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Wet Chemistry Data Package 12/2006
H2M LABS, INC. 1-SLWK WET CHEMISTRY TABLE OF CONTENTS SAMPLE REPORTS II. Q.C. SUMMARY III. RAW DATA 00 0 0 E1 H2M LABS, INC. SAMPLE REPORTS 1- 2M "U%s INC. 575 Broad Hollow Road, Melvlle W 11747 (631)694-3040. FAX (631)4205436 WSDOH ID# 10478 Town of Southold Landfill Attn To Original Collected :12/6/2006 3:20:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original Cc LABORATORY RESULTS Lab No. : 0612702-001 Client ID. : EB Sample Information... Type : Blank Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 12/07/2006 4:00 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/07/2006 2:50 PM Bromide < 0.5 1 mg/L E320.1 12/22/2006 9:10 AM Chloride < 2.0 1 mg/L E325.2 12/07/2006 1:00 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/12/2006 12:23 PM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/15/2006 11:10 AM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12121/2006 11:03 AM Nitrate as N < 0.10 1 mg/L E353.2 12/07/2006 3:24 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 8:30 AM Sulfate < 5.0 1 mg/L SW9038 12/20/2006 1:34 PM Total Dissolved Solids <10 1 mg/L E160.1 12/11/2006 3:44 PM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2006 11:54 AM Total Organic Carbon < 1.0 1 mg/L SW9060 12/18/2006 8:48 PM Qualifiers: E - Value above quantitation range -t D - Results for Dilution D.F. = Dilution Factor Laboratory Manager, Date Reported : 12/28/2006 Page 1 of 13 U24 "US, INC. 575 Broad Hoilav Road, Mdvllle NY 11747 (631)694-3040.FAx(631)42H436 NYSDOHID#10478 Town of Southold Landfill i ttn To : Original Collected :12/6/2006 2:00:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0612702-002 Client ID. : MW -31) Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 875 20 mg/L E310.1 12/07/2006 4:08 PM Biochemical Oxygen Demand 3 1 mg/L E405.1 12/07/2006 2:55 PM Bromide 1.4 1 mg/L E320.1 12/22/2006 9:15 AM Chloride 231 10 mg/L E325.2 12/07/2006 1:01 PM Chemical Oxygen Demand 112 1 mg/L E410.4 12/12/2006 12:24 PM Hardness (As CaCO3) 360 20 mg/L El 30.2 12/15/2006 11:15 AM Nitrogen, Ammonia (As N) 72.0 50 mg/L E350.1 12/21/2006 11:04 AM Nitrate as N < 0.10 1 ' mg/L E353.2 12/07/2006 3:25 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 8:45 AM Sulfate 45.0 2.5 mg/L SW9038 12/20/2006 1:36 PM Total Dissolved Solids 1050 2 mg/L E160.1 12/11/2006 3:46 PM Nitrogen, Kjeldahl, Total 108 100 mg/L E351.2 12/20/2006 4:04 PM Total Organic Carbon 35.3 1 mg/L SW9060 12/18/2006 9:19 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 12/28/2006 Page 2 of 13 d' 00 O O l.4 U2M ""S4, INC. 575 Broad Hollow Road, Md& NY 11747 (631)694.3 .FAX -(631)42M436 WSDOH ID# 10478 Town of Southold. Landfill Attn To : Original Collected :12/5/2006 1:00:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0612702-003 Client ID.: MW -3S Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 385 20 mg/L E310.1 12/07/2006 4:16 PM Biochemical Oxygen Demand 4 1 mg/L E405.1 12/07/2006 3:00 PM Bromide - 6.6 1 mg/L E320.1 12/22/2006 9:20 AM Chloride 61.2 1 mg/L _ E325.2 12/07/20061:01 PM Chemical Oxygen Demand 51.2 1 mg/L E410.4 12/12/200612:25 PM Hardness (As CaCO3) 324 4 mg/L El 30.2 12/15/2006 11:20 AM Nitrogen, Ammonia (As N) 18.5 10 mg/L E350.1 12/21/2006 11:05 AM Nitrate as N < 0.10 1 mg/L E353.2 12/07/2006 3:26 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 9:00 AM Sulfate 49.2 2.5 mg/L SW9038 12/20/2006 1:38 PM Total Dissolved Solids 460 1 mg/L E160.1 12/11/2006 3:48 PM Nitrogen, Kjeldahl, Total 26.6 20 mg/L E351.2 12/20/2006 11:56 AM Total Organic Carbon 12.9 1 mg/L SW9060 12/18/2006 9:49 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 12/28/2006 Page 3 of 13 1---12M "U%s INC. 575 BroadHo6av Road, McWe NY 11747 LABORATORY RESULTS (631)694-3040.FAX(631)42M436 NYSDOH ID# 10478. Sample Information... Town of Southold Landfill Lab No.: 0612702-004 Type : Groundwater Origin: Attn To Original Client ID. : MW -4D Collected :12/6/2006 11:45:00 AM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original cc Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 173 10 mg/L E310.1 12/07/2006 6:24 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/07/2006 3:05 PM Bromide 1.4 1 mg/L E320.1 12122/2006-9:25 AM Chloride 23.2 1 mg/L E325.2 12/07/20061:02 PM Chemical Oxygen Demand 28.6 1 mg/L E410.4 12/12/200612:26 PM Hardness (As CaCO3) 270 10 mg/L E130.2 12/15/2006 11:25 AM Nitrogen, Ammonia (As N) 0.65 1 mg/L E350.1 12121/200611:06 AM Nitrate as N 8.59 10 mg/L E353.2 12/07/2006 3:27 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 9:15 AM Sulfate 79.5 2.5 mg/L SW9038 12/20/2006 1:40 PM Total Dissolved Solids 374 1 mg/L E160.1 12/11/2006 3:50 PM Nitrogen, Kjeldahl, Total 2.58 20 mg/L E351.2 12/20/2006 11:56 AM Total Organic Carbon 10.5 1 mg/L SW9060 12/18/2006 10:19 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 4 of 13 K1' - Laboratory Manager U2M "US -5 INC. 575 Broad Hollow Road, Melville NY 11747 LABORATORY RESULTS (631)694,3040.FAX (631)420E4W NYSDOHID#10478 Town of Southold Landfill Lab No. : 0612702-0055 Attn To : Original Collected :12/5/2006 3:15:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original cc Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID. : MW -4S Sample Information... Type : Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed 790 20 mg/L E310.1 12/07/2006 4:24 PM 3 1 mg/L E405.1 12/07/2006 3:10 PM 2.7 1 mg/L E320.1 12/22/2006 9:30 AM 293 10 mg/L E325.2 12/07/2006 1:03 PM 83.9 1 mg/L E410.4 12/12/200612:27 PM 520 20 mg/L E130.2 12/15/2006 11:30 AM 51.5 50 mg/L E350.1 12/21/2006 11:07 AM 0.36 1 ' mg/L E353.2 12/07/2006 3:28 PM 5.9 1 pg/L E420.1 12/20/2006 9:30 AM 120 5 mg/L SW9038 12/20/2006 1:42 PM 1200 2 mg/L E160.1 12/11/2006 3:52 PM 75.6 100 mg/L E351.2 12/20/2006 4:05 PM 25.9 1 mg/L SW9060 12/18/2006 10:49 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 5 of 13 ii r�`3.t Laboratory Manager U2M 1A13S, INC. 575 Broad Hollow Road, Melville NY 11747 LABORATORY RESULTS (631)694-3040.FAX (631)420-84W NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0612702-006 Type : Groundwater Origin: Attn To Original Client ID.: MW -513 Collected :12/6/2006 9:15:00 AM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 743 20 mg/L E310.1 12/07/2006 4:32 PM Biochemical Oxygen Demand 12 1 mg/L E405.1 12/07/2006 3:15 PM Bromide 5.6 1 mg/L E320.1 12/22/2006 9:35 AM Chloride 280 10 mg/L E325.2 12/07/2006 1:04 PM Chemical Oxygen Demand 94.0 1 mg/L E410.4 12/12/2006 12:28 PM Hardness (As CaCO3) 520 20 mg/L E130.2 12/15/2006 11:35 AM Nitrogen, Ammonia (As N) 58.0 50 mg/L E350.1 12/21/2006 11:09 AM Nitrate as N < 0.10 1 mg/L E353.2 12/07/2006 3:30 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 9:45 AM Sulfate 142 10 mg/L ' SW9038 12/20/2006 1:44 PM Total Dissolved Solids 1230 2 mg/L E160.1 12/11/2006 3:54 PM Nitrogen, Kjeldahl, Total 92.0 10 mg/L E351.2 12/23/2006 9:46 AM Total Organic Carbon 24.4 1 mg/L SW9060 12/18/2006 11:19 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 6 of 13 Laboratory Manager 00 00 O O C/1 U2AA "US, INC. 575 BroadHdlox Road, Melville NY 11747 LABORATORY RESULTS (631)6943040. FAX:(631)42M436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. 