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HomeMy WebLinkAboutWet Chemistry Data Package 09/2006Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL007 Water Samples Received: 9/13/06 XAII=T rLJF:RfilQTV DATA DArICAr-= 2 2 I -A I-Aus'M I EInvironmental Testing 1-6boratories 575 Broad Hollow Road, Melville, N.Y. N C. 11747 N s H2M LABS, INC. SL U -J+ WET CHEMISTRY TABLE OF CONTENTS 1. SAMPLE REPORTS H. Q.C. SUMMARY I11. RAW DATA rt U2AA "USS INC. 575 Broad Hokw Road, Mme NY 11747 LABORATORY RESULTS (631)694-3040.FAX- (631)420$4W WSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0609809-001 Type: Blank Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 1 of 13 Laboratory Manager Origin: Attn To : George Desmarias Client ID.: EQPT BLANK Collected :9/121200610:00:00 AM Received :9/1312006 4:15:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 09/19/2006 11:15 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 12:10 PM Bromide < 0.5 1 mg/L E320.1 09/29/2006 9:40 AM Chloride < 2.0 1 mg/L E325.2 09/15/2006 3:14 PM Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:02 PM Hardness (As CaCO3) < 100 20 mg/L E130.2 09/20/2006 3:12 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:40 PM Nitrate as N < 0.10 1 mg/L E353.2 09/21/2006 12:20 PM Phenolics, Total Recoverable < 5.0 1 pg1L E420.1 09/20/2006 6:32 AM Sulfate < 5.0 1 mg/L SW9038 09/29/2006 11:04 AM Total Dissolved Solids <10 1 mg/L E160.1 09/18/2006 1:04 PM Nitrogen, Kjeldahl, Total 0.10 1 mg/L E351.2 09/19/2006 10:19 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 1:42 PM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 1 of 13 Laboratory Manager 1-2A4 "US, INC 575 Broad Hcbm Road, Melvilka NY 11747 LABORATORY RESULTS (631) 694.3040, FAX (631)4205436 WSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. 0609809 -*002 Type: Groundwater Origin: Attn To George Desmarias Client ID. MWA D Collected :9/1212006 10:40:00 AM Received :9/13/2006 4:15:00 PM Collected by V003 Copies To :Original cc Parameter(s) Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 25.2 1 mg/L E310.1 09119/2006 111:40 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 12:15 PM Bromide < 0.5 1 mg/L E320.1 09/29/2006 9:45 AM Chloride, 23.9 1 mg/L E325.2, 09/16/2006 3`14 PM Chemical Oxygen Demand I <10 1 mg/L E410.4 09/18/2006 12:03 PM Hardness (As CaCO3) 160 5 mg/L E130.2 09/210/2006 3:14 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:42 PM Nitrate as N 5.42 5 mg/L' E353.2 09/21/2006 12:22 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 09/20/2006 6:33 AM Sulfate 92.0 5 mg/L SW9038 09/29/2006 11:06 AM Total Dissolved Solids 221 1 mg/L E160.1 09/18/2006 1:06 PM " Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 09119/2006 10:20 Am Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 2:13 PM Qualifiers: E -Value, above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported 1019/2006 Page 2 of 13 H2M "USs INC. 575BroadHolow Road, Melville NY 11747 (631)694-30�t0. FAX (631)4205436 NYSDOH ID# 10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 10:10:00 AM Received :9/13/2006 4:15:00 PM Collected -By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-003 Client ID.: MW -1S Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total: (As CaCO3) 10.2 1 mg/L E310.1 09/19/2006 11:45 AM Biochemical Oxygen Demand < 2 1 mg/L E405-1 09/14/2006 12:20 PM Bromide < 0.5 1 mg/L E320.1 09/29/2006 9:50 AM , Chloride 64.4 1 mg/L E325.2 09/15/2006 3:15 PM . Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:04 PM Hardness (As CaCO3) 46.0 2 mg/L E130.2 09/20/2006 3:16 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:43 PM Nitrate as N 4.84 10 mg/L E353.2 09/21/2006 12:23PM Phenolics, Total Recoverable < 5.0 1 - pg/L E420.1 09/20/2006 6:34 AM Sulfate 25.1 1 mg/L SW9038 09/29/2006 11:08 AM Total Dissolved Solids 186 1 rng/L E160.1 09/18/2006 1:08 PM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 09/19/2006 10:22 AM Total Organic Carbon < 1.0 1 mg1L SW9060 10/02/2006 2:44 PM Qualifiers: E - Value above quantitation range D- Results for Dilution D -F. = Dilution Factor Date Reported : 10/9/2006 Page 3 of 13 Laboratory Manager 575 Broad Hollow Road, Mdvile W 11747 LABORATORY RESULTS (631)6943040.FAX-(631)4205436 WSDOHID#10478 Town of Southold Landfill Lab No. : 0609809-004 Attn To : George Desmarias Collected :9/12/2006 11:38:00 AM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon . Client ID.: MW -3D Sample Information... Type : Groundwater Origin: Results Qualifier D.F. Units Method Number Analyzed < 1.0 1 mg/L E310.1 09/19/2006 11:50 AM < 2 1 mg/L E405.1 09/14/2006 12:25 PM < 0.5 1 mg/L E320.1 09/29/2006 9:55 AM 64.4 1 mg/L E325.2 09/15/2006 3:17 PM <10 1 mg/L E410.4 09/18/2006 12:05 PM 46.0 2 mg/L E130.2 09/20/20063:18 PM < 0.10 1 mg/L E350.1 09/26/2006 4:44 PM 5.30 10 mg1L E353.2 09/21/2006 12:24 PM, < 5.0 1 Vg/L E420.1 09/20/2006 6:35 AM 35.3 1 mg/L SW9038 09/29/2006 11:10 AM 199 1 mg/L E160.1 09/18/2006 1:10 PM 0.11 1 mg/L E351.2 09/19/2006 10:23 AM < 1.0 1 mg/L SW9060 10/02/2006 3:16 PM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 4 of 13 Laboratory Manager U2M ""S4. INC. 575 Broad Hollow Road, Melvile NY 11747 LABORATORY RESULTS (631)6943040. FAX -(631)4208436 NYSDOHID#10478 Town of Southold Landfill Lab No. : 0609809-0055 Attn To : George Desmarias Collected :9/12/2006 11:15:00 AM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Alkalinity, Total (As CaCO3) 10.2 Biochemical Oxygen Demand < 2 Bromide 0.6 Chloride 64.9 Chemical Oxygen Demand <10 Hardness (As CaCO3) 52.0 Nitrogen, Ammonia (As N) < 0.10 Nitrate as N 4.83 Phenolics, Total Recoverable < 5.0 Sulfate 24.8 Total Dissolved Solids 185 Nitrogen, Kjeldahl, Total <0.10 Total Organic Carbon < 1.0 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Client ID. I: MW -3S D.F.. Units 1 mg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L 2 mg/L 1 mg/L 10 mg/L 1 pg/L 1 mg/L 1 mg/L 1 mg/L 1 mg/L Page 5 of 13 Sample Information... Type: Groundwater Origin: Method Number E310.1 E405.1 E320.1 E325.2 E410.4 E130.2 E350.1 E353.2 E420.1 SW9038 E160.1 E351.2 SW9060 Analyzed 09/19/2006 11:55 AM 09/14/2006 12:30 PM 09/29/2006 10:00 AM 09/15/2006 3:18 PM 09/18/2006 12:06 PM 09/20/2006 3:20 PM 09/26/20064:45 PM 09/21/2006 12:25 PM 09/20/2006 6:36 AM 09/29/2006 11:12 AM 09/18/2006 1:12 PM 09/19/2006 10:23 AM 10/02/2006 3:47 PM Laboratory Manager 0 l,4 E"i U2M "USS .1sce 575 Broad Hollow Road, Mdrie NY 11747 (631)6943040.FAX (631)42054W NYSDOHID#10478 Town of Southold Landfill Attn To George Desmarias Collected :9/12/2006 2:40:00 PM Received :9113/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-006 Client ID.: MW -4D Sample Information... Type: Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 43.6 1 mg/L E310.1 09/19/2006 12:00 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 12:35 PM Bromide 1.3 1 mg/L E320.1 09/29/2006 10:05 AM Chloride 15.2 1 mg/L E325.2 09/15/2006 3:19 PM Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:07 PM Hardness (As CaCO3) 80.0 4 mg/L E130.2 09/20/2006 3:22 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:47 PM Nitrate as N 2.17 5 mg/L E353.2 09/21/2006 12:27 PM Phenolics, Total Recoverable < 5.0 1 ug/L E420.1 09/20/2006 6:37 AM Sulfate 41.0 2.5 ' mg/L SW9038 09/29/2006 11:14 AM Total Dissolved Solids 164 1 mg/L E160.1 09/18/2006 1:14 PM Nitrogen, Kjeldahl,Total 1.21 10 mg/L E351.2 09/19/2006 10:24 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 4:18 PM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 6 of 13 Laboratory Manager U28t "USs ISC. 575 Broad Hollow Road, Melvile NY 11747 (631) 6943040.FAX (631)4205436 NYSDOH ID# 10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 2:10:00 PM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609$09-007 Client ID.: MW -4S Sample Information... Type: Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 43.6 1 mg/L E310.1 09/19/2006 12:05 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/200612:40 PM Bromide 2.2 1 mg/L E320.1 09/29/2006 10:10 AM Chloride 14.9 1 mg/L E325.2 09/15/2006 3:19 PM Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:08 PM Hardness (As CaCO3) 80.0 4 mg/L E130.2 09/20/2006 3:24 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:48 PM Nitrate as N 2.11 10 mg1L E353.2 09/21120061:14 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 09/20/2006 6:38 AM Sulfate 39.7 1 mg/L SW9038 09/29/2006 11:16 AM Total Dissolved Solids 175 1 mg/L E160.1 09/18/2006 1:16 PM Nitrogen, Kjeldahl, Total 1.56 1 mg/L• E351.2 09/19/2006 10:25 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 4:49 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 7 of 13 Laboratory Manager 575BroWHo1w Road, Melville NY 11747 (631)694MC.FAX (631)420.84W NYSDOHID#10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 12:50:00 PM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-008 Client ID.: MW -51) Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 09/19/2006 12:10 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 12:45 PM Bromide 4.7 1 mg/L E320.1 09/29/2006 10:15 AM Chloride 66.0 1 mg/L E325.2 09/15/2006 3:20 