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HomeMy WebLinkAboutMetals Data Package 06/2006Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSL006 Water Samples Received: 6/23/06 MPTai q n®TA PAr.KAGE I A 1- /Ak u S -W I Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. V 11747 ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 6/23/06 SDG NO.: TSL006 1. NYS DEC SUMMARY FORMS 1'I. SDG NARRATIVES Ill. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY us, INC. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION cnr_• Tci nna SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY Analytical Requirements Customer Sample Code Laboratory Sample Code ME we EQPT 0606916-001 X X i INW-1D 0606916-002 X _l- X i MW -1S 0606916-003 X X Mw -3D 0606916-004 X X MW -3S 0606916-005 X X I MW -4D 0606916-006 X X MW -4S 0606916-007 X X MW -5D 0606916-008 X X MW -5S 0606916-009 X X MW -6D 0606916-010 X X MW -6S 0606916-011 _ X X -j MW -8D 0606916-012 X X MW -8S _ 0606916-013 X X O O CLI , - LP lease indicate year of protocol) , TCUTAL, HSL, Priority Pollutant, tJ S NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSL006 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested Dat Recd at Lab Date Analyzed 0606916-001 IEQPT WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-002 MW -1D WATER I CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-003 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-004 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-005 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-005DUP MW-3SD I WATER cA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-005MS MW-3SS WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-006 MW -4D WATER I CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-007 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 123 -Jun -06 06/06 0606916-008 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-009 MW -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-010 MW -6D WATER I CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-011 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-012 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 0606916-013 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 23 -Jun -06 06/06 TSL006 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY INORGANIC ANALYSIS SDG: TSI -006 i Laboratory I Samp ID f Client Sample IDI Matrix Tests DateRecd at Lab Date Analyze 0606916-001 EQPT Blank i SELECT WET CHEMISTRY ** 06/23/06 I 06/06 - 07/06 0606916-002 MW -1D + Groundwater SELECT WET CHEMISTRY ** I 06/23/06 06/06 - 07/06 0606916-003 MW -IS I Groundwater SELECT WET CHEMISTRY ** 06/23/06 I 06/06 - 07/06 0606916-004 ( MW -3D Groundwater ` SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-005 MW -3S I Groundwater I SELECT WET CHEMISTRY ** I 06/23/06 I 06/06 - 07/06 0606916-005DUP I MW-3SDUP I Groundwater I SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-005MS MW-3SMS Groundwater I SELECT WET CHEMISTRY ** 06/23/06 I 06/06 - 07106 0606916-006 I MW -41) Groundwater SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-007 I MW -4S Groundwater SELECT WET CHEMISTRY ** I 06/23/06 06/06- 07/06 0606916-008 I MW -51) Groundwater SELECT WET CHEMISTRY** 06/23/06 I 06/06 —07/06 0606916-009 I MW -5S Groundwater i SELECT WET CHEMISTRY ** I 06/23/06 I 06/06 - 07/06 0606916-010 I MW -61) Groundwater SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-011 M.W-6S Groundwater SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-0.12 MW -81) Groundwater i SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 0606916-013 MW -8S Groundwater I SELECT WET CHEMISTRY ** 06/23/06 06/06 - 07/06 ** Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand ; Chloride; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable ; Sulfate ; Total Dissolved Solids ; Total Organic Carbon ; IH214 "Us, 1 N C. 11. SDG NARRATIVES For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 6/23/06 SDG#: TSL006 EQPT MW -5D MW -11) MW -5S MW -1S MW -61) MW -31) MW -6S MW -3S MS/MSD MW -8D MW -41) MW -8S MW -4S Thirteen water samples were received by H2M Labs, Inc. on 6/23/06 for select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument. Sample MW -3S was utilized for QC analysis and reporting. ICP serial analysis did not reproduce within acceptance ranges for iron. Iron data was reported flagged "E" on Forms 1 and 9. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: June 30, 2006 Vincent Stancampiano Vice President O O F-+ U2A ISC. For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLE RECEIVED: 6/23/06 SDG#: TSL006 EQPT MW -5D MW -1D MW -5S MW -1S MW -6D MW -3D MW -6S MW -3S MS/MSD MW -8D MW -413 MW -8S MW -4S EPA 325.2 Thirteen water samples'were received by H2M Labs; Inc. on 6/23/06 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: Alkalinity EPA 310.1 Nitrate EPA 353.2 BOD EPA 405.1 Phenols EPA420.1 Bromide EPA 320.1 Sulfate EPA 9038 Chloride EPA 325.2 TDS EPA 160.1 COD EPA 410.4 TKN EPA 351.2 Hardness EPA 130.2 TOC EPA 9060 Ammonia EPA 350.1 Sample MW -3S was utilized for QC analysis and reporting. Ammonia sample value -for MW -8S (0.38 mg/L) was greater than the total kjeldahl nitrogen value (0.18 mg/L). The values slightly exceeded ± the CRDL of 0.1 mg/L. Duplicate TKN analysis did not reproduce within ± the CRDL of 0.1 mg/L (when value is less than five times the CRDL). Biochemical oxygen demand (BOD) analysis of sample MW -4D did not fall within the analytical dilution range (> 66 mg/L BOD). The reported BOD value of 182mg/L was estimated from the chemical oxygen demand (COD) analysis. No other problems were noted during the analysis of tlus sample group. I certify that this data package is in compliance with the terms and conditions of .the contract; both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: July 14, 2006 Vincent Stancampiano Vice President 00 O O 2A CUs, l%Co III. CHAIN OF CUSTODY DOCUMENTATION 1-1�..1 1135 INC. AC7q 0-f ldniinui 1714 Mnivilin 1UY 117A7.A07R 1537'', EXTERNAL CHAIN OF CUSTODY Tel: (516) 694-3040 Fax: (596) 420.8436 CLIENT:. H2M SDG NO: TS LCOG PROJECT'NAME/NUMBERNOTES: / 0l u V OP 150OR I Q 3 Ra N alp v a a o E o {v as -,i Project Contact: BR C - F C L s -71 Phone Number. 1`a -t ; L C2) GO Dl NH3 / NO -6 / PHSWLS TPN SAMPLERS: (signature)/Client DELIVERABLES: /� c 6 J —7 0 o � Z =° o U F - ANALYSIS REQUESTED TURNAROUND TIME: 5 ORGANIC INORG. DATE TIME MATRIXFIELD I.D. ,c IL "� Z m m u ° a I �/ �) W 2 Z U LAB I.D. NO. REMARKS: e 23'00 12,0-0 Ir !M W' I S 0 l 00--;� 1136 1 r z a$3 0 W- 13 `j S M S SMS D 0 00 - I 11-2. { � C� `I30 M UV - (0S 3 . I I a /0--01 Iry _60 b 7 1/00 - 8 S I I 1-613 103 0 .M 3 I I -- Z Relinquis b : (Si re jJ,f� Date 23 4(p Time l3'. SS Received b : (Signature) Date b -Y5 Time 13',68 LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record?Y or N Explain: Samples were: • Shipped_ or Hand Delivered_Airbill# 2. Ambient or chilled 3. Received in good condition: Y or N 4. Properly preserved: Y or N 5. Samples resumed to lab _ Hrs from collection. COC Tape was: 1. Present on outer package: Y or N 2. Unbroken on outer package: Y or N 3. COC record present & complete upon sample receipt: YorN elinquish by: (Signature) D e Time Recei ed by: (Signature) Date Time Relinquished b : (Signature) q y ( g ) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by: (Signature) Dale Time V�'b W06FAUbRIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY A. U kv _ INC 187 - EXTERNAL CHAIN OF CUSTODY 5i3 areaa rlcifay.- mg, rnreya 6V' IT S a ....-....... Tel: (631) 694-3040 Fax. (631) 420-8436 PROJECT NAME/NUMBER ,SO.r-D & O, N �" � r �t�J p� -FOWN (d !" cSOU I V 1 O li D ! �(o Rd �N1C �00LJ a CLIENT: a N a p (� �` 1 _ H2M SDG NO: S L NOTES: Protect Contact 80D5( B� G L ) .So v Phone Number: n `�� Tll'1�') MS �a 1 PIS/Quote # a) COO i 013� SAMPLERS: (signature)/Client M DELIVERABLES: 05-70 J 70 o g Z c U° ANA1. YSIS REQUESTED ORGANIC INORG. . TURNAROUND TIME: -- T fl l 1 Z LAB I.D. NO. REMARKS: DATE TIME MATRIXFIELD I.D. 2 t/. pqoQ. y M W -41) MW -51)- 3. f -c)o o 8930 /030 E4 P 1/00 Relioqui try: (Skina Date I,+ 3k Time 13:5$ Received by, (s Date b123 Date Time 13', SS Time LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y of N Explain: samples were: t. SNpped_orHand Deinrered_AirbW 2. Ambient or cN1ed, Temp 3. Received in good condition: Y or N <. Property preserved: Y or N COC Tape was: 1. Present on outer package: Y or N 2. Unb mken on outer package: Y or N 3. COC record present & corroate upon sample receipt: YorN Reltnqulshee by-. (Signature) a Time Received by: (signature) Rellnquished by: (Signature) Date Time Received by-. (Signature) Date Time Relinquished by (Signature) Date Time Received by. (signature) Date Time LTA( �Yl ORIGINAL YELLOW COPY - CLIENT PINK CUPY - LAbUtIA I UNT H2M LABS, INC. Client Name PCTSL Work Order Numbe 0606916 Sample Receipt Checklist Date and Time Receive Received by PS _TJL_0Cb 6/23/2006 1:58:00 PM Checklist completed b(,p 2 � Reviewed by Y G Signature Date � Initials Date Matrix Carrier name Hand Delivered Shipping container/cooler in good condition? Yes No ❑ Not Applicable ❑ Custody -seals intact on shippping container/cooler? Yes ❑ No ❑ Not Applicable ❑�/ Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable Chain of custody. present? Yes No ❑ Chain of custody signed when relinquished.and received? Yes No ❑ Chain of custody agrees with sample labels? Yes No ❑ Samples in proper container/bottle? Yes EVI No ❑ Sample containers intact? Yes 91 No ❑ Sufficient sample volume for indicated test? Yes 0 No ❑ All samples received within holding time? Yes W No ❑ Container/Temp Blank temperature in compliance? Yes W No ❑ Water - VOA vials have zero headspace? No VOA vials submitted ❑ Yes 66 No ❑ Water - pH acceptable upon receipt? Yes M No ❑ Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section b ----------------------------------------------- ---------------------------------------------- Client contacted Contacted by: Comments: Corrective Action Date contacted: Regarding Person contacted tj2A UA", INC. INTERNAL CHAIN OF CUSTODY CLIENT: 'FC -TS L DELIVERABLES: BS -10 p TURNAROUND TINE. 21 T:>� MATRIX: GfooMVdjy pH CHECK&., N SDG 9: CASE 9: REMARKS:— pis #('CU Kl-SL 0-5 RECEIVED BY: PS—SIGNAIWRE.iDATE: q23[o-TME--J3 CLIENT ID MM LAB N DATE: COLLECTED BOTTLE TYPE N OF BOTTLESI TESTS S �TE D REQUESTED ESQ691 p CE0- 6 G12,0 EN raoio-w-p ci LseQ MW -ID -00 E 3 3D S mst fAS D -owe 3 p 00GE 5D • E E: N 6=23.0 11 -011 E: 11 8 D -o12E RAE 612W(A 17 L METALS P 0232 INC* CLIENT: 1 SDG LOO INTERNAL CHAIN OF CUSTODY - SAMPLEPURPOSE RELINQUISHED DATE TIME BY SAMPLE RECEIVED BY sI Slow BOTTLE TYPE tv E - SIV OF CHANGE OF CUSTODY I s' T4s INIT 23 15,y 9I I slow SIG" slow allow slow SION . ._. Ilion 9ION . sIMF slaw SIGN SIGN f ;;low slow Slaw, SIGN . slow s=cm Slum SIGN SIGN GN 310a Illy SIGN 97— 31019 CN SIoa slum SION SION - SION SIGN - 31019 slam sI07i - SIGN . ON. SIGN _ g1Ga slam SION SIam Slow - SIGN S SION SIGN - P 0233 t12A UA -US, INC* INTERNAL CHAIN OF CUSTODY CLIENT: FCTq L DELIVERABLES: 6-10D -TURN AROUND TIME: -21 T)oj�r- sDG -9: . TS CASE #: MATRIX: pH CHECK(Dor REMARKS: -PIs--w M-2–,pCTRL M RECEIVED BY: SIGNATURE:�DATE-*,4MTUiE--j_3_:5e) WET CHEMISTRY P 0283 Elmo P, WA= OMNI E90710TIM mmuffimmm No ffis 0 m— m m ■ m mmommm MOM I wo WET CHEMISTRY P 0283 IH2A UAU%�� INC, CLIENT: L OO(P INTERNAI, CHAIN.OF C-USTODY WET CHEMISTRY VV- - e11. DO N ETA UA".., INC, --ENT: SDG INTERNAL CHAIN OF.CUSTODY DATE TIME 'SAMPLE RELINQUISHED BY SAMPLE RECE 13Y ECE BOTTLE TYPE- PURPOSE OF CHANGE OF CUSTODY INIT tN� Blow al sic" slow slow Blow SION SION gIOli glOy Blow 9I Ow SION SION SIGH SIGH SIGN SICK SIGN 31 GH SIC" ION SION SIGN SIGH .3108 SIGN slow SI 14 Slow SION 310H SIGH 310H SIGH 310" SION ------------ SIGH 310M 31 310H sI.G)T ON SIG SIGH SIGH WET CHEMISTRY P 0285 r2A ILAUS, INC. IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY H2M lAI3S, INC. TSLOQ& METALS TABLE OF CONTENTS 1. REPORTS II. QC SUMMARY Ill. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSLO06 SOW No.: ILM04.1 EPA Sample No. EQPT MW -1D MW -1S MW -3D MW -3S MW -4D MW -4S MW -5D MW -5S MW- 6 D MW -6S MW -8D MW -8S Were ICP interelement corrections applied? Were ICP background corrections applied? If yes -were raw data generated before application of background corrections? Comments: DATE REPORTED: JUNE 29, 2006 Lab Sample ID. 0606916-001 0606916-OO5DUP 0606916-OO5MS 0606916-006 0606916-007 0606916-008 0606916-009 0606916-010 0606916-011 0606916-012 0606916-013 Yes/No YES Yes/No YES Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and in the computer -readable data submitted on diskette has been authorized by the Laboratory Manager or the Manager's designee, as verified by the following signature Signature: _ Name: Vincent Stancampiano Date: Title: Vice President COVER PAGE - IN ILMO4.1 u2M "U%S INC. REPORTS FOR METALS U2M "USs INC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 11.5%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than. the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO 7440-43-9 INORGANIC ANALYSIS DATA SHEET 7440-70-2 122 BI P j EQPT Lab Name: H2M LABS, INC. Contract: j _ 1.91 U Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-001 Level (low/med): LOW Date Received: 6/23/2006 % Solids: 0.0 163 B I P Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte ConcentrationtC� Q M 7440-43-9 !Cadmium 0.67 B P 7440-70-2 122 BI P 7439-89-6 .Calcium (Iron L 4 5. 31 BI E P 7439-92-1 (Lead _ 1.91 U P 7439-95-4 Magnesium —10.3[B ;_P .7439-96-5 (Manganese 0. 63; U P 17440-09-7 Potassium _ _ 41.2 B P 7440-23-5 ;Sodium -- -L— 163 B I P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.34'U P 7440-70-2 Calcium I MW -1D Lab Name: H2M LABS, INC. Contract: 1 ; 204 Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-002 Level (low/med): LOW Date Received: 6/23/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration I CI Q r M 7440-43-9 Cadmium 0.34'U P 7440-70-2 Calcium 1210 B'I P 7439-89-6 Iron ; 204 E P 7439-92-1 Lead 1.9 U i P 7439-95-4 IMagnesium 231 B� P 7439-96-5 IManganese 2.8 B, P 7440-09-7 Potassium 3551 B1 P I 7440-23-5 Sodium 179001 1 P Color Before:_ COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP Level ( ow me . % Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L �No. �_CAS � 744 0-43-9 Analyte Cadmium 1 EPA SAMPLE NO 7440-70-2 INORGANIC ANALYSIS DATA SHEET B P —� Iron 188 E P j 939-92ead 7 -1 MW -1S F7Lab Lab Name: H2M LABS, INC. Contract: (Magnesium J- — 215 B P Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-003 1 / AN LOW Date Received: 6/23/2006 Level ( ow me . % Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L �No. �_CAS � 744 0-43-9 Analyte Cadmium Concentration 0.34 Cj Q M U P 7440-70-2 Calcium 1090 B P 7439-89-6 Iron 188 E P j 939-92ead 7 -1 L 1..9 U 7439-95-4 (Magnesium J- — 215 B P 7439-96-5 IManganese 2.5,B! P 17440-09-7 jPotassium 352 B P X7940-23-5 Sodium 17300 Color Before: COLORLESS_ Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 INO CD O. V1 H U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -3D Lab Name: H2M LABS,, INC. Contract: Lab Code: 10478 Case No. SAS No.:, SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-009 Level (low/med): LOW Date Received: 6/23/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte ( Concentration I CQ j M 7440-43-9 ICadmium 0.34'U I P i 7440-70-2 Calcium 1020 B P 7439-89-6 lIron 185 ( E P j X7439-92-1 ILead 1.9 U P 7439 95 4 IMagnesium 227,B i P 793r 9-96-5 Manganese 11.8 B I P j7440-09-7 jPotas3ium 1190 B P '774440-23-5 Sodium 20200 P Color Before: COLORLESS_ Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 00 O CD 0n H U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.': Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No�Analyte Concentration,C Q j M 7440-43-9 Cadmium_ 0.341U I P 7440-70-2 Calcium 9591 B1 P 7439-89-6 Iron 2021 1 E P 77439-92-1 Lead ; 1. 