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Metal Data Package 09/2006
Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL007 'Water Samples Received: 9/13/06 UPTAi n A T A PAC KAG E )6 1/4 1 SC40 Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 U2/M "US., INC. ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 9/13/06 SDG NO.: TSI -007 NYS DEC SUMMARY FORMS II. SDG NARRATIVES Ill. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY IH2M "USS IMC. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SD(,- TSI.t)n7 SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY Anal ical Requirements Customer Sample Code Laboratory Sample Code ME we EQ�PT BLANK 0609809-001 X X 0609809-002 X X Mw -Is 1S 0609809-003 X X MW -3D 0609809-004 X X I MW -3S 0609809-005 X –i j X MW -4D 0609809-006 X X MW -4S 0609809-007 X �— X MW -5D 0609809-008 X X MW -5S 0609809-009 X X j MW -6D 0609809-010 X X MW -6S _ 0609809-011 X X MW -8D 0609809-012 X X MW -8S 0609809-013 X�uX Please indicate year ofAAP v i o{q cu, i01ill ou M O O F-+ NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSL007 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0609809-001 EQPT BLANK WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-002 MW -ID WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-003 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-004 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-005 MW -3S WATER CA,CD,FEK,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-006 MW -4D WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-007 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-008 MW -5D WATER CA;CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-009 MVV -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-009DUP MW-5SD WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-009MS MW-5SS WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-010 MW -6D WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-011 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-012 MW -8D I WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 0609809-013 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 13 -Sep -06 09/06 TSL007 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSI -007 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Tests DateRec d at Lab I Date Analyze 0609809-001 EQPT BLANK Blank SELECT WET CHEMISTRY ** 09/13/06 09/06- 10/06 0609809-002 MWAD I Groundwater SELECTWET CHEMISTRY** 09/13/06 ) 09/06 - 10/06 0609809-003 MW -1,S Groundwater SELECT WET CHEMISTRY ** I 09/13/06 09/06 - 1.0/06 0609809-064 MW -3D Groundwater SELECT WET CHEMISTRY'* I 09/13/06 09/06 - 10/06 0609809-005 MW -3S Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-006 MW -4D Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-007 MW -4S Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-008 MW -51) Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-009 MW -5S I Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-009DUR MW-5SDUP Groundwater SELECT WET CHEMISTRY ** 09/13/06. 09/06 - 10/06 0609809-009MS MW-5SMS Groundwater I SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 0609809-010 MW -6D Groundwater I SELECT WET CHEMISTRY ** 09/13/06 09/06 -10/06 0609809-011 MW -6S Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06 - 10/06 6609809-012 MW -8D Gdwater SELECT WET CHEMISTRY *' 09/13/06 09/06 - 10/06 0609809-013 MW -8S Groundwater SELECT WET CHEMISTRY ** 09/13/06 09/06- 10/06 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand ; Chloride; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable; Sulfate; Total Dissolved Solids; Total Organic Carbon; O O Cn E-+ U2AA "US, IMC. 11. SDG NARRATIVES 0-12M 1A�3S' Isco For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 9/13/06 SDG#: TSL007 EQPT BLANK MW -1D MW -1S MW -3D MW -3S MW -4D MW -4S MW -5D MW -5S MS/MSD MW -6D MW -6S MW -8D MW -8S Thirteen water samples were received by H2M Labs, Inc. on 9/13/06 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument. Sample MW -SS was utilized for QC analysis and reporting. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: October 9, 2006 Vice President U2AA 1LA13S9 IMC. For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLE RECEIVED: 9/13/06 SDG#: TSL007 EQPT BLANK MW -1D MW -1S MW -3D MW -3S MW -4D MW -4S MW -5D MW -5S MS/MSD MW -6D MW -6S MW -8D MW -8S Thirteen water samples were received by H2M Labs, Inc. on 9/13/6 for select wet chemistry analysis. Samples were prepared and analyzed using the following EPA methods: Alkalinity EPA 310.1 Nitrate EPA 353.2 BOD EPA 405.1 Phenols EPA420.1 Bromide EPA 320.1 Sulfate EPA SW846 9038 Chloride EPA 325.2 TDS EPA 160.1 COD EPA 410.4 TKN EPA 351.2 Hardness EPA 130.2 TOC EPA SW846 9060 Ammonia EPA 350.1 Sample MW -5S was utilized for QC analysis and reporting. Samples were diluted and reanalyzed as required to keep instrument readings within calibration range. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data kage has been authorized by the Laboratory Manager or his designee, as verified "e f lowing signature. Date Reported: October 9, 2006 Vincent campiano Vice President 00 O O 1-1284iL us3 isce III. CHAIN OF CUSTODY DOCUMENTATION 1 AK TABS; 1SIC. EXTERNAL CHAIN OF CUSTODY • 010ormiunuflu" JAW, 0.6 TPeP x (639) 694-304OFa(63')420-8436 PROJECT NAME/NUMBER 60f17-060 TOWN OF c90 vT�oL AD L.AN0 FILL .3(n0 R0 /N 200 to Q3 CLIENT: s° s CL —► A o � Z O 0 cc I z :� �, :�- H2M SDG NO: (. NOTES: Project Contact: (�) saps SR� Gwb cs� C L 904 Phone Number: j / TOT. 14LK Xr'l010 /X /42Y �s PIS/Quote # —� 62) C O D� N 0 3 Pk F -M 6 L S ` 14 %v SAMPLERS: (S gnature�Cllent DELIVERABLES: Z c U° t.. ANALYSIS REQUESTED TURNAROUND TIME: i.T—b ORGANIC iNORG. , LAB I.D. NO. REMARKS: DATE- -TIME MATRI FIELD I.D. 10:*0 w w MW-- 4 D M w— 3-5 Al W'_ S D a �t 13 3 ► j 2 C0 -DUB m ,2:2s r2: sa /3.3a M W- 6 S -oil ` dl� Reil t (s ) D l3 o Time /I? % /S ReceivedReceived by -.(S lure f J nme 16 'ts LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y or N Explain: sen,otes were: 1. shipped_ or Hand Delivered F„ a irbtlf+y2 Amblent or died, Temp 3. Received in good ition 4. Property Y N COC Teoe was: 1. Present on outer package: Y or® 2. Unbroken on outer paokege: Y or N record present & complete upon sample receipt or N Relinquished try (Signature) Time R by: (S Date Time Relinquished by: (Signature) Date Time Received try. (Signature) Date Time Relinquished by. (Signature) Date Time Received by (Signature) Date Time ,IVHLIb�,�CP10 PINK COPY -LABORATORY ORIGINAL YELLOW COPY - CLIENT -VA '� I�[3S, TIC. A75 Broad Hollow Rd, Melville, NY 11747-5076 18 EXTERNAL CHAIN OF CUSTODY Tel. -(631) 694-3040Fax: (631) 420-8436 CLIENT: I H2M SDG NO: -TSG CO" PROJECT NAMEINUMBER 61Y 7 -06o 70WAf OF SOUMOLb L,+1VrfbF1LL 360 ,e 0 OVA[ 2.006 & 3 .. 21 s O VS � �- Csn PreJectContact/ NOTES: 8R F I BODS 1 (- / wD C.T Phone Number: -t oT, !� L r- Ix/b/0 /X l q g V PIS(Quote # COD/ NHS/ N 0 3/ PHeN0LS� T/< Af SAMPLERS: (signaturepClient )ywj DELIVERABLES: 6S 7� D e g ANALYSIS REQUESTED TURNAROUND TIME: S TD ORGANIC INORG. . DATE' TIME. IMATRIXFIELD I.D. LAB I.D. NO. REMARKS: I2,/Db lS,.lO L_ 1Y1W— 85 $ 3. 1 1 2 -013 15.30 1. MW QPT 8L4NK -tel Reli t try t<un) Date qI� 01p Time 16 %1 Received by: (S p to 1 �� O�O /Time 617r l LABORATORY USE ONLY Discrepancies Between Sample labels and . COC Record? Y or N Explain: �SNp 6 were: Hand Delhrered �Akbin+R 2 Aunt or chiliad, Temp 3. Received in good Y N 4. Property preserved Y N COC TeM was: 1. Present on outer package: Yoe 2. Unbroken on outer package: Y or N COC record present & complete upon sample receipt: N ReikAuWW by (Signature) to Time R ) Dat Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by. (Signature) Date Time Received by. (Signature) Date Time 1 K1fM9 T 1 ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY "?M LABS, INC. Sample Receipt Checklist Client Name PCTSL Date and Time Receive 9/13/2006 4:15:00 PM work Order Numbe 0609809 Received by dmc Checklist completed b �— �^O Reviewed by Date —------_ Si alure Initials I D e Matrix Carrier name Hand Delivered Sf�ipping container/cooler in good condition? Yes custody seals intact on shippping container/cooler? Yes ❑ custody seals intact on sample bottles? Yes ❑ Chain of custody present? Yes 9 Cain of custody signed when relinquished and received? Yes R Chain of custody agrees with sample labels? Yes ❑ Samples in proper container/bottle? Yes Wl Sample containers intact? Yes ❑d Sufficient sample volume for indicated test? Yes❑ I samples received within holding time? Yes (] Iontainer/Temp Blank temperature in compliance? Yes 0 water - VOA vials have zero headspace? No VOA vials Water - pH acceptable upon receipt? submitted 0 Yes ❑� Adjusted? No ❑ Not Applicable ❑ No ❑ Not Applicable 0 No ❑ Not Applicable No ❑ No ❑ No No ❑ No ❑ No ❑ No ❑ No ❑ Yes ❑ No ❑ Checked b No ❑ y No and/or NA (not applicable) response must be detailed in the comments section b — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - r enl contacted 0 Date contacted: Person contacted_— by. Regarding !!!�C SZova w f i, Sdy Action WA UAUSq INC, INTERNAL CHAIN OF CUSTODY CLIENT: PC TS U _DELfVERABLES& - 76 D TURN AROUND TWE: SDG fl: :aL. CO:? CASE #-, MATRIX: G pH CHECK N REMARKS: RECEIVED BY: SIGNATURE- DATE- "TWIE'- METALS P 0199 " mp. Kum m- SIMENIMEME110101 MIMI 010�0=1-mmlmm - "NA MIN W- INIENE E b -"q NMI! m ME METALS P 0199 1--H2M LAUSs ISC. � �Cr S SDs: I INTERNAL CHAIN OF'CUSTODY 4DATIME SAMPLE RELINQUISHED SAMPLE BY RECEIVED BY BOTTLE TYPE PURPOSE OF CHANGE OF CUSTODY INIT 6190 --9I � �qc� P �� nb 93 aI071 SICK ►`�l S /D� /330 sIv qt Z:3 0 lI OIQI a� SIaN DIaw SIGN Arlo$ S1oN slow SIGN slow SIcN SION SIGN SIGN SIGN SIGN SIGN slow SIGN SION SIG SION ICN - SIGN SION 9ION SION SIGN SIO# .`SIGN. slow SIGN SI SIGN - slow SIGN ' 310" .SIGN .. I310N SIC" SIGN SIGN - i METALS P 0200 IH2A I-A"s INC* INTERNAL CHAIN OF CUSTODY CLMW-. S L DELIVERABLES: a_TURN AROUND TIME: - SDG #: CASE #: MATRIX: pH CHEO& N REMARKS: Oqz locTsL- cis: RECErVED BY: SIGNATURE: WET CHEMISTRY 1H2AS LA[3S,71 INC. jCLIENT: rs i SDG ,•J-1 ?SLS INTERNAL CHAIN OF CUSTODY 1210 WET CHEMISTRY 'D mule �• .e••. .• . CMNGE CUSTODY e. e• ;� i ora � � r�►i������ :_ 1210 WET CHEMISTRY 'D mule JjWkAUS,- INC, CLIENT: SDG Ql TNTERNAL CHAIN OF. CUSTODY L. WET CHEMISTRY U2M, "US, INC. IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY 00 O O h H2M LABS, 1NC. 13LOD+ METALS TABLE OF CONTENTS I. REPORTS II. QC SUMMARY III. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Lab Code: 10478 Case No SOW No.: ILM04.1 EPA Sample No. EQPT BLANK MW -1D MW -1S MW -4D MW -4S MW-5SD MW-5SS MW -8D Were ICP interelement corrections applied? Were ICP backqround corrections applied? If yes -were raw data generated before application of background corrections? Comments: DATE REPORTED: SEPTEMBER 18, 2006 Contract: SAS No.: SDG No.: TSL007 Lab Sample ID. 0609809-001 0609809-002 0609809-003 0609809-004 0609809-005 0609809-006 0609809-007 0609809-008 0609809-009 0609809-009DUP 0609809-009MS 0609809-010 0609809-011 0609809-012 0609809-013 Yes/No YES Yes/No YES Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in.this hardcopy data package and in t e computer -readable data submitted on diskette has been authorized by e L boratory Manaqer or the Manager's designee, as verified by the followi g gna ure Signature- Name: Vincent Stancampiano Date: Title: Vice President COVER PAGE - IN ILM04.1 H2M LABS, 1NC. REPORTS FOR METALS H2M LABS, 1NC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. ; Analyte 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET --- - —_ 85.0 B P F--- '7439-89_6 j.� Iron —' EQPT BLANK Lab Name: H2M LABS, INC. Contract: ! !Magnesium _ 8.3j B ! P Lab Code: 10478 Case No. SAS No.:, SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-001 Level (low/med): LOW Date Received: 9/13/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. ; Analyte !Concentration i C Q M i 17440-43-9 I 0.38( B (7440-70-2 _Cadmium^ Calcium --�- —_ 85.0 B P F--- '7439-89_6 j.� Iron —' i 17.8 U1 x7439-92-1 'Lead 2. 1! B i P 17439-95-4 !Magnesium _ 8.3j B ! P 7939-96-5 iMa_nganese i 0.38; U P !7940-09-71Potassium j 5991 B ; r 7440-23-5 ISodium_ _ !_ 53.8^B�—i P Color Before: COLORLESS Clarity Before: CLEAR — Texture: Color After: COLORLESS Clarity After: CLEAR_ Artifacts: Comments: DATE REPORTED: SEPTEMBER 006 FORM I - IN ILM04.1 O O V) N U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L I CAS No. i Analyte ; Concentration C Q i M 7440-43-9 ;Cadmium 0.241 B I 1 EPA SAMPLE NO 28400; _ INORGANIC ANALYSIS DATA SHEET -------�} 17439-96-5 IMangane.se 6.61 B j— MW-1D Lab Name: H2M LABS, INC. Contract: 20200; P i Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-002 Level (low/med): LOW Date Received: 9/13/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L I CAS No. i Analyte ; Concentration C Q i M 7440-43-9 ;Cadmium 0.241 B I P 17440-70-2 !Calcium 28400; _ ( P j !741 89-6 (Iron F439-92-1 ;Lead 439-95-4 Magnesium ! 1391 P 1. 2! B {�—P 13800+—j P 17439-96-5 IMangane.se 6.61 B j— —i 7940-09-7 !Potassium j _ _ --TP 22601B ; P 7440-23-5 'Sodium�i 20200; P i Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: SEPTEMBER 18, 2006 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case' No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. '7 i Analyte Concentration ! C Q I M 44 43-9 'ICadmium 0.122U j P 7440-70-2 ;Calcium ( 102001 1 1 P !7439-89-6 E}E7439-92-1 !Iron !Lead 1881 i ( 1.2. B� ; P I ( P j !7439-95-4 ;Magnesium 6260; 1 I P 117439-96-5 _ (Manganese ! 16.9; { P 7440-09-7 ;Potassium ! 30501 B ; ( P L7490-23-5 ;Sodium j 49000 P� EPA SAMPLE NO MW -1S i i SDG No.: TSL007 9/13/2006 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: SEPTEMBER 18, 20 FORM I - IN ILM04.1 0 0 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET -- MW -3D i Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-004 Level (low/med): LOW Date Received: 9/13/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No.; Analyte Concentration C Q t M 7440-43-9 Cadmium j - --0.12;U; P ; 17440-70-2 10300i — 10300; i P 17439-89-6 (Iron 199; I P� 17939-921 (Lead „_---- (_ ^----1.5 B j P (7439-95_4 ;Magnesium _ _ 62801.;— P - --' 17439-96-5 M_ nganese-- - _— 2110;- ! j P :7440-09-7 !Potassium �3020,1B, P .7440-23-5 'Sodium ; 445001 ! _ _—I P 1-7 Color Before: COLORLESS Clarity Before: CLEAR Texture: — Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: SEPTEMBER 18, 2006 FORM ILM04-I 00 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET —'— — i MW -3S j ! Lab Name: H2M LABS, INC. Contract. Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-005 Level (low/med): LOW Date Received: 9/13/2006 % Solids: 0_0 Concentration Units (ug/L or mg%kg dry weight): UG/L Analyte i Concentration C I Q ! M CAS No. 7490-43-9 iCadmium _ 0.14; B 1- P 7440-70-2 ;Calcium 10100; i __.._-_;_..._P._. '7439-89-6 ;Iron - --- - - --- --.� ----- — ;7439-92-1 Lead -----...-�_�. 1.1I U I p1 :7939-95-4 ;Magnesium - ---� 62201 P i 7439-9- 6 Manganese 23.4' j(- _ P 17440-09-7 ,Potassium ------3050! 0 1 P 7440-23-5 'Sodium ( 44100 I P Color Before:_ COLORLESS Clarity Before: CLEAR - Texture: Color After: COLORLESS Clarity After: CLEAR - Artifacts: Comments: DATE REPORT SEPTEMBER 18, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET f MW -4D Lab Name: H2M LABS, INC. I Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample LD: 0609809-006 Level (low/med): LOW Date Received: 9/13/2006 Solids: 0.0 Concentration Units (ug/L or mg' /kg dry weight): UG/L CAS No. Analyte Concentration 1Cj Q M 7440-43-9 ;Cadmium 0.351 B P^ 7440-7(1-2 ;Calcium _ _ ; 19700 CLEAR I i I i C l 7439-89_-6 ;Iron j 1-7.81 U j P G7439-92-1 ;Lead---�— _ ---`------ 1. 1j U j P ;7439-95-4 ;Magnesium 10900 — 17939-96 5 ,Manganese _ . ._ .19701 ; I P' I _ 7440 09 7 Potassium _ 12600; ; P :7440-23-5 :Sodium 18000. P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR I i I i C l Comments: DATE REPORTED: SEPTEMBER 18, 2.006 Texture: Artifacts: FORMS I - IN ILM04.1 U.S. EPA - CLP C CAS No. I Analyte j Concentration f C i1 EPA SAMPLE NO P ! INORGANIC ANALYSIS DATA SHEET F- I 47439-89-6 (Iron 36 4' B j P MW -4S ! Lab Name: H2M LABS, INC. Contract: - - i 10400! Y P i --i Lab Code: 10478 Case No. DSAS No.: SDG No.: TSL007 Matrix_ (soil/water): WATER i Lab Sample ID: 0609809-007 Level (low/med): LOW Date Received: 9/13/2006 % Solids: 0.0 f j Concentration Units (ug/L or mg/kg dry weight): UG/L C CAS No. I Analyte j Concentration f C COLORLESS 7440-43-9 'Cadmium -- '�--- 0.121 U P ! 17440-70-2 !Calcium ( 19600 ! P 47439-89-6 (Iron 36 4' B j P ;_7439_-92-1 !Lead , 1.51 B ; P - -r---- `— i7439-95-4 Ma nesium - - i 10400! Y P i --i 17439-96-5 IMang_anese 19801 j P i- ---� ; — --- - 17 4 9 0-0 9-7 jPotass_ium - ------ !_-- 6670!-� !—i P i I :7440-23-5 !Sodium 123001 P Color Before: COLORLESS Clarity Before: CLEAR 1.--..-- Texture: Color After: COLORLESS Clarity After: CLEAR _ I Artifacts: Comment DA 4.1 r-+ 0 h4 V) U.S. EPA - CLP Concentration Units (ug/L or mglkg dry weight): UG/L ---.... - ---- - --- --_- `-»_�--- --i 'CAS No Analyte ;Concentration C Q M Before: it EPA SAMPLE NO '7440-70-2 INORGANIC ANALYSIS DATA SHEET - - i7439-89-6 - _ Iron 14821 MW -5D Lab Name: H2M LABS, INC. Contract: i_P 17_4_39-95-44 Lab Code: 10478 Case No. ISAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-008 Level (low/med): LOW i Date Received: 9/13/2006 % Solids: 0.0 Concentration Units (ug/L or mglkg dry weight): UG/L ---.... - ---- - --- --_- `-»_�--- --i 'CAS No Analyte ;Concentration C Q M Color Before: COLORLESS P '7440-70-2 'calcium 101001 - i7439-89-6 - _ Iron 14821 After: 17439-92-1 ;Lead i — G 2 21 BI- i_P 17_4_39-95-44 (Magnesium6240E - _ P '7_43_9-96-5 !7990-09-7 !Manganese ---;---- ------ 1Potassium 26.6Y'� --- — 26301 B_, — ; P ' PP� ;7440-23-5 -' !Sodium 443001�i P --- Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: COmmE a 4.1 U.S. EPA = CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L i CAS No. Analyte 1 Concentration ; C I Q M 7940-93 9 Cadmium 0.37, B j i P 7440-70-2 ;Calcium -'-----t 147001 - P 17439-89-6 — --- - ;Iron 17.81 U j P 17439-92-1 ;Lead 1.21 B --- i P 17439-95-4 Magnesium 104001 P 17439-96-5 _i_ !Manganese --i _ 1970 P_� 17440-09-7 iPotassium i 12300' f ! P 7440-23-5 ES odium _ 178001 _ P _ Color Before: COLORLESS 'Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: SEPTEMBER 18, 2006 ` VLGHR EPA SAMPLE NO MW -5S t, SDG No.: TSL007 0609809-009 Texture: Artifacts: FORM I - IN ILM04.1 M C) 0 F4 V) U.S. EPA - CLP CAS No. i Analyte I Concentration C 1 1 EPA SAMPLE NO -- 0.12 U 1 - INORGANIC ANALYSIS DATA SHEET --� I_ ___ P '7939-89-6 jIron -- CC 17.81 U j MW -6D Lab Name: H2M LABS, INC. Contract: ---! 45601 BT Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-010 Level (low/med): LOW Date Received: 9/13/2006 o Solids: 0.0 Texture: Color After: COLORLESS Clarity After: CLEAR _ Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. i Analyte I Concentration C 1 Q t M '7440-43-9 Cadmium -_i--- -- 0.12 U 1 - —_ P i ---r--_ 17_940__70-2 !Calcium c 18800 I_ ___ P '7939-89-6 jIron -- CC 17.81 U j _ P f 17439-92-1 ,Lead 117439-95-4 ;Magnesium 45601 BT P , :7439-96-5 ;Manganese ;7940-09-7 ;Potassium ; _105001—j- _ �CP 7440-23-5 ;Sodium 36601B i - � P Color Before: COLORLESS Clarity Before: CLEAR - Texture: Color After: COLORLESS Clarity After: CLEAR _ Artifacts: 311 Comments: DATE REPORTED:_ SEPTEMBER 18, 2006 ------ FORM I - IN ILM04.1 U.S. EPA - CLP I EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -6S Lab Name: H2M LABS, INC. Contract: i t Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-011 Level (low/med): LOW Date Received: 9/13/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L i CAS No. i Analyte ' Concentration C i Q M 17440-43-9 !Cadmium 0.58, B� �4-P 7440-70_-2 !Calcium �_ 19000 F i P 1 79_39-89-6 !Iron 33.81 B 1—I P 7439-92-1T !Lead 1.61 B _ P 7439-95-4 ;Magnesium i 45901B P 1 7439-96-5 !Manganese I _ 2590 i ! P '7440-09-7 iPotassium 10200! P 7440-23-5 -- -----,---------- 1Sodium _._-. -- 3650 Bj P Color Before: COLORLESS Clarity Before: CLEAR_ Texture: Color After: COLORLESS- Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: SE 18. 2006 FORM I - IN ILM04.1 O O N U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: o Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: DATE REPORTED: SEPTEMBER 18, 2006 EPA SAMPLE NO I MW -8D I t SDG No.: TSL0O7 0609809-012 9/13/2006 Texture: _ Artifacts: FORM I - IN . ILM04.1 0 O ! Concentration ; C Q i M 1 CAS No. Analyte 17440-43-9 lCadmium 1 —_0.121 U .----- al_c_ium1740-70-_ 2 ;-------� 1910 i 7439-89-6 11ron 1161 1 ice_ ! P 7439-92-1 !Lead_ 1.5, B i_P !7439-95-4 !Magnesium 4630 Bi T ;7439-96-5 ;Manganese —_ 4 2700, _.- - ; P ? !7940-09-7 'Potassium i - 10200;—,_ ? 7440-23-5 _--------x- sodium 37701 B _ P Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: DATE REPORTED: SEPTEMBER 18, 2006 EPA SAMPLE NO I MW -8D I t SDG No.: TSL0O7 0609809-012 9/13/2006 Texture: _ Artifacts: FORM I - IN . ILM04.1 0 O U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET ;- ---- i MIDI- S S Lab Name: H2M LABS, INC. Contract: -- Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Matrix (soil/water): WATER Lab Sample ID: 0609809-013 Level (low/med): LOW Date Received: 9/13/2006 Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte ConcentrationC 1 Q M 7990-93-9 4Cadmium I0.14€ B _. _ i P - -- r7440-70-2 ;Calcium 193001 1 P- i7439-89-6 ;Iron 325. -- -- - -- (_P i7439-92-1 Lead _ 1.1� U , _I -P i7439-95-4 +Magnesium ^_ 4790; B 17439-96-5 iManganese 27501 i_ P 17440-09-7 ]Potassium 10200] j P ^-3840 X7940-23-5 Sodium — _ _ i _ B P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: SEPTEMBER 18, 2006--- FORM I - IN ILM04.1 r- C) 0l 1--1 H2M LABS, INC. II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS J. ICP SERIAL -DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS 00 0 0 U . S . ,EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration 4 True Found %R(l) 1 True Continuing Calibration Found %R(l) Found j %R(1) M jCadmium 2500T2526.18 ; 101.0 i 2500.0 { 101.8 { 2543.83 101.8 P (Calcium 15000_0._0 97.4 50000.01 _2544.63 49042.47 9Y 8.148800.66 97.6 P 1 11ron _48719.22 - 50000.0. 4996_1.38 lj 99.9 (50000.0! 50327.28 ? 