PM Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:09 PM Hardness (As CaCO3) 50.0 5 mg/L E130.2 09/20/2006 3:26 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 - 09/26/2006 4:49 PM Nitrate as N 5.33 10 mg/L E353.2 09/21/2006 12:29 PM Phenolics, Total Recoverable 49.7 1 pg/L E420.1 09/20/2006 6:39 AM Sulfate 43.5 2.5 mg/L SW9038 09/29/2006 11:18 AM Total Dissolved Solids 185 1 mg/L E160.1 09/18/2006 1:18 PM Nitrogen, Kjeldahl, Total 0.12 1 mg/L E351.2 09/19/2006 10:25 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 5:20 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 8 of 13 _ .. Laboratory Manager 0 9) 1-2A* "US. ISC. 5758rwdHdw Road, Marie NY 11747 (631)6943040.FAX(631)420ZW NYSDOHID#10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 12:25:00 PM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-009 Client ID. : MW -5S Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 74.2 2 mg/L E310.1 09/21/2006 10:10 AM Biochemical Oxygen Demand 16 1 mg/L E405.1 09/14/2006 12:50 PM Bromide 0.5 1 mg/L E320.1 09/29/2006 10:20 AM Chloride 29.5 1 mg/L E325.2 09/15/2006 3:28 PM Chemical Oxygen Demand <10 1 mg/L E410.4 09/18/2006 12:10 PM Hardness (As CaCO3) 84.0 4 mg/L E130.2 09/20/2006 3:28 PM Nitrogen, Ammonia (As N) 0.40 1 mg/L E350.1 09/26/2006 4:50 PM Nitrate as N 2.18 5 mg/L E353.2 09/21/2006 12:30 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 09/20/2006 6:40 AM Sulfate 47.5 5 mg/L SW9038 09/29/2006 11:20 AM Total Dissolved Solids 166 1 mg/L E160.1 09/18/2006 1:20 PM Nitrogen, Kjeldahl, Total 1.37 1 mg/L E351.2 09/19/2006 10:26 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 5:51 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor i - Date Reported : 10/9/2006 Page 9 of 13 Laboratory Manager O O O F--1 U2M "US, INC. 575 Broad FUm Road, Mdvile NY 11747 (631)6943040. FAX (631)4208436 NYSDOHID#10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 2:00:00 PM Received :9/1312006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-010 Client ID. : MW -6D Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 62.9 2 mg/L E310.1 09/19/2006 12:20 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 1:00 PM Bromide < 0.5 1 mg/L E320.1 09/29/2006 10:35 AM Chloride 4.4 1 mg/L E325.2 09/15/2006 3:23 PM Chemical Oxygen Demand 11.0 1 mg/L E410.4 09/18/2006 12:13 PM Hardness (As CaCO3) 75.0 5 mg/L El 30.2 09/20/2006 3:34 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:58 PM Nitrate as N 1.58 5 mg/L E353.2 09/21/2006 12:36 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 09/20/2006 6:41 AM Sulfate 13.5 1 mg/L SW9038 09/29/2006 11:26 AM Total Dissolved Solids 116 1 mg/L E160.1 09/18/2006 1:26 PM Nitrogen, Kjeldahl, Total 0.31 1 mg/L E351.2 09/19/2006 10:28 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 8:24 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution factor Date Reported : 10/9/2006 Page 10 of 13 Laboratory Manager F2M "US, INC. 575 Broad Hollow Road, M&k NY 11747 (631)6943040. FAX (631)420-8436 NYSDOH ID# 10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 1:30:00 PM Received :9113/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-011 Client ID. : MW -6S Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 61.5 2 mg/L E310.1 09/19/2006 12:25 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 1:05 PM Bromide < 0.5 1 mg/L E320.1 09/29/2006 10:40 AM Chloride 4.4 1 mg/L E325.2 09/15/2006 3:23 PM Chemical Oxygen Demand 11.0 1 mg/L E410.4 09/18/200612:14 PM Hardness (As CaCO3) 72.0 4 mg/L El 30.2 09/20/20063:36 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 4:59 PM Nitrate as N 1.60 5 mg/L E353.2 09/2112006 12:37 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 09/20/2006 6:42 AM Sulfate 13.1 1 mg/L SW9038 09/29/2006 11:28 AM Total Dissolved Solids 115 1 mg/L El 60.1 09/18/2006 1:28 PM Nitrogen, Kjeldahl, Total 0.54 1 mg/L E351.2 09/19/2006 10:30 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 8:55 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 10/9/2006 Page 11 of 13 1-2M "US, INC. 575 Broad Hollow Road, Melvle W 11747 LABORATORY RESULTS (631)6943040. FAX -(631)42041436 WSDOHID#10478 Town of Southold Landfill Lab No. 0609809-012 Attn To : George Desmadas Collected :9/12/2006 3:30:00 PM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID.: MW -81) Sample Information... Type : Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed 61.4 2 mg/L E310.1 09/19/2006 3:25 PM < 2 1 mg/L E405.1 09/14/2006 1:10 PM 0.6 1 mg/L E320.1 09/29/2006"l 0:45 AM 4.6 1 mg/L E325.2 09/15/2006 3:26 PM 46.2 1 mg/L E410.4 09/18/2006 12:15 PM 76.0 4 mg/L E130.2 09/20/2006 3:38 PM < 0.10 1 mg/L E350.1 09/26/2006 5:00 PM 1.69 5 mg/L E353.2 09/21/2006 12:39 PM < 5.0 1 ug/L E420.1 09/20/2006 6:43 AM 12-4 1 mg/L SW9038 09/29/2006 11:30 AM 111 1 mg/L E160.1 09/18/2006 1:30 PM 0.32 1 mg/L E351.2 09/19/2006 10:31 AM < 1.0 1 mg/L SW9060 10/02/2006 9:26 PM Qualifiers: E -Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 12 of 13 Laboratory Manager M 0 l.4 t12M "US, INC. 575 Broad Hofow Road, Md✓7e NY 11747 (631) 6943040. FAX(631)4208436 NYSDOHID#10478 Town of Southold Landfill Attn To : George Desmarias Collected :9/12/2006 3:10:00 PM Received :9/13/2006 4:15:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0609809-013 Client ID.: MW -8S Sample Information... Type : Groundwater _ Origin: Parameter(s) Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 42.8 2 mg/L E310.1 09/19/2006 4:25 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 09/14/2006 1:15 PM Bromide < 0.5 1 mg/L E320.1 09/29/200610:50 AM Chloride 4.6 1 mg/L E325.2 09/15/2006 3:26 PM Chemical Oxygen Demand 46.2 1 mg/L E410.4 09/18/2006 12:16 PM Hardness (As CaCO3) 72.0 4 mg/L E130.2 09/20/2006 3:40 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 09/26/2006 5:01 PM Nitrate as N 1.65 1 mg1L E353.2 09/21/2006 12:40 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 09/20/2006 6:44 AM Sulfate 30.5 1 mg/L SW9038 09/29/2006 11:32 AM Total Dissolved Solids 129 1 mg/L El 60.1 09/18/2006 1:32 PM Nitrogen, Kjeldahl, Total 0.36 1 mg/L E3512 09/19/2006 10:31 AM Total Organic Carbon < 1.0 1 mg/L SW9060 10/02/2006 9:54 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 10/9/2006 Page 13 of 13 _... Laboratory Manager H2M LABS, INC. Q.C. SUMMARY H2M LABS, INC. Date: 03 -Oct 06 QC SUMMARY REPORT SDG: TSL007 Spike Sample Recovery RPDRef %RPD Sam le ID. Client Sample ID: Analyte -Result Units Amount Result %REC Limits Value %RPD UCL MB -092106 MB-092106Alkalinity, Total (As CaCO3) <1 I mg/L LCS-092106 'LCS-092106 !Alkalinity, Total (As CaCO3) 25.2 1 mg/L 25 < 1� 101 180 120 0609809-009dms )MW-5SMS ;Alkalinity, Total (As CaCO3) 124 1 mg/L 50 74.2 100 75 125 i 0609809-009ddup iMW-5SDUP IAlkalinity, Total (As CaCO3) 172.7 i mg/L -- 174.2 ! 2.0 20 MB -091906 MB -091906 IAlkalinity, Total (As CaCO3). ............_ LCS-091906 JLCS 091906 IAlkalinity Total (As CaCO3) 26 6mglL�____......._. ._____.__.__.._. 26.6 ... MB-091406•MB-091406 {Biochemical Oxygen Demand I < 2 mg/L LCS-091406 (LCS-091406 Biochemical Oxygen Demand 167 mg/L 200 < 2 I -84 0609809-009DDUP - !MW-5SDUP (Biochemical Oxygen Demand 118-- mg/L I ( I I l 6 111.8 120 MB -092906 18romide 1 < 0.5 mg/L I CCS -092906 --_ Bromide I-4_7_1 mg/L 5 <0.5 94 80 1201 -- 5.8 mg/L 5 j 0.5 106 75 MW-5SMS 125 P ---- MW-5SDUP -'- _____IBromide Bromide ------------ 0.6 I mglL - - - i-- -� it ---� 0.5 _ 18.2 MB -091806 LCS-091806 0609809-009CMS MB -091806 LCS-091806 MW-5SMS Chemical Oxygen Demand Chemical Oxygen Demand Chemical Oxygen Demand988 <10 967 mg/L mg/L ( mg/L 1000 ! <10 1000 1 <10 97 I 99 80 120 75 125 ---...---._-......150.... LCS1-091506 ;LCS1-091506 Chloride 1_--- 0609809-009CDUP - -- --- - - - MW-5SDUP - - --_— _---�.-_- Oxygen Chemical Oxen Demand -_.--. < 10 -----'- mg/L -- -- 0609809-009DUP BMW-5SDUP 1— - < 10 -- 20 '-- M61-091506 MB1-091506 Chloride 2 9--__-___.__,___._...._.-... ---...---._-......150.... LCS1-091506 ;LCS1-091506 Chloride - -- 50.3 mg/L 50 <2 101 80 --�- 120 120 -29.5 —1.3" - -20 0609809-009DUP BMW-5SDUP m !L 29.9- 9.__-_.L._--. -- --- __----(Chloride.-__-__--__-_-�- 0609809-009DMS MW-5SMS Chloride _ - _ _. __ .._. ____._....-----..---.--_.f.__ 56.6 mglL ---_-._.. 25 29.5 1.._ 108 75 125 1 TSL007 W16 QC SUMMARY REPORT SDG: TSL007 Spike Sample Recovery RPDRef %RPD Sample IDClient Sample 1D:_ - - Analyte - - Result Units Amount Result %REC Limits Value %RPD UCL MB 92006 MB 92006 Hardness As CaCO3 < 5 g L mg/L I LCS 92006. ...LCS-92006 - iHardness(As-CaCO3)..._..__,._._t.9030 ' - ,µ- - -- lmg1L 1000.1._<5 .._.-103 400 84.0 80 120 ►1 { � i 102 � 75 125 0609809 009Bdup ,MW-5SDUP Hardness (As CaCO3) - -_ 88 0- mglL- _I. 1' 84 0 -,- 4.6 20 1 MB -092106 MB 092106 Nitrate as N < 0,1 mg/L I I LCS-092106 9-009CMS LCS-092106 INitrate as N 1.19 _ _-- _ -L___.__--_ ._ _. _ __._. -- { ._._____--. MW 5SMSNitrate as N 4.66 mg/L - -__ mg/L 1.13 I < 0.1 105 1 80 1120 ___-. _-----_---_ 2.5 i.1 99 75 125 1 j < 0.1 0609809-009CDUP MW 5SDUP Nitrate as N 1 2.18 I mg/L 12.18 I 0 20 I 8403 MB -092606 Nitrogen, Ammonia (As N) i < 0.1 mglL mg/L 20 - < 5 18403 LCS-092606 Nitrogen, Ammonia (As N) { 1.00 { mg/L 1 j < 0.1 100- i 80 120 Phenolics, Total Recoverable 809-009CMS MW IVIS Nitrogen, Ammonia As N 5.91 mg/L 5 0.40 110 75 1125' B09-009CDUP MW-5SDUP �Nitroaen. Ammonia (As N) 0.40 mg/L Phenolics, Total Recoverable } ` 10.40 0 MB -18304 -091906 Nitrogen, Kjeldahl, Total < 0.1 mg/L --._._._........ J.MB .._- -- :-4 --LCS-18304 LCS-091906 Nitrogen, Kjeldahl, Total 3.91 mg/L 41 < 0.0609809-009CMS MW-5SMS Nitrogen, Kjeldahl, Total 5.55. mg/L .1 1.37 102 1 75 1 125 { 0609809-009CDUP MW-5SDUP Nitrogen, Kjeldahl, Total 1.35 mg/L 1.37 1.5 20 1 -092006 �MB-092006 Phenolics, Total Recoverable < 5. ug/L mg/L 20 - < 5 94 ' 80 { 120 - - -- - 7 LCS-092006 LCS 092006 Phenolics, Total Recoverable 28.6 ug/L 30 < 5 95 80 + 120 I 0609809-009Cms MW-5SMS Phenolics, Total Recoverable } 19.4 ug/L 20 < 5 97 75 125 -_-- 47_5- 2.1- 20-I 0609809 P MW-5SDUP 009Cdu - --- - Phenolics, Total Recoverable ---------�- < 5 uglL -- --- -- - -�---) I -- < 5 ?0.. MB -092906 �MB-092906 _...__...___._....._......-_._.. _........ _...___._....__. LCS-092906 (Sulfate _.__._.__-_.__.___.._._.-.-.._._.__........._..__-----------__..._._._.___. LCS-092906 Sulfate < 5 __:__._._...--_-.--. 18.9 - mg/L 20 - < 5 94 ' 80 { 120 - - -- - 7 0609809-009DMS MW-5SMS Sulfate 146 mg/L 100 47.5 98 75 125 0609809-009DDUP MW-5SDUP Sulfate 48.5 mg/L - -- { - -_-- 47_5- 2.1- 20-I IN TSL007 W17 QC SUMMARY REPORT SDG: TSL007 Spike Sample Recovery RPDRef %RPD Sampo -IDs Client Sample I.D AnalvtC _ —.;Result -M-Units Amount Result_%DREG - Limits Value %RPD UCL (MB 091806 MB 091806 Total Dissolved Solids <10 m9IL }T — _.._.. _ LCS-091806 LCS-091806 Total Dissolved Solids 306 mglL 300 < 10 I 102 80 120 I I �— 0609809-009DMS jMW-5SMS Total Dissolved Solids 511 mg/L 300 166 1� 15 —75 1125 - ----- — .. -- ._ ....__..__.. _.1_._._.._._.._ _ -- -- — - -- ---.._ —. ----_ _ _ -- - ----- - -- _ _..._..._ j0609809-009DDUP IMW-5SDUP Total Dissolved Solids 175 �mgiL^ j _ 1166 I 5 3 20 1 100206 MB -100206 Total Organic Carbon < 1. mglL 100206 LCS-100206 ]Total Organic Carbon 24.1 mg/L 25 j < 1 96—j 80 120 3809-009AMS IMW-5SMS jTotal Organic Carbon 9.9 mg/L 10 < 1—j 99 j 75 1251 3809-009ADUP ;MW-5SDUP jTotal Organic Carbon <1 mg/L ( I I !� < 1 _ ( 20 3 TSL007 W 18 H2M LABS, INC. III. RAW DATA CODES FOR MANUAL CORRECTIONS T: Transcription error. CE: Calculation error CC: Changed per client request SC: Sample cancelled LB: Wrong spot in logbook The following codes are specific to chromatography: GC / IC: MS (Match standard): The integration of the continuous calibration or the sample was different from that used for the initial calibration, e.g. more or less of the tail was included. BL (Baseline): Incorrect integration due to changing baseline (rise or fall). NP (Negative peak): Due to a negative displacement in the baseline, wrong areas were integrated, which usually are too high. FP (Fused peak): A contamination is not resolved from the peak that is eluting in the retention time window and is included in the area. Areas are allocated for the two (or more) unresolved peaks in the manual integration. WB (Wrong basepoint): The start or finish of the peak ("basepoint") was put too high or too low, and the basepoint is corrected to match to projected baseline. R (Rider): The peak is riding on a largercontamination, and is reintegrated as a rider. GC -MS: MP: Missed peak MIP: Misintegrated peak WI: Wrong isomer TI: Total of isomers TSL007 W21 TSL007 W22 tV W t 3T TALK 16W c.'*v *'t* -'25"' "If VF 100 9 119120*06-: . . ...... . .......... . 38" A -LK 16� T ".U., 'ag 3—, 4 40 15 P M$ 39- TALK low 0609805�-012d 00, PM 416: 0;24 61 40 ' MV r8 -4-4 . 57 4U` TALK IOW 106,980 0' iY: W, N*'0'6-�.?.!V.,:;.! JZ 4,15 `4 Q.2 -it -4- k, 41 TALK low Iflo- W:�Mngll:,.- W19120. 6' 2-17 Ze,:� j 4i,5 42 �E, vi 43 TALK*IciW 1' 1 V": 25J /I 100 06!a!�,i:ir'!.'�; 91. i 44 :TALK w 9c V8,7 TSL007 W23 TSL007 W24 S� eyl 2 (,i,U O� � �� 1 X'eP ��-3o-Q-7 0 �GGS� t� S5� 19 TALK low ' 0609897 002d 900 9/21/2006 3 78 0 00 0-00 IOW.'. i { �24i X24 00 20 TAL` IC low 05098117 003dr X900 9/21/2006 33'28 0 00 3 29 0 00 0 00 24 347-5 SW h1`'44'43M ' =25:: ; •:;.; 226.50:::: . 21 TALK low 0609817 004d'' 100 9121/2006 6 00 1 86 4 16 ` 0:24 : 16201 ' SW 3 1'1 .7. 12 AM,. 22 TALK� low r! Of60981 `7�b05d' a"b0' 9121 /2006 6 78 >3 1°6 4` 1 T " 0:21 '29:55 �SW4 1:1 53 31 AM 23 TALK low 0609817 006d 50 9121/2006 6 75 3 42 416 0 24` 63.60 SW 5 12 02,11 PM 24 TALK lows' �,060u98'17 0074- �1K00 9/2r1�2006 2 79. 0.00 Zi77 0A0 0 00 4= �x 25 TALK low .r.� .,: ccv tv 25 mg/l 100 9121 /2006 10 01 2. 67 417 ' 0:19 24.80. 99:2 ..1212 26 TgLK how cCb 100' 3%21/20Q6 5 70 W2_0 ,, 9 3 75 4:16 :' 0 26 349 5 598.5'0 '199 6 22 TSL007 W25 354.* 12 s20 i { �24i X24 00 25 331 25" 28 '505 25� 139'2 24 347-5 RPD=: =25:: ; •:;.; 226.50:::: . TSL007 W25 37 TALK K ow ... ­7 25'' 11 8 0 25.25'101 53'.-.00 RPD= 2.08, 3$PM...TOIL 2 70.1 (Y 26 T 39 TALK -low 060984$ oolf 1 _... � 201" 9/2'T/20 :1 t I � 243:25 091206 TS T 40 TALK IoVv 0609848' 10 V Wr T_ 2'87.50V 41 TALK low 06098481,403C 10 9!21/2006 7 06 7 091206 T5,b15,. . . .. ...... - v4 42 TALK 76, 9848-�004f 288 D G ....... .. 4 0609848 006f'; 9!21/2006,_Y ­;.'.::.q...:,_ 6.* .8: 5' -8 , d, . ..... ..... 4 : 2 0 368 00' ss 09 pi 9 0.11 . . ......... . 44 'Al -KI" 0609918AMP 16 00 46, TALKNll 06000OB: 007f S.... EL Aw- .4 4-----w'�_w'.-,�i'.. A .2 I I sal '16W ,`A' 0990 W11,00 8E5 X4 14 0'22 352 00 �T-A titi98 re 4 TALK W!::';` To 587. F .17 ... .. 1 so TSL007 W26 53'.-.00 RPD= 2 70.1 (Y 26 T TSL007 W26 TSL007 W27 e z i o # � v � '` .. �r � • e r�gr e sJ' ° v lv*w 55 TALK low 0609931 001E 5 3721/2006 6 88 2 17 4 17 ` 0:22 -391%.00 ' 08150515 032 5.10 55 PM 56F TALK 1'ow " 060993,1 ©D2f 9/21/2006 8.6 413 _ 0 27 5'V,.'00 S !10 ;6°92' 57 TALK low 0609931 g04f' 1Q0 9%21-72006 5 56 0 2D 4 76.:` 0;98 0.20" ' 091506 TS 035 5 28 49 FM _: . 58 TALK`tow ccu tu. 25 tngtl x100, 9 9T 2 70 413 0;20 25:05 100.2 ,9/21f/2006 59 TALK IoW ' 100 9127/2006 5 63 0 18 4 14 0:22 z1' Pc 5;4511,. PM ::. TSL007 W27 �`.4► �ii� f�k°i `•ate: a�e4. ` � �,. Imo„: 4.•. ;. U2M LABS, INC. ANALYST: N o� DATE IN: 1 O 2 %6b DATE OUT: qO r� STANDARD DUPLICATE TRUE VALUE SAMPLE#jj� RESULT RESULT % RECOVERY DUPLICATE RPD' / .BOD5 pc(5 X03 WMI'm '1'• • w a 0 1 • 1 • • 1 • ® 1 • • 1 .• �'��r/���ii�l�iii 0 CALIBRATION CHECK: I ' O WINKLIPM -� METER f= `1 mL Qj mL .inn.' a A A, c r• '1•/„ '1'• • SEM • 11 ��� 11:•1 :• 1 .• �'��r/���ii�l�iii pit M� 0 wl�Milj tt`1• 14JLVV / V1 LrV j„] 01/10 7 I �, I U2A to US' INC. BOD ANALYST: ,vw .CALIBRATION CHECK: "" "T"" DATE IN: 9 /'y o � VaNKLER DATE OUT: o METER STANDARD DUPPdATE / TRUE VALUE S LE # f= L ►1 II 1• 1• • 1• �L�� 1• :.1 Chlonne 1• le • I• ®� 1• :e 1 RESULT RESULT % RECOVERY DUPLICATE RPD'. ►1 II 1• 1• • 1• �L�� 1• :.1 Chlonne 1• le • I• ®� 1• :e 1 -- - Chlorine ', '��' le 1• 1• �� le :•1 to _ , r ,t'e, ML ' /11 r s 1e/ '1'e • 1• �� 1e:•/ :•1� �--k F2A FIBS, INC, BODS ANALYST: DATE IN: DATE OUT: STANDARD DUP ATE 5 /Iff TRUE VALUE LE # AVG' BOD RESULT RESULT % RECOVERY DUPLICATE RPD ■ M LAB# 5 /Iff % SAMP. AVG' BOD ■ M MWOM I CALIBRATION. CE WIN M o LAB#,,zo BOD % SAMP. ■ M I CALIBRATION. CE WIN M o LAB#,,zo BOD ■ M �L3 -wl AVG LAB# 0 0 OMOZ-4A BOD NNIM ML "I, Chlorine �L3 -wl AVG LAB# 0 0 OMOZ-4A BOD NNIM ML "I, U2M "ES, INC. BODS ANALYST: DATE IN: DATE OUT: o STANDARD DUPLIC TRUE VALUE SA E # RESULT SULT % RECOVERY DUPLICATE RPD LA&TMfj&jfM BOD r� 1 IJLV V / • • ✓ 1 i Lko S� CALIBRATION CHECK: WINKLER METER f= IN F7fiL = ML i n /' 'OKI IM. r� 1 IJLV V / • • ✓ 1 i Lko S� CALIBRATION CHECK: WINKLER METER f= IN F7fiL = ML i n /' 'OKI IM. y L :'i.fil: ma 1.9::LU�)J h:.�i'}A Um3 U2M "IBS,NC. BODS ANALYST: DATE IN: / DATE OUT: STANDARD 2UPLIeATE TRUE VALUE S LE # RESULT SULT % RECOVERY DUPLICATE RPD 1 JLVV / YY JL M �� 1 CALIBRATION CHECK: IN WIIVKLER METER f= _ -ML f - 7 ••. X .. -,AVG R AVG BOD ■r��,���i ��ii�ii 1 JLVV / YY JL M �� 1 CALIBRATION CHECK: IN WIIVKLER METER f= _ -ML f - 7 ••. X .. -,AVG ■r��,���i ��ii�ii Y 0091 J U2M "US. INC, BODS ANALYST: CALIBRATION CHECK: IN DATE IN: O WINKLER DATE OUT: METER STANDARD DUP ATE TRUE VALUE S LE # RESULT RESULT % RECOVERY DUPLICATE RPD IV Chlorine M91L . :.. f�iiilfiiill 1 • / • . 1 . �. 1 . :. 1 �iiiiii� 1 • 1 • • 1 . ► 1 • :. 1 TSLUU"/ WJJ .f = mL = ML ,1,. 1. . I• �� �iiiiii� 1 • 1 • • 1 . ► 1 • :. 1 TSLUU"/ WJJ .f = mL = ML ,1,. 1. . I• �� 1•:.. :.1 .. Chlorine Mg PFA P 0092 PFA P 0092 H2M LABS, INC. BROMIDE DATE: Z. 3 ANALYST: G g A = AMIE- ABS Br (mg/L) =13,320 x A x B_ D x E D= DsAmnE - DsLAxx C F A13LAx2 = 3 -.: mL DBLMK = -4 mL LAB # CLIENT ID MISUSED C & F MLS OF 0.0075N Na2SzO, TITRATED FOR DIFFERENCE G - H RESULT MG/L IODIDE + BR ASAwLE IODIDE DsAwLE ICV 5.0 mg/L _oI -0 0.00035 zs .� I B 31 6 0. aQaa Ob Lo —clov K (il -,� _ 0 "0 - QoaGc s S cj ,� p -000Q100 eo —Coco mw .6 L o _OoUO��s rrw-4S S -8 W p g.S i �.o o q a-.0ab 3 u S. 1 CCV 5.0 mg/L 0 Q u `, Q 0 -dd&u 1 CCB a _� 0 -0000o o -T obo o1^ oorm Z).g o . o oCo b : C Z. _1-� -a poaU12S o -S" . 3. —0(/0h 4. — 012D W4- 34 1. I o....ou3cv e-C,-/� 6. 7 >1. ea 9. 