0612702-007 Type : Groundwater Origin: Attn To Original Client ID. : MW -5S Collected :12/6/2006 10:30:00 AM Received :1216/2006 4:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 64.0 5 mg/L E310.1 12/07/2006 5:12 PM Biochemical Oxygen Demand 8 1 mg/L E405.1 12/07/2006 3:25 PM Bromide 1.4 1 mg/L E320.1 12/22/2006 9:50 AM Chloride 16.0 1 mg/L E325.2 12/07/2006 1:06 PM Chemical Oxygen Demand 16.0 1 mg/L E410.4 12/12/2006 12:31 PM Hardness (As CaCO3) 96.0 2 mg/L E130.2 12/15/2006 11:50 AM Nitrogen, Ammonia (As N) 1.55 1 mg/L E350.1 12/21/2006 11:12 AM Nitrate as N 2.18 5 mg/L E353.2 12/07/2006 3:33 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/200610:30 AM Sulfate 38.5 1 mg/L SW9038 12/20/2006 1:50 PM Total Dissolved Solids 192 1 mg/L E160.1 12/11/20064:00 PM Nitrogen, Kjeldahl, Total 3.36 20 mg/L E351.2 12/20/2006 11:59 AM Total Organic Carbon 7.5 1 mg/L SW9060 12/19/2006 12:49 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 7 of 13 Laboratory Manager O� 00 O 0 1-12M "US, INC. 575 Broad Hollow Road, MdVle W 11747 (631)694-3040.FAX(631)42H436 WSDOHID#10478 Town of Southold Landfill Attn To Original Collected :12/6/2006 3:00:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC LABORATORY, RESULTS Lab No. : 0612702-008 Client ID.: MW -6D Sample Information... Type: Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 41.5 2 mg/L E310.1 12/07/2006 5:20 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/07/2006 3:30 PM Bromide 3.1 1 mg/l- E320.1 12/22/2006'9:55 AM Chloride 38.0 1 mg/L E325.2 12/07/2006 1:07 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/12/2006 12:32 PM Hardness (As CaCO3) 210 10 mg/L E130.2 12/15/2006 11:55 AM Nitrogen, Ammonia (As N) 0.12 1 mg/L E350.1 12/21/2006 11:13 AM Nitrate as N 3.30 5 mg/L E353.2 12/07/2006 3:34 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 10:45 AM Sulfate 145 10 mg/L SW9038 12/20/2006 1:52 PM Total Dissolved Solids 299 1 mg1L E160.1 12/11/2006 4:02 PM Nitrogen, Kjeldahl, Total 0.23 1 mg/L E351.2 12/20/2006 12:00 PM Total Organic Carbon 1.6 1 mg/L SW9060 12/19/2006 1:17 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported: 12/28/2006 Page 8 of 13 O 00 O O U214 "Uss INC. 575 BroadH09O✓v Road, McVile W 11747 LABORATORY RESULTS (631) 694-3040. FAX (631)420$436 WSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No.: 0612702-009 Type : Groundwater Origin: Attn To Original Client ID.: MW -6S Collected :12/5/2006 12:15:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 54.2 5 mg/L E310A 12/07/2006 5:28 PM Biochemical Oxygen Demand <2 1 mg/L E405.1 12/07/2006 3:35 PM Bromide 0.6 1 mg/L E320.1 12/22/2006 10:00 AM Chloride 5.3 1 mg/L E325.2 12/07/2006 1:08 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/12/2006 12:33 PM Hardness (As CaCO3) 90.0 2 mg/L E130.2 12/15/2006 12:00 PM Nitrogen, Ammonia (As N) 0.11 1 mg/L E350.1 12/21/2006 11:19 AM Nitrate as N 2.64 5 mg/L E353.2 12/07/2006 3:38 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 11:00 AM Sulfate 8.2 1 mg/L SW9038 12/20/2006 1:54 PM Total Dissolved Solids 119 1 mg/L E160.1 12/11/2006 4:04 PM Nitrogen, Kjeldahl, Total 0.46 1 mg/L E351.2 12/20/2006 4:08 PM Total Organic Carbon 3.8 1 mg/L SW9060 12/19/2006 2:51 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. =Dilution Factor Date Reported : 12/28/2006 Page 9 of 13 Laboratory Manager r -+ 00 O O 1.4 C4 E-+ 1-2M "M1 1NCo 575 Broad Mow Road, Melville NY 11747 LABORATORY RESULTS (631)6943040. FAX- (631)42M436 WSDOHID#10478 Town of Southold Landfill Lab No. 0612702-010 Attn To Original Collected :12/6/2006 1:00:00 PM Received :1216/2006 4:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID.: MW -8D Sample Information... Type: Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed 431 20 mg/L E310.1 12/07/2006 5:36 PM 3 1 mg/L E405.1 12/07/2006 3:40 PM 1.7 1 mg/L E320.1 12/22/2006 10:05 AM 111 5 mg/L E325.2 12/07/2006 1:09 PM 53.8 1 mg/L E410.4 12/12/2006 12:34 PM 380 10 mg/L E130.2 12/15/2006 12:05 PM 31.9 20 mg/L E350.1 12/21/2006 11:20 AM 6.68 10 mg/L E353,2 12/07/2006 3:39 PM 10.5 1 pg/L E420.1 12/20/2006 11:15 AM 108 5 mg/L SW9038 12/20/2006 1:56 PM 690 2 mg/L E160.1 12/11/2006 4:06 PM 46.3 20 mg/L E351.2 12/20/2006 12:03 PM 19.5 1 mg/L SW9060 12/19/2006 3:21 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 10 of 13 Laboratory Manager N 00 O O 14 LC/) L U2/4 "U%s INC. 575 Broad Hollow Road, Melville NY 11747 LABORATORY RESULTS (631)6943040.FAX- (631)42M436 NYSDOH ID# 10478 Town of Southold Landfill Lab No. : 0612702-011 Attn To : Original Collected :12/5/2006 2:15:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original . CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics; Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID. : MW -8S Sample Information... Type: Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed 390 10 mg/L E310.1 12/07/2006 5:44 PM 8 1 mg/L E405.1 12/07/2006 3:45 PM 3.2 1 mg/L E320.1 12/22/2006 10:10 AM 52.5 1 mg/L E325.2 12/07/2006 1:09 PM 66.3 1 mg/L E410.4 12/12/2006 12:35 PM 320 20 mg/L E130.2 12/15/2006 12:10 PM 14.2 10 mg/L E350.1 12/21/2006 11:21 AM < 0.10 1 mg/L E353.2 12/07/2006 3:40 PM < 5.0 1 pg/L E420.1 12/20/200611:30 AM 7.3 1 mg/L SW9038 12/20/2006 1:58 PM 407 1 mg/L E160.1 12/11/2006 4:08 PM 21.0 20 mg/L E351.2 12/20/2006 12:04 PM 20.6 1 mg/L SW9060 1.2/19/2006 3:51 AM Qualifiers: E -Value above quantitation, range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 11 of 13 4101. Laboratory Manager M 00 O O 1.4 1H2M "U%s INC. 575 BroadHdov Road, Melville NY 11747 LABORATORY RESULTS (631)694 .FAX(631)42084W NYSDOHID#10478 Town of Southold Landfill Lab No. : 0612702-012 Attn To Original Collected :12/6/2006 2:05:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID.: SOUTHHOLD 2 Sample Information... Type : Groundwater Origin: Results Qualifier D.F. Units Method Number Analyzed 882 10 mg/L E310.1 12/07/2006 5:52 PM 5 1 mg/L E405.1 12/07/2006 3:50 PM 2.1 1 mg/L E320.1 12/22/2006 10:15 AM 244 10 mg/L E325.2 12/07/2006 1:10 PM 114 1 mg/L E410.4 12/12/2006 12:36 PM 380 20 mg/L E130.2 12/15/2006 12:15 PM - 78.8 50 mg1L E350.1 12/21/2006 11:22 AM < 0.10 1 mg/L E353.2 12/07/2006 3:42 PM 8.0 1 pg/L E420.1 12/20/2006 11:45 AM 45.2 2.5 mg/L SW9038 12/20/2006 2:00 PM 1060 2 mg/L E160.1 12/11/2006 4:10 PM 116 100 mg/L E351.2 12/20/2006 4:08 PM 36.0 1 mg/L SW9060 12/19/2006 4:22 AM Qualifiers: E - Value above quantitation range D - Results for Dilution } D.F. = Dilution Factor Date Reported : 12/28/2006 Page 12 of 13 Q/1t%ll- . Laboratory Manager 7t 00 O 0 l.-4 E"I U284 "US, INC. 575 Broad Hollow Road, Melville NY 11747 (631) 694-3040. FAX (631) 420.84W NYSDOH ID# 10478 Town of Southold Landfill Attn To : Original Collected :12/6/2006 3:15:00 PM Received :12/6/2006 4:50:00 PM Collected By VG03 Copies To :Original cc LABORATORY RESULTS Lab No. : 0612702-013 Client ID.: FB Sample Information... Type : Field Blank Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 12/07/2006 6:00 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 12/07/2006 3`.55 PM Bromide < 0.5 1 mg/L E320.1 12/22/2006 10:20 AM Chloride < 2.0 1 mg/L E325.2 12/07/2006 1:10 PM Chemical Oxygen Demand <10 1 mg/L E410.4 12/12/2006 12:37 PM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 12/15/2006 12:20 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 12/21/2006 11:24 AM Nitrate as N < 0.10 1 mg/L E353.2 12/07/2006 3:43 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 12/20/2006 12:00 PM Sulfate < 5.0 1 mg/L SW9038 12/20/2006 2:02 PM Total Dissolved Solids <10 1 mg/L E160.1 12/11/2006 4:12 PM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 12/20/2006-12:05 PM Total Organic Carbon 1.3 1 mg/L SW9060 12/19/2006 4:53 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 12/28/2006 Page 13 of 13 Laboratory Manager V7 r --a 00 O O l E"t H2M LABS, INC. II. Q.C. SUMMARY 00 0 0 DO E -I H2M LABS, INC. Date: 28 -Dec -06 QC SUMMARY REPORT SDG: TSL008 Spike Sample Recovery RPDRef %RPD 'Ramnle ID: Client Samale ID: Analvte Result Units Amount Result %REC Limits Value %RPD UCL MS -120706 MB -120706 Alkalinity, Total (As CaCO3) < 1 mg/L LCS-120706 LCS-120706 Alkalinity, Total (As CaCO3) 27.2 mg/L 25 < 1 109 80 120 0612702-006DMS MW-5DMS Alkalinity, Total (As CaCO3) 1300 mg/L 500 743 111 75 125 0612702-006DDUP MW-5DDUP Alkalinity, Total (As CaCO3) 778 mg/L 743 4.6 20 V1B-120706 MB -120706 19iochemical Oxygen Demand < 2 mg/L _CS -120706 LCS-120706 Biochemical Oxygen Demand 169 mg/L 200 < 2 84 80 120 D612702-006DDUP MW-5DDUP Biochemical Oxygen Demand 5 mglL 12 82 20 MB -122206 MB -122206 Bromide < 0.5 mglL LCS-122206 LCS-122206 Bromide 4.8 mg/L 5 < 0.5 96 80 120 0612702-006Dms MW-5DMS Bromide 10.4 mg/L 5 5.6 96 75 1125 0612702-006Ddup MW-5DDUP Bromide 5.7 mg/L 5.6 1.8 20 MB -121206 MB -121206 Chemical Oxygen Demand <10 mg/L LCS-121206 LCS-121206 Chemical Oxygen Demand 942 mg/L 1000 <I 0 94 80 120 0612702-006CMS MW-5DMS Chemical Oxygen Demand 1040 mg/L 1000 94.0 95 75 125 0612702-006CDUP MW-5DDUP Chemical Oxygen Demand 109 mg/L 94.0 14.8 20 MB -127006 MB -127006 Chloride < 2 mg/L LCS-120706 LCS-120706 Chloride 47.3 mg/L 50 < 2 95 80 120 0612702-006DMS MW-5DMS Chloride 539 mg/L 250 280 104 75 125 0612702-006DDUP MW-5DDUP Chloride 276 mg/L 280 1.5 20 MB -121506 MB -121506 Hardness (As CaCO3) < 5 mg/L LCS-121506 LCS-121506 Hardness (As CaCO3) 1030 mg/L 1000 < 5 103 80 120 0612702-006Bms MW-5DMS Hardness (As CaCO3) 2660 mg/L 2000 520 107 75 125 0612702-006Bdup MW-5DDUP Hardness (As CaCO3) 520 mg/L 520 1 0 20 1 TSL008 W17 QC SUMMARY REPORT SDG: TSL008 Spike Sample Recovery RPDRef %RPD Sample ID• Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MBI -120706 MB1-120706 Nitrate as N < 0.1 mg/L LCSI-120706 LCS1-120706 Nitrate as N 1.17 mg/L 1.13 < 0.1 104 80 120 d2O 0612702-006CMS MW-5DMS Nitrate as N 0.57 mg/L 0.5 < 0.1 114 75 125 0612702-006CDUP MW-5DDUP Nitrate as N < 0.1 mg/L I <0.1 MB -19212 MB -122106 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS-19212 LCS-122106 Nitrogen, Ammonia (As N) 1.03 mg/L 1 < 0.1 103 80 120 0612702-006CMS MW-5DMS Nitrogen, Ammonia (As N) 62.7 mg/L 5 58.0 94 75 125 0612702-006CDUP MW-5DDUP Nitrogen, Ammonia (As N) 58.6 mg/L 58.0 1.1 20 MB -19244 MB -122306 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS-19244 LCS-122306 Nitrogen, Kjeldahl, Total 4.16 mg/L 4.1 < 0.1 101 80 120 0612702-006CMS MW-5DMS Nitrogen, Kjeldahl, Total 127 mg/l- 41 92.0 85 75 125 0612702-006CDUP MW-5DDUP Nitrogen, Kjeldahl, Total 92.2 mg/L 92.0 0.22 20 MBl-19210 MBI -122006 Nitrogen, Kjeldahl, Total < 0.1 mg/L MB -19210 MB -122006 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS1-19210 LCS1-122006 Nitrogen, Kjeldahl, Total 4.10 mg/L 4.1 <0.1 100 80 120 LCS-19210 LCS-122006 Nitrogen, Kjeldahl, Total 4.52 mg/L 4.1 < 0.1 110 80 120 MB -122006 MB -122006 Phenolics, Total Recoverable < 5 ug/L LCS-12206 LCS-12206 Phenolics, Total Recoverable 28.2 ug/L 30 < 5 94 180 120 0612702-006CMS MW-5DMS Phenolics, Total Recoverable 18.5 ug/L 20 < 5 92 75 125 0612702-006Cdup MW-5DDUP Phenolics, Total Recoverable < 5 ug/L < 5 20 MB -122006 MB -122006 Sulfate < 5 mg/L LCS-122006 LCS-122006 Sulfate 18.9 mg/L 20 < 5 94 80 120 0612702-006DMS MW-5DMS Sulfate 342 mg/L 200 142 100 75 125 0612702-006DDUP MW-5DDUP Sulfate 143 mg/L 142 0.70 20 TSL008 W18 QC SUMMARY REPORT SDG: TSL008 Spike Sample Recovery RPDRef %RPD Sample I.D: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -121106 MB -121106 Total Dissolved Solids <10 mg/L --<--10 LCS-121106 LCS-121106 Total Dissolved Solids 313 mg/L 300 104 80 120 0612702-006DMS MW-5DMS Total Dissolved Solids 1860 mg/L 600 1230 105 75 125 0612702-006DDUP MW-5DDUP Total Dissolved Solids 1220 mg/L 1230 0.65 20 MB -121806 MB -121806 Total Organic Carbon < 1 mglL LCS-121806 LCS-121806 Total Organic Carbon 24.6 mg/L 25 < 1 98 80 120 0612702-006AMS MW-5DMS Total Organic Carbon 34.8 mg/L 10 24.4' 104 75 125 0612702-006ADUP MW-5DDUP Total Organic Carbon 23.8 mglL 24.4 2.6 20 TSL008 W19 H2M LABS, INC. I11. RAW DATA O N 00 O O r4 C/) F-+ CODES FOR MANUAL CORRECTIONS T: Transcription error. CE: Calculation error CC: Changed per client request SC: Sample cancelled LB: Wrong spot in logbook The following codes are specific to chromatography: GC / IC: MS (Match standard): The integration of the continuous calibration or the sample was different from that used for the initial calibration, e.g. more or less of the tail was included. BL (Baseline): Incorrect integration due to changing baseline (rise or fall). NP (Negative peak): Due to a negative displacement in the baseline, wrong areas were integrated, which usually are too high. FP (Fused peak): A contamination is not resolved from the peak that is eluting in the retention time window and is included in the area. Areas are allocated for. the two (or more) unresolved peaks in the manual integration. WB (Wrong basepoint): The start or finish of the peak ("basepoine') was put too high or too low, and the basepoint is corrected to match to projected baseline. R (Rider): The peak is riding on a larger.contamination, and is reintegrated as a rider. . GC -MS: MP: Missed peak MIP: Misintegrated peak WI: Wrong isomer TI: Total of isomers r N 00 O O r4 F-+ `\ Author: bmk Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual H2MLabm Inc. ` '--' Channel 1:Set 2of2 1IUumy1L vi0.008 mg/L 8.217 CO 4 0.200 1 3.048 1072 0.5 12121/2006 10:57;30 AM ce) C14 rl— C14 C3 1.596 g/L co 71111 Pon , ' 0.000f -- Table tNH3 Date :13/21/2D0& R. Figure tNH3 M NH3 concentration, mg1l- 3.080 Area ~1O.585°Conu'[.17U Conc=U.00U°Area +0.O1O Correlation Coefficient Vi=O.8g9Sa No Weighting Run:nh3122106 -3- Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 1IUumy1L vi0.008 mg/L Figure tNH3 M NH3 concentration, mg1l- 3.080 Area ~1O.585°Conu'[.17U Conc=U.00U°Area +0.O1O Correlation Coefficient Vi=O.8g9Sa No Weighting Run:nh3122106 -3- Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 4 0.200 1 3.048 1072 0.5 12121/2006 10:57;30 AM Figure tNH3 M NH3 concentration, mg1l- 3.080 Area ~1O.585°Conu'[.17U Conc=U.00U°Area +0.O1O Correlation Coefficient Vi=O.8g9Sa No Weighting Run:nh3122106 -3- 'lH2A LABS, INC. PC Tf b O'D ? 19z/uZl*' AMMONIA DISTILLATION NAME: DATE: /0: � LAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE VOLUME' MLS FINAL VOLUME MLS -ANALYZED DATE SPIKE )� 10-09f e s_0 yep 702- w6C, kta Z—oo?c 9-5 W65 m 7,02 - ott', ts 9�2_ 0(2t - 1V 7102 -0 Qc F b ro 613 os l- Vol SO kFb 7V:: .0 P 0053 04OF1SIaS L "7 A 0% Z� ,•I W3 S y.b Lts J!� 5S bb I be g�!) .p CS 50'At{Ol-D& . F3 Author: bnk H2M Labs. Inc. Date : 12/7/2006 Original Run Filename: OM_12-7-2006_03-10-51PM.OMN created 12/7/2006 3:10:51 PM Original Run Author's Signature: [bnk] Current Run Filename: no3120706a.omn last modified 12/7/2006 3:52:05 PM Current Run Authors Signature: [bnk] Description: Default New Run -Ts L e -o s Sample Cup No. Channel 2 Nitrate m Ng Conc. (m N/L) ADF Area NNO MDF "Cal Std 5:ical5:no3 dw" S1 2.000 21.273 False "Cal Std 4:ical4:no3 dw" S2 1.000 10.600 % of High Standard "Cal Std 3:ical3:no3 dw" S3 0.500 5.329 Direct/Bipolar "Cal Std 2:ical2:no3 dw" S4 0.100 1.104 "Cal Std 1:ical1:no3 dw" S5 0.050 0.563 "Cal Std O:icalO:no3 dw" S16 0.000 -0.006 "CRa:cra:no3 dw" S4 0.100 1.080 Known Cone: 0.100 Calibration: Table/Fig. 1 "LCS1-120706:lcs:no3 dw" S6 1.166 12.402 Known Cone: 1.130 "MB1-120706:mblk:no3 dw" 1 S16 -0.001 0.010 - Known Cone: 0.000 "0612702-001 C:SAMP:NO3 W' 1 0.001 0.033 "0612702-002C:SAMP:NO3 W' 2 0.053 0.577 "0612702-003C:SAMP:NO3 W 3. 0.011 0.135 "0612702-004C:SAMP:NO3 W' 4 8.588 9.137 10.00 "0612702-005C:SAMP:NO3 W' 5 0.356 3.797 "0612702-006C:SAMP:NO3 W' 6 0.080 0.865 "0612702-006CMS:MS:NO3 W' 7 0.572 6.091 "0612702-006CDUP:DUP:NO3 W' 8 0.079 0.854 "0612702-007C:SAMP:NO3 W' 9 2.187 4.663 5.00 "0612702-008C:SAMP:NO3 W' 10 3.302. 7.031 5.00 "CCV:CCV:NO3 W' S2 0.986 10.487 Known Cone: 1.000 "CCB:CCB:NO3 W' I S16 0.000 0.017 Known Cone: 0.000 "0612702-009C:SAMP:NO3 W' 11 2.642 5.628 5.00 "0612702-01OC:SAMP:NO3 W' 12 6.675 7.106 10.00 "0612702-011C:SAMP.NO3 W' 13 0.038 0.420 "0612702-012C:SAMP:NO3 W' 14 0.053 0.584 "0612702-013C:SAMP:NO3 W' 15 0.035 0.383 "LFB1-120706:LFB:NO3 W' 1 16 0.481 5.123 "LFBD1-120706:LFBD:NO3 W' 17 0.485 5.169 "CCV:CCV:NO3 W' S2 0.978 10.406 Known Cone: 1.000 "CCB:CCB:NO3 W' 1 S16 -0.000 0.016 Known Cone: 0.000 Analyte Properties Table for no3120706a.omn Property Channe12 Nitrate as N Concentration Units mg NIL Callibration Fit Type First Order Clear Calibration True Force Through Zero False Calibration Weighting None Auto Dilution Trigger True % of High Standard 100 Quik Chem Method 10-107-04-1-C Chemist Direct/Bipolar Calibration by Height 'I False Run: no3120706a -1- T 11r-1•13TI�- 9,-c (030/,- 1?,Ov00G. Ke -c- q IO .0 O-/ ✓= 0, S. M- (Z -0-C. K (O °% ? eec. qBq/ , Author: bnk H2M Labs. Inc. Date: 12/7/2006 Inject to Peak Start 14 Peak Base Width 1 54 Channel 2 (No2/No3) : Set 1 of 2 3.469 — -01 CO 0 c ui ig vl COI I az „� I CO z m ml 0 3 0 to MI z z N ' MO MO z : cel 000 �g NMI N 3 CO O p v a O w a Z 2.159-T } C 3 ,- v I O z z Z o O ¢ z Q. U [] ¢ f!) (j CO U ri v M� 3 v 3 �I in U o C n a o: n 2 c5 O U g ¢ o O O n O f0 M 0 N MI p c ?� �I J Y ¢ w ¢ fU N o O 4 N O O Co O N U U U in N r rg 1.166 �3 0 N,U 0 �`�j 0 0 r o o N o 0.986 mg 1.000 g N _ r- o 0.859"g Ncj o c� U (n B i2 civ •7 No N o N r 9 ti N n 0.572 N g him 0.66 g NIL 0.500Ug NU U ;y U o 0 0 0.35609 o 0.43II g/ II J0,1000.050 r0.000 J mg iZ 11 �g N-0.0010.000530.01 g 1 0.08 g N0.07 g ! 