9' U ; P ,7439-95-4 (Magnesium 2131 B P 17439-96-5 F7 -40-09-7 1Manganese 1Potassium 2.Oi B i PP — 3191 B P I 7440-23-5 jSodium 16200 _P EPA SAMPLE NO MW -3S SDG No.: TSL006 0606916-005 6/23/2006 Color Before:_ COLORLESS Clarity Before: CLEAR _ Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO (Cadmium INORGANIC ANALYSIS DATA SHEET (Calcium _1: 11501 BI _--- I�, P--� j7439-89-6 T� tIron j MW -4D i Lab Name: H2M LABS, INC. Contract: i Magnesium- Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-006 Level (low/med): LOW Date Received: 6/23/2006 o Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M I !7440-43-9 (Cadmium 0.341 U I P 17440--70-2 (Calcium _1: 11501 BI _--- I�, P--� j7439-89-6 T� tIron { 208 jTE I r l X7439-92-1 1Lead 1.9( U ; P 7439-95-9 Magnesium- 3231 B ; P 7439-96-5 jManganese j 38.7j_I i P X7440-09-7 jPotassium 3620 ! P 17440-23-5 jSodium 1 24900! j P j - -_� 0_-_ j _1 Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 29, 2006 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -4S Lab Name: H2M LABS, INC. Contract: � Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-007 Level (low/med): LOW Date Received: 6/23/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L fCAS No. 17440-43-9 I Analyte Concentration CI— Q M Cadmium 0.341P P } 7440-70-2 ;Calcium 9431 B —� P 7439-89-6 Iron 2001 E P 7439-92-1 iLead1.9 U� P 17439-95-4 Magnesium 211 B } P 7439-96-5 iManganese 2.11 B 11 j P ;7490-09-7 Potassium 295 B, 7440-23-5 Sodium _ 15900 ! P Color Before: COLORLESS Clarity Before: CLEAR Texture: — Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 r" O O H U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. I Analyte I Concentration CI 4 I 1 EPA SAMPLE NO 0.34 U� ! INORGANIC ANALYSIS DATA SHEET 1060 B, _ ! 185 E P P Ii 7439-92-1'Lead 7439-95-4 IMagnesium 1.9 U� 1 234 BI P P 7439-96-5 1manganese MW -5D Lab Name: H2M LABS, INC. Contract: �744r-0-23-5 !Sodium — r 175001 P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-008 Level (low/med): LOW Date Received: 6/23/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. I Analyte I Concentration CI 4 I M 7440-43-9 Cadmium_ 0.34 U� ! P X7440 70-2 Calcium --� 7939-89-6 Iron 1060 B, _ ! 185 E P P Ii 7439-92-1'Lead 7439-95-4 IMagnesium 1.9 U� 1 234 BI P P 7439-96-5 1manganese 1 11.0[ 7440-D9-7 Potassium 11101 B I �744r-0-23-5 !Sodium — r 175001 P f 1 I Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 29, 2006 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. -744 0-43-9 {Cadmium Analyte 1 EPA SAMPLE NO 17440-70-2 INORGANIC ANALYSIS DATA SHEET { P { 7439-89-6 Iron 216 E P 7439-92-1 MW -5s Lab Name: H2M LABS, INC. Contract: Magnesium —� Manganese 226 B 2.2 B _ ` P� PP 17440-09-7 Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-009 Level (low/med): LOW Date Received: 6/23/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. -744 0-43-9 {Cadmium Analyte Concentration�C� 0.34 U Q 1 M FP 17440-70-2 Calcium 1090 B { P { 7439-89-6 Iron 216 E P 7439-92-1 lLLead 1.9 U -('-P 1 17 4 3 9-95-4—i ;7439-96-5 Magnesium —� Manganese 226 B 2.2 B _ ` P� PP 17440-09-7 ,Potassium 332 Bj P { diem 16800 { P ,7440-23-5 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: s Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L jCAS No. 17440-43-9 Analyte (Concentration CE Q i M ICadmium 0.34 Uj P ; 7440-70-2 lCalcium 1080 B P 7439-89-6 lIron 243 It E P 7439-92-1 Lead 1.9 U P 7439-95-4 (Magnesium 232 B P 7439-96-5 Manganese 2.7-B P 7440-09-7 11 otassium 377 B P ;7490-23-5 Sodium i 17500�P� Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: DATE REPORTED: JUNE 29, 2006 EPA SAMPLE NO MW -6D SDG No.: TSL006 Texture: Artifacts: FORM I - IN ILM04.1 r-1 O O CA H U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO 7440-43-9 INORGANIC ANALYSIS DATA SHEET P X7440-70---2-ICr alcium- 11001 B i P 7439-89-6 MW -6S Lab Name: H2M LABS, INC. Contract: ,Lead 1--1.9 _P U P� 7439-95-4 Lab Code: 10478 Case No. SAS N*o.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-011 Level (low/med): LOW Date Received: 6/23/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration CI Q 1 M 1 i 7440-43-9 Cadmium 0.341U P X7440-70---2-ICr alcium- 11001 B i P 7439-89-6 Iron l 208 E ; 743f- 9-92-1 ,Lead 1--1.9 _P U P� 7439-95-4 jMagnesium T _— 221 B P_ T439-9-6-5 794; 0 -7 Manganese Potassium 2.4 370 B) P B P 1-7-4-4023-5 Isodium 17600 P I _ Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET I MW -8D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-012 Level (low/med): LOW Date Received: 6/23/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L ICAS No. Analyte Concentration I C Q i M I 7440-43-9 ICadmium 0.34 U 1 P ' 7440-70-2 lCalcium 1370 BJ j P 7439-89-6 Iron 207 1 E_ P 7439-92-1 Lead 1.91 UI — P 7439-95-4 Magnesium 303 --i P ' 7439-96-5 ,Manganese 26.3 P 7440-09-7 Potassium 2660 B P 7440-23-5 Sodium 230001 P �) Color Before: COLORLESS Clarity Before: Color After: COLORLESS Clarity After: CLEAR Texture: CLEAR Artifacts: Comments: DATE REPORTED: JUNE 29, 2006 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M I 7440-43-9+admium 1 EPA SAMPLE NO P INORGANIC ANALYSIS DATA SHEET 13101 B - I 7439-89-6 ,Iron { 2071 E P MW -8S Lab Name: H2M LABS, INC. Contract: 17439 -96 -:Manganese j 2.7 B, Lab Code: 10478 Case No. SAS No:: SDG No.: TSL006 Matrix (soil/water): WATER Lab Sample ID: 0606916-013 T---' (low/med)• LOW Date Received: 6/23/2006 % Solids: 0_0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M I 7440-43-9+admium _ 0.341U P (7440-70-2 (Calcium 13101 B P ; 7439-89-6 ,Iron { 2071 E P 7439-92-1 7439-95-4 {Lead {Magnesium 1. 91 U _ 244 B P P 17439 -96 -:Manganese j 2.7 B, i P ' 7440-09-7 jPota3,9iUM { 5,111B P M j7440-23-5 !Sodium 169 P LI Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: DATE REPORTED: JUNE 29, 2006 Texture: Artifacts: FORM I - IN ILM04.1 O O H U2M "USS INC. II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.. SAS No.: SDG No.: TSL006 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity . Concentration Units: ug/L 1 Analyte Initial Calibration ; True Found %R(l) True Continuing Calibration Found %R(1) Found T , %R(l) I MI Cadmium Calcium 2500.0 1 2535 150000.0 .5,5 52933.43 101.4 105.9 2500.0 150000.01 2556.66 53208.80 102.3 106.4 2595.40 52105.74 101.8 104.2 P��' P I Iron 150000.01 51830.86 103.7 150000.0' 52243.94 i 104.5 52190.97 j 104.4 P Lead 1 500.0 503.61 100.7 1 500.0 1 505.75 101.2 491.58 98.3 P Magnesium 150000.0 50729.35 101.5_ 50000.01 51035.21 102.1 50362.09 100.7 P Manganese 2500.0 1 2556.07 � 102.2 2500.0 2568.65 102.7 2540.92 101.6 � P Potassium jSod1 ium 80000.01 60000.01 79021.73 77996.34 98.8 97.5 80000.0 80000.01 78556.74 78053.39 98.2 1 97.6 77209.86 1 76974.75 96.5 I 9_6.22 P I (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 CN • O O FORM II (Part 1) - IN ILM04.1 i/1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O O FORM II (Part 1) - IN ILM04.1 Initial Calibration Continuing Calibration Analyte i True Found %R(1) True Found %R(1) Found %R(l)LM Cadmium 2500.0 2582.05 103.3 2550.87 102.0¢ Calcium - i 50000.01 52703.33 105.4 1 52362.23 104.1 I P P Iron �- j 50000.0, 52988.84 106.0 52377.25 104.8 Lead j 1 500.0 1 497.89 _99.6 492.3098.5 P Magnesium Mang ( --- 50000.0 2500.0 51193.29 2577.82 102.4 E 103.1 1 50697.58 i,2550.26 101.4 102.0 j P j P ; anese Potassium I _ 1 � 80000.01 78601.79 98.3 ; 77753.50 Sodium 180000..0 78494.85 98.1 77192.77 96.5 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O O FORM II (Part 1) - IN ILM04.1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration ? True Found %R(1) True i i Continuing Calibration j Found %R(1) Found %R(1) M Iron j 2500.0 2425.76 i 97.0 2500.0 2429.42 97.2 2416.61 96.7 P Sodium (2500.0 2473.60 98.9 2500.0 2465.04 98.6 i 2474.34 _99.0 _ P j i (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N O O FORM II (Part 1) - IN ILM04.1 V1 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N O O FORM II (Part 1) - IN ILM04.1 H Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) i M' —_ - Iron 2500.0 2411.31 96.5 2492.69 99.7 P 2500.0 1 2440.67 97.6 2429.38 97.2 ( P Sodium j — i (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N O O FORM II (Part 1) - IN ILM04.1 H U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AA CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purity Concentration Units: ug/L SDG No.: TSL006 FORM II (Part 2) - IN ILM04.1 I CRDL Standard for AA CRDL Standard for ICP ! i Initial Final Analyte , True Found %R True Found %R Found %E2 Cadmium _~� + 10.0'__ 10.391 103.91. 11.091 110.9 ;Lead i 6.0 6.391 106.5— 4.59 76.5 Man a_n_ese ! 30.01 29.421 98.11 31.071 103.6 FORM II (Part 2) - IN ILM04.1 U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg).: UG/L FORM III - IN N O O ILM04.1 Initial Calib. Continuing Calibration i! Prepa- I Blank i Blank (ug/L) I ration 3 C- Blank Ci M Analyte (ug/L) Ci 1 C 2 C ICadrriium 0.3 0 1 0.3 JUI 0.31 U 1 0.3 JU 0. 34 41 U Calcium J�_ 12.5; U T 12.5 U 12.5 U 12.5 JU I 16.6001B P j Iron 3.7i U i 3.7 U 3.7 U 3.7 U j 3.668 U f P Lead 1. 9i U 1 1. 9 U 1. 91 U 1.9 U I' 1. 904 U I P Magnesium 9.7 U' 9.7 ul 9.71 U 9.7 U 9.702 U, P Manganese_ 0.6 U 0.6 j U1 0.6 U1 0. 6 U _ -0.6281U! P i Potassium 15.9 U( 19.9 25.0 B 22.8 l a i l 18.100 B P Sodium 57.1! B i �Bj 44.2 B 48.1 B 52.4 IB I 114.0001B P j FORM III - IN N O O ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Preparation Blank Matrix (soil/water) U.S. EPA - CLP 3 BLANKS Contract: SAS No.: WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL006 FORM III - IN ILM04.1 Initial j Calib. Continuing Calibration I prepa- Blank i Blank (ug/L) i ration ( j Analyte. (ug/L) C1 1 C 2 C 3 C i Blank C MI Cadmium i I 0.3 I U j j P (Calcium j 12.5 U f j P Iron j 3.7 U (Lead �— 1.9 U I � � i I P `Magnesium —�-- j 997 U I ; Manganese 0.6 U — _I r i Potassium J 15.9 , U I P I Sodium j w j 30.9' B f P --- J i FORM III - IN ILM04.1 U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: ICP ID Number: TJA61EDV ICS Source: SDG No.: TSL006 MV Labs/High Purity Concentration Units: ug/L ' 1 Analyte i True Sol. Sol. i A AB Initial Found Sol. Sol. i A AB Final Found Sol. Sol. %R A AB %R (Aluminum i 500000 500000 _ 535893 536588.01 107.31 538086 i 543671.21 108.71 _ I 1000 957.2 95.7 ; 1016.1 101.6 FCadmi�'um Calcium i, 500000 500000 521322 515205.31 103.0 529016 534582.01- 106.9 Iron j 200000 i 200000 �_ 204295 202530.8 101.3. 212085 213627.3 106.8 Lead 1000 961.6 96.2; 985.1 98.5 Magnesium Manganese 1 500000 500000 500 521545 516786.6 519.5 103.41 103 533769 538313.1 538.2 107.7 107.6; N O O Un H FORM IV - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO F-7MW-3SS SDG No.: TSL006 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Comments: FORM V (Part 1) - IN ILM04.1 II j ! Control I Limit Spiked Sample Sample Spike I %R IQ M Analyte %R Result (SSR) C Result (SR) C Added (SA) (Cadmium T 75-125 51.41001 0.3439 U 50.00 102.8 P' Iron 75-125 1184.8900 201.7600 1000.00 98.3, P Lead _ i 75-125 75-125 L 20.1631 516.8900 1.9043 1.9700 Ul 20.001 R1 500.00 100.8 P 103.0 P Man anese _ Comments: FORM V (Part 1) - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES MW -3S Contract: L i SAS No.: SDG No.: TSL006 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Control Analyte ' Limit Sample (S) I C i Duplicate (D) CE RPD ! QIM Cadmium 0.3439 U 0.34391U, P Calcium 5000.000011 959.1800 B 1023.4900 B 6.5 P Iron {100.00001i201.7600, _' 215.7900 I 6.7 P (Lead 1.9043 U 1.90431 U i P ; �nesium Manganese �' 5001 0.0000_1 ! 1 005 00 213.4700 B 1.9700 B 227.06001B 2.19001B _T ; j 6.2 10. 61 PI 1PI Potassium 15000. 00001 _ _ 1 318.8500 B I 325.20001B 2.0 P (Sodium ;5000.0000 16244.7300 , 16830.97001 3.51_ I P FORM VI - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSL006 I Aqueous (ug/L) Solid (mg/kg) ! Analyte ; True Found %R True Found C Limits %R Cadmium !_ 2500.0 2501. 221 100.01 Calcium ! _ 50000.0 _ 523 69 40104.81 Iron_ _ ; 50000.01 51825.671 103.7' _ Lead i_ 500.01 494.901 99.01 Ma nesium 50000.0 50290.8211 100.61 Manganese 1 2500-01 2543.11 101.7' Potassium 80000.01 77203.32( _i Sodium i 80000.01 77706.43 97.1 FORM VII - IN Lab Name: H2M LABS, INC. Lab Code: 10478 Case No U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No.: Concentration Units: ug/L SDG No.: TSL006 EPA Sample IAJO ADD 1 ADD I 2 ADD ( 3 ADD Final No. ABS CON ABS I CON ABS ! CON ABS Conc. f r (Q FORM VIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Contract: .SAS No.: Concentration Units: ug/L MW -3S ' SDG No. TSL006 Level (low/med): LOW FORM IX - IN ILM04.1 Serial i i % II Initial SampleDilution Differ- f {Analyte Result (I) C Result (S) C ence I Q M 1 Cadmium ( 0.34{ U 1.70 U i P Calcium 959.18 B { 1008.85 BI 1 5.2 �l P Iron (-{ 201.76 I 176. 05 B! 12.7 1E P Lead { 1.90 9.50 U ' I P Ma nesium ( 213.47 B 1 i 208.85 B 2.21 { P ManC anew 1. 97; B j I 3.10 U 100.0' --- P Potassium 318.8 B5 ( 315.45] B! 1.1 P Sodium 16244.731 —__17045.90B 4.9 _� P FORM IX - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: TJA61EDV Flame AA ID Number: Furnace AA ID Number: Comments: Contract: SAS No.: Date: 3/27/2006 SDG No.: TSL006 (Analyte Wave- length Back- (nm) groundi CRDL (ug/L) ' IDL (ug/L) M (Cadmium 226.501 5.0; 0.31P Calcium 317.9315000. 011 12.51 P Iron 1 259.941 1 100.01 3.71 P Lead , 220.351 1 3.01 1.91 P Magnesium :Man anese 1 279.081 1 257.611 5000.0 15.01 9.7 0. 61 P P Potassium 1 766.491 1 5000.01 15.91 P Sodium 588.99 5000.0[_. 91 P FORM X - IN - ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) I i Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL006 ICP ID Number: TJA61EDV Date: 04/13/2006 j Analyte 1 Wave- length (nm) �� 1 Interelement Al Ca Correction Factors for: Fe Mg i Ij( Co f jAluminum i Antimony j 308.22i1 6.83�j 0.0000000; 0.000000011 0.0000000 0.0000000 0.0000000 0.0000000 0.00000001 0.0000000 0.0000000 1 0.0000000Arsenic 1 9.0411 H 0.0000000( 0.0000000 -0.1120000 0.0000000 0.0000000 Barium i 3.41;,7-1---0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 i Per lli-UM 1 313.04;1 0.00000001 0.0000000) 0.00000001 0.0000000 0.0000000 Boron_ 1 249.6811 0.0000000' 0.0000000 0.00000001 0.0002000 Cadmium j 226.501 1 0.0000050 0.0000000 _-0.00004001 0.00007201 0.0000000 0.0000000 Calcium 317.93 1 0.00000001 0.0000000 0.0000.0001 0.00000001 0.0000000 Chromium ; 267.62T 0.0000000 0.00000001 0.00000000.0000000 0.0000000 Cobalt 1 228.62 1 0.00000001 0.00000001 0.0000noo 0.0000000 0.0000000 ' CpRer_ ! 324.75 0.000000011 0.00000001 0.00002H1 0.0000000 0.0000000 Iron 259.941 0.00000001 0.0000000 0.0000000 0.0000000 0. 0 0000 00 Iron ? 