100.7 50306.48 100.6 i P !,Lead 500 0 )- 493.48 ; 98.7 { 500.0 1 494.03 98.8 { 493.69 98.7 j' P 1Magnesium 50000.0( 51091.07 102.2150000 01 �; 51600.30 103.2 151233.90 102.5 } P 1 `- - "'----"--�� _ j 2500.0 2492_30 99_7 r 2500.0 ' 2507.80 ; 100.3 i 2500.74 ; �_ 85864.057 _ 100.0 ; 107.3 li P G'Manganese Potassi.um (Sodium 800_00.0 85520.69 1106.9 180000.01 84032.6.7 _105.0 000.0' 180000 Oii 86024_81 ; 107.5 1 84829.36 1 106.0 j 84947.78 106.2 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 " 01 O O FORM II (Part 1) - IN ILM04.1 V) U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Analyte True Found %R(1) Continuing Calibration i True Found %R(1) Found %R(1) I M� !Cadmium - _ ! �f- ; 2500.0 r 2528.41 101.1 2531.45 101.3 I P ICa1_c_ium �,50 0 ( 97.3 j 48657.02 97.3 i 0 -j - -� Iron ! E ---'--_--^ -48645.69 j50000.Oj 50187.24 10-0.4 50186.66 1100.4 98.4f j 491.19 98-.2 P j P Lead 500.0 . 492.07 I 102.4 i,� Ma nesium ' I ------ g- - -- ---. -� -- -- 150000.0! 51079.16 j 102.2 151215.67 j _ 1 2500 0 2499.35 100.0 2494.97 99.8 -r P Manganese....__. i - 80000.0. 86219.53 107.8 86048.56 - 107. Potassium Sodium `._.._ ilium - -- -._J----_ j80000.0 85107.68 106.4 84851.97 j - 106.1 ! P-� (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O O r4 FORM II (Part 1) - IN ILM04.1 V) U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L I Initial Calibration N Continuing Calibration Analyte } True Found %R(1) True (---94 Found %R(1) Found %R(1) M ---- r------; Iron -!2500.0 ; ...�_ 2501.50 j 100.1 '2500.0 -- — 24.72 j 99.8 2489.40 r-- } 99.6 - P P Sodium 2500.0 1 2548.61 i 101.9 ,2500.0 ( 2535.44 101.4' 2553.40 102.1 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N O O FORM II (Part 1) - IN ILM04.1 Cj U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) I True Found %R(1) Found %R(1) M iron um-- i -- - -- -- -- --- -- - -- --- - -- — --- ;2500 0 1 2514.66 100 6 2519.89 100.8 P j j j I2500.0� 2593.06 10-3.7-1 583.37 103.3 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N O O FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AP; CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purity SDG No.: TSL007 FORM II (Part 2) - IN ILM04.1 Concentration Units: ug/L -- ^i CRDL Standard for AA j CRDL Standard for ICP Initial Final Analyte True Found oR j True Found oR Found %R j 10.0' — 10.55! 105.5 J —10.57] 105.7 Cadmium Lead f 6.0' 6.42!1--! 06.9 6.541, 109.0 Man anese i O.Oi 30.64; 102.1; 30.51 101.7 FORM II (Part 2) - IN ILM04.1 U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg) UG/L SDG No.: TSL007 FORM III - IN ILM04.1 Initial ! �EE i ; Calib. j Continuing CalibrationPrepa- Blank ! Blank (ug/L) ration i) Blank C Analyte ! (ug/L) C 1 C 2 C 3 C i M 1 dmium _ 0.2j B { — 7.4 U 0. _2 �B�_ 7.4 1=! 0_.21Bi 7`4 0.1 (U! 7.4 U -0.1801Bi 10.800 B P Calcium ' .i.0 17.8 U j _ _U 17 UT---- 17.8 U C 17.763 U i P Iron !Le - ----- Leaa � 17.8; U 1.1! U , l —! 1 1. 1 , U ._.-._._._ .8, 1.1 ` U i-----• ---- 1.1 ` U -- 1.126 U U .P P Ma nesium 8.2 U, g- - -- - --' -- --- --- r --!--— IMan g anese 0.4 U ! - : - r ..... _ -- -- - 9-9 B j _ — — 0. 4 F U -- --- -- _- 8.2j U j 8.2 I (7 [-�-- 0.4; U _ 0.9 ; U j 22.9 B 8.230 j _-0.380 B ( T9, 800 B P P iPotassium - 30 0 B a -- 15 0 Ui 26.0 j B 15.0�U 25 8 B-} 15 04Ui_ ; 15.0!U! . — _� _14.979 U; - P Sodium ! -'— 1 i T{ - FORM III - IN ILM04.1 U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L FORM III - IN i I I Initial E Calib. j Continuing Calibration Prepa- I Blank Blank (ug/L)(� ration Analyte (ug/L) i C 1 C 2 C 3 C1 Blank C' M I Cadmium - - --- Ca l c i um —_ Calcium jIron — 0.3 ' B ' 7.4 _i U IT . 8 UP i -- -- 1-- i ( i J- I TF - —,--�—, - II 'Lead ! ))Manganeser I 1.1 U i 14.7 B I--' 0.4 1 U i._...------1 r 1 — — 1 P' L_ i rPot s ium__.._,_.----------!---I -- 2 9 Z i g - 1--- P a s --,------ !Sodium — 15 O I U I --__ - -P I j FORM III - IN U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA ICS Source: MV Labs/High Purity Concentration Units: ug/L FORM IV - IN ILM04.1 ! j ; True i Initial Found iFinal Found Sol. Sol. Sol. Sol. Sol. Sol. ! Analyte i A AB A AB %R i A AB %R Aluminum ! 500000 500000 ! 497061 500241.11 100.01-491224_ i 493134.41 Y 98.6 -- - ---------------- 1000 870.8 87.11 j 850.8 85.1! 96. 1j . !Calcium ; 500_000 ; 500000 489526_ 495003.1; 99.0; 979524 i 980963.0 �201890.1j 98.7 Iron_ ! 200000 1 200000 - 1000 199593 100.9196897 19748_6.1 ----.� 872.93----87.21 � j— 855.9-- 85.6 8 96.8! !Magnesium 500000 - ' 500000 1 694672 489654.3 98.9. 48203 969132�9; --- — 437.7 - 87.51 9285.01 Man anese --g -- - -- 500 I — - -- -- ----- — �- —� FORM IV - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO MW-5SS I 1 SDG No.: TSL007 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Comments: FORM V (Part 1) - IN ILM04.1 j Control Limit Spiked Sample Sample i Spike I Analyte %R Result (SSR) C Result (SR) C1 Added (SA) ' %R { Q i M 'Cadmium 75-125 50.9100 { 0.3700 ; B I 50.00 _ 101.11 P !Iron { 75-125 j 986.37001 17.7629jU 0 0.00E9898 6 Pj Lead 75-125 j 20.2590 i — 1.2364 JBL 20.00i 95.11 P ,Manganese 175-125 2419.480 — 1966.6300 C 500.00 — 90.61 Comments: FORM V (Part 1) - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES - l MW -5S 1 Contract: SAS No.: SDG No.: TSL007 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L 00 N O O FORM VI - IN ILM04.1 Control Analyte i Limit � }_ Sample (S) C I Duplicate (D) C ( RPD { � Q IM - Cadmium i 5.0000i _ 0.3700 B �_ 0.24001B 42.6; f ! P _ ;Calcium 5000.00n0-0-- 14673.7100 ; ^T 14881.0300 1 1.41 P Iron ;_; 17.7629 U Lead 3. 0 000 ------1.2364 B!---- _ _ 17.7629 ---- 1 .4 7 9 5 U B r I 17.91 P FP `'-�-- 1Ma�cnesium x5000.6 H! ! _10369.9800 I i t 10515.9500) I 1.41 j P I _ Manganese i-_�1966. 6300T_ i 1993.5700 ; j 1.9� I P1 ;Potassium 15000.P ; - -_12288. 0300 ! j ' - 12522. 9100( r- 1.9 I P !Sodium 15000.0000! 17779.3400 1_;�- 18068.4300�i-;-'-' 1.6 P _ 00 N O O FORM VI - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSL007 FORM VII - IN N O O ILM04.1 C% Aqueous (ug/L) + Solid (mg/kg) ! Analyte I True Found %R i True Found C Limits %R Cadmium i 2500.0 2562.08;102.5 !Calcium 50(To 0.01, 49010.591 98.0 11ron 50000.01 50394.631 100. 8�`� 1 1Lead 00 0. ; 500.0. —491_85-; 98.4! f Magnesium 50000. ^01 440 51.15' 102.9 I -- --' ,Manganese_! 2500.01 _2529.40; 101.2 P_otassiu__m_ 1 80000.01— 86966. 621_108.- 71 _ Sodium - i...-80000.01 k I —86186.79! 107 7 -- FORM VII - IN N O O ILM04.1 C% Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No.: Concentration Units: ug/L SDG No.: TSL007 EPA ! i Sample 0 ADD I 1 ADD 2 ADD 3 ADD ! Final I No. Ani ABS i CON ABS CON ABS I CON ABS Conc. r Q FORM VIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Contract: SAS No.: Concentration Units: ug/L -- MW -5S SDG No.: TSL007 Level (low/med): LOW FORM IX - IN ILM04.1 Serial % i Initial Sample '1 I Dilution 1Differ-!� C I ence (� Q M Analyte i Result (I) C Result (S) Cadmium __-- 0. 371 B (! 0. 611 U � _ 10 0 0 -Pi Calcium CI 14673.71] 11 _, _. 14534 B! I 0.91 1 P 1 Iron Lead_ ----'�- 1 j 1'7. 8 0 T 1.24 B 1 1 -------0369.98 88.80 U1 5. 60j U BI I I P , 100.01 1 P f 0.9711 P ! Magnesium Manganese Potassium i i i , 1 1 1966.63 i 12288.031 1 1 1777 10278.75. 1955.10 !i 11531.15: B B_ 16894 .40 0.611 Pi 6.21 IP 5Sodium 01 FORM IX - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: TJA6IEA Flame AA ID Number: Furnace AA ID Number: Comments: Contract: SAS No.: Date: 3/15/2006 SDG No.: TSL007 ' jAnalyte Pave- length Back- i (nm) ground! CRDL (ug/L) i IDL (ug/L) i M Cadmium ! 226.501 j 5.01 _0.11 P 1 `Calcium ,Iron _.... 317.931! 259.901 T ! 050! 050 00.01 100.0; 7.41 17.81 P ;Lead 220.35, i 3.01 1. 11 _P_ P _ IMagnesium 5000.0; 8.21 P _!279.08 Manganese , i_ 'Potassium ; 257.61 _--� 766.49; �4 Y1 T _15. 01 5000.01 0. 41 16.01 P_ P (Sodium 1 588.901 1 5000.Oj 15.01 P FORM X - IN ILM04.1 N M CD O C/) F_4 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA Date: 12/19/2005 i Wave- � Interelement Correction Factors for: 1 length 1 4Analyte(nm) Al Ca Fe Mg Co Aluminum 308 2- 2- 0 000000011 0000000 0.0000000{ 0.00000001-0.0163000 Antimony- 206._84? r 0.00000001 0.0000000 0.02000001 0.0000000 _0.0000000 (Antimony _y 206.8411 0.00000001 0.000000_0 0.03200_00; 0.0000000 0.0000000 , Arsenic x__1_89.04 1 0.00000001_ 0.0000000; -0.0100000' 0.0000000 -0.2040000 __ Barium ! 493 41`1 0.0000000! 0.0000000 -0.00000001 0.0000000, 0.0000000 Beryllium 313:04! 0.00000001 0.0000000 0.00000001 0.00000001 0.0000000 Boron ; 249.68f 0.00000001 0.00000001 -0.000340011 0.0000000; 0.0014300 1Cadmium 226.50;! _0.0000000;_ 0.0000000; 0.00011301 0.00000001 0.0000000 _ Calcium 1 317.931 1 0.00000001 0.0000000 0.00000001 0.00000001 0-0000000 i - Chromium j 267.62;; 0.0000000; -1 0.0000000-_.0.0000000_ 0.0000000 0.0000000 Cobalt- -i 228.621; 0.0000000 0.0000000; 0.0000000; 0.0000000 0.0000000 Copper 324.75_1 ;_ 0.000000_0; 0.00000001 -0.0000400; 0.00000001 -0.0003670 i }Iron - 259.941 0.0000000; 0.00000001-_0.0000000; 0.00000001 0.0000000 1 Iron 271 44 0.00000001 0.0000000 0.000OD00 0.0000000) 01 0.0000000 0 . Lead +- 220.35!; - ---i- -0.2720000 0.00000001 0.004200001 0.0000000; 0.0000000 _ _ _ Lead;- 220.351_ 0.52600001 0.0000000 - 0.0830000 0.0000000; -0.7550000; _ ---- Magnesium 1 279.0811 - 0.00000001 0.00000001 0.0000000 0.00000001 0.0000000 �Ma_n anese 257.61; -0_.0001400':• 0.00000001 0.00002301 -0.0000000` -0.0004900 __ ..g _ Molybd_enum ---- 202_.03; 1_-_ 0.00000001 0.0000000 0.000OO66E 0.0000000; 0.0000000 'Nickel 1 231.601 1 0.00000_00; 0.0000000 0.0000000' 0.0000000' -0.0004500 !Po_tassi.um_1 766.491i 0.00000001- 0.0000000 O.000OOOOi O.000OOOOi 0.0000000 1 Selenium 196.031; 0.00000001 0.0000000 0.00000001 0.0000000 0.0000000 Sele_n' 196.03;'_ 0.000OOOOT 0.0000000 0.00000001 0.0000000; 0.4080000 _ 1 Silicon 288.16' 0.0000000; 0.0000000; 0.0000000, _ 0.0000000; 0.0000000 1 Silver 328_071 0.00000001 0.00000001 0.0000000; 0.00000001 0.0000000 _ Sodium 330.23! 0.0000000i 0.00000001 0.0000000: 0.0000000_ (Sodium_ 589.0011_- 0.00000001 _0.00000001 0.000000OL 0. (L000001 0.0000000; 0.0000000 _ Strontium 1 407.77'1 0.00000001- 0.00000001 0.0000000; 0.00000001 0.0000000 j Thallium 190.8611-__0.00000001_ 0_00000001.0.33200001_ 0.0000000;-0.5310000 Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA Date: 12/19/2005 Comments: FORM XI (PART 1) - IN ILM04.1 Wave- 11 i Interelement Correction Factors for: length 11 (Analyte I (nm) Al Ca Fe Mg Co Tin I_ 189.99; 0.0000000' 0.0000000 -0.00- 0204 0.000000011 0.0000000 , ITitan um 0.00000001 0.0000000 0.00000001 0.0000000 - 0.0000500 I - -- {.--anadium _334.9_4 0.00000001 0.00000001 0.00002001 0.00000001 0.0000000 Zinc _(__ _292.90; _ 213.86;11 0.000000011 0.00000001 0.00015801 0.0000000 0.0000000 Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA Date: 12/19/2005 I Comments: FORM XI (PART 2) - IN ILM04.1 Wave- t1 Interelement Correction Factors for: length 'Analyte 1 (nm) 11 Cr Cu Mn Ni V 'Aluminum 308.22TE 0.0000000( 0.00000001 -0.0003880 0.00000001 0.0170000 Antimony_ 206.8411 8.57100001- 0.0000000 0.0000 100001 0.0000000 1Antimon - ---y --�---- 206.84( ; 9 85700 0 0.0000000 0.0000000; -1.1020000 -6.4900000 !Arsenic_ 189.0411 0.24500001 0.0000000 -0.2700000; 0.0000000, 0.0000000 _ !Barium 1 493.41;1_0.0000000; 0.0000000 0.0000000' 0.00000001 0.0000000 (Beryllium 313.04 0.00000001 0.000OOOOL 0.0000000j 0.00000001 0.0002000 Boron 249.68);T 0.00000001 0.0000000 0.00000001 0.00000001 -0.0002500 _ _I- 1Cadmium 226.50,' 0.0000610; 0.00000001 0.0000000; -0.00018401 0.0000000 , Calcium 7.j 0.0000000; 0.0000000; 000 00000 0.0000000; 0.0000000 !Chromium 7_217 I 0.00000001 00000001 0.00000001 0.0005100 ; Cobalt _ _000000001 2_28.621; 0.0000000; 0.0000000; _0. 0.00000001- 0.00020401 0.0000000 _ _ Copper 324.7511 0.00000001 0.00000001 0.00000001_ 0.00000001 0.0000000 1 _i Iron 259.9411 0.0000000 0.00000001 0.00000001 0.0000000; 0.0000000 Iron ......-------;------- 271.441! - 0.00000001 - 0.0000000 0.0000000 0,00000001 0.0000000 -- Lead' 220.351� 0.00000001 0.0000000 0.15500001 0.1430000: -0.1570000 1 _ Lead 220.3511 0.00000001 0.0000000 0.00000001 0.3140000. 0.0000000 _v Magnesium 279.08;( -0.00010001 -- -. - 0.0000000 -0.0035000 0.0000000:. 0.0000000 Manganese 1_257.61! 1Mobdenum �- 10_00000001, 202.0311- 0.00_00000; 0_0000000 0.0000000! 0.00000001 0.0000000 -0.0001000 0.00000001 0 0000000 Nickel ! 231.60;1 0.00000001 0.0000000 _0.0000000 0.00000001 0.0000000 0.0000000 1Po.tassium1 766.:4.91 0.00000001 0.0000000 0.00000001 0.00000001 0.000.0000 Selenium 1 _ 196 03 . 0.0000000 0.0000000 0.27500001 0.00000001 0.0000000 I -- -' Selenium 1- - - ------ - - 196 0311 - 0.0 000000; - 0.0000000 1 0.4450000 0.00000001 0.2350000 LSilicon ! 288.16;1 0.0000000; 0.000000-0.00000001 0 0.0000000; 0.0000000 ;Silver 328A71 1 0.00_00000! 0.00000001 0.18500001 0.0000000! 0.0000000 Sodium i 330. 23! j 0.00000001_ 0.0000000; 0.0000_000!- 0.0000000_1 0.0000000 Sodium 1 5_89 00!_1 0.00000001 0.00000001 0.00000001 0.0000000; 0. 0 00 , !Strontium �I 407.77111 0.0000000; 0.0_0000001-0.00000001 0.00000001 0.0000000 ,Thallium 1 190.86'1 0.20000001 0.00000001 -0.65000001 0.0000000 -0.8430000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA Date: 12/19/2005 Comments: FORM XI (PART 2) - IN ILM04.1 Wave- ;i Interelement Correction Factors for: j length 1Analyte ! j (nm) i� Cr Cu Mn Hi V I jTin 189_9911 00000000! 0.00000001 0.00000001` 0.00000001 0.0000000 _..__it !Titanium t 334.941) _ 0.0000000 0.0000000 0._0000_0001 0.00_0_0000 0.0000000 !Vanadium 292.40, 0_.0000000; 0.0000_000; 0.0000000 'Zinc 1 _—_0.0000000;_ 213.86'1 0.00000001_ _0.0000000, 0.00040001 0.00000001 0.0050400; 0.0000000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL007 ICP ID Number: TJA6IEA Date: 05/10/2006 Comments: FORM XII - IN ILM04.1 I Time i Concentration Analyte (Sec.) ( (ug/L) M Cadmium i 15.001 20000P j Calcium 15.001 10000001P I I r o n _.._.__.---.---•-------..15.0. _ 0 0 � _ 2 5 0 0 0 lead 1 15.00;500001P i M ,agnesium ;_ 15.00 — 1000000 — iMan an_ese_! 15.00 20000 1 Potassium ;_ 15.001 250000`P Sodium 15.001 750000{P I i I FORM XII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL007 -----EPA -- r— i { Sample Preparation Weight Volume No. Date (gram) (mL) �EQPT BLANK 09/14/2006 { 50 ILCSW _ 09/14/2006 j_ 50-j rMW-1D _ r— 09/14/2006 i 50 i Mw -is I 09/14/_2006 i --� 50 - MW -3D ^ - _ 09/14/2006 ; 50 j MW -3S- _ 09/14/2006 —� 50 j MW -4D Mw -4s - ( 09/14/2006 _j` -j---09/19/2006—+--5o 50 MW -5D0_9/14/2006 50 r Mw -55-------T-09/14/2006 Mw-5SD 09/14/2006 MW-5Ss -- ! 09/14/2006 i — T —50 Mw -6D 1 09/14/2006 50 MW -6S — 09/1_4/2006 50 MW -8D --- ----i--09/14/2006 _� Mw -8S 09/14/20^ _50 50 PBW -- 09/14/2006 i 50 FORM XIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 09/15/2006 EPA U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL007 09/15/2006 Analytes Sample i D/F i Time % R IAjSIAiB BICIC!CICICIF PIMIM H NKSIAINIT'VsZiCI No. ! i �BSIAIEID!A!R?OIU!E B;GIN IL BI GiII IEIGJA`L iNINI s0 --- ^1.00 1.00 1 1248 i T1255 I jxj (—�I X X! i XIXIX XI I Ix I XI j�I is ! is Is .._.... 1.0 0 ! 13 0 l ! 1.00 ! 1306 ( j Tx� I x ( ! ! x _; s 1.00 1312 !s I _1.00 7 1345_? S.__- - --1.00_ 135_0 �- I I I ix'x X -I I ! I i ! _I -}-X i I I X X i I X ~1.00 1355 ! iii X I X € X� X X i !ICV I !ICB 1.00 1.0.0 1402 i 1410 1 ? ! I I-- x I i xix ! ! IXIX XIX I I i X { !X �X 1917 i _;_ - _I _ X� x 4 x '�- i ! �� !CRI._ _. I IICSA ! 1.00 -; 1.00 i ; 1425 - -- !-- - T— !X ! ? ?XIX!—I j ;XjXIX X I i i _? --� IICSAB� ` ' 143_2 X i I X I X! x X X i_.-- --- i }CCV j ._T_._.. __.1.00 1.00 1 .0 0! _— _ 14 4 0 jj 1-- - I I j ! j I X X i I �X I X XX i�X) �- !_ X! X CCv -_- CCB �- -- 1.00 -- -----' 1447 it 1455 ----f x I , ?— I I iX!X•: ( j IX X X XI 1 iX! I X I PBW ILL_Csw-__-_..- --1.00 1.00 1502 ! 11510 ! i XIX! IX`X!X X '.__.+i�l I i X j xi X ; X X X X! ! ' I f X! j X--�{---�� (— IEQPT-BLANK! -1.00 i 1517 !` __.�_ --i I—! -!XIX I IX XIXIX! ! IxI X! I i I� ?MW -1D I _ ---- --- !M[a-is I ?MW-3D 1.00 ---------- 1.00 _- 1525 ! ---- 1532 -- ! !X X! ; j ?X X!XjXi --! j —{ ?_ x x ? x x' x x' - �—1�� --`1-x7 X IX; X! ! IX ! X x x_ -X I X !_ ! 1.00 1 I X I X=1 'Mw -3S �M - --{ MW -41D _1540 1.00 1.0 ( 1547 j ! 1555 ;—! -i i I ,X X j I XX X!x' X_0 I ! �I 1 jX X; ` -IXjx X, I Iv XI I ;X! IX - X! j !X_ !-iX i--i-X�_! I I ! i MW -4S i 1.00 _16 ! ! X I _ I X!X!x1xi ! tXIX —;'-� I i MW -5D I CCV — �.-- 1.00 ^1.00 i 1610 _ ! 1620Ixjx XIXI j ? XXi I i i I I ixiXIXIXj —=— X;X �!_ . ; 'XI ,X :—-1-1—TJ I i ; ( ! ICCV - j jCCB -- 1. 00 1.00 -- i 1628 1635 ! ! i i_; _j_' x I I _I i j-j�;X XI !_!XIX X Xf- ! I i i I x X X ! IMG1-5s _ _ MW-5SD 1 00 1.00 1643 ? 1650 j �^ i IXIX I IX;X X ; X! X ! X X j _ �! X ! X E I ; !X jX! I j ; X I j X_ -X) i ; ! ( M MW-5SS 1_00 1_658 'mom _; !^—_I X`XI X X I- xIx 1 I. J�Ixf I !M6d-5SL _ 5.00 ^1705 — II i --jXXl —;XIX X!XX —I Xi _ I T { IMW-61) ! 1.00 1713 i ! ! Ix!�XjXjX X! ?X' ! ;X I,MW-6S ! 1.00 ! 1720 ! I ! jX!x IX!XIX!X IX ! iX FORM XIV - IN ILM04.1 V) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 09/15/2006 FPA U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL007 09/15/2006 Analytes Sample ! � D/F � ! Time i I o R IA�SIA jBIB CC(CIC�C�FIPfM�M�H ItL,B!S;A A R�OjU EIB G NiGII N KISjAiN�T�V E G A Z L N,N C No. i f E'D j j l I!( �I !MW -8D MW -8S ! ; 1.00 1.00 ! 1728 i 1735! I i x x j IXIX;Xlx ( ! ! jXjXi ;-; jXIX;XjX X ;X It 1XI IX 1 ! 1 j �Cci 1.00 1 1743v 1750Cv ! !�'•I!I i _ ! XX1.00 I _ ;CCs 1.00 1758 j € I t i ; I j :X XIX X ; ,X !CRI -- - I I CSA - -- !----1 1.00 0 0 1805 !� ! 1813 j _ -r-•--r-� -{-j x ! _T I� X i X; X : I x X X , X_ ! x --- - �ICSAB -- _ -' _ 1.01820 1 -_-..I - -i - X! -^,I �X X, X XiXI-!�- ccv CCV iiccs ! 1.0 828 i 1.00 i 1836 j j jX;x; i ;xlx1x;x I �T� _ -� - --�- XX ix _ ( X �x I X I j -------- -- ! !--- 1.00 ---, 1.00 11893 -- - -, ---- 1851 X.X1 i I t! - --i- -- . - j-- t- ! -{ jzzzzzz (zzzzzz zzzzzz z ! 1.00 ! 1.00 i 1858: ? 1906 ! i i 'r T�1 i ! jzZZZZ2 jzzzzzZ j 1.00 1.00 ! 1913 1921 i �vi� zzzzzz !zzzzzz1 j zzzzzz . I 1.00 1928�- 1_.0_0 'I 1936 -- 1 0 0` 19 4 3T�--- - -- zzzzzz Izzzzzz ! 1.00 1.00 1 1951 j 1958 j �- r I--' 1� zzzzzz - 5 -- 1.00 6-0-,1 2006 (zzzzzz- zzzzzz - -- v - 1.00 2013 2021 I ! :, ! i _ f ' - I-- I j--�i zzzzzz zzzzzz i - -_ 1.00 y 1.00 2028 2036 :zzzzzz i 1.00 20.4 .zzzzzz 1.00 2051 - zz 1.00 2059 !Zzzzzz - - -- jZZZZZZ I 1.00-1 1. 00 2106- :2114: ; zzzzzz ! 1.00 ! 21211 ._ E ! -�---- �I -- - _ - - jZZZZZZ 1.00 1_2129 !' t _ j j--^ j - -i jzzzzZz ---._-__.---T---1 _ -1 - --;_ 1_00-' 2136 _4 ( _ TI- I j 1 -+- A.-. I ' I - ( i � -j I I C T_C f2zzZzz i.00 2144 _ FORM XIV - IN ILM04.1 ttj H2M. LABS, INC. III. RAW DATA FOR METALS A. ICP DATA 12M LA ".9 INC. CLIENT i 5e- 0 o '-:t- I (Z: TASK. C--L.P\ RESULT FILE_ —D 0-0, i5y(- DATE Q �I ANALYSTQ,Q21.nq,�� ,L #_;- SAMPLE NOTES ; # SAMPLE NOTES ; 17 � 1 IGS/ ; 26;000SSN�, - o•9€S`,o , �I - S S ,� ; i 2 i 1 C✓L i ; 27i , 43 4 ; e.rZ 29 - orz�; ' 20 C C� Z ; 45 ; � o o1�M S i 5 ; ICSSE:f--o11ga; GwC Z ; ; 46 ;9 - via A., , , e 6 , t GS AR / ; 31 ; CCIV ; 22; 7 C /t , r 32, , Gcwc-3 ; 23' 0076 �. 8 CGS`- t ; 48 ` o t 3 33 r 9i ; GC. t 34 i G (4 /-" i 1Qi IA (3. i 24 ; 35; ( C"Ai::� ; ' 49;d4o9-}5 � , 25.E "ao,6�All 36 ' , , i 12 iObo51%,3 - Ob/rz; Gl� 37: C LVt f amu; P 0030 38! 1 14; oo39i� 39; cC'f3'( r r , , i 16,' , 17 � vat ; �� i`� 421,0 09la: I 0 04c 43 20 C C� Z ; 45 ; � o o1�M S 21 ' GwC Z ; ; 46 ;9 - via A., , 22; CL 47; - O 23' 0076 �. j\%� \JJ S S' 48 ` o t 3 A, 24 ; od� ' 49;d4o9-}5 � , 25.E "ao,6�All ' r r amu; P 0030 I I 1281 LA", INC. CLIENT ^T%(z.i DATE1�'0� TASK: RESULT FILE: ANALYSTCLL,,�ti2 �S L # SAMPLE ; NOTES # SAMPLE NOTES 1 1 1 1 I 1 1 3 1 c WLS� 26 i 2 ; cL%SS ; ; 27 S _ 3 -to iia �L L��-�� ; 28; ■ GJ , 1 1 1 P -0031 Standardization Rpt. ] od: CLP1 Standard: StdBLANK Time: 09/15/06 12:48:19 Elem Ag Al As1890 Avge -.00377 .0049 .00055. SDev .00005 .0000 .00159 %RSD 1.3845 .6261 291.18 #1 -.00382 .0049 .00211 #2 -.00372 .0048 .00060 #3 -.00376 .0048 -.00107 Elem Cd Co Cr Avge -.0006 .0000 .0017 SDev .0003 .0001 .0004 %RSD 48.54 265.5 25.39 #1 -.0003 .0001 .0012 #2 -.0006 .0000 .0018 #3 -.0009 -.0000 .0021 Elem Mg Mn Mo Avge .0006 .0028 .0002 SDev .0002 .0003 .0001 %RSD 29.45 11.35 42.12 #.3 Elem Avge SDev %RSD #1 #2 #3 Elem Avge SDev %RSD #1 #2 #3 .0004 .0006 .0007 2203/2 -.00038 .00121 316.87 .00020 .00043 -.00177 Sr .0001 .0001 43.50 .0001- .0001 .0002 .0025 .0029 .0031 2068/1 -.00149 .00051 34.275 -.00158 -.00195 -.00094 Ti .0003 .0000 10.60 .0002 .0003 .0003 .0001 .0003 .0002 2068/2 .00155 .00095 61.123 .00067 .00143 .00255 T11908 -.00247 .00073 29.351 -.00291 -.00287 -.00163 09/15/06 12:55:44 PM B .0008 .0001 9.662 .0008 .0007 .0008 Cu .0020 .0000 1.086 .0020 .0020 .0020 Na -.0162 .0004 2.266 -.0166 -.0160 -.0160 1960/1 -.00550 .00150 27.339 -.00558 -.00697 -.00396 v .0000 .0000 91.46 .0001 .0000 .0000 Ba .0000 .0000 34.46 .0000 .0000 .0000 Fe .0001 .0000 26.44 .0001 .0001 .0001 Na .3299 .0039 1.188 .3270 .3284 .3344 1960/2 .00075 .00068 90.904 .00153 .00043 .00029 Zn .0007 .0000 .4382 .0007 .0007 .0007 Be -.0010 .0000 1.162 -.0010 -.0010 -.0010 Fe .1735 .0231 13.32 .1479 .1796 .1929 Ni .0010 .0001 15.63 .0008 .0011 .0011 Si .1062 .0033 3.066 .1086 .1076 .1025 page 1 Ca .0051 .0001 1.933 .0050 .0051 .0051 K .0062 .0005 7.536 .0058 .0060 .0067 2203/1 .00864 .00186 21.498 .00734 .00782 .01077 Sn .0038 .0015 38.46 .0025 .0054 .0035 Standardization Rpt. 09/15/06 01:01:41 PM page 1 ] od: CLP1 Standard: StdAGSBH Time: 09/15/06 12:55:50 Elem Ag 2068/1 2068/2 Avge .60853 2.2079 1.3925 SDev .00572 .0252 .0216 %RSD .93952 1.1420 1.5538 ##1 .60437 2.1853 1.3874 ##2 .60617 2.2033 1.3739 #$3 .61505 2.2351 1.4162 Standardization Rpt. 09/15/06 01:06:51 PM page 1 P od: CLP1 Standard: StdICSH Time: 09/15/06 13:01:47 Elem. Al Ca Fe Avge 26.97 41.01 .4805 SDev .09 .07 .0012 RSD .3153 .1819 .2444 #1 27.07 41.10 .4818 #2 26.93 40.97 .4800 #3 26.92 40.96 .4796 Mg 53.57 .10 .1896 53.69 53.53 53.49 Standardization Rpt. 09/15/06 01:12:48 PM ] tod: CLP1 Standard: StdFURNH 1_r__ Time: 09/15/06 13:06:57 Elem As1890 2203/1 2203/2 1960/1. 