10. CCV 5.0 m i 4p V ,0 G, d0U331.S CB P 0017 b`Author: cmo 1-112M.Labs. Inc. Date : 9/15/2006 Original Run Filename: OM_9-15-2006_02-52-35PM.OMN created 9/15/2006 2:52:35 PM Original Run Author's Signature: [cmo] Current Run Filename: CL091506a.omn last modified 9/15/2006 4:39:33 PM Current Run Author's Signature: [cmo] Description: Default New Run -(�L-gr7 t-tw -3T) MW -3S hw-NC hw-Sig nw_�4 tiv-ic Hui -4k Sample Cup No. Channell Concde m /L Area ADF MDF Vs CalStd 6:ical6:cl dw S1 100.000 20.163 CalStd 5:ical5:cl dw S2 75.000 16.330 CalStd 4:ical4:01 dw S3 50.000 12.360 CalStd 3:ical3:cl dw S4 20.000 5.822 CalStd 2:ical2:cl dw S5 10.000 3.197 CalStd 1:ical1:cl dw S6 2.000 0.773 CalStd O:icalO:cl dw S16 0.000 0.011 CRA:CRA:CL dw 60 1.764 0.637 Known Cone: 2.000 Calibration: Table/Fig. 1 LCS1-091506:LCS:CL dw 1 59 50.330 12.277 Known Cone: 50.000 MB1-091506:MBLK:CL dw S16 0.088 0.044 Known Cone: 0.000 "0609845-001A:SAMP:CL DW" 1 12.390 3.908 "0609845-002A:SAMP:CL DW" 2 7.247 2.415 "0609845-005A:SAMP:CL DW" 3 84.127 17.844 "0609845-006A:SAMP:CL DW" 4 10.893 3.488 "0609845-007A:SAMP:CL DW" 5 3.819 1.331 "0609845-008A:SAMP:CL DW" 6 5.040 1.726 "0609845-009A:SAMP:CL DW" 7 4.462 1.540 "0609845-010A:SAMP:CL DW" 8 3.550 , 1.242 "0609850-001A:SAMP:CL DW" 9 10.379 3.341 "0609850-002A:SAMP:CL DW" 10 15.257 4.684 CCV:CCV:CL DW S2 74.691 16.398 Known Cone: 75.000 CCB:CCB:CL DW I S16 0.072 0.038 Known Cone: 0.000 "0609850-002AMS:MS:CL DW" 11 42.912 10.878 "0609850-002ADUP:DUP:CL DW" 12 15.469 4.740 "0609850-003A:SAMP:CL DW" 13 10.135 3.271 "0609851-001A:SAMP:CL DW" 14 3.323 1.166 "0609851-002A:SAMP:CL DW" 15 33.856 9.047 "0609851-003A:SAMP:CL DW" 16 16.697 5.061 "0609851-004A:SAMP:CL DW" 17 24.145 6.892 "0609809-001 D:SAMP:CL W" 18 0.053 0.031 7'0609809-002D:SAMP: CL W" 19 23.916 6.838. "0609809-003D:SAMP:CL W" 20 64.406 14.735 CCV:CCV:CL DW S2 74.418 16.355 Known Cone: 75.000 CCB:CCB:CL DW I S16 0.144 0.064 Known Cone: 0.000 "0609809-004D:SAMP:CL W" 21 64.378 14.730 "0609809-005D:SAMP:CL W" 22 64.907 14.818 "0609809-006D:SAMP:CL W" 23 15.186 4.665 "0609809-007D:SAMP:CL W" 24 14.897 4.588 "0609809-008D:SAMP:CL W" 25 66.031 15.004 "0609809-009D:SAMP:CL W" 26 29.576 8.125 "0609809-009DMS:MS:CL W" 27 29.853 8.186 "0609809-009DDUP:DUP:CL W" 28 29.518 8.112 "0609809-010D:SAMP:CL W" 29 4.433 1.531 "0609809-011 D:SAMP:CL W" 30 4.413 1.525 CCV:CCV:CL DW S2 74.495 16.367 Run: CL091506a -1- rod (?-0 loo`j� 47.v to M ttw-0 Mw-9� 1W -SS qWE vbv9`w5 Author: cmo H2M Labs. Inc. Date : 9/15/2006 Analyte Properties Table for CL091506a.omn Property Known Conc: 75.000 m /L CCB:CCB:CL DW 1 S16 0.098 0.047 Force Through Zero Known Conc: 0.000 None "0609809-012D:SAMP:CL W" 31 4.560 1.572 "0609809-013D:SAMP:CL W" 32 4.563 1.573 "0609884-001A:SAMP:CL W" 33 12.113 3.831 "0609891-001A:SAMP:CL W" 34 107.566 6.265 5.00 'a8609S9,M- 09A:SAMP:CL W" 35 29533 8.116 "9699894-009Ams:ms:CL W" 36 56.557 13.393 "G669894-009Adu :du :CL W" 37 29.922 8.201 CCV:CCV:CL DW S2 74.547 16.376 Known Conc: 75.000 CCB:CCB:CL DW I S16 0.1081 0.051 Known Conc: 0.0001 1 Analyte Properties Table for CL091506a.omn Property Channell chloride Concentration Units m /L Callibration Fit Type Second Order Clear Calibration True Force Through Zero False Calibration Weighting None Auto Dilution Trigger True % of High Standard 100 Quik Chem Method Chemistry Direct/Bipolar Calibration by Height False Inject to Peak Start 7 Peak Base Width 32 Run: CL091506a -2- m! zsNy1���=101�5�c LZ.0 c 0 Ul 0 m d w CD Volts to v o Volts to � c cNr, 01 (D:3 (D O (A (n C 0 N........ .. ... .......... .........._ ..��_.........._... ....; 1.......... -... .......... .............. .... ... ..... ... n a CCV:CCV'CL DW o o 6:ical6:cl dw - coCalStd o _ t�D N -_—._:_._--- O CalStd 5:i6al5:cl dw o nom, "d609850-002AMS:MS:CL_DW" o CalStd 4;ical4;cl_dw .......... CD cn "09850-002ADUP:DUP;CL DW" ....q.... J O C5CD. N0CalSfd'3:ical3:cl_dw m 06 o -I 9850-003A:SAMP:CL_DW" o-CaIStd2:ical2:cl_dw 9' 0609851-001A:SAMP:CL_DW" oa oFCalStd 1:ical1:cl_dw oo n w "0609851-002A:SAMP:CL_DW" oo CalStd O:icalO:cl_dw m_ cn x,'609851-003A:SAMP:CL DW" ... o. o• - 'CRA:CRA:CL dw _ 4 '0609851-004A:SAMP:CL_DW"3 o LCS1-091506:LCS:CL dw r P 'd-69809-001D:SAMP:CL_W" o _!_ W o MB1-091506:MBLK:CL_dw o c to _..._... in cn _ w W" _. 3 ! CD i"0609845-001A:SAMP:CL ca a co N DW" — 0 A "0609809-003D:SAMP:CLW" _ m N3"0609845-002A:SAMP:CL_DW" CCV:CCV:CL_DW . I -" - co B �� .A '0609845-005A:SAMP:CL_D CCB:CC L DW - �. N o "0609845-006A:SAMP:CL DW" __.__._...-. �_ "0609809-004D:SAMP:CL_W" j cD P' -"0609845 -DW" ...._.. "0609809-005D:SAMP:CL_W" o "0609845-008A:SAMP:CL—DW" -_i_. 4 o 11060 09-006D:SAMP:CL_W" 9 "0609845-009A:SAMP:CL-DW" __. m '.060?809-007D:SAMP:CLW" �' "0609845-01OA SAMP:CL_DW" a, 0609809-008D:SAMP:CL_W'o + "0609850-001A:SAMP:CL DW" _ — j co "0 P: cNo 9$09-009D:SAMCL_W" _w w "0609850-002A:SAMP:CL_DW" N o V cn Ow -4 m f� N IV N V � r TSL007 W37 Author: cmo H2M Labs. Inc. Date 9/15/2006 Channel 1: Set 3 of 3 9.535 i a I J a N U JI JI JI JI JI U a E a JI v> > v U U U cv a Q < CLU o a a > (L a o > m api Q Q U Q Q to Q 0)rn U U Co Co to to cn to Q o o p 0 0 o p U O O o Q 0 U p U I _ _ o cD U I u'5.125 a o 0 0 74.495.-big/t-5) o ado CO o 0 74.547-- ng/L > 0 0 0 o m 0 CO m o 56.557ang/L m CO U CO 0 0 0 _ U 29.8529r IUnghp, i m m m o 9.5 g/129.922 mg ' co X33 p r?1 /L 098r4Y+9 0 -/ 21.5 1 g i U U i 0.108 mg/L 0.000-=---- ._ ............... . .._.__.._:f_._. _ ...:_ �. - ------- .--- ..i_..._ ..:_. __. _._... ............ _ -........_....,__.............,. ._._- .. -- ._ .._.._.... ---- 1756.1 Time (s) 2590.3 Table 1: chloride Figure 1: chloride 20.163, Run: CL091506a Area = - 0.001 ' Conc^2 + 0.284 * Conc +.0.254 Conc = 0.110' Area ^2 + 2.748 * Area - 0.032 Correlation Coefficient (r) = 0.99959 No Weighting chloride concentration, mg/L 100.000 -4- Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 1 100.000 1 20.163 2.396 -0.9 9/15/2006 2:54:41 PM 2 75.000 1 16.330 1.996 2.1 9/15/2006 2:55:22 PM 3 50.000 1 12.360 1.550 -0.5 9/15/2006 2:56:04 PM 4 20.000 1 5.822 0.751 -4.1 9/15/2006 2:56:46 PM 5 10.000 1 3.197 0.415 -6.2 9/15/2006 2:57:28 PM 6 2.000 1 0.773 0.099 5.7 9/15/2006 2:58:10 PM 7 0.000 1 0.011 0.002 9/15/2006 2:58:54 PM Figure 1: chloride 20.163, Run: CL091506a Area = - 0.001 ' Conc^2 + 0.284 * Conc +.0.254 Conc = 0.110' Area ^2 + 2.748 * Area - 0.032 Correlation Coefficient (r) = 0.99959 No Weighting chloride concentration, mg/L 100.000 -4- 1H2A4 I-AtSs INC. COD Analyst: A Date: vulp ql)?Id 6 Start time: j1._ a �S�cSu`1 S viol CLIENT SAMPLE ID LAB# MLS USED ABS. DILUTIONS- --'MG/L NOTES ICV (1000 MGn) OJ q-7 qgF ICB AN 2w -4LC (9 00 Geo 3 4 —3h a 2 0 'oo coo 0. oo -qp 6.00S 6, 0 0OF6 0. - 60 z po /-to q 3. ,7rg A G63 CCVA 000 MGA ) 94 7p CCB 2— 0,600 2 -016c 2, Z- /o 0,001 21— c) 23 6.25 $SV AML vq - I —amu �10 - CCV (1000 MG111 0, q 7 ly jCCB 0 b I lH2A4 I-AUSs INC. Analyst COD Date: Start time: Calibration 1212912005 cone abs p, 0 10 2514 *0.025 5p 125 0.06 250 0.109 375 0:958 500 0.209 625 0.263 750 0.303 87,1510.345 1000 0.396 Intercept(b) .11.624 slope (m) 2514 r 0.9992 1100 1000 900 800 ., 700. 600 500 c 400 v 300 200 100 0 -10C COD Calibration 12129/05 Absorbance Page 1 of 1. cont —Linear (cone) . ......... . . . ..... - lH2AA "US, INC. -V,4 -w-0 PL2 HARDNESS 'rst' 00? -7 gyp ju A6 (X7 HARDNESS = B x N x 100,000 A DATE: 47 - ;o ANALYST: TITRANT = O 0 t N CLIENT ID LAB# MLS USED MLS. MG/L I NOTES I (A) TITRATED (B) ICV(l 000 mg/1) 10, 1030 ICB 40 0. o Z- 3. 10 4. s. An QN AM[ Y) 0"(:6 aD 6. 1 TO 4A 8. Q Pr A k- 001 s 6w -o et,9 9. 00)-o 'W - leo 10. M V- C903p 5v �1' 3 CCV(l 000 mg/1) lo b-3 CCB oo O'C2 1. /4 w �fi - ON 5o MW -35 o6Jq52- 3. P V opm- 50 4. A U/- oo-m' 05 6(-3 5. /41 W- 5D 0616 6. w. 00go ply 11W�f 7. -J9 z+ COL 8. 'Dup m(d 60 Woo ao -+5 0116 A5 -+ L CCV(l 000 mg/1) i 0 '22 B [b0 0.0 P 0045 N ........... ....... R 'VS mr4w"o HARDNESS r. DATE: �0,-06 ANALYST: HARDNESS = B x N x 100,000 TITRANT N A CLIENT 11) LAB# MLS USED I (A) MLS. TITRATED (13) MG/L NOTES ICV(l 000 MgA) ICB 1 -42- 3. A LIP 4. S. 6. 7. 8. 9. to. CCV(i 000 mg/1) CCB 0.a 1. 2. 3. 4. S. 6. 7. 8. 9. 