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Wet Chemistry Data Package 12/2005
Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL004 Water Samples Received: 12/8/05 IAII=T r L41=RAI-QTRY DATA PACKAGE 1AA L/tusa� I EInvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. sula 11747 U2M UAUS, INC. i'SLOoy TABLE OF CONTENTS SAMPLE REPORTS II. Q.C. SUMMARY III. RAW DATA U2M TAUS, 1 N C. SAMPLE REPORTS U2M TAUS, INC. 575BrcadHolaly Road, Mdvie NY 11747 LABORATORY RESULTS (631) 690M - FAX (631)42084W NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. 0512218-001 Type : Groundwater Attn To Origin: Collected :12/8/2005 8:30:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Client ID. : MW -1 D Parameterts) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 31.4 1 mg/L E310.1 12/09/2005 10:30 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:15 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:10 AM Chloride 4.0 1 mg/L E325.2 12/12/2005 4:55 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:02 AM Hardness (As CaCO3) 13.0 1 mg/L E130.2 12/20/2005 12:10 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 1:55 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:30 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 8:00 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 11:44 AM Total Dissolved Solids 59 1 mg/L E160.1 12/13/2005 10:34 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:33 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 5:46 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 1 of 13 Laboratory Manager U2M "US. INCe 57513roadl-Um Road, Mdvie NY 11747 LABORATORY RESULTS (631)a9 -3C)40- NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-002 Type : Groundwater Attn To : Origin: Client ID. : MW -1S Collected :12/8/2005 8:00:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 30.6 1 mg/L E310.1 12/09/2005 10:35 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:20 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:15 AM Chloride 4.7 1 mg/L E325.2 12/12/2005 4:56 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:03 AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/20/2005 12:15 PM Nitrogen, Ammonia (As N) 0.12 1 mg/L E350.1 12/15/2005 1:56 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:30 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 8:15 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 11:46 AM Total Dissolved Solids 65 1 mg/L E160.1 12/13/2005 10:35 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:34 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 6:15 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 2 of 13 ? awo. A 1-d&V41-Aj Laboratory Manager U2M "US, INC. 575&oadl blow Road, McKie NY 11747 LABORATORY RESULTS (631)689-3 - FAX (631)4X}8436NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-003 Type: Groundwater Attn To Origin: Client ID. r MW -3D Collected :12/8/2005 11:00:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 47.8 1 mg/L E310.1 12/09/2005 10:40 AM Biochemical Oxygen Demand 895 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:20 AM Chloride 13.0 1 mg/L E325.2 12/12/2005 4:57 PM Chemical Oxygen Demand 1280 2 mg/L E410.4 12/21/2005 11:04 AM Hardness (As CaCO3) 7.0 1 mg/L E130.2 12/20/2005 12:20 PM Nitrogen, Ammonia (As N) 8.28 10 mg/L E350.1 12/15/2005 3:04 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:31 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 8:30 AM Sulfate 15.2 1 mg/L SW9038 12/15/2005 11:48 AM Total Dissolved Solids 608 1 mg/L E160.1 12/13/2005 10:36 AM Nitrogen, Kjeldahl, Total 15.4 20 mg/L E351.2 12/20/2005 5:34 PM Total Organic Carbon 1170 40 mg/L SW9060 12/13/2005 5:05 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 3 of 13 Laboratory Manager 0 U2M "US, INCe 57513toadHolow Road, Mdvk NY 11747 LABORATORY RESULTS (631) 694.3040. FAX (631) 4248436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-004 Type: Groundwater Attn To : Origin: Client ID. : MW -3S Collected :12/8/2005 10:30:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 29.8 1 mg/L E310.1 12/09/200510:45 AM Biochemical Oxygen Demand 8 1 mg/L E405.1 12/08/2005 3:25 PM Bromide 1.0 1 mg/L E320.1 12/20/2005 9:25 AM Chloride 4.0 1 mg/L E325.2 12/12/2005 4:57 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:05 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 12:25 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 1:57 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:32 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 8:45 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 11:50 AM Total Dissolved Solids 61 1 mg/L E160.1 12/13/2005 10:37 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:35 PM Total Organic Carbon 9.3 1 mg/L SW9060 12/12/2005 7:15 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 4 of 13 ? awl'. A 1-dl"� Laboratory Manager U2M LAUS, INCe 575BmadFUM Reed, Melville NY 11747 LABORATORY RESULTS (631)694-3040.FAX (631)42084W NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218=0055 Type : Groundwater Attn To Origin: Client ID. : MW -4D Collected :12/8/2005 9:50:00 AM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 22.4 1 mg/L E310.1 12/09/2005 10:50 AM Biochemical Oxygen Demand 1203 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:30 AM Chloride 7.0 1 mg/L E325.2 12/12/2005 4:58 PM Chemical Oxygen Demand 1720 4 mg/L E410.4 12/21/2005 11:06 AM Hardness (As CaCO3) 8.0 1 mg/L E130.2 12/20/2005 12:30 PM Nitrogen, Ammonia (As N) 0.57 1 mg/L E350.1 12/15/2005 1:58 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:32 PM Phenolics, Total Recoverable 16.0 1 Ng/L E420.1 12/16/2005 9:00 AM Sulfate 10.7 1 mg/L SW9038 12/15/2005 11:52 AM Total Dissolved Solids 543 1 mg/L E160.1 12/13/2005 10:38 AM Nitrogen, Kjeldahl, Total 5.78 10 mg/L E351.2 12/20/2005 6:01 PM Total Organic Carbon 454 40 mg/L SW9060 12/13/2005 5:33 PM Qualifiers: E - Value above quantitation range t D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 5 of 13 Laboratory Manager 1-2M "U%o INC. 575 Broad FtbN Road, Mtdvile NY 11747 LABORATORY RESULTS (631)694,9040.FAX(631)42084W NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab. No. : 0512218.006 Type: Groundwater t Attn To Origin: Client ID. : MW -4S Collected :12/8/2005 9:15:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 37.2 1 mg/L E310.1 12/09/200510:55 AM Biochemical Oxygen Demand 22 1 mg/L E405.1 12/08/2005 3:30 PM Bromide 1.1 1 mg/L E320.1 12/20/2005 9:35 AM Chloride 6.9 1 mg/L E325.2 12/12/2005 4:59 PM Chemical Oxygen Demand 1540 4 mg/L E410.4 12/21/2005 11:07 AM Hardness (As CaCO3) 14.0 1 mg/L E130.2 • 12/20/200512:35 PM Nitrogen, Ammonia (As N) 1.03 1 mg/L E350.1 12/15/2005 1:59 PM Nitrate as N < 0.10 1 mg/L E353.2 12/14/2005 12:31 PM Phenolics, Total Recoverable 24.0 1 pg/L E420.1 12/16/2005 9:15 AM Sulfate 12.2 1 mg/L SW9038 12/15/2005 11:54 AM Total Dissolved Solids 464 1 mg/L E160.1 12/13/200510:40 AM Nitrogen, Kjeldahl, Total 54.8 50 mg/L E351.2 12/20/2005 6:02 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/2005 6:03 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 6 of 13 Laboratory Manager 00 0 U2M "US, INC. 575 BroadHADw Road, Md IIe NY 11747 LABORATORY RESULTS (631)694-�.FAX (631)42DS436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218.007 Type : Groundwater Attn To Origin: Client ID. : MW -51) Collected :12/7/2005 11:30:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original Cc Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 29.8 1 mg/L E310.1 12/09/2005 11:20 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:40 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:40 AM Chloride 4.6 1 mg/L E325.2 12/12/2005 5:02 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:10 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 12:50 PM Nitrogen, Ammonia (As N) 0.13 1 mg/L E350.1 12/15/2005 2:01 PM Nitrate as N 0.30 1 mg/L E353.2 12/13/2005 5:35 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 10:00 AM Sulfate <5.0 1 mg/L SW9038 12/15/2005 12:00 PM Total Dissolved Solids 73 1 mg/L E160.1 12/13/2005 10:45 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:39 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 9:40 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 7 of 13 Laboratory Manager U2M "US, INC. 575B+oWFkJb r Road, Mahle NY 11747 LABORATORY RESULTS (631)694,W-FAX(631)42D8436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-00$ Type : Groundwater Attn To Origin: Client ID. : MW -5S Collected :12/7/2005 11:00:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 31.0 1 mg/L E310.1 12/09/2005 11:25 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:45 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:45 AM Chloride 4.4 1 mg/L E325.2 12/12/2005 5:03 PM Chemical Oxygen Demand 112 1 mg/L E410.4 12/21/2005 11:11 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 12:55 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 2:01 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:36 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 10:15 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:02 PM Total Dissolved Solids 48 1 mg/L E160.1 12/13/2005 10:46 AM Nitrogen, Kjeldahl, Total 0.22 1 mg/L E351.2 12/20/2005 5:40 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 10:09 PM Qualifiers: E - Value above quantitation range i 0 D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 8 of 13 Laboratory Manager 1H2M "US, INC. 57513roadt-t1cw Road, Mdvile NY 11747 LABORATORY RESULTS (631)W4.3040 -FAX (631)42054W NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. 0512218-009 Type : Groundwater Attn To Origin: Client ID. : MW -6D Collected :12!7/200512:40:00 PM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original Cc Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 25.9 1 mg/L E310.1 12/09/2005 11:30 AM Biochemical Oxygen Demand 220 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:50 AM Chloride 5.9 1 mg/L E325.2 12/12/2005 5:03 PM Chemical Oxygen Demand 314 1 mg/L E410.4 12/21/200511:14 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 1:10 PM Nitrogen, Ammonia (As N) 0.17 1 mg/L E350.1 12/15/2005 2:03 PM Nitrate as N 0.16 1 mg/L E353.2 12/13/2005 5:38 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 10:30 AM Sulfate 8.0 1 mg/L SW9038 12/15/2005 12:04 PM Total Dissolved Solids 224 1 mg/L E160.1 12/13/2005 10:47 AM Nitrogen, Kjeldahl, Total 2.64 10 mg/L E351.2 12/20/2005 6:03 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 11:37 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 9 of 13 Laboratory Manager U2M "US, INCe 575BroedFd w Road, Melville NY 11747 LABORATORY RESULTS (631)694�010.FAX (631)4aW4W WSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. 