0.000 - 65.7 Run: no3120706a -2- Time (s) 1585.4 Author: bnk H2M Labs. Inc. Date: 12/7/2006 Channel 2 (No2Mo3) : Set 2 of 2 3.469 2.159- 49 .159- 49 > 0.000 -- 1585.0 Table 1: Nitrate as N Time (s) 3104.8 Cone. (mg NIL) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time I 2.000 1 21.273 1.611 -0.1 12/7/2006 3:13:06 PM O Z 1 10.600 0.807 MI �I 3:14:18 PM Z Q QII 1 I 0.405 Z m 1217/2006 3:15:31 PM N U Z ? Z Z tmi Z V 3:16:44 PM rn o n � a. Q g Q io r o U > 3:17:57 PM 0 o N u fn V cn o N v U MI OI N Z - o N 0 0 M o 7 m � 0 m 0.978 NIL U N 0.6689 NM N J J m9 U M 0.52 g N N 0.4810t NIb L m 0 0 L, o U D.0 a 0.03§%gww +g -0.000 mg NIL 0.000 -- 1585.0 Table 1: Nitrate as N Time (s) 3104.8 Figure 1: Nitrate as N 21.273, Nitrate as N concentration, mg NIL 2.000 Area = 10.620 * Conc + 0.017 Conc = 0.094 * Area - 0.002 Correlation Coefficient (r) =1.00000 No Weighting Run: no3120706a - 3 - Cone. (mg NIL) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 1 2.000 1 21.273 1.611 -0.1 12/7/2006 3:13:06 PM 2 1.000 1 10.600 0.807 0.3 1217/2006 3:14:18 PM 3 0.500 1 5.329 0.405 -0.0 1217/2006 3:15:31 PM 4 0.100 1 1.104 0.084 -2.4 1217/2006 3:16:44 PM 5 0.050 1 0.563 0.043 -2.7 12/7/2006 3:17:57 PM 6 0.000 1 1 -0.006 -0.0001 1 12/7/2006 3:19:11 PM Figure 1: Nitrate as N 21.273, Nitrate as N concentration, mg NIL 2.000 Area = 10.620 * Conc + 0.017 Conc = 0.094 * Area - 0.002 Correlation Coefficient (r) =1.00000 No Weighting Run: no3120706a - 3 - ME gluffii - a-, "111 "Ill. -I. WE...- ii "UvISCO Phenols Method 420.1 PCT�k oc,,Analyst: *? Distillation Date: Date: Time: 9: 00 P 0075 TSL008 W27 Phenols Calibration 1-4-06 conc abs 0 0.000 5 0.012 10 0.025 20 0.048 30 0.068 40 0.095 50 0.12 Intercept (b) -0.0069 slope (m) 421.33 r 0.9994 TSL008 W28 Pe 75k ON? SULFATE DATE: /Z • 4v - /3:.W ANALYST: i Si �6 to CLIENT ID LAB# MLS USED ABS. MG/L (GRAPH MG/LTZ;S ICV (20.0 mg/L) �s (a f D Ig. 9 ICB-� �6 a� 4.000 x S-.0 3p oo I Eg .. t 6 f r S.Q;c Y� 2 O -C 3t. Fr-) fig• J3 2Y• x.s : lW CCV(20.0 mg/L) 0 , f 6 r� ; , CCB �Sr 0.00 GJ'• t� 2-0610 0 IY•z xto, / .2 �v2-va S ,o.3z 3Y.2x�v� 3Y2 )t W2 tY3 �pSD`��QA tY.Sn149 !YS' CCV(20:0 mg/L) Z J 0.1 O f �• % Y Sr. CCB c0. O00 .0 S • � 6( 2- 004 -8�D ,r,7. 0, til? it lo fS (Urt 50 �• O� , s Gk oL 2 z- 0 rx t o p. 16 2_ 1. F b �,oL_or3A 01000 /-S./D CCV(20.0 mg/L) if 0. l4 D l9-? CCB is- 0,0010 ,CS fl pe p 0 - 009A 10 0. 3,57$ 36.�x,t.S; 9l-3 M -003 23- ,o . rB X 2 q — (0 . z.S•,? 2 �. 9 -Oas to 0.,539 35'.1 x I -S,:- CCV(20.0 mg/L) .� S b. op• qY. S CCB �S 0 00 t7 x,50 0 F 0039 Calibration 11/27/06 conc abs 0 0.000 5 0.023 10 0.06 15 0.118 20 0.175 25 0.226 30 0.284 35 0.347 40 0.400 Intercept (b) 2.7511 slope (m) 95.06 corr. Coeff. 0.9956 y = 40 30 95.064x SO4.11127/06 + 2.7511 ♦ / J / E 20 . conc I c Linear (con c) O U 10 0 0.000 0.100. 0.200 0.300 0.400 0.500 0.600 Absorbance ♦ Page 1 of 1 TSL008 W30 (JDried Wt.(a) - Tare Wt. (a))xl oo0)x100o Solids(mgll)= mL Sample ANALYST: "A TQ. /7 /SJ QTA OT. lL/ tm IDS TD SS/ TS TEMP. Lit uurrvrv. // .9A71, %/" s6 ova' gooq��D7 V -in llj MCI I TSL008 W31 W TZ T -M ARE SOLID ETIM M, t z, �ammm mo mmmmm TSL008 W31 rforled Wt (4)- Tare Wt (a1}x10001x1000 Sollds(rrigll)= mL Sample ANALYST: f/ TEMP. I SOLIDS TD SSI TS DATE: START: PAN/ SAMPLE mUIVIlD1TY: DRIED TARE SOLID RESULT DRIED IGNITED VOL. VO E LAB # CLIENT ID CRUC. ML WT G WEIGHT G WEIGHT G MG1L WT G WT G WT G S. (MG/L) :�oyq v O/W r1 �l�i 6`f -0�1A PSD 9 /co 2- —6bz.b m 5T o o 97, /o o�7 �o /.3/0 T 6 E 9 TSL008 W32 SOLIDS rfOried Wt M -Tare VVt.-Cq)lxl 00IX1000 SS/ TS Solids(mg/l)=' mL Sample ANALYST: TEMP. I A TSLOO8 W33 10 Mi SOLID WE ;MM Mw4ffinn =mom ■ M, Moe- MW im IMMMM/./ol MIAMM , , ; :�. M , ,, 11MM"40MM % mom @mint MAPMM M/ M w'', on -M m / MMM -M -�IMR/zs M- M. -M TSLOO8 W33 10 l{Drled Wt(q) - Tare Wt, WW0001x1000 Solids(mg/I)= mL Sample ANALYST: 11 I 1 SOLIDS I�S/ TS TEMP. . .. LAB # CLIENT ID PAN/ CRUC. SAMPLE ML DRIED WT G TARE WEIGHT G SOLID WEIGHT G RESULT MG/L DRIED WT G IGNITED WT G VOL. WT G VOLA MG/L) ell (� L? G/o /,702 • Ga9R 5 /YfM AV,,; , Ape 1. G o//o �s /� w a z �� . (� e '60� --mus MS fio 77 .,6 o . o yS �• ZG �v: ►� v; •� �Di '1 D , SSD PilQ 11 TSL008 W34 Effective immediately, when analyzing any matrix other than potable water for IDS, ,please take the conductivity of the sample and record it in the last column of the logbook. Please use the following guide for dilutions based on the conductivity. READING ON CONDUCTIVITY METER MLS OF SAMPLE TO USE On C up to 200/ on D under 800 100 mis Over 800 on D/up to 2.00 on E 50 mis On E from 2.00 to 5.00 25 mis On E from 5.00 to 8.00 20 mis Anything ast 8.00 on E to F 10 mis On F reading of 20 or higher 5 mis for 25 or lower 1 ml for 25 or higher All potable water samples should be analyzed at 100 mis. For fresh kills total and filtered samples use the same amount of sample volume for both sets of samples. TSL,008 W35 12/20/2006 12:33:30 PM Page 1 of 2 Concentration listed after Optical Blank Correction. fKNData Preparation dilution factor not applied to results. Peak SampleID SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 1 Primer PRIM 3.08 mg/I 1 3.08 12/20/2006 11:45:16 AM tkn_w 2 Drift DRIF 3.03 mg/I 1 3.03 12/20/2006 11:45:54 AM tkn_w 3 High HIGH 2.99 mg/I 1 2.99 12/20/2006 11:46:32 AM tkn_w 4 Low LOW 0.05 mg/I 1 0.05 12/20/2006 11:47:18 AM tkn w 5 Low LOW 0.05 mg/I 1 0.05 12/20/2006 11:47:57 AM tkn_w 6 Cal. CALB 3.01 mg/I 1 3.01 12/20/2006 11:48:40 AM tkn_w 7 Cal. CALB 0.97 mg/I 1 0.97 12/20/2006 11:49:19 AM tkn_w 8 Cal. CALB 0.48 mg/I 1 0.48 12/20/2006 11:49:59 AM tkn w 9 Cal. CALB 0.2 mg/I 1 0.2 12/20/2006 11:50:39 AM tkn_w 10 Cal. CALB 0.09 mg/I 1 0.09 12/20/2006 11:51:09 AM tkn_w 11 Cal. CALB 0 mg/I 1 00 12/20/2006 11:51:53 AM tkn_w 12 OPTICAL BLK QUAL 0.72 mg/I 1 0.72 12/20/2006 11:52:40 AM tkn_w 13 LCS-19210 ?l/.K•1 jA,5jL lcs 0.452 mg/l 10 4.52 12/20/2006 11D°J 11:53:19 AM tkn w 14 MB -19210 mblk 0.01 mg/I 1 0.01 12/20/2006 ta• 1 11:54:00 AM tkn w 15 0612702-OOIC < SAMP -0.03 mg/1 1 -0.03 12/20/2006 11:54:40 AM tkn w 16 0612702-002C , -u W - 3 D SAMP 3.8265 mg/1 20 76.53 12/20/2006 11:55:21 AM tkn_w Jar,., 17 0612702-003C M'`I " 3 SAMP 1.332 mg/I 20E----26-641 12/20/2006 11:56:00 AM tkn w 18 0612702-004C J lW - `OD SAMP 0.129 mg/I 20 2.58 12/20/2006 11:56:40 AM tkn w 19 0612702-005C kW - K 5 SAMP 3.8295 mg/I 20 76.59 12/20/2006 11:57:20 AM tkn w (' , A dt/v� 1• 20 0612702-606C 5� SAMP 3.7755 mg/I 20 75.51 12/20/2006 11:58:00 AM tkn_w ItU..a OJ C°-1' 21 0612702-006CMS ms 3.7745 mg/I 20 75.49 12/20/2006 11:58:40 AM tkn w ti Vcr6'1• 22 0612702-006CDUP dup 3.773 mg/l 20E---75.46 12/20/2006 11.59. 20 AM tkn &,,, wu-C`I. _w 23 0612702-007C KW ` CJS SAMP 0.168 mg/I 20 3.36 12/20/2006 11:59:58 AM tkn_w 24 0612702-008C KW SAMP 0.23 mg/I 1 0.23 12/20/2006 _ 12:00:40 PM tkn w 25 CCV 1.0 ccv I mg/I 1 12/20/2006 12:01:20 PM tkn w 26 CCB ccb 0.04 mg/I 1 0.04 12/20/2006 L0. l 12:01:58 PM tkn w 27 0612702-009C K W - $ SAMP 0.0485 mg/I 20 0.97 12/20/2006 12:02:27 PM tkn w a(AA � �� 28 0612702-OIOC M W- SAW 2.3145 mg/1 20 46.29 12/20/2006 12:03:20 PM M ft -W 29 0612702-OIIC R v- '65 SAMP 1.052 mg/I 20 21.04 12/20/2006 12:04:00 PM tkn w O 30 0612702-012C � ���-1� SAMP 3.7985 mg/I 20 75.97 12/20/2006 12:04:41 PM tkn w 9,, pie,-(k4R 12/20/2006 12:33:30 PM Page 1 of 2 Peak SamplelD SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 31 0612702-013C 'F3 SAMP -0.01 mg/l 1 -0.01 12/20/2006 12:05:20 PM tkn_w 32 0612750-OOIA SAMP 0.371 mg/l 10 3.71 12/20/2006 12:06:00 PM tkn_w 33 0612750-002A SAMP 0.639 mg/I 10 6.39 12/20/2006 12:06:40 PM tkn_w 34 0612751-001A SAMP 0.643 mg/l 10 6.43 12/20/2006 12:07:13 PM tkn_w 35 0612751-002A SAMP 0.191 mgA 10 1.91 12/20/2006 12:07:48 PM tkn_w 36 0612774-OOIA SAMP 0.748 mg/l 10 7.48 12/20/2006 12:08:40 PM tkn_w 37 CCV 1.0 ccv 0.99 mg/l 1 0.99 12/20/2006 00. 12:09:20 PM tkn w 38 CCB ccb 0.03 mg/l 1 0.03 12/20/2006k0- 12:10:00 PM tkn_w 39 0612774-002A SAMP 1.372 mg/l 10 13.72 12/20/2006 12:10:40 PM tkn_w 40 0612812-OOIA SAMP 0.76 mg/l 20 15.2 12/20/2006 12:11:20 PM tkn_w 41 0612829-OOIA SAMP 0.3695 mg/l 20 7.39 12/20/2006 12:12•:00 PM tkn_w - 42 0612829-002A SAMP 0.558 mg/l 20 F 11.16 12/20/2006 12:12:40 PM tkn w 43 0612830-OOIA SAMP 0.5715 mg/l 20 11.43 12/20/2006 12:13:20 PM tkn w 44 0612830-002A SAMP 0.5785 mg/l 20 11.57 12/20/2006 12:14:00 PM tkn w 45 0612847-OOIA SAMP 0.5755 mg/l 20 11.51 12/20/2006 12:14:40 PM tkn w 46 0612847-002A SAMP 0.5385 mg/l 20 10.77 12/20/2006 12:15:20 PM tkn_w 47 0612899-OOIA SAMP 1.294 mg/l 20 25.88 12/20/2006 12:16:00 PM tkn w 48 0612899-002A SAMP 0.701 mg/l 20 14.02 12/20/2006 12:16:40 PM tkn_w I mg/l 1 �� 12/20/2006 N5'(. 