.39 53.67 ff: 2.473 2.489 2.481 2.499 52.67 H88.01 53.67 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC High LC Pass Sigh 2.750 2.750 2.750 2.750 55.00 88.00 55.00 mow 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Clem Mn Mo Na Ni 2203/1 2203/2 2068/1 hits ppm ppm ppm ppm ppb ppb ppb kvge 2.474 .2.524 84.64 2.468 524.61 505.54 1006.4 SDev .002 .003 .21 .002 2.64 1.14 1.1 ''SRSD .0880 .1146 .2459 .0883 .50243 .22454 .10911 #1 2.472 2.521 84.70 2.466 523.05 505.03 1005.6 #2 2.475 2.525 84.81 2.467 523.12 506.84 1006.0 13 2.476 2:527 84.41 2.470 527.65 504.74 1007.7 ;rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK sigh 2.750 88.00 2.750 .low 2.250 72.00 2.250 .lem 2068/2 1960/1 1960/2 Si Sn Sr Ti hits ppb ppb ppb ppm ppm ppm ppm kvge 1001.2 522.26 515.71 1.920 2.482 2.508 2.480 ;Dev 5.4 .71 1.74 .009 .006 .002 .003 ;RSD .54406 .13647 .33659 .4889 .2510 .0797 .1308 1.002.4 522.87 514.57 1.910 2.476 2.506 2.476 995.19 521.48 514.84 1.924 2.482 2.510 2.482 3 1005.9 522.45 517.71 1.927 2.488 2.508 2.482 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 12/14/05 07:28:38 PM Hz^h L( Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 511.59 2.493 2.590 511.89 1002.9 517.89 SDev 1.36 .001 .002 .74 3.9 1.22 %RSD .26504 .0598 .0625 .14532 .38618 .23471 #1 511.51 2.492 2.588 511.03 1003.5 517.34 #2 512.98 2.493 2.590 512.26 998.79 517.05 #3 510.27 2.495 2.591 512.37 1006.5 519.28 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 .nalysis Report 12/14/05 07:36:06 PM page 1 [ethod: CLP1 Sample Name: CCVL4 Operator: CO .ur '"4.me: 12/14/05 19:28:45 'or it: TSL004 .ou= : CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .54386 .0566 -.09969 .0154 .0005 .0005 .0875 SDev .25269 .0044 .49199 .0010 .0001 .0001 .0065 %RSD 46.463 7.830 493.54 6.686 17.74 14.57 7.370 #1 .83525 .0606 -.63186 .0165 .0006 .0006 .0939 #2 .41140 .0519 .33860 .0153 .0005 .0005 .0811 #3 .38493 .0572 -.00580 .0145 .0005 .0005 .0875 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0007 .0004 .0002 .0009 2.497 .0575 .0500 SDev .0001 .0003 .0003 .0001 .002 .0070 .0063 %RSD 20.83 84.05 147.2 9.727 .0702 12.17 12.51 41 .0008 .0007 .0003 .0009 2.495 .0648 .0560 42 .0005 .0001 -.0001 .0008 2.498 .0508 .0435 4 .0006 .0004 .0003 .0009 2.499 .0569 .0505 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Sigh 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Jnits ppm ppm ppm ppm ppb ppb ppb %vge .0003 .0024 2.634 -.0003 -1.0201 .40849 .22862 SDev .0001 .0013 .010 .0003 .8940 1.1951 1.2388 '.RSD 37.06 55.12 .3635 103.9 87.646 292.57 541.86 41 .0004 .0038 2.637 -.0001 -1.8376 1.5073 .57556 42 .0002 .0023 2.623 -.0006 -.06535 -.86397 -1.1466 43 .0003 .0012 2.642 -.0002 -1.1573 .58217 1.2569 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK -sigh 2.750 mow 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti 7nits ppb ppb ppb ppm ppm ppm ppm Wge -2.0429 .67574 .23325 -.1154 .0012 -.0002 .0003 SDev .6999 2.5270 2.5309 .0015 .0009 .0001 .0001 ''RSD 34.260 373.96 1085.1 1.293 72.59 53.75 29.85 k -2.8509 1.2731 3.1540 -.1139 .0021 -.0001 .0004 kz -1.6282 -2.0964 -1.3130 -.1155 .0013 -.0002 .0002 k3 -1.6495 2.8506 -1.1413 -.1169 .0003 -.0002 .0003 ?rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK. NOCHECK NOCHECK d - O analysis Report 12/14/05 07:36:06 PM page 2 Hiah Zn Lc Sb2068 Elem