0512218i.010 Type : Groundwater Attn To, Origin: Client ID. : MW -6S Collected :12/7/2005 12:10:00 PM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original cc Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 28.2 1 mg/L E310.1 12/09/2005 11:35 AM Biochemical Oxygen Demand 801 1 mg/L E405.1 12/21/2005 Bromide 0.7 1 mg/L E320.1 12/20/2005 9:55 AM Chloride 5.1 1 mg/L E325.2 12/12/2005 5:04 PM Chemical Oxygen Demand 1140 2 mg/L E410.4 12/21/2005 11:15 AM Hardness (As CaCO3) 6.0 1 mg/L E130.2 12/20/2005 1:15 PM Nitrogen, Ammonia (As N) 0.44 1 mg/L E350.1 12/15/2005 2:04 PM Nitrate as N 0.21 1 mg/L E353.2 12/13/2005 5:38 PM Phenolics, Total Recoverable 9.1 1 pg/L E420.1 12/16/2005 10:45 AM Sulfate 5.6 1 mg/L SW9038 12/15/2005 12:06 PM Total Dissolved Solids 150 1 mg/L E160.1 12/13/2005 10:48 AM Nitrogen, Kjeldahl, Total 8.74 20 mg/L E351.2 12/20/2005 6:04 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/2005 12:03 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 10 of 13 Laboratory Manager N r-+ E -i U2M ILAUS, INC. 5758roadFUM Road, Mdvk NY 11747 LABORATORY RESULTS (631)694.3040.FAX (631)4M436 NYSDOHID#10478 Town of Southold Landfill Lab No. :0512218-011 Sample Information...Type : Groundwater Attn To : Origin: Client ID. : MW -8D Collected :12!7/2005 2:00:00 PM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D_F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 32.6 1 mg/L E310.1 12/09/2005 11:40 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:50 PM Bromide 0.7 1 mg/L E320.1 12/20/2005 10:00 AM Chloride 4.4 1 mg/L E325.2 12/12/2005 5:05 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:16 AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/20/2005 1:20 PM ' Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 2:05 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:39 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 11:00 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:08 PM Total Dissolved Solids 65 1 mg/L E160.1 12/13/2005 10:49 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:42 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/2005 12:36 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 11 of 13 Laboratory Manager U2M "US, INC. 575 Band Hdow Road, Md& NY 11747 (631)694-.'i -FAX(631)42D8436 NYSDOH ID# 10478 Town of Southold Landfill Attn To Collected :12/7/20051:30:00 PM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC LABORATORY RESULTS Lab No. : 0512218-012 Client ID. : MW -8S Sample Information... Type: Groundwater Origin: Parameters) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 29.6 1 mg/L E310.1 12/09/2005 11:45 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:55 PM Bromide 0.6 1 mg/L E320.1 12/20/2005 10:05 AM Chloride 4.4 1 mg/L E325.2 12/12/2005 5:05 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:17 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 1:25 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 2:05 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:40 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 11:15 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:10 PM Total Dissolved Solids 54 1 mg/L E160.1 12/13/2005 10:50 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:43 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/2005 1:02 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 12 of 13 Laboratory Manager U2M "US, INCe 575RMadFUav Road, Mldvie NY 11747 LABORATORY RESULTS (631)694-.3U10.FAX (631)42D4B436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0551221$-013 Type: Blank Attn To Origin: Client ID. : EQPT BLANK Collected :12/8/2005 Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original GC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 12/09/2005 11:50 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 4:00 PM Bromide 0.6 1 mg/L E320.1 12/20/2005 10:10 AM Chloride < 2.0 1 mg/L E325.2 12/12/2005 5:06 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:18.AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/20/2005 1:30 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 2:06 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:40 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16/2005 11:30 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:12 PM Total Dissolved Solids <10 1 mg/L E160.1 12/13/200510:51 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:44 PM Total Organic Carbon 1.11 1 mg/L SW9060 12/13/2005 1:35 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 13 of 13 ? alt"It. Laboratory Manager W) �--I 0 0} 1--1 C/1 U2M "US, INC. II. Q.C. SUMMARY H2M LABS, INC. Date: 27 -Dec -05 SDG: TSL004 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL 905 MB -120905 Alkalinity, Total (As CaCO3) < 1 mg/L 0905 E0512218-006bdup LCS-120905 Alkalinity, Total (As CaCO3) 23.8 mg/L 25 < 1 95 80 120 8-006bms MW-4SMS Alkalinity, Total (As CaCO3) 60.0 mg/L 25 37.2 91 75 125 0512218-006BDUP MW-48DUP Alkalinity, Total (As CaCO3) 34.6 mg/L 37.2 7.4 20 MB -120805 MB -120805 Biochemical Oxygen Demand <2 mg/L LCS-120805 ILCS-120805 Biochemical Oxygen Demand 164 mg/L 1 200 < 2 82 80 120 0512218-006bdup MW-4SDUP Biochemical Oxygen Demand 21 mg/L 22 4.6 20 MB -122005 MB -122005 Bromide < 0.5 mg/L LCS-122005 LCS-122005 Bromide 5.4 mg/L 5 < 0.5 108 80 120 0512218-006BMS MW-4SMS Bromide 6.4 mg/L 5 1.1 106 75 125 0512218-006BDUP MW-4SDUP Bromide 0.9 mg/L 1.1 20.0 20 MB -122105 MB -122105 Chemical Oxygen Demand <10 mg/L LCS-122105 LCS-122105 Chemical Oxygen Demand 969 mg/L 1000 < 10 97 80 120 0512218-006cros MW-4SMS Chemical Oxygen Demand 5420 mg/L 4000 1540 97 75 125 0512218-006cdup MW-4SDUP Chemical Oxygen Demand _ 1470 mg/L 1540 4.7 20 MB -121205 MB -121205 Chloride <2 mg/L LCS-121205 LCS-121205 Chloride 50.5 mg/L 50 < 2 101 80 120 0512218-006BMS MW-4SMS Chloride 34.0 mg/L 25 6.9 108 75 125 0512218-006BDUP MW-4SDUP Chloride 7.3 mg/L 6.9 4.7 20 MB -122005 MB -122005 Hardness (As CaCO3) < 5 mg/L LCS-122005 LCS-122005 Hardness (As CaCO3) 1030 mg/L 1000 < 5 103 80 120 0512218-006dms MW-4SMS Hardness (As CaCO3) 109 mg/L 100 14.0 95 75 125 0512218-006ddup MW4SDUP Hardness (As CaCO3) 14.0 mg/L 14.0 0 20 1 TSL004 W17 QC SUMMARY REPORT SDG: TSL004 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID• Analyte Result Units Amount Result %REC Limits Value %RPD UCL mb-121405 mb-121405 Nitrate as N < 0.1 mg/L Ics-121405 les -121405 Nitrate as N 1.11 mg/L 1.13 < 0.1 98 80 120 0512218-0O6CMS MW-4SMS Nitrate as N 0.49 mg/L 0.5 < 0.1 98 75 125 0512218-006CDUP MW-4SDUP Nitrate as N < 0.1 mg/L < 0.1 20 mbl-121305 mb1-121.305 Nitrate as N < 0.1 mg/L < 0.1 mg/L Ics-15656 MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0.1 Ics1-121305 Icsl-121305 Nitrate as N 1 1.11 1 mg/L 1 1.13 1 < 0.1 98 180 11201 < 0.1 116 80 120 LCS-15643 LCS-121505 MB1-15643 MB1-121505 Nitrogen, Ammonia (As N) < 0.1 mg/L Ics-15656 MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0.1 mg/L MW-4SMS LCS1-15643 LCS1-121505 Nitrogen, Ammonia (As N) 1.16 mg/L 1 < 0.1 116 80 120 LCS-15643 LCS-121505 Nitrogen, Ammonia (As N) 1.15 mg/L 1 < 0.1 115 80 120 0512218-006CMS MW4SMS Nitrogen, Ammonia (As N) 5.83 mg/L 5 1.03 96 75 125 0512218-006CDUP MW4SDUP Nitrogen, Ammonia (As N) 1.03 mg/L1 11.03 0 120 mb-15656 mb-122005 Nitrogen, Kjeldahl, Total < 0.1 mg/L Ics-15656 Ics-122005 Nitrogen, Kjeldahl, Total 4.22 mg/L 4.1 < 0.1 98 80 120 0512218-006cros MW-4SMS Nitrogen, Kjeldahl, Total 59.5 mg/L 4.1 54.8 114 75 125 0512218-006cdup MW-4SDUP Nitrogen, Kjeldahl, Total _ 53.4 mg/L _ 54.8 �2.6 20 MB -121605 MB -121605 Phenolics, Total Recoverable -� < 5 ug/L LCS-121505 LCS-121605 LCS-121605 Phenolics, Total Recoverable 28.1 ug/L 30 < 5 94 80 120 0512218-006CMS MW-4SMS Phenolics, Total Recoverable 43.4 ug/L 20 24.0 97 75 125 0512218-006Cdup MW4SDLIP Phenolics, Total Recoverable 24.8 ug/L 24.0 3.3 20 MB -121505 MS -121505 Sulfate < 5 mg/L LCS-121505 LCS-121505 Sulfate 18.4 mg/L 20 < 5 92 80 120 0512218-006BMS MW-4SMS Sulfate 32.0 mg/l. 20 12.2 99 75 125 0512218-00613dup MW-4SDUP Sulfate 12.4 mg/L w1.6 20 TSL004 W 18 QC SUMMARY REPORT SDG: TSL004 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121305 MB -121305 Total Dissolved Solids <10 mg/L LCS-121305 LCS-121305 Total Dissolved Solids 306 mg/L 300 <10 102 80 120 0512218-006bms MW-4SMS Total Dissolved Solids 693 mg/L 300 464 76 75 125 0512218-006bdup MW-4SDUP Total Dissolved Solids 465 mg/L 464 0.22 20 MB -121305 MB -121305 Total Organic Carbon < 1 mg/L LCS-121305 LCS-121305 Total Organic Carbon 26.4 mg/L 25 < 1 106 80 120 0512218-006AMS MW-4SMS Total Organic Carbon 9.0 mg/L 10 < 1 90 75 125 0512218-006ADUP MW-4SDUP Total' Organic Carbon < 1 mg/L < 1 20 MB -121205 MB -121205 Total Organic Carbon < 1 mg/L LCS-121205 ILCS-121205 Total Organic Carbon 24.4 mg/L 1 25 < 1 98 80 120 TSL004 W19 U2M UAUS, INC. III. RAW DATA IZA t00"ISZ , W -/Y/ GA& -4 �,&/, _ /W10pt Analysis Ident Amount .. TALK low ICV TV=25mg/I 100 12/9/2005 9.35 2.47 4.19 0.09 23 80 95.20% 9:05:02 AM TALK low ICB 100 12/9/2005 5.16 0.07 4.15 0.06 0.10 <1.0 9',15:57 AM TALK low 0512183-001 a 100 1.2/9/2005 5.83 2.93 4.15 0.17 27.60 9:19:16 AM TALK low 0512200-001 a 100 12/9/2005 7.70 4.95 4.14 0,17 47.85 9:26:34 AM TALK low 0512200-002a 100 12/9/2005 6.61 4.68 4.19 0.16 45.20 9:39:45 AM TALK low 0512211-001 a. 100 12/9/2005 5,37 0.31 4.17 0.12 1.95 9:49:05 AM TALK low 0512224-008a 100 12/9/2005 5.85 1.81 4.15 0.14 16.75 9:53:57 AM TALK low 0512220-001a 100 12/9/2005 5,87 0.15 4.16 0.07 0.80 <1.0 10:01:36 AM TALK low 0512203-001 a 100 12/9/2005 5.07 0.40 4.14 0.17 2.35 10:05:52 AM TALK low 0512203-002a 100 12/9/2005 7.34 5.09 4.17 0.18 49.10 10:10:47 AM TALK low 0512204-001 a 100 12/9/2005 6.78 6.99 4.19 0.17 68.20 10:20:56 AM TALK low 0512204-002a 100 12/9/2005 6.83 7.16 4.15 0.21 69.55 10:29:42 AM TALK low CCV TV=25mg/I 100 12/9/2005 9.40 2.59 4.19 0.09 25.00 100% 10:38:39 AM TALK low CCB 100 12/9/2005 5.50 0.11 4.18 0.08 0.35 <1.0 10:49:54 AM TALK low 0512204-003a 100 12/9/2005 6,30 4.87 4.19 0.18 46.95 10:53:28 AM TALK low 0512204-004a 100 12/9/2005 7.21 4.88 4.18 0,19 46.95 11:00:57 AM TALK low 0512207-001 a 100 12/9/2005 6.86 4.85 4.17 0.19 46.60 11:10:33 AM TALK low 0512218-001 b 100 12/9/2005 7.26 3.29 4.17 0.1.5 31.40 MW -11D 11:19:35 AM TALK low 0512218-002b 100 12/9/2005 6.79 3.20 4.17 0,14 30.60 MW -1S 1 11:29:25 AM �-• mss/ �.-i Ci. Udt/Y eters 5L (moi-# SIS/ Pago 2 e -x ylCe zzrn tooIsi Analysis Ident Amount Date initial pH mIs at 4.5 End value mis af 4.2 TALK % rec TALK low 0512218-003b 100 12/9/2005 5.87 5.27 4.18 0.50 47.75 MW -31D 11:38:03 AM TALK low 0512218-004b 100 12/9/2005 6.64 3.14 4.150.16 29.80 MW -3S 11:44:17 AM TALK low 0512218-005b 100 12/9/2005 6.20 2.59 4.16 0.36 22.35 . MW -4D 11:53:15 AM TALK low 0512218-006b 100 12/9/2005 6.20 4.13 4.16 0.41 37.25 MW -4S 12:00:08 PM TALK low 0512218-006bms 100 12/9/2005 6.69 6.46 4.13 0.47 59.95 90.80% TV=25mgA 12:06:57 PM MW -4S TALK low CCV TV=25mg/l 100 12/9/2005 9.44 2.61 4.15 0.15 24.65 98.60% 12:15:09 PM TALK low CCB 100 12/9/2005 5.37 0.10 4.17 0.09 0.10 <1.0 12:27:29 PM TALK low 0512218-006bdup 100 12/9/2005 6.24 3.87 4.16 0.41 34.60 rpd=7.38% MW -4S 12:31:28 PM TALK low 0512218-007b 100 12/9/2005 6.85 3.14 4.17 0.16 29.85 MW -5D 12:37:45 PM TALK low 0512218-008b 100 12/9/2005 6.89 3.25 4.16 0.16 30.95 MW -5S 12:47:22 PM TALK low 0512218-009b 100 12/9/2005 6.59 2.86 4.15 0.27 25.90 MW -6D 12:56:33 PM TALK low 0512218-010b 100 12/9/2005 6.74 3.00 4.18 0.18 28.20 MW -6S 1:04:18 PM TALK low 0512218-011 b 100 12/9/2005 6.90 3.42 4.17 0.17 32.55 MW -8D 1:14:05 PM TALK low 0512218-012b 100 12/9/2005 6.89 3.11 4.18 0.16 29.55 MW -8S 1:22:58 PM TALK low 0512218-013b 100 12/9/2005 5.48 0.10 4.18 0.10 0.05 <1.0 EQPT BLANK 1:33:18 PM TALK low CCV TV=25mg/l 100 12/9/2005 9.42 2.62 4.14 0.14 24.80 99.20% 1:37:07 PM TALK low CCB 100 12/9/2005 4.97 0.06 4.17 0.09 -0.30 71.0 1:49:25 PM Page • bow H2M S, C. ANALYST: )ATE IN: )ATE OUT: O ;TANDARD DUPLICATE RUE VALUE SAMPLE # :ESULT RESULT I RECOVERY DUPLICATE RPD tD01— HAd'.:,B# Chlorine m /LSAMP. DOF A DO S.C. BOD CALIBRATION CHECK: IN OUT _ 4 WIMETER LA r G� f= mL AVG BOD I -SC BOD C.FJi 9 i,?b- « LAB# i, 00,&S -t, ...... r.� `�I :`J` WNW for ill 1H2AM "13S9 INC. BODS ANALYST CALIBRATION CHECK: IN OUT DATE IN: WINKLER DATE OUT: METER STANDARD DUPLICATE TRUE VALUE "SAMPLE # mL = RESULT RESULT f - RECOVERY DUPLICATE ML RPD ChlorineG•• Now NOW - Chlorine mg/L I BOD � � �� � � - _� -_ --•--- --�- . .__ -------v'i'a WApwm �. Ls r�'=rW=EWM1NMM1� ChlorineG•• Now NOW - TSL004 W24 Chlorine m /L I BOD � � �� � � - _� -_ --•--- --�- . .__ -------v'i'a WApwm �. Ls r�'=rW=EWM1NMM1� OWN�r���� NORM TSL004 W24 .,1...r-. n1!'. f .. ^.l^/1 .. Chlorine mm •ChlorineG•• � � �� � � - _� -_ --•--- --�- . .__ -------v'i'a WApwm �. Ls r�'=rW=EWM1NMM1� OWN�r���� .,1...r-. n1!'. f .. ^.l^/1 WIW&W wi INW, •ChlorineG•• � � �� � � - _� -_ --•--- --�- . .__ -------v'i'a t-�WNt�a����■� OWN�r���� NORM WIW&W wi INW, ---�� r � � �� � � - _� -_ --•--- --�- . .