271.4411; 0.0000000 0.0000000 0.0000000 0.0000000 _ Lead220.35: (Lead 1 220.35' _0.00000001 _-0.10700001 0.12000001 0.0000000 0.0000000 0.0319000 0.0000000 0.0000000 0 .0518000 0.0000000( 0.0000000 Ma nesium I 279.0811 Manganese 2_57.6111 0.00000001 0.00000001 0.000 0001 0.00000001 0.0000000 0.00000001 0.00000001 0.00000001 0.0000000 0.0000000 Molbdenuml 202.03--'11 0.0000000, 0.0000000 0.0000000 0.0000000 _ 0,0000000 j Nickel i 231.6011 0.0000000` 00000000 0.0000400 0.0000000 0.0000000 Potassium 766.49 0.0000000 0..000000011 0.0000000 0.00000001 0.0000000 . Selenium i 196.03 1 0.00000001 0.0000000 -0.4140000 0.0000000 -1.2940000 Selenium I 196.0311 0.00000001 0.0000000 0.0470000 0.00000001 0.4000000 ' Silicon con 288.16 0.00000001 0.0000000 0.0000000 0.00000001- 0.0000000 Silver 328.071 1 0.00000001 0.00000001 -0.01040001 0.00000001 0.0000000 Sodium 1 330.231 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 89.00; Strontium 407.7_71_ 0.00000001 0.00000001 _ 0.000000010.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Thallium ! 190.86] 0.00000001 0.00000001 -0.4940.0001 0.0000000 0.4310000 Tin � 189.99'1 0.00002081 0.00000001 0.0000000: 0.00000001 0.0000000 - Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL006 ICP ID Number: TJA61EDV Date: 04/13/2006 Comments: FORM XI (PART 1) - IN ILM04.1 Wave- Interelement Correction Factors for: 1 length Analyte (nm) II Al Ca Fe Mg Co I I I� Titanium 1.-334. 941 0.00000001 o.0000oo.01 0.00000001 0.0000000 0.0000000 Vanadium 1 292.4011 0.0000000' 0.00000001 0.00000001 0. 00000001 0.0000000 1 Zinc ji 213.86; 0.00000001 0.00000001 0.0001500 0.0000000 0.0000_ 000 iLj Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP I 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL006 ICP ID Number: TJA61EDV Date: 04/13/2006 Wave- �I Interelement Correction Factors for: jlength Analyte (nm) Cr Mn Ni V Aluminum 308.22!! 0.0000000; 0.0000000F 0.0000000 0.0160000 1 Antimony -j--206.831 4.12000001 0.0000000 0.0000000 -2.3400000 Arsenic 11 189.0411 0.0000000! 0.0000000 0.0000000 Barium i 493.4111 1 _0.14120001. 0.00000001 0.0000000, 0.0000000 0.0000000 Beryllium 313.091 0.00000001 0.0000000! 0.0000000 0.0001200 Boron + 249249 68 0.00000001 0.00000001 0.0000000 0.0000000 Cadmium �1226.50j! 0.00000001 0.00000001 0.0000410 0.0000000 Calcium 1 ' 317.931 0.00000001 0.0000000! 0.0000000 0.0000000 Chromium j 267.621 0.00000001 0.00000000 0.0000000 0.0000000! Cobalt 1 228.621 0.00000001 0.0000000 0,.:0000000 0.00000001 Copper 324.75, 0.00000001 0.0000000 0.0000000 0.0000000 Iron 6 259.94 1 0.000000011 0.0000000 0.0000000 0.00028001 Iron j 271.44 1 0.00000001_ 0.0000000 0.0000000 0.0002800 Lead_ I 220.35] 0.00000001 0.13000001 0.0000000 -0.1600000 Lead 1 220.35 i 0.00000001 0.0950000 0.0000000 -0.0800000 Magnesium 279.08;1 0.00000001 0.0000000, 0.0000000 0.00000001 Manganese_ i 257.61!; 00000001 0.00000001 0.0000000 0.000000011 Mol bdenum 202.0310.0000000; 0.00000001 0.0000000 0.00000001 Nickel 231.60 1 0.000000011 0.0000000. 0.0000000 0.00000001 Potassium ; 766.49' 0.0000000 0:00000001 0.0000000 0.0000000 Selenium 1 196.0 1 0.0000000 0.3040000 0.0000000 0.2200000 Selenium! 0.0000000! 0.2860000 0.0000000 0.0838000 Silicon ' 288.161 0.0000000; 0.0000000 0.0000000 0.0000000 Silver ! 328.0711 0.0000000 0.0000000 0.0000000! 0.0000000 Sodium i 330 23 j 0.0000000 0 00000001 0. 00.000001 0.0000000 Sodium ! 589.00!1 0.00000001 0.00000001 - 0.00000001 0.0000000 Strontium ! 407.771 0.00000001 0.0000000! 0.00000001 0.0000000 1Thallium190.86' 0.19410001 -0.51300001 0.00000001 -0.29760006 I Tin 189.9911 1 0.00000001 0.0000000 0.00000001 0.0000000 I Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL006 ICP ID Number: TJA61EDV Date: 04/13/2006 Comments: FORM XI (PART 2) - IN ILM04.1 Wave- Interelement Correction Factors for: length Analyte (nm) Cr Mn Ni V Titanium 334 9411 1 0.00000001 0.0000000 0.0000000 0.0000000 Vanadium ( 292.40111 0.0000000; 0.00000001 0.0000000 0.0000000; Zinc 213.86' -0.00120001 0.0000000, -0.0002200 0.0000000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S: EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) I I Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL006 ICP ID Number: TJA61EDV Date: 05/10/2006 Comments: FORM XII - IN ILM04.1 Integ. I Time Concentration Analyte I (Sec.) I (ug/I. M i Iron 15.00 250000P i Man anese_ 15.00 20000 P FORM XII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL006 j EPA Sample No. j I Preparation i DateI Weight (gram) Volume (mL) EQPT 06/26/2006 50 j LCSW 06/26/2006 j 50 j Mw -1D 06/26/2006 50 Mw -is 06/26/2006 50 MW -3D 06/26/2006 50 i MW -3s 06/26/2006 j 50 i Mw-3SD MW-3SS { 06/26/2006 i 06/26/2006 50 j 50 I Mw -4D 06/26/2006 i 50 MW -4S 06/26/2006 -----� 50 I MW -5D , j 06/26/2006 50 MW -5S 06/26/2006 50 MW -6D 06/26/2006 i 50 j MW -6S 50 _ MW -SD _06/26/2006 �— 06/26/2006 _ 50 j MW -8S { 06/26/2006 50 Paw 06/26/2006 i 50 j FORM XIII - IN ILM04.1 y rn MT _ nrx grana - ---�j-�-!XIX +y XX _; X X X X XIX I ; X X i X X i I - I_ I j £ZbT ZTbt ( 00'T- I S9-Mwi OO;T I _ a9-Mwj I ! ! TO'vt j 00'T SS -MW x X X X X IXI ! XI jx'x'x x' ' X.1 X j I- x X 1 TS£T j 00'T aS-Mw X, 1 1X X x1X1XI 1 x'Xj I I I 1 Ob£T 00't ! S6 -MW 1 1' X I X xi X x X { - x X 1 6Z£T 1 00' T i a'v-Mwj � � X' X IX X x IxIX1 1 H' �6T£T 00'Z I X! I I 1x i ; 80£t 00't n03 1 (X I 1X IXIx X L x! 'X!XI ! LSZT; 00'T n00 X I 1 X 1 ! ! X X X' X X X j LbZt 00'5 i ISE_Mwi IXT� x' ! lx x x x { I lxjxl I ! i { 9£ZT I 00'T I SSE -Mw X �1 X _ -! X { X X X j� X 1 X l - SI ZZT S T Z T 00't `1 aSE-Mw, 00-T x ! x X X I -- j X' X1 X X X x _;, X X j I I I 60ZI 00't j GE -mi! I X X Ix X x x I Ix X` ! £STT OUT ST -Mw _I X I X X X 1 XIX IXI x ( xlx x x( j I X X I I xlx i ! i I £bTt 1 Z�tti 00-T at -Mw{ oo't j saa�! 00't MSoII !; I; X X X( X x x I ; X. X ! X �X X' X x X I _ XIX �_ �_ TZTt tTtt� __i 00'1 I Msd! I j X X Ix X i x X{ X X I 1 OOTT OUT i e0�j i -�} l x l i x X --I�� X I j X x X x j X X -�- Xrx- i i X- X-;-�-'i X i X J-_1 II -h- ----� I I x i os 6£ 0 t i_8ZOT l oo't I nDD O 0' t nDD 00' T I HKs�I; _ -- fi X X X { 1 X X' i X"j _ STOT 00'Txx I i 1 X{ I 1 I LOOT j 00't ( IED III---( X( !xl I !X`X X1XI IXi-Xl -I -- j 9S60 I OUT SDI IX' I X. XIX (XIX X'X! ( ! Xjx' I_�-� i— 9660 i S£60 i OUT 1 ADIl 00'T ( ADI! X_ X {� j ( j -' I X 1 1 X. 1 I i X -I_ I -I- i I i T£6::0Q-6-0 8S80 i S£ 8 0! ' T -- S ! 00' T ! SI 0 0' t 1 S ' X 6280 00'I s� s ! X X' I- X --� x x �i it I J -' 1— I x i( 1 EZ80 9T'T 80 -- solo I 00' T_ 00 s os oo't 1 jI ! x x l I X I x x x` i t I -- --_.-- 1 i j !N;N Z K J 3I I J N J S 3n C 2ilKl S�g17 I ! ON IO Z n Z N K SIM N�H�w w d 31O!O 0!Oj�I.els KISIK' 'd o f auiTS' 3/a aTdUIPS Kai 99-4AT2uK 9002/8Z/90 900'ISL : '.ON Jas :ag2a Pu3 d :Pougaw :,ON SKS :4oeaquoO 50'I NnU SIS.C'IKNK bT d'IO - Kd 3 ` S ' n 900Z/8Z/90 :aqua 4a2gS AGaT9Krs :aaqumN GI quaumagsul -ON as?3 8LbOT :aPoO gu'i ONI ' SHK'I wZH : GWPN gez Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA61EDV Start Date: 06/28/2006 U.S. EPA - CtP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL006 06/28/2006 EPA Analytes Sample D/F i No. Time % R AISIAIBIB L B SIA E C DIj CCICIC1F ARIO UIE�B P MIM'H GIN G NIKIS AINIT II E GIA VIZIC L IZ N MW -8D i 1.00 11433 j I i XIX I IX X XIXI i 1 X I 1X I II I I MW -BS 1.00 ( 1444 I I i XIX I_ IX X X(X ,X X t - I zzzzzz 1.00 CCy I 1.00 .1.455 I 1.1505 jJ-I jJI X { X 1—� X _ -X I �X-�{ X— X -� X � H 'CCv 1.00 I 1516 r i I X I i i i_ X CCB _ j 1.00 CRI 1.00 11527 I 1537 I ; I r �— X X X I i --T- X X X X, X X__ I X X ICSA I 1.00 j 1548 i X j { X I X X X X I X II ICSAB i 1.00 11559 XI XiX —jXIX X X ' I CCv _ I 1.00 ccv — 1.00-I i 1609 _ 1620 1 { { �I- X X X X X X I X X:R i X I f j CCB, 1.00 { 1631 i I j IX�X EENx' X X IX I I FORM XIV - IN ILM04.1 U2M "US -9 INC. III. RAW DATA FOR METALS A. ICP DATA 'ZM LA[3S INC* DATE SvNC L$, Zoo4 CLIENT pa lS�- Dol cal 4DS ANALYST �-` • �- RESULT FILE- e,0(-?-'60(oe,0(-?-'60(o TASK- _ NOTES ## SAMPLE NOTES ' ## ' SAMPLE , ' ' 26 ; UGo(oglrf - 0096 ; �� SS 1 27 -OIOL ; f-Aw - Go i. 2 i 281, i 3-� 29 !K -J - i6'30", S 5 i S0 S le ' t , fsw _ y sgZg'oox,10c -ata , t , t 31 q $S-00`14 i , O S S� ►o 6 ; ^`s t 1000f t , 32: 7 i. CC -Q Gcvt-\ ; f 33 i GcvL� 8 q ' 10 ; rv�t3- 1'I L c, ,til 35 cam-; r ' t � t 3H t 1. Gg .a 36 , t .12- C Q P i � 37 1scs�4 F , i-Oo2C o 38 i I C—1 13, t , 14 -.0036 (l - I S 39 I ; M 4.0 1 Gc3�( 15 i t , 16, -Dost t1 t , 17 -0o E , D" 1 i H�5 i 1$i -oos rµ g 43 1 i 0 19i SV. i 20i t , N t S ' cC-\-) 21, 46 ' t t 47 i 22:' i 23 , 0G 1 - O (a cr w • � 48 i t i c r i 4S l�nw-,��tuioc. 49: 5 t , ' 25� -OfRc MW-5So 1.50' p 0044 Standardization Rpt. iod: DVCLPI Standard: StdBLANK Time: 06/28/06 08:05:42 Be Elem Ag Al As1890 Avge -.00003 .0095 -.02087 SDev .00015 .0002 .00258 %RSD 472.66 1.732 12.377 #1 .00010 .0094 -.02329 #2 -.00019 .0095 -.01815 #3 .00000 .0097 -.02116 Elem Cd Co Cr Avge -.0005 -.0002 .0003 SDev .0005 .0001 .0001 %RSD 101.0 68.18 21.50 #1 -.0009 -.0001 .0003 #2 -.0006 -.0003 .0002 #3 ".0000 -.0001 .0002 Elem Mg Mn Mo Avge .0001 .0004 .0001 SDev .0001 .0001 .0007 %RSD 67.50 19.51 446.1 411. .0002 .0005 .0007 -.0009 .0000 .0003 .0003 1 .0001 .0004 -.0006 Elem 2203/1 2203/2 Sb2068 Avge -.00192 .00212 .00346 SDev .00590 .00331 .00064 %RSD 306.66 156.45 18.445 #1 -.00332 .00307 .00342 #2 .00455 .00484 .00411 #3 -.00700 -.00157 .00284 Elem V Zn Avge .0000 .0001 SDev .0001 .0001 %RSD 16850. 32.24 #1 .0000 .0001 #2 -.0001 .0002 #3 .0001 .0001 06/28,/.8:16:14 AM page 1 B Ba Be Ca .0007 .0001 .0006 .0037 .0003 .0001 .0001 .0000 34.82 68.18 8.397 .6509 .0005 .0000 .0007 .0038 .0010 .0001 .0006 .0037 .0007 .0000 .0006 .0037 Cu Fe Fe K .0061 .0007 .0057 .0216 .0004 .0001 .0007 .0007 6.629 9.485 12.44 3.421 .0065 .0006 .0065 .0211 .0058 .0008 .0055 .0224 .0060 .0007 .0052 .0212 Na Na Ni P .0005 .1494 .0026 .0004 .0003 .0081 .0011 .0019 57.79 5.421 41.49 541.3 .0004 .1557 .0038 .0026 .0008 .1403• .0017 -.0009 .0002 .1524 .0023. -.0006 1960/1 1960/2 Sn T11908 -.00278 .00374 .0004 -.00191 .00124 .00108 .0006 .00076 44'.519 28.904 154.9 39.848 -.00421 .00481 -.0000 -.00278 -.00213 .00378 .0012 -.00165 -.00201 .00264 .0001 -.00132 i i Standardization Rpt. 06/28/06 08:22:59 AM page 1 hod: DVCLPI Standard: StdAGPSB Time: 06/28/06 08:16:21 Elern Ag P Sb2068 Avge 1.5164 1.045 2.3296 SDev .0031 .005 .0201 %RSD .20588 .4608 .86246 ##1 1.5151 1.039 2.3075 #2 1.5143 1.048 2.3346 #3 1.5200 1.047 2.3468 Standardization Rpt. 06/28/06 08:28:58 AM page 1 iod: DVCLPI Standard: StdICSEL Run Time: 06/28/06 08:23:07 Elem Al Ca Fe Avge 17.00 19.62 4.763 SDev .04 .01 .002 %RSD .2154 .0381 .0442 #1 16.96 19.62 4.762 #2 17.00 19.61 4.762 #3 17.04 19.63 4.766 Mg 3.522 .002 .0589 3.522 3.519 3.524 page 1 06/28/06 08:35:44 AM Standardization Rpt. hod: DVCLPI Standard: StdFURNC Run Time: 06/28/06 08:29:06 Elem As1890 2203/1 2203/2 1960/1 1960/2 T11908 Avge 2.1219 2.5493 2.2062 .32547 .75434 .64694 SDe-v .0123 .0191 .0137 .00429 1.318.3 .00779 1.0320 .00262 .40528 %RSD .58115 .74833 .62246 #1 2.1351 2.5647 2.2085 .32142 .74959 .64888 #2 2.1106 2.5554 2.2186 .32997 .76332 .64395 #3 2.1201 2.5280 2.1915 .32502 .75011 .64798 page 1 Standardization Rpt. 06/28/06 08:44:03 AM page 1 zod: DVCLPI Standard: StdMULTI Time: 06/28/06 08:35:51 Elem B Ba Be Cd Co Cr Cu Avge 4.669 7.904 17.09 24.25 4.115 3.621 5.220 SDev .006 .016 .07 .10 .025 .008 .014 0-oRSD .1299 .2028 .4064 .4222 .5963 .2256 .2622 #1 4.667 7.922 17.00 24.13 4.088 3.612 5.236 #2 4.676 7.894 17.12 24.31 4.136 3.629 5.212 #3 4.664 7.895 17.13 24.31 4.122 3.623 5.213 Elem Mn Mo Ni Sn V Zn Avge 3.380 4.792 7.368 5.130 2.711 .8128 SDev .007 .024 .031 .025 .004 .0052 %RSD .2008 .5017 .4229 .4923 .1625 .6402 #1 3.373 4.765 7.337 5.102 2.707 .8071 #2 3.386 4.811 7.399 5.151 2.716 .8172 #3 3.382 4.801 7.367 5'.137 2.711 - .8142 Standardization Rpt. :iod: DVCLPI Standard: StdFENAL null Time: 06/28/06 08:44:10 Elern Fe Na Avge .0194 320.8 SDev .0006 2.5 %RSD 3.165 .7865 #1 .0200 322.8 #2 .0191 321.8 #3 .0189 318.0 06/28/06 08:49:1.5 AM page 1 00 O O H Standardization Rpt. nod: DVCLPI Standard: StdFENAL Run Time: 06/28/06 08:58:23 Elem Fe Na Avge 5.493 12.41 SDev .033 .09 %RSD .5960 .7147 #1 5.484 12.37 #2 5.530 12.51 #3 5.466 12.35 06/28/06 09:03:28 AM page 1 Standardization Rpt. 1od: DVCLPI Standard: StdNAKHI xun Time: 06/28/06 09:03:36 Elem K Na Avge .3894 .0295 SDev .0004 .0003 %RSD .1033 .9096 #1 .3891 .0298 #2 .3894 .0293 #3 .3899 .0295 06/28/06 09:07:54 AM page 1 Standardization Report 06/28/06 09:07:54 AM page 1 zod: DVCLPI Slope = Conc(SIR)/IR Element Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGPSB StdBLANK 1318.84 .041546 06/28/06 09:03:36 Al 308:215 StdICSEL StdBLANK 1.47805 .012881 06/28/06 09:03:36 As1890 189.042 StdFURNC StdBLANK 466.676 9.73870 06/28/06 09:03:36 B 249.678 StdMULTI StdBLANK 1.07111 -.000802 06/28/06 09:03:36 Ba 493.409 StdMULTI StdBLANK .632598 -.000051 06/28/06 09:03:36 Be 313.042 StdMULTI StdBLANK .292699 -.000186 06/28/06 09:03:36 Ca 317.933 StdICSEL StdBLANK 1.90400 -.001310 06/28/06 09:03:36 Cd 226.502 StdMULTI StdBLANK .206173 .000098 06/28/06 09:03:36 Co 228.616 StdMULTI StdBLANK 1.21493 .000197 06/28/06 09:03:36 Cr 267.716 StdMULTI StdBLANK 1.38081 -.000384 06/28/06 09:03:36 Cu 324.754 StdMULTI StdBLANK .958904 -.005842 06/28/06 09:03:36 Fe 259.940 StdFENAL StdBLANK .911126 -.005225 06/28/06 09:03:36 Fe 271.441 StdICSEL StdBLANK 20.9972 -.014729 06/28/06 09:03:36 K 766.491 StdNAKHI StdBLANK 249.809 -5.35273 06/28/06 09:03:36 Mg 279.079 StdICSEL StdBLANK 1.29073 -.000032 06/28/06 09:03:36 Mn 257.610 StdMULTI StdBLANK 1.47946 -.000605 06/28/06 09:03:36 Mo 202.030 StdMULTI StdBLANK 1.04334 -.000155 06/28/06 09:03:36 Na 330.232 StdNAKHI StdBLANK 56.1585 -.025223 06/28/06 09:03:36 Na 588.995 StdFENAL StdBLANK .407757 -.060936 06/28/06 09:03:36 Ni 231.604 StdMULTI StdBLANK .678907 -.001768 06/28/06 09:03:36 P 178.287 StdAGPSB StdBLANK 4.78755 -.001707 06/28/06 09:03:36 2203/1 220.351 StdFURNC StdBLANK 391.961 .754392 06/28/06 09:03:36 2203/2 220.352 StdFURNC StdBLANK 453.705 -.959788 06/28/06 09:03:36 ^'-?068 206.838 StdAGPSB StdBLANK 859.779 -2.97341 06/28/06 09:03:36 30/1 196.021 StdFURNC StdBLANK 3046.42 8.47992 06/28/06 09:03:36 196.022 StdFURNC StdBLANK 1332.27 -4.98625 06/28/06 09:03:36 --SO/2 Sn 189.989 StdMULTI StdBLANK .974702 -.000409 06/28/06 09:03:36 T11908 190.864 StdFURNC StdBLANK 1541.19 2.95069 06/28/06 09:03:36 V 292.402 StdMULTI StdBLANK 1.84415 -.000001 06/28/06 09:03:36 Zn 206.200 StdMULTI StdBLANK 6.15240 -.000902 06/28/06 09:03:36 Pb2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Se1960 196.026 NONE NONE 1.00000 .000000 *NOT STANDARDIZED O O H Standardization Readback Report iiod: DVCLPI Element Wavelength Standard Ag 328.068 StdBLANK StdAGPSB Element Wavelength Standard Al 308.215 StdBLANK StdICSEL Element Wavelength Standard As1890 189.042 StdBLANK StdFURNC Element Wavelength Standard B 249.678 StdBLANK StdMULTI Element Wavelength Standard Ba 493.409 StdBLANK StdMULTI �ment Wavelength Standard 313.042 StdBLANK StdMULTI Element Wavelength Standard Ca 317.933 StdBLANK StdICSEL Element Wavelength Standard Cd 226.502 StdBLANK StdMULTI Element Wavelength Standard Co 228.616 StdBLANK StdMULTI Element Wavelength Standard Cr 267.716 StdBLANK StdMULTI Element Wavelength Standard t"I 324.754 StdBLANK StdMULTI 06/28/06 09:07:54 AM Known Concentration .000000 2000.00 Known Signal .026972 25.1414 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000' Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .005809 37.3551 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Signal .009534 17.0012 Measured Concentration -.000000 1000.000 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00060 Measured Signal .003739 19.6199 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration -.0.00000 5.00000 Measured Concentration .000000 5.00000 page 1 Residual Concentration .000000 -.000122 Residual Signal .017438 8.14025 Residual Concentration .000000 .000061 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 -.000600 Residual Signal .002070 17.7352 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 O .000000 H Standardization Readback Report Element Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard Fe 271.441 StdBLANK StdICSEL Element Wavelength Standard K 766.491 StdBLANK StdNAKHI Element Wavelength Standard Mg 279.079 StdBLANK StdICSEL Element Wavelength Standard Mn 257.610 StdBLANK StdMULTI --=_ment Wavelength Standard 202.030 StdBLANK StdMULTI Element Wavelength Standard Na 330.232 StdBLANK StdNAKHI Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTI Element Wavelength Standard P 178.287 StdBLANK StdAGPSB Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNC 06/28/06 09:07:54 AM d Known Measure Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000, .000000 100.000 100.000 Known Measured Signal Signal .033463 .021561 91.9351 .389449 Known Measured Signal Signal .000159 .000148 4.54544 3.52163 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Signal Signal .001282 .000472 1.63314 .029530 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00029 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 page 2 Residual Concentration -.000000 ' .000000 Residual Concentration -.000000 .000000 Residual Signal .011902 91.5456 Residual Signal .000011 1.02382 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Signal .000810 1.60361 Residual Concentration -.000000 .000000 Residual Concentration -.000000 -.000291 Residual Concentration .000000 .000000 M Residual Concentration -.000000 ,-0 .000000 O 0� H Standardization Readback Report 06/28/06 09:07:54 AM --hent Wavelength Standard 2203/2 220.352 StdBLANK StdFURNC Element Wavelength Standard Sb2068 206.838 StdBLANK StdAGPSB Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNC Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNC Element Wavelength' Standard Sn 189.989 StdBLANK StdMULTI 'PI-ment Wavelength Standard .908 190.864 StdBLANK StdFURNC Element Wavelength Standard V 292.402 StdBLANK StdMULTI Element Wavelength Standard Zn 206.200 StdBLANK StdMULTI Element Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration 'Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Signal Signal .000000 .000000 .000000 .000000 Known Measured Signal Signal .000000 .000000 .000000 .000000 page 3 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000061 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Signal .000000 .000000 Residual Signal .000000 .000000 Analysis Report 06/28/06 09:18:33 AM page 1 hod: DVCLPI Sample Name: ICV Operator: CO It Ull Time: 06/28/06 09:08:02 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 991.34 50.91 515.11 2.596 2.502 2.518 51.76 SDev 6.81 .23 10.47 .022 .012 .028 .59 %RS:D .68691 .4593 2.0322 .8309 .4728 1.127 1.134 #1 989.64 50.85 513.44 2.588 2.500 2.501 51.41 #2 985.54 50.72 505.58 2.579 2.492 2.502 51.44 #3 998.83 51.17 526.31 2.620 2.515 2.551 52.44 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm Ppm ppm Ppm Avge 2.477 2.487 2.501 2.551 50.63 C.0000 49.61 SDev .030 .015 .022 .011 .51 .0000 .54 %RSD 1.225 .5932 .8688 .4399 .9990 .0000 1.097 #1 2.457 2.486 2.488 2.554 50..33 C.0000 49.28 ? 2.462 2.473 2.490 2.539 50.35 C.0000 49.31 S 2.512 2.502 2.526 2.561 51.22 C.0000 50.24 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Low LC Pass High 2.750 2.750 2..750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb Avge 2.510 2.565 H2532. 2.446 -.0084 503.84 494.75 SDev .021 .030 7. .025 .0122 7.79 3.34 %RSD .8308 1.163 .2617 1.039 145.4 1.5461 .67514 #1 2.500 2.543 H2526. 2.433 -.0049 501.77 493.03 #2 2.497 2.553 H2530. 2.429 .0017 497.30 492.61 #3 2.534 2.599 H2539. 2.475 -.0220 512.46 498.59 Errors LC Pass NOCHECK LC High LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 997.81 514.29 509.31 2.486 504.82 2.523 2.457 SDev 12.87 14.18 2.69 .036 9.19 .018 .037 %RSD 1.2900 2.7574 .52911 1.468 1.8209 .7189 1.490 #1 984.02 506.94 506.27 2.461 501.14 2.513 2.431 2 999.92 505.28 510.26 2.470 498.04 2.512 2.441 3 1009.5 530.63 511.41 2.528 515.28 2.544 2.499 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 09:18:33 AM page 2 __-gh 1100.0 Low 900.00 Elem Pb2203 Se1960 Units ppb ppb Avge 497.78 510.97 SDev 4.79 6.02 %RSD .96250 1.1775 #1 495.94 506.50 #2 494.17 508.60 #3 503.21 517.81 Errors LC Pass LC Pass High 550.00 550.00 Low 450.00 450.00 550.00 2.750 450.00 2.250 2.750 2.250 Standardization Rpt. hod: DVCLPI Standard: StdNAKHI ..�i Time: 06/28/06 09:31:04 Elem K Na Avge 55.27 1.179 SDev .51 .012 %RSD .9280 1.035 #1 54.89 1.167 #2 55.08 1.178 #3 55.86 1.191 06/28/06 09:35:22 AM page 1 Standardization Report 06/28/06 09:35:22 AM page 1 .hod: DVCLPI Slope = Cond(SIR)/IR Element Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGPSB StdBLANK .1318.84 .041546 06/28/06 09:31:04 Al 308.215 StdICSEL StdBLANK 1.47805 .012881 06/28/06 09:31:04 As1890 189.042 StdFURNC StdBLANK 466.676 9.73870 06/28/06 09:31:04 B 249.678 StdMULTI StdBLANK 1.07111 -.000802 06/28/06 09:31:04 Ba 493.409 StdMULTI StdBLANK .632598 -.000051 06/28/06 09:31:04 Be 313.042 StdMULTI StdBLANK .292699 -.000186 06/28/06 09:31:04 Ca 317.933 StdICSEL StdBLANK 1.90400 -.001310 06/28/06 09:31:04 Cd 226.502 StdMULTI StdBLANK .206173 .000098 06/28/06 09':31:04 Co 228.616 StdMULTI StdBLANK 1.21493 .000197 06/28/06 09:31:04 Cr 267.716 StdMULTI StdBLANK 1.38081 -.000384 06/28/06 09:31:04 Cu 324.754 StdMULTI StdBLANK .958904 -.005842 06/28/06 09:31:04 Fe 259.940 StdFENAL StdBLANK .911126 -.005225 06/28/06 09:31:04 Fe 271.441 StdICSEL StdBLANK 20.9972 -.014729 06/28/06 09:31:04 K 766.491 StdNAKHI StdBLANK 1.66329 -.002400 06/28/06 09:31:04 Mg 279.079 StdICSEL StdBLANK 1.29073 -.000032 06/28/06 09:31:04 Mn 257.610 StdMULTI StdBLANK 1.47946 -.000605 06/28/06 09:31:04 Mo 202.030 StdMULTI StdBLANK 1.04334 -.000155 06/28/06 09:31:04 Na 330.232 StdNAKHI StdBLANK 1.38479 .000629 06/28/06 09:31:04 Na 588.995 StdFENAL StdBLANK 407757 -.060936 06/28/06 09:31:04 Ni 231.604 StdMULTI StdBLANK .678907 -.001768 06/28/06 09:31:04 P 178.287 StdAGPSB StdBLANK 4.78755 -.001707 06/28/06 09:31:04 2203/1 220.351 StdFURNC StdBLANK 391.961 .754392 06/28/06 09:31:04 2203/2 220.352 StdFURNC StdBLANK 453.705 -.959788 06/28/06 06/28/06 09:31:04 09:31:04 ch?068 206.838 StdAGPSB StdBLANK StdBLANK 859.779 3046.42 -2.97341 8.47992 06/28/06 09:31:04 3c)/1 196.021 196.022 StdFURNC StdFURNC StdBLANK 1332.27 -4.98625 06/28/06 09:31:04 -30/2 189.989 StdMULTI StdBLANK .974702 -.000409 06/28/06 09:31:04 Sn T11908 190.864 StdFURNC StdBLANK 1541.19 2.95069 06/28/06 06/28/06 09:31:04 09:31:04 v 292.402 StdMULTI StdBLANK 1.84415 6.15240 -.000001 -.000902 06/28/06 09:31:04 Zn 206.200 StdMULTI StdBLANK NONE 1.00000 .000000 *NOT STANDARDIZED Pb2203 Se1960 220.353 196.026 NONE NONE ; NONE 1.00000 .000000 *NOT STANDARDIZED 00 O O H Standardization Readback Report 06/28/06 09:35:22 AM page 1 hod: DVCLPI I Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration Ag 328.068 StdBLANK .000000 -.000000 .000000 StdAGPSB 2000.00 2000.00 -.000122 Known Measured Residual Element Wavelength Standard Signal Signal Signal Al 308.215 StdBLANK .026972 .009534 .017438 StdICSEL 25.1414 17.0012 8.14025 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration As1890 189.042 StdBLANK .000000 -.000000 .000000 StdFURNC 1000.00 1000.000 .000061 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration B 249.678 StdBLANK .000000 .000000 -.000000 StdMULTI 5.00000 5.00000 .000000 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration Ba 493.409 StdBLANK .000000 -.000000 .000000 StdMULTI 5.00000 5.00000 .000000 Known Measured Residual >ment Wavelength Standard Concentration Concentration Concentration 313.042 StdBLANK .000000 -.000000 .000000 yv StdMULTI 5.00000 5.00060 -.000600 Known Measured Residual Element Wavelength Standard Signal Signal Signal Ca 317.933 StdBLANK .005809 .00373`9. .002070 StdICSEL 37.3551 19.6199 17.7352 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration Cd 226.502 StdBLANK .000000 -.000000 .000000 StdMULTI 5.00000 5.00000 .000000 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration Co 228.616 StdBLANK .000000 -.000000 .000000 StdMULTI 5.00000 5.00000 .000000 Known Measured Residual Element Wavelength Standard Concentration Concentration Concentration Cr 267.716 StdBLANK .000000 -.000000 .000000 StdMULTI 5.00000 5.00000 .000000 V) Known Measured Residual. Element Wavelength Standard Concentration Concentration Concentrationo r„. 324.754 StdBLANK .000000 .000000 -.000000 a StdMULTI 5.00000 5.00000 . 000000 H Standardization Readback Report 06/28/06 09:35:22 AM L,�ment Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard Fe 271.441 StdBLANK StdICSEL Element Wavelength Standard K 766.491 StdBLANK StdNAKHI Element Wavelength Standard Mg 279.079 StdBLANK StdICSEL Element Wavelength Standard Mn 257.610 StdBLANK StdMULTI :ment Wavelength Standard 202.030 StdBLANK StdMULTI Element Wavelength Standard Na 330.232 StdBLANK StdNAKHI Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTI Element Wavelength Standard P 178.287 StdBLANK StdAGPSB Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNC Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 100.000 100.000 Known Measured Signal Signal .033463 .021561 91.9351 55.2746 Known Measured Signal Signal .000159 .000148 4.54544 3.52163 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Signal Signal .001282 .000472 1.63314 1.17889 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00029 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 page 2 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Signal .011902 36.6604 Residual Signal .000011 1.02382 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Signal .000810 .454250 Residual Concentration -.000000 .000000 Residual Concentration -.000000 -.000291 Residual Concentration .000000 .000000 O Residual Concentration -.000000' O .000000 CD V1 H Standardization Readback Report 06/28/06 09:35:22 AM nent Wavelength Standard 2203/2 220.352 StdBLANK StdFURNC Element Wavelength Standard Sb2068 206.838 StdBLANK StdAGPSB Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNC Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNC Element Wavelength Standard Sn 189.989 StdBLANK StdMULTI Element Wavelength Standard 908 190.864 StdBLANK StdFURNC Element Wavelength Standard V 292.402 StdBLANK StdMULTI Element Wavelength Standard Zn 206.200 StdBLANK StdMULTI Element Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Signal Signal .000000 .000000 .000000 .000000 Known Measured Signal Signal .000000 .000000 .000000 .000000 page 3 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000061 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Signal .000000 .000000 Residual Signal .000000 .000000 06/28/06 09:46:02 AM page 1 Analysis Report hod: DVCLPI Sample Name: ICV Operator: CO Time: 06/28/06 09:35:30 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb 525.77 ppm 2.631 ppm 2.555 Ppm 2.578 ppm 52.93 Avge 1005.4 51.91 1.51 Oil .007 .004 .17 SDev %RSD 1.2 .12401 .26 .4971 .28687 .3992 .2621 .1436 .3228 #1 1006.8 52.19 524.26 2.643 2.561 2.583 53.13 #2 1004.8 51.87 527.27 2.626 2.554 2.577 52.88 #3 1004.5 51.67 525.78 2.624 2.548 2.576 52.80 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 55.00 High 1100.0 55.00 550.00 2.750 2.750 2.750 45.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 Elem Cd 'Co Cr Cu Fe K Mg Units ppm ppm ppm 2.551 Ppm 2.583 Ppm 51.83 Ppm 79.02 ppm 50.73 Avge 2.536 2.527 .014 .09 .31 .12 SDev %RSD .002 .0819 .017 .6846 .006 .2542 .5424 .1759 .3966 .2381 #1 2.538 2.521 2.558 2.598 51.93 79.33 50.87 u2 2.534 2.513 2.547 2.582 51.80 .79.03 50.69 3 2.535 2.546 2.546 2.570 51.76 78.71 50.64 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 55.00 High 2.750 2.750 2.750 2.750 55.00 88.00 72.00 45.00 Low 2.250 2.250 2.250 2.250 45.00 Na Ni P 2203/1 2203/2 Elem Unitsppm Mn Mo ppm ppm ppm ppm ppb 504.77 ppb 503.03 Avge 2.556 2.612 78.00 2.481 -.0045 2.67 3.40 SDev .007 .002 .54 .012 .4760 .0049 109.2 .52952 .67669 %RSD .2561 .0746 .6873 #1 2.563 2.614 78.43 2.494 -.0007 507.58 501.51 #2 2.555 2.611 78.17 2.480 -.0101 502.27 500.64 #3 2.550 2.610 77.40 2.470 -.0027 504.45 506.92 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb Ppm Ppb 515.63 ppm 2.574 ppm 2.502 Avge 1018.7 527.88 526.67 2.547 2.54 .002 SDev 1.3 10.11 1.9156 1.21 .004 .1506 .49173 .008 .2937 .0993 %RSD .12606 .23038 #1. 1017.2 538.99 528.03 2.552 517.32 2.582 2.505 �2 1019.3 519.21 525.69 2.545 516.85 2.573 2.500 93 1019.5 525.45 526.29 2.545 512.71 2.567 2.501 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass page 2 2.750 2.250 06/28/06 09:46:02 AM Analysis Report 550.00 2.750 high 1100.0 450.00 2.250 Low 900.00 Elem Pb2203 Se1960 Units ppb ppb Avge 503.61 527.07 SDev 2.46 4.18 %RSD .48836 .79214 #1 503.53 531.68 #2 501.18 523.53 #3 506.10 526.01 Errors LC Pass LC Pass High 550.00 550.00 Low 450.00 450.00 page 2 2.750 2.250 06/28/06 09:56:40 AM page 1 Analysis Report hod: DVCLPI Sample Name: ICVL Operator: CO Run Time: 06/28/06 09:46:09 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm ppb ppm ppm ppm .0005 ppm .0276 Avge .06596 .0098 .68169 .0072 .0011 .0006 .0002 .0001 .0024 SDev %RSD .11284 171.09 .0033 33.53 .67579 99.135 15.04 28.14 24.16 8.699 #1 .13102 .0127 1.1246 .0084 .0007 .0006 .0293 #2 .13119 .0103 1.0167 .0067 .0007 .0006 .0286 #3 -.06434 .0062 -.09616 .0063 .0004 .0004 .0249 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm PPM Ppm Ppm 2.426 ppm .0335 ppm .0088 Avge .0005 .0006 .0005 .0003 .0011 .0003 .006 .0059 .0050 SDev %RSD .0001 24.14 .0002 32.42 73.12 32.77 .2.677 17.45 56.33 #1 .0005 .0006 .0006 .0010 2.426 .0354 .0093 2 .0005 .0007 .0008 .0014 2.432 .0383 .0135 3 .0003 .0004 .0001 .0007 2.419 .0270 .0036 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK 2.750 High 2.250 Low Na Ni P 2203/1 2203/2 Elem Units Mn ppm Mo ppm ppm ppm ppm Ppb -1.5094 ppb -.34382 Avge .0001 .0119 2.474 -.0008 .0056 .0041 2.8262 1.10654 SDev .0001 165.3 .0056 47.26 .011 .4522 .0006 74.71 73.33 187.24 321.84 %RSD #1 .0183 2.475 -.0008. .0104 -.46159 -1.5104 #2 .0001 .0002 .0100 2.484 -.0015 .0028 .64319 -4.7099 .69081 -.21184 #3 -.0001 .0075 2.462 -.0002 .0037 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb Ppm ppb -.15266 ppm .0009 ppm .0015 Avge 8.0664 -2.4625 5.2803 -.0005 0006 03 085 SDev 6.6058 2224991 105040 11302 2171598 301064 2003 %RSD 81.88 #1 15.221 -.24895 4.9981 -.0010 3.5809 .0012 .0018 #2 6.7790 -8.7150 4.9509 -.0007 -2.7534 .0006 .0015 #3 2.1994 1.5763 5.8919 .0001 -1.2855 .0008 .0012 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Errors NOCHECK Analysis Report nlgh Low Elem Pb2203 Se1960 Units ppb ppb Avge -.73157 2.7023 SDev 1.24892 2.0823 %RSD 170.72 77.055 #1 -1.1608 3.2513 #2 .67535 .40057 #3 -1.7093 4.4552 Errors NOCHECK NOCHECK High Low 06/28/06 09:56:40 AM page 2 Analysis Report 06/28/06 10:07:19 AM page 1 hod: DVCLPI Sample Name: ICE Operator: CO tcun Time: 