10. CCV(l 000 mg/1) CCB P 0046 kyeefAuthor: bnk H2M Labs. Inc. Date : 9/26/2006 Original Run Filename: OM_9-26-2006_04-26-30PM.OMN created 9/26/2006 4:26:30 PM Original Run Author's Signature: [bnk] Current Run Filename: NH3092606.omn last modified 9/26/2006 5:15:12 PM Current Run Author's Signature: [bnk] Description: 10-107-04-1-C fi �G �-7 1 Sample Cup No.Conc. Channell (m /L) Area j ADF (Vs) I MDF j "CalStd7:ical7:nh3 W S1 j 3.000 49.266 False "CalStd6:ical6:nh3 w" S2 1.000 16.514 % of High Standard "CalStd5:ical5:nh3 W I S3 0.500 7.375 "CalStd4:ical4:nh3 W S4 1 0.200 2.9041 1 "CaIStd3:ical3:nh3 W" S5 0.100 1.087 "CalStd2:ical2:nh3 w" S6 1 0.050 0.195 "CalStd1:ical1:nh3 W S8 0.000 -0.000 "CRA:cra:nh3 W S5 0.091 1.071 Known Conc: 0.100 Calibration: Table/Fig. 1 "LCS-18403:LCS:nh3 W 1 60 1.000 16.138 Known Conc: j 1.000 "MB-18403:MBLK:nh3 w" 1 59 0.024 -0.045 Known Conc: 0.000 "0609809-001 C:SAMP:NH3 W" 1 0.028 0.015 "0609809-002C:SAMP:NH3 W" 2 0.027 -0.001 1 "0609809-003C:SAMP:NH3 W" 3 0.007 -0.321 "0609809-004C:SAMP:NH3 W" 4 0.007 -0.328 "0609809-005C:SAMP:NH3 W" 5 -0.001 -0.454 "0609809-006C:SAMP:NH3 W" 6 -0.019 -0.756 "0609809-007C:SAMP:NH3 W" 7 -0.011 -0.633 "0609809-008C:SAMP:NH3 W" 8 0.002 -0.411 "0609809-009C:SAMP:NH3 W" 9 0.401 6.211 "0609809-009CMS:MS:NH3 W" 10 5.910 9.359 10.00 "CCV:CCV:NH3 W" S2 1.015 16.393 Known Conc: 1.000 "CCB:CCB:NH3 W" 1 S8 0.028 0.024 Known Conc: 0.000 "0609809-009CDUP:DUP:NH3 W" 11 0.405 6.274 "0609809-010C:SAMP:NH3 W" 12 0.010 -0.282 "0609809-011C:SAMP:NH3 W" 13 -0.015 -0.686 "0609809-012C:SAMP:NH3 W" 14 -0.004 -0.518 "0609809-013C:SAMP:NH3 W" 15 0.005 -0.355 "0610114-001A:SAMP:NH3 W' 16 0.417 6.473 "0610116-001A:SAMP:NH3 W" 17 0.317 4.818 "0610116-006A:SAMP:NH3 W" 18 0.395 6.116 "CCV:CCV:NH3 W" S2 0.992 16.008 Known Conc: 1.000 "CCB:CCB:NH3 W" S8 0.027 0.000 Known Conc: 0.000 Analyte Properties Table for NH3092606.omn Property Channell NH3 Concentration Units m /L Callibration Fit Type First Order Clear Calibration True Force Through Zero False Calibration Weighting None Auto Dilution Trigger True % of High Standard 100 Run: NH3092606 -1 - Z 2 w o co N Q7 O m TSL007 W45 Volts (n O O N o_ o a 'wo "CalStd7:ical7:nh3_ 0 0 o "CalStd6:ical6:nh3_w" =1 _ o "CaIStd5:ical5:nh3_w"cn r o �7 N "CalStd4:ical4:nh3 w" o "' C) t= 0 3"CaIStd3: ical3: nh 3_W" "CalStd2: ica 12: n h3_w" "CalStdl:ical1;nh3 w" Flo "CRA:cra:nh3 w" s o "LCS-18403:LCS:nh3_w" - o"'MB-18403:MBLK:nh3_w" (3D r nennann nn+�.en�nn.�uo tnn o "0609809-002C:SAMP:NH3_W" io "0609809-003C:SAMP:NH3_W' 0 V o "0609809-004C:SAMP:NH3_W" 0 v o "0609809-005C:SAMP:NH3_W" 0 0 o "0609809-006C:SAMP:NH3_W" 0 o "0609809-007C:SAMP:NH3_W" 0 a "0609809-008C:SAMP:NH3 W" o a "0609809-009C:SAMP:NH3 W" Cil"0609809-009CMS:MS:NH3_W' 0CYI N 3 O 0 N 0 c O cr 7 v C CD to N rn N O 0 cn Author: bnk Channel 1: Set 2 of 2 6.204 5.001- 2 .001- 2 1-112M Labs. Inc. 2.660 --f -- 1593.2 Table 1: NH3 Time (s) Date : 9/26/2006 0.027 mg/L 3083.6 Co' Rep Peak Area (Volt -s) �I � I Detection Date SS 71 z S SS 7 > = SS S c, > M 2 Z I M co S Z Z MI = z I I p = _ I _ I _ a :ED a a z U z z p a n- Z o Z a c4 Q. cn Q U U U U 22 9/26/2006 5:15:00 PM ¢ Qo U UI U o co U U) U U) U_ 0 0 o fU 0.100 _ = o o r N CO 9/26/2006 C° 0.992 mg/L 1.015 mg/L m rn o 0 0 0 m 0 0 0 co 5:15:00 PM 7 U coo 0 0 U o C) 0 0 0 0 9/26/2006 5:15:00 PM co 09 �014059g/Lo rn 0 M 0 ! !Il I 0' g/C m /L f�l� mg 2.660 --f -- 1593.2 Table 1: NH3 Time (s) Date : 9/26/2006 0.027 mg/L 3083.6 Figure 1: NH3 Z M ca m aD CL NH3 concentration, mg/L 3.000 Area = 16.582 * Conc - 0.440 Conc = 0.060 * Area + 0.027 Correlation Coefficient (r) =0.99984 No Weighting Run: NH3092606 - 3 - Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 1 3.000 1 49.266 2.301 0.1 9/26/2006 5:15:00 PM 2 1.000 1 1 16.514 0.778 -2.3 9/26/2006 5:15:00 PM 3 0.500 1 7.375 0.350 6.1 9/26/2006 5:15:00 PM 4 0.200 1 2.904 0.138 -1.0 . 9/26/2006 5:15:00 PM 5 0.100 1 1.087 0.050 10.8 9/26/2006 5:15:00 PM 6 0.050 1 0.195 0.008 49.8 9/26/2006 5:15:00 PM 7 0.000 1 -0.000 0.000 9/26/2006 5:15:00 PM Figure 1: NH3 Z M ca m aD CL NH3 concentration, mg/L 3.000 Area = 16.582 * Conc - 0.440 Conc = 0.060 * Area + 0.027 Correlation Coefficient (r) =0.99984 No Weighting Run: NH3092606 - 3 - 11 Li m IH2A LABS, Isce.. \00 AMMONIA DISTILLATION NAME: DATE: u loo& laoo P 0017 CLIENT ID SAMPLE WEIGHT GRAMS . SAMPLE voLUmE NES FINAL VOLUME IVES —ANALYZED DATE SPIKE LAB NO. cNe -\-oi L —D)SL -SO -01c -011C _013C < o P 0017 ss d I H Author: bnk 1-12M Labs. Inc. Date : 9/2112006 Original Run Filename: OM-9-21-2006_12-07-38PM.OMN created 9/21/2006 12:07:38 PM 'Original Run Author's Signature: [bnk] Current Run Filename: N03092106.omn last modified 9/21/2006 1:20:24 PM Current Run Author's Signature: [bnk] Description: Default New Run Sample Cup No. Channel 2 Nitrate as N Conc. (mg N/L ADF Area s MDF "Cal Std 5:ical5:no3 dw" S1 2.000 23.637 "Cal Std 4:ical4:no3 dw" S2 1.000 11.809 "Cal Std 3:ical3:no3 dw" S3 0.500 5.952 "Cal Std 2:ical2:no3 dw" S4 0.100 1.162 "Cal Std 1:ical1:no3 dw" S5 0.050 0.620 "Cal Std O:icalO:no3 dw" S16 0.000 0.008 "CRa:cra:no3 dw" S4 0.098 1.165 Known Conc: 0.100 Calibration: Table/Fig. 1 "LCS-092106:lcs:no3 dw S6 1.186 14.020 Known Conc: 1.130 "MB-092106:mblk:no3 dw" I S16 0.002 0.036 Known Conc: 0.000 "0609809-001 C:SAMP:NO3 W" 1 0.003 0.045 "0609809-002C:SAMP:NO3 W" 2 5.413 12.799 5.00 "0609809-003C:SAMP:NO3 W" 3 4.836 5.725 10.00 "0609809-004C:SAMP:NO3 W" 4 5.300 6.272 10.00 "0609809-005C:SAMP:NO3 W" 5 4.831 5.719 10.00 "0609809-006C:SAMP:NO3 W" 6 2.171 5.142 5.00 "0609809-007C:SAMP:NO3 W" 7 2.147 25.367 1.00 "0609809-008C:SAMP:NO3 W" 8 5.333 6.312 110.00 "0609809-009C:SAMP:NO3 W" 9 2.173 5.145 5.00 "0609809-009CMS:MS:NO3 W" 10 4.659 11.019 5.00 "CCV:CCV:NO3 W" S2 1.032 12.199 Known Conc: 1.000 "CCB:CCB:NO3 W" I S16 0.003 0.043 Known Conc: 0.000 "0609809-009CDUP:DUP:NO3 W" 11 2.175 5.150 5.00 "0609809-01OC:SAMP:NO3 W" 12 1.577 3.738 5.00 "0609809-011C:SAMP:NO3 W" 13 1.6021 3.7961 5.00 "0609809-012C:SAMP:NO3 W" 14 1.6921 4.0081 5.00 "0609809-013C:SAMP:NO3 W" 15 1.649 19.490 "0609817-001 C`SAMP:NO3 W" 16 0.013 1 0.165 "0609817-002C:SAMP:NO3 W" 17 35.984 8.513 50.00 "0609817-003C:SAMP:NO3 W" 18 36.861 8.720 150.00 "0609817-004C:SAMP:NO3 W" 19 41.212 9.748 50.00 "0609817-005C:SAMP:NO3 W" 20 0.057 0.687 "CCV:CCV:NO3 W" S2 1.028 12.151 ! Known Conc: 1.000 "CCB:CCB:NO3 W" I S16 ! 0.002 0.034 Known Conc: 0.000 "0609817-006C:SAMP:NO3 W" 21 0.019 0.239 "0609817-007C:SAMP:NO3 W" 22 0.023 0.284 "0609817-008C:SAMP:NO3 W" 23 0.103 1.230 "0609817-008CMS:MS:NO3 W" 24 0.604 7.144 "0609817-008CDUP:DUP:NO3 W" ! 25 I 0.102 1.213 "0609817-009C:SAMP:NO3 W" 26 0.104 1.246 "0609817-01OC:SAMP:NO3 W" 27 0.027 0.333 "0609877-001 A:SAM P:NO3 W" 28 ! 1.988 4.710 5.00 "0609877-002A:SAMP:NO3 W" 29 i 6.337 7.497 10.00 "0610067-001A:SAMP:NO3 W" 30 1.528 3.622 5.00 "CCV:CCV:NO3 W" ! S2 ! 1.031 12.188 Known Conc: I 1.000 Run: N03092106 -1- 7 ,?ec r 0,3,4 i t/=D,�i��/� Vcr 1031 Author: bnk H2M Labs. Inc. "CCB:CCB:NO3 W" S16 0.003 0.050 Known Conc: 0.000 Clear Calibration "0610067-002A:SAMP:NO3 W" 31 2.367 5.605 5.00 "0610068-001A:SAMP:NO3 W" 32 0.755 8.929 "0610068-002A:SAMP:NO3 W" 33 5.507 13.023 5.00 "0610084-001A:SAMP:NO3 W" 34 0.037 0.451 "0610084-002A:SAMP:NO3 W" 35 0.543 6.430 "0610085-001A:SAMP:NO3 W" 36 0.054 0.647 "LFB-092106:LFB:NO3 W" 37 0.501 5.934 "LFBD-092106:LFBD:NO3 W" 38 0.502 5.940 "0609809-007C:SAMP:NO3 W" 39 2.107 2.501 10.00 "CCV:CCV:NO3 W" S2 1.013 11.976 Known Conc: 1.000 "CCB:CCB:NO3 W" 1 S16 0.002 0.035 Known Conc: I 0.000 Analyte Properties Table for N03092106.omn Property Channel2 Nitrate as N Concentration Units mg N/L Callibration Fit Type First Order Clear Calibration True Force Throu h Zero False Calibration Weighting None Auto Dilution Trigger True % of High Standard 100 Quik Chem Method 10-107-04-1-C Chemist Direct/Bipolar Calibration by Height False Inject to Peak Start 27 Peak Base Width 50 Run: N03092106 -2- Date : 9/21/2006 Rpt D ;u Z 0 W O 0 rn w p C=) 00 m 0 V NS U7 N O m ry op p -4 CD O N 0)N 0 "CCB:CCB:NO3 W' o - V S 3 S :" O N O rr ^' "Cal Std 5:ical5:no3 dw" o - - o t--,- "0609809-009CDUP:DUP:NO3W' o CD Z o "Cal Std 4:ical4:no3_dw" v w r= "0609809-O1OC:SAMP:NO3_VT o cc P "Cal Std 3:ical3:no3_dw" m ED - —� vQ x '0609809-011C:SAMP:NO3_W' o o P "Cal Std 2:ical2:no3_dw" o wo "0609809-012C:SAMP:NO3_VV o "Cal Std 1;ical1:no3_dw" w - _ _--- - -o --g s "0609809-013C:SAMP:NO3 W' m o• b "Cal Std O:ical0:no3_dw" -- Z cAo o "U�09817-001C3AMP:NO3 W' o o: w-- z "060981] 002C:SAMP:NO3_W' �Z-- o "CRa:cra:no3_dw" coo ? B LCS-092106:lcs:no3_dw" —§' "0609817-003C: SAM P: NO3 W' rn —_ C, MB-092106:mblk:no3_dw" N "0609817-004C:SAMP:NO3 W' N Z 3 B _ o "0609809-001C:SAMP:NO3 W' a m o "0609 17-005C:SAMP:NO3 W" z n w "0609809-002C:SAMP:NO3 W' "CCV:CCV:NO3 W' `n w z "0609809-003C:SAMP:NO3 W" z co "CCB:CqB:NO3_VT N .'pA OD u "0609809-004C:SAMP:NO3 W' Z "0609817=006C:SAMP:NO3_W"0 w o "0609809-005C:SAMP:NO3 W' _ - "0609817-007C:SAMP:NO3_W'� _ w ,, • 0609809-006C:SAMP:NO3 W' "0609817-008C:SAMP:NO3_W° w �- B; I" 110609809-007C:SAMP;NO3_ o "0609817-008CMS:MS:NO3_W' P "0609809-OO8CS AMP:NO3 W' - P "09817-008CDUP:DUP:NO3_W' CD pl"0609809-009C:SAMP:NO3 W' N Zw "0E&817-009C:SAMP:NO3 W' c`O m 110609809-009CMS:MS:NO3 W' _o w c W "0609817-01OC:SAMP:NO3_W' j —� Xo "CCV:CCV:NO3 W' O N m p 3= W w =N f O (p Z O Z TSL007 W50 Author: bnk Channel 2 (No2/No3) : Set 3 of 3 5.257 :82.670 - 1-12M Labs. Inc. Date: 9/2112006 0.000 +} 3062.0 Table 1: Nitrate as N Time (s) 4516.6 Cone. (mg NIL) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual I Detection Date Detection Time 1 2.000 1 23.637 1.871 -0.0 9/21/2006 12:10:00 PM 2 1.000 1 11.809 0.943 0.1 9/21/2006 O 3 0.500 1 5.952 �I -0.6 9/21/2006 12:12:25 PM 1 OII z M _I 0.0931 O Z 4 ¢ 5 MOI Z - �I O MI 9/21/2006 12:14:51 PM O 0.000 O 0.0081 0.001 9/21/2006 1 12:16:06 PM z OZ ► n Q p CL � a CO z z M ¢ Q > CO Q D.. - U �- LL m -r! a Q zz CO o U O r C1 U I o °° O 00 qq ¢ o V ¢_ o N N m p U I lZ n1 CO U U (O O 0 = O 1.101 N O O O O m O P Z rn (0 1.031 �g N/� �g 1.013 NIL m `? o o 0.634 mg L U o 0.75. N/ o CO ®g -1 � o U U 0.39 N&.30 U NIS?