1960/2 T11908 Avge .78403 2.8917 1.2384 .60363 .43581 .67903 SDev .00491 .0144 .0030 .00596. .00313 .00488 %RSD .62680 .49828 .23975 '.98681 .71784 .71867 #1 .78341 2.8800 1.2407 .59900 .43644 .67723 #2 .78923 2.9078 1.2393 .61035 .43857 .68456 #3 .77946 2.8873 1.2350 .60154 .43241 .67532 page 1 7t O O E-+ Standardization Rpt. I od: CLP1 Standard: StdMULTH Time: 09/15/06 13:12:53 1.435 Elem B Ba Be Avge 1.114 4.528 5.064 SDev .007 .017 .019 %RSD .5939 .3705 .3736 #1 1.106 4.509 5.043 #2 1.119 4.541 5.079 #3 1.116 4.5.33 5.070 Elem Mn Mo Ni Avge 13.35 1.349 1.469 SDev .05 .005 .003 %RSD .3799 .3626 .2017 #1 13.30 1.344 1.467 #2 13.40 1.352 1.472 $3 13.37 1.353 1.467 Elem v Zn Avge .9761 3.330 SDev .0040 .013 %RSD .4080 .4046 .9716 3.315 .9793 3.341 4T3 .9774 3.333 09/15/06 01:19:31 PM page 1 Cd Co Cr Cu 42.55. 1.435 1.907 1.140 .06 .007 .007 .006 .1392 .5222 .3634 .5285 42.50 .1.427 1.899 1.133 42.61 1.441 1.913 1.145 42.54 1.438 1.909 1.142 Si Sn Sr Ti 1.345 6.170 8.979 1.567 .039 .045 .039 .001 2.911 .7254 .4364 .0343 1.303 6.118 8.935 1.567 1.353 6.196 9.010 1.567 1.380 6.195 8.991 1.568 00 d' O O H Standardization Rpt. l od: CLP1 Standard: StdFENAL Time: 09/15/06 13:19:38 Elem Fe Na Avge 32.24 3.4.26 SDev .89 .86 %RSD 2.755 2.519 #1 31.23 33.27 #2 32.88 34.86 #3 32.62 34.64 09/15/06 01:24:42 PM page 1 Standardization Rpt. iod: CLP1 Standard: StdFENAL Time: 09/15/06 13:25:27 Elem Fe Na Avge 32.11 34.25 SDev .53 .48 %RSD 1.637 1.389 #1 31.55 33.75 #2 32.19 34.30 #3 32.59 34.70 09/15/06 01:30:31 PM page 1 Standardization Rpt. 1 god: CLP1 Standard: StdFENAL 1,-,. Time: 09/15/06 13:31:32 Elem Fe Na Avge 31.82 33.94 SDev 1.10 1.03 %RSD 3.451 3.046 #1 30.56 32.75 #2 32.51 34.58 #3 32.40 34.49 09/15/06 01:36:36 PM page 1 Standardization Rpt. 09/15/06 01:45:18 PM page 1 I .od: CLP1 Standard: StdBLANK Time: 09/15/06 13:37:53 Elem Ag Al As1890 Avge -.00380 .0053 -.00116 SDev .00008 .0001 .00031 %RSD 2.2237 1.727 26.547 #1 -.00373 .0054 -.00124 #2 -.00377 .0052 -.00082 #3 -.00389 .0052 -.00142 Elem Cd Co Cr Avge -.0000 .0001 .0004 SDev .0012 .0001 .0001 %RSD 2579. 66.71 26.21 #1 .0013 .0002 .0005 #2 -.0004 .0001 .0004 #3 -.0010 .0001 .0003 Elem Mg Mn Mo Avge .0006 .0022 .0005 SDev .0001 _0002 .0000 %RSD 14.10 9.050 4.612 f.5 Elem Avge SDev %RSD #1 #2 #3 Elem Avge SDev %RSD #1 #2 #3 .0007 .0005 .0007 2203/2 -.00162 .00111 68.726 -.00118 -.00080 -.00289 Sr .0002 .0001 23.96 .0003 .0002 .0002 .0024 .0022 .0020 2068/1 -.00382 .00289 75.670 -.00251 -.00182 -.00714 Ti .0003 .0000 4.124 .0003 .0003 .0003 .0005 .0005 .0005 2068/2 .00174 .00166 95.517 .00357 .00033 .00131 T11908 -.00298 .00061 20.509 -.00244 -.00286 -.00365 B .0009 .0000 4.646 .0010 .0009 .0009 Cu .0019 .0001 2.353 .0019 .0020 .0019 Na -.0159 .0005 2.837 -.0154 -.0162 -.0162 1960/1 -.00520 .00132 25.350 -.00501 -.00659 -.00398 v .0001 0001 114.5 .0001 .0000 .0000 Ba .0001 .0000 24.89 .0001 .0001 .0001 Fe .0001 .0000 33.29 .0001 .0001 .0000 Na .4367 .0276 6.310 .4123 .4666 .4312 1960/2 .00082 .00052 63.368 .00022 .00109 ..0 0116 Zn .0022 .0002 8.214 .0020 .0021 .0024 Be -.0009 .0000 2.447 -.0009 -.0009 -.0010 Fe .0701 .0003 .5019 .0703 .0703 .0697 Ni .0001 .0000 .1167 .0001 .0001 .0001 Si .0960 .0004 .4063 .0957 .0964 .0958 Ca .0053 .0001 1.587 .0052 .0053 .0054 K .0074 .0003 4.535 .0077 .0075 .0070 2203/1 .01000 .00152 15.170 .01000 .00848 .011.52 Sn .0044 .0006 14.66 .0038 .0051 .0043 Standardization Rpt. 09/15/06 01:50:50 PM page 1 P od: CLP1 Standard: StdFENAL 1,,,, Time: 09/15/06 13:45:46 Elem Fe Na Avge 32.66 34.53 SDev .12 .12 %RSD .3622 .3332 #1 32.54 34.44 #2 32.77 34.66 #3 32.67 34.47 Standardization Rpt. P od: CLP1 Standard: StdNAKH Time: 09/15/06 13:50:57 Elem K Na Avge 7.979 1.689 SDev .010 .002 %RSD .1272 .1383 #1 7.980 1.690 #2 7.969 1.687 #3 7.989 1.691 09/15/06 01:55:14 PM page 1 Standardization Report 09/15/06 01:55:14 PM page 1 P od: CLPI Slope = Conc.(SIR) /IR' Element Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGSBH StdBLANK 3266.22 12.4016 09/15/06 01:50:57 Al 308.215 StdICSH StdBLANK. 18.5410 -.097979 09/15/06 01:50:57 As1890 189.042 StdFURNH StdBLANK 1273.57 1.47999 09/15/06 09/15/06 01:50:57 01:50:57 B 249.678 StdMULTH StdBLANK StdBLANK 4.50044 1.10428 -.004197 -.000098 09/15/06 01:50:57 Ba Be 493.409 313.042 StdMULTH StdMULTH StdBLANK .987351 .000921 09/15/06 01:50:57 Ca 317.933 StdICSH StdBLANK 1.40489 -.002179 09/15/06 01:50:57 Cd 226.502 StdMULTH StdBLANK .117491 .000005 09/15/06 01:50:57 Co 228.616 StdMULTH StdBLANK 3.4,8468 -.000438 09/15/06 01:50:57 Cr 267.716 StdMULTH StdBLANK 2.62337 -.001107 09/15/06 01:50:57 Cu 324.754 StdMULTH StdBLANK 4.39299 -.008486 09/15/06 01:50:57 Fe 271.441 StdICSH StdBLANK 1.25492 -.000029 09/15/06 01:50:57 Fe 259.940 StdFENAL StdBLANK .153431 -.010755 09/15/06 01:50:57 K 766.491 StdNAKH StdBLANK 1.00294 -.000686 09/15/06 01:50:57 Mg 279.079 StdICSH StdBLANK 1.16912 -.000160 09/15/06 01:50:57 Mn 257.610 StdMULTH StdBLANK .374464 -.000831 09/15/06 01:50:57 Mo 202.030 StdMULTH. StdBLANK 3.70645 -.001811 09/15/06 01:50:57 Na 330.232 StdNAKH StdBLANK 1.18242 -.009785 09/15/06 01:50:57 Na 588.995 StdFENAL StdBLANK .146676 -.064058 09/15/06 01:50:57 Ni 231.604 StdMULTH StdBLANK 3.40331 -.000302 09/15/06 01:50:57 2203/1 220.351 StdFURNH StdBLANK 347.014 -3.47005 09/15/06 09/15/06 01:50:57 01:50:57 2203/2 220.352 StdFURNH StdBLANK StdBLANK 806.467 904.257 1.30774 3.45509 09/15/06 01:50:57 2068/1 8/2 206.831 206.832 StdAGSBH StdAGSBH StdBLANK 1438.06 -2.50002 09/15/06 01:50:57 0/1 196.021 StdFURNH StdBLANK 1642.51 8.53324 09/15/06 01:50:57 1960/2 196.022 StdFURNH StdBLANK 2298.93 -1.88948 09/15/06 09/15/06 01:50:57 01:50:57 Si 288.158 StdMULTH StdBLANK StdBLANK 3.95946 -.379969 -.003559 09/15/06 01:50:57 Sn 189.989 421.552 StdMULTH StdMULTH StdBLANK .810769 .556890 -.000136 09/15/06 01:50:57 Sr Ti 334.941 StdMULTH StdBLANK 3.19073 -.000968 09/15/06 01:50:57 T11908 190.864 StdFURNH StdBLANK 1466.24 4.37406 09/15/06 09/15/06 01:50:57 01:50:57 v 292.402 StdMULTH StdBLANK StdBLANK 5.12267 1.50265 -.000303 -.003270 09/15/06 01:50:57 Zn Pb2203 213.856 220.353 StdMULTH NONE NONE 1.00000 .000000 *NOT STANDARDIZED Sb2068 206.838 NONE NONE 1.00000 .000000 *NOT STANDARDIZED *NOT STANDARDIZED Se1960 196.026 NONE NONE 1.00000 .000000 tn O O N Standardization Readback N od: CLP1 Element Wavelength Standard Ag 328.068 StdBLANK StdAGSBH Element Wavelength Standard Al 308.215 StdBLANK StdICSH Element Wavelength Standard As1.890 189.042 StdBLANK StdFURNH Element Wavelength Standard B 249.678 StdBLANK StdMULTH Element Wavelength Standard Ba 493.409 StdBLANK StdMULTH ient Wavelength Standard .be 313.042 StdBLANK StdMULTH Element Wavelength Standard Ca 317.933 StdBLANK StdICSH Element Wavelength Standard Cd 226.502 StdBLANK StdMULTH Element Wavelength Standard Co 228.616 StdBLANK StdMULTH Element Wavelength Standard Cr 267.716 StdBLANK StdMULTH Element Wavelength Standard r 324.754 StdBLANK StdMULTH Report 09/15/06 01:55:14 PM Known Measured Concentration Concentration .000000 .000000 2000.00 2000.00 Known Measured Concentration Concentration .000000' .000000 500.000 500.000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00840 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00095 Known Measured Signal Signal .005266 .005299 57.6118 41.0096 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.99930 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00108 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.99875 page 1 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000031 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.008400 Residual Concentration .000000 .000000 Residual Concentration .000000 -.000950 Residual Signal -.000034 16.6023 Residual Concentration .000000 .000700 Residual Concentration .000000 .000000 Residual Concentration -.000000 -.001080 Residualp Concentration 0 .000000 .001245 [� Standardization Readback Report 09/15/06 01:55:14 PM F ent Wavelength Standard Fe 271.441 StdBLANK StdICSH Element Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard K 766.491 StdBLANK StdNAKH Element Wavelength Standard Mg 279.079 StdBLANK StdICSH Element Wavelength Standard Mn 257.610 StdBLANK StdMULTH F- tent Wavelength Standard T 202.030 StdBLANK StdMULTH Element Wavelength Standard Na 330.232 StdBLANK StdNAKH Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTH Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNH Element Wavelength Standard 2203/2 220.352 StdBLANK StdFURNH Known Signal :000055 .602976 Known Concentration .000000 5.00000 Known Signal .006759 8.00205 Known Signal . 000.584 ..62.6316 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal -.028601 1.98779 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 1000.00 Measured Signal .000067 .480512 Measured Concentration -.000000 5.00000 Measured Signal .007423 7.97927 Measured Signal .000637 53.5715 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00000 Measured Signal -.015913 1.68939 Measured Concentration .000000 5.00000 Measured Concentration .000000 4.99790 Measured Concentration -.000000 1000.00 Measured Concentration -.000000 1000.00 page 2 Residual Signal -.000012 .122465 Residual Concentration .000000 .000000 Residual Signal -.000665 .022779 Residual Signal -.000052 9.06009 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Signal -.012688 298394 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .002100 Residual Concentration .000000 .000000 Residual Concentration O .000000 C) -.000061 E-� Standardization Readback Report 09/15/06 01:55:14 PM Known Measured ____nent Wavelength Standard Concentration Concentration 2068/1 206.831 StdBLANK .000000 .00000.0 StdAGSBH 2000.00 2000.00 Element Wavelength Standard 2068/2 206.832 StdBLANK StdAGSBH Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNH Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNH Element Wavelength Standard Si 288.158 StdBLANK StdMULTH nent Wavelength Standard 189.989 StdBLANK StdMULTH Element Wavelength Standard Sr 421.552 StdBLANK StdMULTH Element Wavelength Standard Ti 334.941 StdBLANK StdMULTH Element Wavelength Standard T1.1908 190.864 StdBLANK StdFURNH Element Wavelength Standard V 292.402 StdBLANK StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 1000.00 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration .000000 1000.00 Measured Concentration -.000000 1000.000 Measured Concentration .000000 4.94713 Measured Concentration -.000000 4.99870 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00000 Measured Concentration -.000000 1000.00 Measured Concentration .000000 5.00000 Known Measured Element Wavelength Standard Concentration Concentration 9n 213.856 StdBLANK .000000 -.000000 StdMULTH 5.00000 5.00000 page 3 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000061 Residual Concentration -.000000 .052870 Residual Concentration .000000 .001300 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 00 .000000 Residual Concentrationp .000000 .000000 Standardization Readback Report 09/15/06 01:55:14 PM ]____lent Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard Sb2068 206.838 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Analysis Report 09/15/06 02:02:45 PM page 1 D od: CLP1 Sample Name: ICV Operator: CD Time: 09/15/06 13:55:20 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm Ppm Ppm Avge 998.81 49.43 509.93 2.569 2.565 2.549 48.72 SDev 2.43 .23 1.43 .012 .007 .004 .09 %RSD .24297 .4663 .28137 .4840 .2706 .1671 .1916 ##1 997.73 49.33 510.12 2.559 2.563 2.549 48.70 ##2 997.11 49.27 508.40 2.564 2.558 2.544 48.63 #3 1001.6 49.70 511.25 2.583 2.572 2.553 48.82 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K. Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.526 2.494 2.527 2.582 49.96 85.52 51.09 SDev .005 .006 .006 .011 .09 .44 .16 %RSD .2013 .2334 .2412 .4420 .1806 .5092 .3217 #1 2.530 2.490 2.525 2.575 49.99 85.27 51.01 2.520 2.491 2.522 2.575 49.86 85.27 50.99 2.529 2.501 2.533 2.595 50.04 86.02 51.28 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.492 2.573 84.03 2.493 501.00 489.72 982.72 SDev .005 ..008 .55 .007 .75 2.14 11.35 %RSD .2004 .2977 .6575 .2806 .14915 .43752 1.1553 2.491 2.567 83.64 2.498 500.99 492.19 969.74 _#1 #2 2.488 2.570 83.79 2.485 500.26 488.38 987.67 ##3 2.498 2.582 84.67 2.495 501.76 488.59 990.77 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 196.0/2 Si Sn Sr Ti Units ppb ppb Ppb Ppm Ppm Ppm Ppm Avge 981.65 513.29 508.86 2.840 2.499 2.529 2.601 SDev 6.58 4.10 4.61 .084 .008 .007 .011 0-oRSD .67027 .79850 .90508 2.957 .3213 .2580 .4195 977.50 510.95 503.60 2.764 2.495 2.526 2.614 978.22 510.89 512.15 2.826 2.494 2.523 2.593 #3 989.24 518.02 510.84 2.930 2.509 2.536 2.597 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 02:02:45 PM �h Low Elem T1'1908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 501.39 2.516 2.584 493.48 982.01 510.34 SDev 4.38 .006 .007 1.46 7.44 3.79 %RSD .87303 .2324 .2770 .29564 .75738 .74238 #1 498.83 2.514 2.581 495.12 974.92 506.05 #2 498.90 2.511 2.579 492.33 981.37 511.73 #3 506.45 2.523 2.592 492.98 989.75 513.23 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 09/15/06 02:10:15 PM page 1 od: CLP1 Sample Name: ICVL Operator: CD Time: 09/15/06 14:02:51 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890. B Ba Be Ca Units ppb Ppm PPbPPm ppm Ppm PPm Avge .57926 .0081 1.1125 .0031 .0004 .0004 -.0005 SDev .55852 .0044 2.3851 .0016 .0002 .0002 .0028 %RSD 96.420 54.83 214.39 51.34 43.28 36.11 563.8 #1 1.1776 .0126 .03056 .0046 .0006 .0006 .0021 #2 .48864 .0080 -.53989 .0034 .0004 .0005 -.0002 #3 .07159 .0037 3.8468 .0014 .0002 .0003 -.0034 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0000 .0002 .0004 2.502 .0435 .0063 SDev .0003 .0001 .0003 .0001 .009 .0134 .0044 %RSD 61.23 362.5 171.6 42.67 .3638 30.80 70.08 #1 .0009 .0001 .0005 .0004 2.491 .0543 .0104 0006 .0001 _0002 .0005 2.508 .0475 .0067 .0002 -.0001 -.0001 .0002 2.506 .0285 .0017 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb- ppb ppb Avge -.0003 .0059 2.549 .0007 .05697 -.33797 7.0656 SDev .0002 .0029 .011 .0004 1.1921 .78431 4.2575 %RSD 62.22 49.37 .4430 63.34 2092.5 232.07 60.257 #1 -.0001 .0091 2.538 .0011" -.36254 -1.0071 11.960 #2 -.0003 .0051 2.560 .0005 -.86869 .52513 5.01.37 #3 -.0005 .0035 2.548 .0004 1.4021 -.53196 4.2226 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.1897 3.3538 2.5863 .0914 -.0004 .0004 .0004 SDev .9547 .0410 1.0327 .0220 .0004 .0002 .0003 %RSD 29.930 1.2237 39.929 24.04 116.7 43.87 71.98 2.8165 3.3982 2.4427 .1143 -.0002 .0005 .0008 is 4.2745 3.3458 3.6833 .0893 -.0000 .0004 .0004 #3 2.4779 3.3174 1.6330 .0706 -.0008 .0002 .0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK N O O H Analysis Report 09/15/06 02:10:15 PM _�h Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.3193 .0003 .0014 -.20641 4.4804 2.8418 SDev .6324 .0006 .0002 .50813 1.4017 .6921 %RSD 47.934 192.4 13.02 246.18 31.286 24.353 #1 1.0394 .0004 .0016 -.79240 5.8615 2.7609 #2 2.0434 .0009 .0014 .06104 4.5207 3.5708 #3 .87521 -.0004 .0012 .11214 3.0589 2.1938 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low page 2 Analysis Report 09/15/06 02:17:46 PM page 1 1 iod: CLP1 Sample Name: ICB Operator: CD Time: 09/15/06 14:10:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .00385 .0029 .60569 -.0000 .0001 .0001 -.0059 SDev .33721 .0038 .63902 .0002 .0000 .0000 .0008 %RSD 8767.3 129.8 105.50 1721. 34.48 20.86 13.60 #1 .22660 .0073 1.0558 .0001 .0000 .0001 -.0068 #2 -.38411 .0008 -.12573 -.0002 .0001 .0001 -.0052 #3 .16904 .0006 .88698 .0001 .0001 .0001 -.0056 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 -.0001 -.0000 .0000 -.0042 .0300 .0008 SDev .0000 .0001 .0000 .0001 .0005 .0014 .0024 %RSD 19.80 59.37 82.44 150.9 12.65 4.480 298.6 #1 .0002 -.0001 -.0001 .0001 -.0038 .0315 .0035 �^ .0003 -.0001 -.0001 -.0000 -.0040 .0297 -.0002 .0002 -.0002 -.0000 .0001 =.0048 .0289 -.0009 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0001 .0008 -.0086 .0004 .67331 .32706 2.7305 SDev .0000 .0001 .0005 .0003 .50811 .27992 1.0531 %RSD 62.83 5.710 5.999 96.66 75.464 85.5.86 38.568 #1 -.0001 .0008 -.0086 .0004 .70042 .57694 3.3988 #2 -.0001 .0008 -.0081 .0007 .15219 .02457 1.5166 #3 -.0000 .0009 -.0092 -.0000 1.1673 .37968 3.2762 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si 'Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.7052 .32227 -.07179 .0291 -.0008 .0001 .0002 SDev 2.7954 1.5694 1.02837 .0032 .0017 .0000 .0001 %RSD 163.94 486.96 1432.6 11.15 201.5 23.09 87.41 -2.1483 2.0825 1.0180 .0328 -.0002 .0001 .0002 1.2854 -.18505 -1.0251 .0278 .0004 .0001 .0000 #3 -4.2525 -.93066 -.20825 .0266 -.0028 .0001 .0003 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 7t O O E-� Analysis Report 0.9/15/06 02:17:46 PM 3h Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge _16247 .0002 .0006 .44241 -.22805 .05946 SDev 2.7046 .0002 .0001 .32524 1.55518 1.1468 %RSD 1664.7 150.6 16.23 73.515 681.94 1928.7 #1 .98898 .0004 .0008 .61810 -.30110 1.3725 #2 -2.8590 -.0001 .0006 .06711 1.3624 -.74535 #3 2.3574 .0002 .0006 .64201 -1.7454 -.44879 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 kn O O C/1 LE9'TT llS"8TT LOEL'9 8£Ti0' 0£OT' T90'EZ F ZL9'OT T£'9TT E809'S £E:H 9ZOT' EZfii'ZZ: Z# L8L'OT SE'OTT LOT6'9 8£:�0 TEOT' ZET'8T T# 09LL OT89'E 866'OT S8T9' L8ZZ' 6E9'ZT QSd% LZS' i�Z'i� LSOL' E000' 2000' 089'Z AaQS Z£0'TT LO'STI 99T:V'9 LEVO' 6ZOT' SOZ'TZ aDBAV qdd qdd qdd iuudd wdd qdd SgTun, 096TGS 890ZgS EOZZgd uZ A 806TTL waTg :VTTZ' 0000'- T8LO' O:DLT' Ev9'OT LZ9'ET SZ'LTT £# 80TZ' 0000'- 86LO' LILT' 089'TT EZS9'8 6L'9TT Z# SZTZ' 0000'- TLLO' S89T' LE:i'ZT LT8:i'L 0O'OTT T# T:iOtv' Z6' 6fiV 06L' T Tv09' T SILL' L 068' ZE :�T:VS' E QS'd% 6000' 0000' 'vT00' LZ00' T06' 8Z9Z'E 90'v AaQS 9TTZ' 0000'- E8LO' :VTLT' L8S'TT ZOZ6'6 89'7vTT a5AV wdd wdd wdd wdd qdd qdd qdd SgTun. TZ as us TS Z/096T T/096T Z/8902 waTs ET'TZT OE8T'8 LTZ8'E 9E80' OOTO'- OOZO' LOEO' £# 9E'STT 6LT8'S :�88T'S EE80' S800'- b6T0' SOEO' Z# 90'TTT i,88L'L SZST'S 8E80' 0600'- 96T0' LOEO' T# 6Z9E' V H, , * LT 66V' 9T L98Z' 89L,8 Z9�,' T 86SE' QS'd% SO'S OL9Z'T 68LL' 2000' 8000' E000' T000' narFQ S8'STT TE9Z'L 60ZL—V 9E80' Z600'- L6T0' 90E0' ;DE qdd qdd qdd wdd wdd wdd wdd s -4T T/890Z Z/EOZZ T/EOZZ TN pN ON uW waTH LZ00'- 6TZ0' 8L00'- 9ZS0' ivOZO' SZOT' 90T0' E# OE00'- ZZZO' 9L00'- TZSO' 9020' 6TOT' LOTO' Z# TZ00'- PTZO' 8L00'- SZSO' SOZO' 9ZOT' FOTO' T# OL' 8T :i98' T TSS' T LL9T7' L8Z'i' vIV9E' Z98' T QS2i% S000' il000' T000' E000' T000' iv000' 2000' AaQS 9Z00'- 8TZO' LL00'- iVZSO' SOZO' TvZOT' 90TO' abnV wdd wdd wdd wdd wdd wdd wdd s-4Tun gW x a3 n0 z0 00 PO waTg :VOTO'- 90T0' 0000'- 9LOZ' 09T'TZ 8S00' T0:�'OZ E# EOTO'- SOTO' 0000' t90Z' 80t'61 E900' 90£'OZ Z# 9TT0'- 90T0' 0000'- 6LOZ' TE9'6T 9iv00' LSZ'OZ T# E08'9 :VS99' 69'98 LIVSE' 6TSL'TV 6T'9T L809E' QS2I% L000' T000' 0000' 8000' 'vS6' 6000' ELO' AaQS 80T0'- 90TO' 0000'- ELOZ' 990'OZ 9S00' TZE'OZ @BAV wdd wdd wdd wdd qdd wdd qdd S:lTun PO g El 068TSV TV 5V W;DTH T :aogopa •aao0 ON00 :@POW :-quawwo0 TS:LT::VT 90/ST/60 :awry -_-. QO :aogpaad0 II2d0 :awpN aTdwps TdZa =Pot [ T a5 -2d Wd 9T:SZ:ZO 90/ST/60 �aoda� sTs�iTpu� Analysis Report 09/15/06 02:32:46 PM page 1 iod: CLP1 Sample Name: ICSAI Operator: CD Time: 09/15/06 14:25:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .58140 497.1 9.7059 .0196 .0011 .0003 489.5 SDev .60819 6.3 2.5416 .0006 .0000 .0000 7.2 %RSD 104.61 1.275 26.186 3.209 2.582 5.881 1.466 #1 1.2183 502.5 10.418 .0201 .0012 .0003 495.3 #2 .00676 498.6 11.815 .0199 .0011 .0003 491.7 #3 .51909 490.1 6.8840 .0189 .0011 .0003 481.5 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .00.50 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0045 -.0003 .0063 -.0006 199.6 .0402 489.7 SDev .0001 .0006 .0005 .0003 3.0 .0039 5.7 %RSD 1.680 212.0 8.419 41.48 1.493 9.637 1.172 #1 -.0045 .0004 .0067 -.0005 202.1 .0417 494.3 "- -.0045 -.0005 .0065 -.0005 200.4 .0431 491.4 -.0046 -.000.8 .0057 -.0010 196.3 .0358 483.2 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0059 -.0054 .0250 .0036 1.8540 -1.0369 .18188 SDev .0004 .0003 .0015 .0000 4.6479 4.0824 4.0055 %RSD 6.225 6.289 5.953 1.244 250.70 393.73 2202.3 #1 -.0062 -.0050 .0265 .0036 6.8382 -4.7640 -4.2328 #2 -.0055 -.0056 .0249 .0036 1.0856 -1.6727 1.1946 #3 -.0060 -.0056 .0235 .0036 -2.3619 3.3262 3.5838 Errors LC Pass NOCHECK NOCHECK LC Pass -NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 6.7044 -2.9340 -3.6064 .0374 .0398 -.3162 .0023 SDev 9.3432 10.2393 3.2534 .0081 .0024 .0037 .0001 %RSD 139.36 348.99 90.211 21.70 6.064 1.185 4.148 17.489 8.8602 -3.5298 .0446 .0416 -.3200 .0024 1.5726 -8.1130 -6.8974 .0391 .0408 -.3161 .0022 #3 1.0518_ -9.5493 -.39197 .0286 .0371 -.3125 .0023 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 02:32:46 PM �h Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge L-13.472 -.0001 -.0025 -.07417 4.5324 -3.3825 SDev 5.380 .0004 .0002 1.30650 4.9614 3.9495 %RSD 39.935 343.2 6.905 1761.5 109.47 116.76 #1 -7.2620 -.0006 -.0026 -.90045 10.255 .59609 #2 L-16.435 -.0002 -.0024 -.75414 1.4467 L-7.3021 #3 L-16.719 .0003 -.0023 1.4321 1.8950 -3.4413 Errors LC Low LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5'.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 00 O O Analysis Report 09/15/06 02:40:16 PM page 1 zod: CLP1 Sample Name: ICSABI Operator: CD Time: 09/15/06 14:32:52 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 952.85 500.2 1036.1 1.059 .4823 .4615 495.0 SDev 2.93 1.7 1.8 .001 .0012 .0009 1.2 %RSD .30800 .3301 .17753 .0771 .2424 .2022 .2333 #1 955.99 502.0 1037.3 1.060, .4837 .4625 496.2 #2 952.39 499.9 1037.2 1.060 .4818 .4612 494.9 #3 950.18 498.8 1034.0 1.058 .4815 .4607 493.9 .Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm, ppm ppm Avge .8708 .4308 .4558 .5021 201.9 .0345 494.7 SDev .0030 .0006 .0010 .0007 .6 .0021 1.3 %RSD .3452 .1362 .2134 .1376 .3021 5.968 .2640 #1 .8737 .4313 .4568 .5026 202.5 .0352 496.2 "- .8711 .4308 .4558 .5023 201.8 .0362 494.2 .8677 .4302 .4549 .5013 201.3 .0322 493.7 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .4377 1.02.8 .0104 .86.33 882.57 867.37 -8.4267 SDev .0007 .002 .0004 .0060 2.01 2.96 2.0447 %RSD .1522 .2260 4.249 .6889 .22819 .34101 24.264 #1 .4384 1.031 .0110 .8698 883.72 868.51 -7.5620 #2 .4377 1.026 .0102 .8580 883.75 864.01 -10.762 #3 .4370 1.027 .0102 .8622 880.25 869.58 -6.95.65 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb -ppm ppm ppm ppm Avge -5.5674 996.69 993.14 ..7291 1.061 -.3184 .0016 SDev 1.8791 1.63 2.38 .0025 .001 .0009 .0001 %RSD 33.752 .16395 .24011 .3487 .1379 .2950 7.401 -7.4373 998.01 990.48 .7262 1.063 -.3191 .0017 -3.6792 994.86 995.08 .7307 1.061 -.3186 .0017 #3 -5..5856 997.20 993.86. .7305 1.061 -.3173 .0015 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 02:40:16 PM Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 981.84- .4522 .9517 872.43 -6.5195 994.32 SDev 2.19 .0004 .0016 1.61 .8308 1.16 %RSD .22317 .0994 .1734 .18508 12.743 .11646 ##1 979.39 .4526 .9535 873.57 -7.4788 992.99 ##2 982.55 .4523 .9512 870.58 -6.0377 995.01 ##3 983.60 .4517 .9503 873.13 -6.0421 994.98 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 Analysis Report 09/15/06 02:47:47 PM page 1 ,iod: CLP1 Sample Name: CCV1. Operator: CD Time: 09/15/06 14:40:22 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1005.9 49.80 515.79 2.584 2.575 2.562 49.04 SDev 7.2 .32 5.25 .025 .019 .021 .35 %RSD .71719 .6346 1.0183 .9689 .7256 .8063 .7079 #1 1000.4 49.60 510.08 2.561 2.560 2.544 48.76 #2 1003.2 49.64 516.85 2.581 2.569 2.557 48.94 #3 1014.0 50.16 520.42 2.611 2.596 2.585 49.43 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.545 2.506 2.542 2.596 50.33 86.02 51.60 SDev .017 .022 .019 .021 .39 .54 .36 %RSD .6648 .8764 .7576 .7931 .7744 .6295 .7023 #1 2.531 2.486 2.526 2.579 50.03 85.70 51.29 "- 2.540 2.503 2.537 2.590 50.19 85.72 51.51 2.563 2.530 2.564 2.619 50.77 86.65 52.00 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.508 2.593 84.83 2.510 499.97 491.07 986.42 SDev .020 .025 .48 .017 4.12 2.75 16.42 %RSD .7805 .9467 .5616 .6798 .82333 .55985 1.6646 #1 2.491 2.571 84.45 2.498 497.24 487.89 967.59 #2 2.503 2.588 84.68 2.503 497.96 492.52 997.80 #3 2.529 2.620 85.36 2.530 504.70 492.78 993.86 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 987.20 515.58 515.80 2.863 2.512 2.536 2.624 SDev 10.47 6.67 4.91 .078 .019 .020 .018 %RSD 1.0605 1.2931 .95127 2.739 .7577 .7858 .6934 O O 977.95 510.95 510.13 2.783 2.494 2.520 2.615 985.09 512.57 518.78 2.867 2.511 2.531 2.612 #3 998.57 523.22 518.47 2.940 2.532 2.558 2.645 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 02:47:47 PM Low Elem 511908 v - Zn Pb2203 -Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 505.65 2.529 2.601 494.03 986.94 515.72 SDev 3.51 .020 .021 2.88 11.44 4.90 0-oRSD .69479 .7853 .8234 .58376 1.1588 .95030 #1 502.69 2.511 2.583 491.01 974.50 510.40 #2 504.73 2.524 2.596 494.34 989.32 516.71 #3 509.53 2.550 2.625 496.75 997.00 520.05 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report iod: CLP1 Sample Name: CCVL1 ..��. Time: 09/15/06 14:47:53 Ca Comment: ppm ppm ppm Mode: CONC Corr. Factor: 1 .0006 Elem Ag Al As1890 Units ppb ppm ppb Avge .46235 .0521 .84783 SDev .01764 .0185 .91327 %RSD 3.8156 35.44 107.72 #1 .47967 .068.8 1.3040 #2 .44440 .0552 -.20366 #3 .46299 .0323 1.4432 Errors NOCHECK NOCHECK NOCHECK High ppm ppb ppb Low .0003 -.51701 1.4335 Elem Cd Co Cr Units ppm ppm ppm Avge .0007 .0002 .0003 SDev .0003 .0003 .0000 %RSD 47.42 149.1 10.45 #1 .0008 .0004 .0003 NOCHECK .0008 -.0001 .0003 .0003 .0002 .0003 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge -.0002 .0060 2.535 SDev .0002 .0032 .013 %RSD 98.72 53.88 .5100 #1 -.0000 .0094 2.548 #2 -.0001 .0056 2.522 #3 -.0003 .0030 2.536 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 1.8529 1.8681 1.7317 SDev 3.8813 2.1855 3.0565 %RSD 209.48 116.99 176.50 5.8725 4.3792 5.2379 _ 1.5594 .39565 .32796 #3 -1.8734 .82951 -.37077 Errors NOCHECK NOCHECK NOCHECK 09/15/06 02:55:17 PM page 1 Operator: CD B Ba Be Ca ppm ppm ppm ppm .0033 .0005 .0006 .0406 .0018 .0002 .0003 .0206 55.75 33.64 45.12 50.61 .0053 .0007 .0008 .0606 .0026 .0005 .0006 .0418 .0019 .0004 .0003 .0195 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg ppm ppm ppm ppm .0003 2.495 .0383 .0503 .0004 .010 .0063 .0198 138.0 .4095 16.47 39.49 .0007 2.507 .0454 .0701 -.0000 2.488 .0360 .0503 .0001 2.489 .0334 .0304 NOCHECK LC Pass NOCHECK NOCHECK 2.7.50 2.250 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0003 -.51701 1.4335 7.6192 .0002 .37067 1.0265 2.3276 65.61 71.694 71.605 30.549 .0003 -.09344 2.1224 9.5450 .0006 -.78202 1.9243 8.2798 .0001 -.67559 .25378 5.0327 NOCHECK NOCHECK NOCHECK NOCHECK SiSn Sr Ti ppm ppm ppm ppm .0868 .0000 .0004 .0005 .0220 .0015 .0002 .0002 25.31 3483. 41.81 41.57 .1105 .0010 .0006 .0007 .0827 -.0016 .0004 .0005 .0672 .0008 .0002 .0003 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 02:55:17 PM page 2 Jh Zn Low Sb2068 Elem T11908 Units ppb Avge 1.6461 SDev 1.7488 %RSD 106.24 #1 .211.26 #2 3.5941 #3 1.1329 Errors NOCHECK High 88.380 Low .0005 V Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0006 .0012 .78402 3.7731 1.7771 .0003 .0003 .74930 3.3346 2.7541 48.07 23.31 95.572 88.380 154.98 .0005 .0015 1.3846 7.0955 4.9519 .0009 .0011 1.0231 3.7973 .35053 .0003 .0010 -.05566 .42637 .02894 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report iod: CLP1 Sample Name: CCBl Time: 09/15/06 14:55:23 Be Comment: ppm ppm Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .32634 .0148 .89766 SDev .15675 .0066 1.7159 %RSD 48.032 44.32 191.15 #1 .29021 .0078 2.8768 #2 .49801 .0208 -.01120 #3 .19082 .0158 -.17261 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge .0002 -.0002 .0001 SDev .0001 .0002 .0001 %RSD 46.00 100.1 73.32 #1 .0001 -.0003 .0002 51.04 .0003 -.0004 .0001 .0273 .0002 .0000 .0000 Errors LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem Mn Mo Na Units ppm ppm ppm Avge -.0001 .0009 -.0104 SDev .0000 .0004 .0020 %RSD 16.63 47.18 18.99 41 -.0001 .0011 -.0126 #2 -.0001 .0011 -.0087 #3 -.0001 .0004 -.0100 Errors LC Pass NOCHECK LC Pass High .0150 -1.6378 5.000 Low -.0150 .0007 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge .99122 -.90698 .94192 SDev .18580 2.81927 1.4237 %RSD 18.745 310..84 151.15 .84365 -3.9362 .73350 Sn .93013 1.6402 -.36611 #3 1.1999 -.42490 2.4584 Errors NOCHECK NOCHECK NOCHECK 09/15/06 03:02:48 PM page 1 Operator: CD B Ba Be Ca ppm ppm ppm ppm .0007 .0001 .0001 .0038 .0004 .0000 .0000 .0068 60.49 42.67 8.078 178.2 .0004 .0000 .0001 -.0040 .0012 .0001 .0001 .0087 .0005 .0001 .0001 .0068 LC Pass LC Pass LC Pass LC Pass .2000 .2000 .0050 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K Mg ppm ppm ppm ppm -.0001 .0000 .0260 .0099 .0002 .0029 -.0015 .0050 153.4 49670. 5.888 51.04 -.0001 -.0032 .0273 .0041 .0001 .0022 .0243 .0129 -.0004 .0011 .0262 .0128 LC Pass LC Pass LC Pass LC Pass .0250 .1000 5.000 .2000 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0003 -.51252 1.3462 2.4565 .0004 1.36983 .7109 2.3213 111.1 267.27 52.808 94.496 -.0001 -1.6378 1.3106 5.1223 .0007 1.0128 .65376 .88161 .0004 -.91252 2.0742 1.3656 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti ppm ppm ppm ppm .0254 -.0000 .0001 .0001 .0039 .0015 .0000 .0001 15.44 4347. 27.89 169.2 O O .0238 .0013 .0000 .0002 .0298 -.0017 .0001 -.0001 H .0225 .0003 .0001 .0001 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 03:02:48 PM jh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.53038 .0001 .0007 .72729 1.4792 .32625 SDev .31948 .0004 .0001 .37754 .7045 1.1601 %RSD 60.237 328.5 12.56 51.910 47.627 355.59 #1 -.45319 .0003 .0006 .32883 2.2685 -.82151 #2 -.25656 .0004 .0007 .77336 .91399 .30198 #3 -.88138 -.0003 .0007 1.0797 1.2551 1.4983 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3..0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 09/15/06 03:10:19 PM page 1 I iod: CLP1 Sample Name: MB -18255 Operator: CD ku,.i Time: 09/15/06 15:02:54 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .14182 .0041 -.86231 -.0008 -.0000 -.0000 -.0108 SDev .14131 .0011 .61410 .0005 .0000 .0001 .0008 %RSD 99.641 26.35 71.215 64.92 175.6 3715. 7.043 #1 .30331 .0052 -1.5714 -.0003 -.0000 .0001 -.0117 ##2 .04089 .0031 -.50518 -.0007 -.0000 -.0001 -.0107 ##3 .08125 .0038 -.51035 -.0013 .0000 .0000 -.0101 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm. ppm ppm Avge -.0002 -.0006 .0001 -.0003 -.0051 .0198 -..0010 SDev .0002 .0001 .0003 .0002 .0002 .0016 .0029 %RSD 92.88 20.92 257.1 59.69 4.816 7.870 297.9 #1 .0.000 -.0006 .0003 -.0001 -.0048 .0216 .0023 -.0003 -.0004 .0002 -.0005 -.0053 .0188 -.0027 -.0002 -.0007 -.0002 -.0003 -.0052 .0190 -.0025 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0004 .0001 -.0102 -.0002 1.8642 .43054 1.5547 SDev .0001 .0010 .0003 .0003 .8504 .93325 1.7530 %RSD 23.48 1682. 3.217 178.6 45.617 216.76 112.75 ##1 -.0003 .0011 -.0099 -.0001 .88482 .97060 3.5788 ##2 -.0004 -.0003 -.0105 .0001 2.2921 -.64708 .55450 #3 -.0004 -.0007 -.0103 -.0005 2-.4156 .96809 .53076 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.35550 -4.5537 1.8282 -.0370 .0016 -.0001 .0007 SDev .62496 2.4298 1.4855 .0042 .0010 .0000 .0000 %RSD 175.80 53.360 81.255 11.25 64.70 28.61 5.264 -.49254 -5.1287 1.1191 -.0413 .0004 -.0000 .0007 -.90058 -1.8879 3.5354 -.0367 .0025 -.0001 .0007 Tt� ##3 .32660 -6.6444 .83019 -.0330 .0019 -.0001 .0007 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 03:10:19 PM page 2 00 O O H Low o Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.51123 .0002 .0018 .90798 .28061 -.29692 SDev .67796 .0006 .0001 56001 .64720 1.78923 %RSD 132.61 294.8 4.372, 61.676 230.64 602.60 #1 -1.2222 .0008 .0018 .94208 .86324 -.96142 #2 .12802 -.0002 .0018 .33170 -.41602 1.7295 #3 -.43952 -.0001 .0017 1.4502 .39461 -1.6588 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200' 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 00 O O H Analysis Report 09/15/06 03:17:49 PM page 1 od: CLP1 Sample Name: LCS-18255 Operator: CD Time: 09/15/06 15:10:24 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 996.31 49.94 512.10 H3.231 2.599 2.582 49.01 SDev 2.48 .11 1.39 .007 .007 .006 .14 %RSD .24888 .2221 .27114 .2052 .2610 .2379 .2802 #1 998.14 50.04 513.17 H3.233 2.605 2.586 49.11 #2 993.49 49.82 512.60 H3.224 2.591 2.575 48.85 #3 997.29 49.95 510.53 H3.236 2.600 2.584 49.07 Errors LC Pass LC Pass LC Pass LC High LC Pass LC Pass LC Pass High 1200.0 60.00 600.00 3.000 3.000 3.000 60.00 Low 800.00 40.00 400.00 2.000 2.000 2.000 40.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.562 2.525 2.562 2.622 50.39 86.97 51.44 SDev .009 .007 .007 .004 .16 .16 .11 %RSD .3464 .2609 .2747 .1622 .3272 ..1858 .2107 #1 2.571 2.529 2.568 2.624 50.55 87.09 51.51 2.554 2.517 2.554 2.617 50.22 86.78 51.32 46 2.561 2.528 2.564 2.624 50.42 87.03 51.50 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 3.000 3.000 3.000 3.000 60.00 96.00 60.00 Low 2.000 2.000 2.000 2.000 40.00 64.00 40.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb - Avge 2.529 2.616 86.19 2.529 499.18 488.18 994.78 SDev .007 .004 .10 .008 3.30 .47 1.39 %RSD .2679 .1509 .1218 .3313 .66171 .09611 .14008 #1 2.535 2.617 86.22 2.538 500.47 488.69 995.20 #2 2.522 2.611 86.07 2.522 495.43 488.09 993.23 #3 2.532 2.619 86.27 2.527 501.65 487.77 995.92 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 3.000 96.00 3.000 Low 2.000 64.00 2.000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 992.57 513.18 510.19 6.478 2.534 2.560 2.653 SDev 2.40 2.99 2.47 .034 .004 .005 .020 %RSD .24139 .58177 .48390 .5223 .1472 .2140 .7352 0 994.95 513.81 510.00 6.469 2.538 2.564 2.674 990.16 515.81 507.82 6.450 2.531 2.554 2.635 #3 992.60 509.94 512.75 6.516 2.534 2.562 2.650 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 03:17:49 PM -�-jh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 498.27 2.549 2.623 491.85 993.31 511.19 SDev 1.14 .005 .006 1.14 1.96 .67 %RSD .22788 .2117 .2358 .23205 .19693 .13091 #1 498.84 2.553 2.629 492.62 995.03 511.27 ##2 496.97 2.543 2.617 490.54 991.18 510.48 #3 499.02 2.551 2.625 492.39 993.70 511.81 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 600.00 3.000 3.000 600.00 1200.0 600.00 Low 400.00 2.000 2.000 400.00 800.00 400.00 page 2 O 00 O O Analysis Report 09/15/06 03:25:20 PM page 1 ] Lod: CLP1 Sample Name: 0609809-001E Operator: CD Time: 09/15/06 15:17:55 Comment: 6 Cf�,-- Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .11645 .0170 -.35944, .0042 .0006 .0004 .0850 SDev .12932 .0026 .48531 .0011 .0002 .0002 .0023 %RSD 111.05 15.36 135.02 26.41 30.83 39.85 2.657 ##1 .26571 .0199 .08851 .0054 .0007 .0006 .0873 #2 .04581 .0161 -.29181 .0035 .0005 .0004 .0847 #3 .03784 .0150 -.87502 .0035 .0004 .0003 .0829 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0004 .0000 .0004 .0841 .0088 .5992 .0083 SDev .0001 .0001 .0002 .0005 .0033 .0059 .0050 %RSD 17.22 272.3 55.72 .5808 37.95 .9772 60.32 #1 .0005 -.0001 .0007 .0846 .0124 .6059 .0134 #2 .0004 .0002 .0002 .0838 .0082 .5952 .0083 #3 .0003 .0000 .0004 .0838 .0058 .5964 .0033 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb 4e .0002 .0060 .0538 .0008 2.1881 2.1204 1.7439 SDev .0002 .0028 .0056 .0003 .8767 1.8603 1.6294 %RSD 97.08 47.28 10.36 32.14 40.068 87.732 93.435 #1 .0004 .0092 .0598 .0011. 3.1568 3.5312 3.6245 #2 .0002 .0047 .0528 .0007 1.4489 2.8180 .85322 #3 .0000 .0040 .0488 .0007 1.9586 .01218 .75395 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb Ppm ppm Ppm Ppm Avge .74288 -.88305 2.0354 -.0761 -.0004 .0003 .0015 SDev 1.3014 2.23319 1.2422 .0238 .0017 .0002 .0003 %RSD 175.19 252.89 61.031 31.23 414.1 61.08 18.52 #1 1.9440 .18428 3.3360 -.0507 .0014 .0005 .0018 #2 -.63981 -3.4496 1.9090 -.0800 -.0019 .0003. .0015 #3 .92442 .61619 .86122 -.0978 -.0007 .0001 .0013 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .41940 .0005 .0594 2.1430 1.0762 1.0636 SDev 1.2851 .0002 .0002 1.3861 1.3354 1.1086 %RSD 306.40 40.67 .3557 64.681 124.08 104.23 #1 1.6874 .0006 .0597 3.4065 2.5036 2.2865 -.88210 .0003 .0593 2.3621 -.14261 .12458 .45296 .0006 .0593 .66040 .86768 .77965 i Analysis Report 09/15/06 03:32:50 PM P god: CLP1 Sample Name: 0609809-002E Operator: CD kun Time: 09/15/06 15:25:25 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .24507 .1339 .41835 .0140 .0374 .0001 SDev .19249 .0015 .90739 .0005 .0002 .0000 %RSD 78.545 1.144 216.90 3.789 .4565 19.76 ##1 .24591 .1350 1.2076 .0134 .0373 .0001 ##2 .05216 .1322 -.57307 .0142 .0373 .0001 #3 .43713 .1346 .62049 .0144 .0376 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0002 -.0005 .0018 .0008 .1389 2.261 SDev .0001 .0002 .0001 .0000 .0006 .008 %RSD 40.61 49.8-4 3.118 1.991 .4708 .3613 #1 .0004 -.0006 .0017 .0008 .1394 2.260 #2 .0002 -.0002 .0018 .0008 .1382 2.254 #3 .0002 -.0007 .0018 .0009 .1392 2.270 Elem Mn Mo Na Ni 2203/1 2203/2 Lts ppm ppm ppm ppm ppb ppb 3e .0066 .0009 20.15 .0011 .90268 1.3628 SDev .0001 .0009 .09 .0009 1.1857 1.9903 %RSD .9933 96.40 .4390 79.01 131.35 146.04 #1 .0066 .0020 20.08 .0001 .95133 2.2481 #2 .0066 .0005 20.14 .0013 -.30660 2.7569 ##3 .0067 .0004 20.25 .0019 2.0633 -.91650 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge -.56629 -2.5396 1.6793 6.148 -.0006 .0984 SDev 1.26321 1.5846 2.0854 .021 .0007 .0003 %RSD 223.07 62.395 124.18 .3360 116.7 .3366 #1 -.58864 -3.0161 .92650 6.141 -.0009 .0982 #2 -1.8182 -.77145 4.0365 6.131 .0002 .0982 #3 .70795 -3.8312 .07478 6.171 -.0011 .0988 Elem T11908 v Zn Pb2203 Sb20.68 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .13413 .0012 .0164 1.2097 .47227 .27441 SDev .47302 .0001 .0002 .9827 .66765 1.9181 %RSD 352.66 10.77 1.243 81.239 141.37 698.98 ##1 .68024 .0012 .0162 1.8163 .47262 -.38638 - -.14678 .0011 .0162 1.7368 -.19556 2.4355 -.13108 .0014 .0166 .07584 1.1397 -1.2259 page 1 Ca ppm 28.37 .13 .4625 28.29 28.30 28.52 Mg ppm 13.78 .06 .4349 13.74 13.75- 13.85 2068/1 ppb 2.5524 .5265 20.626 2.5983 3.0545 2.0045 Ti ppm .0073 .0002 2.553 .0076 .0072 .0073 N 00 O O CJ H Analysis Report 09/15/06 03:40:20 PM 1 od: CLP1 Sample Name: 0609809-003E Operator: CD 1_-., Time: 09/15/06 15:32:56 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .16569 .0881 .62695 .0215 .0724 .0001 SDev .34235 .0020 1.7254 .0003 .0001 .0000 %RSD 206.62 2.250 275.20 1.472 .1738 1.951 #1 .56083 .0902 2.1291 .0212 .0723 .0001 #2 -.04178 .0878 1.0092 .0216 .0725 .0001 #3 -.02199 .0863 -1.2575 .0218 .0723 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 -.0002 .0254 .0018 .1881 3.049 SDev .0001 .0003 .0001 .0.001 ..0008 .003 %RSD 54.34 185.5 .5082 5.065 .4010 .0929 #1 .0002 -.0005 .0254 .0017 .1880 3.046 #2 .0001 -.0002 .0253 .0017 .1888 3.052 #3 .0001 .0002 .0256 .0019 .1873 3.048 Elem Mn Mo Na Ni 2203/1 2203/2 .ts ppm ppm ppm ppm ppb ppb {e .0169 .0001 44.01 .0073 .62501 1.5110 SDev .0000 .0004 .15 .0003 .87110 1.7060 %RSD .2155 494.3 .3314 4.411 139.37 112.90 #1 .0169 .0001 43.90 .0076 -.09726 2.9344 #2 .0168 .0006 44.18 .0071 1.5924 1.9787 #3 .0169 -.0003 43.96 .0070 .37987 -.38006 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge -1.8018 -3.3206 2.4514 3.527 -.0008 .0598 SDev .7470 2.9671 1.2103 .013 .0019 .0001 %RSD 41.456 89.356 49.370 .3697 234.4 .2503 #1 -2.5821 -6.5936 2.4476 3.528 -.0020 .0597 #2 -1.0934 -.80689 1.2430 3.540 -.0018 .0600 #3 -1.7298 -2.5612 3.6635 3.514 .0014 .0597 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.51647 .0003 ..0114 1.2160 -.10225 .52932 SDev .92617 .0001 .0002 1.1637 .44226 1.0772 %RSD 179.33 39.20 1.722 95.692 432.51 203.51 #1 .46555 .0003 .0112 1.9249 -.48598 -.56309 41� -.64073 .0003 .0115 1.8501 .38143 .56040 -1.3743 .0005 .0115 -.12694 -.20221 1.5906 page 1 Ca PPM 10.23 .02 .2217 10.22 10.26 10.22 Mg PPM 6.256 .015 .2422 6.248 6.274 6.247 2068/1 ppb 3.3018 .4285 12.978 3.7125 3.3355 2.8575 Ti PPM .0048 .0000 .7050 .0048 .0048 .0049 M 00 O O C/1 F-+ Analysis Report 09/15/06 03:47:51 PM ] Lod: CLP1 Sample Name: 0609809-004E Operator: CD kun Time: 09/15/06 15:40:26 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .26308 .0959 .13225 ..0219 .0724 .0001 SDev .33326 .0020 1.0314 .0003 .0003 .0000 %RSD 126.68 2.112 779.88 1.520 .4205 47.58 ##1 .45142 .0982 1.1520 .0223 .0726 .0001 #2 .45953 .0944 -.91047 .0217 .0726 .0001 #3 -.12172 .0951 .15526 .0218 .0721 .0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 .0001 .0279 .0020 .1994 3.021 SDev .0002 _ .0002 .0001. .0003 .0007 .011 %RSD 160.4 353.7 .3188 17.14 .3408 .3497 #1 .0003 .0003 .0279 .0024 .1998 3.021 #2 .0000 -.0001 .0279 .0017 .1999 3.032 #3 -.0000 .0000 .0278 .0019 .1986 3.010 Elem Mn Mo Na Ni 2203/1 2203/2 its ppm ppm ppm ppm ppb ppb je .0210 -.0005 44.47 .0076 .49508 1.9674 SDev .0001 .0007 .08 .0004 1.2105 .6328 %RSD. .6454 143.3 .1765 4.663 244.50 32.165 #1 .0211 .0001 44.47 .0078 1.0054 1.5686 #2 .0211 -.0004 44.55 .0072 -.88698 2.6971 #3 .0209 -.0012 44.40 .0079 1.3668 1.6367 Elem 2068/2 1960/1 196.0/2 Si Sn Sr Units ppb ppb ppb ppm ppm Ppm Avge 1.3407 -2.8604 1.7201 3.489 -.0003 .0596 SDev .7239 1.1439 1.0442 .013 .0012 .0001 %RSD 53.996 39.990 60.704 .3833 350.6 .1769 #1 1.6226 -4.0710 2.2322 3.492 -.0010 .0597 #2 .51825 -1.7977 .51875 3.501 -.0010 .0597 #3 1.8813 -2.7125 2.4094 3.475 .0010 .0595 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.66159 .0006 .0156 1.4772 1.5081 .19484 SDev 1.53412 .0002 .0001 .0860 .2393 .48118 %RSD 231.88 38.36 .4925 5.8205 15.868 246.96 #1 .26037 .0006 .0155 1.3811 1.7842 .13328 u^ -2.4325 .0008 .0157 1.5037 1.3777 -.25260 .18739 .0004 .0156 1.5469 1.3622 .70384 page 1 Ca' PPM 10.31 .04 .3653 10.33 10.34 10.27 Mg PPM 6.280 .023 .3733 6.288 6.298 6.253 2068/1 ppb 1.8431 1.4073 76.353 2.1079 3.0992 .32225 Ti PPM .0047 .0001 2.612 .0048 .0048 .0046 00 O O 0� N Analysis Report 09/15/06 03:55:22 PM page 1 ] Lod: CLP1 Sample Name: 0609809-005E - Operator: CD Imuii Time: 09/15/06 15:47:57 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .18963 .1484 .16178 .0212 .0725 .0001 10.14 SDev .13145 .0021 .53823 .0005 .0006 .0000 .06 %RSD 69.319 1.423 332.70 2.463 .7621 32.64 .6282 #1 .26303 .1470 .30020 .0217 .0720 .0001 10.09 #2 .03787 .1474 -.43214 .0207 .0723 .0001 10.11 #3 .26799 .1508 .61728 .0210 .0731 .0001 10.21 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0000 .0418 .0022 .3313 3.054 6.221 SDev .0002 .0001 .0004 .0003 .0026 .018 .040 %RSD 108.2 298.9 .9559 12.95 .7835 .5791 .6391 #1 .0003 .0001 .0415 .0020 .3294 3.036 6.185 #2 .0000 -.0001 .0416 .0020 .3303 3.056 6.212 #3 .0001 -.0001 .0423 .0025 .3342 3.072 6.264 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb �e .0234 -.0003 44.06 .0082 -.23720 1.3320 2.1878 SDev .0002 .0003 .26 .0005 1.06267 .6210 1.7364 %RSD .7731 110.8 .5973 6.305 448.01 46.621 79.364 #1 .0233 -.0002 43.77 .0086 -1.4535 1.0949 3.0924 #2 .0233 44.13 .0076 .51144 .86442 3.2852 #3 .0236 .-.0000 -.0007 44.29 .0083 .23045 2.0365 .18597 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.91446 -.88073 1.0849 3.492 -.0004 .0590 .0075 SDev 2.54661 .17789 1.5060 .026 .0004 .0005 .0000 %RSD 278.48 20.198 138.82 .7389 91.63 .7825 .5281 #1 -3.8550 -1.0082 2.7477 3.467 -.0009 .0586 .0074 #2 .54035 -.67749 -.18744 3.491 -.0002 .0590 .0075 #3 .57124 -.95654 .69438 3.519 -.0002 .0595 .0075 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb_ ppm ppm ppb ppb ppb Avge .50028 .0006 .0133 .80948 .11863 .43034 SDev 1.1014 .0002 .0001 .59687 1.5240 .95638 %RSD 220.16 37.54 .9520 73.736 1284.7 222.24 #1 1.2703 .0008 .0132 .24634 -1.5415 1.4970 ''-.35063 .99191 .0004 .0132 .74694 1.4544 -.76136 .0006 .0134 1.4352 .44297 .14465 00 O O Analysis Report 09/15/06 04:02:52 PM page 1 1 Lod: CLP1 Sample Name: 0609809-006E Operator: CD icuii Time: .09/15/06 15:55:27 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .12571 .0246 -.01093 .0904 .0683 .0001 14.73 SDev .04986 .0010 .97955 .0009 .0006 .0000 .13 %RSD 39.662 4.215 8961.6 .9825 .8156 35.70 .8899 #1 .18166 .0258 -.17783 .0901 .0678 .0001 14.63 #2 .08597 .0241 1.0413 .0897 .0681 .0001 14.67 #3 .10950 .0240 -.89631 .0914 .0689 .0000 14.88 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0004 .0006 .0011 .0040 .0091 12.57 10.43 SDev .0001 .0002 .0001 .0003_ .0000 .0.9 .09 %RSD 29.76 35.50 9.754 6.892 .2249 .7438 .8995 #1 .0003 .0009 .0011 .0038 .0092 12.52 10.37 #2 .0003 .0006 .0010 .0038 .0091 12.51 10.39 #3 .0005 .0004 .0011 .0043 .0091 12.68 10.54 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb je 1.969 -.0005 17.95 .0089 .67631 1.0950 1.6602 SDev .017 .0004 .16 .0005 1.1274 .8447 1.3200 %RSD .8808 81.68 .8748 5.961 166.69 77.139 79.507 #1 1.957 -.0008 17.86 .0086 1.7122 1.6341 2.3426 #2 1.962 -.0000 17.87 .0086 -.52435 .12153 2.4992 #3 1.989 -.0008 18.13 .0095 .84108 1.5294 .13871 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.4457 -1.3699 1.5643 4.452 -.0008 .0805 .0011 SDev 1.4684 1.5922 1.0800 .039 .0014 .0008 .0001 %RSD 101.57 116.23 69.041 .8697 179.5 .9575 8.491 #1 .12485 .46751 .42866 4.427 -.0020 .0799 .0010 #2 -2.7845 -2.3430 1.6859 4.433 .0007 .0803 .0010 #3 -1.6774 -2.2342 2.5784 4.497 -.0011 .0814 .0012 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .05178 -.0000 .0188 .95566 -.41141 .58725 SDev 1.2602 .0001 .0001 .92623 1.10427 .34005 %RSD 2433.7 159.3 .7969 96.921 268.41 57.906 ##1 -.23397 -.0001 .0186 1.6602 .86340 .44160 .an -1.0410 -.0001 .0187 -.09348 -1.0250 .34428 1.4303 .0000 .0189 1.3003 -1.0726 .97586 Analysis Report 09/15/06 04:10:23 PM page 1 lod: CLP1 Sample Name: 0609809-007E Operator: CD Time: 09/15/06 16:02:58 Comment: M W-uS Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .11489 .0399 -1.4686 .0873 .0691 .0001 14.62 SDev .31174 .0025 .5549 .0026 .0023 .0000 .51 %RSD 271.33 6.239 37.782 2.927 3.325 32.14 3.509 #1 .2.6152 .0371 -1.2747 .0844 .0665 .0001 14.03 #2 -.24313 .0407 -2.0944 .0886 .0704 .0001 14.92 #3 .32629 .0419 -1.0367 .0889 .0705 .0001 14.92 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0005 .0013 .0036 .0364 6.671 10.40 SDev .0002 .0003 _ .0001 .0004 .0017 ..1.91 ...36 %RSD 168.3 58.46 9.085 10.71 4.639 2.861 3.421 #1 .0001 .0003 .0012 .0032 .0345 6.451 9.986 #2 .0003 .0004 .0012 .0037 .0375 6.782 10.61 #3 -.0001 .0009 .0014 .0039 .0373 6.781 10.60 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb 4e 1.984 -.0009 12.29 .0098 2.4185 1.0629 3.1645 SDev .069 .0005 .38 .0006 1.3486 .4710 1.6610 %RSD 3.465 59.64 3.107 6.104 55.761 44.315 52.488 #1 1.904 -.0006 11.85 .0092 3.1401 .51987 2.7534 #2 2.024 -.0005 12.52 .0102 3.2526 1.3077 1.7477 #3 2.023 -.0015 12.50 .0102 .86262 1.3611 4.9925 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.47300 -6.4248 1.8987 4.433 .0001 .0817 .0022 SDev 2.25682 1.6871 •.5112 .162 .0007 .0030 .0003 %RSD 477.13 26.259 26.922 3.647 596.9 3.618 11.18 41 1.9485 -4.4987 1.3345 4.247 .0004 .0783 .0020 #2 -.84970 -7.1350 2.3311 4.527 .0006 .0834 .0025 #3 -2.5178 -7.6406 2.0304 4.526 -.0007. .0834 .0023 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.87160 .0000 .0148 1.5143 .73832 -.87301 SDev .92439 .0004 .0006 .3945 1.2803 .29450 %RSD 106.06 1315. 