__ -------v'i'a OWN�r���� P G0�ls's •� •� ..I� 7rr Tamil "i.d brl i�d fl�.l lm. 6, i i-- U2M &AUS, 1 ;C. BOL5 ANALYST;CALIBRATION ('lIE('K: IN Oli"I" DATE IN: WINKI.ER DATE OUT: ME- - STANDARD .....—DUPLICATE TRUE VALUE SAMPLE # RESULT RESULT % RECOVERY DUPLICATE Chlorine 7-00) H Ad'.: AVG ff rr�� LAB# Chlorine N3L;tf m /L BOD % SAMP. DO_2REN I 0 DO S . DO -SC BOD :•� TSL004 W25 f - mL C9 � R RZ -00"---� Chlorine mg/L Im NSI • ' ' \ -IF , , i Chlorine mg/L =W. RAMin������� w01 m-vm5'1b.a[811 � i"mWkm • ' ' \ -IF , , i Chlorine mg/L WIN w01 m-vm5'1b.a[811 � i"mWkm P 00's!i IH2M "1?S, INC. BODS ANALYST; DATE IN; DATE OUT:1p STANDARD .DUPLICATE TRUE VALUE SAMPLE # RESULT RESULT % RECOVERY DUPLICATE /. RPD i gr Adj.: Chlorine Bsw •• AVG ` Coo est_ s• Chlorine m :•. air Coo est_ s• :•• air 1 "1.J V NJ --r TV LrV I 11 md Now mw Now wmw wood L. CALIBRATION CHECK: IN OUT WINKLER METER f= rnL s! 7�ri 31► I 1_1 Chlorine air . . . n M tt_�+ r: Q _Chlorine nifyG1� air rkWm F "qmmk_w9 P 00!)() a M �..rrrn....,. �maw 7bmw IN" i..l U2M [APS, INC. BODS ANALYST: CALIBRATION CHECK: IN OUT DATE IN: WINKLER DATE OUT: METER STANDARD .r• "' ` DUPLICATE TRUE VALUE SAMPLE # RESULT RESULT % RECOVERY DUPLICATE RPD nri[nOR►-1 r.n I< 14 PH'Adi.: AVG :•• 1• I• •I• A• :•1 ��go' .J Vwffloma_�_�_ nri[nOR►-1 r.n I< 14 • t :•Chlorine:•� Chlorine mg/L :. • . WNW now ala, • t :•Chlorine:•� ' WNW TSL004 W27 J'= mL = mL g. alb -o1 t a e) pH Adj.: AVG � 1 � LAB# Chlorine ma/L BOD 1• 1 • 1• • 1• • 1 � a i, m loop== OR �Pry pH, 1 M W. P 0.O`.) i H2M LABS, INC. BROMIDE. DATE:I L .2 0 5 ANALYST: G H A=AsAmpE:_AHLMM g:ao Br i BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run report Name of Run c1121205 Name of Analysis :cl.ANL Date of Report 12/12/05 System No. :1 Date of Run 12/12/05 Type of System :TRAACS Operator cp Start/Stop time :16:25 - 17:14 Comment tsl Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/l mg/L Calibr. Fit Quadratic Corr. Coeff. 1.0000 Base 67 Gain 18 Sensitivity 0.5720 Sample Limit 1 Sample Limit 2 ` Pk Cup Sample Id Value V '1/e 0 0 B Baseline 0.011 0 1 1 P Primer 100.568 1 2 1 D Drift 99.485 1 3 1 H1 High 99.610 1 4 0 L1 Low 0.222 1 5 0 L1 Low 0.222 1 6 1 C Cal. 100.142 1 7 2 C Cal. 74.613 1 8 3 C Cal. 50.323 1 9 4 C Cal. 19.936 1 10 5 C Cal. 9.962 1 11 0 C Cal. 0.012 1 12 9 QC3 CRA 2.0 1.765 1 13 10 QC1 LCS 50 50.512 J01 >, 1 14 0 QC10MBLK -0.045 < 2. :�7 1 15 11 S 0512224-008A 8.996 1 16 12 S 0512233-001A 7.111 1 17 13 S 0512260-004A 8.799 1 18 14 S 0512263-001A 9.447 1 19 15 S 0512263-002A 9.770 1 20 16 S 0512263-003A 8.780 1 21 17 S 0512263-004A 9.615 1 Post -run Report BRAN+LUEBBE AACE 5.47 22 18 S 0512263-005A 9.337 1 23 19 5 0512263-006A 9.265 1 24 20 S 0512263-007A 9.413 1 25 2 QC1 ccv75 75.293 1CIO >. 1 26 0 QC1 ccb -0.008 < 1 27 21 S 0512263-OOBA 10.186 1 28 22 S 0512265-001A 25.823 1 29 23 S 0512268-OOIA 11.718 1 30 24 S 0512218-001B IAW- I 4.000 1 31 25 S 0512218-002B KW - 15 4.688 1 32 26 S 0512218-003B NW - 3'P 12.994 1 33 27 S 0512218-004B hW - 35 4.008 1 34 28 S 0512218-005B HW - Liti 7.038 1 35 29 S 0512218-006B V4 - S 6.940 1 36 30 S 0512218-006BMS tY`_ Z S 33.960 1 G$ / 1 37 2 QC1 ccv75 75.200 38 0 QC1 ccb 0.117 39 31 S 0512218-006BDUP hW h S 7.272 '(ZQ7 40 32 S 0512218-007B h W- +7 4.560 1 41 33 S 0512218-OOBB MW ' s 4.429 1 42 34 S 0512218-009Biyts - E l7 5.879 1 43 35 S 0512218-OIOB MW - 6 s 5.101 1 44 36 S 0512218-011B i";iv- $ i7 4.418 1 45 37 S 0512218-012B 11W - S 4.383 1 46 38 S 0512218-013BCQ?i 94-4MV, 0.185 1 47 39 S 0512220-OOIA 0.204 I 48 40 S 0512237-001A 70.649 1 49 2 QC1 ccv75 74.328 50 0 QC1 ccb 0.041 Z_2 51 41 S 0512237-001AMS 'TV-- 2S 93.270 10 %. 1 52 42 S 0512237-OOIADUP 69.542 53 2 QC1 ccv75 74.298 54 0 QC1 ccb 0.095 G_'2 r 1 55 1 D Drift 99.485 1 56 0 B FinalEase 0.011 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused Post -run Report BRAN+LUEBBE RACE 5.47 QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 1.0 ** <END OF REPORT> ** Post -run Report BRAN+LUEBBE AACE 5_.47 H2M LABS INC. Post -run chart Name of run :c1121205.RUN Comment Post -run chart Name of analysis :cl.ANL Page 1 of 3 BRANILUEBBE AACE 5.47 Name of run :c1121205.RUN Comment 18 201 221 241 26 281 301 32 f Post -run chart Name of analysis :cl.ANL i :8C 50.323, �9C 19.9361 I 10 9.962 ---------------------------------------------------- ------------------' �11C 0.012 12QC3 1.765 13QC150.512 -----------------'--------------------------------------------------------' 14QC1.00.045 ' 115S 8.996 16S 7.111 i Ii i ----------- ------------------ r - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -, ,17S 8.799 ' i18S 9.447 119S 9.770 ---------- -------'- ----------------- ii-----------------i------------- - - - - -, ,20S 8-780 121S 9.615 i ,22S 9.337 - - - - - - - - - - - - - - - - J ------------------ L----------------- J ------------------ ; '23S 9.265 i24S 9.413 r i i 25QC175.293 - - - - - - - - - - - - - - - ------------------ r---- - ------------ - - - - - - - 26QC1--0.008 :27S 10.186 128S 25.823 -------------- --------------------- ' ' :29S 11.718 130S 4.000 131S 4.688 i - - - - - - - - - - - -- - - - J ------------------ L ----------------- J ------------------ -----------------32S 32S 12.994 �33S 4.008 �34S 7.038 , :35S 6.940 gfn Page 2 of 3 BRM4LUEBBE RACE 5.47 Name of run :c1121205.RUN Comment 36 381 401 421 46 48 50 52 Post -run chart Name of analysis :cl.ANL I I 1 I I I 1 1 37QC175.200 I I 1 - - - -1 I ---------------------------- ----------------------------------------- � i38QC1 0.117 I I I I I I I 1 ' ' I 139S 7.272 I I I 1 I I 1905 4.560 i I I I - - - - - - ----------------------------------------------- J ------------------ ' ' 1 ' 141S 4.429 1 I I 1 I I I I 42S 5.879 I 1 1 I I I 1 43S 5.1.01 ------ ----------7------------------r------------------------------------199S 9.918 r I I 1 r I I I 1 1 I I 1 1 I 145S 4.383 I I 1 1 1 1 I I 1 i 146S 0.185 1 I I I 1 1 - - - - - - - - - -- --------------2------------------i-------- ,------------ - ----, 147S 0.204 1 I I I 1 I I 48S 70.649 1 I I 149QC174.328 ' 1 I - - --------------- J ------------------ L ----------------- - - - - - - - - - - - - - - - - - - ' 150QC1 0.041 I 1 I 151S 93.270 I I I 1 1 I f 152S 69.592 I -------- --------- I I I 153QC174.298 1 I 1 :54QC1 0.095 I 1 , I I , 1 I � 1 155D 99.985 - - - - - - - - - - I ' ' ------------------------i---------------------------- I 1 I I I I I 156B 0.011 1 I I I 1 I I 1 -----------------J------------------L---------- 1 I 1 1 I I I I I , I I I 1 I I I Page 3 of 3 �t M d" 0l 1--i Cn Fq BRAN+LUEBBE AACE 5.41 H2M LABS INC. Calibration Curve Name of run :c1121205.RUN Comment Calibration Curve Name of analysis :cl.ANL Channel :2 Method :Method 2 Curve fit :quadratic a= -2.5810E+000 b=9.4333E-004 c=1.7400E-008 Corr. coeff. :1.0000 Peak [�J 100 80 i 60 40 20 0 0.00 10.00 20.00 30.00 40.00 50.00 60.00 70.00 80.00 90.00 100.00 110.00 Conc. [ mg/l J Page 1 of 1 Calibration 1/5/2005 cone abs 0 0 10 0,01 25 0.016 50 0.025 125 0.055 250 0,105 375 0,153 500 0.202 625 0.257 750 0.305 8751 0.363 - 10001 0.404 Intercept (b) slope (m) r TSL004 W37 -10.742 2501 0.9989 COD Calibration 1/05/2005 1100 1000 Y = 00.7x - 10.742 900 800 .. 700- 600. • cone E 500 —Linear (cone) u C 400- 300- 200- 100 00300200100 0 -100 42 Absorbance Page 1 of 1 U2M IL AUS, INC. HARDNESS = B x N x I00 000 A HARDNESS DATE: ANALYST: TI'�RANT = Do/M N6,D77 BRAN+LUEBBE AACE 5.47 Post -run Report H2M LABS INC. Post -run report Name of Run NH3121505B Name of Analysis :NH3.ANL Date of Report 12/15/05 System No. :1 Date of Run 12/15/05 Type of System :TRAACS Operator cmo Start/Stop time :13:35 - 14:13 Comment Unit mg/L mg/L PCTSL Pc`�5 oo(-( Calibr. Fit Channel Type Real Data Channel 2 2 Method NH3 Dilution Unit mg/L mg/L Calibr. Fit Linear Corr. Coeff. 0.9993 Base 77 Gain 35 Sensitivity 0.2922 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value 0 0 B Baseline 0.025 0 1 1 P Primer 3.009 1 2 1 D Drift 3.033 1 3 1 H1 High 3.063 1 4 0 L1 Low 0.065 1 5 0 L1 Low 0.066 1 6 1 C Cal. 3.024 1 7 2 C Cal. 0.944 1 8 3 C Cal. 0.448 1 9 4 C Cal. 0.204 1 10 5 C Cal. 0.110 1 11 0 C Cal. 0.045 1 12 5 QC1 CRA 0.1 0.078 1 13 9• QC4 LCS-15643rV=/•v` 1.153 i15�% 1 14 10 QC10MB-15643 0.000 G J�1 1 15 11 S 0512218-001C 0.056 1 ;H,w - lb 16 12 S 0512218-002C 0.115 1 rt e - 1 S 17 13 s 0512218-003C p_ 3.604 n+" 4 1 0Vtr ,el 3D 18 14 S 0512218-004C -0.016 L .� 1 AAA 35 Q1 19 15 S 0512218-OOSC 0.568 1 W N./ 3 20 16 S 0512218-006C 1.025 1 21 17 S 0512218-006CMS'Tf/= 5•C 5.830 q(e�(o 10 ��j O BRAN+LUEBBE AACE 5.47 2 QC 1 Cond. 1 Below Limit 1 0.080 Cond. 2 Above M N S 22 18 S 0512218-006CDUP 1.025 00-""f21 23 19 S 0512218-007C 0.127 0.600 1 l7 24 20 S 0512218-008C 0.040 i,'( 1 25 2 QC4 CCV 1.0 0.914 '11014 1 0.800 26 0 QCIOCCB 0.056 LJ' + 1 Unused 27 21 S 0512218-009C 0.167 Unused 1 H b 28 22 S 0512218-OIOC 0.440 QC10 1 29 23 S 0512218-011C 0.050 1 : 30 24 S 0512218-012C 0.094 �t.� 1 �' S 31 25 S 0512218-013C 0.048 1. 1�•'Ji°"t� 32 26 S 0512167-OOIA 0.076 ,rl!/ 1 33 27 S LFB-15643 —rV= J 5.516 10 34 28 S LFBD-15643 5.33700-331"410 35 2 QC4 CCV 1.0 0.890 �� 1 36 0 QC10CCB 0.058 37 1 D Drift 3.033 1 38 0 B FinalBase 0.025 1 QC Limits Channel 2 QC 1 Cond. 1 Below Limit 1 0.080 Cond. 2 Above Limit 2 0.120 QC 2 Cond. 1 Below Limit 1 0.400 Cond. 2 Above Limit 2 0.600 QC 3 Cond. 1 Below Limit 1 2.000 Cond. 2 Above Limit 2 3.000 QC 4 Cond. 1 Below Limit 1 0.800 Cond. 2 Above Limit 2 1.200 QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Post -run Report BRAN+LUEBBE RACE 5.47 Post -run Report Baseline Yes Drift Yes Carry over Yes %: 3.4 ** <END OF REPORT> ** BRAN+LUEBBE RACE 5.47 H2M LABS INC. Calibration Curve Name of run :NH3121505B.RUN Comment Calibration Curve Name of analysis :NH3.ANL Channel :2 Method :NH3 Curve fit :linear a= -2.0663E-001 b=5.7897E-005 Corr. coeff. :0.9993 Peak [�] 100 1 80 ' I I I ,, - - - - - - - - - - L - - - - - - - - - -'------------ - - I I 1 I 1 I 1 1 I I I I I I I I I 1 - 1 I I I I I I I 1 I I 1 I I � I I 1 I I 1 I , ' � I 1 I I I 1 I 20 ' ' I 1 I 1 1 1 I 1 1 I I Y I I I ' 0 I I 1 1 I C C 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/L ] U Page 1 of 1 BRAN-LUEBBE RACE 5.47 H2M LABS INC. Post -run chart Name of run :NH3121505B.RUN Comment min Channel : 2 Method : NH3 Unit : mg/L Base 77 Gain 35 Corr. 0.9993 Post -run chart Name of analysis :NH3.ANL ' I 1 2 - ------- -- - -- - ------ --- - - - - -- , I , I ' 1 ' I I I I I I I I , � I ' ' I I I I I I ' I 1 I ' ' 1 1 I I , 1 ' I I I 1 I � 1 ' � 1 I , � I ' ' ' I 1 ' I 1 I I 1 I � 1 ' � I ' I I 8 - -- ------------- ------------------I------------------i- ------------ - - - - -i 1 I I I I 1 •I IOB I 1 1 ' I I I , I ;1P I 12 ---------------- 1 —1 12D ' I 1 I I I I 1 I , :3H ' I , ' I I I 14L ' I , I I I ' 1 1 1 , I ' 1 I ' 16C , I 1 1 1 1 , 1 I 17C ' 1 I Page 1 of 3 0.025 3.009 3.033 3.063 0.065 0.066 3.024 0.944 BRANrLUEBBE AACE 5.47 Name of run :NH3121505B.RUN Comment Post -run chart Name of analysis :NH3.ANL Page 2 of 3 BRAN+LUEBBE RACE 5.47 `Name of run : NH3121505B. RUN Comment Post -run chart Name of analysis :NH3.ANL ' ' I 1 1 I ' '37D 3.033 36 - - - - - --- - - - - -- ' I ' ' � 1 ' I I I ' ' � I ' :38B 0.025 ' ' I 38 -----------------'------------------------- -�---- -----' I I I , I 40 ' I I I , 1 I , ' I , I , , ' I 1 � , I I 1 ' � 1 , , I I , ' 1 I , 42 --------------- I 1 I 1 I--------------- ------------------ ---_________________ J ------------------ L ------------------------------------ 46 ____-___-__-__-_J___-_-_ ___ I , I I , I I ' I , ------------------ I I I 1 , I 1 I I I ' ' I I ' ' I I I ' , I I ' � 1 ' ' I , I I ' I , ' ' I I , I I ' I ' ' 1 I I , I 52 -----------------------------------'----- Page 3 of 3 BRAN+LUEBBE AACE 5.47 H2lll..MMM LABS INC. Post -run report Name of Run NH3121505C Name of Analysis :NH3.ANL Date of Report 12/15/05 System No. :1 Date of Run 12/15/05 Type of System :TRAACS Operator cmo Start/Stop time :14:44 - 15:09 Comment Linear PCTSL 0.9994 % VV Channel Type Real Data Channel 2 2 Method NH3 Dilution Unit mg/L mg/L Calibr. Fit Linear Corr. Coeff. 