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HomeMy WebLinkAboutSample Data Summary Package 12/2005I Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL004 Water Samples Received: 12/8/05 cennpi F n®TA SUMMARY PACKAGE 1/4 VAUS4�� I Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. SU40 11747 u2M "uss INC. TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 12/8/05 SDG NO.: TSI -004 1. NYS DEC SUMMARY FORMS 2. CHAIN OF CUSTODY DOCUMENTATION 3. SDG NARRATIVES 4. SAMPLE REPORTS 4.1 METALS 4.2 WET CHEMISTRY 5. DUPLICATE SUMMARY RESULTS 5.1 METALS 5.2 WET CHEMISTRY 6. SPIKE SAMPLE RESULTS 6.1 METALS 6.2 WET CHEMISTRY 7. BLANK SUMMARY DATA AND RESULTS 7.1 METALS 7.2 WET CHEMISTRY cn d- 0 0 r� E-{ U2M I AUS, INC. 1. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY SDG: TSL004 Anal ical Requirements M Cn 'd - O O CLP on -C Please indicate year of protocol) AS P 13 to iqs' Cj TCUTAL, HSL, Priority Pollutant, h Customer Sample Code Laboratory Sample Code ME we MW -ID _ 0512218-001 X X MW -1s 0512218-002 X X MW -3D _ 0512218-003 X X MW -3S 0512218-004 X X MW -4D _ 0512218-005 X X MW -4S 0512218-006 X X MW -5D 0512218-007 X X MW -5S 0512218-008 X X MW -6D 0512218-009 X X MW -6S 0512218-010 X X MW -8D 0512218-011 X X MW -8S 0512218-012 X X IEQPT BLANK 0512218-013 X X M Cn 'd - O O CLP on -C Please indicate year of protocol) AS P 13 to iqs' Cj TCUTAL, HSL, Priority Pollutant, h NEW YORK STATE DEPARTMENT OF EN% .. _JNMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG. TSI -004 INORGANIC ANALYSIS LaboratoryDateRecd Samp ID Client Sample ID Matrix Metals Requested I Date at Lab Analyzed 0512218-001 MW -1D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-002 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-003 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-004 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-005 MW -4D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-006 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-006DUP MW-4SD WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-006MS MW-4SS WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-007 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-008 MW -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-009 MW -6D WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-010 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-011 MW -81) WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-012 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 0512218-013 JEQPT BLANK WATER CA,CD,FE,K,MG,MN,NA,PB, 08 -Dec -05 12/05 TSL004 S4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG TSL004 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Tests DateRecd at Lab Date Analyze 0512218-001 MW -1D Groundwater i SELECT WET CHEMISTRY *' 12/08/05 12/05 0512218-002 MW -1S Groundwater SELECT WET CHEMISTRY'* 12/08/05 12/05 0512218-003 MW -3D Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-004 MW -3S Groundwater SELECT WET CHEMISTRY ** 12/08/05 12/05 0512218-005 MW -4D Groundwater SELECT WET CHEMISTRY ** 12/08/05 12/05 0512218-006 MW -4S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-006DUP MW-4SDUP Groundwater SELECT WET CHEMISTRY *' 12/08/05 12/05 0512218-006MS MW-4SMS Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-007 MW -513 Groundwater SELECT WET CHEMISTRY *' 12/08/05 12/05 0512218-008 MW -5S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-009 MW -6D Groundwater SELECT WET CHEMISTRY *' 12/08/05 12/05 0512218-010 MW -6S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-011 MW -813 Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-012 I MW -8S Groundwater SELECT WET CHEMISTRY" 12/08/05 12/05 0512218-013 IEQPTBLANK Blank SELECT WET CHEMISTRY ** 12/08/05 12/05 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand ; Chloride ; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable; Sulfate; Total Dissolved Solids; Total Organic Carbon ; O O F-+ u2M TAUS, INC. 2. CHAIN OF CUSTODY DOCUMENTATION UZ' " TAUS, INC. 575 Brom r.w,.ow Rd, Melville, NY 11747-5076 1233 EXTERNAL CHAIN OF CUSTODY Tel: (516) 694-3040 Fax: (516) 420-8436 PROJECT NAMEMUMBER pftR T 36D &0 f"miy ' ! � 20&V CLIENT: = � s E� —� •� CTS L., * � x � JPhone '- a a ti Q a f 414. 0 o f (� 1 I 1-12M SDG NO• � NOTES: Project Contact: ' �• � C �Ic f3o D! 8� Number: J.56 � x Talk S� /494 SAMPLERS: (signatureyClient yaA DELIVERABLES: 5-70 e Z c V . ANALYSIS REQUESTED TURNAROUND TIME:J IR a,�YS ORGANIC INORG. DATE TIME MATRIXFIELD I.D. U11 }. ;� $ � Z U LAB I.D. NO. REMARKS: 11 8nin V4 V4 MW - I S 934 M W - /030 MIN- -32 1100 M W - 3D / MW -- 4S C, M5/ MSD MW- L40 $ a 1 1 ECLE17 SL46K, Relinquished by: (Signature) Date 12 8 Time i� .53 by. StgnetuA at Ti %! I LABORATORY USE ONLY ancies Between Sample Labels and COC Record? Y or N Explain: Samples were: • Shipped_ or Hand Delivered_ Afrbili# 2. Ambient or chilled StmIAr ?QtwS'r tt. IMIZL 3. Received in good conditio : Y or N 4. Property preserved: Y or N S. Samples returned to lab _ Hrs from collection. COC Tape was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y or N 3. COC record present b complete upon sample receipt: YorN Relinquished b . S nq y (Signature) Da Time Repelved by. (Signalu ) e Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by. (Signature) Date Time TU06 6ffPY - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY V"'.