� 0.47 L - 0.543 N&.501 � ii'ag NIL 0.211 mg L v 0.03 Np.05 0.002 mg NIL 0.000 +} 3062.0 Table 1: Nitrate as N Time (s) 4516.6 Figure 1: Nitrate as N 23.637, m Y N Q_ 0.0pO Nitrate as N concentration, mg NIL 2.000 Area = 11.812 * Cone + 0.012 Cone 0.085 ' Area - 0.001 Correlation Coefficient (r) = 1.00000 No Weighting Run: N03092106 -4- Cone. (mg NIL) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual I Detection Date Detection Time 1 2.000 1 23.637 1.871 -0.0 9/21/2006 12:10:00 PM 2 1.000 1 11.809 0.943 0.1 9/21/2006 12:11:12 PM 3 0.500 1 5.952 0.475 -0.6 9/21/2006 12:12:25 PM 4 0.100 1 1.1621 0.0931 2.6 9/21/2006 12:13:38 PM 5 0.050 1 0.6201 0.049 -2.9 9/21/2006 12:14:51 PM 6 0.000 1 0.0081 0.001 9/21/2006 1 12:16:06 PM Figure 1: Nitrate as N 23.637, m Y N Q_ 0.0pO Nitrate as N concentration, mg NIL 2.000 Area = 11.812 * Cone + 0.012 Cone 0.085 ' Area - 0.001 Correlation Coefficient (r) = 1.00000 No Weighting Run: N03092106 -4- , 26 . 4l.. "; ' I1 112/4 ILAUS, 1 N C. Phenols Method 420,1 Distillation Date: 9-M-06 Time: 6:3ry PCM, 0,07 - Analyst: 1/1 5il- Date: ' ®' �- Calibration 1-4-06 conc abs 0 0.000 5 0.012 10 0.025 20 0.048 30 0.068 40 0.095 50 0.12 Intercept (b) -0.0069 slope (m) 421.33 r 0.9994 Phenol Calibration 1/4/06 m 50 40 J a� z 30 0 U 20 10 1.33x - 0.0069 0 0.000 0.050 0.100 0.150 Absorbance Paae 1 of 1 £Sm L00"IS,L ♦ conc —Linear (conc} 0 SULFATE pcnlo DATE: 17-z9-19-4 1/100 ANALYST: .1 Vf.f :�CLIENT ID LAB# MLS USED ABS. — MG/L MG (GRAPH =(Gl MG/L NOTES ICV (20.0 mgt) ICB FQPT 060 EEL VOW 00 myl- IV 0-90- -sp P.9 CCV(20.0 mg/L) 0 CCB q(p obv�_poy_ Ov6p 10 Sw 39 sp M- va?P 10 0.1 to 17. y?V-F-- IJ. 0.100 Y7.s- 14. Y6 -s CCV(20.0 mg/L) is, 10.17-0 /9 - CCB 23 f - S, 6P— fq OM gr -65— 11.150 1 Yo tz• -95 is- 0, 5?zL 30. - CCV(20.0 mg/L) CCB 0.000 '0 p _4v 0. ot C? X5.0 J" 0 CCV(20.0 mg/L) 4S- _o.2-�o Ju. CB a3 1 9. Von 00 M14 P -0083 Calibration 8117/06 cone abs 0 0.000 5 0.034 10 0.089 15 0.154 20 0.247 25 0.304 30 0.386 35 0.46 40 0.538 Intercept (b) 2.4695 slope (m) 71.33 torr. Coeff. 0.9962 TSL007 W55 S048/17/06 y = 71.327x + 2.4695 40 30 J E ♦ cone 20 —Linear (cone) c 0 U 10- 0 0.000 0.100 0.200 0.300 0.400 0.500 0.600 Absorbance Page 1 of 1 • oo S OLIDS I SSI Ts Solids(mg/I)= mL Sample TEMP. ANALYST fk.+% HUMIDITY: 72' DATE: C%'��� START: ;DRIED PAN/ SAMPLE DRIED TARRWT G VOL,IWT G WT G vOI ATI LAB # CLIENT ID CRUC. ML WT G WEIGHT G WEIGHT G MGILT (330�' o� )0 0 rOD /o y6 0' 00 Q5 < a S 160 ozep in w- ! p 5� ° AI y 70 IDS q0 /05- -3 .0 ��' 326► -gyp -fin l4� log 11 la 0, 920 0• 3s to a gas, 03 0.a 85 2q� 2 �S P4� O.a17S !7� 2�D 5D (�c fP 1(7 C6?�117 a5 00 0166 1 G6 I _ c►'� nwn � Na �q l� dor �'S'� V M3 �,� TSL007 W56 2. A SOLIDS EDeed W= Tare" ra�tX1000ix1000 (tDpSSI TS Solids(mg/I)= mL.Sample J TEMP. 616WD ANALYST: p� START: HUMIDITY: VOL. VO DATE: TARE SOLID RESULT DRIED IGNITED PAN/ SAMPLE DRIED WT G WT G (MGIL LAB # CLIENT ID CRUC. ML WT G WEIGHT G WEIGHT G MGIL WT G q5 00311 J 3 jt� layo 33 01. 36' o . o 00 a3, �a oloa -6D 5 �8`6Mb. 6 l� �S csl IN r 06, }t.$ 63 o12p f>o'y —013p Ift 00 c d7.3 a 0 ✓� —asp (pp Jo9►08'8 J��.a��� o.���� q . y 3 TSL007 W57 SOLIDS f(Dried Wt.(q) -Tare Wt. (g)1x10001xl000 /1 J /J SSI TS Solids(mgll)= mL Sample ANALYST: /?& DATE: q�9. a START: TEMP. HUMIDITY: LAB # CLIENT ID PAN/ CRUC. SAMPLE ML DRIED WT G TARE WEIGHT G SOLID WEIGHT G RESULT MGlL DRIED WT G IGNITED WT G VOL. WT G VO ILE s.(MG/L) ro6-'37 lk")6q`0 a. O aq 9. q. 3�. l0 OL 6 .0�z - 50 101.31 -1510'7 - loo 1.a7, ao I0�, �`1aa �. 05q( 53 `31,6 )Q3,)30( 0.0 9a a Do 7 :3 03.0 y 1M� _ Iw OC.°t d56 501 R�w�� uo / ps', NiOD;1 0.61)) ) I 3 2 �• 60 1065 f06.SY 6 ouy) LI 65,6 d 60 9 03A P '0 ll= A LU ar, 9�,n � U/ � W U/ w 107 �(��(v 0 037 L (o�,���5 0 OJ►7 3/;P' jos `/6'0 u, s l � 0.0 00 < ) o M TSL007 W58 C' P _3 TSL007 W59 U L...: -j U lu l l l 1 1 Effective immediately, when analyzing any matrix other than potable water for TDS, please take the conductivity of the sample and record it in the last column of the logbook: Please use the following guide for dilutions based on the conductivity, READING ON CONDUCTIVITY METER MLS OF SAMPLE TO USE On.0 up to 200/ on D under 800 10Qmis Over 800 on D/up to 2.09. on -E 50 mis On E from 2.00 to 5.00 25 mis On E from 5.00 to 8,.00 20 MIS An thin piist 8.00 on E to F 10 rnls, On F reading of 20 or higher 5 mis fok 25 or lower 1 nil for -2-5 oi�hi her All potable water samples should be analyzed at 100 mis. For fresh kills total and filtered samples use the same amount of samplevol=e for both sets of samples, 4"9* ( o63as i.+-tt 836645 /�� 4 � �-- / 7 191, Concentration listed after Optical Blank Correction. TSL pe7 TKN Data Preparation dilution factor not applied to results. Peak SampleID SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 1 Primer PRIM 2.97 mg/1 1 1 2.97 9/19/2006 09:57:15 AM tlai_w 2 Drift DRIF 3 mg/I 1 � 9/19/2006 09:57:55 AM tkn_w 3 high HIGH 3.01 mg/I 1 1 _ 3.01 9/19/2006 09:58:35 AM tkn w 4 Low LOW 0.02 mg/I 1 0.02 9/19/2006 09:59:13 AM tkn_w 5 Low LOW 0.02 mg/I I F 0.02 9/19/2006 09:59:57 AM tkn_w 6 Cal. CALB 3.01 mg/I 1 3.01 9/19/2006 10:00:35 AM tkn_w 7 Cal. CALB 0.99 mg/l 1 0.99 9/19/2006 10:01:08 AM tkn_w 8 Cal. CALB 0.48 me 1 0.48 9/19/2006 10:01:50 AM tkn_w 9 Cal. CALB 0.21 mg/1- 1 0.21 9/19/2006 10:02:34 AM tkn_w 10 Cal. CALB 0.11 mg/1 10.11 9/19/2006 10:03:16 AM tkn_w I 1 Cal. CALB 0.01 mg/I 1 A.O1 9/19/2006 10:03:43 AM tkn_w 12 OPTICAL BLK ` QUAL 0.71 mg/1 1 -0.71 9/19/2006 10:04:36 AM tkn_w 13 LCS-18304 1%%N,5I 1- lcs 0.391 mg/1 10 F 3.91 9/19/2006 10:05:10 AM tkn_w 14 MB -18304 mblk 0 mg/I 1 0 9/19/2006 Lp• I 1.0:05:55 AM tkn_w 15 0609331-001GZW41 :-rr3m5 T SAMP 0.12 mg/1 1 0.12 9/19/2006 10:06:35 AM tkn_w 16 0609331-001 GMS'?I� ti- 4i f t ms 0.406 mg/1 10 4.06 9/19/2006 y6 10:07:13 AM tkn_w 17 0609331-OOIGDUP dup 0.1 mg/I 1 0.1 9/19/2006Qp({; 16'/,10:07:54 AM tkn_w 18 0609331-002GZWML:Z-r31o:r t SAMP 0.35 mg/I 1 0.35 9/19/2006 10:08:33 AM tkn_w 19 0609331-0036 Z it=2'r?/o22 SAMP -0.41 mg/1 1 0.41 9/19/2006 10:09:03 AM tkn_w 4,A Yk)' 20 0609331-004GZ--Je%v-x T3rva SAMP 0.11 mg/1 1 0.11 9/19/2006 10:09:56 AM tkn w 21 0609331-005G7Wet%' X3057 SAMP 0 mg/1 1 9/19/2006 10:10:29 AM tkn_w 22 0609385-001G ZtJil �T3612 SAMP 0:04 mg/1 I 0.04 9/19/2006 10:11:14 AM tkn_w 23 0609385-002G?w47-:'1-'T34S? SAMP 0.19 mg/1 1 F 0.19 9/19/2006 10:11:55 AM tkn w 24 0609385-003G 2 52:*'t 311 g 1 SAMP 1.12 mg/1 1 1.12 9/19/2006 10:12:37 AM tkn_w 25 CCV 1.0 ccv 0.96 mg/1 I 0.96 9/I9/2006rt 1, 10:13:16 AM tkn_w 26 CCB ceb 0.03 mg/I 1 0.03 9/19/2006 (,a,f 10:13:42 AM tkn_w 27 0609385-004G2,alS1: 'r3o7+� sAMP 0.87 mg/1 1 0.87 9/19/2006 1.0:14:36 AM tkn w 28 0609385-005G ZwgL! -1-r 311 1) SAMP -0.16 mg/I 1 -0.16 9/19/2006 10:15:17 AM tkn w he � 29 0609385-008GZti51 _T1"3M-VO-tt-SAMP -0.25 mg/I 1 -0.25 9/19/2006 10:15:57 AM tkn_w JU'wk ft? 1` O 30 0609686-002A SAMP 1.241 mg/1 20 24.82 9/19/2006 10:16:37 AM tkn_w )/19/2006 10:54:28 AM Page 1 of 'Peak SamplelD SampT_y Cone Units DF Cone x DF AnalDate AttalTime TestCod 57 LFB-18304 �1/ cl,l (a Ifb 0.43 mg/l 10 4.3 9/19/2006 191.1 10:34:38 AM 31 0609697-001B 231 - U v 1 SAMP 0.4 mg/l 1 �- 4 9/19/2006 10:17:17 AM tkn_w tkn_w 59 CCV 1.0 ccv 0.97 mg/l 1 0.97 9/19/2006cp( 10:35:56 AM 32 0609697-001 BMS '1L_ K,1 A31 L ms 0.406 mg/l 10 4.06, 9/19/2006 �9 �/, 10:17:56 AM tkn_w 33 0609697-OOIBDUP dup 0.38 mg/1 1 0.38 9/19/2006 ON F� 10:18:36 AM tkn_w 34 0609802-001B 2311-1 _ SAMP 0.35 mg/l I F 0.35 9/19/2006 10:19:16 AM tkn_w 35 0609809-001 C /,OM SAMP 0.1 mg/1 10 1 9/19/2006 10:19:56 AM tkn_w 36 0609809-002C M W _ 1 TD SAMP 0 mg/l 1 ( OI 9/19/2006 10:20:36 AM tkn_w 37 CCV 1.0 ccv 0.94 mg/l 1 � 0.94 9/19/2006 7y% 10:21:16 AM tkn_w 38 CCB ccb 0 mg/l 1 � 9/19/20061,04 10:21:57 AM tkn_w 39 0609809-003C K vJ - 1 S SAMP 0.07000 mg11 1 0.070000000 9/19/2006 10:22:36 AM tkn_w 40 0609809-004C "3 SAMP 0.11 mg/l 1 0.11 9/19/2006 10:23:16 AM tkn_w 41 0609809-005C - 3 S SAMP 0.08000 mg/1 1 0.080000000 9/19/2006 10:23:56 AM tkn_w 42 0609809-006C SAMP 0.121 mg/l 10 1.21 9/19/2006 10:24:37 AM tkn_w 43 0609809-007C - K SAMP 1.56 mg/l t 1.56 9/19/2006 10:25:16 AM tkn_w 44 0609809-008C - Sb SAMP 0.12 mg/l 1 0.12 9/19/2006 10:25:56 AM tkn_w 45 0609809-009C - SS SAMP 1.37 rng/l 1 1.37 9/19/2006 10:26:36 AM tkn_w 46 0609809-009CMS `N q.�l�� L ms 0.555 mg/l 10 5.55 9/19/2006 Itt'/, 10:27:10 AM tkn_w 47 0609809-009CDUP dup 1.35 mg/l 1 1.35 9/19/2006 Q.��' �� 10:27:56 AM tkn_w 48 0609809-OIOC SAMP 0.31 mg/l 1 0.31 9/19/2006 10:28:36 AM tkn_w 49 CCV 1.0 ccv 0.96 mg/l 1 0.96 9/19/2006 ` 1*1 10:29:09 AM tkn_w 50 CCB ccb 0.01 mg/l 1 O.OI 9/19/2006 10.1 10:29:57 AM tkn w 51 0609809-011C KVf SAMP 0.54 mg/l 1 0.54 9/19/2006 10:30:36 AM tkn w 52 0609809-012C - $) SAMP 0.32 mg/l 1 0.32 9/19/2006 10:31:16 AM tkn_w 53 0609809-013C SAMP 0.36 mg/l 1 0.36 9/1912006 10:31:56 AM tkn_w 54 0609784-OOIA SAMP 0.794 mg/1 10 7.94 9/19/2006 10:32:36 AM tkn w 55 0609784-002A SAMP 1.922 mg/l 10 19.22 9/19/2006 10:33:16 AM tkn_w 609891 OOIA SAMP 252 mg/l 1 2.52 9/19/2006 10:33:56 AM tkn_w ty1„v p/ 4, (, 9/19/2006 10:54:28 AM Page 2 of 3 57 LFB-18304 �1/ cl,l (a Ifb 0.43 mg/l 10 4.3 9/19/2006 191.1 10:34:38 AM tkn_w 58 LFBD-18304 t / Ifbd 0.418 mg/l 10 4.18 9/19/2006 Pyr 3 *k 10:35:16 AM tkn_w 59 CCV 1.0 ccv 0.97 mg/l 1 0.97 9/19/2006cp( 10:35:56 AM tkn_w 60 CCB ccb 0.03 mgtl 1 0.03 9/19/2006 Ga,{ 10:36:37 AM tkn_w 61 Drift DRIF 3 mg/l 1 33 9/19/2006 10:37:16 AM tkn_w 9/19/2006 10:54:28 AM Page 2 of 3 Peak SampleID 62 End SampTy Conc Units DF Conc x DF AnalDate END 0 mg/l 1 �. 