0.9994 Base 77 Gain 35 Sensitivity 0.2907 Sample Limit 1 / Sample Limit 2 r J Pk Cup Sample Id Value OW /ae"'; 0 0 B Baseline 0.028 0 1 1 P Primer 3.004 1 2 1 D Drift 3.028 1 3 1 H1 High 3.064 1 4 0 Ll Low 0.068 1 5 0 Ll Low 0.068 1 6 1 C Cal. 3.023 1 7 2 C Cal. 0.947 1 8 3 C Cal. 0.451 1 9 4 C Cal. 0.201 1 10 5 C Cal. 0.107 1 11 0 C Cal. 0.043 1 12 5 QC1 CRA 0.1 0.076 1 ff 13 9• QC4 LCS1-15643"rv= I•V 1.161 1"0010 1 14 10 QC10MB1-15643 -0.006 L0'1 1 15 11 S 0512218-003C 8.284 10 16 2 QC4 CCV 1.0 0.880 19$% 1 17 0 QClOCCB 0.059 18 1 D Drift 3.028 1 19 0 B FinalBase 0.028 1 Post -run Report 0 C/O H BRAN+LUEBBE AACE 5.47 QC Limits Channel 2 2 QC 1 Cond. 1 Below Carry over Limit 1 0.080 3.5 Cond. 2 Above Limit 2 0.120 QC 2 Cond. 1 Below Limit 1 0.400 Cond. 2 Above Limit 2 0.600 QC 3 Cond. 1 Below Limit 1 2.000 Cond. 2 Above Limit 2 3.000 QC 4 Cond. 1 Below Limit 1 0.800 Cond. 2 Above Limit 2 1.200 QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %' 3.5 ** <END OF REPORT> ** Post -run Report BRAN+LUEBBE AACE 5.47 H2M LABS INC. Calibration Curve Name of run :NH3121505C.RUN Comment Calibration Curve Name of analysis :NH3.ANL Channel :2 Method :NH3 Curve fit :linear a= -2.0461E-001 b=5.8039E-005 Corr. coeff. :0.9994 Peak [ ] 100 1 I I I I 1 1 1 I 1 I I 1 I 1 1 I 1 1 I 1 1 I 1 1 1 ! 1 1 I 1 I 1 I I I 1 I I I 1 I 1 1 I I I I 1 1 I 1 I I 1 I I 1 I 1 1 I I I I 1 1 I I I 1 60 I I , , ----------1----------- I I 1 I 1 1 1 I I i 1 1 I I I 1 I 1 1 I I 1 1 I I 1 I I 1 1 ! 1 I I 1 1 I 1 1 1 1 1 1 1 I 1 1 1 1 I I 1 1 1 I I I I 1 1 I 1 I 1 1 1 ---------- 1 1 I 1 I 1 1 1 I I I C 0() C 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/L ] L E Page 1 of 1 BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run chart Name of run :NH3121505C.RUN Comment Post -run chart Name of analysis :NH3.ANL Page 1 of 2 BRAN+LUEBBE RACE 5.47 Name of run :NH3121505C.RUN Comment Post -run chart Name of analysis :NH3.ANL Page 2 of 2 PC ►"s� 00Y LA US, INC. 1156 Y 3 AMMONIA DISTILLATION LAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE VOLUME MLS FINAL VOLUME MLS DATE ANALYZED SPIKE sa 0 I•� 009.E J 3 oS - "le -j! - A -pole--/ S-oo —30 ,' -3 -Yoo -YS S' o Alf -off -s Ive . vege 60 w Q t f UAAr— -�� pvCpP kFho C C U F P 0098 BRAN+LUEBBE AACE 5.47 Name of Run no3121305aR1 Date of Report 12/13/05 Date of Run 12/13/05 Operator cp Comment bnls,tsl Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 6 H1 High/not 4 0 L1 Low 5 0 L1 Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. 11 0 C Cal. 12 5 QC1 cra0.1 13 10 QC1 lcsl.13 14 0 QC1 mblk 15 11 S 0512182-001A 16 12 S 0512182-002A 17 13 S 0512194-OOIA 18 14 S 0512194-002A 19 15 S 0512196-OOIA 20 16 S 0512196-002A 21 17 S 0512197-OOIA H2M LABS INC. Post -run report Name of Analysis :NO3.ANL System No. :1 Type of System :TRAACS Start/Stop time :16:58 - 17:46 ?6 f4L 5 8125- , T 5 L 00q Real Data 1 2 NO3 Dilution mg/1 mg/L Linear 1.0000 88 12 0.8841 Value ValAre V "V\ 0.004 0 2.006 1 2.011 1 2.041 1 0.016 1 0.016 1 2.005 1 0.997 1 0.487 1 0.202 1 0.100 1 0.007 1 0.093 1 1. 111 �_ 1 0.004 1 1.222 5 0.824 5 4.803 5 0.424 1 0.229 1 4.467 10 0.903 5 Post -run Report N 7t 0 BRAN+LUEBBE AAcE 5.47 1 QC 1 Unused 22 18 S 0512198-001B 2119C- 001 7.087 Unused 10 23 19 S 0512220-OOIA 0.004 QC 8 1 24 20 S 0512275-OOIB 218`10- col 4.771 10 25 2 QCl ccvl.0 1.016 toe., 1 26 0 QC1 ccb 0.004 L0. ( 1 27 21 S 0512218-001C NW - D 0.014 1 28 22 S 0512218-002C MW -15 0.008 1 29 23 S 0512218-003C MW - 9> 0.013 1 30 24 S 0512218-004C NW - 35 0.003 1 31 25 S 0512218-005C MW -14.4 0.048 1 32 26 S 0512218-006C f1W _ `1 S 0.011 1 1 '^ 33 27 S 0512218-006CMS j f I�_� 0.344 cg,/. 1 I WC 34 28 S 0512218-006CDUP �!I 0.036CO O(C 1 WI 35 29 S 0512218-007C MW - S 0.304 1 36 30 S 0512218-008C H W- S S 0.010 1 37 2 QCl ccvl.0 0.975 1 38 0 QC1 ccb 0.001 L •( 1 39 31 S 0512218-009C 1'10 - �'� 0.159 1 40 32 S 0512218-OIOC I'IW - C S 0.207 1 41 33 S 0512218-OIIC 1110 0.063 1 42 34 S 0512218-012C MW - 5 0.008 1 43 35 S 0512218-013C t �11't 9LA 0.083 1 44 36 S 1fb-121305 Ti= 0.5 0.461 45 37 S lfbd-121305 0.468 Qji) I 1 46 2 QCl ccvl.0 0-985 /- 1 47 0 QC1 ccb 0.004 <e - 1 1 48 1 D Drift 2.011 1 49 0 B FinalBase 0-004 1 QC Limits Channel 1 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel I Baseline Yes •}-0o LoW Post -run Report BRAN+LUEBBE RACE 5.47 Drift Yes Carry over Yes %: 1.6 ** <END OF REPORT> ** Post -run Report BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run chart of run :no3121305aR1.RUN Comment min Channel 1 Method NO3 Unit mg/l Base 88 Gain 12 Corr. 1.0000 Post -run chart Name of analysis :NO3.ANL I I 1 I I I I 1 I I 1 I I I I I I I I I 1 I I 1 2 ----------------J------------------L-----------------i------------------1 1 I I 1 1 1 I I 1 I I 1 I I 1 I I 1 1 I I 1 I 1 I 1 1 I I I I I 1 1 1 I I I I I 4 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ - _ _ _ _ - _ _ _ _ _ _ - _ _ _ - _ _ ,_. _ _ - - _ - _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ - - _ _ _ _ _ _ _ _ _ - - _, 1 I I 1 I I I 1 I I I 1 I I 1 1 I I 1 , 1 8 - - - - - - - - - - - - - - - - - -I - - - - - - -I I ------------------------------- , I 1 , , 10 -----------------4------------------ -----------------4-------------------' 12 ----------------- 1 1 , 1 1 I i I , I 19 _________________J 1 _-____-__-_-__--__! I 1 I I I 1 I IOB I , I , 1 I j1P , I 1 1 1 ' '2D ' 1 I ' � I Page 1 of 3 v I 0.004 tn 2.006 d. 2.011 BRANT LUEBBE RACE 5.47 Name of run :no3121305aRl.RUN Comment 181 20{ 22f 24 E 26 28 301 32 F Post -run chart Name of analysis :NO3.ANL - I 1 14L 0.016 1 I I r 1 I I I i i5L 0.016 I I r - - - - - - - - - - - - - - - - - ------------------ I -------------------- --------------16C 2.005 1 1 1 ' I I 1 ,7C 0.997 I I 1 1 I I r ' 1 18C 0.487 1 I 1 1 1 I I 1 -------------------'------------------ -- ----------- - - - - - - ------------------'9C 0.202 1 I I I IlOC 0.100 1 I I I I I r 1 1 I I 111C 0.007 1 I I I I I I - -----------------------------r--------- - - - - - - --------------- - - - - - I 1 , , 112QC10.093 '13QC1 1.111 1 I 1 1 �14QC1 0.004 1 I I I - - - - - - - - -------- - - - - - - - - - - - - - - - - - - I I 1 ----------------- ;------------------1155 1.222 I 1 I 1 I ; :16S 0.824 1 I I 1 I I 1 1 ' ' 117S 4.803 I 1 - - _ _ _ _ - _ _ _ - J _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 1II _ _ - _ - - _ - - _ - - - _ _ _ _ _1 - _ - _ _ _ - _ _ _ _ _ _ _ _ - _ _ 1I1I 185 0.424 I19S 0.229 1205 4.467 ' r I -- - - - -----------ti------------------r------------------------------------1r 215 0.903 I , 1 1225 7.087 ' 1 I i23S 0.004 I , ' I'24S 4.771 1 I 1 I I 1 1 r I 125QC1 1.016 1 I I I 1 I 1 126QC1 0.004 I I 1 1 _ _ -------------- J ------------------ L ------------------ ------------------ 27S -__________-__---27S 0.014 I I I 1 I I 1 �28S 0.008 1 I i i29S 0.013 ' 1 1 I S .003 1 I 1 1 1315 0.048 Page 2 of 3 BRAN+LUEBBE AACE 5.47 Name of run :no3121305aR1.RUN Comment Post -run chart Name of analysis :NO3.ANL 1 I I I '32S 0.011 1 I 1 I I I I I 36 - - - - - - - - - -------------------------:------------------------------ - - - - - ' '33S 0.344 1 1 1 1 1 I I I 34S 0.036 1 1 1 r 1 1 I I '35S 0.304 I 1 I I 1 I I I 38 _ _ -------------- J ------------------ L ----------------- J ------------------ 1 1 I I 1365 0.010 1 I 1 1 1 :37QC1 0.975 1 I I I 1 I I 1 I I 1 1 1 1 138QC1 0.001 I I I 1 40 ' ' I 1 i39S 0.159 1 I I 1 1 i :40S 0.207 1 I I I ' ' 1 1415 0.063 1 I I I 92 ' ' ' 1 ---------------- �------------------�----------------- ;------------------1925 0.008 1 1 I I 1 1 I 1 1 I I I 1 1 I 1435 0.083, I 1 I I 1 ' '44S 0.461 I 1 I 1 1 I 1 I _________________J__----------------- L_________________1__________________195$ 0.468 ' 1 1 1 I I 1 I 1 1 I I i i i46QC1 0.985 I 1 I 1 1 I I 47QC1 0.004 I I 1 1 I 198D 2.011 ' 1 48 ' ' ---__---49B 0.004 1 1 I I 1 , 1 50------------------ J------------------ : ------------------ ' , I I Page 3 of 3 BRANtLUEBBE RACE 5.47 H2M LABS INC. Calibration Curve 'Name of run :no3121305aR1.RUN Comment Calibration Curve Name of analysis :NO3.ANL Channel :1 Method :NO3 Curve fit :linear a= -8.7912E-002 b=3.7440E-005 Corr. coeff. :1.0000 Peak [$] 100 80 60 40 20 0 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 Conc. [ mg/1 ] Page 1 of 1 00 d' O CD BRAN+LUEBBE AACE 5.47 - T -4j -z,_V40�� H2M LABS INC. Post -run report Name of Run no3121405 Name of Analysis :NO3.ANL Date of Report 12/14/05 System No. :1 Date of Run 12/14/05 Type of System :TRAACS Operator cp Start/Stop time' :12:05 - 12:49 Comment mg/l mg/L tsl Fit 75L oo4 Channel Type Real Data Channel 1 2 Method NO3 Dilution Unit mg/l mg/L Calibr. Fit Linear Corr. Coeff. 0.9999 Base 89 Gain 12 Sensitivity 0.8680 Sample Limit 1 Sample Limit 2 �✓ / Pk Cup Sample Id Value Va e 0 0 B Baseline 0.007 0 1 1 P Primer 1.990 1 2 1 D Drift 2.008 1 3 6 H1 High/not 2.050 1 4 0 L1 Low 0.023 1 5 0 L1 Low 0.023 1 6 1 C Cal. 2.007 1 7 2 C Cal. 0.993 1 8 3 C Cal. 0.485 1 9 4 C Cal. 0.197 1 10 5 C Cal. 0.103 1 11 0 C Cal. 0.008 1 12 5 QC1 cra0.1 0.096 1 13 10 QC1 lcsl.13 1.114 1 14 0 QC1 mblk 0.009 < 1 15 11 S 0512359-OOIA 8.825 10 16 12 S 0512359-003A 8.201 10 17 13 S 0512385-006A 6.757 10 18 14 S 0512385-007A 1.418 5 19 15 S 0512385-008A 4.493 10 20 16 S 0512218-006C nw—A6 ) 0.019 1 21 17 S 0512218-006CMS i r= 0.5 0.489 Post -run Report Nt 0 0 BRAN+LUEBBE AACE 5.47 1 QC 1 22 18 S 0512218-006CDUP hN - 0.016 ICP> N 1 23 19 s 0512225-OOIA 1.979 5 24 20 S 0512225-002A 1.772 5 25 2 QC1 ccvl.0 1.052 10S7 1 26 0 QC1 ccb 0.011 L 4.1 1 27 21 S 0512227-OO1B 2.187 5 28 22 S 0512303-001A 8.844 10 29 23 S 0512303-002A 4.130 5 30 24 S 0512303-003A 6.772 10 31 25 S 0512304-001A 2.181 5 32 26 S 0512304-002A 4.627 5 33 27 S 0512307-001A 0.215 1 34 28 s 0512307-002A 2.500 5 35 29 s 0512307-003A 1.678 5 36 30 S 0512307-004A 1.199 5 37 2 QC1 ccvl. 0 0.957 �6 /_ 1 38 0 QC1 ccb 0.011 �_I 1 39 31 S 0512307-004AMS-f Z.� 3.573 9S �S 40 32 S 0512307-004ADUP 1.193 IZ16 � l 5 41 2 QC1 ccvl.0 0.952 42 0 QC1 ccb 0.007 Lo _ 1 1 43 1 D Drift 2.008 1 44 0 B FinalBase 0.007 1 QC Limits Channel 1 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 1 Baseline Yes Drift Yes Carry over Yes %: 1.4 Post -run Report BRAN+LUEBBE AACE 5.47 ** <END OF REPORT> ** Post -run Report BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run chart Name of run :no3121405.RUN Comment min Channel 1 Method NO3 Unit mg/l Base 89 Gain 12 Corr. 0.9999 Post -run chart Name of analysis :NO3.ANL i r r r • r r , r r r r r r r i r 2 ------------------ J ------------------ L ------------------ J ------------------ I r r r r r r r r r r r r r r r r 4 ------------------ ------------------ ------------ - - - - --------------- - - - - -r r , , 8 ----------------:------------------'------------------------------------' � r , r r r r i r r r r 10 -- --------------4------------------ -- - - - - - - - - - - - - - - --------------- - - - - - r r r i r 12 ' ' ---------- - - - - -- ' iOB r , , 14 -----------------'------------------'- r r1P � r , , r r :2D ' � r , r r3H 161 --- Page 1 of 3 0.007 N 1.990 yIND 2.008 0 2.050 0 s, i BRAN+LVEBBE AACE 5.47 Name of run :no3121405.RUN Comment 181 201 221 241 26 28 301 32 1 Post -run chart Name of analysis :NO3.ANL 1 1 I 1 I 1 I 15L 0.023 I 1 1 1 1 1 6C 2.007 , I I - - - - - - - - - -' - - - - - - - - - - - - ' - - - - - - - - - - - - - - - - j - - - - - - - - - - - - - - - - - - ' -- ---- -- i- ' - - - i - , 17C 0.993 I I 1 1 I I I 1 i8C 0.485 I 1 I I 9C 0.197 1 I I I I I 1 I ------------------ J ------------------ L_------_____-____ J ------------------ 10C __-__-______-____10C 0.103 I I I 1 I 1 1 I '11C 0.008 1 I I 1 I I I I i12QC1 0.096 I 1 I I I 1 I -----------------i-----=-----------r----------------- i------------------ :13QC11.119 I 1 I 14QC1 0.009 I I I I 1 1 1 15S 8.825 1 1 1 - - - - - - - - - - - - - - - - ' - - I - - - - - - - - - - - - - - - - - 1 - ----------------- ---------------- ' ' 116S 8.201 I I I 1 I 1 1 , 117S 6.757 1 1 1 I 1 1 1 118S 1.418 I I I I 1 I I I - - - - - - - - - - - - - - - - - J - - - - - - - - - - - - - - - - - - - - - - - J - - - - 1 1 1 119S 4.493 I I 1 I 1 I 1 1 20S 0.019 1 1 I 1 I I 121S 0.489 1 I I 1 ----------------- -1------------------r------------------1------------------i22S 0.016 1 1 ' 123S 1.979 1 1 I 1 i24S 1.772 --------------------- - - - - -- - - - - -------------------2------------------� 1 ' 1'25QC1 1.052 I I I 1 I 1 126QC1 0-011 127S 2.187 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ J _ - _ _ _ _ _ - _ _ _ _ _ _ _ _ _ L _ _ _ _ - _ _ - _ _ _ _ _ _ _ _ _ J _ _ _ _ _ _ _ _ _ _ - _ _ _ - _ _ _ 1 128S 8.844 I I , 1 1 I 1 I I �29S 4.130 1 I I 1 1 , I I 1 I I 1 1305 6.772 1 I I 1 I I I , ,31S 2.181 1 I I i 132S 4.627 Page 2 of 3 BRAN4LUEBBE RACE 5.47 Name of run :no3121405.RUN Comment 36 38 40 42 46 48 50 52 Post -run chart Name of analysis :NO3.ANL I 1 1 I I I I �33S 0.215 1 1I ---------- - - ---- ------------------------------------------------------ 1 I 1 1 - '34S 2.500 1 1 1 I I I 1 I 135S 1.678 i 1 I I I I 1 1 I ' 136S 1.199 1 I I 1 1 1 -- - - - - - - - - - - - - - - - J - - - - - - - - - ------ L - - - - - - - - - - - - - - - --------------------137QC10.957 I I 1 I 1 I I I 1 1 I I I 1 I 38QC1 0.011 I I i i I I 139S 3.573 1 I I I I - - - - - - - - - - - - - - - - -1-- - - - - - - - - - - - - - - - - I-- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - I 1.193 1 I 1 1905 1 1 1 I 1 I I 41QC1 0.952 1 1 1 1 I 42QC1 0.007 1 I I 1 --------------'43D i I I I I 1 2-008 I I I I I 1 I I I I I I I I I 1 I I I I 1 1 1 1 144B 0.007 . - - - - - - - - - - - - - - - - - J _ - _ _ _ _ _ _ _ - _ - - _ _ _ _ _ L _ _ - _ _ - _ - - _ - - _ _ - _ _ ! _ - _ _ _ - - _ _ _ _ _ _ _ _ _ _ I I I I 1 I I 1 I _ I 1 1 I I I I 1 1 I I I I I 1 1 I 1 I 1 1 I I 1 I I I I I 1 I I I I 1 i I 1 I I 1 I I I I I I I I I I I I I I 1 1 I 1 . _ _ _ _ _ _ _ _ _ _ _ _ _' 1 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ 1 _ _ _ _ - _ _ _ _ _ _ - _ _ - - _ _ _ - _ - - _ _ _ _ - - - _ _ _ _ I I I I I I I I I 1 1 I _1 1 1 1 I I 1 I I I I 1 1 1 1 I 1 I I I I I I 1 I -- - - - - - - - - - - - - - - -J- - - - - - - - - ------- -- L- - - - - - -- ----- -------- ---- ----- -- - - I 1 I I I 1 1 I -' 1 1 I I I I 1 I I I 1 I I I I I I I 1 I 1 _ _ _ _ _ _ _ - _ - _ -.4 - _ _ - - _ _ - _ _ _ _ _ _ I I 1 I I 1 I I I 1 I 1 1 I I I 1 I I I I I 1 1 I 1 1 I I I Page 3 of 3 BRAN+LUEBBE AACE 5.47 H2M LABS INC. Calibration Curve Calibration Curve Name of run :no3121405.RUN Name of analysis :NO3.ANL Comment Channel :1 Method :NO3 Curve fit :linear a= -9.1590E-002 b=3.7770E-005 Corr. coeff. :0.9999 Peak [$] 100 80 60 40 .. .. .. 20 0 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 Conc. [ mg/l j Page 1 of 1 Nt O O -.' `-" `•—� •—• �--r z --r ��..I Lrl L�.I W.w Irrrw �.� Y�111 rnrrl �..,r ` J 1...._t U21 "US, INC. Phenols Method 420.1 Distillation Date:I,=S Time: PC i �k ooY V,p t 00 6 Analyst: Date: u CLIENT ID# H2M LAB# mL SAMPLE GRAMS ABS UG/L DILUTION UG/L MG/KG %TS NOTES/CALCULATIONS DISTILLED USED ICV 30 UG/L) 50 o, og 18, g.1 C IB B STD NONE NONE o•®e o zS. 0 ' PREP BLANK 50 0.0V( ,S' : I S. o A, oo�o its^.v .e.s': O 2 0.,06�8•� xr0v �8 3 �9 -oo °. S moo Y4 go °•S o 1p• PsO= oc0 ex.o .4�.0 7 ; 8 M Y� -e°� �0.®0 ,cS.0 CCV 30 UG/L) 50 -0.059 0.06g 16.0 29-f Ib -0 CCB 1 NONE 0.000 ,c 1, 0 .4S.0 -1 oSmPI -00 o o, os AY•o 2 2 3 o•rob Y3• . $.If;#-AorqlA - M 4 - 1/9°.o t0 a . g � 13 '' (0-Q0I �S':J 4-r.,o 5 6 A 0.002-/-S.4 xS.0 J/1-00#6 to. 00 4s,.,o -ZIr. 0 7 W -o oC 0.01, •1 8 " S Bkif -o r 0.0102. .49.0 2s.O xw 0.00 'es.O �S.O saw gp��QdrC CCV 30 UG/L 50 0.000 4s,-0 lzs- 0 19,1 29.1 CCB NONE -0-069 1 0.000 Z z S.,) Phenols TSL004 W66 Intercept (b) 0.6708 slope (m) 402.96 r 0.9997 TSL004 W67 50 40 z 30 c 0 v 20 10 Phenol Calibration 1/24/05 0.050 0.100 0.150 Absorbance Page 1 of 1 96X + 0.6708 • conc --Linear (conc) SULFATE PC t S,2 voy DATE: 12 -/S- a -r I" vo 6 ANALYST: Ni Si v /l �Y0 I'll, 0�t CLIENT ID LAB# MLS USED MG ABS. (G H) JAI MG/L NOTES 1. ICV (20.0 mg/L) is 0.203 1' /I. Y 93' . A. ICB 1 0.000 0.00 00, L J, ip v19D -ovlb -/TO mv 0-00 c.r. 0 Rt t 0.1,6f ls: 2- Atvt— 3 - cog 2. 0-0/1 lS � V - 0.1193 /0• CCV(20.0 mg/L) I3- 0-203 18. y 93 CCB Is- 0.000 .0 J-. O Mir - ys oS - av6 .2sS 0-113 11.2- W t2ff- COCA 2f o. 31 r 31.0 4 -14. J/8-006 li 0.f),6 /z•Y P=l*&," rr— _RP CCV(20.0 mg/L) at s 0.103- �• �i 93 , CCB �s 0.00,0 _ Alt- 0 os*1121 - sip9h If 0.0?2- 8•0 ►u�-6 - Ilf - 0116 Jf 4. off 1 D a IT dl �►�-D 2f CCV(20.0 mg/L) is / d • y Q 3 CCB �.� 0-0010 1S. 0 GS -11- 3Q3 -ogle .S.o 0 . lLI 12.6 x S� 0.0 393-©e/F s.0 0.31 32.3 Xs 16(. RfC�98.S•; S µSet m-aggr SO 0.130 12. E x S= 63.5 R P4J -�W? 7. CCV(20.0 mg/L) S r g • Y 43 •,. Z CCB Zf' �0, Ovo z -r. a &Atjl,,d too Aq /,6 P 0019 00 d - C) 0 CJ] E-� Calibration 08/22/05 conc abs 0 0.000 5 0.032 10 0.09 15 0.142 20 0.207 25 0.271 30 0.338 35 0.417 40 0.480 Intercept (b) 2.3181 slope (m) 80.49 corr. Coeff. 0.9964 SO4 08/22/05 y = 80.494x + 2.3181 030CO40- 30- CO E20 • conc --.Linear (conc) C 0 V • 10- 0 0.000 0.100 0.200 0.300 0.400 0.500 0.600 Absorbance P1 of 1 69M tOOISI WllQ3(m9/i)= mL Sample `.i 'SS/ TS L ANA�rsY, f /� - DATE:TEMP.,q,6�c-1L `l L Oda START. 10:3 HUMIDITYN .5' PAN/ SAMPLE DRIED (?�,v LAB # CLIENT ID CRUC. TARE SOLID RESULT DRIED IGNITED VOL. ML WT G WEIGHT G WEIGHT G V TILE '�" MG/L WT G � WT G WT G R L D �D° 10 o.O3 U? �-Ct3 7+ `gyp 05. r. 150 -847 5 COIL j (7D tnLf I .5l v.v� 05(0"1qcl C636 >D UD � � � .0to 0s & � `� 183 0,0 �(03 fs L+3 L C7� � LF -q (��� cso co5.c�i3 L OD I 1.��3 3 1 TSL004 W70 0 IDSv • -� IfOried VUt (a) -Taro Wt ian„,nnn+....,,... / �c, TS Solids(mg/I)= mL Sample S ANALYST: -*)n .............. DATE: �01 f'3 0 START:"" M HUMIDITY: PAN/ Iii TSL004 W71 ■ r s N 1V TSL004 W71 ■ ■ N 1V IfDrled inn ��� -Tare vv� r..,, eSollds,., LIDS ml Sample (mgA)- x,000 SS/ TS 0 ANALYST: 4R5M DATE: j START: HUMIDITY: PAN/ SAMPLE DRIED TARE SOLID RESULT DRIED IGNITED VOL. LAB # CLIENT ID CRUC. ML WT G WEIGHT G WEIGHT G MG/L VOLATILE CC{% Nr, —3 t—rj� _ � G WT G WT G RES. (MG/L CIO ' ��// t �. �17 105 1 &0- C, (p, �C'Rq -6,q P a� l`JI a` f �5 � Cb3ALFA 3 X50 R C a �00 s2i--s1.7 ` . I l*-� TSL004 W72 3 1 SL °oy s 4251 TKN Data Concentration listed after Optical Blank Correction. Preparation dilation factor not applied to results. SampleED SampTy Conc Units. DF Couc z DF AnalDate AnalTime TestCod I Prima PRIM 3.006 mg/l I 3.006 1220/05 0520:40 PM tlM w 2 Drift DRIP 3.015 ft4 1 3.015 1220/09 0521:20 PM tin w 3 High HIGH 3.011 mg/l 1 3.01 } W20105 0522:00 PM tlM w 4 Low IOW 0.014 mg/l 1 0.014 12!20105 0522:42 PM tkn w 5 Low LOW 0.014 mg1l 1 F 0.014 MOM 052320 PM dm -w 6 Cal. CAL13 3.013 mg/1 1 3.013 1220/05 0524:00 PM tlM w 7 Cal. CAM 0.965 mg/l 1 0.965 1220105 05:24:39 PM tkn w 8 Cal. CALB 0.481 mg/1 1 0:4x1 1220/05 05:2521 PM dM -w 9 Cal. CALB 0.202 mg1l 1 0202 1220105 0526:01 PM tkn w 10 Cal. CAM 0.11 mg4 1 0.11 1220/05 0526:41 PM tkn w 11 Cal. CAM 0.018 mg4 I 0.018 1220!05 0527:22 PM tkn w 12 optical bink QUAL 0.807 mg/l I r 0.807 1220105 0538:00 PM tkn w 13 lcs-15656 Ics I r. 0.4223 mg/l 10 4223 1220/05 1,034' 0528:40 PM tkn w 14 mb-15656 mblk 0.041 mg4 1 0.041 1220/05 X0.1 05:29:20 PM tkn_w 5 0512116-001 B 2197 ka'l SAMP 0.553 mg/l 1 0.553 1220/05 0530:00 PM tkn w .6 0512116-OOIBMS ms's j -z 11,1 0.457 mg/l 10 487 1220105 , 0530:41 PM tkn w 17 0512116-OOIBDUP dup 0.832 mg/l 1 0.832 1220105 00 t'1&. 05:31:21 PM tkn_w 18 0512198-OOI B 211T0 - UD 1 SAMP 0.657 mg/l I 0.657 1220/05 05.32:00 PM tkn w 19 0512275-OOIB Z1110- :#D1 SAMP 3.161 mg/! I 3.161 12/20/05 IGV-4M 05:32:42 PM tkn w a~ 20 0512218-001 C M W - 1 SAW 0.059 mg/1 1 0.059 1220/05 05:33:19 PM dM -w 21 0512218-002C MJ ' IS SAMP 0.015 mg/l 1 F 0.015 1220/05 05:34:00 PM tkn w 22 0512218-003C 11W - 3� SAMP 0.77125 mg/l 20E----15.4251 1220/05. 0534:40 PM tkn w 23 0512218-004C P1W' 3S SAW 0.07 mg/l 1 0.07 1220105 05:3520 PM tkn w 24 0512218-005C I(bJ - 14D SAMP 3.166 mg/l I 3.166 1220105 05`36:02 PM tkn w Ok49-6-a . 25 ccv1.0 ccv 1.073 mg/l 1 1.073 1220/05 tD T 05:36:39 PM tkn w 26 ccb ccb 0.036 mg/l 1 0.036 1220105 40.1 0537:21 PM tkn_w 27 0512218-0060 1t1r1 �} S SAMP 3.8991 mg/l 10 38.991 1220105 Iia 05:38:02 PM tkn w Q�t f 28 0512218-006CMS ms T�1= (1.' 3.8709 mg/l 10 F 38.709 1220/05 05:38:42 PM tkn w 29 0512218 006CDUP dup 3.8713 mg/1 10 38.713 1MOM 05:39:21 PM tkn_w M 30 0512218-007C n t,J- SAMP 0.078 mg/1 1 0.078 1220105 05:39:58 PM tkn w 12005 6:13:51 PM Page 1 of 3 O Peak SamplelD SampTy Conc Units DF Cone: DF AnaWate AnalTime TestCod 31 0512218-008C kw' `F $ SAW 0.22 mg4 1 12120005 05:40:41 PM tlm w 12 0512218-009C hW - CD SAMP 2.989 mg4 1 2989 IYMM atlet* 05.41:21 PM tkn w o -t-- tl't . 33 0512218-010C (1W - S S SAW 3.147 mg/l I 3.147 12/20105 V 05:42:02 PM dm -w 34 0512219-011C ttW SAMP 0.094 mg4 1 1220105 05.42:39PM dw w 35 0512218-012C IIIJ - X 5 SAW 0.094 mg4 1 1220105 05.4330 PM dm -w 36 0512218-013C EQ?'I aL#NSC SAW 0.083 mg/l 1 0.083 12/20105 05:44:01 PM tlm w 37 ccvl.0 ccv 0.97 mg/l I 097 1220105 Sj'T %. 05:44:40 PM tlm w 38 ccb ccb 0.02 mg/l I 0.02 1220105 L D.1 05.4532 PM tkn_w 39 0512196-OOIA SAMP 1.469 mgQ 10 14.69 IMAM 05:46:00 PM tkn w 40 0512196-002A SAMP 2.443 mg/l 1 2443 1220105 ►2j&., 05:46:41 PM tkn Mee ee f C* - 41 0512197-OOIA SAMP . 1.5345 mg/l 20 30.69 1220105 05:47:20 PM dm -w 42 0512182-001 A SAMP 0.7943 mg/l 10 7.943 IMAM 05:47:59 PM tkn w 43 05121824002A SAMP 2.0878 mg/1 10 20.87E 1220105 05:48:40 PM tkn w 44 0512194-OOIA SAMP 1.268 mg4 I 126E 12MM 05.4930 PM dm -w 45 0512194-002A SAMP 2.18475 mg/l 20 43.695 1220105 05:50:00 PM tkn w 46 0512220-002A SAMP 0.167 mg/l 1 0.167 1220105 05:50.40 PM tkn_w 17 0512225-OO1 A SAMP 0.6894 mg/l 10 6.894 1220105 05:51:20 PM tkn_w 18 0512225 -MA SAMP 0.7993 mg/l 20F'15.986! IMAM 05:52:01 PM tkn_w. . 49 ccv 1.0 ccv 0.975 mg/l 1 09751 1220105 05:52:41 PM tkn_w 50 ccb ccb 0.014 mg/l 1 � I220105 <'.J. 05:53:19 PM tkn w 51 0512226-OOIA SAW 0.41194 mg/l 50 20.5971 12211105 05:54:01 PM tkn w 52 0512227-OOIB SAW 1.4674 mg/l 10 14.674 12110105 05:54:40 PM dm -w 53 0512230-OOIA lrO►7! SAMP 1.47406 mg/l 50E--73.703'1 1220105 05:5530 PM dm -w ' 54 0512230-002A I i 2L ! SAW 1.8443 mg4 50' 92215 1220105 05:56:00 PM ft -w 55 0512237-OOIA SAW 02837 mg1l 10 2.837 1220105 05:56:39 PM tkn w 56 05122464002A SAMP 0.596 mg11 I 1220105 05:5731 PM tkn w 57 lfb-15656 )fb 11- 11 OA194 mg/l 10 4.191 1220105 147 / 05:57:59 PM tkn w 58 lfbd-15656 Ifbd OA062 mg/! 10 4.062 1220105 bili 3%.05:58:41 PM tkn w 59 ccvl.0 ccv 0.963 mg/l I 0.963 1220105 E / 05:59:21 PM tkn w 60 ccb ccb 0.008 mg/1 1 1220105 < 0. 06:00:01 PM tkn w 61 0512275-001b 2111 ---Cl SAW 02882 mg/l 10 2.8821 1220105 06:00:40 PM dm -w � 2005 6:13:51 PM Page 2 of 3 O O H Peak Ss mpleID SampTy Cone Units DF Cone a DF AnalDate AnalTime TestCod F2 0512218-005, ItW—� (i SAMP 0.5776 mg/l 10 5.776 12/20/05 06:0121 PM dm—w ''3 0512218-006c }1W — 11 S SAW 1.0963 mgA 50 54.815 12/20/05 06:02:01 PM flm w 64 0512218-006c ms MWI4.1 1.19056 mg/! 50 59.528 12/20/05 115'/'. 06:02:41 PM dm—w 65 0512219-MMup DUP 1.0676 mg4 50E---53-318 1220/05 Rtb 3i 06.03:21 PM dm 66 051221 &009c — (p DO SAMP 0.2642 mgA 10 2.642 1220/05 06:03:59 PM Urn w 67 0512218-010c fjW — 65 SAMP 0.4369 mgA 20 8.738 1220/05 06:04.41 PM tlm w 68 0512196-002a SAMP 02251 mgA 10 2.251 1220/05 06:0521 PM tim w 69 ccv1.0 ccv 0.957 mgA 1 0.957 1220/05 6 /. 06:06:00 PM tkn w 70 ccb ccb 0.005 mgA 1 0.005 1220/05 G 0.1 06:06:39 PM tlm w 71 Drift DRff 3.015 mgA 1 3.015 1280/05 06:07:20 PM tkn w 72 End END 0.01 mg/l 1 0.01 1220/05 06:08:39 PM tkmw 2005 6:13:51 PM Page 3 of 3 O H BRAN+LUEBBE RACE 5.47 Post -run Report H2M LABS INC. Post -run report Name of Run . tkn122005 Date of Report : 12/20/05 Date of Run . 