� ' L X , _ INC 575 Broad rronow Rd, Melville, NY 11747-5076 1233 EXTERNAL CHAIN OF CUSTODY 1 el: (07 0) 694-3W0 Fax. (516) 420.8436 PROJECT NAMEMUMBER Slaw, - 003 Q CLIENT: OC 8 .5E C Ice �,�' ki I I J 7 .5 J J 1-12M SDG NO. NOTES: Project Contact: w-& 9-k-c�-SD4 C T F «�' t ��S Phone Number: X 4 SAMPLERS: (signature)/Client DELIVERABLES: 1 o z o V �► ANALYSIS RE ESTED TURNAROUND TIME: n OC ORGANIC INORG. DATE TIME MATRI FIELD I.D. - S ca $ 2 r t- 0v LAB I.D. NO.. c5l REMARKS: M, W - 513 12.10 M - 0 /2 W • - 530 MW - SS 4 rT W - �l Relinquished by: (Signmw) Ara Relinquished by: (Signature) Date I1S Die Time c i'1 `�� Time R by: (S tura) R to D a Time ime LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y or N Explain: Samples were: 1 • Shipped_ or Hand Delivered_ Airbili# 2. Ambient or chilled e cJ -R 3. Reoeived in good conditio : Y or N 4. Properly preserved: Y or N (CL 5. Samples returned to lab _ Hrs from collection. COC Tape was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y or N 3. COC record present b complete upon sample receipt: YorN Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) mrnr -yr. a nn Date Time Received by. (Signature) Date Time JL V5MPWCWY - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY 1-12M LABS, INC. Client Name PCTSL Work Order Numbe 0512218 Checklist completed b Matrix c LOO J Sample Receipt Checklist Date and Time Receive 12/8/2005 11:53:00 AM Received by BGL Carrier namd Hand Delivered Reviewed by,�D- Initials ate jj--"--" Shipping container/cooler in good condition? Yes W No ❑ Not Applicable ❑ Custody seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable IV] Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable ❑� Chain of custody present? Yes C No L Chain of custody signed when relinquished and received? Yes No ❑ Chain of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes IV] No L Sample containers intact? Yes No Sufficient sample volume for indicated test? Yes No i._I samples received within holding time? Yes No ❑ Containerfremp Blank temperature in compliance? Yes 0 No ❑ Water - VOA vials have zero headspace? No VOA vials submitted Yes ! !! No Water - pH acceptable upon receipt? Yes No L.J Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section b — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - Client contacted Contacted by: Comments: Date contacted: Regarding Person contacted -Toc- Now C— a{ �i5 -- �©Vnt� A{� M � Corrective Action I " I WAA CAUS9 INC. INTERNAL CHAIN OF CUSTODY CLIENT: DELIVERABLES: TURN AROUND TUBE - SDG k lS L C04 CASE 0.: MATRIX: pH I V N REMARKS: METALS =map-, MEVL"al immommm immsomm LIM, WMEOWFA Moo, SLWO M! W q C mm METALS U2A UAUS, INC. CLIENT: _k�6 Li .i SDO METALS D __ — - r--1 r4 C4 CD H INTERNAL CHAIN OF CUSTODY SAiSPLE PURPOSE OF RHLINQDIS D SAMPLE BOTTLE CHANCE OF D TIME rBY' RECEIVED BY TYPE CUSTODY INIT ,$ •` ' SI .rw �` . . �J �i11 Grr.�l� G slow 6t�100 li L- l%'r(, 9imr 1�1 V 031= Simi S{CCc� /Iapl Slml Slmr Slow J 910W .11cm sly 9IC11 3100 SIGw 31OY SICN S1ON SIGN Sial SIGN SIOw SIGN slow SICN SION 9I ON slow slow Slmi SICN SIOw SIGN - Sion SION 9100 Slow glow 91CN S10w SICN Slow SICN SIGN SICN METALS D __ — - r--1 r4 C4 CD H UM tAlBS9 INCe INTERNAL CHAIN OF CUSTODY CLIENf:r- DELIVERABLES TURN AROUND TIME: SDG #: L CASE # _ MATRIX: —(21v— yx ctEc a - RECEIVED BY: SIGNATURE: WET CHEMISTRY s, _. P 0163 INS HIM mmm m J L re "I IS imomm SMIN 11110,1100, HIM I SEIM 11110 IS Eff wimm HIM ISOM 0 HIM lmm EIENIIE imummmom SM. Me, ml on - �IhPll I'm MIN WET CHEMISTRY s, _. P 0163 f a TwlkRNAL CHAIN : OF .CUSTODY WET CHEMISTRY P 0164 "Es INC4 wLIENr: SDG dro q INTERNAL CHAIN OF.CUSTODY WETCtIE-MISTRY COD U2M I AUS, INC. 3. SDG NARRATIVES U2M LAM, INC. For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 12/8/05 SDG#: TSL004 EQPT BLANK MW -5D MW -1D MW -5S MW -1S MW -6D MW -3D MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S MS/MSD Thirteen water samples were received by H2M Labs inc. on 12/8/05 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument. Sample MW -4S was utilized for QC analysis and reporting. ICP serial dilution analysis did not reproduce within acceptance ranges for calcium. Calcium data was reported flagged "E" on forms I and 9. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the fW!q w'g signature. Date Reported: December 30, 2005 o:\qc\naTr2005\tsl\metals\ts]004.doc ****ale************** *** **************** ent Stancampiano President U2M UAUS, INC. For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLE RECEIVED: 12/8/05 SDG#: TSL004 EQPT BLANK MW -5D MW -1D MW -5S MW -IS MW -6D MW -3D MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S MS/MSD Thirteen water samples were received by H2M Labs, Inc. on 12/8/05 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: PARAMETER Alkalinity BOD Bromide Chloride COD Hardness Ammonia METHOD # EPA 310.1 EPA 405.1 EPA 320.1 EPA325.2 EPA 410.4 EPA 130.2 EPA 350.1 PARAMETER Nitrate Phenols Sulfate TDS TKN TOC METHOD # EPA 353.2 EPA420.1 EPA 9038 EPA 160.1 EPA 351.2 EPA 9060 aample MW -4S was utilized for duplicate and spike QC analysis and reporting. Biological oxygen demand (BOD) values for samples MW -3D, MW -4D, MW -6D and MW -6S were calculated using chemical oxygen demand (COD) values. Aliquots utilized for BOD analysis depleted the oxygen content. Results reported as estimated values. Several ammonia values slightly exceeded the total kjeldahl nitrogen (TKN) values. All differences were within ± the CRDL. Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: January 4, 2006 Vincent Stancampiano gc\narr2005\ts1\wet chem\ts1004,doc Vice President U2M LABS, INC. 4. SAMPLE REPORTS 4.1 METALS 4.2 WET CHEMISTRY 00 cn 0 0 H U2M "UV, INCe QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P Lab Name: H2M LABS, INC. Contract: B E EQPT BLANK Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-013 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0 0 P 7439-96-5 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 112 B E P 7439-89-6 Iron 5.8 B P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 5.2 U P 7439-96-5 Manganese 0.40 U P 7440-09-7 Potassium 63.4 B P 7440-23-5 Sodium 354 B P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U2M "US, INC. 575DoadFUDN Road, MEW NY 11747 LABORATORY RESULTS (631)8943W.FAX (631)42M436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-013 Type: Blank Attn To Origin: Client ID. : EQPT BLANK Collected :12/8/2005 Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(sl Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 12/09/200511:50 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 4:00 PM Bromide 0.6 1 mg/L E320.1 12/20/200510:10 AM Chloride < 2.0 1 mg/L E325.2 12/12/2005 5:06 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/200511:18 AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 1212020051:3Q PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/152005 2:06 PM Nitrate as N < 0.10 1 mg/L E353.2 12/132005 5:40 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/200511:30 AM Sulfate < 5.0 1 mg/L SW9038 12/15200512:12 PM Total Dissolved Solids <10 1 mg/L E160.1 12/13200510:51 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12202005 5:44 PM Total Organic Carbon 1.1 1 mg/L SW9060 12/1320051:35 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 13 of 13 Laboratory Manager U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P 7440-70-2 Calcium 626 B E MW -1D Lab Name: H2M LABS, INC. Contract: P 7439-92-1 Lead Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-001 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Potassium 361 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 626 B E P 7439-89-6 Iron 165 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 170 B P 7439-96-5 Manganese 3.3 B P 7440-09-7 Potassium 361 B P 7440-23-5 Sodium 21000 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 N N O O Cn H U2M "US, INC. 575 Broad HIm Road, Mdvile NY 11747 (631)6943010. FAX (631)4208436 NYSDOH ID# 10478 Town of Southold Landfill Attn To Collected :12/8/2005 8:30:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original Cc LABORATORY RESULTS Lab No. : 0512218-001 Client ID. : MW -113 Sample Information... Type: Groundwater Origin: Parameter(sl Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 31.4 1 mg/L E310.1 12/09/2005 10:30 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:15 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:10 AM Chloride 4.0 1 mg/L E325.2 12/12/2005 4:55 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/200511:02 AM Hardness (As CaCO3) 13.0 1 mg/L E130.2 12/20/2005 12:10 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 1:55 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:30 PM Phenolics, Total Recoverable < 5.0 1 ug/L E420.1 12/16/2005 8:00 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 11:44 AM Total Dissolved Solids 59 1 mg/L E160.1 12/13/2005 10:34 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:33 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 5:46 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 1 of 13 ? awo. �h/-AUPC'106J Laboratory Manager M N COOO 0 14 C4 1-4 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 444 B E P 7439-89-6 Iron 78.7 B P 7439-92-1 Lead 1.4 B P 7439-95-4 Magnesium 122 B P 7439-96-5 Manganese 1.8 B P 7440-09-7 Potassium 351 B P 7440-23-5 Sodium 21100 P EPA SAMPLE NO MW -is SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1. U2M "US, INC. 575BroadHJcw Road, Maw W 11747 LABORATORY RESULTS (631)694.-040.FAX(631)42084W NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-002 Type: Groundwater y Attn To Origin: Collected :12/8/2005 8:00:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Client ID. : MW -1S Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 30.6 1 mg/L E310.1 12/09/200510:35 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:20 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:15 AM Chloride 4.7 1 mg/L E325.2 12/12/2005 4:56 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/200511:03 AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/20/2005 12:15 PM Nitrogen, Ammonia (As N) 0.12 1 mg/L E350.1 12/15/20051:56 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:30 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/2005 8:15 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 11:46 AM Total Dissolved Solids 65 1 mg/L E160.1 12/13/2005 10:35 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:34 PM Total Organic Carton < 1.0 1 mg/L SW9060 12/12/2005 6:15 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 2 of 13 Laboratory Manager U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 EPA SAMPLE NO MW -3D SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-003 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 988 B E P 7439-89-6 Iron 199 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 1170 B P 7439-96-5 Manganese 4.1 B p 7440-09-7 Potassium 6610 P 7440-23-5 Sodium 23100 P Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: Date Reported: 12/19/05 %-,.UZ M Texture: Artifacts: FORM I - IN ILM04.1 U2M LABS, INC. 575BtaadFtbN Road, Mdvile NY 11747 LABORATORY RESULTS (631)694.30M. FAX (631)4208436 NYSDOH ID# 10178 Sample Information... Town of Southold Landfill Lab No. : 0512218-003 Type: Groundwater Alin To Origin: Client ID.: MW -31) Collected :12/8/2005 11:00:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(sl Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 47.8 1 mg/L E310.1 12/09/2005 10:40 AM Biochemical Oxygen Demand 895 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:20 AM Chloride 13.0 1 mg/L E325.2 12/12/2005 4:57 PM Chemical Oxygen Demand 1280 2 mg/L E410.4 12/21/200511:04 AM Hardness (As CaCO3) 7.0 1 mg/L E130.2 12/20/200512:20 PM Nitrogen, Ammonia (As N) 8.28 10 mg/L E350.1 12/15/2005 3:04 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:31 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/2005 8:30 AM Sulfate 15.2 1 mg/L SW9038 12/15/200511:48 AM Total Dissolved Solids 608 1 mg/L E160.1 12/13/200510:36 AM Nitrogen, Kjeldahl, Total 15.4 20 mg/L E351.2 12/20/2005 5:34 PM Total Organic Carbon 1170 _ 40 mg/L SW9060 12/13/2005 5:05 PM Qualifiers: E - Value above quantitation range D - Results for Dilution DF_ = Dilution Factor Date Reported : 1/4/2006 Page 3 of 13 Laboratory Manager U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 618 B E P 7439-89-6 Iron 171 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 155 B P 7439-96-5 Manganese 2.8 B P 7440-09-7 lPotassium 333 B P 7940-23-5 ISodium 20300 P EPA SAMPLE NO MW -3S SDG No.: TSL004 12/8/2005 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 00 N Cn O O C!