T11908 Units ppb Avge 3.5968 SDev 1.1548 %RSD 32.107 #1 2.2826 #2 4.4498 #3 4.0580 Errors NOCHECK High 41.789 Low .0009 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0007 .0034 -.06718 -1.2865 .38060 .0002 .0001 .49944 .5376 2.0575 24.48 3.067 743.42 41.789 540.60 .0009 .0035 .39347 -1.7099 2.5276 .0007 .0033 -.59799 -1.4678 -1.5739 .0006 .0033 .00298 -.68164 .18803 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK .nalysis Report 12/14/05 07:43:33 PM page 1 ethod: CLP1 Sample Name: CCB4 Operator: CO .un 'T',me: 12/14/05 19:36:12 ong _: TSL004 ods. CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .32190 .0205 -.71813 -.0013 .0002 .0001 .0510 SDev .26459 .0048 1.27127 .0005 .0001 .0001 .0055 %RSD 82.198 23.32 177.03 36.27 34.46 44.82 10.70 #1 .62728 .0200 .53971 -.0007 .0002 .0002 .0525 42 .17717 .0256 -2.0024 -.0015 .0002 .0002 .0556 43 .16123 .0161 -.69168 -.0016 .0001 .0001 .0450 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Jnits ppm ppm ppm ppm ppm ppm ppm !�.vge .0003 .0003 -.0000 .0005 .0096 .0487 .0181 SDev .0001 .0002 .0002 .0003 .0023 .0073 .0059 'RSD 38.00 59.37 692.8 62.63 24.00 15.10 32.67 41 .0004 .0004 .0001 .0006 .0104 .0525 .0186 #2 .0002 .0005 .0001 .0008 .0114 .0533 .0238 #3 .0003 .0001 -.0003 .0002 .0070 .0402 .0120 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh .0050 .0500 .0100 .0250 .1000 5.000 .2000 jow -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 7nits ppm ppm ppm ppm ppb ppb ppb �vge .0001 .0005 .0228 -.0005 -.22704 .63030 -.17080 SDev .0001 .0004 .0046 .0001 .59696 .44061 1.14166 ;RSD 91.18 87.05 20.13 18.27 262.93 69.904 668.40 kl .0002 .0010 .0270 -.0004 -.91119 1.0899 -.29888 k2 .0002 .0005 .0233 -.0005 .18791 .21155 -1.2430 !3 -.0000 .0001 .0179 -.0006 .04216 .58944 1.0295 ;rrors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK [igh .0150 5.000 .0400 ,ow -.0150 -5.000 -.0400 :lem 2068/2 1960/1 1960/2 Si Sn Sr Ti (nits ppb ppb ppb ppm ppm ppm ppm .vge .88382 1.4939 -.67579 -.2253 -.0017 -.0005 -.0001 Dev 1.5050 .9467 1.69252 .0011 .0004 .0001 .0001 RSD 170.28 63.367 250.45 .4999 22.70 13.16 73.76 1� -.40939 .40333 -2.2435 -.2243 -.0014 -.0005 -.0001 2 2.5358 2.1034 1.1187 -.2250 -.0017 -.0004 -.0001 3 .52511 1.9751 -.90258 -.2265 -.0022 -.0006 -.0002 rrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK .nalysis Report 12/14/05 07:43:33 PM H.: ' L( Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.7601 .0003 .0030 .34484 .53265 .04673 SDev .2625 .0002 .0000 .12250 .83662 1.4044 oRSD 14.915 50.67 1.366 35.522 157.07 3005.3 #1 2.0306 .0005 .0031 .42358 -.37257 -1.3621 #2 1.5064 .0002 .0031 .20371 1.2774 1.4466 #3 1.7434 .0003 .0030 .40723 .69309 .05570 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 V2M LABS, INC. IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE 1 112M labs, Inc. CLP Client: ,�CT s ` -- G #: i 5 c ooy 'rix: -e_? VI Method:_ IOl� D* estion Lo Analyst Signature: Date: 1- 1110,7 Time 0,— Time Started/Ended:_ ja ; 43� p,L4 •Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. 'Description of texture: fine, medium, coarse. 'Description of clarity: clear, cloudy, opaque. 'Description of artifacts: yes or no and describe OJWBOOKS/CI-Migestionlog 7h O P" U2M LAOS, INC. SDG NO.: iSLoaY SCAN: /i'(ETP'kg This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Sign, Date Revio Date