12/20/05 Operator . cp Comment :#15656 tsl,fkit Name of Analysis :tkn.ANL System No. :1 Type of System :TRAACS Start/Stop time :17:09 - 18:09 Channel Type Real Data Channel 2 2 Method tkn Dilution Unit mg/l Calibr. Fit Linear Corr. Coeff. 0.9998 Base 75 Gain 23 Sensitivity 0.4069 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value Va e 0 0 B Baseline 0.010 0��,,�/� 1 1 P Primer 3.006 1 2 1 D Drift 3.015 1 3 1 H1 High 3.011 1 4 0 L1 Low 0.014 1 5 0 L1 Low 0.014 1 6• 1 C Cal. 3.013 1 7 2 C Cal. 0.965 1 8 3 C Cal. 0.481 1 9 4 C Cal. 0.202 1 10 5. C Cal. 0.110 1 11 0 C Cal. 0.018 1 12 8 QC1 optical bink 0.807 1 13 9 QC1 lcs 4.1 5.030 10 14 10 QC1 mblk 0.848 1 15 11 S 0512116-OO1B 1.360 1 16 12 S 0512116-OOIBMS 5.377 10 17 13 S 0512116-OOIBDUP 1.639 1 18 14 S 0512198-OO1B 1.464 1 19 15 S 0512275-OO1B 3.968 1 20 16 S 0512218-OOIC 0.866 1 21 17 S 0512218-002C 0.822 1 d. 0 0 BRAN+LUEBBE AACE 5.47 22 18 S 0512218-003C 16.232 23 19 S 0512218-004C 0.877 24 20 S 0512218-005C 3.973 25 .2 QC1 ccvl.0 1.073 26 0 QC1 ccb 0.036 27 21 S 0512218-006C 39.798 28 22 S 0512218-006CHS 39.516 29 23 S 0512218-006CDUP 39.520 30 24 S 0512218-007C 0.885 31 25 S 0512218-OOBC 1.027 32 26 S 0512218-009C 3.796 33 27 S 0512218-010C 3.954 34 28 S 0512218-011C 0.901 35 29 S 0512218-012C 0.901 36 30 S 0512218-013C 0.890 37 2 QC1 ccvl.0 0.970 36 0 QC1 ccb 0.020 39 31 S 0512196-001A 15.497 40 32 S 0512196-002A 3.250 41 33 S 0512197-001A 31.497 42 34 s 0512182-ODIA 8.750 43 35 S 0512182-002A 21.685 44 36 S 0512194-OOIA 2.075 45 37 S 0512194-002A 44.502 46 38 S 0512220-002A 0.974 47 39 S 0512225-OOIA 7.701 48 40 S 0512225-002A 16.793 49 2 QC1 ccvl.0 0.975 50 0 QC1 ccb 0.014 51 41 S 0512226-001A 21.404 52 42 S 0512227-OO1B 15.481 53 43 S 0512230-ODIA 74.510 54 44 S 0512230-002A 93.022 55 45 S 0512237-001A 3.644 56 46 S 0512246-002A 1.403 57 47 S lfb-15656 5.001 58 48 S lfbd-15656 4.869 59 2 QC1 ccvl.0 0.963 60 0 QC1 ccb 0.008 61 51 S 0512275-001b 3.689 62 52 S 0512218-005c 6.583 63 53 S 0512218-006c 55.622 64 54 S 0512218-006cros 60.335 65 55 S 0512218-006cdup 54.187 66 56 S 0512218-009c 3.449 67 57 S 0512218-010c 9.545 68 58 S 0512196-002a 3.058 69 2 QC1 ccvl.0 0.957 70 0 QC1 ccb 0.005 20 1 1 1 1 10 10 10 1' 1 1 1 1 1 1 1 1 10 1 20 10 10 1 20 1 10 20 1 1 50 10 50 50 10 1 10 10 1 1 10 10 50 50 50 10 20 10 1 1 Post -run Report BRAN+LUEBBE AACE 5.47 Post -run Report 71 1 D Drift 3.015 1 72 0 B FinalBase 0.010 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC B Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 0.7 ** <END OF REPORT> ** HIW+LMBL MICE 5.47. Name of run :tkn122005.RUN Comment :#15656 min Channel : 2 Method : tkn Unit : mg/1 Base 75 Gain 23 Corr. 0.9998 2F -- 4F-- 101 12 10 H2M LABS INC. Post -run chart Post -run chert Name of analysis :tkn.ANL 1 1 t 1 1 t 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 I 1 1 1 I 1 1 1 I --------------------------------L-----------------1------------------1 I 1 I 1 1 17C 1 1 I 1 1 1 1 1 1 1 I 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1 1 1 1 I 1 - - - - - - - - - - - - - - - - - - - - - - - - ----------------- - - - - - - - - - 1- - - - - - - - - - - - - - - - - - -- ------------------ 1 1 1 I I 1 1 1 1 I 1 1 1 I 1 1 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 --------------- -------------1r ------------------------------------- 1 I 1 1 1 1 1 '• f IOB 0.010 1 1 i 1 I t 1 1 1 1 I t 1 1 ----------------- I 1 1 1 1 1 1 t ---------------------------- - - - - - - ---------- 1 1 1 1 1 Page 1 of 4 1P 3.006 I 1 1 1 I I 3.015 1 I I 1 1 1 1 , 1 0.014 1 - - - - - - - - - - - - - - - - - - - - - - - -- - - - - - - - 1 1 1 1 1 1. 3.013 1 I 1 17C 1 1 1 1 I 1 I 1 1 1 I I 1 1 1 1 1 l I I 1 1 1 1 1 1 1 1 t I 1 •-- --—————— — — — — — — ------------------1------- ----+------------------1 1 1 I 1 1 1 1 1 1 '• f IOB 0.010 1 1 t 1 1 ----------------- I 1 1 1 1 1 1 t ---------------------------- - - - - - - ---------- 1 1 1 1 1 Page 1 of 4 1P 3.006 I 1 12D 3.015 1 1 1 :3H 3.011 1 1 1 , :4L 0.014 - - - - - - - ------------------ -----------------15L 15L 0.014' 1 1 1 1 �6C 3.013 1 1 17C 0.965 1 BWrB+LUMM AAM 5.47 Name of run :tkn122005.RUN Comment :#15656 18 20 22 24 26 28 30 32 Post -run chart Name of analysis :tkn.ANL ----- - - - - -- ------------------- ------------ - - - - --------------- - - - - -' r i '8C 0.481 r r r r r r r r i r i 19C 0.202 r r r r r r r r r 116S 5.377 r r :10C 0.110 r r r --- -------- - - - - ----------- --------- L - - - - - - - - - - - - - - - ----------- ---- - - - - -r r r r r r r r i r11C 0.018 1185 1.464 r r r r r r r r i r r r :12QC1 0.807 S 3.968* r r r r r r r r r r13QC1 5.030 r r r r ----- - - - - -- ------------------- ------------ - - - - --------------- - - - - -' r i r i14QC1 0.848 r r r r r r r r r i ' '15S 1.360 r r r r ------------------'-----------------'------------------' r r r 116S 5.377 r r r r r r r r r :17S 1.639 S 3.973* r r r r i i 1185 1.464 r r r r r i r r r r r S 3.968* r r i r r r i20S 0.866 r 1 1 r r r r r r r X215 0.822 r r r r i r ! ' r r ' 122S 16.232 r r r i r ------------------'-----------------'------------------' r �— �23S 0.877 r r r r r r S 3.973* i i �25QC1 1.073 r r r ------------- '26QC1 0.036 r r r r r r r r r r r -- - - - - - - - - - - - - - -- ----------------------------- r r r r r r S 39.798* S 39.516* S 39.520* r :30S r '31S ----------- :32S r r i34S r r r -- - - - - -- - - -- - - - - - - - - - - - - - - - - - - r ' r r'35S r r r r r r r r r Page 2 of 4 0.885 1.027 3.796 3.954* 0000 0.901 0.901 BRX"LBLBBE NICE 5.17 Name of -run :tkn122005.RUN Comment :$15656 36', 381 401 421 46 481 501 521 Post -run chart Name of analysis :tkn.ANL ------------ - - - - - - I I � I r I � 7fl �37QC1 0.970 --------------- ------------------ r r -----------------------------------I r � r r r 1380C1 0.020 r r r I 1545 I r � r i r X395 15.497 I r i I r I I r 3.644 I r r ' '40S 3.250 r --------------r------------------ -----------------I � ------------------ - ---------L-----------------1------------------ --------- L ------------------------------------ r 156S :41S 31.497 I I I r r I r r I r r 142S 8.750 I I I r I I r :43S 21.685 I I 1 I r :585 4.869 ' :445 2.075 ----- - - - - ---J------------------L-----------------1------------------' r r I I i45S 44.502 I r I I I :465 0.974 --2- -- - - - - --------------- --- - -- ----- ----------------------- - - - - - I I 1475 7.701 I I I r r i i r :485 16.793 I i i ' :490C1 0.975 - - - -- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - L - - - - - - - - - - - - - - - - - J - - - - - - - - - - - - - - - - - -' �50QC1 0.014 r I I I :51S 21.404 r I i r i I I i52S 15.481 I ------------ - - - - - - ----------- i59QC1 0.963 I I 53S 74.510 :60QC1 0.008 r � I r r I I r r I i 61S 3.689 1545 93.022 r r i r I r i I r r :555 3.644 I 1 1 r ' -------------- --------------r------------------ -----------------I I 1635 r 156S 1.403 I I I ,575 5.001 I r r r 1 I I 1 :585 4.869 ----- - - - - ---J------------------L-----------------1------------------' Page 3 of 4 r ---q 00 O Ol 1--i UO) F4 i i59QC1 0.963 I I I :60QC1 0.008 r r I r r I i 61S 3.689 I r I r -- - - - - --------'-------------------------------------'------------------' �62S 6.583 r r I I r r r ' 55.622' 1635 r r I :64S 60.335 Page 3 of 4 r ---q 00 O Ol 1--i UO) F4 BFJg4LOLBBE AACE 5.47 Name of run :tknl22005.RUN Comment :#15656 ------------------------ 1 1 1 I 1 1 1 1 1 1 56 ---------------J----------------- I 1 I I 1 1 1 1 1 1 I 1 I 1 1 - -----------------J 1 1 1 I I I 1 1 I 1 1 1 Poet -run chert Name of analysis :tkn.ANL ------------------I 165S 54.187 1 1 i66S 3.449 I 1 167S 9.545 ------------------1 68S 3.058 I I 690C1 0.957 I i70QC1 1 I 1 1 �71D 1 1 I 68 70F I I 1 1 1 1 1 1 1 1 I I I 1 I I 1 1 1 I 1 I I ------------------------------ I 172B --------- ---- -------1 1 1 I • 1 1 1 1 60 1 1 1 - - - - - - - - - - - -' --- -------- - - - - -------- - - - - -- 1 1 1 I 1 1 1 1 1 1 1 1 I 1 I I 1 I 1 t I 1 1 1 1 1 I 1 1 I I 1 1 1 1 1 1 1 1 62 - - - - - - - - - - - - - - - --------- - - - - -- i I ----- ------------------------------------ I 1 1 1 1 1 1 1 1 I 1 I 1 I 1 I I I i I I 1 I I 1 1 1 I I 1 I 1 1 I I 64 1 I 1 1 ------------------+------------------'------------------a------------------1 I 1 1 1 1 1 1 1 1 I 1 t 1 I 1 1 1 I 1 1 1 I 1 1 1 1 66 i 1� ----------- - - - - -------- - - - - ------------ - - - - ---- - - - - -------- 1 1 1 1 1 1 I 1 1 1 1 68 70F I I 1 1 1 1 1 1 1 1 I I 1 I 1 1 1 1 i ------------------------------ -----� 1--------------- 1 --------- ---- -------1 1 1 I 1 I I 1 1 I I 1 1 I 1 I 1 1 1 1 1 I 1 1 1 I 1 1 -----------------'----------------- 1 ----------------------------------- 1 1 1 1 1 1 I _ 1 1 1 1 I 1 — ~ — — — — — — — — — — — — — — — — — •� ------------------ ----------------- ----------------- I I 1 t I I 1 I I 1 1 1 1 1 1 1 I 1 1 1 1 1 1 1 1 1 1 1 1 1 1 I I 1 I 1 1 1 Page 4 of 4 0.005 3.015 0.010 BRAN+IAEBBE AACE 5.47 H2M LABS INC. Calibration Curve Name of run :tknl22005.RUN Comment :115656 Channel :2 Method :tkn Curve fit :linear a= -1.8690E-001 b=6.3519E-005 Corr. coeff. :0.9998 eak [%] 18C 1 60 1 40 20 .n Calibration Curve Name of analysis :tkn.ANL . . . . . . . . . . . . . . I.... ... ....... .... ........ .. .. ...... .... . . I 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ] Page 1 of 1 H2M► I- AUS Nbs Bzs ' INC.' . Pei i4 �Y A �r�6sb TOTAL P S/TRN DIGESTIONS NAME • N► DATE • - Or LAB NO. CLIENT ID �EMPLE WEIGHT GRAMS S=AMPMLE -VOLU E MLS FINAL VOLUME MLS DATE ANALYZED SPIKE 11 �ffll 19 M.I; P QO�:b 00 0 0 h 1Y ir12M LAOS, INC. I TK -J r eirosyo � TOTAL PS/TKN DIGESTIONS i 'f' • r I -E /SAMPLE SAMPLE FINALCGHTNo. CLIENT ID WE] VoLUJME VoLUJME DATE SPIKEGRAM MLS MLS ANALYZED kn 00 0 0 i kn 00 0 0 ,s�,,;,d IZl1de Sample Results Report Print Date/Time: 05/12/13 10:44.25 Sample ID Result Std. Dev. RSD Mode ALT DI 0.3521 L 24.3531 I 0.3101 CRI =sY :.f fef ......................�lrxh MBLK 41-0 0.0900 0512218-001A MIV-(p 4 G 0.1974 0512218-002A.fAV;- S..............4y e 0.2543... 0512218-003A &4W -3A 60.6148 0512218-004A KVJ-3S 9.2592 0512218-005A.kAW-.Li ................469..9008... 0512218-006A AMS- 4S 3.9508 0512218-006AMS * 9.1318 0512218-006ADUP.. .............. ... 0.9076... 0512218-007A tAW- CO z1.0 0. 6696 0512218-008A KW- e'S t! -G 0.5065 ccv-.V: 5fr ...................9:Q- 24.8971... CCB VD 0.4007 0512218-009A MVJ-GO AO 0.2601 0512218-010A.!%W.- U ................4-0 0.2497.. . 0512218-011A MW -$a ZIP 0.3405 0512218-012A MuJ-? 4/-0 0.4861 0512218-013A.C-QFr.V1a+,.............. 1.1162... 3CV i �; 15Ptr. j5.8'/, 23. 9550 CCB coo 0.3807 0.0230 6.53 UTILITY 0.4759 1.95 TOC 0.0391 12.60 TOC 0.1087.. 9.12...TOC 0.0967 107.49 TOC 0.0746 37.78 TOC 0.1115.. 43.86 ... TOC 115.7488 190.96 TOC 0.3021 3.26 TOC 20.6129.. 4 .39 ... TOC ,Q,_ Pqj 0.1642 4.16 TOC Cq(U"j 0.1727 1.89 TOC 0.2009.. 22.14 ... TOC .. 0.0720 10.75 TOC 0.0775 15.30 TOC 1.0039.. 4.03 ... TOC .. 0.0432 10.78 TOC 0.10606 40.98 TOC 0.1194.. 47.80 ... TOC .. 0.0340 10.00 TOC 0.0893 18.37 TOC 0.0450.. 4.03 ... TOC .. 0.4178 1.74 TOC 0.0406 10.68 TOC 110 00 0 0 Sample Results Report Print Date/Time: 2005/12/13 10:44:25 Method ID Sample Type Vial Timestamp Message Cleaning Procedure Sample sp 2005/12/12 15:19 T, kSTE WATER Sample 1 2005/12/12 15:47 Ti kSTE WATER Sample 2 2005/12/12 16:17 Low Sample Detect TOC WASTE WATER ...Sample .. 3..2005/12/12 16:47 ..Low Sample Detect TOC WASTE WATER Sample 4 2005/12/12 17:16 Low Sample Detect TOC WASTE WATER Sample 5 2005/12/12 17:46 Low Sample Detect TOC WASTE WATER ...Sample .. 6..2005/12/12 18:15 ..Low Sample Detect TOC WASTE WATER Sample 7 2005/12/12 18:47 Low Sample Detect TOC WASTE WATER Sample 8 2005/12/12 19:15 TOC WASTE WATER ...Sample .. 9..2005/12/12 19:45 .. TOC WASTE WATER Sample 10 2005/12/12 20:13 TOC WASTE WATER Sample 11 2005/12/12 20:41 TOC WASTE WATER ...Sample .. 