� H U2M ILAUS, INC. 575BrcadHcbN Road, Wd le NY 11747 LABORATORY RESULTS (631)aX-3040.FAX (631)420 M NYSDOHID#10478 Sample Information... Town of Southold landfill Lab No.: 0512218-004 Type: Groundwater Attn To Origin: Client ID. : MW -3S Collected :12/8/2005 10:30:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original Cc Parameter(sl Results Qualifier D.F.. Units Method Number Analyzed Alkalinity,, Total (As CaCO3) 29.8 1 mg/L E310.1 12/09/2005 10:45 AM Biochemical Oxygen Demand 8 1 mg/L E405.1 12/08/2005 3:25 PM Bromide 1.0 1 mg/L E320.1 12/20/2005 9:25 AM Chloride 4.0 1 mg/L E325.2 12/12/2005 4:57 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:05 AM Hardness (As CaCO3) . 5.0 1 mg/L E130.2 12/20/2005 12:25 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 1:57 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:32 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/2005 8:45 AM Sulfate < 5,0 1 mg/L SW9038 12/15/2005 11:50 AM Total Dissolved Solids 61 1 mg/L E160.1 12/13/2005 10:37 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:35 PM Total Organic Carbon 9.3 1 mg/L SW9060 12/12/2005 7:15 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 4 of 13 awl'. )h'00�1� Laboratory Manager 01 N coo0 C) U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 1440 B E P 7439-89-6 Iron 222 P 7439-92-1 Lead 1.8 B P 7439-95-4 Magnesium 676 B P 7439-96-5 Manganese 11.6 B P 7440-09-7 Potassium 7630 P 7440-23-5 Sodium 24500 P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date : 12/19/05 EPA SAMPLE NO MW -4D SDG No.: TSL004 0512218-005 12/8/2005 Texture: Artifacts: FORM I - IN ILM04.1 O M Cn d' O O F-+ U2M LAOS, INC. 575 Broad FUDW Road, M*Ile NY 11747 LABORATORY RESULTS (631)6943040.FAX (631)42DMW NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-005'5 Type : Groundwater Attn To Origin: Client ID. : MW41) Collected :12/8/2005 9:50:00 AM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 22.4 1 mg/L E310.1 12/09/2005 10:50 AM Biochemical Oxygen Demand 1203 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:30 AM Chloride 7.0 1 mg/L E325.2 12/12/2005 4:58 PM Chemical Oxygen Demand 17.20 4 mg/L E410.4 12/21/2005 11:06 AM Hardness (As C?CO3) 8.0 1 mg/L E130.2 12/20/2005 12:30 PM Nitrogen, Ammonia (As N) 0.57 1 mg/L E350.1 12/15/20051:58 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:32 PM Phenolics, Total Recoverable 16.0 1 pg/L E420.1 12/16/2005 9:00 AM Sulfate 10.7 1 mg/L SW9038 12/15/2005 11:52 AM Total Dissolved Solids 543 1 mg/L E160.1 12/13/2005 10:38 AM Nitrogen, Kjeldahl, Total 5.78 10 mg/L E351.2 12/20/2005 6:01 PM Total Organic Carbon 454 40 mg/L SW9060 12/13/2005 5:33 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 5 of 13 Laboratory Manager U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS -DATA SHEET 0.58 BI P 7440-70-2 Calcium 1320 B • E MW -4S Lab Name: H2M LABS, INC. Contract: 1 P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-006 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 P 7440-09-7 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.58 BI P 7440-70-2 Calcium 1320 B • E P 7439-89-6 Iron 190 1 P 7439-92-1 Lead 2.3 BI P 7439-95-4 Magnesium 601 BI P 7439-96-5 Manganese 10.4 B P 7440-09-7 Potassium 6600 P 7440-23-5 Sodium 23100 P Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: Date Reported: 12/19/05 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U2M LAUso INC. 575BMadHcbw Road, MEW NY 11747 LABORATORY RESULTS (631)694.3040. FAX(631)4208436 WSDOH ID# 10478 Town of Southold Landfill Lab No. : 0512218-006 Attn To Collected :12/8/2005 9:15:00 AM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC Parameters) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Client ID.: MW4S Sample Information... Type : Groundwater Origin: Results Qualifier D.F. Units Method Number Analyzed 37.2 1 mg/L E310.1 12/09/200510:55 AM 22 1 mg/L E405.1 12/08/2005 3:30 PM 1.1 1 mg/L E320.1 12/20/2005 9:35 AM 6.9 1 mg/L E325.2 12/12/2005 4:59 PM 1540 4 mg/L E410.4 12/21/2005 11:07 AM 14.0 1 mg/L E130.2 12/20/2005 12:35 PM 1.03 1 mg/L E350.1 12/15/20051:59 PM < 0.10 1 mg(L E353.2 12/14/200512:31 PM 24.0 1 Ng/L E420.1 12/16/2005 9:15 AM 12.2 1 mg/L SW9038 12115/200511:54 AM 464 1 mg/L E160.1 12/13/2005 10:40 AM 54.8 50 mg/L E351.2 12/20/2005 6:02 PM < 1.0 1 mg/L SW9060 12/13/2005 6:03 PM Page 6 of 13 Laboratory Manager U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. Matrix (soil/water): WATER Level (low/med): LOW % Solids: 0.0 EPA SAMPLE NO MW -5D SAS No.: SDG No.: TSL004 Lab Sample ID: 0512218-007 Date Received: 12/8/2005 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 740 B E P 7439-89-6 Iron 241 P 7439-92-1 Lead 1.3 U1 P 7439-95-4 Magnesium 187 B P 7439-96-5 Manganese 3.2 B P 7440-09-7 Potassium 360 B P 7440-23-5 Sodium 21300 P Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: Date Reported: 12/19/05 I.LGHIC Texture: Artifacts: FORM I - IN ILM04.1 1-12M tAUS, INC. 5758madHdw Road, M*Ile NY 11747 LABORATORY RESULTS (631)694.040. FAX (631)4205436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-007 Type: Groundwater Attn To Origin: Client ID.: MW -5D Collected :12!1/2005 11:30:00 AM Received :1218/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 29.8 1 mg/L E310.1 12/09/2005 11:20 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:40 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:40 AM Chloride 4.6 1 mg/L E325.2 12/12/2005 5:02 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:10 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/200512:50 PM Nitrogen, Ammonia (As N) 0.13 1 mg/L E350.1 12/15/2005 2:01 PM Nitrate as N 0.30 1 mg/L E353.2 12/13/2005 5:35 