12:17:20 PM tkn_w 49 CCV 1.0 ccv 50 CCB ccb 0.04 mg/l 1 0.04 12/20/2006 I-0 • t 12:18:01 PM tkn w 51 0612876-OOIA SAMP 0.907 mg/l 20 18.14 12/20/2006 12:18:41 PM tkn w 52 0612876-002A SAMP 1.4795 mg/l 20 29.59 12/20/2006 12:19:20 PM tkn w 53 0612897-001A SAMP 1.313 mg/l 10 13.13 12/20/2006 12:20:00 PM tkn_w 54 0612897-002A SAW 1.427 mgA 10 14.27 12/20/2006 12:20:40 PM tkn_w 55 0613051-002A SAMP 0.284 mg/l 5 1.42 12/20/2006 12:21:20 PM tkn w 56 LFB-19210 � q, (,,*-j lib 0.451 mg/l to 4.51 12/20/2006 2:22:00 PM tkn w 57 LFBD-19210 `t' lfbd 0.447 mgfl 10 4.47 12/20/2006 WO ty 12:22:40 PM tkn w 1 mgfl 1 12/20/2006 1001 12:23:20 PM tkn w 58 CCV 1.0 ccv 59 CCB ccb 0.05 mgA 1 0.05 12/20/2006 LC• ( 12:24:00 PM tkn w 60 Drift DRIF 3.03 mg/l 1 3.03 12/20/2006 12:24:40 PM tkn w 61 End END .0.05 mg/l 1 0.05 12/20/2006 12:26:26 PM tkn_w 12/20/200612:33:30 PM Page 2 of 2 Post -run Report BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Post -run report Name of Run tkn122006R1 Name of Analysis :TKN.ANL Date of Report 12/20/2006 System No. :1 Date of Run Operator 12/20/2006 Cmo Type of System Start/Stop time :TRAACS :11:34 - 12:27 Comment #19210 Channel Type Real Data _ Channel ? z. Method Method 2 Dilution Unit mg/l mg/l Calibr. Fit Linear Corr. Coeff. 0.9997 Base 55 Gain 23 Sensitivity 0.4233 Sample Limit 1 Sample Limit 2 0 rl J 1, Pk Cup Sample Id Value 0 0 B Baseline 0.05 0 1 1 P Primer 3.08 1 2 1 D Drift 3.03 1 3 1 Hl High 2.99 1 4 0 L1 Low 0.05 1 5 0 L1 Low 0.05 1 6 1 C Cal. 3.01 1 7 2 C Cal. 0.97 1 8 3 C Cal. 0.48 1 9 4 C Cal. 0.20 1 10 5 C Cal. 0.09 1 11 0 C Cal. 0.00 1 12 8 QC1 OPTICAL BLK 0.72 1 13 9 QC1 LCS-19210 5.24 10 14 10 QC1 MB -19210 0.73 1 15 11 S 0612702-001C 0.69 1 16 12 S 0612702-002C 77.25 20 17 13 S 0612702-003C 27.36 20 1S 14 S 0612702-004C 3.30 20 19 15 S 0612702-005C 77.31 20 TKN.ANL / tkn122006R1.rUn Page 1 00 M 00 14 V) P" q Post -run Report BRAN+LUEBBE AACE 5.48 20 16 S 0612702-006C 76.23 20 21 17 S 0612702-006CMS 76.21 20 22 18 S 0612702-006CDUP 76.18 20 23 19 S' 0612702-007C 4.08 20 24 2.0 S 0612702-008C 0.95 1 25 2 QCl CCV 1.0 1.00 1 26 0 QC1 CCB 0.04 1 27 21 S 0612702-009C 1.69 20 28 22 S 0612702-OIOC 47.01 20 29 23 S 0612702-011C 21.76 20 30 24 'S 0612702-012C 76.69 20 31 25 S 0612702-013C 0.71 1 32 26 S 0612750-001A 4.43 10 33 27 S 0612750-002A 7.11 10 34 28 'S 0612751-OOIA 7.15 10 35 29 S 0612751-002A 2.63 10 36 30 S 0612774-OOIA 8.20 10 37 2 QC1 CCV 1.0 0.99 1 38 0 QCl CCS - 0.03 1 39 31 S 0612774-002A 14.44 10 40 32 S 0612812-OOIA 15.92 20 41 33 S 0612829-OOIA 8.11 20 42 34 S 0612829-002A 11.88 20 43 35 S 0612830-001A 12.15 20 44 36 S 0612830-002A 12.29 20 45 37 S 0612847-001A 12.23 20 46 38 S 0612847-002A 11.49 20 47 .39 S 0612899-OOIA 26.60 20 48 40 S 0612899-002A 14.74 20 49 2 QC1 CCV 1.0 1.00 1 50 0 QC1 CCB 0.04 1 . 51 41 S 0612876-001A 18.86 20 52 42 S 0612876-002A 30.31 20 53 43 S' 0612897-001A 13.85 10 54 44 S 0612897-002A 14.99 10 55 45 S 0613051-002A 2.14 5 56 46 S LFB-19210 5.23 10 57 47 S LFBD-19210 5.19 10 58 2 QC1 CCV 1.0 1.00 1 59 0 QC1 CCH 0.05 1 60 1 D Drift 3.03 1 61 0 B FinalBase 0.05 1 QC Limits Channel 2 TM.ANL / tknl22006R1.run Page 2 Post -run Report BRAN+LUEBBE RACE 5.48 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused. QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 1.4 ** <END OF REPORT> ** TKN.ANL / tkn122006R1.run Page 3 0 7t OO 0 BPAN,LUBBBE RACE 5.48 H2M Labs Inc. Calibration Curve Name of run :tknl22006R1.RUN Comment - C.Iib-li.. cu— Name of analysis :TKN.ANL TSL008 W41 Page 1 of 1 Channel :2 Method :Method 2 Curve fit :linear a--i.4769E-001 b=6.1706E-005 Corr. coeff. :0.9997 Peak [lk] 100 BO 60 40 20 0 O 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 [ 7 Conc. mg/l TSL008 W41 Page 1 of 1 BRAN:LUEBBE RACE 5.48 H2M Labs Inc. Post -run chart Name of run :tknl22000R1.RUN Comment - . Post -run chart Name of analysis :TKN.ANL min Channel 2 Method t Method 2 Unit mg/l Base 55 Gain 23 Corr. 0.9997 2 4 6 8 10 OB 0.05 1P 3.08 2D 3.03 12 3H 2.99 4L 0.05 5L 0.05 14 6C 3.01 7C 0.97 8C 0.48 16 Page -1 of 3 BRAN.LUEBBE RACE 5.48 me of run :tk4122006R1.RUN nment Post -run chart Name of analysis :TKN.ANL Page 2 of 3 min 9C 0.20 T. 10C 0.09 11C 0.00 18 12QC1 0.72 13QC1 5.24 14QC1 0.73 20 15S 0.69 S 77.25* 17S 27.36 22 18S 3.30 S 77.31* S 76.23* 24 S 76.21* S 76.18* 23S 4.08 26 24S 0.95 25QC1 1.00 26QC1 0.04 27S 1.69 28S 47.01 29S 21.76 30 S 76.69* 31S 0.71 32S 4.43 32 33S 7.11 34S 7.15 35S 2.63 34 36S 8.20 37QC1 0.99 Page 2 of 3 BRAN.LUEBBE AACE 5-48 me of run :tknl22006R1.RUN mment Post -run chart Name of analysis :TKN.ANL min 38QC1 0.03 36 39S 14.44 40S 15.92 41S 8.11 38 42S 11.88 43S 12.15 44S 12.29 40 45S 12.23 • - 46S 11.49 47S 26.60 42 48S 14.74 49QC1 1.00 SOQC1 0.04 44 51S 18.86 52S 30.31 53S 13.85 46 54S 14.99 55S 2.14 56S 5.23 48 57S 5.19 58QC1 1.00 59QC1 0.05 50 60D 3.03 52 f 61B 0.05 54 Page 3 of 3 00 0 C) L� L c Pd TAvv? TOTALjR6's'/TKN,DIGESTION*S NAME :_1VJW PPVPAW LAB NO. CLIENT ID .GRAMS, SAMPLE. WIGHT SAMPLE VOLUME -MLS FINAL �VOLUME MLS DATE �Wjjyl, ANALYZED - S E 06 2S� o010 OP - Z, 00k �b F02 - a0z r- Hie - Sp 762 - o06 C - IL k 5s 13-- 702- voeC 11 - Yo k9 P 001,9 10 F2A -t-A"'q INC. TOTAL XPSITKN DIGESTIONS NAME: *Alt? t' Li. bazmww DATE.: 11-19--19-z LAB NO. CLIENT ID SAMPLE. WEIGHTS GRAMS SAMPLE VOLUME .VOLUME m-r.S FINAL MLS DATE ANALYZED. SPIKE ,o6 �z - Al �—lp gl3o -901 el?7 ao2 le— JD Y.1 UAA o F bg) p -"()o'o A� 00 TKN Data Concentration listed after Optical Blank Correction. to Preparation dilution factor not applied results. Peak SampleID SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 1 Primer PRIM 2.96 mg/I 1 2.96 12/20/2006 03:55:26 PM tkn w 2 Drift DRIF 2.98 mg/I 1 2.98 12/20/2006 03:56:06 PM tkn w 3 High HIGH 2.99 mg/I 1 2.99 12/20/2006 03:56:46 PM tkn w 4 Low LOW 0.02 mg/I I 0.02 12/20/2006 03:57:25 PM tkn_w 5 Low LOW 0.02 mg/I 1 0.02 12/20/2006 03:58:05 PM tkn w 6 Cal. CALB 3.01 mg/I 1 3.01 12/20/2006 03:58:46 PM tkn_w 7 Cal. CALB 0.98 mg/I 1 0.98 12/20/2006 03:59:26 PM tkn_w 8 Cal. CALB 0.48 mg/I 1 0.48 12/20/2006 04:00:06 PM tkn_w 9 Cal. CALB 0.21 mg/I I 0.21 12/20/2006 04:00:46 PM tkn w 10 Cal. CALB 0.11 mg/I 1 O.I 1 12/20/2006 04:01:26 PM tkn w 11 Cal. CALB 0.01 mg/1 1 0:01 12/20/2006 04:01:53 PM tkn_w 12 OPTICAL BLK QUAL 0.66 mg/1 1 0.66 12/20/2006 04:02:46 PM tkn w 13 LCS1-19210 71%x{;1 Ics 0.41 mg/l 10 4.1 12/20/2006 04:03:26 PM tkn_w 14 MBI -19210 �1l/ mblk 0.01 mg/l 1 0.01 12/20/2006 LO •l 04:04:06 PM tkn w 15 0612702-002C KVJ-3a SAMP 1.085 mg/1 100 108.5 12/20/2006 04:04:46 PM tkn w 16 0612702-005C M V/- L(5 SAMP 0.7556 mg/1 100 75.56 12/20/2006 04:05:26 PM tkn w 17 0612702-006C M W - rj 1) SAMP 0.7192 mg/1 100 71.92 12/20/2006 04:05:59 PM tkn w 18 0612702 -006C %y1n511-ms 0.9173 mg/l 100 91.73 12/2012006Jt04:06:47 PM tknw M + 11¢c�✓cr 19 0612702 006CDUP dup 0.7263 mg/l 100 2.63 12/20/2006 �1'1'� 04:07:19 PM tkn _w 20 0612702-009C MW -65 SAMP 0.46 mg/l 1 0.46 12/20/2006 04:08:06 PM tkn w 5aJ}l+�F�l� 2 21 0612702-012C ` 4rWj tzlwko6 CK-QD SAMP 1.1591 mg/l 100 115.91 12/20/2006 04:08:46 PM tkn w 22 LFB 1-19210 X71/ L(. (k.3 Ifb 0.425 mg/1 10 4.25 12/20/2006 bwi. 04:09:26 PM tkn_w 23 LFBD1-19210 %L Md 0.426 mg/I 10 4.26 12/20/2006 M a 404:10:06 PM tkn_w 24 CCV1.0 cev 0.97 mg/I 1 0.97 12/20/2006 9t"7'(. 04:10:46PM tkn_w 25 CCB ccb 0.01 mg/I 1 0.01 12/20/2006 604 04:11:26 PM tkn w 26 Drift DRiF 2.98 mg/1 1 2.98 12/20/2006 04:12:06 PM tkn w 27 End END 0 mg/l 1 12/20/2006 04:16:28 PM tlm w 00 O O 12/26/2006 4:22:14 PM Page 1 of 1 [-� BRAN+LUEBBE RACE 5.48 Name of Run tkn122000R1 Date of Report 12/20/2006 Date of Run 12/20/2006 Operator Cmo Comment #19210 Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 1 H1 High 4 0 Ll Low 5 0 L1 Low 6 1 C cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. 