12..2005/12/12 21:10 ..Low Sample Detect TOC WASTE WATER Sample 13 2005/12/12 21:40 Low Sample Detect TOC WASTE WATER Sample 14 2005/12/12 22:09 Low Sample Detect TOC WASTE WATER ...Sample .. 15..2005/12/12 22:38 .. TOC WASTE WATER Sample 16 2005/12/12 23:04 Low Sample Detect TOC WASTE WATER Sample 17 2005/12/12 23:37 Low Sample Detect TOC WASTE WATER ...Sample .. 18..2005/12/13 00:03 ..Low Sample Detect TOC WASTE WATER Sample 19 2005/12/13 00:36 Low Sample Detect TOC WASTE WATER Sample 20 2005/12/13 01:02 Low Sample Detect TOC WASTE WATER ...Sample .. 21..2005/12/13 01:35 ..Low Sample Detect POC WASTE WATER Sample 22 2005/12/13 02:04 POC WASTE WATER Sample 23 2005/12/13 02:34 Low Sample Detect Detailed Analysis Report Print Date/Time: 2005/12/13 10:44:28 Sample ID: DI # ppm C Mode: UTILITY Method: Cleaning Procedure Filename: 12121455 Ca urve: TOC WW CURVE 093005 Timestamp: 2005/12/12 15:19 Op or ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 0.0168 9288 Baseline Baseline Time 1 0.3513 0.1757 44695 9.764 9.964 131 2 0.3843 0.1922 48369 9.805 10.004 130 3 0.3412 0.1706 43564 9.750 9.949 128 4 0.3314 ----------------------------------------------------------------------------- 0.1657 42476 9.750 9.948 128 <Statistics>>> Mean: 0.3521 Std Dev: 0.0230 RSD: 6.53 Sample ID: LCS 120 Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 15:47 Operator ID: JASON SAMUEL Sample Type: Sample' Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 23.7563 1.1878 270235 9.674 10.669 110 2 24.6017 1.2301 279655 9.685 10.680 110 3 24.8442 1.2422 282357 9.716 10.711 110 4 24.2103 ----------------------------------------------------------------------------- 1.2105 275294 9.678 10.675 110 :< itistics>>> Mean: 24.3531 Std Dev: 0.4759 RSD: 1.95 Sample ID: ICB Mode: TOC 9ethod: TOC WASTE WATER Filename: 12121455 :al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 16:17 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending. Integration Baseline Baseline Time 1 0.3354 0.0168 9288 9.575 9.581 120 2 0.3479 0.0174 9428 9.555 9.558 120 3 0.2948 0.0147 8836 9.538 9.559 120 4 ----------------------------------------------------------------------------- 0.2624 0.0131 8475 9.539 9.528 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 0.3101 Std Dev: 0.0391 RSD: 12.60 ample ID: CRI fethod: TOC WASTE WATER al. Curve: TOC WW CURVE 093005 -perator ID: JASON SAMUEL P, ppm C ug C Raw Data Mode: TOC Filename: 12121455 Timestamp: 2005/12/12 16:47 Sample Type: Sample Beginning Ending Integration 00 00 O O F"{ Sample ID: 0512218-OOIA Method: TOC WASTE WATER ::P1 Curve: TOC WW CURVE 093005 D] for ID: JASON SAMUEL 2ep # ppm C ug C Raw Data 1 0.3029 0.0151 Baseline Baseline Time 1 1.2285 0.0614 19239 9.613 9.634 120 2 1.2096 0.0605 19028 9.627 9.649 120 3 1.2913 0.0646 19939 9.641 9.662 120 4 1.0372 - ------------------------------------------------------------------------ 0.0519 17108 9.631 9.639 120 LL__'Message: Low Sample Detected Sample Detected <<<Statistics>>> ----------------------------------------------------------------------------- ----------------------------------------------------------------------------- Mean: 1.1916 Std Dev: 0.1087 RSD: 9.12 Sample ID: MBLK Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 17:16 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.1992 0.0100 7771 9.680 9.693 120 2 0.1245 0.0062 6938 9.699 9.731 120 3 0.0663 0.0033 6290 9.704 9.704 120 4 -0.0300 ----------------------------------------------------------------------------- -0.0015 5217 9.707 9.704 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.0900 Std Dev: 0.0967 RSD: 107.49 Sample ID: 0512218-OOIA Method: TOC WASTE WATER ::P1 Curve: TOC WW CURVE 093005 D] for ID: JASON SAMUEL 2ep # ppm C ug C Raw Data 1 0.3029 0.0151 8926 2 0.1963 0.0098 7739 3 0.1379 0.0069 7088 4 ------------------------------------ 0.1525 0.0076 7251 :,ast Message: Low Sample Detected :«Statistics>>> Mean: 0.1974 ;ample ID: 0512218-002A fethod: TOC WASTE WATER :al. Curve: TOC WW CURVE 093005 >perator ID: JASON SAMUEL Mode: Filename: Timestamp: Sample Type: TOC 12121455 2005/12/12 17:46 Sample Beginning Ending Baseline Baseline 9.620 9.619 9.583 9.584 9.574 9.574 9.587 -------------------------- 9.573 Std Dev: 0.0746 RSD: 37.78 Mode: Filename: Timestamp: Sample Type: ,ep # ppm C ug C Raw Data Beginning 120 9.500 120 9.470 Baseline 1 0.3845 0.0192 9836 9.565 2 0.2377 0.0119 8200 9.512 3 0.2800 0.0140 8671 9.471 4 --------------------------------------------------- 0.1149 0.0057 6832 9.405 1� Message: Low Sample Detected Integration Time 120 120 120 120 TOC 12121455 2005/12/12 18:15 Sample Ending Integration Baseline Time 9.540 120 9.500 120 9.470 120 9.379 ------------------------- 120 <<<Statistics>>> Mean: 0.2543 Std Dev: 0.1115 RSD: 43.86 Sa le ID: 0512218-003A Mode: TOC M d: TOC WASTE WATER Filename: 12121455 Ca Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 18:47 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 161 2 Baseline Baseline Time 1 234.2110 11.7105 2615043 10.436 11.428 104 2 5.5300 0.2765 67165 9.863 9.758 120 3 2.0189 0.1009 28045 9.589 9.569 120 4 0.6993 ----------------------------------------------------------------------------- 0.0350 13343 9.514 9.482 120 Last Message: Low Sample Detected 149 :«Statistics>>> <<<Statistics>>> Mean: 60.6148 Std Dev: 115.7488 RSD: 190.96 Sample ID: 0512218-004A Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 19:15 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 9.5177 0.4759 111594 9.422 10.411 101 2 8.9828 0.4491 105635 9.419 10.406 102 9.0128 0.4506 105969 9.443 10.428 101 9.5235 -- -------------- - 378---- 10.376 :«Statistics>>> -0_4762----111659--------- Mean: 9.2592 Std Dev: 0.3021 ------102----- --------- _ RSD: 3.26 Sample ID: 0512218-005A Mode: TOC 4ethod: TOC WASTE WATER Filename: 12121455 :al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 19:45 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 468.6432 23.4322 5227000 9.518 10.517 161 2 441.3155 22.0658 4922525 13.763 14.726 121 3 482.5124 24.1256 5381526 10.199 11.194 142 4 ----------------------------------------------------------------------------- 487.1322 24.3566 5432997 9.922 10.920 149 :«Statistics>>> Mean: 469.9008 Std Dev: 20.6129 RSD: 4.39 amp e ID: 0512218-006A Mode: TOC ethod: TOC WASTE WATER Filename: 12121455 al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 20:13 0tor ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Ending Integration Baseline Baseline Time 1 3.9949 0.1997 50061 9.223 10.222 98 9 3.7452 0.1873 47279 9.178 10.173 97 3.9228 0.1961 49258 9.163 10.159 97 _ 4.1402 ----------------------------------------------------------------------------- 0.2070 51681 9.143 10.142 97 <<<Statistics>>> Mean: 3.9508 Std Dev: 0.1642 RSD: 4.16 120 Sample ID: 0512218-006AMS Mode: TOC 15942 Method: TOC WASTE WATER Filename: 12121455 'jast Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 20:41 Operator ID: JASON SAMUEL Sample Type: Sample 0.9076 Std Rep # ppm C ug C Raw Data Beginning Ending Integration 8.928 120 Baseline Baseline Time 1 9.1390 0.4569 107375 9.163 10.156 103 2 8.9168 0.4458 104899 9.139 10.138 103 3 9.3397 0.4670 109611 9.088 10.076 104 4' 9.1317 ----------------------------------------------------------------------------- 0.4566 107294 9.059 10.052 102 <<<Statistics>>> Mean: 9.1318 Std Dev: 0.1727 RSD: 1.89 Sample ID: 0512218-006ADUP Mode: TOC Hethod: TOC WASTE WATER Filename: 12121455 Sal Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 21:10 DI for ID: JASON SAMUEL Sample Type: Sample F-+ hep # ppm C ug C Raw Data Beginning Ending Integration WASTE WATER Filename: 12121455 Baseline Baseline Time 1 1.1679 0.0584 18564 8.853 8.851 120 2 0.8430 0.0421 14944 8.828 8.860 120 3 0.6872 0.0344 13208 8.836 8.846 120 4 ----------------------------------------------------------------------------- 0.9325 0.0466 15942 8.839 8.881 120 'jast Message: Low Sample Detected 2 0.6767 0.0338 13091 :«Statistics>>> Mean: 0.9076 Std Dev: 0.2009 RSD: 22.14 0.0362 ;ample ID: 0512218-007A Mode: TOC iethod: TOC WASTE WATER Filename: 12121455 .al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 21:40 )perator ID: JASON SAMUEL Sample Type: Sample ;ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.7110 0.0355 13473 8.914 8.914 120 2 0.6767 0.0338 13091 8.879 8.898 120 3 0.7248 0.0362 13627 8.884 8.928 120 r� 01 4 0.5660 0.0283 11858 8.920 8.951 120 r� ----------------------------------------------------------------------------- Message: Low Sample Detected CD CD F-+ <<<Statistics>>> Mean: 0.6696 Sample ID: 0512218-008A Me d: TOC WASTE WATER Ca curve: TOC WW CURVE 093005 Operator ID: JASON SAMUEL Std Dev: 0.0720 RSD: 10.75 ----------------------------------------- ----------------------------------------- Mode: TOC Filename: 12121455 Timestamp: 2005/12/12 22:09 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.6030 0.0302 12270 8.935 8.955 120 2 0.5333 0.0267 11493 8.967 9.003 120 3 0.4595 0.0230 10671 8.987 8.998 120 4 0.4304 ----------------------------------------------------------------------------- 0.0215 10347 8.981 8.993 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5065 Std Dev: 0.0775 RSD: 15.30 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 22:38 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 25.5887 1.2794 290651 9.008 9.998 110 2 23.4409 1.1720 266722 9.025 10.018 110 3 25.0221 1.2511 284338 9.042 10.035 110 25.5365 -- ------------------------------------------------------------------------ 1.2768 290070 9.029 10.028 110 <<<Statistics>>> Mean: 24.8971 Std Dev: 1.0039 RSD: 4.03 Sample ID: CCB Mode: TOC 4ethod: TOC WASTE WATER Filename: 12121455 ,al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 23:04 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.4520 0.0226 10588 8.972 8.991 120 2 0.4151 0.0208 10176 8.985 9.009 120 3 0.3851 0.0193 9842 8.981 8.985 120 4 0.3506 ----------------------------------------------------------------------------- 0.0175 9458 8.965 8.977 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 0.4007 Std Dev: 0.0432 RSD: 10.78 :ample ID: 0512218-009A Mode: TOC fethod: TOC WASTE WATER Filename: 12121455 'al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/12 23:37 )F for ID: JASON SAMUEL Sample Type: Sample N C� d' O O L/1 F-+ Rep # ppm"C ug C Raw Data Beginning Ending Integration - 120 2 0.3463 Baseline Baseline Time 1 0.2743 0.0137 8608 8.663 8.607 120 2_ 0.2712 0.0136 8573 8.550 8.537 120 0.3767 0.0188 9749 8.403 8.393 120 0.1181 ------------------------------------------------------------------------------ 0.0059 6868 8.363 8.337 120 Last Message: Low Sample Detected 0.0340 RSD: 10.00 <<<Statistics>>> Mean: 0.2601 Std Dev: 0.1066 RSD: 40.98 Sample ID: 0512218-010A Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 00:03 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time .1 0.3866 0.0193 9859 8.173 8.171 120 2 0.3130 0.0157 9039 8.134 8.149 120 3 0.1483 0.0074 7204 8.128 8.119 120 4 0.1511 ----------------------------------------------------------------------------- 0.0076 7235 8.117 8.113 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.2497 Std Dev: 0.1194 RSD: 47.80 Sample ID: 0512218-011A Me 3: TOC WASTE WATER Ca ::urve: TOC WW CURVE 093005 Operator ID: JASON SAMUEL Rep # ppm C ug C Raw Data Mode: TOC Filename: 12121455 Timestamp: 2005/12/13 00:36 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 1 0.3854 0.0193 9846 8.063 8.080 120 2 0.3463 0.0173 9410 8.061 8.078 120 3 0.3068 0.0153 8970 8.043 8.042 120 4 ----------------------------------------------------------------------------- 0.3234 0.0162 9155 8.005 8.017 120 �ast Message: Low Sample Detected :«Statistics>>> Mean: 0.3405 Std Dev: 0.0340 RSD: 10.00 Sample ID: 0512218-012A 9ethod: TOC WASTE WATER i .al. Curve: TOC WW CURVE 093005 )perator ID: JASON SAMUEL tep # ppm C ug C Raw Data 1 0.4739 0.0237 10832 2 0.4231 