3.738 26.050 173.40 33.734 #1 -1.7937 -.0004 .0142 1.3925 2.2165 -.60791 .05504 .0000 .0150 1.9554 .01526 -.82111 -.87612 .0005 .0152 1.1952 -.01683 -1.1900 00 O O E-+ Analysis Report 09/15/06 04:17:54 PM page 1 P god: CLP1 Sample Name: 0609809-008E Operator: CD 1,,,, Time: 09/15/06 16:10:29 Comment: fAw- Sb Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .19533 .2064 -.47593 .0211 .0744 ..0001 10.10 SDev .11807 .0018 1.19439 .0002 .0003 .0000 .02 %RSD 60.445 .8831 250.96 1.156 .3742 33.64 .2352 #1 .29356 .2073 .62844 .0211 .0746 .0001 10.11 #2 .22808 .2076 -1.7436 .0208 .0746 .0001 10.11 #3 .06434 .2043 -.31268 .0213 .0741 .0001 10.07 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 .0003 .0574 .0025 .4815 2.629 6.235 SDev .0001 .0002 .0002 .0001 .0008 .011_ .018 %RSD 231.9 82.92 .2868 3.912 .1654 .4127 .2888 #1 .0001 .0004 .0575 .0024 .4819 2.640 6.248 #2 .0001 .0000 .0575 .0026 .4821 2.628 6.243 #3 -.0001 .0004 .0572 .0025 .4806 2.618 6.215 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb 4e .0266 -.0006 44.31 .0094 1.9584 2.2609 3.1822 SDev .0004 .0004 .22 .0007 2.2550 1.6878 1.5045 %RSD 1.396 59.35 .5011 7.583 115.14 74.650 47.277 #1 .0270 -.0010 44.50 .0098 2.3835 3.3738 2.0066 #2 .0266 -.0003 44.38 .0099 -.47886 3.0900 4.8776 #3 .0262 -.0004 44.07 .0086 3.9707 .31895 2.6623 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.0173 -4.6680 1.5259 3.524 -.0007 .0595 .0104 SDev .9914 1.7358 1.6474 .010 .0021 .0001 .0001 %RSD 97.452 37.186 107.96 .2861 288.5 .2360 1.372 #1 -1.6960 -2.7002 3.2429 3.532 .0012 .0596 .0106 #2 -1.4764 -5.3219 1.3765 3.527 -.0030 .0596 .0103 #3 .12040 -5.9819 -.04165 3.512 -.0004 .0594 .0105 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -2.6209 .0010 .0667 2.1603 .38112 -.53662 SDev 1.8311 .0002 .0001 .7871 .74915 1.66467 %RSD 69.864 21.78 .1468 36.434 196.56 310.21 #1 -3.6476 .0013 .0666 3.0441 -.46303 1.2639 -3.7082 .0008 .0668 1.9017 .63953 -.85403 -.50684 .0010 .0667 1.5350 .96685 -2.0197 00 00 O O Analysis Report 09/15/06 04:28:05 PM page 1 iod: CLP1 Sample Name: CCV2 Operator: CD Time: 09/15/06 16:20:40 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1005.4 49.92 513.15 2.570 2.570 2.548 48.80 SDev 2.3 .12 .60 .009 .006 .007 .13 %RSD .22751 .2376 .11698 .3336 .2409 .2787 .2618 #1 1004.4 49.89 513.19 2.564 2.570 2.544 48.71 ##2 1003.8 49.82 513.74 2.566 2.564 2.544 48.75 #3 1008.0 50.05 512.54 2.580 2.576 2.556 48.95 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.544 2.489 2.531 2.592 50.31 85.86 51.23 SDev .005 .007 .006 .007 .10 .17 .14 0 -.RSD .1880 .3003 .2392 .2894 .1992 .1931 .2799 #1 2.545 2.484 2.528 2.590 50.24 85.78 51.14 2.539 2.486 2.527 2.586 50.26 85.76 51.16 2.548 2.498 2.538 2.600 50.42 86.06 51.40 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn - Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.501 2.595 84.95 2.512 499.05 491.01 984.59 SDev .006 .008 .14 .005 .39 2.39 6.15 %RSD .2501 .2995 .1651 .1799 .07836 .48769 .62415 #1 2.498 2.592 84.87 2.509 499.41 490.35 978.45 #2 2.497 2.589 84.86 2.509 499.09 489.01 984.57 #3 2.508 2.604 85.11 2.517 498.64 493.66 990.75 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 992.61 518.41 513.80 2.901 ! 2.497 2.524 2.645 SDev 7.80 .93 4.74 .086 .008 .007 .007 %RSD .78566 .17912 .92305 2.955 .3162 .2704 .2796 983.64 517.39 511.58 2.816 2.492 2.521 2.653 996.35 518.61 510.58 2.899 2.493 2.520 2.638 #3 997.83 519.22 519.25 2.987 2.506 2.532 2.645 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 O O F-+ Analysis Report 09/15/06 04:28:05 PM Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 504.14 2.514 2.589 493.69 989.94 515.34 SDev .71 .007 .006 1.50 7.11 3.38 %RSD .14024 .2746 .2476 .30388 .71842 .65626 ##1 504.66 2.512 2.587 493.37 981.92 513.51 ##2 504.43 2.509 2.585 492.37 992.43 513.26• #3 503.33 2.522 2.597 495.32 995.47 519.24 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report P od: CLP1 Sample Name: CCVL2 F Time: 09/15/06 16:28:11 ppm Comment: .0033 .0007 .0008 Mode: CONC Corr. Factor: 1 .0003 Eleni Ag Al As1890 Units ppb ppm ppb Avge 52366 .0216 .89746 SDev .12352 .0073 .81321 %RSD 23.589 33.80 90.612 #1 .61039 .0298 1.2202 #2 .57835 .0193 -.02757 #3 .38223 .0157 1.4998 Errors NOCHECK NOCHECK NOCHECK High .0056 171.0 .6853 Low 46.89 .0002 2.509 Elem Cd Co Cr Units ppm ppm ppm Avge .0007 .0003 .0003 SDev .0004 .0002 .0002 %RSD 59.94 48.83 63.64 #1 .0011 .0005 .0006 '- .0006 .0003 .0002 ppb .0003 .0002 .0002 Errors NOCHECK NOCHECK NOCHECK High 2.2359 61.52 1196.5 Low 27.219 .0010 -1.1055 Elem Mn Mo Na Units ppm ppm ppm Avge .0000 .0066 2.553 SDev .0003 .0029 .019 %RSD 1406. 43.54 .7479 #1 .0004 .0096 2.575 #2 -.0001 .0061 2.539 #3 -.0002 .0040 2.546 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 1.9028 .95955 -.12643 SDev .6735 2.5578 .14003 0-oRSD 35.395 266.56 110.76 2.0180 3.9044 .03338 2.5112 -.70810 -.18500 #3 1.1791 -.31762 -.22766 Errors NOCHECK NOCHECK NOCHECK 09/15/06 04:35:36 PM page 1 Operator: CD B Ba Be Ca ppm ppm ppm ppm .0033 .0007 .0008 .0029 .0015 .0003 .0003 .0059 44.07 47.54 40.96 203.8 .0049 .0010 .0011 .0094 .0031 .0006 .0007 .0016 .0020 .0004 .0005 -.0022 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg ppm ppm ppm ppm .0001 2.489 .0449 .0120 .0002 .017 .0114 .0056 171.0 .6853 25.29 46.89 .0002 2.509 .0571 .0176 .0002 2.476 .0428 .0122 -.0001 2.484 .0347 .0063 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0007 .13541 1.4035 8.2145 .0004 1.6202 1.1198 2.2359 61.52 1196.5 79.786 27.219 .0010 -1.1055 2.4680 10.628 .0008 -.45663 1.5069 7.8024 .0002 1.9683 .23560 6.2133 NOCHECK NOCHECK NOCHECK NOCHECK Si Sn Sr Ti ppm ppm ppm ppm .0949 .0003 .0006 .0008 .0255 .0015 .0003 .0004 26.82 440.4 52.61 43.31 .1233 .0010 .0010 .0012 .0872 .0015 .0005 .0008 .0741 -.0014 .0003 .0005 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 04:43:06 PM page 2 --jh Zn Low Sb2068 Elem T11908 Units ppb Avge -.77430 SDev 1.50511 %RSD 194.38 #1 -2.4354 #2 -.38634 #3 .49885 Errors LC Pass High 10.000 Low -10'.000 v Zn Pb2203 Sb2068 Se1960 ppm ppm ppb ppb ppb -.0001 .0006 .21592 .59011 1.0143 .0001 .0001 .14278 1.0327 1.1189 110.1 17.37 66.129 175.00 110.31 -.0002 .0005 .14715 1.6361 2.3051 .0000 .0007 .38008 -.42879 .32097 -.0002 .0007 .12054 .56302 .41681 LC Pass LC Pass LC Pass LC Pass LC Pass .0500 .0200 3.0000 60.000 5.0000 -.0500 -.0200 -3.0000 -60.000 -5.0000 Analysis Report 09/15/06 04:50:37 PM page 1 iod: CLP1 Sample Name: 0609809-009E Operator: CD Time: 09/15/06 16:43:12 Comment: to W -SS Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .21338 .0252 -.35414 .0899 .0682 .0001 14.67 SDev .22359 .0023 1.24395 .0007 .0003 .0000 .05 %RSD 104.78 9.249 351.26 .7427 .5112 27.46 .3420 #1 .46390 .0278 .17462 .0900 .0684 .0001 14.68 #2 .03406 .0242 .53808 .0892 .0684 .0001 14.72 #3 .14218 .0235 -1.7751 .0906 .0678 .0001 14.62 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0004 .0004 .0013 .0036 .0149 12.29 10.37 SDev .0001 .0002 _ .0001. .0001 .0004 .04 .04 %RSD 27.44 51.19 11.23 4.238 2.725 .3009 .4033 #1 .0005 .0006 .0014 .0035 .0153 12.30 10.38 #2 .0003 .0003 .0014 .0037 .0149 12.32 10.41 #3 .0003 .0002 .0011 .0034 .0145 12.25 10.32 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 -- its ppm ppm ppm ppm ppb ppb ppb 3e 1.967 -.0002 17.78 .0089 2.8976 .40690 1.6354 bi,ev .007 .0001 .06 .0003 1.0171 1.4438 1.9995 %RSD .3697 36.53 .3256 3.796 35.102 354.84 122.27 #1 1.968 -.0002 17.76 .0092 2.5330 -.96077 1.0712 #2 1.973 -.0003 17.84 .0089 4.0468 1.9164 -.02143 #3 1.959 -.0002 17.73 .0086 2.1130 .26508 3.8564 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .00503 -3.0763 4.7544 4.419 -.0005 .0804 .0015 SDev 1.9829 3.4666 .9858 .017 .0011 .0003 .0001 %RSD 39428. 112.69 20.734 .3885 222.7 .3067 10.20 #1 1.2102 .09373 5.7796 4.423 -.0011 .0804 .0016 #2 -2.2836 -6.7780 4.6704 4.433 .0008 .0807 .0015 #3 1.0885 -2.5446 3.8133 4.400 =.0013 .0802 .0013 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.2588 .0002 .0201 1.2364 .54796 2.1468 SDev .4096 .0002 .0002 1.2502 1.8489 1.5635 %RSD 32.535 107.1 .8385 10.1.11 337.41 72.831 #1 -1.2557 .0005 .0201 .20273 1.1639 3.8862 #2 -1.6699 .0001 .0203 2.6259 -1.5303 .85809 -.85084 .0000 .0200 .88051 2.0102 1.6962 Analysis Report 09/15/06 04:58:08 PM page 1 ] tod: CLP1 Sample Name: 0609809-009EDUP Operator: CD I.... Time: 09/15/06 16:50:43 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.00101 .0252 .05327 .0909 .0691 .0001 14.88 SDev .11520 .0014 .53975 .0004 .0001 .0000 .01 %RSD 11454. 5.668 1013.1 .4523 .1431 18.45 .0893 #1 -.10552 .0254 .07946 .0913 .0691 .0001 14.89 #2 -.02000 .0265 .57945 .0905 .0690 .0001 14.87 #3 .12251 .0237 -.49909 .0911 .0692 .0001 14.89 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0005 .0012 .0035 .0075 12.52 10.52 SDev .0001 .0001 .0002 .0001 .0002 .03 .01 %RSD 20.46 13.98 17.41 3.009 3.266 .2434 .1112 #1 .0003 .0006 .0013 .0035 .0076 12.52 10.51 #2 .0002 .0005 .0009 .0034 .0077 12.50 10.51 #3 .0003 .0005 .0012 .0036 .0072 12.56 10.53 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb �e 1.994 -.0002 18.07 .0093 1.1808 1.6286 3.3451 SDev .002 .0005 .07 .0006 .5974 .2923 .7763 %RSD .0898 247.2 .3868 6.283 50.591 17.951 23.207 #1 1.994 .0004 18.03 .0091 .50276 1.9624 4.1845 #2 1.992 -.0005 18.03 .0100 1.4099 1.4184 2.6530 #3 1.995 -.0004 18.15 .0089 1.6296 1.5049 3.1978 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.7918 -1.2646 2.1119 4.488 .0003 .0815 .0014 SDev .8457 .6624 2.3895 .010 .0009 .0002 .0001 %RSD 47.199 52.376 113.15 .2323 356.8 .2135 5.524 #1 -2.4291 -.50990 .11561 4.494 .0002 .0814 .0014 #2 -.83237 -1.5346 4.7595 4.476 -.0006 .0814 .0015 #3 -2.1139 -1.7493 1.4605 4.495 .0012 .0817 .0014 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.9529 .0002 .0175 1.4795 -.08120 .98753 SDev 2.0932 .0003 .0001 .0655 .35952 1.4716 %RSD 107.18 156.4 .3079 4.4273 442.78 149.02 #1 .24123 .0005 .0175 1.4764 -.22679 -.09266 47 -3.9279 .0001 .0174 1.4156 .32829 2.6636 -2.1721 -.0001 .0175 1.5465 -.34509 .39167 E9S'OT ES'E67v L68'6T TGZS' T86:' E89'S:i 9TL'TT 8E'E6:i EST'OZ SEES' SZOS' LTL'OS c.ff S69'OT LE'Z6:i LZL'OZ FEES' OZOS" 9Ti9'9:� T# TZ7vL'S S08ZT 6S60'Z 6L9%' TLL%' 9E09'S CIM TE9' E9' SzV SZOO' :Zoo" ZL9'Z AaQS Z66'OT 60'E6:� 6SZ'OZ 6TES' 600S' Z89'L:� a5AV qdd qdd qdd wdd wdd qdd sgTun 096TaS 890ZgS £oZZgd uZ n 806TTZ waTH 9T00' OSLO' 8000' 9SUIV 806'TT 0898'L L8'Mty E# TvTOO' L8LO' tlo00" Z6E':i 880':�T £996'9 08'Z6:� Z# ZTOO' 98L0' OT00'- T8E':i 60E'TT L99:V'6 Z9'E6i, T# 66'TT 9LTS' TSZ%' 09L'TT ZE9'ST 8TTTZ' QSE% Z000' Ii000' 6000 6T0' Z9iv'T E99Z'T :�o'T naQS :�T00' :�8L0' 0000' LLE, T, SE:�'ZT EOOT'8 9L'E67 abAV wdd wdd wdd wdd qdd qdd qdd sgtun TI as us TS Z/096T T/096T Z/8902 waT E8' 06t, 9ZZ' 6T T:�Z' TZ TLOS' 9V LT 9T00' - 90il' Z £# :VS'%6b 80Z'OZ EDIO'0z ZITS' ES'LT 'V000'- LZV Z Z# S8'68� Z99'OZ 9S8 oz: :VZTS' 9V LT 0000'- SZD"Z T# T:�EOS' 8299' E ZtS6' Z ZMS' 9otIZ' £' 9TT 6TLV CIMI% 8fii'Z %EL' ZT9' 0£00' 7v0' 8000' TTO' AaQS TvL' T6:� ZEO' OZ :VTL' OZ 90TS' 6:V' LT LOW- 6TV Z GE qdd qdd qdd wdd wdd wdd wdd s-qZ T/890Z Z/EOZZ T/EOZZ TN -eN ow uW waTz[ 60'0T 6Z'ZT TT86' SZ9Z' SEOZ' EZ6:V' 90SO' E# LT'OT :iE'ZT 9686' 6fi9Z' 9SOZ' 'vL61,' OTSO'. Z# ST'OT ZE'ZT X886' 6E9Z' ll:voZ' LE6v' TTSO' T# ZOLE' LIVEZ' LS9V 9Z9:v OOOS' :i9ZS" TZ9S' QS2i% %O" EO' 9:0o' ZTOO' OTOO' 9200' E000' naQS t,T' OT ZE' ZT X986' 8E9Z' SIVOZ' S:V6:' 6050' a)BAV wdd wdd wdd wdd wdd wdd wdd sgzun bW X a3 nO -7D oO PO waTg 9Z':iT ETSO' 'vOT' Z TvL80' OTS' LE %;6' T 9TE' Zig E# 8E''iT 8TSO' ZZT'Z 6L80' :�£VOD, TV96'T ZLL'Zig Z# 9UPT LTSO' OZT'Z 8L80' ZES'8E 096'T 966'Z'v T# 6E:V' PZVP 06Sv* V90E' 8T817'E 9ZIVS' EtZT8' QS2i% 90' 2000" OTO' E000" SSE'T TTO' L:iE' AaQS EE`VT 9TSO' STT'Z LL80' SZ6'8E 9S6'T S69'Zv 95AV wdd wdd wdd wdd qdd wdd qdd sgzun -ea ag L -H g 068TsV TSI 5V waTH Stii T : aogs-e3 • .z D ONOD : aPoW S S - M VI : -quawwoO IVT : BS: 9T 90/ST/60 : aw?Z TTY"\T QO :.zogpa@d0 SWS600-6086090 : aw-eN aTdw-eS TdrIO :poL T aFD,2d Wd 6E:SO:SO 90/ST/60 q.zodag szsAT-euV Analysis Report 09/15/06 05:13:10 PM page 1 iod: CLP1 Sample Name: 0609809-009ESD Operator: CD Time: 09/15/06 17:05:45 Comment: µ W- Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .12517 .0143 -.65747 .0167 .0140 .0000 2.907 SDev .09624 .0009 1.96446 .0005 .0001 .0000 .007 %RSD 76.884 6.330 298.79 2.743 .6592 48.35 .2332 #1 .20866 .0133 .10211 .0173 .0141 .0000 2.902 #2 .14693 .0151 -2.8883 .0164 .0141 .0000 2.915 #3 .01992 .0146 .81379 .0166 .0139 .0000 2.904 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0000 .0001 .0000 .0004 .0078 2.306 2.056 SDev .0001 .0001 .0003 _.0002 .0001 .004 .006 %RSD 797.4 177.8 528.7 48.53 1.406 .1532 .2720 #1 -.0001 .0002 -.0002 .0002 .0078 2.308 2.053 #2 .0001 .0001 .0003 .0003 .0079 2.309 2.062 #3 -.0000 -.0001 .0000 .0006 .0077 2.302 2.052 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 -- its ppm ppm ppm ppm ppb ppb ppb fie .3910 -.0011 3.379 .0021 .25631 .36417 2.2682 ZjL)ev .0010 .0000 .009 .0003 .62053 1.0234 1.1563 %RSD .2572 4.422 .2580 15.28 242.10 281.04 50.979 #1 .3902 -.0011 3.381 .0020 .00542 .38449 .98351 #2 .3921 -.0011 3.386 .0025 .96300 -.66929 2.5955 #3 .3908 -.0010 3.369 .0019 -.19949 1.3773 3.2256 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units- ppb ppb ppb ppm ppm ppm ppm Avge -.85537 2.1178 1.3340 .8480 .0016 .0157 .0003 SDev 1.76694 2.5664 .7212 .0105 .0007 .0000 .0000 %RSD 206.57 121.18 54.061 1.238 41.65 .2569 14.18 #1 -.36174 .32546 1.3080 .8382 .0024 .0156 .0003 #2 .61226 5.0577 .62617 .8467 .0011 .0157 .0003 #3 -2.8166 .97011 2.0678 .8591 .0015 .0157 .0003 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .04734 .0002 .0048 .32829 .18480 1.5950 SDev 1.8461 .0001 .0000 .49272 1.0421 .5682 %RSD 3899.9 30.46 .6813 150.09 563.93 35.621 #1 -1.5666 .0001 .0048 .25830 .08625 .98087 #2 2.0604 .0003 .0047 -.12569 1.2727 2.1019 -.35179 .0003 .0048 .85227 -.80456 1.7023 Analysis Report 09/15/06 05:20:41 PM page 1 iod: CLP1 Sample Name: 0609809-010E Operator: CD Time: 09/15/06 17:13:16 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .01447 .0392 -1.3223 .0934 .0573 .0001 18.76 SDev .15145 .0013 .8626 .0007 .0003 .0000 .04 %RSD 1046.9 3.216 65.233 .7394 .5544 2.148 .1959 #1 -.15913 .0401 -2.2859 .0936 .0576 .0001 18.80 #2 .11957 .0398 -.62210 .0940 .0572 .0001 18.76 #3 .08296 .0378 -1.0590 .0927 .0570 .0001 18.72 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0012 .0016 .0047 .0174 10.47 4.557 SDev .0001 .0002 .0001 .0001 .0000 .06 .010 . %RSD 124.3 13.20 8.284 2.519 .1781 .5394 .2141 #1 .0001 .0011 .0016 .0048 .0174 10.52 4.567 #2 .0002 .0014 .0014 .0046 .0174 10.48 4.557 #3 -.0000 .0012 .0016 .0046 .0173 10.41 4.547 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb je 2.536 -.0009 3.662 .0070 1.5509 .52548 1.8629 SDev .005 .0002 .018 .0006 1.5005 1.0129 1.0115 %RSD .1938 23.21 .5024 8.455 96.751 192.75 54.298 #1 2.541 -.0007 3.678 .0066 1.4439 1.4854 2.8578 #2 2.536 -.0011 3.667 .0068 .10676 .62411 1.8953 #3 2.531 -.0010 3.642 .0077 3.1021 -.53307 .83554 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.01037 -4.1119 3.4177 3.739 -.0004 .0452 .0018 SDev .92900 .9814 1.8360 .016 .0009 .0001 .0004 %RSD 8958.9 23.867 53.721 .4376 243.5 .1959 24.75 #1 .69267 -4.4058 1.2977 3.752 .0005 .0453 .0023 #2 -1.0636 -4.9127 4.4622 3.744 -.0012 .0452 .0015 #3 .33977 -3.0171 4.4932 3.721 -.0004 .0452 .0015 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.6318 .0002 .0156 .86701 .61344 .91037 SDev 1.3238 .0001 .0001 .53565 .75185 1.3493 %RSD 81.125 29.53 .7070 61.782 122.56 148.21 #1 -2.5904 .0001 .0156 1.4717 1.4137 -.60152 49 -2.1837 .0003 .0157 .45187 -.07824 1.3404 -.12135 .0003 .0155 .67750 .50489 1.9923 Analysis Report 09/15/06 05:28:13 PM page 1 P od: CLP1 Sample Name: 0609809-011E Operator: CD Time: 09/15/06 17:20:48 Comment: R W- G 5 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.00341 .0374 -1.6708 .0942 .0581 .0001 19.01 SDev .44888 .0013 1.5872 .0026 .0018 .0001 .57 %RSD 13167. 3.428 94.997 2.800 3.005 104.9 2.998 #1 .11502 .0360 -.21695 .0912 .0562 .0001 18.38 #2 .37438 .0380 -3.3641 .0963 .0596 .0000 19.49 #3 -.49962 .0383' -1.4313 .0950 .0586 .0000 19.15 Elem Cd Co Cr - Cu Fe _ K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0014 .0029 .0046 .0338 10.15 4.594 SDev .0001 .0002 .0000 .0001 .0014 .28 .139 %RSD 11.65 13.68 .4176 2.966 4.069 2.798 3.026 #1 .0006 .0015 .0029 .0045 .0323 9.837 4.439 #2 .0007 .0012 .0030 .0047 .0348 10.39 4.709 #3 .0005 .0015 .0029 .0047 .0344 10.24 4.633 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb je 2.588 -.0015 3.654 .0080 2.3919 1.1874 .99408 SDev .077 .0003 .119 .0003 .9501 1.0393 1.3683 %RSD 2.960 19.28 3.245 3.651 39.723 87.523 137.64 #1 2.504 -.0012 3.521 .0079 1.3297 2.1482 2.2616 #2 2.654 -.0016 3.749 .0083 2.6851 1.3297 1.1772 #3 2.607 -'.0017 3.691 .0077 3.1609 .08435 -.45654 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.1682 -4.7959 2.2749 3.767 -.0008 .0461 .0021 SDev .7303 3.3161 .9743 .126 .0013 .0016 .0001 %RSD 62.510 69.144 42.829 3.350 153.4 3.388 6.216 #1 -1.1345 -4.2338 1.2725 3.628 .0005 .0443 .0019 #2 -1.9148 -8.3572 2.3338 3.873 -.0020 .0473 .0021 #3 -.45543 -1.7968 3.2185 3.800 -.0010 .0465 .0022 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.3827 .0001 .0124 1.5885 -.44817 -.07964 SDev 1.3437 .0002 .0005 .4181 .44084 1.44866 %RSD 97.179 2.59.8 4.163 26.319 98.365 1819.1 #1 -1.8520 .0000 .0118 1.8757 -.00357 -.56105 -2.4288 -.0001 .0127 1.7811 -.88516 -1.2263 .13271 .0003 .0126 1.1089 -.45578 1.5484 Analysis Report 09/15/06 05:35:44 PM page 1 1 od: CLP1 Sample Name: 0609809-012E Operator: CD 1,-,, Time: 09/15/06 17:28:19 Comment: �,t W - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .49762 .0850 -.31249 .0942 .0593 .0000 19.11 SDev .09593 .0007 .07058 .0009 .0003 .0000 .06 %RSD 19.279 .8125 22.588 .9083 .4167 95.14 .2933 #1 .40051 .0847 -.23663 .0933 .0591 .0001 19.05 #2 .59234 .0858 -.37623 .0941 .0593 .0000 19.13 #3 .50001 .0845 -.32460 .0951 .0595 -.0000 19.16 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0020 .0080 .0049 .1155 10.23 4.634 SDev .0001 .0002 .0001 .0.001 .0005 .05 .020 %RSD 78.31 9.369 1.816 2.254 .4280 .5005 .4263 #1 .0001 .0022 .0078 .0048 .1150 10.17 4.612 #2 .0000 .0018 .0081 .0048 .1156 10.24 4.639 #3 .0001 .0020 .0081 .0050 .1160 10.27 4.650 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 .ts ppm ppm ppm ppm ppb ppb ppb 1e 2.695 -.0012 3.767 .0079 2.2570 1.1822 1.5264 SDev .007 .0002 .030 .0001 .6974 .8831 .7362 %RSD .2782 18.12 .8067 1.769 30.897 74.698 48.234 #1 2.687 -.0009 3.736 .0080 1.9421 2.1495 1.9476 #2 2.698 -.0013 3.768 .0080 3.0563 .41918 1.9554 #3 2.701 -.0012 3.797 .0078 1.7726 .97787 .67627 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.5087 -4.3159 .02702 3.837 -.0004 .0466 .0037 SDev 2.7438 .8225 3.7176 .019 .0020 .0001 .0001 %RSD 181.87 19.057 13757. .4936 449.8 .2735 2.794 #1 4.6065 -5.2652 3.3103 3.817 -.0015 .0464 .0037 #2 .53509 -3.8659 -4.0095 3.839 .0018 .0467 .0038 #3 -.61556 -3.8167 .78027 3.855 -.0016 .0467 .0036 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.6318 .0004 .0150 1.5402 1.5146 -1.4192 SDev 1.1583 .0005 .0001 .4688 2.0019 2.2828 %RSD 70.983 117.7 .9382 30.435 132.17 160.86 #1 -2.9159 .0010 .0148 2.0805 3.7211 .45467 41) -.66603 .0001 .0150 1.2974 1.0081 -3.9616 -1.3133 .0001 .0151 1.2426 -.18536 -.75049 Analysis Report 09/15/06 05:43:15 PM page 1 1 iod: CLP1 Sample Name: 0609809-013E Operator: CD Time: 09/15/06 17:35:50 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .38310 .1493 .30128_ .0973 .0606 .0000 19.33 SDev .20096 .0063 1.1996 .0006 .0008 .0000 .27 %RSD 52.457 4.247 398.15 .6659 1.291 36.95 1.411 ##1 .60526 .1566 -.12058 .0978 .0615 .0000 19.65 #2 .21398 .1462 1.6548 .0966 .0601 .0000 19.14 #3 .33006 .1451 -.63036 .0974 .0601 .0000 19.21 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0027 .0186 .0053 .3255 10.19 4.740 SDev .0001 .0003 .0005 .0002 .0046 .10 .062 %RSD 57.47 11.75 2.503 4.609 1.401 .9385 1.311 #1 .0002 .0031 .0191 .0056 .3307 10.30 4.811 #2 .0002 .0025 .0183 .0051 .3229 10.11 4.698 #3 .0000 .0026 .0182 .0052 .3228 10.15 4.710 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb Te 2.754 -.0012 3.842 .0080 -.93780 1.6740 1.9134 ol,zv .038 .0001 .033 .0001 1.46055 .5140 .0535 %RSD 1.387 5.898 .8570 1.454 155.74 30.707 2.7979 #1 2.798 -.0013 3.880 .0078 -2.1064 1.6886 1.9740 #2 2.728 -.0012 3.817 .0081 -1.4065 2.1805 1.8936 #3 2.736 -.0012 3.830 .0080 .69951 1.1528 1.8726 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .80512 -1.3148 -.70541 4.018 -.0010 .0468 .0087 SDev 2.2900 2.0204 .60671 .058 .0006 .0004 .0001 %RSD 284.43 153.66 86.008 1.451 62.31 .8814 1.471 #1 2.7678 .93376 -.04327 4.084 -.0006 .0473 .0088 #2 1.3584 -2.9775 -.83831 3.976 -.0017 .0465 .0086 #3 71.7109 -1.9007 -1.2347 3.992 -.0007 .0466 .0086 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .77696 .0008 .0144 .80429 1.1742 -.90833 SDev .69779 .0004 .0002 .32866 1.5428 1.03202 %RSD 89.810 46.45 1.649 40.864 131.39 113.62 #1 .86119 .0012 .0147 .42489 2.5035 .28210 42 .04088 .0005 .0143 .98607 1.5367 -1.5506 1.4288 .0007 .0143 1.0019 -.51754 -1.4564 Analysis Report 09/15/06 05:50:46 PM page 1 Zod: CLP1 Sample Name: CCV3 Operator: CD Time: 09/15/06 17:43:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890' B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1006.5 50.05 515.07 2.567 2.574 2.546 48.65 SDev 7.6 .36 2.92 .023 .019 .020 .39 %RSD .75796 .7231 .56727 .8839 .7509 .7838 .7960 #1 1000.2 49.74 512.95 2.549 2.559 2.531 48.37 #2 1004.3 49.95 513.85 2.560 2.567 2.538 48.48 #3 1015.0 50.45 518.40 2.593 2.596 2.568 49.09 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.528 2.485 2.526 2.602 50.19 86.22 51.08 SDev .018 .020 .020 .021 .36 .61 .41 %RSD .7257 .7985 .7935 .8008 .7272 .7100 .7958 #1 2.516 2.469 2.513 2.583 49.95 85.68 50.77 2.520 2.478 2.517 2.597 50.00 86.09 50.93 2.550 2.507 2.549 2.624 50.61 86.89 51.54 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm. ppm ppm ppm ppb ppb ppb Avge 2.499 2.588 85.11 2.500 500.32 487.95 982.35 SDev .019 .027 .53 .019 3.48 4.12 11.35 %RSD .7684 1.035 .6243 .7657 .69627 .84345 1.1555 #1 2.485 2.566 84.58 2.491 498.03 485.37 970.92 #2 2.491 2.579 85.11 2.488 498.61 485.79 982.51 #3 2.521 2.618 85.64 2.522 504.33 492.70 993.62 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 985.07 511.45 511.64 2.808 2.498 2.530 2.652 SDev 12.01 3.71 4.32 .130 .020 .019 .015 %RSD 1.2195 .72544 .84473 4.617 .7924 .7639 .5818 975.81 507.71 507.97 2.679 2.480 2.515 2.643 980.75 511.52 510.53 2.809 2.494 2.524 2.642 #3 998.64 515.13 516.40 2.938 2.520 2.552 2.669 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 05:50:46 PM ��,gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 503.07 2.515 2.587 492.07 984.16 511.58 SDev 5.40 .021 .021 3.90 11.65 4.09 oRSD 1.0731 .8323 .7984 .79352 1.1842 .80026 #1 497.18 2.499 2.572 489.59 974.18 507.89 #2 504.22 2.507 2.579 490.06 981.33 510.86 #3 507.79 2.538 2.610 496.57 996.97 515.98 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 N O O O C/1 N Analysis Report I Lod: CLP1 Sample Name: CCVL3 Time: 09/15/06 17:50:52 ppm Comment: ppm .0025 .0004 Mode: CONC Corr. Factor: 1 .0014 Elem Ag Al As1890 Units ppb ppm ppb Avge .17491 .0161 1.7678 SDev .13492 .0031 .5131 %RSD 77.139 19.48 29.025 #1 .02580 .0197 2.3024 #2 .28855 .0142 1.7215 #3 .21037 .0143 1.2794 Errors NOCHECK NOCHECK NOCHECK High .0044 .0010 314.8 Low 11.69 13.28 .0003 Elem Cd Cc Cr Units ppm ppm ppm Avge .0005 -.0000 .0001 SDev .0001 .0001 .0000 %RSD 29.16 555.1 42.00 #1 .0007 -.0002 .0001 2203/1 .0005 -.0000 .0001 ppb .0004 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK High 1.0651 2.3579 38.85 Low 132.81 35.702 .0011 Elem Mn Mo Na Units ppm ppm ppm Avge .0001 .0064 2.593 SDev .0002 .0034 .058 %RSD 235.9 53.50 2.219 #1 .0002 .0103 2.659 #2 .0001 .0053 2.564 #3 -.0001 .0037. 2.556 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge .84403 1.5231 1.9629 SDev 2.3483 1.2286 .8832 %RSD 278.23 80.660 44.996 3.4261 2.8614 2.3369 .27020 .44647 2.5975 #3 -1.1642 1.2615 .95420 Errors NOCHECK NOCHECK NOCHECK 09/15/06 05:58:17 PM page 1 Operator: CD B Ba Be Ca ppm ppm ppm ppm .0025 .0004 .0005 .0000 .0014 .0001 .0001 .0022 54.01 30.96 17.14 21280. .0039 .0005 .0005 .0020 .0025 0005 0005 .0003 .0012 .0003 .0004 -.0023 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg ppm ppm ppm ppm .0001 2.515 .0380 .0076 .0002 .067 .0044 .0010 314.8 2.674 11.69 13.28 .0003 2.592 .0401 .0076 -.0000 2.475 .0411 .0087 -.0001 2.476 .0329 .0067 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0008 .20990 .80192 6.6043 .0003 .07548 1.0651 2.3579 38.85 35.958 132.81 35.702 .0011 .29264 -.10721 9.2810 .00.08 .14480 1.9737 5.6970 .0005 .19227 .53924 4.8348 NOCHECK NOCHECK NOCHECK NOCHECK Si Sn Sr Ti ppm ppm ppm ppm .0802 -.0012 .0004 .0006 .0255 .0020 .0001 .0001 31.88 157.6 30.14 16.57 .1081 .0009 .000.5 .0007 .0744 -.0029 .0004 .0006 .0580 -.0017 .0003 .0005 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 05:58:17 PM page 2 -- jh Zn Low Sb2068 Elem T11908 Units ppb Avge 3.0014 SDev .7762 %RSD 25.861 #1 3.7604 #2 2.2091 #3 3.0348 Errors NOCHECK High 84.980 Low .0006 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0004 .0016 .60482 2.7622 1.8165 .0001 .0003 .68751 2.3473 .7297 28.82 18.26 113.67 84.980 40.171 .0006 .0019 .02598 5.3758 2.5116 .0003 .0016 1.3647 2.0773 1.8813 .0004 .0014 .42374 .83349 1.0566 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 '06:05:49 PM page 1 I Lod: CLP1 Sample Name: CCB3 Operator: CD Time: 09/15/06 17:58:23 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.05823 .0101 .45544 -.0002 .0001 .0002 -.0031 SDev .15301 .0023 1.2008 .0002 .0000 .0000 .0005 %RSD 262.78 22.64 263.65 98.96 13.20 11.11 17.83 #1 -.04298 .0124 .47600 -.0004 .0001 .0002 -.0036 #2 -.21829 .0079 1.6458 .0000 .0001 .0002 -.0031 #3 .08659 .0101 -.75549 -.0002 .0001 .0002 -.0025 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0005 -.0002 -.0003 .0021 .0229 .0013 SDev .0001 .0003 .0001 .0001 .0004 .0038 .0013 %RSD 87.09 68.17 59.38 52.59 17.14 16.72 93.68 #1 .0000 -.0002 -.0002 -.0001 .0021 .0212 -.0001 .0002 -.0004 -.0001 -.0003 .0018 .0272 .0024 .0001 -.0008 -.0003 -.0004 .0025 .0202 .0017 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0000 .0003 -.0062 .0005 -.13902 .36895 2.8665 SDev .0000 .0004 .0002 .0002 .31158 .17827 .9561 %RSD 140.3 169.7 3.922 34.33 224.13 48.318 33.354 #1 .0000 -.0000 -.0063 .0003 .07321 .56884 2.7625 #2 .0001 .0008 -.0064 .0006 .00648 .31162 1.9667 #3 .0000 .0000 -.0059 .0006 -.49673 .22641 3.8704 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .61731 .78133 2.2691 .0153 -.0003 .0001 .0001 SDev .71058 1.5307 2.1991 .0037 .0011 .0000 .0000 %RSD 115.11 195.92 96.915 24.19 334.6 24.43 4.378 -.19980 1.4477 4.2519 .0168 -.0014 .0001 .0001 1.0905. 1.8659 2.6515 .0180 .0009 .0001 .0001 #3 .96119 -.96965 -.09612 .0111 -.0005 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 06:05:49 PM - -jh Low Elem T11908 v Zn Pb2203, Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .53146 -.0000 .0008 .19984 1.3663 1.7737 SDev 1.7686 .0003 .0001 .20928 .5718 1.9279 %RSD 332.77 4078. 12.73 104.72 41.851 108.69 #1 2.2879 -.0003 .0008 .40384 .78666 3.3182 ##2 .55543 .0003 .0009 .21005 1.3823 2.3899 #3 -1.2490 .0000 .0007 -.01436 1.9300 -.38699 Errors LC Pass LC Pass LC Pass LC Pass_ LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 O O O r4 V) H Analysis Report 09/15/06 06:13:20 PM page 1 Lod: CLP1 Sample Name: ORIF Operator: CD xuri Time: 09/15/06 18:05:55 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 20.217 .0112 19.910 .2053 -.0000 .0105 -.0109 SDev .31.3 .0026 1.448 .0041 .0000 .0002 .0001 %RSD 1.5498 22.73 7.2'731 2.010 79.73 1.663 .9220 #1 20.088 .0106 21.278 .2013 -.0000 .0103 -.0109 #2 20.574 .0140 20.060 .2095 -.0000 .0107 -.0108 #3 19.988 .0090 18.393 .2051 -.0000 .0105 -.0109 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm. ppm ppm Avge .0106 .1015 .0206 .0521 -.0081 .0202 -.0017 SDev .0002 .0026 .0006 .0014 ._0004 .0007 .0009 %RSD 1.474 2.528 3.089 2.640 4.500 3.441 51.33 #1 .0104 .0991 .0200 .0507 -.0078 .0209 -.0020 #2 .0107 .1042 .0213 .0535 -.0080 .0196 -.0025 #3 .0105 .1011 .0205 .0520 -.0085 .0200 -.0008 Elem Mn Mo Na -Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb je .0305 .0196 -.0089 .0828 5.3256 7.1502 115.03 SDev .0007 .0008 .0010 .0018 1.4143 .8211 6.47 %RSD 2.187 3.978 11.14 2.118 26.556 11.484 5.6247 #1 .0299 .0187 -.0089 .0813 5.9213 7.7146 107.64 #2 .0312 .0201 -.0079 .0848 3.7109 6.2082 119.70 #3 .0304 .0199 -.0098 .0825- 6.3446 7.5277 117.75 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 116.09 10.426 10.153 .1587 .0774 -.0000 .2137 SDev 5.83 1.245 1.494 .0126 .0016 .0000 .0045 %RSD 5.0260 11.942 14.711 7.962 2.034 168.8 2.098 #1 109.36 9.8544 11.553 .1449 .0763 .0000 .2096 #2 119.74 9.5692 10.326 .1697 .0792 -.0000 .2185 #3 119.17 11.854 8.5811 .1614 .0767 -.0000 .2130 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 20.666 .1023 .0442 6.5426 115.74 10.244 SDev 1.760 .0023 .0010 1.0098 6.04 .675 %RSD 8.5162 2.224 2.185 15.434 5.2179 6.5859 #1 22.589 .1001 .0434 7.1174 108.79 10.988 u^ 20.275 .1047 .0452 5.3766 119.73 10.074 19.135 .1020 .0440 7.1338 118.70 9.6710 Analysis Report 09/15/06 06:20:52 PM page 1 iod: CLP1 Sample Name: ICSAF Operator: CD Time: 09/15/06 18:13:27 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .63965 491.2 10.577 .0186 .0011 .0003 479.5 SDev .55591 5.5 1.013 .0010 .0000 .0000 4.4 %RSD 86.909 1.111 9.5761 5.313 1.675 10.64 .9223 #1 .57177 491.4 11.356 .0196 .0012 .0004 479.6 #2 .12079 496.6 10.943 .0185 .0011 .0003 483.9 #3 1.2264 485.7 9.4317 .0176 .0011 .0003 475.1 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0044 -.0001 .0060 -.0004 196.9 .0382 482.0 SDev .0003 .0003 .0001 .0002 1.8 .0053 4.0 %RSD 6.831 239.3 2.521 52.71 .9125 13.81 .8343 #1 -.0043 .0002 .0061 -.0003 197.1 .0422 48.1.9 �^ -.0048 -.0001 .0058 -.0006 198.6 .0322 486.1 -.0042 -.0005 .0061 -.0003 195.0 .0402 478.1 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0092 -.0051 .0144 .0032 -1.7599 -.30414 3.0021 SDev .0009 .0012 .0007 .0001 2.6438 2.58806 3.1338 %RSD 10.09 23.16 5.010 4.584 150.22 850.96 104.39 #1 -.0102 -.0038 .0142 .0030 .61185 -3.0391 .04121 #2 -.0085 -.0055 .0152 .0032 -4.6104 2.1064 6.2840 #3 -.0088 -.0060 .0138 .0033 -1.2812 .02024 2.6810 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 5.1307 -9.3872 -3.7078 .0188 .0394 -.3136 .0022 SDev 4.9426 .7641 1.8473 .0030 .0021 .0025 .0002 %RSD 96.334 8.1396 49.823 15.76 5.398 .7958 8.322 9.9079 -8.5284 -5.6665 .0184 .0395 -.3151 .0024 .03789 -9.9917 -1.9968 .0220 .0414 -.3150 .0020 #3 5..4462 -9.6416 -3.4600 .0161 .0372 -.3107 .0022 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 06:20:52 PM nlyh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge L-16.841 .0001 -.0024 -.78887 4.4219 L-5.5990 SDev .997 .0001 .0002 .90693 2.2540 .9827 %RSD 5.9195 86.46 8.249 114.97 50.974 17.551 #1 L-16.420 .0003 -.0023 -1.8233 6.6223 L-6.6195 #2 L-17.979 .0000 -.0026 -.13022 2.1179 -4.6591 #3 L-16.123 .0001 -.0022 -.41310 4.5254 L-5.5184 Errors. LC Low LC Pass LC Pass LC Pass LC Pass LC Low High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 ON O O O C/O Analysis Report 09/15/06 06:28:23 PM page 1 D od: CLP1 Sample Name: ICSABF Operator: CD kun Time: 09/15/06 18:20:58 Comment: Mode: CONC Corr. Factor: 1 Eleni Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 937.72 493.1 1014.3 1.033 .4732 .4505 480.5 SDev 12.53 7.3 18.7 .014 .0071 .0066 7.5 %RSD 1.3363 1.474 1.8391 1.374 1.505 1.472 1.551 #1 944.29 497.3 1024.6 1.041 .4773 .4538 484.1 #2 923.27 484.7 992.79 1.017 .4649 .4429 471.9 #3 945.61 497.4 1025.6 1.042 .4773 .4548 485.4 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm_ ppm Avge .8508 .4193 .4448 .4939 197.5 .0335 484.1 SDev .0122 .0064 .0067 .0079 3.1 .0029 6.7 %RSD 1.431 1.530 1.514 1.599 1.562 8.606 1.375 #1 .8569 .4219 .4486 .4986 199.1 .0354 487.5 .8367 .4120 .4370 .4848 193.9 .0302 476.5 .8587 .4241 .4488 .4984 199.4 .0350 488.4 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .4249 1.006 .0066 .8433 864.92 851.45 -6.4993 SDev .0062 .016 .0012 .0121 9.98 11.75 3.4193 %RSD 1.449 1.542 18.14 1.440 1.1539 1.3804 52.610 #1 .4278 1.013 .0067 .8506 870.06 857.42 -9.2833 #2 .4178 .9884 .0053 .8293 853.41 837.91 -7.5319 #3 .4290 1.017 .0077 .8501 871.28 859.01 -2.6827 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb Ppm PPM PPM PPM Avge -8.8251 981.03 978.21 .6976 1.031 -.3139 .0016 SDev 5.7374 13.31 9.78 .0163 .014 .0046 .0000 %RSD 65.013 1.3571 .99960 2.338 1.336 1.470 1.933 -2.3905 991.89 985.49 .7021 1.036 -.3164 .0016 -10.677 966.17 967.10 .6795 1.015 -.3086 .0016 ff� #3 -13.408 985.02 982.06 7112 1.041 -.3168 .0016 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 06:2.8:23 PM Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 957.33 .4426 .9294 855.93 -8.0506 979.15 SDev 16.04 .0062 .0135 11.16 2.9158 10.95 %RSD 1.6751 1.406 1.448 1.3042 36.219 1.1179 #1 962.94 .4453 .9364 861.63 -4.6858 987.62 ##2 939.24 .4355 .9139 843.07 -9.6294 966.79 #3 969.80 .4471 .9379 863.10 -9.8365 983.04 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1..200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 O O Analysis Report 09/15/06 06:35:55 PM page 1 zod: CLP1 Sample Name: CCV4 Operator: CD xuii Time: 09/15/06 18:28:30 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1003.1 49.77 514.03 2.558 2.562 2.545 48.66 SDev 1.6 .12 3.10 .006 .005 .005 .11 %RSD .15725 .2483 .60359 .2219 .2142 .2107 .2197 #1 1004.5 49.83 517.08 2.557 2.567 2.550 48.77 #2 1001.4 49.62 510.87 2.552 2.556 2.540 48.55 #3 1003.3 49.85 514.14 2.563 2.563 2.543 48.65 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.531 2.484 2.524 2.585 50.19 86.05 51.22 SDev .007 .004 .005 .005 .10 .22 .12 %RSD .2861 .1460 .1801 .1949 .2050 .2596 .2357 91 2.540 2.488 2.529 2.586 50.30 86.08 51.33 2.526 2.481 2.520 2.579 50.10 85.81 51.09 2.529 2.485 2.524 2.589 50.16 86.25 51.22 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.495 2.587 84.85 2.501 499.72 486.93 980.29 SDev .005 .004 .30 .007 2.39 .93 3.98 %RSD .2080 .1501 .3564 .2687 .47781 .18998 .40641 #1 2.500 2.589 84.72 2.508 497.48 487.46 976.12 #2 2.490 2.582 84.64 2.495 499.45 485.86 980.70 #3 2.495 2.589 85.20 2.501 502.23 487.46 984.05 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK 'NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 •Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 988.96 512.30 509.80 2.863 2.499 2.520 2.653 SDev 2.89 1.67 1.87 .068 .002 .005 .013 %RSD .29223 .32628 .36712 2.373 .0922 .2011 .4732 990.17 510.90 511.10 2.796 2.498 2.524 2.667 991.04 511.86 507.65 2.862 2.497 2.514 2.643 ff� #3 985.66 514.15 510.65 2.931 2.501 2.521 2.648 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 06:35:55 PM ,-gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 506.35 2.512 2.582 491.19 986.07 510.63 SDev 3.07 .005 .005 1.05 1.33 1.42 %RSD .60586 .1871 .1858 .21459 .13535 .27844 #1 509.84 2.517 2.586 490.79 985.49 511.03 #2 505.11 2.508 2.577 490.38 987..60 509.05 #3 504.08 2.511 2.583 492.38 985.12 511.81 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 09%15/06 06:43:26 PM page 1 ] Lod: CLP1 Sample Name: CCVL4 nu�Time: 09/15/06 18:36:01 ppm Comment: .0027 .0004 .0004 Mode: CONC Corr. Factor: 1 .0002 Elem Ag Al As1890 Units ppb ppm ppb Avge .53639 .0378 1.0970 SDev .47924 .0122 1:5945 %RSD 89.346 32.24 145.35 #1 .03518 .0497 2.8124 #2 .58385 .0382 .81861 #3 .99013 .0254 -.33990 Errors NOCHECK NOCHECK NOCHECK High .0007 .10758 .00948 Low .0001 .40221 .88547 Elem Cd Co Cr Units ppm , ppm ppm Avge .0005 -.0001 .0002 SDev .0003 .0002 .0003 %RSD 51.18 384.4 137.5 #1 .0008 .0001 .0005 .0006 -.0003 .0002 .0002 -.0000 -.0001 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge -.0003 .0061 2.583 SDev .0002 .0029 .048 %RSD 78.72 48.33 1.873 #1 -.0001 .0094 2.595 #2 -.0003 .0052 2.530 #3 -.0004 .0037 2.625 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 2.8569 .63272 1.9160 SDev 1.1162 1.9106 .9932 %RSD 39.070 301.97 51.835 4.1308 -.92111 2.4373 TV- 2.0497 2.7659 2.5401 #3 2.3904 .05333 .77076 Errors NOCHECK NOCHECK NOCHECK Operator: CD B Ba Be Ca ppm ppm ppm ppm .0027 .0004 .0004 .0220 .0008 .0001 .0002 .0115 29.31 31.87 45.31 52.02 .0036 .0005 .0005 .0330 .0026 .0004 .0005 .0230 .0020 .0002 .0002 .0101 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg ppm ppm ppm ppm .0000 2.520 .0374 .0315 .0001 .060 .0045 .0128 507.3 2.376 12.02 40.53 .0002 2.540 .0424 .0441 -.0001 2.452 .0360 .0318 .0000 2.567 .0338 .0185 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 2203/2 2068/1 PPM ppb ppb ppb .0007 .10758 .00948 5.0852 .0001 .40221 .88547 2.1857 13.98 373.87 9343.9 42.982 .0007 .44042 -1.0028 7.5925 .0006 .22168 .64035 4.0810 .0008 -.33935 .39086 3.5820 NOCHECK NOCHECK NOCHECK NOCHECK Si Sn Sr Ti ppm ppm ppm ppm .0799 -.0006 .0003 .0004 .0233 .0006 .0001 .0001 29.11 108.8 42.67 35.26 .1065 .0001 .0004 .0005 .0632 -.0011 .0003 .0005 .0701 -.0007 .0002 .0002 NOCHECK NOCHECK NOCHECK NOCHECK d O O Analysis Report 09/15/06 06:43:26 PM page 2 High Zn Low Sb2068 Elem T11908 Units ppb Avge 1.3786 SDev .3422 %RSD 24.819 ##1 1.6289 #2 1.5181 #3 .98870 Errors NOCHECK High 40.545 Low .0004 V Zn Pb2203 Sb2068 Se1960 PPM PPM Ppb Ppb Ppb .0005 .0007 .04219 3.5990 1.4887 .0002 .0002 .51967 1.4592 1.0520 33.44 32.13 1231.8 40.545 70.668 .0004 .0010 -.52215 5.2835 1.3189 .0006 .0006 .50098 2.7262 2.6153 .0003 .0006 .14774 2.7872 .53188 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK V) O O Analysis Report 09/15/06 06:50:57 PM page 1 hod: CLP1 Sample Name: CCB4 Operator: CD Time: 09/15/06 18:43:32 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .23933 .0187 1.1302 .0000 .0001 .0002 .0063 SDev .32955 .0025 1.7710 .0002 .0000 .0000 .0046 %RSD 137.69 13.30 156.69 568.0 27.29 21.57 72.87 ##1 .36178 .0162 -.70164 .0001 .0001 .0001 .0011 #2 .49013 .0212 1.2590 .0002 .0001 .0002 .0097 #3 -.13391 .0186 2.8333 -.0002 .0001 .0002 .0080 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 --.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 -.0000 -.0001 -.0002 .0063 .0293 .0147 SDev .0000 .00,01 .0001 .0002 .0021 .0017 .0046 %RSD 10.88 328.9 104.5 99.85 32.48 5.949 31.54 #1 .0002 -.0001 -.0000 -.0004 .0040 .0279 .0100 .0003 .0001 -.0000 .0000 .0080 .0312 .0193 .0003 -.0001 -.0001 -.0002 .0070 .0286 .0148 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0000 .0007 -.0080 .0005 -.31998 .09844 3.1295 SDev .0000 .0004 .0012 .0007 1.63783 1.4442 1.5502 %RSD 168.2 57.93 14.54 138.1 511.86 1467.0 49.536 #1 -.0000 .0011 -.0090 .0002 1.3462 1.5036 4.6745 #2 .0000 .0005 -.0067 .0012 -1.9279 .17358 1.5740 #3 -.0000 .0004 -.0081 -.0000 -.37817 -1.3819 3.1401 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 .1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.84616 .39742 2.5488 .0148 -.0004 .0001 .0001 SDev .54110 1.1796 2.1716 .0061 .0018 .0000 .0000 %RSD 63.948 296.82 85.202 41.56 453.6 23.97 34.72 -.50411 .62652 4.4911 .0218 -.0002 .0001 .0001 -.56436 -.87994 2.9512 .0116 -.0023 .0001 .0001 #3 -1.4700 1.4457 .20414 .0108 .0013 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 06:50:57 PM nlgh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.40482 .0001 .0008 -.04085 .47777 1.8324 SDev .405.36 .0005 .0001 1.31821 .64444 1.3005 %RSD 100.13 443.9 8.371 3227.1 134.88 70.969 #1 -.32974 .0005 .0007 1.4512 1.2204 3.2042 #2 -.84246 .0003 .0009 -.52618 .14775 1.6755 #3 -.04225 -:0004 .0008 -1.0476 .06519 .61759 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 11 Lod: CLP1 Sample Name: MB -18259 Time: 09/15/06 18:51:04 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .37217 .0047 -1.4463 - SDev .33463 .0009 1.4517 %RSD 89.913 19.43 100.37 #1 .69575 .0051 -3.0573 - #2 .39327 .0037 -1.0418 #3 .02749 .0054 -.23977 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge .0000 -.0004 .0001 SDev .0001 .0002 .0003 %RSD 297.1 55.36 225.2 #1 .0000 -.0004 .0004 -.0001 -.0001 .0002 .0001 -.0005 -.0002 Errors LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem Mn Mo Na Units ppm ppm ppm Avge -.0003 -.0001 -.0102 SDev .0001 .0004 .0003 %RSD 17.93 298.5 2.635 #1 -.0002 .0000 -.0101 #2 -.0003 -.0005 -.0099 #3 -.0003 .0001 -.0105 Errors LC Pass NOCHECK LC Pass High .0150 5.000 Low -.0150 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge .06329 -3.8265 1.3933 SDev 1.4399 1.7499 .7964 %RSD 2274.9 45.731 57.158 1.4332 -3.9535 2.2052 -1.4376 -5.5095 1.3614 #3 .19429 -2.01.66 .61337 Errors NOCHECK NOCHECK NOCHECK 09/15/06 06:58:29 PM page 1 Operator: CD B Ba Be Ca ppm ppm ppm ppm .0008 -.0000 .0000 -.0103 .0001 .0000 .0000 .0004 18.35 159.3 38.16 3.854 .0007 .0000 .0000 -.0105 -.0010 -.0001 .0000 -.0106 -.0008 -.0000 .0000 -.0099 LC Pass LC Pass LC Pass LC Pass 2000 .2000 .0050 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K Mg ppm ppm ppm. ppm -.0004 -.0057 .0230 -.0018 .0002 .0001 .0020 .0012 59.52 2.352 8.532 63.04 -.0004 -.0057 .0238 -.0006-.0002 -.0055 .0244 -.0021 -.0006 -.0058 .0208 -.0028 LC Pass LC Pass LC Pass LC Pass 0250 .1000 5.000 .2000 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb 0004 1.1212 1.0060 2.6297 0003 1.7339 1.1063 .0523 67.64 154.66 109.98 1.9873 0004 3.0859 .96006 2.6092 0007 -.19484 2.1345 2.6891 0001 .47239 -.07669 2.5908 LC Pass NOCHECK NOCHECK NOCHECK 0400 -.0400 Si Sn Sr Ti I ppm ppm ppm -.0257 .0002 -.0001 .0006. .0008 .0019 .0000 .0001 3.287 840.1 40.82 10.75 -.0258 .0024 -.0000 .0007 -.0265 -.0011 -.0000 .0006 -.0248 -.0006 -.0001 .0006 NOCHECK NOCHECK NOCHECK NOCHECK 00 O O H 00 O O H Analysis Report 09/15/06 06:58:29 PM ix-gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.56175 .0001 .0006 1.0444 .91794 -.34486 SDev 1.58884 .0002 .0000 .8270 .94632 .545.19 %RSD 282.84 161.3 6.477 79.191 103.09 158.09 #1 .93166 .0001 .0006 1.6680 1.8248 .15440 #2 -2.2313 .0003 .0006 1.3589 -.06339 -.92658 #3 -.38558 -.0001 .0007 .10620 .99236 -.26239 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200. -3.0000 -60.000 -5.0000 page 2 O O Analysis Report hiod: CLP1 Sample Name: LCS-18259 nu,Time: 09/15/06 18:58:36 Comment: Mode: CONC Corr. Factor: 1 09/15/06 07:06:01 PM Operator: CD Elem Ag Al As1890 B Units ppb ppm ppb ppm Avge 991.30 49.08 511.73 2.527 SDev 63.86 3.32 34.19 .162 %RSD 6 4422 6.773 6.6817 6.417 #1 1065.0 52.92 551.21 2. #2 956.62 47.28 492.14 2. #3 952.29 47.05 491.84 2. Errors LC Pass LC Pass LC Pass LC High 1200.0 60.00 600.00 3. Low 800.00 40.00 400.00 2. Elem Cd Co Cr Cu Units ppm ppm ppm pp Avge 2.502 2.457 2.497 2. SDev .167 .161 .168 %RSD 6..692 6.546 6.740 6. #1 2.695 2.642 2.691 2. 