9/19/2006 AnalTime TestCod 10:40:10 AM tkn_w 9/19/2006 10:54:28 AM Page 3 of 3 BRAN+LUEBBE AACE 5.48 H2M Labs Inc. Post -run report Name of Run tkn091906R1 Name of Analysis :TKN,ANL Date of Report 9/19/2006 System No. :1 Date of Run 9/19/2006 Type of System :TRAACS Operator cmo Start/Stop time :09:46 - 10:40 Comment fkit Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/l mg/l Calibr. Fit Linear Corr. Coeff. 0.9999 Base 61 Gain 21 Sensitivity 0.4316 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value Va e 0 0 B Baseline 0.00 0 1 1 P Primer 2.97 1 (� 2 l D Drift 3.00 1 3 1 H1 High 3.01 1 _ 4 0 Ll Low 0.02 1 5 0 L1 Low 0.02 1 6 1 C Cal. 3.01 1 7 2 C Cal. 0.99 1 8 3 C Cal. 0.46 1 9 4 C Cal. 0.21 1 10 5 C Cal. 0.11 1 11 0 C Cal. 0.01 1 12 8 QC1 OPTICAL BLK 0.71 1 13 9 QC1 LCS-18304 4.62 10 14 '10 QC1 MB -18304 0.71 1 15 11 S 0609331-001G 6.83 1 16 12 S 0609331-001GMS 4.77 10 17 13 S 0609331-001GDUP 0.81 1 18 14 S 0609331 -002G 1.06 1 19 15 S 0609331-003G 0.30 1 TKN.ANL / tkn091906R1.run Page 1 Post -run Report BRAN+LUEBBE AACE 5.48 Post -run Report 20 16 S 0609331-004G 0.82 1 21 17 S 0609331-OOSG 0.71 1 22 18 S 0609385-001G 0.75 1 23 19 S 060,9385-002G 0.90 1 24 20 S 0609385-003G 1.83 1 25 2 QC1 CCV 1.0 0.96 1 26 0 QC1 LCB 0.03 1 27 21 S 0609385-004G 1.58 1 28 22 S 0609385-005G 0.55 1 29 23 S 0609385-008G 0.46 1 30 24 S 0609686-002A 25.53 20 31 25 S 0609697-001B 1.11 1 32 26 S 0609697-OOIBMS 4.77 10 33 27 S 0609697-OOIBDUP 1.09 1 ' 34 28 S 0609802-001B 1.06 1 35 29 S 0609809-001C 0.81 1 36 30 S 0609809-002C 0.71 1 37 2 QC1 CCV 1.0 0.94 1 38 0 QC1 CCB 0.00 1 39 31 S 0609809-003C 0.78 1 40 32 S 0609809-004C 0.62 1 41 33 S 0609809-OOSC 0.79 1 42 34 S 0609809-006C 1.92 10 43 '35 S 0609809-007C 2.27 1 44 36 S 0609809-008C 0.83 1 45 37 S 0609809-009C 2.08 1 46 38 S 0609809-009CMS 6.26 10 47 39 S 0609809-009CDUP 2.06 1 48 40 S 0609809-010C 1.02 1 49 2 QC1 CCV 1.0 0.96 1 50 0 QCI CCB 0.01 1 51 41 'S 0609809-011C 1.25 1 52 42 S 0609809-012C 1.03 1 53 43 S 0609809-013C 1.07 1 54 44 S 0609784-OOIA 8.65 10 55 45 S 0609784-002A 19.93 10 56 46 S 0609891-001A 3.23 1 57 47 S LFB-18304 5.01 10 58 48 S LFBD-18304 4.89 10 59 2 _ QC1 CCV 1.0 0.97 1 60 0 QC1 CCB 0.03' 1 61 1 D, Drift 3.00 1 62 0 B FinalBase 0.00 1 QC Limits TKN.ANL / tkn091906RI.run Page 2 BRAN+LUEBBE AACE 5.48 Post -run Report Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel Baseline Drift Carry over ** <END OF REPORT> ** 2 -Yes Yes Yes 1.0 TKN.ANL / tkn091906R1.run Page 3 BRANrLUEBBE AACE 5.48 H2M Labs Inca Calibration Curve Name of run :tkn09l9O6R1.RUN Comment Calibration Curve Name of analysis :TKN.ANL Channel c2 Method _ :Method 2 Curve fit :linear a= -1.6681E-001 b=6.5024E-005 Corr. noeff. :0.9999 Peak [%] 100 80- 06040200.00 60- 40- 20- 0.000.50 1.00 1.50 2.00 2.50 3.00 3.S0 Conc. [ mg/l ] Page 1 of 1 9RAN.LUERLE RACE 5.48 H2M Labs Inc. Post -run chart, Post -run chart Name of run :tkn09l9O6R1.RUN Name of analysis :TKN.ANL Comment min Channel : 2 Method Method 2 Unit mg/1 Base 61 Gain 21 Corr. 0.9999 2 4 6 8 10 OB 0.00 1P 2.97 2D 3.00 12 3H 3.01 4L 0.02 SL 0.02 14 6C 3.01 7C 0.99 8C 0.48' Page 1 of 4 C) O DO 6RAN•LUED&E AACE 5.48 me of run :tkn09l9O6R1.RUN mment Post -run chart Name of analysis :TKN.ANL min 9C 0.21 I 10C 0.11 11C 0.01 18 12QC1 0.71 13QC1 4.62 14QC1 0.71 20 15S 0.83 16S 4.77 17S 0.81 22 18S 1.06 19S 0.30 20S 0.82 24 21S 0.71 22S 0.75 23S 0.90 26 24S 1.83 25QC1 0.96 26QC1 0.03 28 27S 1.56 28S 0.55 295 0.46 30 - 3bs 25.53 31S 1.11 3.2S 4.77 32 33S 1.09 348 1.06 35S 0.81 34 36S 0.71 Page 2 of 4 SMN.LU£BEE AAC£ 5.4E me of run :tkn091906R1.RUN mment Post -run chart Name of analysis :TKN.ANL uin 37QC1 0.94 � 38Qc1 0.00 36 A 39S 0.78 40S 0.82 41S 0.79 38 42S 1.92 43S 2.27 44S 0.83 40 45S 2.08 46S 6.26 _ 47S 2.06 42 48S 1.02 49QC1 0.96 50QC1 0.01 44 51S 1.25 52S 1.03 53S 1.07 46 54S 8.65 55S 19.93 56S 3.23 48 57S 5.01 588 4.89 59Qcl 0.97 50 60QC1 0.03 61D 3.00 52 Page 3 of 4 Post -run chart BP.AN.LUEBBE FACE 5.46 _" ne of run :tkn091906R1.RUN Name of analysis :TKN.ANL nment tin 54 62B 0.00 56 58 60 62 64 66 68 70 72 Page 4 of 4 Fr-.Z F 9-it - v 6 W IH2A LABS, INC. $ Al k- pe , 73?/o TOTAL P.H(! S/TkN DIGESTIONS NAME:' DATE':- it P 0080 IH2A LABS, INC* A 4 19 A Also, s. At, P� T�4 00 7 - TOTAL B� SITKN DIGESTIONS NAME:PdKpl-a AINH - APA DATE:. 1-11-06 IAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE VOLUME MLS. FINAL VOLUME MLS DATE ANALYZED SPIRE 0 79Y A ?mft _ao2 A fq[.,wjk Z- b9b P C) P 0081 - c" Multiple Analysis Report Print Date/Time: 2006/10/03 8:09:56 Sample ID Result Std. Dev. RSD Mode ALT Method ID Sample Type Vial Timestamp Message ID1 0.3483 0.0149 4.28 UTILITY Cleaning Procedure Sample sp 2006/10/02 11:08 LCSTV -, 2SROM24.0597 0.9738 4.05 TOC TOC WASTE WATER Sample 1 2006/10/02 11:38 ICB L/•G -0.4207 0.2317 -55.06 TOC TOC WASTE WATER Sample 2 2006/10/02 12:05 Low Sample D •� Detected CRI.-TY.=.1:Pf6I'1.•••.. ? �• 0.9706... 0.2858.. 29.44...TOC TOC WASTE WATER ...Sample 3..2006/10/02 12:90.Low Sample D n Detected MBLK 41.O -0.2904 0.0378 -13.02 TOC TOC WASTE WATER Sample 4 2006/10/02 13:11 Low Sample D -f Detected 0609809-001A � ��k 1. -0.0740 0.1638 -221.18 TOC TOC WASTE WATER Sample 5 2006/10/02 13:42 Low Sample v -o Detected 0609809-002Aj1W.Jrfl ...... 0.5124... 0.1351.. 26.36 ... TOC TOC WASTE WATER ...Sample 6..2006/10/02 14:13.Low Sample D -i� Detected 0609609-003A �S 0.3285 0.1178 3 .84 TOC TOC WASTE WATER Sample 7 2006/10/02 14:44 Low Sample D ,Detected 0609809-004A 70 0.3644 0.1538 42.22 TOC TOC WASTE WATER Sample 8 2006/10/02 15:16 Low Sample -0 4> Detected 0609809-005A. . ....... . 0.5561... 0.2953.. 44.11 ... TOC TOC WASTE WATER ...Sample 9..2006/10/02 15:47.Low Sample -0 -0 Detected 0609809-006A 40 0.6683 0.1978 22.12 TOC TOC WASTE WATER Sample 10 2006/10/02 16:18 Low Sample -0 + Detected C 0609809-007A 4 0.1163 0.2987 256.95 TOC TOC WASTE WATER Sample 11 2006/10/02 16:49 Low Sample -0 -u Detected 0609809-008A..Sq......... 0.2999... 0.1645.. 54.85... TOC TOC WASTE WATER ...Sample 12..2006/10/02 17:20.Low Sample -0 -i Detected 0609809-009A 5s 0.5752 0.0420 7.31 TOC TOC WASTE WATER Sample 13 2006/10/02 17:51 Low Sample •> ,Detected q$f 0609809-009AMS (0fm 9.8565 0.1562 1.58 TOC TOC WASTE WATER Sample 14 2006/10/02 18:21 CCV.'"`-'1'30 .•........... 24.3253... 0.6091.. 2.50 ... TOC TOC WASTE WATER ...Sample 15..2006/10/02 18:51. CCB �1 6 -0.5105 0.3211 -62.91 TOC TOC WASTE WATER Sample 16 2006/10/02 19:18 Low Sample D -4 Detected 0609809-009ADUP 0.7702 0.2634 34.20 TOC TOC WASTE WATER Sample 17 2006/10/02 19:53 Low Sample D -D Detected 0609809-010A.c4........... 0.7703... 0.3172.. 41.18 ... TOC TOC WASTE WATER ...Sample 18..2006/10/02 20:24.Low Sample D -D Detected 0609809-011A s 0.4816 0.1850 38.42 TOC TOC WASTE WATER Sample 19 2006/10/02 20:55 Low Sample -0 -n Detected 0609809-012A 8� 0.7916 0.0601 7.59 TOC TOC WASTE WATER Sample 20 2006/10/02 21:26 Low Sample -0 + Detected 0609809-013A. k5..-....... 0.7632... 0.1746.. 22.88 ... TOC TOC WASTE WATER ...Sample 21..2006/10/02 21:54.Low Sample fl + Deteced CCV V = Z�e ^ 28.2900 0.9388 1.55 TOC TOC WASTE WATER Sample 22 2006/10/02 22:28 CCB Gf,0 -0.1951 0.1574 -80.71 TOC TOC WASTE WATER Sample 23 2006/10/02 22:55 Low Sample D -G Detected Printed: 10/3/06 8:09:57 AM AM TSL007 W73 Page 1 of 1 Detailed Analysis Report Print Date/Time: 2006/10/03 8:10:01 Sample ID: ID1 Mode: UTILITY Method: Cleaning Procedure Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 11:08 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.3653 0.1827 33532 9.442 9.638 121 2 0.3310 0.1655 30998 9.436 9.634 121 3 0.3548 0.1774 32757 9.449 9.649 122 4 0.3423 0.1712 31834 9.487 9.684 120 ----------------------------------------------------------------------------- <<<Statistics>>> Mean: 0.3483 Std Dev: 0.0149 RSD: 4.28 Sample ID: LCS Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 11:38 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 22.6028 1.1301 173386 9.689 10.680 108 2 24.4854 1.2243 187280 9.748 10.744 108 3 24.6444 1.2322 188454 9.719 10.708 109 4 24.5063 1.2253 187434 9.725 10.714 108 ----------------------------------------------------------------------------- <<<Statistics>>> Mean:. 