06/28/06 09:56:47 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM ppb PPM PPM PPM Ppm Avge -.19094 -.0071 .65542 .0016 .0001 .0001 .0037 SDev .0016 1.4268 .0009 .0001 .0001 .0012 %RSD .07308 38.273 23.21 217.69 55.44 100.6 60.24 32.51 #1 -.14779 -.0060 2.3022 .0023 .0003 .0002 .0050 #2 -.14971 -.0090 -.20855 .0006 .0001 .0001 .0035 #3 -.27532 -.0063 -.12743 .0020 .0000 .0000 .0026 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10:000 .0200 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.0200 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm PPM Ppm -.0027 Ppm .0145 PPM -.0016 Avge .0002 .0002 -.0003 .0003 .0012 .0004 .0012 .0053 .0042 SDev %RSD .0001 49.43 .0001 37.90 98.25 31.96 44.30 36.48 266.4 #1 .0001 -.0001 .0015 -.0014 .0202 -.0007 "2 .0004 .0001 -.0001 .0012 -.0031 .0097 -.0061 3 .0001 .0002 .0003 -.0006 .0008 -.0037 .0137 .0021 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Mo Na Ni P 2203/1 2203/2 Elem Units Mn ppm PPM Ppm PPM Ppm ppb -1.2407 ppb -.99418 Avge -.0004 .0016 .0571 -.0013 .0024 .9497 2.22112 SDev .0000 .0008 48.40 .0054 9.487 .0003 23.78 .0086 355.4 76.544 223.41 %RSD 10.87 #1 -.0003 .0018 .0522 --.0011 .0086 -2.1329 -.89520 #2 -.0004 .0023 .0562 -.0016 .0062 -1.3467 -3.2631 #3 -.0004 .0007 .0630 -.0012 -.0075 -.24247 1.1758 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb Ppm ppb Ppm PPM Avge -1.2942 1.9030 .38414 -.0009 .88922 .0005 .0006 SDev 4.8613 3.7079 .0016 3.8297 .0003 .0003 %RSD .8637 66.736 2'55.46 965.25 171.2 430.68 49.73 52.04 #1 -.34034 -.12084 .94198 .0000 5.3099 .0008 .0006 #2 -1.5190 7.4492 -3.5711 -.0000 -1.2222 .0003 .0009 #3 -2.0233 -1.6195 3.7815 -.0027 -1.4200 .0005 .0003 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 10:07:19 AM page 2 nigh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb Ppb Avge -1.0759 .89029 SDev 1.6762 .97772 %RSD 155.80 109.82 #1 -1.3069 .58845 #2 -2.6245 .09909 #3 .70390 1.9833 Errors LC Pass LC Pass High 3.0000 5.0000 Low -3.0000 -5.0000 10.000 .0500 -10.000 -.0500 .0200 -.0200 Analysis Report hod: DVCLPI Sample Name: CRII Time: 06/28/06 10:07:26 PPM Comment: pprr. .1967 .0001 Mode: CONC Corr. Factor: 1 .0003 Elem Ag Al As1890 Units ppb ppm ppb Avge 18.849 -.0043 20.316 SDev .573 .0031 .293 0-oRSD 3.0384 71.09 1.4429 #1 18.190 -.0078 20.050 #2 19.133 -.0033 20.630 #3 19.224 -.0019 20.266 Elem Cd Co Cr Units ppm ppm ppm Avge .0104 .0999 .0202 SDev .0001 .0007 .0004 %RSD .8489 .6566 2.103 #1 .0104 .0999 .0207 #2 .0103 .0993 .0198 #3 .0105 .1006 .0202 Elem Mn Mo Na Units ppm ppm ppm Tge .0294 .0277 .0370 Dev .0002 .0014 .0012 %RSD .8079 4.864 3.204" #1 .0293 .0291 .0383 #2 .0293 .0278 .0360 #3 .0297 .0264 .0367 Elem Sb2068 1960/1 1960/2 Units ppb ppb ppb Avge 118.19 11.487 12.649 SDev 3.16 1.772 2.558 %RSD 2.6767 15.423 20.226 #1 114.66 13.438 11.966 #2 119.16 9.9799 15.480 #3 120.76 11.042 10.501 Elem Pb2203 Se1960 Units ppb' ppb Avge 6.3898 12.262 SDev .5069 1.493 %RSD 7.9323 12.174 #1 6.8689 12.457 #2 6.4415 13.649 #3 5.8592 10.682 06/28/06 10:17:57 AM page 1 Operator: CO B Ba Be Ca PPM PPM PPM pprr. .1967 .0001 .0102 .01,03 .0003 .0001 .0001 .000's .1517 59.46 .5158 5.3:=15 .1970 .0000 .0102 .0098 .1964 .0002 .0101 .0103 .1967 .0001 .0102 .0109 Cu Fe K Mg PPM PPM PPM ppn` .0521 -.0022 .0108 .0004 .0003 .0004 .0068 00'8 .5329 19.77 62.87 223"9 .0519 -.0018 .0034 .0008 .0524 -.0021 .0124 u,�,:i .0520 -.0027 .01 Ni P 2203i/-, >210 Ppm ppm ppb ppb .0783 .0037 5.9720 6.5979 .0006 .0059 .9061 1.1823 .7627 160.6 15.172 17.9.19 .0776 -.0028 5.472.8 % • .< 4 .0787 .0052 5.4253 6.94.32 .0786 .0088 7.0179 5.2800 Sn T11908 V Zri PPM Ppb PPM PP'r. .0779 20.643 .1015 .0417 .0019 .275 .0008 .000T 2.373 1.3318 .7495 1.005 .0797 20.737 .0760 20.859 .1012 .42_.. .0781 20.333 Analysis Report 06/28/06 10:28:36 AM page 1 hod: DVCLPI Sample Name: ICSAI Operator: CO Time: 06/28/06 10:18:04 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .15793 535.9 -3.5589 .0486 .0007 .0002 521.3 SDev .62597 1.9 3.0485 .0013 .0001 .0000 1.6 %RSD 396.37 .3623 85.658 2.669 9.052 17.47 .3002 #1 -.01442 538.0 -1.6878 .0496 .0006 .0002 522.3 #2 .85202 534.1 -7.0766 .0490 .0007 .0002 522.1 #3 -.36381 535.6 -1.9124 .0471 .0006 .0002 519.5 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000. -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge -.0003 .0025 .0067 -.0004 204.3 .0174 521.5 SDev .0002 .0004 .0005 .0002 .5 0130 1.2 %RSD 85.33 16.63 7.879 45.90 .2598 74.76 .2365 #1 -.0005 .0023 .0062 -.0003 204.9 .0087 522.8 #2 -.0001 .0029 .0072 -.0006 204.1 .0324 521.6 -:0001 .0022 .0066 -.0003 203.9 .0111 520.3 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm Ppm ppm Ppm ppb Ppb Avge .0086 -.0001 .0509 .0016 .0019 -8.3377 3.6870 SDev .0001 .0009 .0020 .0002 .0053 5.1015 4.6495 %RSD .7067 1378. 3.998 13.90 281.8 61.187 126.11 #1 .0086 -.0005 .0495 .0018 -.0012 -6.4739 3.6821 #2 .0085 -.0006 .0533 .0015 .0080 -4.4301 -.96010 #3 .0085 .0009 .0501 .0014 -.0012 -14.109 8.3389 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -..0150 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 9.7278 -12.537 3.9534 -.0112 3.9671 .0047 .0032 SDev 2.7366 7.161 4.3032 .0035 4.4080 .0002 .0004 %RSD 28.132 57.117 108.85 31.25 111.11 5.113 13.94 #1 9.4707 -4.8206 3.4818 -.0144 5.6980 .0046 .0032 2 7.1289 -13.823 -.09461 -.0116 -1.0436 .0047 .0036 3 12.584 -18.968 8-.4730 -.0075 7.2470 .0050 .0027 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report rL.Lgh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb ppb Avge -.31674 -1.5376 SDev 1.58272 2.7958 %RSD 499.69 181.83 #1 .30066 .71752 #2 -2.1151 -4.6658 #3 .86423 -.66457 Errors LC Pass LC Pass High 6.0000 5.0000 Low -6.0000 -5.0000 06/28/06 10:28:36 AM page 2 10.000 ..0500 .0200 -10.000 -.0500 -.0200 O O O 06/28/06 10:39:14 AM page 1 Analysis Report hod: DVCLPI Sample Name: ICSABI Operator: CO Run Time: 06/28/06 10:28:43 Comment: Mode: CONC Corr. Factor: 1 Elem. Ag Al Asb890 Ppm Ba ppm Be Ppm Ca ppm Units ppb ppm PP 1061.4 1.138 .5317 .5141 515 Avge 1071.3 536.6 5.0 .0003 .0005 .4 SDev 1.4 .6 .003 .2639 .0613 .1032 .0840 %RS'D .13438 .1055 .46768 #1 1070.3 536.0 1061.8 1.135 .5313 .5146 515.6 515.3 #2 1072.9 537.1 1056.2 1.140 1.140 .5319 .5140 .5135 514.7 3 1070.5 536.1 1066.1 .5318 Errors LC Pass LC Pass LC Pass LC Pass LC -Pass LC Pass LC Pass 600.0 HiqYi 1200.0 6'00.0 1200.0 1.200 .6000 .6000 .4000 400.0 Love 800.00 400.0 800.00 .8000 .4000 Cd Co Cr Cu Fe Ppm K Ppm Mg ppm Units Unit PPm PP m Ppm Ppm 202:2' .013 516.5 Avge .9572 .4833 .0018 .5123 .0010 .5526 .0010 .0057 41.35 SDev %RSD .0021 .2217 .3678 .2042 .1824 .1111 .1009 #1 .9587 .4852 .5131 .5515 202.8 202.5 .0082 517.3 516.8 2 .9581 .4828 .5126 .5531 202.3 .0197 .0137 516.2 :3 .9548 .4817 .5111 .5533 LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK C Pass Errors High 1.200 .6000 .6000 .6000 240.0 160.0 400.0 Low .8000 .4000 .4000 .4000 Ni P 2203/1 2203/2 Elem Mn Mo Na ppm ppm ppb Ppb Units ppm PP m ppm .0059 961 34 961.27 Avge .5196 1.017 .0330 .9206 .0053 SDev .0005 .004 .0024 7.298 .0005 90.53 .13950 .13215 %RSD .0941 .3755 .0558 1 #1 .5196 1.014 .0350 .9210 .0057 963.17 961.42 959.93 962.42 .5200 1.015 .0336 .9208 .0113 964.06 960.75 #3 .5190 1.021 .0303 .9200 .0007 NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK Errors LC Pass 1.200 High .6000 Low .4000 .8000 Elem Sb22068- 1ppb0/1 PpbO/2 ppm T11908 V ppm Zn ppm Units pp.5206 1062.7 Ppb 1.010 993.64 .9246 Avge 7.2536 1057.6 5.8 .0002 .0018 SDev 3.4211 7.0 .004 .3466 .36737 .0388 .1908 %RSD 47.165 .66640 .54246 O #1 9.4355 1065.7 1061.8 1.014 988.14 988.77 .5208 .9259 .92 54 O #2 3.3107 1052.7 1068.9 1.008 1.008 994.73 .5204 .5205 .922266 #3 9.0145 1054.4 1057.5 NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Errors NOCHECK Analysis Report 06/28/06 10:39:14 AM page 2 1200.0 .6000 1.200 nigh 800.00 .4000 .8000 Low Elem Pb2203 Se1960 Units ppb ppb Avge 961.65 1061.0 SDev .57 4.0 %RSD 05912 .3.7369 #1 961.01 1063.1 #2 962.09 1063.5 #3 961.85 1056.5 Errors LC Pass LC Pass High 1200.0 1200.0 Low 800.00 800.00 N O O CJD F-' Analysis Report 06/28/06 10:49:53 AM page 1 hod: DVCLPI Sample Name: CCV1 Operator: CO Time: 06/28/06 10:39:22 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1008.6 51.74 528.56 2.629 2.555 2.591 53.21 SDev 19.6 .61 16.70 .052 .033 .090 1.91 %RSD 1.9456 1.175 3.1601 1.988 1.273 3.482 3.593 ##1 1028.7 52.44 53.8.67 2.679 2.592 2.666 54.81 ##2 1007.7 51.43 537.72 2.634 2.540 2.615 53.72 ##3 989.45 51.36 509.28 2.574 2.532 2.491 51.09 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.557 2.543 2.564 2.573 52.24 78.56 51.04 SDev .107 .081 .079 .032 1.63 .90 1.75 %RSD 4.188 3.169 3.071 1.232 3.111 1.141 3.429 #$1 2.641 2.614 2.629 2.609 53.64 79.40 52.50 2.593 2.560 2.586 2.562 52.63 77.62 51.51 3 2.436 2.455 2.477 2.548 50.46 78.65 49.10 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Eleni Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb Avge 2.569 2.619 78.05 2.476 .0054 508.21 504.53 SDev .070 .078 680 .088 .0064 16.28 18.16 %RSD 2.714 2.973 1.028 3.560 118.1 3.2042 3.6000 #1 2.630 2.685 78.87 2.546 .0035 522.92 516.24 $#2 2.583 2.639 77.27 2.505 .0125 510.98 513.74 43 2.493 2.533 78.02 2.377 .0002 490.71 483.60 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb' ppm ppb ppm. ppm Avge 1028.6 535.47 532.47 2.562 522.40 2.583 2.528 SDev 22.8 19.02 15.58 .101 12.38 .063 .136 %RSD 2.2181 3.5524 2.9255 3.952 2.3700 2.434 5.390 #1 1031.1 557.19 545.10 2.645 535.47 2.640 2.629 k2 1050.0 527.46 537.25 2.591 520.89 2.593 2.583 #3 1004.6 521.77 515.06 2.449 510.84 2.516 2.373 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 10:49:53 AM page 2 nigh 1100.0 Low 900.00 Elem Pb2203 Units ppb Avge 505.75 SDev 17.36 %RSD 3.4328 #1 518.46 #2 512.82 #3 485.97 Errors LC Pass High 550.00 Low 450.00 Se1960 ppb 533.47 15.92 2.9844 549.13 533.99 517.30 LC Pass 550.00 450.00 550.00 2.750 450.00 2.250 2.750 2.250 Analysis Report hod: DVCLPI Sample Name: CCVLl muu Time: 06/28/06 10:50:01 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .13251 .0288 1.5599 SDev .13330 .0117 1.4781 %RSID 100.59 40.47 94.751 ##1 .26611 .0415 3.0451 #2 .00048 .0266 1.5457 #3 .13190 .0185 .08906 Errors NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Units ppm ppm PPM Avge 0006 .0009 .0008 SDev .0003 .0002 .0004 %RSD 44.61 21.84 46.04 #1 .0009 .0011 .0012 u?0006 .0010 .0006 3 .0003 .0007 .0006 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge .0001 .0120 2.465 SDev .0002 .0057 .021 %RSD 278.3 47.31 .8493 #1 .0002 .0183 2.489 #2 .0000 .0102 2.450 #3 -.0001 .0074 2.456 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem Sb2068 1960/1 1960/2 Units ppb Ppb ppb Avge 9.2190 4.8037 3.6823 SDev 7.4875 2.6721 .5179 %RSD 81.219 55.626 14.063 41 17.859 2.4773 4.1327 �2 4.6262 7.7222 3.7978 J#3 5.1716 4.2116 3.1165 Errors NOCHECK NOCHECK NOCHECK 06/28/06 11:00:32 AM Operator: CO B PPM .0079 .0016 19.63 .0097 .0074 .0067 NOCHECK Cu PPM .0015 .0001 8.346 .0016 .0014 .0016 NOCHECK Ni PPM -.0007 .0008 112.9 -.0000 -.0005 -.0015 NOCHECK Sn PPM .0019 .0008 43.41 .0025 .0022 .0010 NOCHECK Ba ppm .0006 .0002 29.26 .0008 .0006 .0005 NOCHECK Fe PPM 2.429 .012 .4779 2.443 2.421 2.424 LC Pass 2.750 2.250 P ppm .0073 .0040 54.48 .0031 .0110 .0077 NOCHECK T11908 ppb 1.2421 1.2132 97.670 .06701 1.1693 2.4901 NOCHECK Be ppm .0005 .0002 38.01 .0007 .0005 .0004 NOCHECK K Ppm .0246 .0038 15.61 .0223 .0291 .0225 NOCHECK 2203/1 ppb -3.0325 1.5382 5.0.724 -4.6565 =2.8433 -1.5976 NOCHECK V PPM .0012 .0004 30.87 .0017 .0010 .0010 NOCHECK page 1 Ca PPM .0479 .0104 21.73 .0594 .0449 .0393 NOCHECK Mg PPM .0286 .0123 43.17 .0426 .0237 .0194 NOCHECK 2203/2 ppb -.53506 1.98187 370.40 1.3001 -2.6367 -.26855 NOCHECK Zn PPM -.0009 .0002 20.97 -.0010 -.0006 -.0010 NOCHECK Analysis Report __gh Low Elem Pb2203 Se1960 Units ppb ppb Avge -1.3663 4.0562 SDev 1.1595 .9098 %RSD 84.867 22.429 #1 -.68305 3.5818 #2 -2.7051 5.1051 #3 -.71071 3.4816 Errors NOCHECK NOCHECK High Low 06/28/06. 11:00:32 AT✓ pr,--ge 2 Analysis Report 06/28/06 11:11:12 AM page 1 hod: DVCLPI Sample Name: CCB1 Operator: CO Time: 06/28/06 11:00:40 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .14855 -.0079 .62590 .00.21 .0001 .0001 .0082 SDev .32760 .0046 2.6546 .0006 .0000 .0000 .0021 %RSD 220.53 58.94 424.12 26.54 29.44 41.68 25.60 #1 .42578 -.0031 .42526 .0027 .0002 .0002 .0104 #2 :23283 -.0081 3.3751 .0016 .0001 .0001 .0080 #3 -.21296 -.0124 -1.9227 .0019 .0001 .0001 .0062 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .0200 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.0200 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0004 -.0003 .0012 -.0019 .0199 .0026 SDev .0001 .0004 .0002 .0003 .0015 .0081 .0062 %RSD 57.15 107.7 69.09 22.77 80.68 40.86 240.1 #1 .0002 .0004 -.0003 .0015 -.0003 .0280 .0090 u?0001 .0007 -.0001 .0012 -.0021 .0198 .0021 3 .0001 -.0000 -.0006 .0010 -.0033 .0118 -.0034 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low, -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb Avge -.0003 .0015 .0442 -.0015 .0061 -.82246 2.2371 SDev .0001 .0004 .0030 .0005 .0079 .94386 .3154 %RSD 22.79 28.75 6.794 33.79 129.3 114.76 14.099 #1 -.0002 .0018 .0473 -.0018 .0034 .08880 2.1242 #2 -.0003 .0016 .0439 -.0009 .0150 -.76033 2.5934 #3 -.0004 .0010 .0413 -.0019 -.0001 -1.7959 1.9936 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb Ppm Ppb ppm Ppm Avge -.89081 -.99667 .25597 -.0026 .06786 .0006 .0011 SDev 1.26276 5.81668 1.8324 .0015 .72739 .0001 .0005 %RSD 141.75 583.61 715.88 57.58 1071.8 17.31 42.29 -R1 .28295 3.8943 -.26393 -.0030 .55583 .0005 .0015 2 -.72849 -7.4287 2.2921 -.0009 .41593 .0007 .0006 3 -2.2269 .54447 -1.2603 -.0038 -.76817 .0005 .0012 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report iiigh 60.000 Low -60.000 Elem Pb2203 Unit's ppb Avge 1.2187 SDev .4216 %RSD 34.594 #1 1.4469 #2 1.4770 #3 .73217 Errors LC Pass High 3.0000 Low -3.0000 Se1960 ppb -.16077 1.11931 696.20 1.1211 -.94452 -.65893 LC Pass 5.0000 -5.0000 06/28/06 11:11:12 AM page 2 10.000 .0500 .0200 -10.000 -.0500 -.0200 00 O O Analysis Report 06/28/06 11:21:51 AM page 1 hod: DVCLPI Sample Name: MB -17344 Operator: CO tcuii Time: 06/28/06 11:11:19 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb -1.3866 Ppm Ppm .0008 ppm .0000 Ppm .0166 Avge SDev -.04432 -.0073 .0005 .8930 .0020 .0003 .0001 .0000 .0004 %RSD .20724 467.59 7.387 64.402 13.22 6.981 50.69 2.158 #1 -.0072 -1.2509 .0023 .0008 .0000 .0169 #2 .04155 -.28070 -.0079 -.56927 .0018 .0007 .0000 .0166 #3 .10618 -.0068 -2.3397 .0020 .0.008 .0000 .0162 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .0200 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.0200 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm Ppm ppm -.0003 Ppm .0181 ppm .0008 Avge .0000 .0002 .0001 .0002 .0019 .0002 .0006 .0052 .0037 SDev %RSD .0002 804.4 .0003 118.6 226.7 8.640 197.7 28.66 463.4 #1 .0000 -.0001 .0018 .0003 .0146 .0050 1. 