0.0212 10266 0.4315 0.0216 10360 Mode: TOC Filename: 1212145 Timestamp: 2005/12/13 01:02 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 7.955 7.967 120 7.951 7.971 120 7.961 7.999 120 4 0.6158 ----------------------------------------------------------------------------- 0.0308 12413 7.986 8.040 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.4861 Std Dev: 0.0893 RSD: 18.37 Sample ID: 0512218-013A Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 01:35 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 1.0837 0.0542 17626 8.414 8.508 120 2 1.1823 0.0591 18724 8.471 8.572 120 3 1.0926 0.0546 17725 8.564 8.660 120 4 1.1062 ----------------------------------------------------------------------------- 0.0553 17877 8.601 8.703 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 1.1162 Std Dev: 0.0450 RSD: 4.03 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 12121455 Cal_ Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 02:04 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 23.7352 1.1868 270001 8.806 9.796 110 23.9140 1.1957 271993 8.816 9.814 110 3 23.6165 1.1808 268678 8.827 9.827 109 4 24.5543 ----------------------------------------------------------------------------- 1.2277 279126 8.841 9.832 111 ;«Statistics>>> Mean: 23.9550 Std Dev: 0.4178 RSD: 1.74 Sample ID: CCB Mode: TOC 4ethod: TOC WASTE WATER Filename: 12121455 ,al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 02:34 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.3885 0.0194 9880 8.881 8.896 120 2 0.4026 0.0201 10037 8.859 8.874 120 3 0.4103 0.0205 10123 8.844 8.874 120 4 0.3212 ----------------------------------------------------------------------------- 0.0161 9131 8.854 8.874 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 0.3807 Std ------------------------------------------------------- Dev: 0.0406 RSD: 10.68 Calibration Report Print Date/Time: 2005/12/13 10:44:35 Cal. Curve ID: TOC WW CURVE 093005 Created: 2005/10/04 17:01 C-libration Factor (m): 2.228e+05 Y:ercept (b): 5855 r _dared: 0.99963 Standard ID Y X Expected Measured Message Date & Raw Data ug C ug C Time DI 13148 0.000 0.033 Low Sample De 2005/10/04 14:27 0.5PPM 14616 0.025 0.039 Low Sample De 2005/10/04 14:49 1.OPPM 18776 0.050 0.058 Low Sample De 2005/10/04 15:11 5.OPPM 57013 0.250 0.230 2005/10/04 15:33 10.OPPM 111868 0.500 0.476 2005/10/04 15:54 25.OPPM 284040 1.250 1.248 2005/10/04 16:16 50.OPPM 553794 2.500 2.459 2005/10/04 16:38 75.OPPM 848670 3.750 3.782 2005/10/04 17:00 ���s Sample Results Report /Pr Date/Time: 5 1.2/14 9.24: 7 Sample ID V, Result Std. Dev. RSD Mode ALT DI `l 0.3346 LC �,' ZSr^ 26.3539 C. IRI .:I1�:. P!`� ............. t1.0 0. 6361 P .. rag;r• 1.2836... 4BLK ZI-0 0.1164 )512218-003A MW'30 4OX 29.1657 NO )512218-005A.1AWAO......... ..'�O�G 11.3507.'51 )512218-006A MW -4S' zID 0.3910 )512218-006AMS-TV-t0f" � % '�� 8.9840 )512218-006ADUP......... R L NO. A -,.O 0.2746... :cv ?y- ZSR 25.6749 =CB y.o 0.3314 SLvv4 0.0070 2.08 UTILITY 0.5333 2.02 TOC 0.0700 11.01 TOC 0.1387.. 10.80 ... TOC .. 0.1897 162.93 TOC 0.4132 1.42 TOC 0.2252.. 1.98 ... TOC. .. 0.0771 19.71 TOC 0.3043 3.39 TOC 0.0530.. 19.30 ... TOC .. 0.1325 0.52 TOC 0.0198 5.96 TOC 0 0 Sample Results Report Print Date/Time: 2005/12/14 9:24:07 Method ID Sample Type Vial Timestamp Message �leaning Procedure Sample ---------------------------- sp 2005/12/13 14:39 PO LSTE WATER Sample 1 2005/12/13.15:08 CO_ _iSTE'WATER Sample 2 2005/12/13 15:37 Low Sample Detect COC WASTE WATER ...Sample .. 3..2005/12/13 16:07 ..Low Sample Detect COC WASTE WATER Sample 4 2005/12/13 16:36 Low Sample Detect COC WASTE WATER Sample 5 2005/12/13 17:05 COC WASTE WATER ...Sample .. 6..2005/12/13 17:33 .. COC WASTE WATER Sample 7 2005/12/13 18:03 Low Sample Detect 'OC WASTE WATER Sample 8 2005/12/13 18:31 'OC WASTE WATER ...Sample .. 9..2005/12/13 19:01 ..Low Sample Detect 'OC WASTE WATER Sample 10 2005/12/13 19:29 'OC WASTE WATER Sample 11 2005/12/13 19:56 Low Sample Detect Detailed Analysis Report Print Date/Time: 2005/12/14 9:24:09 Sample ID: DI Mode: UTILITY Method: Cleaning Procedure Filename: 12131415 Car' '"urve: TOC WW CURVE 093005 Timestamp: 2005/12/13 14:39 Op' or ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration WW CURVE 093005 Timestamp:. 2005/12/13 15:08 )perator ID: JASON SAMUEL Sample Type: Sample Baseline Baseline Time 1 0.3390 0.1695 43321 9.663 9.861 128 2 0.3245 0.1622 41701 9.701 9.901 126 3 0.3394 0.1697 43370 9.745 9.945 128 4 ----------------------------------------------------------------------------- 0.3354 0.1677 42920 9.851 10.0.49 129 :«Statistics>>> Mean: 0.3346 Std Dev: 0.0070 RSD: 2.08 Sample ID: LCS # ppm C Mode: TOC 9ethod: TOC WASTE WATER Filename: 12131415 ,al. Curve: TOC WW CURVE 093005 Timestamp:. 2005/12/13 15:08 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration 1 0.5886 Baseline Baseline Time 1 26.2463 1.3123 297979 10.202 11.200 112 2 27.1198 1.3560 307710 10.250 11.248 111 3 26.1630 1.3082 297050 10.279 11.274 111 4 25.8864 ----------------------------------------------------------------------------- 1.2943 293968 10.248 11.242 110 X Itistics>>> Mean: 26.3539 Std Dev: 0.5333 RSD: 2.02 ;ample ID: ICB 10.332 Mode: TOC [ethod: TOC WASTE WATER Filename: 12131415 :al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 15:37 Aerator ID• JASON SAMUEL Sample Type: Sample .ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5886 0.0294 12109 10.133 10.177 120 2 0.5941 0.0297 12170 10.289 10.307 120 3 0.6230 0.0311 12492 10.311 10.332 120 4 ---------------------------------------------------------------------------- 0.7387 0.0369 13782 10.364 10.397 120 ast Message: Low Sample Detected <<Statistics>>> Mean: 0.6361 Std Dev: 0.0700 RSD: 11.01 ample ID: CRI ethod: TOC WASTE WATER al. Curve: TOC WW"CURVE 093005 perator ID: JASON SAMUEL ppm C ug C Raw Data Mode: TOC Filename: 12131415 Timestamp: 2005/12/13 16:07 Sample Type: Sample Beginning Ending Integration Sample ID: MBLK C Mode: TOC Baseline Baseline Time 1 1.4481 0.0724 21686 10.322 10.394 120 2 1.3373 0.0669 20452 10.456 10.492 120 3 1.1302 0.0565 18144 10.479 10.475 120 4 -- 1.2188 ------------------------------=----------------------------------------- 0.0609 19131 10.463 10.508 120 La lessage: Low Sample Detected 'last Message: Low Sample Detected 10.443 11.437 <<<Statistics>>> Mean: 1.2836 Std Dev: 0.1387 RSD: 10.80 'ample ID: 0512218-003A Sample ID: MBLK C Mode: TOC Method: TOC WASTE WATER Ending Filename: 12131415 �al. Curve: TOC WW CURVE 093005 al. Curve: Timestamp: 2005/12/13 16:36 operator ID: JASON SAMUEL Baseline Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration 10.403 11.389 Baseline Baseline Time 1 0.0261 0.0013 5842 10.613 10.597 120 2 -0.0987 -0.0049 4452 10.458 10.433' 120 3 0.2106 0.0105 7898 10.420 10.411 120 4 0.3277 0.0164 ----------------------------------------------------------------=------------ 9203 10.396 10.407 120 'last Message: Low Sample Detected 10.443 11.437 110 ;«Statistics>>> Mean: 0.1164 Std Dev: 0.1897 RSD: 162.93 'ample ID: 0512218-003A Mode: TOC lethod: TOC WASTE WATER Filename: 12131415 :al- Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 17:05 )F itor ID: JASON SAMUEL Sample Type: Sample tep #ppm C ug C Raw Data Beginning Ending Integration 12131415 al. Curve: TOC WW CURVE 093005 Timestamp: Baseline Baseline Time 1 29.7273 1.4864 336762 10.403 11.389 110 2 28.7564 1.4378 325945 10.396 11.391 110 3 29.1835 1.4592 330704 10.406 11.402 110 4 ----------------------------------------------------------------------------- 28.9957 1.4498 328611 10.443 11.437 110 :«Statistics>>> Mean: 29.1657 Std Dev: 0.4132 RSD: 1.42 ample ID: 0512218-005A Mode: TOC .ethod: TOC WASTE WATER Filename: 12131415 al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 17:33 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 11.2174 0.5609 130532 10.376 11.365 105 2 11.5108 0.5755 133800 10.351 11.348 106 3 11.5700 0.5785 134460 10.338 11.332 106 4 ---------------------------------------------------------------------------- 11.1045 0.5552 129273 10.347 11.342 105 <<Statistics>>> Mean: ------------ - 11.3507 Std - ------------------------------------------------ Dev: 0.2252 RSD: 1.98 Sample ID: 0512218-006A Method: TOC WASTE WATER Cal. Curve: TOC WW CURVE 093005 Or :or ID: JASON SAMUEL Mode: TOC Filename: 12131415 Timestamp: 2005/12/13 18:03 Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration �:al. Curve: TOC WW CURVE 093005 Timestamp 2005/12/13 18:31 Baseline Baseline Time 1 0.4306 0.0215 10350 10.441 10.440 120 2 0.2764 0.0138 8631 10.430 10.442 120 3 0.4159 0.0208 10186 10.401 10.401 120 4 ----------------------------------------------------------------------------- 0.4410 0.0221 10466 10.381 10.394 120 Last Message: Low Sample Detected RSD: 3.39 Sample ID: 0512218-006ADUP Mode: <<<Statistics>>> 4ethod: TOC Mean: 0.3910 Std Dev: 0.0771 RSD: 19.71 WW CURVE 093005 Sample ID: 0512218-006AMS Mode: TOC Method: TOC WASTE WATER Filename: 12131415 �:al. Curve: TOC WW CURVE 093005 Timestamp 2005/12/13 18:31 Jperator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 0.0115 8111 Baseline Baseline Time 1 8.9508 0.4475 105278 10.305 11.302 104 2 8.7648 0.4382 103206 10.311 11.305 104 3 8.7964 0.4398 103558 10.304 11.296 102 4 9.4239 ----------------------------------------------------------------------------- 0.4712 110549 10.267 11.263 104 :< atistics>>> Mean: 8.9840 Std Dev: 0.3043 RSD: 3.39 Sample ID: 0512218-006ADUP Mode: TOC 4ethod: TOC WASTE WATER Filename: 12131415 ;al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 19:01 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2297 0.0115 8111 10.105 10.091 120 2 0.2280 0.0114 8092 10.072 10.080 120 3 0.3149 0.0157 9060 10.035 10.012 120 4 ----------------------------------------------------------------------------- 0.3257 0.0163 9180 10.013 9.992 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 0.2746 Std Dev: 0.0530 RSD: 19.30 ample ID: CCV Mode: TOC [ethod: TOC WASTE WATER Filename: 12131415 .al. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 19:29 ►perator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 12131415 Zal. Curve: TOC WW CURVE 093005 Timestamp: Baseline Baseline Time 1 25.5030 1.2751 289696 9.856 10.845 111 2 25.8198 1.2910 293226 9.865 10.864 110 3 25.6592 1.2830 291437 9.747 10.732 109 4 ----------------------------------------------------------------------------- 25.7178 1.2859 292090 9.713 10.712 110 ------------------------------------------------------------------------ <<<Statistics>>> Mean: 25.6749 Std Dev: 0.1325 RSD: 0.52 Sample ID: CCB Mode: TOC lethod: TOC WASTE WATER Filename: 12131415 Zal. Curve: TOC WW CURVE 093005 Timestamp: 2005/12/13 19:56 Jperator ID: JASON SAMUEL Sample Type: Sample hep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.3402 0.0170 9342 9.599 9.603 120 2. 0.3547 0.0177 9504 9.585 9.582 120 3 0.3110 0.0156 9017 9.596 9.615 120 4 ----------------------------------------------------------------------------- 0.3198 0.0160 9115 9.604 9.606 120 jast Message: Low Sample Detected :«Statistics>>> Mean: 0.3314 Std Dev: 0.0198 RSD: 5.96 Calibration Report Print Date/Time: 2005/12/14 9:24:14 Cal. Curve ID: TOC WW CURVE 093005 Created: 2005/10/04 17:01 Calibration Factor (m): 2.228e+05 Y rcept (b): 5855 r- -,red: 0.99963 Standard ID Y X Expected Measured . Message Date & Raw Data ug C ug - C Time DI 13148 0.000 0.033 Low Sample De 2005/10/04 14:27 ).5PPM 14616 0.025 0.039 Low Sample De 2005/10/04 14:49 L.OPPM 18776 0.050 0.058 Low Sample De 2005/10/04 15:11 5.OPPM 57013 0.250 0.230 2005/10/04 15:33 10.OPPM 111868 0.500 0.476 2005/10/04 15:54 25.OPPM 284040 1.250 1.248 2005/10/04 16:16 iO.OPPM 553794 2.500 2.459 2005/10/04 16:38 75.OPPM 848670 3.750 3.782 2005/10/04 17:00 U2M UAUS, INC. SDG NO.: SCAN: W This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Sign,, ReviE