24.0597 Std Dev: 0.9738 RSD: 4.05 Sample ID: ICB Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 12:05 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.5013 -0.0251 2870 9.827 9.808 120 2 -0.1941 -0.0097 5138 9.830 9.819 120 3 -0.2787 -0.0139 4513 9.843 9.821 120 4 -0.7088 -0.0354 1339 9.864 9.841 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.4207 Std Dev: 0.2317 RSD: -55.06 Sample ID: CRI Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 12:40 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5731 0.0287 10800 9.941 9.945 120 2 0.9923 0.0496 13894 9.921 9.948 120 3 1.2478 0.0624 15779 9.912 9.950 120 4 1.0691 0.0535 14460 9.920 9.953 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.9706 Std Dev: 0.2858 RSD: 29.44 Sample ID: MBLK -Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 13:11 Operator ID: JASON SAAUEL Sample Type: Sample - Rep ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.3311 -0.0166 4127 10.017 10.005 120 2 -0.2725 -0.0136 4560 10.027 10.011 120 Printed: 10/3/06 8:10:02 AM AM Page 1 of 6 3 -0.2469 -0.0123 4748 10.017 10.033 120 4 -0.3109 -0.0155 4276 10.035 10.044 120 ---------------------------------------------------- Message: Low Sample Detected 7 <<<Statistics>>> Mean: -0.2904 Std Dev: 0.0378 RSD: -13.02 Sample ID: 0609809-001A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 13:42 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.1110 -0.0056 5751 10.066 10.050 120 2 0.1188 0.0059 7447 10.041 10.066 120 3 -0.0300 -0.0015 6349 10.054 10.053 120 4 -0.2740 -0.0137 4548 10.066 10.059 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.0740 Std Dev: 0.1638 RSD: -221.18 Sample ID: 0609809-002A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 14:13 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.7129 0.0356 11831 10.140 10.165 120 2 0.4680 0.0234 10025 10.156 10.142 120 3 0.4211 0.0211 9679 10.137' 10.153 120 4 0.4474 0.0224 9872 10.123 10.129 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5124 Std Dev: 0.1351 RSD: 26.36 Sample ID: 0609809-003A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 14:44 Operator ID: JASON SAMUEL Sample Type: Sample Rep if ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.4664 0.0233 10012 9.889 9.879 120 2 0.3284 0.0164 8994 9.881 9.904 120 3 0.3407 0.0170 9085 9.892 9.895 _ 120 4 0.1787 0.0089 7889 9.914 9.930 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.3285 Std Dev: 0.1178 RSD: 35.84 Sample ID: 0609809-004A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 15:16 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5932 0.0297 10948 9.965 9.924 120 2 0.2704 0.0135 8566 9.951 9.953 120 3 0.2781 0.0139 8623 9.980 9.973 120 4 0.3157 0.0156 89009_984-------G-986-------120----- --- --------- ----------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.3644 Std Dev: 0.1538 RSD: 42.22 Sample ID: 0609809-OO5A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Printed: 10/3/06 8:10:02 AM AM Page 2 of 6 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 15:47 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.7220 0.0361 11899 10.074 10.099 120 2 0.7612 0.0384 12232 10.086 10.111 120 3 0.5046 0.0252 10295 10.125 10.155 120 4 0.2308 0.0115 8274 10.146 10.157 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5561 Std Dev: 0.2453 RSD: 44.11 Sample ID: 0609809-006A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 16:18 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5564 0.0278 10677 10.304 10.282 120 2 0.7013 0.0351 11746 10.291 10.318 120 3 0.5515 0.0276 10641 10.344 10.339 120 4 0.8640 0.0432 12947 10.317 10.346 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.6683 Std Dev: 0.1478 RSD: 22.12 Sample ID: 0609809-007A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 16:49 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5195 0.0260 10404 10.360 10.344 120 2 0.1386 0.0069 7593 10.368 10.383 120 3 -0.0129 -0.0006 6475 10.330 10.267 120 4 -0.1802 -0.0090 5241 10.272 10.248 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.1163 Std Dev: 0.2987 RSD: 256.95 Sample ID: 0609809-008A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 - Cal. Curve: ITOC WW CURVE 092906 - Timestamp: 2006/10/02 17:20 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2792 0.0140 8631 10.142 10.135 120 2 0.0750 0.0037 7124 10.127 10.096 120 3 0.4166 0.0209 9660 10.085 10.079 120 4 0.4267 0.0213 9719 10.075 10.063 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.2999 Std Dev: 0.1645 RSD: 54.85 Sample ID: 0609809-009A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 17:51 Operator ID: JASON SAMUEL Sample Type: Sample_ Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5489 0.0274 10621 10.100 10.108 120 2 0.5705 0.0285 10781 10.093 10.113 120 3 0.6360 0.0318 11264 10.105 10.108 120 4 0.5454 ----------------------------------------------------------------------------- 0.0273 10595 10.128 10.126 120 Printed: 10/3/06 8:10:02 AM AM Page 3 of 6 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5752 Std Dev: 0.0420 RSD: 7.31 Sample ID: 0609809-009AMS Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 18:21 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 9.9485 0.4974 79993 10.233 11.224 104 2 9.8823 0.4941 79505 10.251 11.238 103 3 9.6286 0.4814 77632 10.274 11.262 102 4 9.9665 0.4983 80126 10.260 11.249 104 ----------------------------------------------------------------------------- <<<Statistics>>> Mean: 9.8565 Std Dev: 0.1562 RSD: 1.58 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 18:51 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 24.8297 1.2415 189821 10.176 11.175 108 2 23.5429 1.1771 180324 10.154 11.150 108 3 24.7867 1.2393 189504 10.115 11.107 108 4 24.1419 1.2071 184745 10.062 11.053 108 ----------------------------------------------------------------------------- <<<Statistics>>> Mean: 24.3253 Std Dev: 0.6091 RSD: 2.50 Sample ID: CCB Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 19:18 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.7213 -0.0361 1247 9.992 9.949 120 2 -0.3835 -0.0192 3740 9.963 9.938 120 3 -0.1183 -0.0059 5697 9.944 9.947 120 4 -0.8187 -0.0409 528 9.976 9.926 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.5105 Std Dev: 0.3211 RSD: -62.91 Sample ID: 0609809-009ADUP Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 19:53 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.7909 0.0395 12408 9.960 9.973 120 2 1.0754 0.0538 14507 9.935 9.989 120 3 0.4320 0.0216 9759 9.962 9.971 120 4 0.7825 0.0391 12345 9.935 9.936 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.7702 Std Dev: 0.2634 RSD: 34.20 Sample ID: 0609809-OIOA Method: TOC WASTE WATER Cal. Curve: TOC WW CURVE 092906 Operator ID: JASON SAMUEL Rep r ppm C ug C Raw Data Mode: TOC Filename: 10021043 Timestamp: 2006/10/02 20:24 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time Printed: 10/3/06 8:10:02 AM AM Page 4 of 6 C) I4 V) 1 1.1774 0.0589 15260 10.017 10.013 120 2 0.5964 0.0298 10972 10.018 10.027 120 3 0.4553 0.0228 9931 10.026 10.019 120 4 0.8520 0.0426 12858 10.009 10.020 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.7703 Std Dev: 0.3172 RSD: 41.18 Sample ID: 0609809-011A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 20:55 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2327 0.0116 8288 9.957 9.916 120 2 0.6670 0.0334 11493 9.910 9.931 120 3 0.5601 0.0280 10704 9.879 9.863 120 4 0.4667 0.0233 10015 9.850 9.841 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.4816 Std Dev: 0.1850 RSD: 38.42 Sample ID: 0609809-012A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 21:26 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.8664 0.0433 12964 9.791 9.739 120 2 0.7209 0.0360 11890 9.741 9.737 120 3 0.8005 0.0400 12478 9.712 9.735 120 4 0.7788 0.0389 12318 9.710 9.730 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.7916 Std Dev: 0.0601 RSD: 7.59 Sample ID: 0609809-013A Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 21:54 operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 1.0011 0.0501 13959 9.820 9.801 .120 2 0.7846 0.0392 12361 9.794 9.790 120 3 0.6129 0.0306 11094 9.788 9.772 120 4 0.6544 0.0327 11400 9.750 9.749 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.7632 Std Dev: 0.1746 RSD: 22.88 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 22:28 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Ravi Data Beginning Ending Integration Baseline Baseline Time 1 27.8465 1.3923 212086 9.666 10.653 110 2 28.8945 1.4447 219821 9.683 10.678 109 3 28.1742 1.4087 214505 9.685 10.685 109 4 28.2449 1.4122 215026 9.701 10.700 109 ----------------------------------------------------------------------------- <<<Statistics>>> Mean: 28.2900 Std Dev: 0.4388 RSD: 1.55 Sample ID: CCB Mode: TOC Printed: 10/3/06 8:10:02 AM AM Page 5 of 6 Method: TOC WASTE WATER Filename: 10021043 Cal. Curve: TOC WW CURVE 092906 Timestamp: 2006/10/02 22:55 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.0633 -0.0032 6103 9.741 9.735 120 2 -0.3426 -0.0171 4042 9.743 9.732 120 3 -0.3197 -0.0160 4211 9.744 9.752 120 4 -0.0547 -0.0027 6167 9.728 9.768 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.1951 Std Dev: 0.1574 RSD: -80.71 Printed: 10/3/06 8:10:02 AM AM Page 6 of 6 Calibration Report Print Date/Time: 2006/10/03 8:10:07 Cal. Curve ID: TOC WW CURVE 092906 Created: 2006/09/29 16:14 Calibration Factor (m): 1.476e+05 Y Intercept (b): 4710 r -squared: 0.99912 Standard ID Y X Expected Measured Message Date & Raw Data ug C 4194 0.000 ug C -0.003 Low Sample De Time 2006/09/29 13:26 DI 0.5PPM 9785 0.025 0.034 Low Sample -De 2006/09/29 13:49 1.OPPM 13085 0.050 0.057 Low Sample De 2006/09/29 14:12 5.OPPM 38349 0.250 0.228 2006/09/29 14:34 10.OPPM 70983 0.500 0.449 2006/09/29 14:57 25.OPPM 200810 1.250 1.329 2006/09/29 15:19 75.OPPM 555568 3.750 3.732 2006/09/29 16:05 O 00 0 C) Printed: 10/3/06 8:10:08 AM AM Page 1 of 1 H2M LABS, INC. SDG NO.: 1 ��d q SCAN: 46�u-'\ This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. SignE ReviE 00 0 0