7 .0000 -.0001 .0001 .0003 .0017 -.0002 .0156 -.002.0 3 .0002 .0006 .0001 .0021 -.0009 .0241 -.0006 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0500 .0100 .0250 .1000 5.000 .2000 Low .0050 -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Na Ni P 2203/1 2203/2 Elem Units Mn ppm Mo Ppm ppm Ppm Ppm ppb ppb -.95974 Avge -.0004 .0022 .1135 -.0014 .0134 -.56292 1.26608 .87477 SDev .0001 .0008 34.83 .0009 .0005 37.26 .0069 51.38 224.91 91.147 %RSD 18.66 .7870 #1 -.0003 .0031 .1133 -.0009 .0056 -.01198 -1.5823 #2 -.0004 .0015 .1145 -.0020 .0161 :33435 -1.3373 #3 -.0005 .0021 .1128 -.0014 .0185 -2.0111 .04041 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb 2.3457 Ppm .0005 ppm .0034 Avge -1.4437 5.9935 1.2529 2.5805 3.8847 -.0024 .0013 2.7427 .0002 .0002 SDev %RSD .9256 64.115 20.905 150.54 56.61 116.92 36.87 5.116 +t1 -2.1736 5.1987 6.4935 -.0027 -.59546 .0007 .0036 k2 -1.7550 7.4378 -1.2754 -.0035 4.8334 .0004 .0033 J3 -.40258 5.3440 2.5235 -.0009 2.7991 .0005 .0033 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass, LC Pass LC Pass Analysis Report 06/28/06 11:21:51 AM page 2 High 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb Ppb Avge -.82717 3.7174 SDev .21222 2.2290 %RSD 25.656 59.961 #1 -1.0589 H6.0627 #2 -.78023 1.6265 #3 -.64235 3.4631 Errors LC Pass LC Pass High 3.0000 5.0000 Low -3.0000 -5.0000 10.000 .0500 -10.000 -.0500 .0200 -.0200 O 00 O O H Analysis Report 06/28/06 11:32:30 AM page 1 hod: DVCLPI Sample Name: LCS-17344 Operator: CO Time: 06/28/06 11:21:58 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb Ppm Ppm ppm Ppm Avge 1010.3 52.05 524.73 2.567 2.570 2.565 52.40 SDev 2.8 .22 7.33 .014 .019 .044 1.04 '-.RSD .28003 .4243 1.3964 .5356 .7535 1.706 1.987 ##1 1013.2 51.81 532.36 2,582 2.548 2.616 53.60 #2 1010.0 52.24 524.09 2.562 2.583 2.539 51.81 #3 1007.5 52.11 517.74 2.556 2.579 2.541 51.78 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass- LC Pass High 1200.0 60.00 600.00 3.000 3.000 3.000 60.00 Low 800.00 40.00 400.00 2.000 2.000 2.000 40.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm Ppm Ppm Ppm Ppm Avge 2.501 2.516 2.531 2.570 51.83 77.20 50.29 SDev .067 .049 .042 .013 .78 1.13 .90 0 -.RSD 2.676 1.931 1.652 .5253 1.507 1.459 1.789 #1 2.579 2.571 2.579 2.557 52.73 75.94 51.33 #2 2.462 2.481 2.506 2.584 51.37 .78.12 49.82 3 2.463 2.495 2.508 2.571 51.38 77.55 49.72 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 3.000 3.000 3.000 3.000 60.00 96.00 60.00 Low 2.000 2.000 2.000 2.000 40.00 64.00 40.00 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm 2.565 Ppm 77.71 Ppm 2.405 Ppm .0125 Ppb 499.88 Ppb 492.41 Avge SDev 2.543 .029 .030 .28 .046 .0103 12.91 11.85 %RSD 1.142 1.159 .3542 1.916 82.34 2.5819 2.4063 #1 2.577• 2.599 77.59 2.458 .0243 514.78 506.09 #2 2.525 2.548 78.02 2.379 .0057 492.26 485.41 #3 2.528 2.548 77.51 2.377 .0075 492.59 485.72 Errors LC Pass NOCHECK LC Pass LC -Pass NOCHECK NOCHECK NOCHECK High 3.000 96.00 3.000 Low 2.000 64.00 2.000 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb Ppm Ppb Ppm Ppm Avge 1038.6 526.69 508.22 2.510 509.05 2.564 2.455 SDev 18.4 18.20 4.61 .055 3.76 .020 .099 %RSD 1.7707 3.4564 .90683 2.183 .73859 .7892 4.047 #1 1059.7 547.70 512.51 2.573 512.46 2.587 2.570 :2 1030.3 517.00 503.35 2.484 505.02 2.553 2.396 .'3 1025.8 515.39 508.79 2.473 509.66 2.552 2.399 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 11:32:30 AM page 2 nigh 1200.0 Low 800.00 Elem Pb2203 Se1960 Units ppb ppb Avge 494.90 514.37 SDev 12.20 8.68 %RSD 2.4654 1.6867 #1 508.98 524.23 #2 487.69 507.89 #3 488.01 510.99 Errors LC Pass LC Pass High 600.00 600.00 Low 400.00 400.00 600.00 3.000 400.00 2.000 3.000 2.000 N 00 O O 6f) H Analysis Report 06/28/06 11:43:08 AM page 1 hod: DVCLPI Sample Name: 0606916-001E_ Operator: CO Time: 06/28/06 11:32:37 Comment: �(7� Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .26884 .0131 -.32972 .0042 .0009 .0005 .1220 SDev .23511 .0063 1.61881 .0002 .0004 .0004 .0077 %RSD 87.454 48.61 490.97 5.458 43.83 76.44 6.309 #1 .16512 .0204 1.5394 .0044 .0013 .0010 .1306 #2 .10342 .0094 -1.2801 .0039 .0007 .0004 .1197 #3 .53797 .0094 -1.2485 .0042 .0006 .0002 .1158 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm PPM PPM PPM Ppm Ppm Avge .0007 .0006 .0012 .0027 .0453 .0413 .0103 SDev .0005 .0006 .0005 .0006 .0080 .0044 .0081 %RSD 68.79 98.98 39.98 21.66 17.68 10.58 78.19 #1 .0011 .0013 .0015 .0033 .0542 .0455 .0191 #2 .0007 .0006 .0014 .0028 .0428 .0367 .0085 #3 .0002 .0000 .0007 .0021 .0388 .0416 .0033 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb age .0003 .0077 .1633 -.0004 .2203 -1.9292 -.06245 )ev .0004 .0039 .0147 .0006 .0127 1.2529 1.04531 okSD 130.5 50.59 9.013 141.0 5.760 64.940 1673.8 #1 .0008 .0122 .1798 -.0000 .2064 -1.5734 -.10895 #2 0002 .0061 .1586 -.0001 .2234 -.89280 -1.0837 #3 .0000 .0049 .1515 -.0010 .2313 -3.3215 1.0053 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb Ppm Ppb Ppm Ppm Avge -.81481 4.0468 3.3564 -.0017 2.6308 .0010 .0095 SDev 1.56808 9.1487 1.3700 .0006 3.1847 .0003 .0006 %RSD 192.45 226.07 40.816 38.66 121.06 29.80 6.741 #1 -2.6125 14.306 4.8566 -.0024 6.1414 .0014 .0103 #2 .27149 1.0989 3.0408 -.0012 1.8236 .0009 .0091 #3 -.10344 -3.2645 2.1717 -.0014 -.07272 .0008 .0092 Elem Pb2203 Se1960 Units ppb ppb Avge -.68370 3.5867 SDev .30200 3.9579 %RSD 44.172 110.35 #1 -.59623 8.0036 #2 -1.0198 2.3945 #3 -.43508 .36185 M 00 O O L/1 page 1 Ca PPM 1.209 .010 .7950 1.205 1.220 1.202 Mg ppm .2309 .0041 1.772 .2314 .2347 .2265 2203/2 ppb 1.9944 .7382 37.014 1.1606 2.5647 2.2579 Zn PPM .0590 .0004 .6919 .0587 .0594 .0588 06/28/06 11:53:47 AM Analysis Report zod: DVCLPI Sample Name: 0606916-002E Operator: CO Run Time: 06/28/06 11:43:15 Comment: µU--� Mode: CONC Corr. Factor: 1 .Eleni Ag Al As1890 B Ba Be Units ppb Ppm Ppb Ppm PPM .0017 Ppm .0000 Avge -.23659 .0260 -1.5447 .0100 .0004 .0000 .0000 SDev .20690 .0009 3.454 .0793 5.1365 4.067 .7059 44.78 %RSD 87.451 #1 -.47247 .0249 -1.6021 .0101 .0017 .0000 #2 -.15146 .0265 -1.5778 .0095 .0017 .0000 .0001 #3 -.08584 .0264 -1.4542 .0103 .0017 Eleni Cd Co Cr Cu m Fe PPM K PPM Units ppm PPM Ppm PP .0651 .2045 .3546 Avge 0001 .0007 .0014 .0003 .0004 .0018 .0029 SDev %RSD .0002 209.4 .0003 42.93 25.48 .6522 .8795 .8122 #1 -.0000 .0006 .0012 .0647 .2038 .3512 #2 .0003 .0005 .0012 .0655 .2065 .3560 .3564 #3 .0000 .0011 .0018 .0651 .2031 Mo Na Ni P 2203/1 Elem nits Mn ppm ppm PPM PPM ppmPP b -.13786 vge 0029 .0029 17.93 .0013 :6277 .0065 2.56454 SDev .0000 .0001 4.023 .13 .0003 18.71 1.033 1860.3 %RSD 1.040 .7314 #1 .0029 .0030 17.83 .0015 .6331 .2.7348 -2.196E #2 .0028 .0028 18.08 .0010 .6295 -.9515_` #3 .0029 .0029 17.89 .0015 .6205 Elem Sb2068 1960/1 1960/2 Sn 1908 T1b V Units ppb ppb ppb PPM PP -1.9181 PP m .0010 Avge -.05169 3.5833 1.3478 2.6805 -.0019 3.2764 .0003 SDev 1.90625 4.5247 126.27 198.88 .0007 38.03 170.82 27.40 %RSD 3687.8 #1. 1.0637 6.8415 -.39823 -.0024 -2.1465 .0007 #2 -2.2528 -1.5829 4.4341 -.0011 -.0023 -5.0743 1.4666 .0010 .0013 #3 1.0340 5.4912 .00754 Elem Pb2203 Se1960 Units ppb ppb Avge 1.2848 2.0926 SDev .3624 .3063 %RSD 28.204 14.637 #1 1.6852 2.0130 #2 .97952 2.4309 #3 1.1896 1.8340 page 1 Ca PPM 1.209 .010 .7950 1.205 1.220 1.202 Mg ppm .2309 .0041 1.772 .2314 .2347 .2265 2203/2 ppb 1.9944 .7382 37.014 1.1606 2.5647 2.2579 Zn PPM .0590 .0004 .6919 .0587 .0594 .0588 Analysis Report 06/28/06 12:04:25 PM hod: DVCLPI Sample Name: 0606916-003E Operator: CO Time: 06/28/06 11:53:54 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.20946 .0196 -.44915 .0098 .0014 .0000 SDev .06278 .0012 1.43807 .0006 .0001 .0000 %RSD 29.971 6.235 320.18 6.534 4.929 56.77 #1 -.27201 .0209 -.23796 .0092 .0014 .0000 #2 -.14646 .0194 .87164 .0105 .0015 .0000 #3 -.20993 .0185 -1.9811 .0097 .0014 .0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 .0009 .0012 .0556 .1884 .3517 SDev .0001 .0002 .0001 .0004 .0003 .0058 %RSD 54.24 21.29 10.96 .7037 .1835 1.662 #1 .0002 .0010 .0012 .0551 .1887 .3450 #2 .0000 .0010 .0013 .0559 .1880 .3542 43 .0002 .0007 .0011 .0557 .1885 .3559 Elem Mn Mo Na Ni P 2203/1 Units ppm ppm ppm ppm ppm ppb rae .0025 .0008 17.28 .0012 .5914 -.76016 )ev .0000 .0005 .03 .0004 .0079 1.06402 0-oRSD .2628 60.97 .1668 34.78 1.339 139.97 #1 .0025 .0011 17.25 .0014 .5823 -1.6389 #2 .0025 .0011 17.28 .0015 .5961 .42285 #3 .0025 .0002 17.30 .0007 .5959 -1.0644 Elem Sb2068 1960/1 1960/2 Sn T11908 V Units ppb ppb ppb ppm ppb ppm Avge .22591 .78812 3.7008 -.0008 1.5724 .0006 SDev 1.9113 2.1075 1.8020 .0015 2.9808 .0001 %RSD 846.05 267.41 48.693 188.7 189.57 20.97 #1 2.4144 -.55474 4.7221 .0009 -.86028 .0006 #2 -.62145 3.2172 1.6201 -.0014 .67992 .0005 #3 -1.1153 -.29805 4.7602 -.0018 4.8975 .0008 Elem Pb2203 Se1960 Units ppb ppb Avge 1.0729 2.7313 SDev .3507 .5045 %RSD 32.688 18.470 $1 1.2394 2.9653 #2 1.3093 2.1523 ##3 .66995 3.0762 page 1 Ca Ppm 1.094 .002 .1470 1.093 1.096 1.093 Mg PPM .2154 .0052 2.397 .2099 .2201 .2162 2203/2 ppb 1.9874 .6059 30.488 2.6758 1.7512 1.5352 Zn PPM .0439 .0006 1.326 .0438 .0445 .0434 V) Do O O F-+ 00 O O H 06/28/06 12:15:05 PM page 1 Analysis Report hod: DVCLPI Sample Name: 0606916-004E - Operator: CO Time: 06/28/06 12:04:33 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM Ppb PPM PPM PPM .0000 PPM 1.018 Avge -.12700 .0266 -2.1664 1.7824 .0079 .0001 .0017 .0001 .0000 .004 SDev %RSD .48952 385.44 .0002 .7195 82.275 1.281 3.528 27.31 .3919 #1 -.66109 .0268 -4.2199 .0078 .0017 .0000 1.021 #2 .0264 -1.2602 .0079 .0018 .0000 1.019 #3 .30032 -.02023 .0265 -1.0192 .0080 .0017 .0000 1.013 Elem Cd Cc Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM .1846 PPM 1.193 PPM .2271 Avge -.0000 .0008 .0008 .0004 .0435 .0002 .0010 .009 .0026 SDev %RSD .0001 1178. .0001 11.15 55.05 .4158 .5217 .7481 1.128 #1 -.0001- .0009 .0007 .0434 .1850 1.186 .2242 #2 -.0001 .0007 .0004 .0434 .1853 1.203 .2290 #3 .0001 .0008 .0013 .0437 .1835 1.190 •2281 Mo Na Ni P 2203/1 2203/2 Elem TTnitsppm Mn PPM PPM PPM PPM 3.488 Ppb .18374 Ppb .97429 vge 0118 .0008 20.21 .0010 .036 2.0063 1.2549 -Dev .0001 .0001 17.23 .19 .9457 .0006 61.42 1.035 1091.9 128.80 %RSD .5608 #1 .0008 20.42 .0004 3.463 -.70508 2.4226 #2 .0117 .0006 20.13 .0010 3.530 -1.2246 .28898 #3 .0119 .0117 .0009 20.06 .0016 3.473 2.4809 .21132 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb Ppb Ppb 2.7703 PPM -.0019 Ppb -.10963 PPM .0006 PPM .0275 Avge -1.6672 1.3479 2.9542 4.6120 .0020 3.90242 .0001 .0003 SDev %RSD .8703 52.198 219.17 166.48 104.2 3559.5 8.641 1.244 #1 -.71881 3.7465 1.5020 -.0038 -2.3434 .0005 .0272 #2 -2.4291 2.2491 -1.0747 -.0021 4.3964 .0005 .0278 .0276 #3 -1.8537 -1.9520 7.8838 .0002 -2.3820 .0006 Elem Pb2203 Se1960 Units ppb ppb Avge .71146 2.2971 SDev .82827 2.2885 %RSD 116.42 99.629 #1 1.3815 2.2498 #2 -.21461 .03251 #3 .96753 4.6089 00 O O H Analysis Report 06/28/06 12:25:44 PM hod: DVCLPI Sample Name: 0606916-005E Operator: CO nus, Time: 06/28/06 12:15:12 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm Ppb -.59947 Ppm .0043 Ppm .0009 Ppm .0000 Avge SDev .25305 .0027 .0034 1.27226 .0005 .0001 .0000 %RSD .20209 79.864 125.4 212.23 12.49 7.123 164.8 #1 .48354 .0055. .75763 .0048 .0009 .0000 #2 .16937 .0037 -1.7652 .0038 .0010 .0000 #3 .10623 -.0011 -.79081 .0044 .0009 -.0000 Elem Cd Co Cr Cu Fe K Units ppm Ppm PPM PPM PPM .2018 Ppm .3189 Avge -.0000 .0009 .0007 .0004 .0478 .0006 .0006 .0069 SDev %RSD .0001 133.8 .0003 33.40 56.38 1.164 .2947 2.168 #1 -.0001 .0012 .0011 .0473 .2024 .3251 #2 -.0001 .0006 .0003 .0484 .2016 .3200 #3 .0000 .0008 .0008 .0476 .2013 .3114 Elem Mn Mo Na Ni P 2203/1 Ppb TT -lits ppm PPM PPM 16.24 Ppm .0014 PPM .4662 .39335 sqe .0020 .0008 .0007 .02 .0004 .0093 2.7712 _-Dev %RSD .0001 2.310 94.06 .1167 31.00 1.995 704.52 #1 .0016 16.26 .0017 .4752 -2.0763 #2 .0020 .0020 .0005 16.22 .0015 .4566 -.13399 #3 .0019 .0002 16.25 .0009 .4669 3.3903 Elem Sb2068 1960/1 1960/2 Sn T11908 V Units ppb ppb ppb 3.2268 PPM -.0016 ppb -.71564 Ppm .0006 Avge SDev -.36582 1.33175 -.42543 7.25554 1.0314 .0014 3.12268 .0003 %RSD 364.05 1705.5 31.965 90.29 436.35 52.89 #1 1.1650 2.3828 4.3112 -.0018 1.9524 .0009 #2 -1.0050 -8.6654 3.1112 -.0030 -4.1502 .0006 #3 -1.2575 5.0062 2.2581 -.0001 .05090 .0003 Elem Pb2203 Se1960 Units ppb Ppb Avge .66543 2.0110 SDev .86857 2.4556 %RSD 130.53 122.11 #1 .06041 3.6694 #2 .27520 -.81004 43 1.6607 3.1736 page 1 Ca PPM .9592 .0010 .0998 .9597 .9598 .9581 Mg ppm .2135 .0045 2.107 .2172 .2147 .2085 2203/2 ppb .80062 .32385 40.450 1.1265 .47885 .79650 Zn ppm .0176 .0006 3.643 .0181 .0178 .0169 00 00 O O C% N 06/28/06 12:36:23 PM page 1 Analysis Report zod: DVCLPI Sample Name: 060691'6-005EDUP Operator: CO Run Time: 06/28/06 12:25:51 Comment: K�,j-3S i7.rP Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM ppb PPM PPM 0010 PPM pp'm 1.0123 Avge Avge .06433 .0351S -.17711 .0048 .0000 SDev .31762 .0033 2.64585 .0004 .0001 .000.E 4.028 3? 5 %RSD 493.71 9.464 1493.9 9.124 5.815 #1 .10672 .0326 .84651 .0047 .0011 .0000 1.026 #2 .35863 .0389 -3.1818 .0053 .0011 .0000 1.025 #3 -.27235 .0338 1.8040 .0044 .0010 .0000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm PPM PPM ppm .3252 Ppm .`271 Avge -.0000 .0009 .0043 .0496 .2158 .0009 .0081 .0052 SDev %RSD .0001 1166. .0003 36.16 .0003 7.064 .0001 .3109 .4315 2.491 2.279 #1 .0012 .0047 .0494 .2152 .3257 .2:73 #2 .0000 -.0001 .0005 .0042 .0495 .2169 .33::1 -22*18 #3 .0001 .0010 .0041 .0497 .2153 .3169 .2-2 Mo Na Ni P 2203%1 220.-:'2 Elem --zits Mn ppm PPM PPM PPM PPM .5433 ppb -2.1773 Ppb .26319 sge 0022 0004 16.83 .0016 .0092 1.7694 1.2827 DDev .0000 .0003 76.03 .07 .0003 15.67 1.689 81.265 48'7.36 %RSD 2.023 .4291 #1 .0022 .0001 16.78 .0017 .5492 -3.7748 .2-'-601 -1.0108 #2 .0021 .0006 16.80 .0013 .5479 -2.4816 -.27549 1.5544 #3 .0022 .0003 16.91 .0018 .5327 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb Ppb Ppb PPM Ppb 1.8560 PPM .0006 ppm .0208 Avge -.13882 .03640 5.1967 2.8223 1.5820 -.0004 .0007 3.0495 .0001 .0000 SDev 0 -.RSD 2.03511 1466.0 14277. 