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/200510:00 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:00 PM Total Dissolved Solids 73 1 mg/L E160.1 12/13/2005 10:45 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:39 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 9:40 PM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 7 of 13 Laboratory Manager U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: MW -5S Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-008 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U1 P 7440-70-2 Calcium 752 B E P 7439-89-6 Iron 239 P 7439-92-1 Lead 1.4 B P 7439-95-4 Magnesium 187 B P 7439-96-5 Manganese 3.2 B P 7440-09-7 Potassium 362 B P 7440-23-5 Sodium 21200 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 1H2M "US.3 INC. 575BtoadH0lav Road' Mdvie NY 11747 LABORATORY RESULTS (631)fiB43010.FAX (631)42MW NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-008 Type : Groundwater Atin To Origin: Client ID.: MW -5S Collected :12/7/200511:00:00 AM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 31.0 1 mg/L E310.1 12/09/200511:25 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:45 PM Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:45 AM Chloride 4.4 1 mg/L E325.2 12/12/2005 5:03 PM Chemical Oxygen Demand 112 1 mg/L E410.4 1221/200511:11 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 1220200512:55 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/152005 2:01 PM Nitrate as N < 0.10 1 mg/L E353.2 12/132005 5:36 PM Phenolics, Total Recoverable < 5.0 1 ug/L E420.1 12/16200510:15 AM Sulfate < 5.0 1 mg/L SW9038 12/152005 12:02 PM Total Dissolved Solids 48 1 mg/L E160.1 12/13/2005 10:46 AM Nitrogen, Kjeldahl, Total 0.22 1 mg/L E351.2 1220/2005 5:40 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 10:09 PM Qualifiers: E - Value above quanlitabon range D - Results for Dilution D.F. = Dilution Factor Date Reported : 1/4/2006 Page 8 of 13 Laboratory Manager U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 1 EPA SAMPLE NO U INORGANIC ANALYSIS DATA SHEET Calcium 1160 B E Lab Name: H2M LABS, INC. Contract: 228 MW -6D Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-009 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 1160 B E P 7439-89-6 Iron 228 P 7439-92-1 Lead 1.8 B P 7439-95-4 Magnesium 464 B P 7439-96-5 Manganese 7.8 B P 7440-09-7 Potassium 5390 P 7440-23-5 ISodium 22600 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U2/4 tAUS4 INC. 575BroedM w Road, MdAle W 11747 LABORATORY RESULTS (631)694.9040. FAX (631)420-K% NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-009 Type: Groundwater Attn To : Origin: Client ID. : MW -6D Collected :12/7/200512:40:00 PM Received :12/8/200511:53:00 AM Collected By CLIENT Copies To :Original CC Parameters) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 25.9 1 mg/L E310.1 12/09/2005 11:30 AM Biochemical Oxygen Demand 220 1 mg/L E405.1 12/21/2005 Bromide < 0.5 1 mg/L E320.1 12/20/2005 9:50 AM Chloride 5.9 1 mg/L E325.2 12/12/2005 5:03 PM Chemical Oxygen Demand 314 1 mg/L E410.4 12/21/200511.14 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 12/20/2005 1:10 PM Nitrogen, Ammonia (As N) 0.17 1 mg/L E350.1 12/15/2005 2:03 PM Nitrate as N 0.16 1 mg/L E353.2 12/13/2005 5:38 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/200510:30 AM Sulfate 8.0 1 mg/L SW9038 12/15/2005 12:04 PM Total Dissolved Solids 224 1 mg/L E160.1 12/13/2005 10:47 AM Nitrogen, Kjeldahl, Total 2.64 10 mg/L E351.2 12/20/2005 6:03 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/12/2005 11:37 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 9 of 13 Laboratory Manager M 0 0 1--4 C4 F-4 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P 7440-70-2 Calcium 847 B E MW -6S Lab Name: H2M LABS, INC. Contract: P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-010 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 847 B E P 7439-89-6 Iron 188 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 249 B P 7439-96-5 Manganese 3.9 B P 7440-09-7 Potassium 1600 B P 7440-23-5 Sodium 20900 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 O �t d - O O V) N U2M l Uss INC. 575 Broad Hollow Road, Mel i* NY 11747 LABORATORY RESULTS (631)6943040. FAX(631)42Q8436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-010 Type : Groundwater Attn To : Origin: Client ID. : MW -6S Collected :12!7/2005 12:10:00 PM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total .(As CaCO3) 28.2 1 mg/L E310.1 12/09/2005 11:35 AM Biochemical Oxygen Demand 801 1 mg/L E405.1 12121/2005 Bromide 0.7 1 mg/L E320.1 12/20/2005 9:55 AM Chloride 5.1 1 mg/L E325.2 12/12/2005 5:04 PM Chemical Oxygen Demand 1140 2 mg/L E410.4 12/21/200511:15 AM Hardness (As CaCO3) 6.0 1 mg/L E130.2 1220/20051:15 PM Nitrogen, Ammonia (As N) 0.44 1 mg/L E350.1 12/152005 2:04 PM Nitrate as N 0.21 1 mg/L E353.2 12/132005 5:38 PM Phenolics, Total Recoverable 9.1 1 pg/L E420.1 12/162005 10:45 AM Sulfate 5.6 1 mg/L SW9038 12/15200512:06 PM Total Dissolved Solids 150 1 mg/L E160.1 12/13200510:48 AM Nitrogen, Kjeldahl, Total 8.74 20 mg/L E351.2 12/20/2005 6:04 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/132005 12:03 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 10 of 13 Laboratory Manager U.S. EPA CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P Lab Name: H2M LABS, INC. Contract: B E MW -8D Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-011 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7940-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 759 B E P 7439-89-6 Iron 242 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 187 B P 7939-96-5 Manganese 3.1 B P 7940-09-7 Potassium 348 B p 7440-23-5 Sodium 20500 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 U2M ILAUS, INC. 575BtoadFUm Road Mdoie W 11747 LABORATORY RESULTS (631)694-3040.FAX (631)42M436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-011 Type: Groundwater Attn To Collected :12!7/2005 2:00:00 PM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Client ID. : MW -8D Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 32.6 1 mg/L E310.1 12/09/200511.40 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/08/2005 3:50 PM Bromide 0.7 1 mg/L E320.1 12/20/200510:00 AM Chloride 4.4 1 mg/L E325.2 12/12/2005 5:05 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/21/2005 11:16 AM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/20/20051:20 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/15/2005 2:05 PM Nitrate as N < 0.10 1 mg/L E353.2 12/13/2005 5:39 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 12/16/2005 11:00 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:08 PM Total Dissolved Solids 65 1 mg/L E160.1 12/13/200510:49 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:42 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/200512:36 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 11 of 13 ? awl'. A /- d&V4^--j Laboratory Manager U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.26 U P 7440-70-2 Calcium 740 B E MW -8S Lab Name: H2M LABS, INC. Contract: P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL004 Matrix (soil/water): WATER Lab Sample ID: 0512218-012 Level (low/med): LOW Date Received: 12/8/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.26 U P 7440-70-2 Calcium 740 B E P 7439-89-6 Iron 294 P 7439-92-1 Lead 1.3 U P 7439-95-4 Magnesium 183 B P 7439-96-5 Manganese 3.0 B P 7440-09-7 Potassium 336 B P 7440-23-5 Sodium 20800 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 12/19/05 FORM I - IN ILM04.1 d' Cn It O O v] F-+ 1-12M tAJUS, INC. 575BroedRADN Road' MdAle W 11747 LABORATORY RESULTS (631)694-3D10. FAX (631)421184.96 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0512218-012 Type : Groundwater Attn To : Origin: Client ID.: MW -8S Collected :12/7/2005 1:30:00 PM Received :12/8/2005 11:53:00 AM Collected By CLIENT Copies To :Original CC Parameterfs) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 29.6 1 mg/L E310.1 12/09200511:45 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/082005 3:55 PM Bromide 0.6 1 mg/L E320.1 12202005 10:05 AM Chloride 4.4 1 mg/L E325.2 12/122005 5:05 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12212005 11:17 AM Hardness (As CaCO3) 5.0 1 mg/L E130.2 122020051:25 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/152005 2:05 PM Nitrate as N < 0.10 1 mg/L E353.2 12/132005 5:40 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/16200511:15 AM Sulfate < 5.0 1 mg/L SW9038 12/15/2005 12:10 PM Total Dissolved Solids 54 1 mg/L E160.1 12/13200510:50 AM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2005 5:43 PM Total Organic Carbon < 1.0 1 mg/L SW9060 12/13/20051:02 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 1/4/2006 Page 12 of 13 Laboratory Manager U2M "US, INC. 5. DUPLICATE SAMPLE RESULTS 5.1 METALS 5.2 WET CHEMISTRY i Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES MW -4S Contract: SAS No.: SDG No.: TSL004 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q M Cadmium 5.0000 0.5800 B 0.2616 U 200.0 P Calcium 5000.0000 1324.0900 B 1492.9500 B 12.0 P Iron 100.0000 189.9200 196.6500 3.5 P Lead 3.0000 2.3099 B 1.8184 B 23.8 P Ma nesium 15000.0000 600.9300 B 639.6200 B 6.2 P Manganese 15.0000 10.3900 B 10.7700 B 3.61 P Potassium 5000.0000 6598.0000 7142.9200 7.9 P Sodium 5000.0000 23086.6800 24932.4500 7.7 P FORM VI - IN ILM04.1 H2M LABS, INC. Date: 27 -Dec -05 MB -120805 MB -120805 Biochemical Oxygen Demand < 2 mg/L LCS-120805 0512218-006bdup QC SUMMARY REPORT SDG: TSL004 mg/L 200 1 < 2 82 1 80 11201 mg/L I I I 1 1 22 4.6 LCS-122005 0512218-006BMS 0512218-006BDUP LCS-122005 MW-4SMS MW-4SDUP Bromide Bromide Bromide 5.4 6.4 0.9 Sample ID: Client Sample ID: Analyte Result Units Spike Amount Sample Recovery RPDRei %RPD Result %REC Limits Value %RPD UCL MB -120905 Mia -120905 Alkalinity, Total (As CaCO3) <1 mg/L LCS-120905 LCS-120905 Alkalinity, Total (As CaCO3) 23.8 mg/L 25 < 1 95 80 120 0512218-006bms MW-4SMS Alkalinity, Total (As CaCO3) 60.0 mg/L 25 37.2 91 75 125 mg/L mg/L mg/L 0512218-006bdup MW-4SDUP Alkalinity, Total (As CaCO3) 34.6 mg/L 37.2 7.4 20 MB -120805 MB -120805 Biochemical Oxygen Demand < 2 mg/L LCS-120805 0512218-006bdup LCS-120805 MW-4SDUP Biochemical Oxygen Demand Biochemical Oxygen Demand 164 21 mg/L 200 1 < 2 82 1 80 11201 mg/L I I I 1 1 22 4.6 MB -122005 MS -122005 Bromide < 0.5 mg/L LCS-122005 0512218-006dms 0512218-006ddup LCS-122005 MW-4SMS MW-4SDUP Hardness (As CaCO3) Hardness (As CaCO3) Hardness (As CaCO3) 1030 109 14.0 mg/L 1000 < 5 103 80 120 mg/L 100 14.0 95 75 125 mg/L 14.0 0 20 LCS-122005 0512218-006BMS 0512218-006BDUP LCS-122005 MW-4SMS MW-4SDUP Bromide Bromide Bromide 5.4 6.4 0.9 mg/L mg/L mg/L 5 5 < 0.5 1.1 108 106 80 75 120 125 1.1 20.0 MB -122105 MB -122105 Chemical Oxygen Demand < 10 mg/L LCS-122105 0512218-006cros 0512218-006cdup LCS-122105 MW-4SMS MW-4SDUP Chemical Oxygen Demand Chemical Oxygen Demand Chemical Oxygen Demand 969 5420 1470 mg/L mg/L mg/L 1000 4000 < 10 1540 97 97 80 75 120 125 1540 4.7 MB -121205 MB -121205 Chloride <2 mg/L LCS-121205 0512218-006BMS 0512218-006BDUP LCS-121205 MW-4SMS MW-4SDUP Chloride Chloride Chloride 50.5 34.0 7.3 mg/L mg/L mglL 50 25 < 2 6.9 101 108 80 75 120 125 6.9 4.7 MB -122005 MB -122005 Hardness (As CaCO3) < 5 mglL LCS-122005 0512218-006dms 0512218-006ddup LCS-122005 MW-4SMS MW-4SDUP Hardness (As CaCO3) Hardness (As CaCO3) Hardness (As CaCO3) 1030 109 14.0 mg/L 1000 < 5 103 80 120 mg/L 100 14.0 95 75 125 mg/L 14.0 0 20 1 TSL004 S48 SDG: TSL004 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID- Analyte Result Units Amount Result %REC Limits Value %RPD UCL tb-121405 mb-121405 Nitrate as N < 0.1 mg/L s-121405 Ics-121405 Nitrate as N 1.11 mg/L 1.13 < 0.1 98 80 120 512218-006CMS MW-4SMS Nitrate as N 0.49 mg/L 0.5 < 0.1 98 75 125 512218-006CDUP MW-4SDUP Nitrate as N < 0.1 mg/L < 0.1 2( ib1-121305 mb1-121305 