2.410 2.367 2.405 2. 2.401 2.360 2.395 2. Errors LC Pass LC Pass LC Pass LC High 3.000 3.000 3.000 3 Low 2.000 2.000 2.000 2. Eleni Mn Mo Na Nj Units ppm ppm ppm pp Avge 2.468 2.559 83.69 2 SDev .164 .171 4.79 %RSD 6.632 6.663 5.720 6 #1 2.657 2.756 89.21 2 #2 2.377 2.468 81.06 2 #3 2.370 2.454 80.78 2 Errors LC Pass NOCHECK LC Pass L High 3.000 96.00 3 Low 2.000 64.00 2 Elem 206.8/2 1960/1 1960/2 S' Units ppb ppb ppb p Avge 980.57 509.66 510.04 2 SDev 52.57 29.24 23.88 %RSD 5.3614 5.7362 4.6817 6 L 1041.1 543.41 537.55 3 -,2 954.39 493.39 497.88 2 #3 946.22 4.92.18 494.69 2 714 436 430 Pass 000 000 m 554 169 621 749 461 452 Pass .000 000 m .471 163 605 659 380 .373 C Pass .000 .000 1 pm .883 .198 .865 .111 .757 .780 Ba ppm 2.533 .166 6.559 2.724 2.440 2.433 LC Pass 3.000 2.000 Fe ppm 49.59 3.41 6.873 53.52 47.72 47.52 LC Pass 60.00 40.00 2203/1 ppb 496.93 27.88 5.6099 529.04 482.85 478.90 NOCHECK Sn PPM 2.474 .160 6.460 2.658 2.384 2.379 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Be ppm 2.518 .167 6.622 2.711 2.425 2.419 LC Pass 3.000 2.000 K ppm 84.99 5.31 6.242 91.11 82.09 81.76 LC Pass 96.00 64.00 2203/2 ppb 483.29 26.43 5.4684 513.78 469.17 466.93 NOCHECK Sr ppm 2.493 .164 6.562 2.681 2.401 2.395 NOCHECK page 1 Ca ppm 48.13 3.20 6.645 51.82 46.36 46.21 LC Pass 60.00 40.00 Mg ppm 50.53 3.33 6.590 54.37 4'8.70 48.50 LC Pass 60.00 40.00 2068/1 ppb 974.84 46.14 4.7328 1027.9 952.42 944.19 NOCHECK Ti ppm 2.623 .185 7.047 2.837 2.520 2.513 NOCHECK Analysis Report 09/15/06.07:06:01 PM ugh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 499.59 2.485 2.554 487.83 978.66 509.91 SDev 33.54 .166 .168 26.91 50.43 25.66 %RSD 6.7141 6.661 6.568 5.5159 5.1528 5.0315 #1 538.31 2.676 2.748 518.86 1036.7 539.50 #2 481.12 2.393 2.462 473.72 953.73 496.38 #3 479.34 2.386 2.453 470.92 945.55 493.86 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 600.00 3.000 3.000 600.00 1200.0 600.00 Low 400.00 2.000 2.000 400.00 800.00 400.00 page 2 Analysis Report 09/15/06 07:13:33 PM page 1 1 iod: CLP1 Sample Name: 0609771-003A Operator: CD xun Time: 09/15/06 19:06:07 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .44827 .3233 2.5894 .0974 .0101 .0005 33.67 SDev .53822 .0023 .4416 .0003 .0001 .0002 .44 %RSD 120.07 .6993 17.055 .2877 .7021 35.28 1.315 #1 1.0625 .3252 2.8326 .0974 .0101 .0007 33.31 #2 .22320 .3208 2.0796 .0971 .0100 .0005 33.55 #3 .05911 .3240 2.8560 .0977, .0100 .0003 34.17 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0009 .0016 .0082 .1692 10.74 23.65 SDev .00.02 .0005 .0002 .0001 .0016 .11 .30 %RSD 37.48 61.21 11.76 1.353 .9370 1.069 1.274 #1 .0008 .0012 .0017 .0083 .1708 10.66 23.40 #2 .0006 .0011 .0016 .0081 .1691 10.68 23.57 #3 .0004 .0003 .0014 .0082 .1676 10.87 23.99 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb 3e .0250 .0104 196.2 .0090 3.0412 .99930 6.8506 SDev .0001 .0035 2.0 .0003 .6186 .55147 1.5530 %RSD .4931 33.92 .9955 3.672 20.340 55.185 22.670 #1 .0249 .0142 195.2 .0089 2.5468 1.4269 8.4298 #2 .0249 .0096 195.0 .0094 2.8420 .37685 6.7967 #3 .0251 .0073 198.5 .0088 3.7349 1.1942 5.3252 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb Ppb Ppm Ppm Ppm Ppm Avge 3.4188 -1.7268 3.1935 2.105 .0148 .1538 .0024 SDev 2.5636 .4716 1.9270 .012 .0002 .0023 .0003 %RSD 74.983 27.311 60.340 .5794 1.317 1.482 13.73 #1 3.5237 -1.4702 4.0106 2.108 .0150 .1520 .0028 #2 5.9283 -1.4391 .99266 2.092 .0148 .1530 .0023 #3 .80446 -2.2710 4.5774 2.115 .0147 .1564 .0022 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.17162 .0206 .2117 1.6793 4.5616 1.5551 SDev 1.01430 .0001 .0026 .4340 2.0208 1.1897 %RSD 591.02 .4239 1.220 25.845 44.301 76.500 #1 .34057 .0206 .2097 1.7998 5.1575 2.1855 "�.2175 48446 .0207 .2108 1.1977 6 .18291 -1.3399 .0205 .2146 2.0403 2.3099 2.2969 Analysis Report 09/15/06 07:21:04 PM page 1 1 Lod: CLP1 Sample Name: 0609771-005A Operator: CD Time: 09/15/06 19:13:39 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .35533 .0943 -.74412 .0848 .0090 .0001 32.76 SDev .48466 .0037 .70985 .0004 .0000 .0000 .20 %RSD 136.40 3.962 95.395 .4500 .4371 19.34 .6105 #1 .19869 .0976 -.07568 .0848 .0091 .0001 32.92 #2 -.03163 .0951 -1.4892 .0851 .0091 .0001 32.82 #3 .89894 .0902 -.66751 .0844 .0090 .0001 32.54 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0002 .0007 .0061 .1472 10.87 23.25 SDev .0001 .0003 .0002 .0001 .0015 .07 .15 0-cRSD 69.94 176.4 28.58 1.216 1.000 ,6540 .6305 #1 .0001 -.0001 .0007 .0060 .1485 10.93 23.37- #2 .0000 .0002 .0010 .0061 .1476 10.89 23.30 #3 .0001 .0005 .0006 .0061 .1456 10.79 23.09 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb 4e .0240 .0058 193.4 .0083 2.1721 .78563 4.4043 SDev .0002 .0007 1.1 .0007 1.5928 .82000 .8953 %RSD .6556 11.85 .5739 8.061 73.329 104.37 20.327 #1. .0242 .0065 194.3 .0084 3.2137 .18405 4.6758 .0241 .0059 193.7 .0089 2.9639 .45318 3.4047 _#2 #3 .0239 .0051 192.2 .0075 .33857 1.7196 5.1324 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.47638 -3.1567 2.5434 1.995 -.0002 .1.495 .0014 SDev 3.94380 2.1463 1.4841 .021 .0014 .0012 .0001 %RSD 827.86 67.993 58.352 1.051 847.0 .8054 3.779 #1 -3.2531 -2.3814 -2.143.4 2.014 -.0018 .1503 .0014 #2 -2.2138 -1.5057 4.1866 1.997 :0008 .1501 .0013 #3 4.0378 -5.5829 1.3003 1.973 .0004 .1481 .0013 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.69890 .0200 .1245 1.2474 1.1489 .64531 SDev 1.06404 .0004 .0007 .0494 2.8208 1.6415 %RSD 1.52.25 2.050 .5733 3.9567 245.52 254.37 #1 -1.8291 .0201 .1252 1.1930 -.61280 .63665 .0203 .1246 1.2893 -.34282 2.2911 .28351 -.55110 .0195 .1238 1.2598 4.4023 -.99180 Analysis Report 09/15/06 07:28:36 PM 1 Lod: CLP1 Sample Name: 0609771-005ADUP Operator: CD 1, Time: 09/15/06 19:21:11 Comment: Mode: CONC. Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .10771 .0917 -.18274 .0829 .0089 .0001 SDev .22168 .0031 1.42291 .0011 .0001 .0000 %RSD 205.81 3.417 778.63 1.336 1.279 26.18 #1 .15750 .0930 .87732 .0832 .0089 .0001 #2 -.13463 .0939 .37435 .0838 .0090 .0001 #3 .30026 .0881 -1.7999 .0816 .0087 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 .0002 .0005 .0059 .1458 10.34 SDev .0001 .0001 .0001 .0001 .0018 .12 %RSD 73.79 28.79 17.61 2.15.9 1.244 1.198 #1 .0000 .0002 .0005 .0061 .1469 10.42 #2 .0001 .0002 .0005 .0060 .1468 10.41 #3 .0001 .0003 .0004 .0058 .1437 10.20 Elem Mn Mo Na Ni 2203/1 2203/2 -- t t s ppm ppm ppm ppm ppb ppb �e .0239 .0048 192.9 .0080 2.1806 1.5914 oLev .0004 .0004 1.7 .0004 .5093 .6868 %RSD 1.488 8.690 .8876 5.068 23.356 43.154 #1 .0241 .0049 194.2 .0083 2.0125 2.2186 #2 .0241 .0043 193.5 .0082 2.7527 .85753 #3 .0235 .0051 190.9 .0075 1.7766 1.6983 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .52041 -2.9160 2.3614 1.99.3 .0003 .1484 SDev 2.3602 1.1429 1.3624 .028 .0018 .0019 %RSD 453.53 39.192 57.693 1.407 531.4 1.306 #1 3.2110 -2.1744 1.0249 2.012 .0010 .1492 #2 -1.2007 -4.2322 3.7483 2.007 .0017 .1498 #3 -.44903 -2.3415 2.3110 1.961 -.0017 .1462 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.53734 .0195 .1242 1.7877 1.1.391 .60403 SDev 1.44424 .0006 .0017 .3352 1.2903 ..58187 %RSD 268.78 3.216 1.336 18.748 113.28 96.330 #1 .37120 .0201 .1250 2.1500 2.5305 -.04042 42 -2.2027 .0194 .1253 1.4887 -.01803 1.0908 .21949 .0189 .1223 1.7244 .90475 .76171 page 1 Ca ppm 32.66 .42 1.296 32.88 32.93 32.17 Mg ppm 23.20 .29 1.257 23.35 23.38 22.86 2068/1 ppb 2.3782 1.2248 51.500 1.1673 2.3509 3.6164 Ti ppm .0013 .0001 5.661 .0012 .0013 .0013 Analysis Report 09/15/06 07:36:08 PM page 1 iod: CLP1 Sample Name: 0609771-005AMS Operator: CD Time: 09/15/06 19:28:42 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 43.822 2.088 41.869 .0829 2.067 .0520 32.70 SDev .283 .024 .695 .0004 .021 .0005 .31 %RSD .64481 1.148 1.6589 .5468 .9944 .9549 .9552 #1 43.531 2.067 41.218 .0827 2.051 .0516 32.42 #2 44.095 2.114 42.600 .0835 2.090 .0526 33.04 #3 43.842 -2.082 41.788 .0827 2.061 .0519 32.64 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0509 .4983 .2058 .2723 1.131 10.64 23.17 SDev .0004 .0052_ .0023 .0030 .011 .11 .23 %RSD .7864 1.035 1.118 1.117 .9953 1.051 1.011 #1 .0507 .4940 .2039 .2698 1.121 10.54 22.97 #2 .0513 .5040 .2083 .2757 1.143 10.76 23.43 #3 .0506 .4970 .2051 .2714 1.128 10.61 23.12 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb - ppb ge .5287 .0043 192.4 .5112 22.684 20.497 503.32 SDev .0051 .0005 2.1 .0036 2.316 1.341 4.43 %RSD .9671 12.35 1.108 .7075 10.211 6.5404 .87997 #1 .5245 .0048 190.5 .5076 23.757 19.954 499.79 #2 .5344 .0038 194.7 .5148 24.269 19.514 508.29 #3 .5273 .0043 192.0 .5112 20.026 22.024 501.89 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 506.43 6.0301 11.775 2.021 .0127 .1489 .0014 SDev 4.18 2.3669 1.170 .023 .0020 .0015 .0001 %RSD .82549 39.252 9.9361 1.135 15.91 1.040 9.690 #1 502.25 6.4927 11.579 2.001 .0106 .1474 .0015 #2 510.61 8.1315 13.031 2.046 .0146 .1505 .0014 #3 506.43 3.4660 10.716 2.016 .0128 .1490 .0013 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 47.461 .5274 .6461 21.226 505.39 9.8621 SDev 1.595 .0051 .0067 .131 4.22 1.5491 %RSD 3.3607 .9600 1.036 .61634 .83589 15.708 #1 45.738 .5233 .6404 21.221 501.43 9.8856 Un 47.761 .5330 .6535 21.097 509.84 11.399 48.885 .5259 .6445 21.359 504.91 8.3014 N O O U1 H Analysis Report 09/15/06 07:43:39 PM page 1 I od: CLP1 Sample Name: 0609772-010A Operator: CD Ruin Time: 09/15/06 19:36:14 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .21626 .0246 -1.5153 .0164 .0126 .0001 14.96 SDev .10179 .0023 .5349 .0004 .0002 .0000 .04 %RSD 47.070 9.522 35.303 2.278 1.893 46.52 .2738 #1 .14494 .0272 -1.5375 .0164 .0128 .0001 14.91 #2 .17101 .0240 -.96959 .0160 .0126 .0001 14.98 #3 .33284 .0226 -2.0388 .0167 .0123 .0000 14.98 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0000 -.0003 .0025 .0148 .0731 1.283 3.354 SDev .0000 .0004 .0002 .0001 .0004 .001 .007 %RSD 38.24 122.3 6.868 .8294 .5174 .1122 .2036 #1 -.0000 -.0001 .0025 .0148 .0732 1.282 3.346 #2 -.0000 -.0001 .0027 .0147 .0734 1.282 3.360 #3 -.0001 -.0008 .0024 .0150 .0727 1.284 3.355 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb 4e .0039 -.0006 8.821 .0013 2.7693 1.3441 2.4201 SDev .0001 .0004 .009 .0006 .9369 .2223 1.9088 %RSD 1.565 63.65 .0995 47.22 33.832 16.542 78.874 #1 .0039 -.0007 8.825 .0020 3.8300 1.4548 2.7310 #2 .0039 -.0002. 8.811 .0008 2.4236 1.4895 .37486 #3 .0038 -.0010 8.827 .0011 2.0544 1.0882 4.1543 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.1359 -3.7718 2.2985 2.393 -.0002 .0387 .0075 SDev 2.4213 3.2249 .4513 .005 .0009 .0002 .0001 %RSD 213.17 85.500 19.635 .1932 451.6 .4968 1.366 #1 1.4283 -.12064 1.7779 2.389 .0004 .0385 .0074 #2 -3.3831 -6.2311 2.5377 2.392 .0002 .0389 .0074 #3 -1.4528 -4.9637 2.5799 2.398 -.0012 .0387 .0076 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.9283 .0007 .0283 1.8188 .04828 .27709 SDev 1.8826 .0002 .0001 .4182 2.0219 .78521 %RSD 97.628 27.47 .2573 22.993 4187.7 283.38 #1 -3.7198 .0009 .0284 2.2458 1.8621 1.1457 u^ -2.0991 .0006 .0283 1.8006 -2.1317 -.38232 .03382 .0006 .0282 1.4100 .41441 .06787 Analysis Report 09/15/06 07:51:11 PM iod: CLP1 Sample Name: 0609772-012A Operator: CD Time: 09/15/06 19:43:46 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .26319 .0325 .50216 .0185 .0135 .0000 SDev .15139 .0009 .49484 .0002 .0001 .0000 0-oRSD 57.520 2.639 98.543 1.134 .3555 117.6 #1 .19055 .0334 .53687 .0183 .0136 .0000 #2 .43720 .0323 -.00912 .0184 .0135 .0000 #3 .16181 .0318 .97874 .0187 .0135 .0000 Elem Cd Co Cr Cu Fe K' Units ppm ppm ppm ppm ppm ppm Avge .0002 .0000 .0031 .1211 .3626 1.661 SDev .0001 .0006 .0002 .0002 .0001 .002 %RSD 90.41 8534. 5.006 .1671 .0292 .1158 #1 .0002 .0005 .0033 .1213 .3625 1.663 #2 .0003 .0001 .0031 .1209 .3627 1.661 #3 .0000 -.0006 .0030 :1212 .3625 1.659 Elem Mn Mo Na Ni 2203/1 2203/2 its ppm ppm ppm ppm ppb ppb 3e .0095 .0003 12.17 .0062 3.0625 2.6482 buev .0001 .0001 .04 .0005 1.6711 .9778 %RSD .4912 40.54 .2956 8.377 54.566 36.924 #1 .0096 .0004 12.12 .0065 4.8761 1.9840 #2 .0096 .0004. 12.18 .0064 1.5851 3.7710 #3 .0095 .0002 12.19 .0056 2.7264 2.1896 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge -.59956 -2.0207 .78452 2.736 -.0006 .0413 SDev 1.81245 3.0337 .42731 .002 .0010 .0001 %RSD 302.30 150.13 54.468 .0601 162.3 .2567 #1 1.4933 -3.9808 1.1872 2.735 -.0000 .0412 #2 -1.6460 -3.5549 .33621 2.738 -.0017 .0413 #3 -1.6460 1.4737 .83018 2.735 -.0000 .0414 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.6121 .0005 .0512 2.7862 .75868 -.14960 SDev 2.2255 .0003 .0001 .3650 .68224 1.05578 %RSD 138.05 51.38 .2318 13.102 89.925 705.74 #1 .41097 .0008 .0512 2.9471 1.4030 -.53373 #2 -1.2514 .0004 .0510 3.0431 .82906 -.95953 -3.9960 .0004 .0513 2.3683 .04398 1.0445 page 1 Ca PPM 16.10 .02 .0939 16.09 16.12 16.10 Mg PPM 3.567 .006 .1674 3.560 3.571 3.570 2068/1 ppb 3.4792 2.2826 65.607 1.2221 5.7865 3.4289 Ti ppm .0062 .0002 2.641 .0061 .0064 .0062 Analysis Report 09/15/06 07:58:43 PM page 1 Zod: CLP1 Sample Name: 0609772-013A Operator: CD Time: 09/15/06 19:51:18 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .35297 .0389 -1.0727 .0184 .0128 .0000 15.42 SDev .17678 .0009 1.3322 .0001 .0000 .0000 .01 %RSD 50.084 2.233 124.20 .7740 .0885 33.74 .0345 #1 .25298 .0399 -.24884 .0183 .0128 .0000 15.42 #2 .24884 .0384 -.35950 .0183 .0128 .0000 15.43 #3 .55709 .0385 -2.6096 .0186 .0128 .0000 15.42 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 -.0004 .0030 .1560 .1215 1.795 3.397 SDev .0001 .0001 .0001 .0003 .0002 .006 .002 %RSD 357.7 22.31 4.081 .2084 .1793 .3117 .0733 #1 .0000 -.0004 .0031 .1557 .1213 1.801 3.396 #2 .0002 -.0003 .0029 .1560 .1217 1.796 3.400 #3 -.0001 -.0004 .0029 .1563 .1215 1.789 3.395 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb ge .0052 .0049 19.64 .0019 4.4152 3.0967 2.5605 SDev .0001 .0001 .02 .0002 1.6220 1.5836 1.8179 %RSD 1.519 1.005 .1065 11.56 36.736 51.138 71.000 #1 .0053 .0050 19.66 .0017 4.4926 1.3956 .61515 #2 .0053 .0049 19.62 .0020 5.9971 3.3663 4.2163 #3 .0051 .0049 19.64 .0021 2.7559 4.5282 2.8500 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .87561 -5.0664 2.1673 2.554 .0015 .0397 .0077 SDev .39110 2.0120 2.0221 .003 .0016 .0001 .0000 %RSD 44.665 39.713 93.303 .1184 109.2 .3897 .1308 #1 .50314 -6.7173 4.4717 2.558 .0026 .0396 .0077 #2 1.2830 -5.6566 1.3411 2.553 .0023 .0397 .0077 #3 .84070 -2.8253 .68908 2.552 -.0004 .0399 .0076 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.0557 .0013 .0355 3.5359 1.4367 -.24153 SDev .8048 .0002 .0001 .9723 .8620 .89195 %RSD 76.235 12.73 .1852 27.497 59.999 369.29 #1 -1.7872 .0011 .0355 2.4270 .54046 .74577 #2 -1.1864 .0014 .0354 4.2425 2.2598 -.98917 -.19353 .0015 .0355 3.9381 1.5098 -.48119 00 N O O Analysis Report 09/15/06 08:06:14 PM page 1 P od: CLP1 Sample Name: 0609775-003A Operator: CD kun Time: 09/15/06 19:58:49 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .13150 .0151 -1.3262 .0065 .0006 .0001 6.673 SDev .32387 .0005 1.0910 .0006 .0000 .0000 .039 %RSD 246.29 3.142 82.264 9.118 7.058 76.44 .5825 #1 -.12422 .0147 -2.2226 .0059 .0006 .0000 6.645 #2 .02303 .0150 -1.6447 .0067 .0006 .0001 6.657 #3 ..49568 .0156 -.11144 .0071 .0006 .0000 6.718 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 -.0004 .0007 .1501 .0305 1.158 2.373 SDev .0001 .0003 .0003 .0003 .0007 .008 .013 %RSD 53.89 78.14 45.82 .2186 2.188 .6760 .5649 #1 -.0002 -.0007 .0005 .1498 .0300 1.152 2.364 #2 -.0002 -.0004 .0005 .1502 .0302 1.155 2.366 #3 -.0001 -.0001 .0010 .1504 .0312 1.166 2.388 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb .003.2 -.0002 8.234 .0031 1.9085 1.7484 3.3177 _4e SDev .0001 .0006 .041 .0003 2.0369 .2431 .6558 %RSD 4.180 262.5 .4965 9.579 106.73 13.906 19.766 #1 .0031 .0003 8.189 .0029 1.3804 1.6732 4.0681 #2 .0031 -.0008 8.268 .0031 4.1574 2.0202 2.8548 #3 .0033 -.0002 8.244 .0034 .18758 1.5517 3.0302 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.4750 -4.1483 1.4281- 3.183 .0003 .0019 .0013 SDev 1.0790 2.1758 2.0590 .014 .0001 .0001 .0001 %RSD 73.154 52.451 144.18 .4514 37.75 3.187 11.35 #1 -2.4555 -2.7053 3.6570 3.167 .0003 .0019 .0012 #2 -1.6506 -3.0886 1.0303 3.186 .0004 .0019 .0012 #3 -.31895 -6.6510 -.40295 3.196 .0002 .0020 .0014 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb Ppb ppb Avge -.40389 .0211 .0574 1.8017 .12098 -.42881 SDev 1.19594 .0005 .0003 .8403 .58864 2.01237 %RSD 296.11 2.336 .5391 46.640 486.57 469.29 #1 .94481 .0214 .0571 1.5758 -.28311 1.5384 �^ -.82127 .0205 .0574 2.7319 -.15030 -.34129 -1.3352 .0214 .0577 1.0975 .79634 -2:4835 Analysis Report 09/15/06 08:13:46 PM page 1 Lod: CLP1 Sample Name: CCV5 Operator: CD nuii Time: 09/15/06 20:06:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1001.7 49.86 513.05 2.553 2.557 2.543 48.70 SDev 2.0 .06 1.12 .003 .004 .004 .08 %RSD .19577 .1138 .21754 .1021 .1548 .1553 .1555 #1 1003.0 49.93 512.13 2.550 2.560 2.546 48.78 #2 1002.7 49.83 512.74 2.554 2.560 2.544 48.70 #3 999.48 49.83 514.29 2.554 2.553 2.538 48.63 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.527 2.486 2.524 2.582 50.15 86.25 51.08 SDev .006 .003 .005 .002 .13 .12 .05 %RSD .2255 .1143 .1827 .0766 .2616 .1415 .0911 #1 2.533 2.487 2.528 2.581 50.27 86.39 51.13 2.526 2.487 2.525 2.584 50.16 86.19 51.08 2.521 2.482 2.519 2.580 50.01 86.17 51.03 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.493 2.584 84.98 2.496 500.76 487.27 976.85 SDev .004 .002 .08 .007 1.20 1.39 7.24 %RSD .1524 .0687 .0918 .2818 .23992 .28541 .74108 #1 2.496 2.583 85.02 2.504 502.15 488.86 968.70 #2 2.494 2.584 84.89 2.492 500.04 486.67 979.31 #3 2.489 2.586 85.02 2.492 500.09 486.29 982.54 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 985.98 513.58 511.61 2.789 2.507 2.518 2.653 SDev 3.39 .70 .70 .086 .007 .003 .009 0-oRSD .34425 .13606 .13744 3.088 .2759 .1382 .3442 982.10 514.24 511.91 2.700 2.500 2.520 2.663 987.40 513.65 512..11 2.794 2.510 2.520 2.651 n� #3 988.42 512.85 510.80 2.872 2.513 2.514 2.645 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK O M O O r4 H Analysis Report 09/15/06 08:13:46 PM n.Ly4h Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 500.73 2.510 2.579 491.76 982.94 512.26 SDev 1.82 .004 .003 1.32 4.67 .68 %RSD .36440 .1576 .1113 .26929 .47525 .13213 #1 501.22 2.513 2.582 493.29 977.64 512.69 #2 498.71 2.511 2.580 491.12 984.71 512.62 #3 502.25 2.505 2.576 490.88 986.46 511.48 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 M O O r4 V) N Analysis Report 09/15/06 08:21:18 PM page 1 zod: CLP1 Sample Name: CCVL5 .Kuri Time: 09/15/06 20:13:52 ppm Comment: ppm .0024 .0004 Mode: CONC Corr. Factor: 1 .0009 Elem Ag Al As1890 Units ppb ppm ppb Avge .41413 .0121 .79664 SDev .20357 .0051 1.4391 %RSD 49.155' 41.98 180.65 #1 .62385 .0178 2.4581 #2 .21732 .0100 -.00918 #3 .40123 .0084 -.05902 Errors NOCHECK NOCHECK NOCHECK High ppb ppb .0005 Low 1.3578 5.4877 .0002 Elem Cd Co Cr Units ppm ppm ppm Avge .0006 .0001 .0001 SDev .0002 .0005 .0001 %RSD 27.97 400.1 121.0 #1 .0006 .0005 .0001 .0008 .0003 .0000 .0004 -.0004 .0000 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge -.0002 .0060 2.583 SDev .0001 .0037 .013 %RSD 45.24 61.87 .5182 #1 -.0001 .0099 2.580 #2 -.0003 .0056 2.597 #3 -.0003 .0025 2.571 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 2.5641 .50208 2.0974 SDev 2.6028 .95021 .6091 %RSD 101.51 189.25 29.043 L 5.3954 1.5874 2.6994 rr2 2.0216 -.17985 1.4813 #3 .27525 .09866 2.1114 Errors NOCHECK NOCHECK NOCHECK Operator: CD B Ba Be Ca PPM ppm ppm ppm .0024 .0004 .0004 -.0009 .0009 .0001 .0001 .0019 38.34 33.52 25.54 206.3 .0035 .0005 .0005 .0011 .0022 .0004 .0004 -.0012 .0016 .0002 .0003 -.0026 NOCHECK NOCHECK NOCHECK NOCHECK Cu Fe K Mg Ppm PPm Ppm Ppm -.0000 2.469 .0374 .0073 .0001 .007 .0034 .0041 295.1 .2926 9.169 55.74 .0001 2.469 .0414 .0116 -.0001 2.476 .0351 .0066 -.0001 2.461 .0358 .0036 NOCHECK LC Pass NOCHECK NOCHECK 2.750 2.250 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0005 -.95753 1.3578 5.4877 .0002 2.09007 .4992 1.9467 49.37 218.28 36.762 35.474 .0006 -2.4358 .82116 7.7320 .0007 1.4337 1.4440 4.4751 .0002 -1.8705 1.8082 4.2560 NOCHECK NOCHECK NOCHECK NOCHECK Si Sn Sr Ti PPM PPM ppm ppm .0654 -.0004 .0003 .0004 .0192 .0011 .0001 .0002 29.32 259.5 32.68 53.41 .0857 .0001 .0005 .0007 .0627 .0003 .0003 .0005 .0477 -.0017 .0002 .0002 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 08:21:18 PM page 2 _jh Zn Low Sb2068 Elem T11908 Units ppb Avge 2.7077 SDev 1.8068 %RSD 66.727 #1 3.1523 #2 4.2508 #3 .72018 Errors NOCHECK High 66.855 Low .0006 v Zn Pb2203 Sb2068 Sel960 PPM ppm ppb ppb ppb .0003 .0014 .58683 3.5377 1.5662 .0003 .0002 .85198 2.3651 .7088 80.07 15.44 145.18 66.855 45.256 .0006 .0017 -.26336 6.1735 2.3291 .0003 .0015 1.4406 2.8387 .92817 .0001 .0012 .58327 1.6008 1.4412 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 08:28:50 PM page 1 1 eod: CLP1 Sample Name: CCB5 Operator: CD Time: 09/15/06 20:21:24 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .26427 .0062 -.18023 -.0003 .0001 .0001 -.0047 SDev .38737 .0006 1.05071 .0006 .0000 .0000 .0005 %RSD 146.58 10.17 582.99 201.3 22.46 10.11 10.89 #1 -.15543 .0067 -1.2310 .0003 .0001 .0001 -.0052 #2 .60808 .0065 .87040 -.0003 .0001 .0001 -.0042 #3 .34014 .0055 -.18006 -.0010 .0000 .0001 -.0048 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0005 -.0002 -.0005 .0013 .0250 .0009 SDev .0001 .0001 .0002 .0003 .0002 .0066 .0014 %RSD 74.84 21.44 105.8 55.44 19.15 26.56 155.8 #1 .0001 -.0004 -.0003 -.0006 .0013 .0221 .0010 .0001 -.0005 .0000 -.0002 .0015 .0326 .0022 .0000 -.0007 -.0003 -.0007 .0010 .0204 -.0006 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0001 .0008 -.0037 .0000 .14962 .78924 3.2343 SDev .0001 .0004 .0007 .0004 .68282 .43072 2.1892 %RSD 65.45 51.07 19.90 2053. 