56.054 167.6 164.31 17.29 .2.07.2 # 1 1.2173 .76510 2.1772 .0002 -.91627 .00 C' 0.2 f) 202) "' #2 .84520 -5.4862 1.6647 -.0012 5.1224 .0005 #3 -2.4789 4.8303 4.6249 -.0003 1.3618 0ti=' Elem Pb2203 Se1960 Units ppb Ppb Avge -.54906 1.8950 SDev 1.31027 2.7098 %RSD 238.64 143.00 #1 -1.0925 1.7074 #2 -1.5002 -.71615 43 .94548 4.6937 00 00 O O C% N Analysis Report 06/28/06 12:47:02 PM hod: DVCLPI Sample Name: 0606916-005EMS Operator: CO Time: 06/28/06 12:36:31 Comment: �kw-3S as Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge 49.339 2.158 37.776 .0036 2.128 .0510 SDev 2.433 .012 3.398 .0031 .015 .0007 %RSD 4.9322 .5473 8.9960 84.65 .7163 1.461 ##1 51.151 2.151 39.725 .0053 2.111 .0518 ##2 46.573 2.151 33.852 .0001 2.140 .0506 #3 50.292 2.172 39.751 .0054 2.132 .0505 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0514 .5105 .2070 .3116 1.185 .2648 SDev .0011 .0077 .0030 .0031 .008 .0641 %RSD 2.222 1.507 -1.436 . .9933 .7092 24.21 #1 .0527 .5190 .2105 .3087 1.195 .3085 #2 .0506 .5088 .2054 .3148 1.180 .1912 #3 .0509 .5039 .2052 .3114 1.180 .2947 Elem Mn Mo Na Ni P 2203/1 Units ppm ppm ppm ppm ppm ppb 'ge .5169 .0001 16.16 .4937 .5399 8.0757 iev .0043 .0003 .23 .0053 .0030 20.593 aRSD .8370 378.9 1.399 1.071 .5529 255.00 #1 .5219 .0003 15.90 .4993 .5378 20.090 #2 .5147 -.0003 16.34 .4930 .5386 -15.703 #3 .5141 .0003 16.22 .4888 .5434 19.840 Elem Sb2068 1960/1 1960/2 Sn T11908 V Units ppb ppb ppb ppm ppb ppm Avge 524.20 -1.3331 18.307 -.0034 44.766 .5135 SDev 5.85 23.7324 10.917 .0053 5.400 .0035 %RSD 1.1166 1780.3 59.634 157.0 12.062 .6785 #1 530.86 13-455 11.577 .0000 50.627 .5174 #2 521.88 -28.707 30.902 -.0094 39.994 .5125 #3 519.86 11.253 12.440 -.0007 43.676 .5107 Elem Pb2203 Se1960 Units ppb ppb Avge 20.163 11.767 SDev .580 .624 %RSD 2.8755 5.2988 #1 19.835 12.203 #2 20.833 11.053 #3 19.822 12.045 page 1 Ca ppm .9361 .0164 1.757 .9549 .9241 .9294 Mg ppm .2051 .0039 1.905 .2085 .2008 .2059 2203/2 ppb 26.197 11.150 42.563 19.706 39.072 19.813 Zn PPM .5278 .0160 3.035 .5462 .5193 .5177 Analysis Report 06/28/06 12:57:41 PM page 1 hod: DVCLPI Sample Name: 0606916-005ESD Operator: CO Time: 06/28/06 12:47:10 Comment: N1 W - 3S 5-b �x Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.40757 -.0179 1.1920 .0012 .0011 .0000 .2018 SDev .12910 .0017 2.7883 .0007 .0005 .0000 .0007 %RSD 31.675 9.610 233.91 56.48 50.29 47.76 .3432 #1 -.53651 -.0161 -.12645 .0006 .0017 .0001 .2023 #2 -.40787 -.0182 -.69245 .0019 .0009 .0000 .2010 #3 -.27832 -.0195 4.3950 .0010 .0007 .0000 .2020 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0006 -.0003 .0114 .0352 .0631 .0418 SDev .0002 .0002 .0006 .0001 .0004 .0083 .0036 %RSD 194.8 33.35 192.0 .8855 1.188 13.11' 8.517 #1 .0003 .0005 .0004 .0115 .0347 .0726' .0451 #2 -.0001 .0005 -.0007 .0113 .0354 .0579 .0423 #3 .0001 .0008 -.0006 .0114 .0355 .0588 .0380 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb ,ge .0003 .0004 3.409 -.0008 .0979 .89557 .15383 )ev .0001 .0001 .010 .0003 .0008 1.1271 1.7122 %RSD 48.63 13.52 .3036 42.33 .7780 125.85 1113.0 #1 .0004 .0004 3.399 -.0006 .0974 1.8825 .14612 #2 .0002 .0005 3.420 -.0012 .0988 -.33258 1.8698 #3 .0002 .0004 3.409 -.0006 .0976 1.1368 -1.5545 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge -.67281 2.0090 .99101 -.0025 1.3450 .0005 .0054 SDev 1.34309 3.1319 3.1725 .0003 1.8055 .0004 .0003 %RSD 199.62 155.90 320.13 13.16 134.24 92.88 5.751 41 .00128 5.3625 -.29626 -.0025 3.4191 .0010 .0054 #2 -2.2194 1.5044 -1.3355 -.0022 .49101 .0002 .0057 #3 .19973 -.84003 4.6048 -.0028 .12484 .0003 .0051 Elem Pb2203 Se1960 Units ppb ppb - Avge .40124 1-.3304 SDev .94007 1.6064 %RSD 234.29 120.75 #1 .72477 1.5885 #2 1.1368 -.38945 #3 -.65788 .2.7921 O O O H t--� O O Cn E-+ 06/28/06 01:08:20 PM page 1 Analysis Report. hod: DVCLPI Sample Name: CCV2 Operator: CO xun Time: 06/28/06 12:57:49 Comment: Mode: CONC Corr. Factor: 1 ElemAl As1890 B Ba Be Ca Units Unit ppb ppm b ppb 525.77 ppm 2.579 Ppm 2.529 Ppm 2.559 Ppm 52.11 Avge 1001.6 51.17 5.64 .032 .021 .025 •59 SDev %RSD 7.9 .78779 .47 .9227 1.0735 1.235 .8429 .9608 1.131 #1 996.80 50.94 523.68 2.561 2.519 2.542 51.73 51.81 #2 997.36 50.85 521.47 2.561 2.515 2.548 2.587 52.78 #3 1010.7 51.71 532.16 2.616 2.553 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 55.00 High 1100.0 55.00 550.00 2.750 2.750 .2.750 2.250 2.250 45.00 Low 900.00 45.00 450.00 ,2.250 8lem Cd Co Cr Cu Fe K Mg Unitsppm ppm Ppm pPm ppm 52.19 ppm 77.21 Ppm 50.36 Avge 2.545 2.532 2.534 ;2.506 •77 45 SDev .017 .017 .022 .035 1.400 .29 .5633 .9934 .8926 %RSD .6592 .6763 .8622 #1 2.533 •2.520 2.517 2.489 51.93 76.97 50.10 50.11 u2 2.538 2.524 2.525 2.482 52.14 76.59 78.07 50.88 3 2.565 2.552 2.558 2.546 52.51 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 88.00 LC Pass 55.00 High 2.750 2.750 2.750 2.750 2.250 55.00 45.00 72.00 45.00 Low 2.250 2.250 2.250 Na Ni P 2203/1 2203/2 Elem Mn Mo Ppm Ppm Ppm Ppb Ppb Units ppm ppm 2.571 76.97 2.399 .0075 499.07 487.84 Avge 2.541 .041 .0036 6.84 4.39 SDev .021 .033 1.296 .65 .8468 1.692 48.00 1.3702 .89991 %RSD .8340 #1 2.527 2.545 76.75 2.374 .0115 493.49 497.03 486.12 484.57 #2 2.531 2.558 76.46 2.376 2.446 .0048 506.70 492.83 #3 2.565 2.608 77.71 .0061 LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK Errors High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb ppm 2.572 ppb 511.84 ppm 2.551 ppm 2.526 Avge 1014.9 538.39 514.07 6.69 .022 .014 SDev 15.9 6.92 1.2857 6.29 1.2238 .014 .5475 1.3063 .8721 .5608 %RSD 1.5714 #1 999.32 540.93 510.46 2.562 510.21 2.536 2.514 2.522 #2 1014.3 530.56 510.40 2.566 6.12 2.540 2.542 3 1031.2 543.69 521.33 2.588 509.19 2.577 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass t--� O O Cn E-+ Analysis Report 06/28/06 01:08:20 PM page 2 1-9h 1100.0 Low 900.00 Elem Pb2203 Se1960 Units ppb ppb Avge 491.58 522.17 SDev 5.08 5.98 oRSD 1.0339 1.1460 #1 488.58 520.61 #2 488.72 517.12 #3 497.45 528.78 Errors LC Pass LC Pass High 550.00 550.00 Low 450.00 450.00 550.00 2.750 450.00 2.250 knalysis Report zod: DVCLPI Sample Name: CCVL2 Run Time: 06/28/06 13:08:28 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb Ppm ppb AvgE� .13192 .0053 1.8791 SDev .17447 .0056 1.1112 %RSD 132.25 104.1 59.134 #1 -.06602 .0109 .88947 #2 .26332 .0052. 3.0811 #3 .19847 -.0001 1.6666 Errors NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Units ppm ppm ppm Avge .0006 .0009 .0005 SDev .0001 .0001 .0003 %RSD 16.58 6.741 58.16 #1 .0006 .0009 .0009 z .0006 .0009 .0003 3 .0005 .0008 .0004 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge .0000 .0112 2.474 SDev .0002 .0059 .013 %RSD 647.3 53.03 .5263 #1 .0002 .0177 2.486 #2 .0000 .0095 2.476 #3 -.0001 .0063 2.461 Errors NOCHECK NOCHECK LC Pass H 2.750 High 2.250 Low Elem Sb2068 1960/1 1960/2 Units ppb ppb ppb Avge 10.455 3.3990 1.4357 SDev 5.229 3.7090 2.3027 %I2SD 50.013 109.12 160.39 41 16.488 .11499 .29806 4;2 7.6361 7.4218 4.0858 #3 7.2401 2.6601 -.07682 NOCHECK Errors NOCHECK NOCHECK 06/28/06 01:18:59 PM ' Operator: CO B PPM .0069 '.0016 23.71 .0086 .0069 .0053 NOCHECK Cu ppm .0015 .0001 5.572 .0016 .0014 .0016 NOCHECK Ni ppm -.0014 .0003 19.79 -.0011 -.0014 -.0016 NOCHECK Sn ppm -.0008 .0013 168.8 .0006 -.0020 -.0009 NOCHECK Fe PPM Ba ppm .0006 .0002 32.83 .0008 .0005 .0005 NOCHECK 2.417 .006 .2470 2.423 2.411 2.415 LC Pass 2.750 2.250 P ppm .0026 .0046 177.3 .0007 .0079 -.0007 NOCHECK T11908 ppb 2.3041 1.4581 63.285 3.8808 2.0270 1.0044 NOCHECK Be ppm .0005 .0001 30.81 .0006 .0005 ..0003 NOCHECK K ppm .0250 .0033 13.29 .0289 .0230 .0232 NOCHECK 2203/1 ppb .07082 1.7792 2512.2 1.7403 .27294 -1.soos NOCHECK V ppm .0007 .0003 39.66 .0010 .0006 .0005 NOCHECK page 1 Ca PPM .0274 .0027 9.867 .0303 .0270 .0250 NOCHECK Mg PPM .0047 .0029 62.78 .0037 .0080 .0023 NOCHECK 2203/2 ppb .23977 1.5873 662.04 1.0212 -1.5868 1.2849 NOCHECK Zn ppm -.0008 .0006ON 85.02 -.0000 -.0010 -.0013 NOCHECK Analysis Report nigh Low Elem Pb2203 Se1960 Units ppb ppb Avge .18392 2.0899 SDev 1.1159 2.7075 %RSD 606.74 129.55 #1 1.2611 .23750 #2 -.96711 5.1971 #3 .25776 .83498 Errors NOCHECK NOCHECK High Low 06/28/06 01:18:59 PM page 2 'tet O O H 06/28/06 01:29:38 PM page 1 Analysis Report hod: DVCLPI Sample Name:. CCB2 Operator: CO xun Time: 06/28/06 13:19:07 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm Ppm .0001 Ppm .0083 Avge .05966 -.0171 1.3094 1.1250 .0016 .0004 .0001 .0001 .0000 .0009 SDev %RSD .28353 475.22 .0022 12.71 85.917 28.17 58.25 43.17 10.75 #1 .04154 -.0156 1.5840 .0018 .0002 .0001 .0090 #2 -.21437 -.0160 .07254 .0018 .0001 .0001 .0086 .0073 #3 .35182 -.0196 2.2717 .0011 .0000 .0001 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .0200 .2000 -.2000 .0050 -.0050 .2000 -.2000 Low -10.000 -.2000 -10.000 -.0200 Elem Cd Co Cr Cu Fe - K Ppm Mg Ppm Units ppm PPm ppm Ppm Ppm -.0022 .0250 .0011 Avcge .0002 .0003 -.0002 .0021 .0003 .0012 .0038 .0020 SDev %RSD .0001 22.94 .0001 44.51 .0002 137.3 15.68 53.89 15.13 177.2 #1 .0002 -.0002 .0021 -.0009 .0272 -.0007 "2 .0002 .0003 .0005 -.0004 .0025 -.0025 .0271 .0008 3 .0002 .0003 .0001 .0018 -.0033 .0206 .0033 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 5.000 LC Pass High 0050 .0500 .0100 .0250 -.0250 .1000 -.1000 -5.000 .2000 -.2000 Low -.0050 -.05.00 -.0100 Na Ni P 2203/1 2203/2 Elem Mn Mo ppm ppm ppm PPb Ppb Units ppm ppm .0481 -.0013 .0059 .7320.4 -.59398 Avge -.0003 .0015 .000 .7347 SDev %RSD .0001 44.51 .0008 40.9 70885 1109072 10264 971464 2714313 #1 -.0002 .0022 .0521 -.0011 .0109 .30674 1.5557 -.70044 -.67510 #2 -.0003 .0010 .0477 -.0013 .0076 -.0008 .33364 -.40641 #3 -.0005 .0014 .0445 -.0014 LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK Errors High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn 1908 I1b V m Zn ppm Units ppb ppb ppb 1.2094 ppm -.0008 pp .08064 PP .0005 .0015 Avge -2.1664 2.9832 04 063 SDev 3.0493 494637 064 192282 15400? 423669 28056 2801 %RSD 140.75 #1 -1.1212 1.7712 -1.4787 .0006 3.0978 .0006 .0020 #2 -5.6008 2.5691 2.5089 -.0012 -3.6292 .0004 .0012 .0014 #3 .22282 4.6093 2.5981 . -.0016 .77332 .0004 NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Errors LC Pass Analysis Report nlgh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb Ppb Avge -.15202 1.8005 SDev .21654 1.9379 %RSD 142.44 107.63 #1 -.36466 -.39614 #2 .06821 2.5293 #3 -.15960 3.2682 Errors LC Pass LC Pass High 3.0000 5.0000 Low -3.0000 -5.0000 06/28/06 01:29:38 PM e 2 10.000 .0500 0200 -10.000 -.0500 - 02;,,0 page 1 Ca pprr 1 7 1 . -49 1.133 I., 172 Mg ppr", 32_1 10144 32 7 ._ _"7 22C -"3i2 ppb .55213 .15237 27.597 57594 .38926 .69120 Zn PPT' 0233 .000', . ? 06/28/06 01:40:17 PI'S Analysis Report hod: DVCLPI Sample Name: 0606916-006E Operator: CO Time: 06/28/06 13:29:46 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb Ppm Ppb -.41800 Ppm .0093 Ppm .0013 ppm .0001 Avge SDev .31760 .0722 .0028 1.15041 .0002 .0002 .0100,1 %RSD .31095 97.907 3.888 275.22 2.424 11.77 47.21 #1 .67462 .0726 .83459 .0096 .0015 .010i #2 .10610 .0693 -1.4273 .0091 .0012 .0001 #3 .17207 .0749 -.66127 .0093 .0013 .0000 Elem Cd Co Cr Cu Fe K Units ppm PPM Ppm Ppm Ppm .2081 Ppm 3.6"18 Avc�e .0001 0002 .0008 .0016 .0001 .0464. .0009 .0040 .05"t SDev1.47j- %RSD 313.7 .0003 38.52 3.093 1.966 1.915 1.471 #1 #1 -.0002 .0011 .0016 .0465 .2082 3.608 #2 .0005 .0016 .0454 .2040 3"570 #3 .0002 .0001 .0007 .0017 .0472 .2120 3.675 Elem Mn Mo Na Ni P 2203/1 ppb TTnits ppm PPM ppm 24.86 PPM .0032 Ppm 11.59 -1.0594 vge .0387 .0020 .0006 .34 .0005 .21 .5300 -Dev %RSD .0006 1.478 32.10 1.363 16.02 1.799 50.029 #1 .0386 .0026 24.76 .0031 11.53 -1.6677 #2 .0013 24.58 .0037 11.41 -.69710 #3 .0382 .0394 .0020 25.24 .0027 11.82 -.81342 Elem Sb2068 1960/1 1960/2 Sn T11908 V Units ppb ppb 7.7673 ppb -.21345 PPM -.0007 ppb -.92344 PPM .0006 Avge SDev 36739 9.7688 .99295 .0004 1.44074 .0004 0 -.RSD .03669 9.9880 125.77 465.18 54.82 156.02 65.66 #1. 18.829 .58925 -.0005 -1.8833 ,00111 #2 .39972 .32751 4.1487 .09420 -.0012 -1.6202 .0003 #3 .37493 .32403 -1.3238 -.0005 .73323 Elem Pb2203 Se1960 Units ppb ppb Avge .01590 2.4445 SDev .18101 3.8186 %RSD 1138.2 156.21 #1 -.17082 6.6635 #2 .02793 1.4447 #3 .19060 -.77469 page 1 Ca pprr 1 7 1 . -49 1.133 I., 172 Mg ppr", 32_1 10144 32 7 ._ _"7 22C -"3i2 ppb .55213 .15237 27.597 57594 .38926 .69120 Zn PPT' 0233 .000', . ? Analysis Report 06/28/06 01:50:57 PM page 1 aod: DVCLPI Sample Name: 0606916-007E Operator: CO xun Time: 06/28/06 13:40:25 Comment: KW --k S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb PPM Ppm Ppm PPM .9427 Avge .18797 .0097 -1.3452 1.1584 .0054 .0005 .0009 .0000 .0000 .0000 .0022 SDev %RSD .12892 68.587 .0026 27.20 86.116 8.772 .3592 124.1 .2331 #1 .0124 -1.1572 .0059 .0009 .0000 .9408 #2 .29145 .22890 .0095 -.29224 .0054 .0009 .0000 .9424 #3 .04355 .0071 -2.5860 .0049 .0009 .0000 .9451 Elem Cd Co Cr Cu Fe K Mg Units ppm. Ppm PPM PPM PPM .1998 PPM .2950 PPM .2108 Avge .0000 .0008 .0007 .0007 .0786 .0004 .0005 .0099 .0041 SDev %RSD .0001 552.1 .0003 38.23 108.1 .4870 .2608 3.344' 1.938 #1 .0001 .0005 .0008 .0786 .1993 .3034 .2155 #2 -.0001 .0009 .0013 .0782 .1999 .2975 .2842 .2082 .2087 #3 .0000 .0011 -.0001 .0790 .2003 Na Ni P 2203/1 2203/2 Elem --Zits Mn Mo PPM PPM PPM Ppb Ppb ppm PPM 15.88 .0026 .5235 1.0022 -.90868 Uge .0021 .0009 .07 .0009 .0053 .6659 2.36123 aDev %RSD .0001 3.561 .0003 31.98 .4593 33.40 1.014 66.441 259.85 #1 .0021 .0009 15.82 .0035 .5295 1.5170 1.2396 1.7803 -1.8630 #2 .0022 .0013 15.87 .0018 .5216 .25019 -2.6434 #3 .0020 .0007 15.96 .0025 .5194 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb Ppb Ppb PPM ppb 1.6553 PPM PP .0005 Pm .0248 Avge .86825 4.,1980 4.5043 2.8698 -.0012 .0009 .8789 .0003 .0005 SDev %RSD 1.3699 157.78 .8092 19.275 63.713 77.09 53.096 57.07 2.089 $#1 1.3903 3.3266 2.1783 -.0003 .66241 .0007 .0242 #2 1.9003 4.3417 7.7114 -.0021 1.9698 2.3337 .0006 .0002 .0250 .0252 43 -.68593 4.9256 3.6233 -.0012 Elem Pb2203 Se1960 Units ppb ppb Avge -.27192 4.4027 SDev 1.75399 2.0364 %R.SD 645.04 46.253 #1 1.6931 2.5611 #2 -.82943 6.5897 #3 -1.6794 4.0573 00 O O H Analysis Report 06/28/06 02:01:36 PM page 1 .hod: DVCLPI Sample Name: 0606916-008E Operator: CO Run Time: 06/28/06 13:51:04 Comment; Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM Ppb ppm Ppm PPM PPM Avge .02243 .0300 -2.8442 .0079 .0013 .0000 1.062 SDev _0033 .9923 .0006 .0000 .0000 .031 %RSD .03630 161.82 11.14 34.890 7.203 3.242 31.04 2.900 ##1 .04344 .0309 -3.8955 .0080 .0013 .0000 1.079 #2 -.01948 .0327 -1.9238 .0084 .0013 .0001 1.081 ##3 .04334 .0263 -2.7132 .0073 .0012 .0000 1.027 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM ppm PPM PPM PPM 1.106 ppm .2336 Avge .0001 .0009 .0011 .0001 .0433 .0014 .1854 .0055 .038 .0066 _SDev % RES D .0001 68.18 .0003 30.30 6.855 3.139 2.943 3.444 2.819 #1 .0000 .0006 .0011 .0441 .1890 1.119 .2355 #2 .0002 .00.11 .0011 .0441 .1881 1.136 .2391 #3 .0001 .0009 .0012 .0417 .1791 1.063 .2263 Elem Mn Mo Na Ni P 2203/1 2203/2 nits ppm PPM ppm 17..52 PPM ppm 3.235 Ppb .25695 Ppb -.06773 vge .0110 .0010 .53 .0013 .0003 .074 1.8989 1.05845 SDev %RSD .0004 3.564 .0005 46.14 3.022 22.67 2.281 739.01 1562.7 #1 .0112 .0005 17.76 .0011 3.283 2.3981 -.23649 $#2 .0112 .0014 17.88 .0016 3.271 -1.2228 1.0650 #3 .0105 .0012 16.91 .0011 3.150 -.40444 -1.0317 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb PPM Ppb Ppm ppm Avge -1.2119 1.4186 4.5613 -.0004 -1.5273 .0005 .0287 SDev 1.0351 2.7018 3.0460 .0013 1.3308 .0003 .0013 %RSD 85.409 190.46 66.779 329.9 87.133 51.71 4.624 #1 -2.1564 3.2697 1.0490 -.0018 -.90698 .0003 .0298 #2 -1.3739 2.6678 6.1562 .0009 -3.0550 .0004 .0290 #3 -.10536 -1.6818 6.4788 -.0003 -.61992 .0008 .0272 Elem Pb2203 Se1960 Units ppb Ppb Avge .04081 3.5152 SDev .76638 1.6172 %RSD 1877.9 46.006 #1 .64126 1.7889 #2 .30356 4.9949 #3 -.82238 3.7617 Analysis Report 06/28/06 02:12:16 Phi page 1 :hod: DVCLPI Sample Name: 0606916-009E Operator: CO Time: 06/28/06 14:01:44 Comment: IMW- 5 S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm PPM' pp`:. Avge -.10434 .0127 -.80088 .0061 .0011 .0000 1.093 SDev .25631 .0016 .61587 .0006 .0001 •0000 .4301 %RSD 245.64 12.27 76.899 8.965 7.051 131.5 _0538 #1 .17069 .0138 -.25402 .0066 .0010 .0000 1.093 #2 -.33654 .0134 -1.4680 .0063 .0011 -.0000 1.093 #3 -.14718 .0109 -.68060 .0055 .0010 .0000 1.094 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm PPM PPM PPM Ppm PPM Avge .0000 .0008 .0107 .0510 .2155 .3323 .2263 SDev .0002 .0007 .0001 .0008 .0008 .0032 %RSD .0001 763.6 24.95 6.5251953 .3721 .2469 1.406 #1 -.0001 .0010 .0099 .0511 .2151 .3332 .2250 #2 .0001 .0008 .0113 0509 .2151 .3-321 .2-300 - #3 .0001 .0006 .0108 .0511 .2165 .3317 22`x1 Elem Mn Mo Na Ni P 2203/1 .220,3;/2 TTnits ppm PPM PPM 16.82 PPM Ppm ppb -1.5859 Ppb .84886 vge .0022 .0006 .0001 .03 .0011 .0002 .5896 .0015 .8677 1.8554 _Dev %RSD .0001 3.530 20.23 .1877 17.42 .2635 54.710 218.58 #1 .0022 .0006 16.79 .0010 .5884 -.91827 rn�; -.685-8 #2 .0022 .0008 16.85 .0009 .5914 -1.2728 2.9109 #3. .0021 .0005 16.82 .0013 .5892 -2.5667 .32154 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb PPM Ppb PPM ppm Avge .71070 3.1034 -.23089 -.0015 .95580 .0005 .0208 SDev 1.1579 .8381 4.96823 .0006 3.8678 .0004 .0001 %RSD 162.92 27.006 2151.8 42.36 404.67 84.76 .6507 #1 -.61397 2.6138 -5.3385 -.0022 4.