INitrate as N I <0.1 I mg/L s1-121305 Ics1-121305 INItrate as IN 1.11 mg/L 1.13 1 < 0.1 1 98 L80 11201 MB1-15643 MB1-121505 Nitrogen, Ammonia (As N) < 0.1 mg/L MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0,1 mg/L LCS1-15643 LCS1-121505 Nitrogen, Ammonia (As N) 1.16 mg/L 1 < 0.1 116 80 1120 LCS-15643 LCS-121505 Nitrogen, Ammonia (As N) 1.15 mg/L 1 < 0.1 115 80 120 0512218-006CMS MW-4SMS Nitrogen, Ammonia (As N) 5.83mg/L 5 1.03 1 96 75 125 0512218-006CDUP MW-4SDUP INitrogen, Ammonia (As N) 1.03 mg/L 1.03 0 20 mb-15656 mb-122005 Nitrogen, Kjeldahl, Total < 0.1 mg/L Ics-15656 les -122005 Nitrogen, Kjeldahl, Total 4.22 mg/L 4.1 < 0.1 98 80 120 0512218-006cros MW-4SMS Nitrogen, Kjeldahl, Total 59.5 mg/L 4.1 54.8 114 75 125 0512218-006cdup MW-4SDUP Nitrogen, Kjeldahl, Total 53.4 mg/L 54.8 2.6 20 MB -121605 MB -121605 Phenolics, Total Recoverable < 5 ug/L LCS-121605 LCS-121605 Phenolics, Total Recoverable 28.1 ug/L 30 < 5 94 80 11201 0512218-006CMS MW-4SMS Phenolics, Total Recoverable 43.4 ug/L 20 24.0 97 75 125 0512218-006Cdup MW-4SDUP Phenolics, Total Recoverable 24.8 ug/L 1 1 24.0 3.3 20 MB -121505 MB -121505 Sulfate < 5 mg/l. LCS-121505 LCS-121505 Sulfate 18.4 mg/L 20 < 5 92 80 120 0512218-006BMS MW-4SMS Sulfate 32.0 mg/L 20 12.2 99 75 125 0512218-006Bdup MW-4SDUP Sulfate 12.4 mg/L 12.2 1.6 20 2 TSL004 S49 SDG: TSL004 QC SUMMARY REPORT , Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analvte Result Units Amount Result %REC Limits Value %RPD UCL AB -121305 MB -121305 Total Dissolved Solids <10 mg/L .CS -121305 LCS-121305 Total Dissolved Solids 306 mg/L 300 < 10 102 80 120 512218-006bms MW-4SMS Total Dissolved Solids 693 mg/L 300 464 76 75 125 512218-006bdup MW-4SDUP Total Dissolved Solids 465 mg/L I464 0.22 2( MB -121305 MB -121305 Total Organic Carbon < 1 mg/L LCS-121305 LCS-121305 Total Organic Carbon 26.4 mg/L 25 < 1 106 80 120 0512218-006AMS MW-4SMS Total Organic Carbon 9.0 mg/L 10 < 1 90 75 125 0512218-006ADUP MW-4SDUP Total Organic Carbon < 1 mg/L <1 20 MB -121205 MB -121205 Total Organic Carbon <1 mg/L LCS-121205 ILCS-121205 ITotal Organic Carbon 24.4 mg/L 11 25 1 <I 1 98 80 120 3 TSL004 S50 u2M L us3 INC. 6. SPIKE SAMPLE RESULTS 6.1 METALS 6.2 WET CHEMISTRY Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO MW-4SS SDG No.: TS1,004 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit %R Spiked Sample Result (SSR) C Sample Result (SR) C Spike Added (SA) %R Q M Cadmium 75-125 48.1200 0.5800 B 50.00 95.11p Iron 75-125 1164.5300 189.9200 1000.00 97.5Lead 75-125 22.1529 2.3099 B 20.00 99.2Man anese 75-125 492.7300 10.3900 B 500.00 96.5 Comments: FORM V (Part 1) - IN ILM04.1 H2M LABS, INC. Date: 27 -Dec -05 SDG: TSL004 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID- Analyte Result Units Amount Result %REC Limits Value %RPD UCL 1-120905 MB -120905 Alkalinity, Total (As CaCO3) < 1 mg/L S-120905 LCS-120905 Alkalinity, Total (As CaCO3) 23.8 mg/L 25 < 1 95 80 120 12218-006bms MW-4SMS Alkalinity, Total (As CaCO3) 60.0 mg/L 25 37.2 91 75 125 12218-006bdup MW-4SDUP Alkalinity, Total (As CaCO3) 34.6 mg/L 37.2 7.4 ; MS -120805 MB -120805 Biochemical Oxygen Demand <2 mg/L LCS-120805 LCS-120805 Oxygen Demand 164 mg/L 200 < 2 82 80 120 0512218.006bdup MW-4SDUP �,ioemical cal Oxygen Demand 21 mgn I I 1 1 22 1 4.6 120 MB -122005 MB -1 22105 MB -122005 Bromide < 0.5 myL LCS-122005 LCS-122005 Bromide 5.4 m91L 5 < 0.5 108 80 120 0512218-006BMS 0512218-006BDUP MW-4SMS MW-4SDUP Bromide Bromide 6.4 0.9 mg/L 5 1.1 106 75 125 mg/L 1.1 20.0 20 - 0 MB-122105 MB -122105 Chemical Oxygen Demand ---Z 10 mg/L LCS-122105 LCS-122105 Chemical Oxygen Demand 969 mg/L 1000 <10 97 80 120 0512218-006cros MW-4SMS Chemical Oxygen Demand 5420 mg/L 4000 1540 97 75 125 0512218-006cdup MW4SDUP Chemical Oxygen Demand 1470 mg/L 1540 4.7 20 MB -121205 MB -121205 Chloride < 2 mg/L LCS-121205 LCS-121205 Chloride 50.5 mg/L 50 <2 101 80 11201 0512218-0068MS MW-4SMS Chloride 34.0 mg/L 25 6.9 108 75 125 0512218-006BDUP MW-4SDUP Chloride 7.3 mg/L I 1 1 6.9 4.7 20 MB -122005 MB -122005 Hardness (As CaCO3) < 5 mglL LCS-122005LCS-122005 Hardness (As CaCO3) 1030 mglL 1000 < 5 103 80 120 0512218-006dms 0512218-006ddup MW-4SMS MW-4SDUP Hardness (As CaCO3) Hardness (As CaCO3) 109 14.0 mg/L 100 14.0 95 75 125 mg/L 14.0 0 20 1 TSL004 S53 SDG: TSL004 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID• Analyte Result Units Amount Result %REC Limits Value %RPD UCL ib -1 21405 mb-121405 Nitrate as N < 0.1 mglL - :9-121405 Ica -121405 Nitrate as N 1.11 mg/L 1.13 < 0.1 98 80 120 512218-006CMS MW-4SMS Nitrate as N 0.49 mg/L 0.5 < 0.1 98 75 125 1512218-006CDUP MW-4SDUP Nitrate as N < 0.1 mg/L <0.1 20 mb1-121305 mb1.121305 I Nitrate as N< 0.1 mg/L MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0.1 Ics1-121305 Ics1-121305 Nitrate as N 1.11 13 1 < 0.1 98 80 120 Nitrogen, Ammonia (As N) MBI -15643 MB1-121505 Nitrogen, Ammonia (As N) < 0.1 mg/L MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS1-15643 LCS1-121505 Nitrogen, Ammonia (As N) 1.16 mg/L 1 < 0.1 1 116 80 120 LCS-15643 LCS-121505 Nitrogen, Ammonia (As N) 1.15 mg/L 1 < 0.1 115 80 120 0512218-008CMS MW-4SMS Nitrogen, Ammonia (As N) 5.83 mg/L 5 1.03 96 75 125 0512218-006CDUP MW-4SDUP INItrogen, Ammonia (As N) 1.03 mglL 1.03 0 1201 mb-15656 mb-122005 Nitrogen, Kjeldahl, Total < 0.1 mg/L ics-15656 Ics-122005 Nitrogen, Kjeldahl, Total 4.22 mg/L 4.1 < 0.1 98 80 120 0512218-006cros MW-4SMS Nitrogen, Kjeldahl, Total 59.5 mg/L 4.1 54.8 114 75 125 0512218-006cdup MW-4SDUP Nitrogen, Kjeldahl, Total 53.4 mg/L 54.8 2.6 20 MB -121605 MB -121605 Phenolics, Total Recoverable < 5 ug/L LCS-121605 LCS-121605 Phenolics, Total Recoverable 28.1 ug/L 30 < 5 94 80 120 0512218-006CMS MW-4SMS Phenolics, Total Recoverable 43.4 ug/L 20 24.0 97 75 125 0512218-006Cdup MW-4SDUP Phenolics, Total Recoverable 24.8 ug/L 24.0 3.3 20 MB -121505 MB -121505 Sulfate < 5 mg/L LCS-121505 LCS-121505 Sulfate 18.4 mg/L 20 <5 92 80 120 0512218-006BMS