456.38 54.573 67.687 #1 -.0001 .0012 -.0036 .0001 .80833 .45099 5.7563 #2 -.0000 .0008 -.0030 .0004 .19552 .64260 1.8244 #3 -.0002 .0004 -.0045 -.0004 -.55500 1.2741 2.1222 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.68566 -1.5092 2.0899 .0051 -.0011 .0000 .0001 SDev 1.79091 1.8124 1.3831 .0038 .0002 .0000 .0001 -RSD 261.19 120.09 66.182 74.96 22.07 53.43 90.19 -2.6545 -2.0267 3.2537 .0063 -.0013 .0000 .0001 .84666 -3.0065 .56079 .0080 -.0012 .0001 .0002 #3 -.24918 .50570 2.4552 .0008 -.0008 .0000 .0000 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 08:28:50 PM -gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.20224 .0002 .0002 .57628 .61970 .89144 SDev 2.53967 .0001 .0001 .08581 .51752 1.3242 %RSD 1255.8 36.08 28.97 14.891 83.511 148.55 #1 -.81679 .0001 .0001 .57003 .14634 1.4954 #2 2.5883 .0003 .0002 .49377 1.1723 -.62708 #3 -2.3782 .0001 .0002 .66505 .54052 1.8060 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 0 page 2 M O O C/1 O O 7J a w E869'E b8T'7v:� SL'fL'Z S8T0' :iTO'Z 8STST'- F' ST'S6Z L06' Z:� :i:K7 'T S8T0' 600' Z ZLO8' T- ( rr 9:i69TV' 8:VS'ZTI TT90'T L8TO' 800'Z Z889T' T# OEZ'TL OTTO'Z 980'TS iv8TS' 6691' SL'LLT QSU% E069'T 9L8' H88' T000' E00' 9SO90'T naQS TELE'Z 9ivS'E:v OTPL'T 9810' OTO'Z L996S'- GBAV qdd qdd qdd wdd wdd qdd S-4zun 096TaS 890ZgS EOZZgd uZ A 806TTZ waTS LT00' 09TT' OT00' ESS'Z 86E0'9 Z6T66'- 08E'E7v E# 8T00' SSTT' TZ00' 6vS'Z Z86E'E L9SO'Z TTO'TP Z# 6T00' 'vSTT' 9Z00'- 8SS'Z EE8U Z Ob9E'E- 9EZ'0t, T## 9Z0'p E89Z' LL'Tlv ZLLT' :�06'LD, 9S':FS£ :�EV6'E QSU% T000' E000' 8000' SOO' 9L88'T 9ELTL'Z 8E9'T AaQS abn.V 8100' 9STT' 6T00' - ESS' Z PO:V6' E 6E99L' - ZPS' T:i wdd wdd wdd Ladd qdd qdd qdd SgTun Ty as us TS Z/096T T/096T Z/8902 LuaTa E6L'S'v OZT6'Z 6LT:�'Z 8ZZ0' 6'LLZ M:60' TS00' £# 60L'6:V E08T'T TE88'T LZZO'. T'LLZ 8260' TS00' Z# 8LT'L'i 6TT7v8' £TOS'T ZEZO' L'SLZ 6260' ZS00' T# 9t,LT " i, TH * L9 908' EZ 960'T 8T76£' 90S£' SZT' T USE % S86'T LOTT'T 7V09:F' E000' T'1 E000' T000' AaQS 09S'Liv S:�1,9'T TiM£6'T 6ZZ0' 6'9LZ TE60' TS00' as. qdd qdd qdd wdd wdd wdd wdd S -4-r T/8902 Z/EOZZ T/EOZZ TN -eN ON uW waTg EZ'LT iv0'OT 6T9Z' 80T0' :100' P000' 0000'- E# 81'LT S66'6 LZ9Z' 90TO' 9T00' 5000' 2000' Z# ST'LT TL6'6 6T9Z' LOTO' 6T0o' 9000' Z000'- T# HTE' :iZbE' 90LT' p9L8' :M —K 80'9T 6' Li,6 QS23% T70' EO' X000' T000' " Z000' T000' Z0o0' A@CJS 6T'LT 00'OT ZZ9Z' L010' 9T00' 5000' 0000'- GFDAV wdd wdd wdd wdd wad wdd Ladd SgTun bW N ag n0 zO oO PO waTS LZ'LT £000' T800' L980' LT8Z'Z OUT' 6ESZT7' E# EZ'LT £000' T800' 1980' EtSZ'i, 6TZT' LZ8tU Z# EZ'LT £000' T800' 0980' TtSZ'Z Z£ZT' ZE981v' T# SLIT' LL'ET TS8T' Z9Eiv' EbT'6E 6Z6S' EL7v'91 CISH% Zo' 0000' 0000' b000' 69:iT'T L000' 8T690' naQS : ULT £000' T800' 2980' OOE6' Z LUT' 666T:V' abnV wdd wdd wdd wdd qdd wdd qdd s:4zull PO ag ag F3 0681SV Tit FDV waTS T :aOgDPa 'zzoO ONOO :aPoW :IuawwoO LS:8Z:OZ 90/ST/60 awiI, *Tnv QO :zogpzad0 V7vOO-SLL6090 :awaN aTdwpS Td`IO :POT T abed Wd £Z:9E=80 90/ST/60 �zodag szsATPu� Analysis Report 09/15/06 08:43:56 PM page 1 iod: CLP1 Sample Name: 0609778-001A Operator: CD Time: 09/15/06 20:36:30 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .26556 .0087 -.52123 .0007 .0002 .0000 .0313 SDev .16159 .0005 1.00519 .0003 .0000 .0000 .0013 %RSD 60.848 5.623 192.85 44.56 12.34 313.8 3.991 #1 .19837 .0091 .08502 .0008 .0003 .0000 .0325 #2 .44989 .0087 -1.6815 .0009 .0002 -.0000 .0313 #3 .14840 .0081 .03283 .0003 .0002 .0000 .0300 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 -.0006 .0001 .0040 .0019 .8089 .0063 SDev .0001 .0002 .0001 .0001 .0003 .0051 .0015 %RSD 1015. 39.26 67.68 3.436 15.57 .6252 23.02 #1 -.0001 -.0009 .0000 .0041 .0016 .8112 .0079 ##2 .0001 -.0005 .0001 .0041 .0019 .8125 .0063 #3 .0000 -.0004 .0001 .0039 .0022 .8031 .0049 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb ge -.0001 .0002 .1938 .0005 .64445 .78093 2.7247 SDev .0001 .0005 .0389 .0006 1.4420 1.1906 1.4870 %RSD 46.45 262.4 20.04 115.6 223.76 152.46 54.577 #1 -.0001 .0007 .2357 .0003 -.45607 2.1414 4.4416 #2 -.0001 -.0004 .1866 ..0012 .11258 -.07087 1.8410 #3 -.0002 .0003 .1591 .0001 2.2768 .27226 1.8915 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.75208 -1.4449 1.2482 -.1479 .0005 -.0000 .0007 SDev 1.11528 3.2903 .1294 .0043 .0014 .0000 .0000 %RSD 148.29 227.72 10.365 2.916 275.5 74.80 6.032 #1 -1.2005 -2.5795 1.3686 -.1437 .0010 -.0000 .0007 ##2 .51761 -4.0177 1.1114 -.1477 .0015 -.0000 .0007 #3 -1.5734 2.2626 1.2647 -.1523 -.0011 -:0000 .0007 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.34056 .0009 .0101 .73552 .40571 .35144 SDev .87856 .0006 .0001 .66700 .72827 1.1266 %RSD 257.98 64.40 .7666 90.684 179.50 320.58 #1 -1.1356 .0016 .0102 1.2765 .67835 .05389 441) -.48879 .0009 .0101 -.00974 .95833 -.59657 .60269 .0004 .0100 .93983 -.41954 1.5970 Analysis Report 09/15/06 08:51:30 PM page 1 ] god: CLP1 Sample Name: 0609778-002A Operator: CD 1_-_. Time: 09/15/06 20:44:03 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .23622 .0090 -1.0882 -.0002 .0003 .0000 .0358 SDev .46154 .0021 1.2182 .0001 .0000 .0000 .0002 %RSD 195.39 23.03 111.94 72.87 4.961 151.8 .5018 ##1 .72412 .0110 -.08312 -.0000 .0003 .0000 .0356 ##2 -.19344 .0091 -2.4431 -.0002 .0003 .0000 .0359 ##3 .17798 .0069 -.73853 -.0002 .0003 -.0000 .0360 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0001 -.0002 .0006 .0040 .0108 .6449 .0029 SDev ._0001 .0002 .0002 .0001 .0001 .0024 .0009 %RSD 49.13 147.8 37.56 3.640 1.200 .3676 30.88 #1 -.0001 .0000 .0004 .0038 .0107 .6453 .0021 #2 -.0002 -.0001 .0008 .0041 .0110 .6470 .0028 #3 -.0001 -.0004 .0006 .0040 .0108 .6423 .0039 Eleni Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb 4e .0002 -.0002 .0642 .0013 1.3489 .77537 1.9405 SDev .0000 .0004 .0042 .0002 .6796 1.5683 .4287 %RSD 21.51 156.5 6.495 17.74 50.382 202.26 22.095 #1 .0001 .0002 .0687 .0012 1.0682 2.5761 1.4554 #2 .0002 -.0005 .0635 .0016 2.1240 -.29086 2.2687 #3 .0001 -.0004 .0604 .0012 .85470 .04085 2.0974 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.85872 -3.9188 1.3612 -.1562 .0007 -.0000 .0014 SDev 2.27332 2.1596 1.5598 .0014 .0008 .0000 .0001 %RSD 264.73 55.109 114.59 .8672 115.9 14.50 5.653 #1 1.5896 -6.0109 .48710 -.1565 .0016 -.0001 .0013 ##2 -1.2628 -1.6975 3.1620 -.1547 .0002 -.0000 .0014 #3 -2.9029 -4.0480 .43442 -.1574 .0002 -.0001 .0014 Eleni T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .52643 .0001 .0140 .96642 .07344 -.39703 SDev 1.4038 .0001 .0001 .96447 1.3982 1.70903 %RSD 266.67 62.85 .5344 99.799 1904.0 430.45 #1 -.42151 .0001 .0141 2.0740 1.5449 -1.6767 417 -.13837 .0000 .0140 .51334 -.08682 1.5438 2.1392 .0001 .0141 .31191 -1.2378 -1.0582 00 M O O F Analysis Report 09/15/06 08:59:03 PM page 1 ] tod: CLP1 Sample Name: 0609609-001A Operator: CD 1.-_: Time: 09/15/06 20:51:37 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .28175 .0005 1.8031 -.0016 -.0001 -.0000 -.0146 SDev .24538 .0018 1.2799 .0001 .0000 .0000 .0003 %RSD 87.089 340.2 70.981 3.574 20.45 36.09 1.988 ##1 .19435 .0024 3.2645 -.0016 -.0001 -.0000 -.0143 ##2 .55887 .0005 .88209 -.0016 -.0001 -.0000 -.0146 ##3 .09205 -.0013 1.2627 -.0015 -.0001 -.0000 -.0149 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 -.0005 -.0006 .0115 -.0077 .0190 -.0025 SDev .0001 .0003 .0002 .0003 .0003 .0088 .0024 %RSD 72.63 52.35 34.75 2.497 3.381 46.44 95.50 #1 .0001 -.0007 -.0005 .0113 -.0075 .0149 -.0035 #2 .0003 -.0002 -.0004 .0118 -.0076 .0291 .0002 #3 .0000 -.0007 -.0008 .0114 -.0080 .0129 -.0042 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Lts ppm ppm ppm ppm ppb ppb ppb le .0002 -.0014 -.0026 .0102 -2.0614 1.8340 -.05355 SDev .0001 .0007 .0026 .000.4 2.7611 1.8717 2.06576 %RSD 36.81 52.76 100.2 3.718 133.94 102.06 3857.9 #1 .0002 -.0022 .0000 .0099 -3.5395 3.0212 1.9415 #2 .0003, -.0012 -.0026 .0106 -3.7687 2.8044 .08135 ##3 .0001 -.0008 -.0052 .0100 1.1241 -.32363 -2.1835 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -3.9410 3.7669 -.66612 -.0537 -.0021 -.0001 -.0007 SDev .5229 3.0359 .82393 .0060 .0019 .0000 .0001 %RSD 13.268 80.594 123.69 11.20 90.14 28.63 10.98 #1 -4.0196 1.8678 -.376.17 -.0594 .-.0004 -.0001 -.0008 #2 -3.3832 7.2682 -.02635 -.0543 -.0018 -.0001 -.0006 #3 -4.4201 2.1646 -1.5958 -.0474 -.0041 -.0001 -.0008 Elem T11908- v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.7353 -.0001 .0110 .53687 -2.6464 .81010 SDev 2.7782 .0002 .0002 .34579 .8963 1.4248 %RSD 160.10 255.6 1.975 64.409 33.868 175.88 #1 3.6858 .0001 .0108 .83652 -2.0346 .37110 R2 -1.4456 -.0001 .0112 .61559 -2.2295 2.4028 2.9657 -.0003 .0111 .15850 -3.6753 -.34357 Analysis Report 09/15/06 09:06:35 PM page 1 Zod: CLP1 Sample Name: 0609609-002A Operator: CD ..�_. Time: 09/15/06 20:59:10 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .74490 .0025 .97722 -.0025 -.0000 -.0000 -.0052 SDev .13527 .0008 1.0697 .0004 .0000 .0000 .0007 %RSD 18.159 30.69 109.46 16.22 119.7 2.839 13.52 #1 .78547 .0030 .48644 -.0022 -.0000 -.0000 -.0059 #2 .85524 .0030 .24098 -.0023 -.0000 -.0000 -.0045 #3 .59399 .0016 2.2042 -.0029 -.0000 -.0000 -.0053 Eleni Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0043 .0037 8.694 .7828 .0228 -.0015 SDev .0001 .0001 .0001 .008 .0006 .0014 .0033 %RSD 44.33 3.042 1.802 .0964 .0805 6.035 216.3 #1 .0001 .0043 .0038 8.699 .7822 .0216 -.0052 #2 .0003 .0045 .0037 8.685 .7827 .0243 .0012 #3 .0002 .0042 .0037 8.699 .7834 .0224 -.0006 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb ge .0081 -.0010 -.0034 .0993 1.9280 4.3371 1.8049 SDev .0001 .0005 .0013 .0003 .6235 .8484 .8312 %RSD .5873 51.21 37.81 .25.66 32.337 19.561 46.054 #1 .0082 -.0015 -.0020 .0995 1.5569 5.0071 1.0485 #2 .0081 -.0005 -.0038 .0990 1,5794 3.3831 2.6948 43 .0081 -.0011 -.0046 .0993 2.6478 4.6209 1.6714 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm .ppm Avge -2.8873 3.3643 -.08753 -.0393 -.0005 -.0001 -.0002 SDev 1.3186 .3421 2.67742 .0004 .0011 .0000 .0001 %RSD 45.668 10.169 3058.7 1.048 214.6 11.90 33.09 #1 -2.6937 3.5961 2.3923 -.0397 -.0008 -.000.1 -.0003 #2 -1.6762 3.5255 -2.9263 -.0393 .0007 -.0001 -.0001 #3 -4.2920 2.9714 .27138 -.0389 -.0014 -.0001 -.0003 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .99831 .0000 .0189 3.5349 -1.3248 1.0620 SDev .68197 .0001 .0001 .6537 1.0481 1.7880 %RSD 68.312 135.7 .6399 18.493 79.120 168.37 #1 .21113 .0001 .0188 3.8583 -1.4475 2.7932 A2 1.3735 .0000 .0190 2.7825 -.22065 -.77782 3 1.4103 .0000 .0190 3.9640 -2.3061 1.1705 Analysis Report 09/15/06 09:14:06 PM page 1 iod: CLP1 Sample Name: 0609769-001A Operator: CD xun Time: 09/15/06 21:06:41 Comment: - Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .30438 .0008 .90783 .0194 -.0001 -.0000 -.0152 SDev .15898 .0005 .56633 .0008 .0000 .0000 .0002 0-oRSD 52.231 66.44 62.383 4.124 24.07 32.33 1.622 #1 .40625 .0014 1.5610 .0185 -.0001 -.0000 -.0155 #2 .12119 .0006 .55453 .0197 -.0001 -.0000 -.0150 #3 .38569 .0004 .60791 .0200 -.0001 -.0000 -.0152 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 -.0006 -.0007 .0126 -.0083 .0150 -.0055 SDev .0002 .0401 .0001 .0005 .0002 .0033 .0034 %RSD 537.0 17.84 15.69 3.786 2.232 22.25 62.26 #1 -.0001 -.0007 -.0006 .0130 -_0086 .0114 -.0058 #2 .0002 -.0007 -.0008 .0128 -.0082 .0180 -.0020 #3 .0000 -.0005 -.0007 .0121 -.0082 .0156 -.0089 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 its ppm ppm ppm ppm ppb ppb ppb ge -.0001 -.0014 .0221 .0109 -2.8108 2.0201 1.3407 SDev .0000 .0003 .0003 .0004 .9341 1.0628 1.5154 %RSD 31.22 18.3.1 1.604 4.069 33.233 52.612 113.03 #1 -.0001 -.0011 .0223 .0109 -1.7466 3.2370 2.4082 #2 -.0001 -.0016 .0222 .0105 -3.1909 1.2738 2.0077 #3 -.0001 -.0015 .0217 .0113 -3.4950 1.5495 -.39378 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.8085 2.0509 -.74354 -.0431 -.0029 -.0001 -.0008 SDev .9845 2.2998. .89517 .0022 .0009 .0000 .0000 %RSD 54.435 112.13 120.39 5.216 31.46 .0085 5.019 #1 -.86809 4.5354 -.90770 -.0445 -.0019 -.0001 -.0008 #2 -2.8318 1.6210 .22235 -.0442 -.0032 -.0001 -.0008 #3 -1.7257 -.00350 -1.5453 -.0405 -.0037 -.0001 -.0008 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm -Ppb ppb ppb Avge .97612 -.0000 .0004 .41145 -.75981 .18705 SDev .23240 .0003 .0000 1.0107 .85165 1.0611 %RSD 23.809 704.1 7.674 245.64 112.09 567.31 #1 1.2394 -.0004 .0004 1.5775 .22295 .90486 .0 1).79955 .0002 .0004 -.21287 -1.2202 .68812 .88941 .0000 .0004 -.13028 -1.2822 -1.0318 Analysis Report 09/15/06 09:21:38 PM page 1 iod: CLP1 Sample Name: 0609769-002A Operator: CD Time: 09/15/06 21:14:13 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .42349 .0017 1.1002 .0217 -.0001 -.0000 -.0146 SDev .20972 .0006 .8620 .0002 .0000 .0000 .0003 %RSD 49.522 37.07 78.356 .9058 54.39 66.09 1.961 #1 .63779 .0022 2.0924 .0219 -.0000 -.0000 -.0149 #2 .21867 .0010 .67283 .0216 -.0001 -.0000 -.0144 #3 .41402 .0019 .53528 .0217 -.0001 -.0000 -.0144 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0007 .0013 2.406 .2191 .0207 -.0029 SDev .0001 .0003 .0001 .004 .0017 ..0028 .0022 %RSD 40.85 40.27 8.985 .1762 .7826 13.44 75.57 #1 .0001 .0008 .0014 2.404 .2171 .0224 -.0044 #2 .0002 .0004 .0012 2.411 .2199 .0175 -.0040 #3 .0001 .0009 .0013 2.403 .2203 .0222 -.0004 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 -- is ppm ppm ppm ppm ppb ppb ppb je .0020 -.0012 .0575 .0442 -1.6253 1.6918 .82265 Lev .0000 .0006 .0003 .0004 1.0598 1.3802 .15616 0-oRSD 2.044 50.08 .4871 .8305 65.203 81.583 18.983 #1 .0021 -.0009 .0578 .0438 -2.8066 1.4092 .98398 #2 .0020 -.0008 .0575 .0446 -1.3115 .47470 .81175 #3 .0020 -.0019 .0573 .0441 -.75796 3.1914 .67223 Elem 2068/2 1960/1 1960/2 Si Sn - Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -2.5741 4.3747 -.06614 -.0454 -.0028 -.0001 -.0006 SDev 1.7177 1.6932 2.72651 .0009 .0009 .0000 .0001 %RSD 66.732 38.705 4122.4 1.892 32.80 22.77 13.06 #1 -4.2095 4.6924 2.8904 -.0455 -.0027 -.0001 -.0006 #2 -2.7282 2.5452 -2.4815 -.0445 -.0037 -.0001 -.0006 #3 -.78447 5.8866 -.60729 -.0462 -.0019 -.0001 -.0007 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.6423 .0001 .0048 .58722 -1.4429 1.4127 SDev .9213 .0001 .0001 1.1181 1.0942 2.1526 %RSD 34.868 66.72 1.248 190.41 75.834 152.37 #1 1.9188 .0001 .0048 .00541 -2.4800 3.4905 42 2.3285 .0000 .0048 -.12005 -1.5494 -.80760 3.6795 .0001 .0047 1.8763 -.29937 1.5552 Analysis Report 09/15/06 09:29:11 PM page 1 1 Lod: CLP1 Sample Name: 0609077-001A Operator: CD 1___-_ Time: 09/15/06 21:21:45 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .31052 .0013 1.4048 -.0026 -.0000 -.0000 -.0136 SDev .30218 .0001 2.2878 .0002 .0000 .0000 .0006 %RSD 97.314 6.540 162.86 6.552 171.9 6.450 4.086 ##1 .47764 .0014 -1.2125 -.0025 -.0000 -.0000 -.0139 #2 .49221 .0013 2.4028 -.0025 .0000 -.0000 -.0130 #3 -.03830 .0014 3.0241 -.0028 -.0001 -.0000 -.0140 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0000 -.0003 -.0003 .0004 -.0090 .0215 -.0017 SDev .0002 .0003 .0004 .0005 .0002 .0057 .0013 %RSD 1527. 92.55 116.3 140.1 1.955 26.62 75.27 ##1 .0000 -.0004 .0000 .0009 -.0088 .0199 -.0024 #2 .0002' .0000 -.0003 .0004 -.0091 .0278 -.0002 #3 -.0002 -.0005 -.0008 -.0002 .-.0090 .0167 -.0024 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 tts ppm ppm ppm ppm ppb ppb ppb �e -.0005 -.0012 -.0144 -.0004 -1.7837 .41607 1.0991 bliev .0001 .0009 .0007 .0004 .5892 .19243 1.0341 %RSD 17.50 75.57 4.564 102.4 33.031 46.250 94.093 #1 -.0005 -.0003 -.0137 -.0002 -2.1805 .38046 2.0076 #2 -.0004 -.0012 -.0144 -.0001 -2.0637 .24394 1.3159 ##3 -.0006 -.0021 -.0150 -.0008 -1.1067 .62383 -.02631 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.5789 5.1240 .73928 -.0520 -.0025 -.0001 -.0006 SDev 1.1160 2.3703 1.1962 .0022 .0014 .0000 .0001 %RSD 70.682 46.259 161.80 4.191 57.63 37.13 23.48 #1 -2.8074 4.7468 -.46600 -.0507 -.0030 -.0001 -.0005 #2 -.62774 2.9650 .75774 -.0545 -.0009 -.0001 -.0006 #3 -1.3015 7.6603 1.9261 -.0507 -.0036 -.0001 -.0008 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.9643 -.0003 -.0010 -.31640 -.68711 2.1994 SDev 1.0585 .0004 .0002 .31630 .63344 1.4214 %RSD 53.888 165.8 18.21 99.968 92.189 64.625 #1 3.1804 .0001 -.0011 -.47232 -1.2040 1.2699 #2 1.4625 -.0002 -.0008 -.52448 .01951 1.4928 1.2500 -.0007 -.0011 .04759 -.87684 3.8356 M It r-, t` O O N Analysis Report 09/15/06 09:36:43 PM page 1 hod: CLP1 Sample Name: CCV6 Operator: CD Time: 09/15/06 21:29:17 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 999.48 49.76 514.38 2.552 2.555 2.535 48.50 SDev 10.44 .54 6.91 .027 .027 .027 .50 0-oRSD 1.0444 1.083 1.3439 1.050 1.052 1.068 1.026 #1 1002.2 49.84 515.41 2.555 2.562 2.541 48.57 #2 1008.3 50.26 520.72 2.577 2.577 2.559 48.96 #3 987.95 49.19 507.01 2.524 2.525 2.506 47.98 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.515 2.478 2.514 2.582 49.93 86.08 50.89 SDev .027 .026 .027 .027 .56 .82 .52 0-oRSD 1.078 1.041 1.064 1.029 1.119 .9495 1.030 #1 2.523 2.482 2.519 2.587 49.99 86.14 50.97 2.538 2.501 2.538 2.606 50.46 86.86 51.37 2.485 2.450 2.485 2.553 49.34 85.23 50.33 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.484 2.581 84.54 2.485 501.70 487.88 983.71 SDev .026 .025 .78 .027 3.69 2.64 11.28 0-oRSD 1.039 .9837 .9278 1.067 .73541 .54021 1.1468 41 2.489 2.583 84.61 2.497 500.29 486.83 974.60 #2 2.507 2.605 85.28 2.504 505.89 490.87 996.33 #3 2.456 2.554 83.72 2.455 498.92 485.93 980.19 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 988.45 515.57 513.68 2.777 2.504 2.515 2.639 SDev 5.54 6.83 4.48 .061 .029 .026 .031 %RSD .56059 1.3250 .87268 2.207 1.171 1.049 1.187 988.18 512.99 509.26 2.707 2.507 2.521 2.654 994.12 523.31 518.23 2.806 2.532 2.538 2.659 #3 983.05 510.40 513.56 2.819 2.473 2.486 2.603 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK d - d O O V) F Analysis Report 09/15/06 09:36:43 PM gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 502.79 2.503 2.576 492.48 986.87 514.31 SDev 4.85 .027 .027 2.99 6.96 4.96 %RSD .96433 1.071 1.032 .60641 .70519 .96427 #1 497.85 2.510 2.580 491.31 983.66 510.51 #2 507.54 2.526 2.600 495.87 994.86 519.92 #3. 502.96 2.473 2.548 490.25 982.10 512.51 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 kn d- r -r O O E-1 Analysis Report 09/15/06 09:44:16 PM page 1 iod: CLP1 Sample Name: CCVL6 Operator: CD Time: 09/15/06 21:36:51 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .29681 .0131 1.4838 .0023 .0004 .0005 -.0016 SDev .16181 .0051 1.7294 .0017 .0002 .0002 .0038 %RSD 54.514 38.74 116.56 73.96 59.50 41.84 242.8 #1 .32558 .0186 2.5264 .0042 .0006 .0006 .0019 #2 .44230 .0121 -.51254 .0019 .0004 .0005 -.0010 #3 .12255 .0086 2.4375 .0009 .0002 .0003 -.0056 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0005 -.0001 .0001 .0002 2.499 .0363 .0072 SDev .0003 .0002 .0003 .0006 .005 .0125 .0053 %RSD 68.04 288.3 191.8 223.6 .2080 34.37 73.16 ##1 .0007 -.0000 .0004 .0008 2.505 .0496 .0121 ___ .0007 .0001 .0001 .0003 2.497 .0343 .0078 .0001 -.0003 -.0001 -.0003 2.495 .0249 .0017 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0003 .0061 2.605 .0009 -2.3902 .72268 5.4327 SDev .0003 .0033 .008 .0006 .7058 1.0068 3.1708 %RSD 95.32 54.85 .3229 60.41 29.528 139.31 58.365 ##1 -.0000 .0098 2.615 .0012 -1.6680 1.4632 9.0050 ##2 -.0003 .0050 2.598 .0013 -2.4243 1.1285 4.3417 #3 -.0006 .0034 2.603 .0003 -3.0783 -.42366 2.9515 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.1619 1.0879 2.6633 .0520 -.0015 .0004 .0004 SDev .8912 3.4453 .9772 .0204 .0002 .0002 .0003 %RSD 76.701 316.69 36.693 39.19 15.96 64.83 89.86 2.1513 3.6746 3.7602 .0745 -.0016 .0006 .0008 .42219 2.4122 2.3441 .0468 -.0016 .0004 .0003 #3 .91219 -2.8231 1.8855 .0348 -.0012 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK O O V) N Analysis Report 09/15/06 09:44:16 PM page 2 - 3h Zn Low Sb2068 Elem T11908 Units ppb Avge 2.9539 SDev 1.1545 %RSD 39.085 #1 4.0935 #2 2.9832 #3 1.7850 Errors NOCHECK High 62.039 Low .0005 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0003 .0010 -.31386. 2.5841 2.1386 .0002 .0002 .89278 1.6032 1.7184 84.38 22.73 284.46 62.039 80.351 .0005 .0013 .42055 4.4336 3.7316 .0002 .0010 -.05452 1.7274 2.3667 .0001 .0008 -1.3076 1.5913 .31757 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK r - It O O 67 N Analysis Report 09/15/06 09:51:50 PM page 1 hod: CLP1 Sample Name: CCB6 Operator: CD Time: 09/15/06 21:44:24 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .14027 .0095 -.01521 .0000 .0001 .0002 -.0036 SDev .19073 .0024 .16480 .0009 .0001 .0001 .0022 %RSD 135.97 24.84 1083.7 7578. 156.3 40.19 60.41 #1 .25416 .0077 .15035 -.0005 -.0000 .0001 -.0056 #2 .24658 .0122 -.01674 .0011 .0001 .0002 -.0013 #3 -.07992 .0087 -.17923 -.0006 .0000 .0001 -.0038 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 -.0003 -.0002 -.0001 .0017 .0235 .0021 SDev .0001 .00.02 .0003 .0003 .0017 .0051 .0025 %RSD 51.15 50.61 150.6 202.0 98.54 21.75 119.6 #1 .0001 -.0004 -.0005 -.0005 .0004 .0177 -.0003 .0003 -.0001 .0001 .0001 .0036 .0274 .0047 .0001 -.0004 -.0003 -.0001 .0011 .0253 .0019 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0001 .0011 -.0041 .0001 -.15025 1.2689 3.7620 -SDev .0001 .0006 .0034 .0005 2.13441 .6317 .2486 %RSD 54.81 53.56 83.26 366.3 1420.6 49.784 6.6077 #1 -.0002 .0013 -.0058 -.0002 -.10696 1.8887 3.9535 #2 -.0000 .0016 -.0002 -.0001 1.9622 .62585 3.8515 #3 -.0001 .0004 -.0064 .0007 -2.3060 1.2923 3.4811 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.70509 .23568 1.1440 -.0199 -.0007 .0001 .0002 SDev 1.02526 1.3107 1.7104 .0139 .0024 .0001 .0001 %RSD 145.41 556.15 149.50 69.98 342.3 59.81 48.40 -1.4013 -1.1836 .76057 -.0074 -.0006 .0000 .0001 .47224 .49020 3.0136 -.0349 .0016 .0002 .0002 #3 -1.1862 1.4005 -.34207 -.0174 -.0031 .0001 .0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/15/06 09:51:50 PM jh Low Elem T1190.8 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .79285 .0004 .0010 .79640 .78247 .84157 SDev 1.2308 .0002 .0001 .61299 .70591 1.1550 %RSD 155.24 42.41 5.900 76.970 90.215 137.25 #1 -.40948 .0003 .0011 1.2242 .38186 .11317 #2 .73774 .0006 .0011 1.0709 1.5976 2.1733 #3 2.0503 .0004 .0010 .09413 .36801 .23822 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 H2M LABS, INC. IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE 1H2M Labs, Inc. CLP Digestion Log t: Analyst Signature: G #: 7S�—ooh Date: 9�iyzoL atrix: C W Time StartedlEnded: 9.3v 413 36 ethod: 30 % 0 Description ' �- 1 tb'L.S S Comment's: I��1� 'Description of colors: red, blue, yellow, green, orange, violet *Description of texture: white, colorless, brown, grey, black. fine, medium, coarse. `Description of clarity: clear, cloudy, opaque_ *Description of artifacts: NEW MINNOW ' �- 1 tb'L.S S Comment's: I��1� OJWBOOKS/Cl-Migestionlog P 0134 O O 'Description of colors: red, blue, yellow, green, orange, violet *Description of texture: white, colorless, brown, grey, black. fine, medium, coarse. `Description of clarity: clear, cloudy, opaque_ *Description of artifacts: yes or no and describe OJWBOOKS/Cl-Migestionlog P 0134 O O H2M LABS, INC. SDG NO.: i Swoq SCAN: This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature Date: ReviE Date: 65 H