11 0 C Cal. 12 8 QC1 OPTICAL BLK 13 9 QC1 LCS1-19210 14 10 QC1 MBl-19210 15 11 S 0612702-002C 16 12 S 0612702-OOSC 17 13 S 0612702,-006C 18 14 S 0612702-006CMS 19 15 S 0612702-006CDUP H2M Labs Inc. Post -run report Name of Analysis :TKN.ANL System No. :1 Type of System :TRAACS Start/Stop time :15:44 - 16:17 Real Data 2 2 Method 2 Dilution mg/l mg/l . Linear 0.9999 56 23 0.4301 Value va z J 11 V 0.00 0 2.96 1 2.98 1 2.99 1 0.02 1 0.02 1 3.01 1 0.98 1 0.48 1 0.21 1 0.11 1 0.01 1 0_66 1 4.76 10 0.67 1 109.16 100 76.22 100 72.58 100 92.39 100 73.29 100 TKN.ANL / tkn122006bR1.run Page 1 Post -run Report 00 00 QC Limits Channel 2 QC 1 Unused QC 2 Post -run Report BRAN+LUEBBE RACE 5.48 QC 4 Unused 20 16 S 0612702-009C 1.12 1 21 17 S 0612702-012C 116.57 100 22 18 S LFB1-19210 4.91 10 23 19 S LFBD1-19210 4.92 10 24 2 QC1 CCv 1.0 0.97 1 25 0 QC1 CCB 0.01 1 26 1 D Drift 2.98 1 27 0 B FinalBase 0.00 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %; 1.0 ** <END OF REPORT> ** TKN.ANL / tknl22006bRl.run Page 2 y� 00 0 BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Calibration Curve Name of run :tknl22006bR1.RUN Comment Calibration Curve Name of -analysis :TKN.ANL Channel :2 Method :Method 2 Curve fit :linear a= -1.1789E-001 b=5.9462E-005 Corr. coeff. :0.9999 Peak [%) 100 80- 06040200 60- 40- 20- OM 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ) Page 1 of 1 O 00 O O V) F-+ BRAN.LUEEEE AACE 5.46 H2M Labs Inc. Post -run chart Name of run :tknl22006bR1.RUN Comment Post -run chart Name of analysis :TKN.ANL Page 1 of 2 r -i 00 0 Channel 2 Method Method 2 Unit mg/1 Base 56 Gain 23 Corr. 0.9999 min 2 4 6 8 10 OB 0.00 1P 2.96 2D 2.98 12 3H 2.99 4L 0.02 SL 0.02 14 6C 3.01 7C 0.98 8C 0.48 16 Page 1 of 2 r -i 00 0 Post -run chart BRAN.LOEBBE AACE 5.48 me of run :tknl22006bR1.RUN Name of analysis :TKN.ANL ,mment min 9C 0.21 10C 0.11 11C 0.01 18' 12QC1 0.66 13QC1 4.76 14QC1 0.67 20 15S 109.16 16S 76.22 175 72.58 22 18S 92.39 19S 73-29 20S 1.12 24 21S 116.57 22S 4.91 23S 4.92 26 24QC1 0.97 25QC1 0.01 26D 2.98 28 30 32 . ii z7B 0.00 34 Page 2 of 2 N 00 O O VA Concentration listed after Optical Blank Correction. TKNData Preparation dilution factor not applied to results. Peak SamplelD SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 1 Primer PRIM 3.01 mg/l 1 3.01 12/23/2006 09:37:28 AM tkn_w 2 Drift DRIF 3.02 mg/l 1 3.02 12/23/2006 09:38:08 AM tkn w 3 High HIGH 3.03 mg/l 1 3.03 12/23/2006 09:38:48 AM tkn_w 4 Low LOW 0.02 mg/I l 0.02 12/23/2006 09:39:26 AM tkn_w 5 Low LOW 0.02 mg/I 1 0.02 12/23/2006 09:39:56 AM tkn_w 6 Cal. CALB 3.01 mgll 1 3.01 12/23/2006 09:40:48 AM tkn_w 7 Cal. CALB 0.98 mg/I I 0.98 12/23/2006 09:41:16 AM tkn_w 8 Cal. CALB 0.49 mg/1 1 0.49 12/23/2006 09:42:07 AM tkn_w 9 Cal. CALB 0.21 mg/l 1 _ 0.21 12/23/2006 09:42:48 AM tkn_w 10 Cal. CALB 0.1 mg/1 1 0.1 12/23/2006 09:43:28 AM tkn w 11 Cal. CALB 0.01 mg/l 1 0.01 12/23/2006 09:44:09 AM tkn_w 12 OPTICAL BLK QUAL 0.71 mg/I 1 0.71 12/23/2006 09:44:48 AM tkn_w 13 LCS-19244 "1%UK54- Ics 0.416 mg/l 10 4.16 12/23/2006 %a1'/ 09:45:27 AM tkn w 14 MB -19244 mblk 0.01 mg/l 1 0.01 12/23/2006 09:46:08 AM tkn w Pf 15 0612702-006C SAMP 0.92 mg/I 10 9.2 12/23/2006 09:46:48 AM tkn w 10 V� g7- i> 16 0612702-006CMS-IV-4i45;1L ms 1.267 mg/I 10 12.67 12/23/2006 $57: 09:47:28 AM tkn_w ��y' IZ-7 -fv = 1-l\1xgi 17 0612702-006CDUP :1 dup 0.922 mg/l 10 9.22 12/23/2006 D oy 09:48:08 AM tkn_w 18 0612951-OOIA SAMP 1.3735 mg/l 20 27.47 12/23/2006 09:48:48 AM tkn_w 19 0612951-002A SAMP 0.284 mg/I 5 1.42 12/23/2006 09:49:26 AM tkn w 20 0612978-OOIA SAMP 1.902 mg/I 10 19.02 12/23/2006 09:50:08 AM tkn w 21 0612978-002A SAMP 2.45 mg/1 10 24.5 12/23/2006 09:50:48 AM tkn w 22 0612980-OOIA SAMP 0.6905 mg/I 20E---13.81 12/23/2006 09:51:28 AM tkn_w 23 0612997-OOIA SAMP 0.6625 mg/1 20 13.25 12/23/2006 09:52:08 AM tkn_w 24 0612997-002A SAMP 1.6465 mg/I 20 32.93 12/23/2006 09:52:48 AM tkn w 25 CCV 1.0 ccv 0.99 mg/I 1 0.99 12/23/2006 q 09:53:28 AM tkn_w 26 CCB ccb 0.01 mg/I 1 0.01 12/23/2006 L 0 • ( 09:54:09 AM tkn_w 27 0613011-001A SAMP 0.737 mg/I 10 7.37 12/23/2006 09:54:48 AM tkn w M 28 0613011-002A SAMP 0.13 mg/1 10 1.3 12/23/2006 09:55:27 AM tkn w 29 0613014-002A SAMP 0.11 mg/I 1 0.11 12/23/2006 09:56:08 AM tkn w O 30 0613033-OOIA SAMP 1.229 mg/I 10 12.29 12/23/2006 09:56:48 AM tkn_w 12/23/2006 10:22:48 AM .�,�/ Page 1 of [� Peak SampleID SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 31 0613033-002A SAMP 0.19 mg/l 1 0.19 12/23/2006 09:57:28 AM tkn w 32 0613126-OOIA SAMP 0.6545 mg/l 20 F 13.09 12/23/2006 09:58:08 AM tkn_w 33 0613126-002A SAMP 1.803 mg/l 20 F 36.06 12/23/2006 09:58:48 AM tkn_w 34 0613141-OOIA SAMP 0.186 mg/I 5 0.93 12/23/2006 09:59:26 AM tkn_w 35 0613141-002A SAMP 1.618 mg/l 5 8.09 12/23/2006 10:00:08 AM tkn_w 36 0613164-OOIA SAMP -0.01 mg/l 1 0.01 12/23/2006 10:00:35 AM tkn w 37 CCV 1.0 ccv 0.99 mg/l 1 0.99 12/23/2006 c?rtll 10:01:28 AM tkn_w 38 CCB ccb 0.01 mg/I 1 0.01 12/23/2006 L0.1 10:02:09 AM tkn_w 39 0613169-OOIA SAMP 0.819 mg/l 10 8.19 12/23/2006 10:02:48 AM tkn_w 40 0613169-002A SAMP 1.605 mg/l 10 16.05 12/23/2006. 10:03:29 AM tkn_w 41 0613185-0OIA SAMP 1.753 mg/l 20 F 35.06 12/23/2006 10:04:-08 AM tkn_�v 42 0613185-002A SAMP 0.174 mg/l 5 0.87 12/23/2006 10:04`46 AM tkn_w 43 0613202-OOIA SAMP 0.559 mg/l 20 I1.] 8 12/23/2006 10:05:28 AM tkn_w 44 0613202-002A SAMP 1.684 mg/l 20 33:68 12/23/2006 10:06:08 AM tkn_w 45 0613203-OOIA SAMP 0.8235 mg/l 20 16.47 12/23/2006 10:06:48 AM tkn w 46 0613204-OOIA SAMP 1.52 mg/l 10 15.2 12/23/2006 10:07:28 AM tkn_w 47 0613204-002A SAMP 3.211 mg/1 10 32.11 12/23/2006 10:08:08 AM tkn w & c,,4 overC-1- 48 0613243-OOIA SAMP 0.632 mgfl 10 6.32 12/23/2006 10:08:46 AM tkn w 49 CCV 1.0 ccv 0.99 mg/l 1 0.99 12/23/2006 'Fly 10:09:28 AM tkn_w 50 CCB ccb 0.01 mg/1 1 0.01 12/23/2006 /0. ( 10:10:06 AM tkn_w 51 0613243-002A SAMP 0.126 mgfl 10 1.26 12/23/2006 10:10:48 AM tkn_w 52 LFB-19244 TV- T • j/ft5 ! / t- Ifb 0.454 mg/l 10 4.54 12/23/2006 10:11:28 AM tkn w 53 LFBD-19244 W lfbd 0.453 mg/( 10 4.53 12/23/2006 00-:410:12:08 AM tkn_w 0.98 mgfl 0 1 0.98 12/23/2006 9 - 10:12:48 AM tkn_w 54 CCV 1.0 ccv 55 CCB ccb 0 mg/1 1 12/23/2006 40`i 10: 13:26 AM tkt w 56 Drift DRIF 3.02 mg/l 1 3.02 12/23/2006 10:14:08 AM tkn_w 57 End EMD 0.01 mg/l 1 0.01 12/23/2006 10:15:29 AM tkn_w 00 O O 12123/2006 10:22:49 AM Page 2 of 2 BRAN+LUEBBE AACE 5.48 Name of Run tknl22304 Date of Report 12/23/2006 Date of Run 12/23/2006 Operator Cmo Comment ? ... H2M Labs Inc. Post -run report Name of Analysis :TKN.ANL System No. :1 Type of System :TRAACS Start/Stop time :09:26 —10:16 Channel Type Real Data Channel _ 2 ? ... Method Method 2 Dilution Unit mg/1 mg/l Calibr. Fit Linear Corr. Coeff. 0.9999 Base 70 Gain 24 Sensitivity 0.4222 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value Vale �l�J 0 0 B Baseline 0.01 0 1 1 P Primer 3.01 1 2 1 D Drift 3.02 1 3 1 H1 High 3.03 1 4 0 L1 Low 0.02 1 5 0 L1 Low 0.02 1 6 1 C Cal. 3.01 1 7 2 C Cal. 0.98 1 8 3 C Cal. 0.49 1 9 4 C Cal. 0.21 1 10 5 C Cal. 0.10 1 11 0 C Cal. 0.01 1 12 8 QC1 OPTICAL BLK 0.71 1 13 9 QC1 LCS-19244 4.87 10 14 10 QC1 MB -19244 0.72 1 15 11 S 0612702-006C 9.91 10 16 12 S 0612702-00GCMS 13.38 10 17 13 S 0612702-006CDUP 9.93 10 18 14 S 0612951-OOIA 28.18 20 19 15 S 0612951-002A 2.13 5 TKN.ANL / tkn122304.run Page 1 Post -run Report In 00 0 0 C/)L L QC Limits Chanel 2 QC 1 Unused Post -run Report BRAN+LUEBBE RACE 5.48 QC 3 Unused 20 16 S 0612978-OOIA 19.73 10 21 17 S 0612978-002A 25.21 10 22 18 S 0612980-001A 14.52 20 23 19 S 0612997-OOIA 13.96 20 24 20 S 0612997-002A 33.64 20 25 2 QC1 CCV 1.0 0.99 1 26 0 QC1 CCB 0.01 1 27 21 S 0613011-001A 8.08 10 28 22 S 0613011-002A 2.01 10 29 23 S 0613014-002A 0.82 1 30 24 S 0613033-OOIA 13.00 10 31 25 S 0613033-002A 0.90 1 32 26 S 0613126-OOIA 13.80 20 33 27 S 0613126-002A 36.77 20 34 28 S 0613141-OOIA 1.64 5 " 35 29 S 0613141-002A 8.80 5 36 30 S 0613164-001A 0.70 1 37 2 QC1 CCV 1.0 0.99 1 38 0 QC1 CCB 0.01 1 39 31 S 0613169-001A 6.90 10 40 32 S 0613169-002A 16.76 10 41 33 S 0613185-001A 35.77 20 42 34 S 0613185-002A 1.58 5 43 35 S 0613202-001A 11.89 20 44 36 S 0613202-002A 34.39 20 45 37 S 0613203-001A 17.18 20 46 38 S 0613204-OOIA 15.91 10 47 39 S 0613204-002A 32.82 10 48 40 S 0613243-OOIA 7.03 10 49 2 QC1 CCV 1.0 0.99 1 50 0 QC1 CCH 0.01 1 51 41 S 0613243-002A 1.97 10 52 42 S LFB-19244 5.25 10 - 53 43 S LFBD-19244 5.24 10 54 2 QC1 CCV 1.0 0.98 1 55 0 QC1 CCB 0.00 1 56 1 D Drift 3.02 1 57 0 B FinalBase 0.01 1 QC Limits Chanel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused TKN.ANL / tknl22304.run Page 2 Vi 00 0 C) BRAN+LUEBBE RACE 5.48 QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel Baseline Drift Carry over ** <END OF REPORT> ** 2 Yes Yes Yes 0.8 TKN.ANL / tkn122304.run Page 3 Post -run Report 00 0 BRAN.LUEBBE RACE 5.48 H2M Labs Inc. Calibration Curve Name of run :tknl22304.RUN Comment Calibration Curve Name of analysis :TKN.ANL Channel :2 Method :Method 2 Curve fit :linear a= -1.4089E-001 b=5.8806E-005 Corr. coeff. :0.9999 eak [W) 100 80- 06040200 60- 40- 20- 0 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. ( mg/1 ) Page 1 of 1 00 00 0 �ll F--1 BRAN.LUEBBE FACE 5-48 H2M Labs Inc. Post -run chart Name of run :tkn122304.RUN Comment Post -run chart Name of analysis :TKN.ANL Page 1 of 3 Post -run chart BRAN•LUEBBE AACE 5.48 Name of analysis :TKN.ANL me of run :tknl22304.RUN Page 2 of 3 BRAN.LUEBEE RACE 5.46 ame of run :tkn122304.RUN 'omment Post -run chart Name of analysis :TKN.ANL min 0.99 36 38QC1 0.01 39S 8.90 40S 16.76 41S 35.77 38 42S 1.58 43S 11.89 34.39 40 44S 45S 17.18 46S 15.91 32.62 42 47S 48S 7.03 49QC1 0.99 50QC1 0.01 44 51S 1.97 52S 5.25 5.24 46 53S 54QC1 0.98 55QC1 0.00 3.02 48 56D 57B 0.01 50 52 s 54 Page 3 of 3 00 0 O 14 IH2A LAUS9 INC. paa oor TOTAL - 3=-g/TKN DIGESTIONS NAM: ,0r4(, DATE: - Y., VOW W&TOP 1cl.) LAB NO. CLIENT ID SAMPLE WEIGHT- GRAMS SAMPLE VOLUME ...VOLUME MLS FINAL - MLS DATE ANALYZED SPTJm M qsl-0014 5ft, ?,q - oolk Ripe - IN -002A v4l5,of got A So 'ply I yt -0014 pee- Spey J j�l-va � 5:� �3 -� k 90 k I kT;QD P 0022 N 00 C) As IH2A LA. US 9 isco - 29 331 TOTAL PdSITKN DIGESTIONS NAME: A%1 !;,M Aparl-tw DATE: 12-2-2-o6 LAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE -VOLUME MLS FINAL VOLUME MLS DATE ANALYZED SPIKE S ki -002A P9 l 10 �.Fb TV F Zf , M 00 0 C) �4 cn E-4 0 Oe tv Multiple Analysis Report Print Date/Time: 2006/12/19 8:49:46 Sample ID Result Std. Dev. . RSD Mode ALT Method ID Sample a Vial Timestamp -- Message------- -----= 0.2554 RCS 0.0067 2.63 UTILITY Cleaning procedure Sample sp 2006/12/18 18:14 1 2006/12/18 18:44 L'1 2S'p�"' 24.6480 0.1881 0.76 TOC TOC WASTE WATER Sample Sample 2 2006/12/18 19:15 Low Sample ICH L�,(�1 0.0710 0.1502 211.62 TOC TOC WASTE WATER -DDete_ej 7. CRI.j.� �•••f�3/ 1.1331... 0.1312.. 11.SS... TOC TOC WASTE WATER Sample 3..2006/12/18 19:46.Low Sample -O Detected A-40 0.1407 -49.51 TOC TOC WASTE WATER Sample 4 2006/12/18 20:17 Low Sample MBLK -0.2841 -u Detected 0.1193 -31.63 TOC TOC WASTE WATER Sample 5 2006/12/18 20:48 Low Sample 0612702-OOIALS �:l�.6 -0.3771 -O Detected * 0612702-002A.No��1 ...... 35.2924... 1.8326.. 5.19 ... TOC TOC WASTE WATER Sample „ 6..2006/12/18 7 2006/12/18 21:19. 21:49 0612702-003A-�' .•6 S� 12.8724 1.0189 7.92 TOC TOC WASTE WATER WATER Sample Sample 8 2006/12/18 22:19 0612702-004A �Lto 10.4807 0.4335 4.14 TOC TOC TOC WASTE WASTE WATER Sample 9..2006/12/18 22:49. 0612702-005A. r`�(i••••••• 25.8524... SL' 1.3000.. 5.03 3.83 ... TOC TOC TOC WASTE WATER Sample 10 2006/12/18 23:49 0612702-006A 24.4212 �(J.I Gnpr^/04% 4.7874 0.9351 0.6694 1.92 TOC TOC WASTE WATER Sample 11 2006/12/18 23:49 0612702-006AM ,P F�� 2.0693.. 8.70...TOC .. TOC WASTE WATER ...Sample ].2..2006/12/19 00:20. 0612702-006ADUP... ....`�b/•23.7914... 0612702-007A f�1�J'� S 7.5413 0.5862 7.77 TOC TOC WASTE WATER Sample 13 2006/12/19 14 2006/12/19 00:49 01:17 Low Sample 0612702-008A 1.6311 0.1518 9.31 TOC TOC WASTE WATER Sample -4Detectedv� CCV-yr-.'F�f g�^�............ 25.3396... 0.2581., 1.02...TOC TOC WASTE WATER Sample Sample 15..2006/12/19 16 2006/12/19 01:47. 02:22 Low Sample CCB 4�.O 0.5353 0.1440 26.90 TOC TOC WASTE WATER -O Detected^ �•� 0612702-009AfA �i 3.8342 0.1955 5.10 TOC TOC WASTE WATER17 Sample 2006/12 19 18..2006/12/19 02:5 03:21. 0612702-010A. :r.fQ....... 19.4818... 0.8138.. 4.18 ... TOC .. TOC WASTE WATER WATER ...Sample Sample 19 2006/12/19 03:51 0612702-OIIAptT 20.6017 d Z 1.2523 1.3079 6.08 3.63 TOC TOC TOC TOC WASTE WASTE WATER Sample 20 2006/12/19 04:22 0612702-012A sO,fi 35.9805 TOC WASTE WATER ...Sample 21..2006/12/19 04:53.Low Sample 0612702-013A. �3....•••••. 1.3049... 0.1403.. 10.75 ... TOC -u Detected , ,� CCV �(..,% U�1�'N 25.7520 0.2245 0.87 TOC TOC WASTE WATER Sample Sample 22 2006/12/19 23 2006/12/19 05:23 05:54 Low Sample CCB LI,Q 0.5509 0.2370 43.02 TOC TOC WASTE WATER -0 Detected Printed: 12119106 8:49:49 AM AM TSL008 W64 Page 1 of 1 -0 -0 -0 Detailed Analysis Report Print Date/Time: 2006/12/19 8:49:51 ===IDI Mode: UTILITY Sample ID: Method: Cleaning Procedure Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 18:14 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2643 0.1322 31651 11.387 11.584 120 2 0.2542 0.1271 30701 11.426 11.624 120 3 0.2552 0.1276 30801 11.432 11.629 120 4 0.2480 0.1240 30129 645120-- 11.445 11_ ------- --------------------------------------------------------- <<<Statistics>>> Mean: 0.2554 Std Dev: 0.0067 RSD: 2.63 Sample ID: LCS Mode: TOC Filename: 12181749 Method: TOC WASTE WATER Timestamp: 2006/12/18 18:44 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 24.5872 1.2294 237112 11.529_ 12.523, 109 2 24.7134 1.2357 238294 11.514 12.511 110 3 24.8672 1.2434 239734 11.495 12.493 110 4 24.4242 1.2212 235586 11.539 12.531 110 ------------------------------------------------------ - Mean: 24.6480 Std Dev: 0.1881 RSD: 0.76 Sample ID: ICB Mode: TOC Filename: 12181749 Method: TOC WASTE WATER TOC WW CURVE 100906 Timestamp: 2006/12/18 19:15 Cal. Curve: .Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 -0.0432 -0.0022 6500 11.466 11.454 120 120 2 0.0066 0.0003 6966 11.455 11.459 3 0.0288 0.0014 7174 11.456 11.449 120 4 0.2917 0.0146 9635 11.440 11.470 120 ------------------------------------------------------ Last Message: Low Sample Detected 0.0710 Std Dev: 0.1502 RSD: 211.62 <<<Statistics>>> Mean: Sample ID: CRI Mode: TOC Filename: 12181749 Method: TOC WASTE WATER TOC WW CURVE 100906 Timestamp: 2006/12/18 19:46 Cal. Curve: operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 1.2366 0.0618 18483 11.482 11.511 120 2 1.1169 0.0558 17362 11.517 11.529• 120 3 0.9537 0.0477 15833 11.548 11.589 120 4 1.2251 0.0613 18375 11.520 --------------------11 589120 --- - ----------------------------------------------------- Last Message: Low <<<Statistics>>> Sample Detected Mean: 1.1331 Std Dev: 0.1312 RSD: 11.58 Sample ID: MBLK Mode: TOC Filename: 12181749 Method: TOC WASTE WATER TOC WW CURVE 100906 Timestamp: 2006/12/18 20:17 Cal. Curve: Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 -0.2184 -0.0109 4860 11.510 11.515 120 2 -0.4937 -0.0247 2282 11.523 11.529 120 Printed: 12119106 8:49:54 AM AM Page 1 of 6 00 V) 3 -0.2313 -0.0116 4738 11.504 11.529 120 - 4 -0.1929 -0.0096 5098 11.472 11.492 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.2841 Std Dev: 0.1407 RSD: -49.51 Sample ID: 0612702-001A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 20:48 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.4532 -0.0227 2661 11.531 11.505 120 2 -0.5009 -0.0250 2215 11.510- 11.457 120 3 -0.3055 -0.0153 4044 11.484 11.465 120 4 -0.2489 -0.0124 4574 11.473 11.434 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.3771 Std Dev: 0.1193 RSD: -31.63 Sample ID: 0612702-002A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 _ Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 21:19 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 37.5856 1.8793 358815 11.535 12.522 111 2 35.9557 1.7978 343554 11.487 12.476 111 3 33.8675 1.6934 324003 11.454 12.452 112 4 33.7606 1.6880 323002 11.478 12.475 111 ----------------------------------------------------------------------------- <<<Statistics>>> Mean: 35.2924 Std Dev: 1.8326 RSD: 5.19 Sample ID: 0612702-003A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 21:49 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 14.1113 0.7056 139027 11.408 12.395 106 2 13.1378 0.6569 129913 11.377 12.368 105 3 12.5549 0.6277 124455 11.361 12.344 105 4 11.6857 0.5843 116317 11.376 12.361 106 --------------- -------------------------------------------------------------- <<<Statistics>>> Mean: 12.8724 Std Dev: 1.0189 RSD: 7.92 Sample ID: 0612702-004A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 .Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 22:19 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 11.0949 0.5547 110785 11.350 12.346 105 2 10.2173 0.5109 102569 11.329 12.316 104 3 10.1387 0.5069 101832 11.333 12.329 105 4 10.4719 0.5236 104952 11.299 12.299 104 ------=---------------------------------------------------------------------- <<<Statistics>5> Mean: 10.4807 Std Dev: 0.4335 RSD: 4.14 _ Sample ID: 0612702-OOSA Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/18 22:49 Operator ID: JASON SAMUEL Sample Type: Sample i Printed: 12119/06 8:49:54 AM AM Page 2 of 6 00 �ll Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 27.7998 1.3900 267191 11.313 12.303 109 2 25.1915 1.2596 242770 11.316 12.304 110 3 25.2913 1.2646 243704 11.252 12.239 109 4 25.1272 1.2564 242168 ---11_232--- -12.224 - -- 109--- ----------------------------------------- <<<Statistics>>> Mean: 25.8524 Std Dev: 1.3000 RSD: 5.03 Sample ID: 0612702-006A Mode: TOC Method: TOC WASTE WATER : 12181749 Filename� Timestamp: 2006/12/18 23:19 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline ; Time 1 24.9773 1.2489 240765 11.248 12.233 108 2 25.4195 1.2710 244905 11.177 12.163 11 109 3 23.8778 1.1939 230470 11.132 12.120 109 4 23.4102 1.1705 226092 121 11_ -- ---------------------- - <<<Statistics>>> Mean: 24.4212 Std Dev: 0.9351 RSD: 3.83 Sample ID: 0612702-006AMS Mode: TOC Method: TOC WASTEWATER Filename: 121817,49 Timestamp: 2006/12/18 23:49 Cal. Curve: TOC WW CURVE 100906 Type: Sample Operator ID: JASON SAMUEL Sample # C ug. C Raw Data Beginning Ending (Integration Rep ppm Baseline , Baseline Time 1 34.7833 1.7392 332577 11.232 12.219 111 2 35.7275 1.7864 341418 11.215 12.204 112 3 34.4255 1.7213 329227 11.227 12.223 112 4 34.2134 1.7107 327242 11.252 12.251 111 ---------------------- ------------------------------------------------------ <<<Statistics>>> Mean: 34.7874 Std Dev: 0.6694 RSD: 1.92' Sample ID: 0612702-006ADUP Mode: I TOC Method: TOC WASTE WATER Filename: 12181749 Timestamp: 2006/1'2/19 00:20 Cal. Curve: TOC WW CURVE 100906 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline I Time 1 26.0456 1.3023 250767 11.438 12.437 109 2 24.9319 1.2466 240339 11.362 12.353 109 3 22.6864 1.1343 219315 11.345 12.340 109 4 21.5017 1.0751 208223 11.312 12.299 108 ----------------------------------------------------- Mean: 23.7914 Std ---------------- Dev: 2.0693 RSD: 8.701 Sample ID: 0612702-007A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 2006/12/19 00:49 Cal. Curve: TOC WW CURVE 100906 Timestamp: Type: Sample Operator ID: JASON SAMUEL Sample # C ug C Raw Data Beginning Ending integration Rep ppm Baseline Baseline Time 1 8.3289 0.4164 84888 10.869 11.658 102 2 7.0280 0.3514 72707. 10.828 11.828 101 3 7.6382 0.3819 78420 10.714 11.700 102 4 7.1700 0.3585 74036 102 ----------------- ------------------ <<<Statistics>>> Mean: 7.5413 Std -----10_667------11_666 Dev: 0.5862 RSD: 7.77 Sample ID: 0612702-008A Mode: , TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/19 01:17 Printed: 12119/06 8:49:54 AM AM Page 3 of 6 00 C) Cl Y ---i GLLS Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 1.8065 0.0903 23818 10.234 10.168 120 2 1.4732 0.0737 20698 10.120 10.082 120 3 1.7038 0.0852 22857 10.017 9.980 120 4 1.5408 0.0770 21331 9.971 9.969 120 --------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: 1.6311 Std Dev: 0.1518 RSD: 9.31 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 12181749 2006/12/19 01:47 Cal. Curve: TOC WW CURVE 100906 Timestamp: Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 24.9601 1.2480 240603 9.832 10.821 109 2 25.5289 1.2764 245929 9.791 10.785 109 3 25.4661 1.2733 245342 9.735 10.734 109 4 25.4033 1.2702 244753 9.721 10.707 109 ---- ------------------------------------ <<<Statistics»> ------------------ Mean: 25.3396 Std Dev: 0.2581 RSD: 1.02 Sample ID: CCB Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/19 02:22 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.4219 0.0211 10854 9.659 9.684 120 2 0.4334 0.0217 10962 9.651 9.697 120 3 0.5542 0.0277 12093 9.679 9.706 120 4 0.7318 0.0366 13756 9.854 9.925 120 ------- ---------- ------------------------------------------------------ Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5353 Std Dev: 0.1440 RSD: 26.90 Sample ID: 0612702-009A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/19 02:51 Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 3.8749 0.1937 43185 10.536 11.532 99 23.6420 0.1821 41004 10.582 11.572 98 3 4.0896 0..2045 45195 10.619 11.614 100 4 3.7301 0.1865 41829 10.692 11.686 99 ------------------- <<<Statistics>>> ------------------------------------- Mean: 3.8342 Std Dev: 0.1955 RSD: 5.10 Sample ID: 0612702-010A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/19 03:21 Operator ID: JASON SAMUEL - Sample Type: Sample Rep # C ug C Raw Data Beginning Ending Integration ppm Baseline Baseline Time 1 20.5616 1.0281 199421 11.041 12.026 108 2 19.5026 0.9751 189506 11.045 12.039 107 3 18.6039 0.9302 181092 11.077 12.068 108 4 19.2589 0.9629 187224 11.055 12.041 107 ------------------------- <<<Statistics>>> ------------------------------- Mean: 19.4818 Std Dev: 0.8138 RSD: 4.18 Printed: 12/19106 8:49:54 AM AM Page 4 of 6 00 00 0 0 Sample ID: 0612702-011A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Timestamp: 2006/12/19 03:51 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL Rep # C ug C Raw Data Beginning Ending Integration ppm Baseline Baseline Time 1 22.1463 1.1073 214258 11.245 12.235 108 2 20.8991 1.0450 202581 11.249 12.238 107 3 20.1974 1.0099 196011 11.229 12.226 108 4 19.1639 0.9582 186334 11.272 12.272 107 ------------------- <<<Statistics>>> Mean: 20.6017 Std Dev: 1.2523 RSD: 6.08 Sample ID: 0612702-012A Mode: TOC Filename: 12181749 Method: TOC WASTE WATER Timestamp: 2006/12/19 04:22 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 37.6905 1.8845 359798 11.419 12.408 112 2 35.5936 1.7797 340165 11.394 12.383 112 3 36:0880 1.8044 344793 11.394 12.385,,,- 112 4 34.5500 1.7275 - 330393 -------------------- 11.371 12.363 113 ----------------------------------------- <<<Statistics>>> Mean: 35.9805 Std Dev:, 1.3079 RSD: 3.63 Sample ID: 0612702-013A Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Timestamp: 2006/12/19 04:53 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 1.2384 0.0619 18499 11.392 11.390 120 2 1.2348 0.0617 18466 11.395. 11.397 120 3 1.5153 0.0758 21092 11.381 11.424 120 4 1.,2312 0.0616 18432--- --11_406------11.432-- ----120 --------------------------------------- Last Message: Low Sample Detected 1.3049 Std Dev:- 0.1403 RSD: 10.75 <<<Statistics>>> Mean: Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Timestamp: 2006/12/19 05:23 Cal. Curve: TOC WW CURVE 100906 Sample Type: Sample Operator ID: JASON SAMUEL # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 25.4802 1.2740 245473 11.476 12.462 110 2 25.9725 1.2986 250083 11.510 12.501 110 3 25.6606 1.2830 247163 11.514 12.503 109 4 25.8946 1.2947----249353--------11.533---- -12.532-------109----- -------------------------- <<<Statistics>>> Mean: 25.7520 Std Dev: 0.2245 RSD: 0.87 Sample ID: - CCB Mode: TOC Method: TOC WASTE WATER Filename: 12181749 Cal. Curve: TOC WW CURVE 100906 Timestamp: 2006/12/19 05:54 Operator ID: JASON SAMUEL Sample Type: Sample # C ug C Raw Data Beginning Ending Integration Rep ppm Baseline Baseline Time 1 0.8463 0.0423 14828 11.601 11.626 120 2 0.6352 0.0318 12651 11.643 11.664 120 3 0.3942 0.0197 10595 11.676 11.686 120 - 4 0.3281 0.0164 9977 -------------------------------------------------------------- 11.671 11.664 120 Printed: 12/19/06 8:49:54 AM AM Page 5 of 6 00 Y4 � Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.5509 Std De v: 0.2370 RSD: 43.02 00 Printed: 12119106 8:49:54 AM AM Page 6 of 6 Calibration Report Print Date/Time: 2006/12/19 6:49:58 Cal. Curve ID: TOC WW CURVE 100906 Created: 2006/10/09 16:09 Calibration Factor (m): 1.873e+05 Y Intercept (b): 11051 r -squared: 0.99620 Standard ID DI 0.5PPM 1.OPPM S.OPPM 10.OPPM 25.OPPM 50.OPPM 75.OPPM y X Expected Measured Message Date & Raw Data 10967 ug C 0.000 ug C 0.000 Low Sample De Time 2006/10/09 13:25 15972 0.025 0.026 Low Sample De 2006/10/09 13:48 17342 0.050 0.034 Low Sample De 2006/10/09 14:11 44773 0.250 0.160 2006/10/09 14:34 97413 0.500 0.461 2006/10/09 14:56 282980 1.250 1.452 2006/10/09 15:19 467665 2.500 2.438 2006/10/09 15:42 710219 3.750 3.734 2006/10/09 16:06 Printed: 12119106 8:50:01 AM AM Page 1 of 1 00 O C) H2M LABS, INC. SDG NO.: - --S loocjQ SCAN: This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knnwledae.