MW-4SMS Sulfate 32.0 mg/L 20 12.2 .99 75 125 0512218-006Bdup MW4SDUP Sulfate 12.4 mg/L 12.2 1.6 20 2 TSL004 S54 QC SUMMARY REPORT SDG: TSL004 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID• Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121305 MS -121305 Total Dissolved Solids <10 mg/L LCS-121305 LCS-121305 Total Dissolved Solids 306 mg/L 300 < 10 102 80 120 0512218-006bms MW-4SMS Total Dissolved Solids 693 mg/L 300 464 76 75 125 0512218-006bdup MW-4SDUP Total Dissolved Solids 465 mg/L 464 0.22 20 MB -121305 MB -121305 Total Organic Carbon < 1 mg/L LCS-121305 LCS-121305 Total Organic Carbon 26.4 mg/L 25 < 1 106 80 120 0512218-006AMS MW-48MS Total Organic Carbon 9.0 mg/L 10 < 1 90 75 125 0512218-006ADUP MW-4SDUP Total Organic Carbon < 1 mg/L < 1 20 MB -121205 MB -121205 ITotal Organic Carbon < 1 mg/L LCS-121205ILCS-121205 ITotal Organic Carbon 1 24.4 mall 1 25 < 1 1 as 180 11201 TSL004 S55 U2M I AUS, INC. 7. BLANK SUMMARY DATA AND RESULTS 7.1 METALS 7.2 WET CHEMISTRY H U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL004 Analyte Initial Calib. Blank (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 C Prepa- ration Blank C M Cadmium 0.3 U 0.3 U 0.3 U 0.3 JU I 0.262,U P Calcium 33.8 B 42.6 B 32.3 B 32.6 B 117.000 B P Iron 4.3 U 6.9 B 4.3 U 4.3 U 27.600 B P Lead 1.3 U 1.3 U 1.3 U 1.3 U 1.290 U P Magnesium 5.2 U 10.5 B 5.2 U 5.2 U 11.500 B P Manganese 0.4 U 0.4 U 0.4 U 0.4 U 0.410 B P Potassium 45.1 B 41.6 B 45.5 B 48.5 B 174.000 B P Sodium 16.8 U 17.4 B 26.1 B 23.1 B 45.900 BI I P FORM III - IN ILM04.1 U.S. EPA - CLP 4 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL004 Analyte Initial Calib. Blank (ug/L) C Continuing Calibration Blank (ug/L) 1 C 2 C 3 Prepa- ration C Blank C M Cadmium 0.3 U P Calcium 51.0 B P Iron 9.6 B P Lead 1.3 U P Magnesium 18.1 B P Manganese 0.4 U P Potassium 48.6 B P Sodium 22.8 B P I FORM III - IN ILM04.1 00 C4 O O C/1 H H2M LABS, INC. SDG: TSL004 Date: 27 -Dec -05 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MS -120905 MB -120905 Alkalinity, Total (As CaCO3) < 1 mg/L LCS-120905 LCS-120905 Alkalinity, Total (As CsCO3) 23.8 mg/L 25 <1 95 80 120 0512218-006bms MW-4SMS Alkalinity, Total (As CaCO3) 60.0 mg/L 25 37.2 91 75 125 0512218-006bdup MW-4SDUP Alkalinity, Total (As CaCO3) 34.6 mg/L 37.2 7.4 20 MB -120805 MB -120805 Biochemical Oxygen Demand < 2 mg/L LCS-120805 LCS-120805 Biochemical Oxygen Demand 164 mg/L 1 200 1 < 2 1 82 180 11201 D512218-006bdup MW-4SDUP Biochemical Oxygen Demand 21 1 mg/L I j I I 1 1 22 4.6 20 MB -122005 MB -122005 Bromide < 0.5 mg/L LCS-122005 LCS-122005 Bromide 5.4 mg/L 5 < 0.5 108 80 120 0512218.006BMS MW-4SMS Bromide 6.4 mg/L 5 1.1 106 75 125 0512218-006BDUP MW-4SDUP Bromide 0.9 mg/L 1.1 20.0 20 MB -122105 MB -122105 Chemical Oxygen Demand <10 mg/L LCS-122105 LCS-122105 Chemical Oxygen Demand 969 mg/L 1000 < 10 97 80 120 0512218-006cros MW-4SMS Chemical Oxygen Demand 5420 mg/L 4000 1540 97 75 125 0512218-006cdup MW-4SDUP Chemical Oxygen Demand 1470 mg/L 1540 4.7 20 MB -121205 MB -121205 Chloride < 2 mg/L LCS-121205 LCS-121205 Chloride 50.5 mg/L 50 < 2 101, 80 120 0512218-006BMS MW4SMS Chloride 34.0 mg/L 25 6.9 108 75 125 0512218-006BDUP MW-4SDUP Chloride 7.3 mg/L 6.9 4.7 20 MS -122005 MB -122005 Hardness (As CaCO3) < 5 mg/L LCS-122005 LCS-122005 Hardness (As CaCO3) 1030 mg/L 1000 < 5 103 80 120 0512218-006dms MW-4SMS Hardness (As CaCO3) 109 mg/l. 100 14.0 95 75 125 0512218-006ddup MW-4SDUP Hardness (As CaCO3) 14.0 mg/L 14.0 0 20 TSL004 S59 QC SUMMARY REPORT SDG: TSL004 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Unita Amount Result %REC Umita Value %RPD UCL mb-121405 mb-121405 Nitrate as N < 0.1 mg/l. Ica -121405 Ics-121405 Nitrate as N 1.11 mg/L 1.13 < 0.1 98 80 120 0512218-MCMS MW-4SMS Nitrate as N 0.49 mg/L 0.5 < 0.1 98 75 125 0512218-MCDUP MW-4SDUP Nitrate as N < 0.1 mg/L < 0.1 20 mb1-121305 mb1.121305 INitrate as N <0.1 I myL Ic31-121305 ICs1-121305 iNitrate as N 1.11 1 mg/L 1 1.13 1 <0.1 1 98 180 11201 MBI -15643 MB1-121505 Nitrogen, Ammonia (As N) < 0.1 mg/L MB -15643 MB -121505 Nitrogen, Ammonia (As N) < 0.1 mg/l. LCS1-15643 LCS1-121505 Nitrogen, Ammonia (As N) 1.16 mg/L 1 < 0.1 116 80 120 LCS-15643 LCS-121505 Nitrogen, Ammonia (As N) 1.15 mg/L 1 < 0.1 115 80 120 9d 051221 B-006CMS MW-4SMS Nitrogen, Ammonia (As N) 5.63 mg/L 5 1.03 96 75 125 0512218-006CDUP MW-4SDUP Nitrogen, Ammonia (As N) i 1.03mg/L 1 1. 1 1 1.03 mb-15656 mb-122005 Nitrogen, Kjeldahl, Total < 0.1 mg/L IC3-15656 Ics-122005 Nitrogen, Kjeldahl, Total 4.22 mg/l. 4.1 < 0.1 98 80 120 0512218-0DSoms MW-46MS Nitrogen, Kjeldahl, Total 59.5 mg/L 4.1 54.8 114 75 125 0512218-006cdup MW-4SDUP Nitrogen, Kjeldahl, Total 53.4 mg/L 54.8 2.6 20 MS -121605 MB -121605 Phenolics, Total Recoverable < 5 ug/L LCS-121605 - LCS-121605 Phenolics, Total Recoverable 28.1 ug/L 30 < 5 94 80 120 0512218406CMS MW4SMS Phenolics, Total Recoverable 43.4 ug/l. 20 24.0 97 75 125 0512218-006Cdup MW4SDUP Phenolics, Total Recoverable 24.8 ug/L 24.0 3.3 20 MB -121505 MS -121505 Sulfate < 5 mg/l. LCS-121505 LCS-121505 Sulfate 18.4 mg/L 20 < 5 92 80 120 0512218-MBMS MW-4SMS Sulfate 32.0 mg/L 20 12.2 99 75 125 0512218-006Bdup MW-4SDUP Sulfate 12.4 mg/L 12.2 1.6 20 TSL004 S60 QC SUMMARY REPORT r SDG: TSL004 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MS -121305 MB -121305 Total Dissolved Solids <10 mg/L LCS-121305 LCS-121305 Total Dissolved Solids 306 mg/L 300 < 10 102 80 120 0512218-006bms MW-4SMS Total Dissolved Solids 693 mg/L 300 464 76 75 125 0512218-006bdup MW-4SDUP Total Dissolved Solids 465 mg/L 464 0.22 20 MB -121305 MB -121305 Total Organic Carbon < 1 mg/L LCS-121305 LCS-121305 Total Organic Carbon 26.4 mg/L 25 < 1 106 80 120 0512218.006AMS MW-4SMS Total Organic Carbon 9.0 mg/L 10 < 1 90 75 125 0512218.006ADUP MW-4SDUP Total Organic Carbon < 1 mg/L < 1 20 MB -121205 MB -121205 Total Organic Carbon< 1 mg/l.LCS-121205 ILCS-121205 ITotal Organic Carbon 24-.41 mWL 1 25 j < 1 1 98 180 11201 TSL004 S61