`9156 00 S-% 02`x' #2 1.5298 2.6252 4.5852 -.0011 .76485 0001 0 #3 1.2163 4.0711 .06064 -.0012 -2.8130 G' Elem Pb2203 Se1960 Units ppb ppb Avge .03851 .87980 SDev 1.2829 3.3415 %RSD 3331.1 379.80 #1 -.76278 -2.6900 #2 1.5181 3.9329 #3 -.63980 1.3965 Analysis Report 06/28/06 02:22:55 PM page 1 .hod: DVCLPI Sample Name: 0606916-010E Operator: CO ,,-,i Time: 06/28/06 14:12:23 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.06064 .0186 -.79232 .0072 .0013 .0001 1.076 SDev .19050 .0008 1.78144 .0003 .0001 .0001 .017 %RSD 314.15 4.356 224.84 4.548 3.998 126.7 1.534 #1 .10649 .0178 1.1211 .0075 .0013 .0000 1.085 #2 -.26806 .0185 -1.0950 .0072 .0012 .0002 1.085 #3 -.02035 .0194 -2.4030 .0068 .0013 .0000 1.057 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0023 .0134 .0476 .2429 .3772 .2319 SDev .0006 .0023 .0021 .0014 .0026 .0063 .0199 %RSD 176.6 102.8 15.40 3.044 1.079 1.656 8.571 #1 -.0001 .0006 .0121 .0465 .2434 .3793 .2228 ##2 .0010 .0049 .0158 .0492 .2452 .3822 .2547 #3 .0001 .0013 .0123 .0471 .2400 .3702 .2182 Elem Mn Mo Na Ni P 2203/1 2203/2 TTnitsppm ppm ppm ppm ppm ppb ppb vge .0027 .0012 17.52 .0029 .5862 -8.3355 4.6798 .0003 .0009 .15 .0013 .0142 12.1349 5.7663 _-Dev %RSD 11.04 76.10 .8680 43.51 2.420 145.58 123.22 #1 .0025 .0007 17.45 .0023 .5772 1.2421 1.5270 #2 .0030 .0022 17.42 .0044 .6025 -21.982 11.335 #3 .0025 .0006 17.70 .0021 .5788 -4.2666 1.1774 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 3.3915 -14.613 4.9889 -.0008 .19434 .0017 .0282 SDev 6.9977 19.168 5.9598 .0003 3.8628 .0020 .0015 %RSD 206.33 131.17 119.46 35.19 1987.6 115.7 5.279 #1 .08317 .82728 .93316 -.0010 -2.1848 .0007 .0282 #2 11.430 -36.066 11.832 -.0005 -1.8835 .0040 .0296 #3 -1.3386 -8.6003 2.2020 -.0008 4.6513 .0004 .0267 Elem Pb2203 Se1960 Units ppb ppb Avge .34615 -1.5382 SDev 1.0378 2.5113 %RSD 299.81 163.26 #1 1.4325 .89828 #2 .24097 -4.1181 #3 -.63505 -1.3948 06/28/06 02:33:35 PM page 1 Analysis Report hod: DVCLPI Sample Name: 0606916-011E Operator: CO xun Time: 06/28/06 14:23:03 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM ppb PPM PPM Ppm PPM 1.099 Avge -.25346 .0086 -2.2532 3.0369 .0073 .0013 .0000 .0000 .0000 .001 SDev %RSD .25669 101.28 .0014 16.22 134.78 .0005 7.044 1.305 99.29 .1142 #1 -.21165 .0102 -.17037 .0079 .0013 -.0000 1.099 #2 -.52849 .0078 -.85141 .0071 .0013 .0000 1.098 #3 -.02024 .0078 -5.7377 .0069 .0013 .0000 1.100 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM ppm PPM PPM .3705 PPM .2213 Avge .0000 .0009 .0008 .0487 .0003 .2078 .0001 .0038 .0036 SDev %RSD .0001 691.0 .0001 13.07 .0004 49.11 .5456 .0524 1.038 1.643 #1 -.0001 .0008 .0007 .0484 .2079 .3714 .2206 #2 .0002 .0009 .0011 .0490 .2077 .3663 .2252 #3 -.0000 .0010 .0004 .0488 .2078 .3738 .2180 Mo Na Ni P 2203/1 2203/2 Elem --nits Mn ppm ppm PPM ppm Ppb Ppb 1.2682 vie 0024 .0002 17.59 17.59 .0012 .5012 .0115 -1.3537 1.3882 1.0789 SDev .0000 .0002 127.6 .09 .5023 .0001 6.243 2.302 102.55 85.071 %RSD .3153 #1 .0004 17.67 .0012 .5070 -.01537 1.7299 #2 .0024 -.0000 17.60 .0013 .5087 -1.2589 .03531 #3 .0024 .0024 .0001 17.49 .0013 .4880 -2.7869 2.0394 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb PPM ppb -2.3566 PPM .0006 ppm .0293 Avge -.49123 4.5054 3.6513 1.0675 -.0023 .0012 .2591 .0001 .0003 SDev %RSD 1.64562 335.00 .4995 11.087 29.235 55.21 10.995 9.307 .9150 #1 .97897 4.7952 2.5856 -.0008 -2.6109 .0005 .0291 #2 -2.2689 3.9286 3.6479 -.0028 -2.3660 .0005 .0296 #3 -.18376 4.7923 4.7205 -.0031 -2.0929 .0006 .0292 Elem Pb2203 Se1960 Units ppb ppb Avge .39553 3.9361 SDev .77285 .7311 %RSD .195.40 18.575 #1 1.1491 3.3218 #2 -.39523 3.7418 #3 .43267 4.7448 Analysis Report 06/28/06 02:44:14 PM page 1 :hod: DVCLPI Sample Name: 0606916-012E Operator: CO L Time: 06/28/06 14:33:42 Comment: M W- b-k�> Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.12726 .0953 -2.0040 .0094 .0016 .0000 1.374 SDev .31968 .0046 1.8380 .0004 .0001 .0000 .017 %RSD 251.21 4.855 91.713 3.940 4.300 53.98 1.243 #1 -.28047 .0985 -.34905 .0094 .0016 .0000 1.379 #2 .24019 .0974 -3.9821 .0090 .0016 .0000 1.387 #3 -.34150 .0900 -1.6809 .0097 .0015 .0000 1.355 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0007 .0011 .0579 .2066 2.662 .3029 SDev .0001 .0001 .0001 .0008 .0026 .024 .0062 %RSD 55.34 8.122 8.716 1.411 1.263 .8997 2.048 #1 .0001 .0007 .0012 .0583 .20.67 2.677 .3009 #2 .0002 .0006 .0010 .0584 .2092 2.675 .3098 #3 .0002 .0007 .0011 .0570 .2040 2.634 .2979 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb sge .0263 .0004 22.99 .0023 7.576 .44968 .34196 Dev .0003 .0003 .16 .0004 .104 2.9430 1.8729 oRSD 1.092 56.89 .6934 15.83 1.372 654.47 547.70 #1 .0264 .0002 23.12 .0022 7.620 -2.9125 -.25033 #2 .0265 .0006 23.04 .0021 7.651 2.5588 2.4394 #3 .0260 0006 22.81 .0028 7.457 .1.7027 -1.1632 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge -1.9605 .63257 1.3846 -.0006 .12701 .0005 .1060 SDev .9089 7.5277 5.2608 .0003 2.5797 .0003 .0019 %RSD 46.360 1190.0 379.96 51.77 2031.1 51.00 1.753 #1 -2.9734 -7.8391 -4.4349 -.0007 -2.8517 .0005 .1061 #2 -1.6920 3.1836 2.7854 -.0009 1.6029 .0008 .1079 #3 -1.2161 6.5532 5.8032 -.0003 1.6299 .0003 .1042 Elem Pb2203 Se1960 Units ppb ppb Avge .37827 1.1346 SDev 1.8780 6.0126 %RSD 496.48 529.95 #1 -1.1364 -5.5681 #2 2.4796 2.9184 #3 -.20840 6.0534 M O O O Nt O O O H 06/28/06 02:54:54 PM page 1 Analysis Report .hod: DVCLPI Sample Name: 0606916-013E Operator: CO xurl Time: 06/28/06 14:44:22 Comment: kw-(&S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb PPM Ppb Ppm PPM Ppm .0000 Ppm 1.312 Avge -.01919 .0047 .75501 .0063 .0013 .. .0000 .002 SDev .41031 .0020 42.57 .68959 91.335 .0005 8.502 352 2.352 243.4 .1806 %RSD 2138.4 #1 -.45728 .0059 .41595 .0063 .0012 -.0000 1.309 1.314 #2 .04362 .0058 1.5485 .0069 .0013 .0000 1.312 #3 .35610 .0024 .30059 .0058 .0013 .0000 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm PPM PPM PPM PPM .5110 Ppm .2441 Avge .0001 .0008 .0003 .0562 .0003 .2071 .0002 .0106 .0042 SDev %RSD .0001 145.9 .0002 24.92 .0004 127.4 .5423 .0828 2.064 1.724 #1 .0006 -.0001 .0565 .2069 .5084 .2487 #2 .0000 -.0000 .0010 .0003 .0560 .2071 .5226 .2406 #3 .0002 .0008 .0008 .0560 .2073 .5020 .2429 Mo Na Ni P 2203/1 2203/2 Elem nits nit Mn ppm PPM PPM PPM PPM Ppb -1.6738 ppb .13551 .0027 0004 16.95 .0018 .5749 .0083 1.5769 1.8453 -Dev .0000 .0002 49.35 .03 .1540 .0004 19.54 1.452 94.207 1361.7 %RSD 1.542 #1 .0006 16.97 .0020 .5824 -1.5448 1.8297 #2 .0027 .0004 16.92 .0014 .5763 -3.3113 .40762 #3 .0028 .0027 .0002 16.95 .0021 .5659 -.16547 -1.8307 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb PPM PPb 1.0817 PPM .0007 PPM .0440 Avqe .19423 -1.2516 1.3198 1.6787 2.8400 -.0016 .0008 1.4805 .0001 .0003 SDev %RSD 1.8625 958.93 105.45 169.18 51.13 136.87 12.61 .5697 #1 -1.7489 -2.6559 1.5584 -.0009 -.60197 .0008 .0438 #2 1.9640 -1.0620 -1.0992 -.0025 1.6668 .0007 .0440 #3 .36750 -.03682 4.5770 -.0015 2.1802 .0006 .0443 Elem Pb2203 Se1960 Units ppb ppb Avge -.46657 .70330 SDev 1.03996 2.1176 %RSD 222.89 301.09 #1 .70641 .15539 #2 -.83035 -1.0865 #3 -1.2758 3.0410 Nt O O O H Analysis Report 06/28/06 03:05:33 PM page 1 :hod: DVCLPI Sample Name: 0606855-004CPDS Operator: CO Time: 06/28/06 14:55:01 Comment: C-zt,J - `15328, ^Ob����o^ O 1 `?DS Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm Ppm PPM Avge 18.807 .0771 25.387 .3150 .0084 .0099 46.05 SDev .151 .0017 1.272 .0018 .0000 .0000 .11 %RSD .80225 2.229 5.0084 .5728 .4822 .2643 .2486 #1 18.671 .0752 26.412 .3129 .0084 .0099 45.92 #2 18.969 .0785 25.786 .3159 .0084 .0099 46.12 #3 18.779 .0776 23.964 .3162 .0085 .0099 46.12 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0095 .0994 .0238 .0562 25.57 57.05 4.091 SDev .0001 .0003 .0003 .0001 .13 .09 .012 %RSD 1.509 .3152 1.267 .1532 .5065 .1535 .2871 #1 .0094 .0998 .0242 .0562 25.42 56.96 4.086 #2 .0096 .0991 .0237 .0563 25.65 57.07 4.083 #3 .0096 .0994 .0236 ..0562 25.64 57.13 4.105 Elem Mn Mo Na Ni P 2203/1 2203/2 TTnits ppm ppm PPM Ppm PPM Ppb Ppb vge .2417 .0037 49.52 .0759 7.711 6.6031 9.2454 .0011 .0004 .18 .0008 .052 .8950 .6307 _Dev %RSD .4375 11.33 .3580 1.105 .6805 13.555 6.8219 #1 .2405 .0042 49.39 .0763 7.650 5.5745 9.2470 #2 .2424 .0034 49.72 .0750 7.745 7.0304 9.8752 #3 .2421 .0036 49.45 .0765 7.736 7.2043 8.6138 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 116.01 12.174 12.740 -.0014 21.606 .1017 .0531 SDev 1.20 .874 1.248 .0008 2.599 .0003 .0005 %RSD 1.0361 7.1783 9.7958 61.09 12.027 .3350 .8613 #1 116.57 11.524 11.646 -.0004 21.497 .1013 .0531 #2 114.64 13.167 12.474 -.0018 24.258 .1017 .0526 #3 116.84 11.829 14.099 -.0019 19.064 .1020 .0535 Elem Pb2203 Se1960 Units ppb ppb Avge 8.3659 12.552 SDev .4908 .879 %RSD 5.8664 7.0035 #1 8.0245 11.606 #2 8.9283 12.705 #3 8.1449 13.344 Analysis Report 06/28/06 03:16:13 PM page 1 hod: DVCLPI Sample Name: CCV3 Operator: CO xun Time: 06/28/06 15:05:41 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb Ppm Ppm Ppm Ppm Avge 1014.6 52.26 532.34 2.601 2.565 2.591 52.70 SDev .5 .02 2.96 .007 .002 .005 .15 %RSID .04936 .0287 .55548 .2605 .0614 .1808 .2872 #1 1014.4 52.27 529.01 2.597 2.564 2.591 52.73 #2 1015.2 52.26 534.64 2.597 2.567 2.587 52.54 #3 1014.3 52.24 533.39 2.609 2.565 2.596 52.84 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 -55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM Ppm 2.568 Ppm 2.541 Ppm 52.99 PPM 78.60 Ppm 51.19 Avge 2.582 2.558 .003 .004 .04 .12 .05 SDev %RSD .004 .1378 .008 .3238 .1245 .1564 .0763 .1524 .0940 #1 2.583 2.553 2.569 2.539 53.02 78.55 51.22 "2 2.578 2.567 2.565 2.539 53.00 78.74 51.14 3 2.585 2.552 2.571 2.546 52.94 78.52 51.22 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm PPM PPM 78.49 Ppm 2.415 PPM Ppb 505.01 Ppb 494.34 Avge 2.578 2.597 .010 .0131 .0078 2.10 1.28 SDev %RSD .004 .1459 .011 .4078 .16 .2060 .4200 59.67 .41563 .25968 #1 2.581 2.588 78.47 2.415 .0193 506.94 494.37 #2 2.574 2.593 78.67 2.405 .0157 505.32 493.04 #3 2.579 2.608 78.35 2.425 .0043 502.78 495.60 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb PPM Ppb PPM PPM Avge 1033.3 544.44 523.90 2.600 510.52 2.589 2.554 SDev 5.9 5.10 3.13 .002 4.83 .004 .005 %RSD .56963 .93687 .59744 .0760 .94606 .1360 .2130 41 1027.0 549.85 526.53 2.600 510.38 2.591 2.559 �2 1034.4 539.72 520.44 2.602 505.76 2.585 2.548 }#3 1038.6 543.75 524.73 2.598 515.42 2.592 2.553 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 03:16:13 PM page 2 nigh 1100.0 Low 900.00 Elem Pb2203 Se1960 Units ppb ppb Avge 497.89 530.74 SDev .72 3.73 %RSD .14459 .70264 #1 498.56 534.30 #2 497.13 526.86 #3 497.99 531.06 Errors LC Pass LC Pass High 550.00 550.00 Low 450.00 450.00 550.00 2.750 450.00 2.250 2.750 2.250 Analysis Report 06/28/06 03:26:53 PM page 1 .hod: DVCLPl Sample Name: CCVL3 Operator: CO -.uil Time: 06/28/06 15:16:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm ppm Ppm ppm .0361 Avge -.06385 -.0027 .76042 1.0015 .0072 .0007 .0006 .0002 .0049 SDev %RSD .28257 442.52 .0056 208.2 131.71 .0012 16.99 .0002 35.67 33.50 13.51 #1 .0020 1.3915 .0086 .0008 .0008 .0398 #2 .26046 -.25698 -.0012 1.2842 .0068 .0008 .0007 .0379 #3 -.19504 -.0088 -.39440 .0062 .0004 .0004 .0306 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr 'Cu Fe K Mg Units ppm ppm ppm Ppm '.0028 ppm 2.411 ppm .0292 Ppm .0106 Avge .0007 .0011 .0012 .0002 .0001 .003 .0040 .0048 SDev %RSD .0003 43.18 .0001 11.45 18.50 4.106 .1117 13.76 45.02 #1 .0009 .0011 .0013 .0029 2.414 .0337 .0078 u2 .0011 .0012 .0029 2.411 .0258 .0161 3 .0009 .0004 .0009 .0009 .0027 2.409 .0282 .0078 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 2.250 Low Mo Na Ni P 2203/1 2203/2 Elem Units Mn ppm ppm Ppm Ppm ppm Ppb ppb Avge .0002 .0103 2.441 -.0010 .0121 -2.6766 2.3462 .61294 .54793 SDev .0002 .0055 52.85 .019 .0006 62.25 .0135 111.5 87.657 89.394 %RSD 135.4 .7770 #1 .0163 2.450 -.0008 .0011 -.01063 .52351 #2 .0002 .0092 2.453 -.0005 .0271 -3.5922 .11523 #3 .0004 -.0001 .0055 2.419 -.0017 .0080 -4.4270 1.2001 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb Ppb ppb Ppm ppb Ppm Ppm Avge 7.2204 7.8349 5.7796 .0009 2.5427 .0010 .0019 SDev 5.4391 3.2321 1.2702 .0005 1.1685 .0004 .0006 %RSD 75.330 41.253 21.977 55.45 45.957 35.95 33.10 #1 13.491 4.1381 5.2820 .0005 3.7290 .0010 .0021 #2 4.3883 10.127 4.8336 .0008 1.3928 .0014 .0023 #3 3.7817 9.2398 7.2233 .0014 2.5061 .0006 .0012 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report .v,�gh Low Elem Pb2203 Se1960 Units ppb ppb Avge -.48206 6.4644 SDev .75096 1.5012 %RSD 155.78 23.223 #1 .34604 4.9014 #2 -1.1189 6.5966 #3 -.67333 7.8952 Errors NOCHECK NOCHECK High Low 06/28/06 03:26:53 PM page 2 O O O Analysis Report 06/28/06 03:37:33 PM page 1 hod: DVCLPI Sample Ndme: CCB3 Operator: CO rcuii Time: 06/28/06 15:27:01 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm PPM PPM Ppm Avge .12604 -.0249 .15028 .0018 .0001 .0001 .0096 SDev .0026 1.7331 .0007 .0001 .0000 .0003 %RSD .28503 226.14 10.40 1153.3 38.25 105.2 33.79 3.587 #1 -.14787 -.0230 -.91792 .0021 .0001 .0001 .0100 #2 .10497 -.0278 2.1499 .0024 .0000 .0001 .0096 #3 .42103 -.0238 -.78117 .0010 .0000 .0001 .0093 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .0200 .2000 .0050 .2000 Low -10.000 -.2000 .-10.000 -.0200 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm PPM PPM PPM -.0020 PPM .0228 PPM .0003 Avge .0002 .0001 -.0006 .0005 .0029 .0005 .0013 .0063 .0016 SDev %RSD .0000 10.88 .0001 41.77 85.87 16.09 63.15 27.37 614.8 #1 .0002 .0001 -.0001 .0026 -.0006 .0203 -.0007 '12 .0002 -.0011 .0026 -.0026 .0182 -.0006 3 .0002 .0002 .0001 -.0005 .0034 -.0029 .0299 .0021 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm PPM PPM PPM -.0015 PPM Ppb .57824 Ppb -1.3596 Avge -.0004 .0017 .0524 .0029 .0001 .0111 .0143 1.4650 1.5092 SDev %RSD .0000 11.30 .0008 44.37 5.529 6.665 129.3 253.36 111.00 #1 -.0004 .0025 .0558 -.0015 .0269 -1.0243 -1.2006 #2 -.0003 .0010 .0508 -.0014 -.0008 .91009 .06373 #3 -.0004 .0015 .0507 -.0016 .0070 1.8489 -2.9420 Errors LC Pass NOCHECK LC Pass LC.Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb Ppb PPM Ppb PPM PPM Avge -2.9326 -.92845 -.95946 -.0029 2.4795 .0003 .0010 SDev 1.0790 3.15198 2.76953 .0006 1.3592 .0004 .0003 %RSD 36.793 339.49 288.65 22.26 54.816 140.8 35.55 1#1 -3.4262 1.0422 .68980 -.0027 2.9504 .0004 .0006 R2 -3.6766 -4.5638 .58873 -.0023 .94750 -.0002 .0012 43 -1.6951 .73625 -4.1569 -.0035 3.5405 .0007 .0012 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass 0 O O V) H Analysis Report ri.igh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb Ppb Avge -.71391 -.94875 SDev .92360 1.67442 %RSD 129.37 176.49 #1 -1.1415 .80752 #2 .34600 -1.1267 #3 -1.3462 -2.5271 Errors LC Pass LC Pass High 3.0000 5.0000 Low -3.0000 -5.0000 06/28/06 03:37:33 PM page 2 10.000 .0500 .0200 -10.000 -.0500 -.0200 Analysis Report hod: DVCLPI Sample Name: CRIF xun Time: 06/28/06 15:37:41 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge 19.626 -.0228 21.136 SDev .346 .0034 .817 %RSD 1.7631 14.81 3.8662 #1 19.588 -.0192 22.068 #2 19.300 -.0234 20.545 #3 19.989 -.0258 20.793 Elem Cd Co Cr Units ppm PPM ppm Avge .0111 .1068 .0214 SDev .0002 .0017 .0007 %RSD 1.630 1.605 3.342 #1 .0110 .1066 .0206 #2 .0110 .1051 .0216 #3 .0113 .1086 .0220 Elem Mn Mo Na "nits ppm ppm ppm vge .0311 .0280 .0404 -Dev .0002 .0001 .0014 %RSD .7137 .4011 3.411 #1 .0309 .0279 .0417 #2 :0310 .0281 .0406 #3 .0313 .0279 .0390 Elem Sb2068 1960/1 1960/2 Units ppb ppb ppb Avge 126.06 15.752 13.813 SDev 4.26 3.141 5.601 %RSD 3.3798 19.938 40.548 #1 122.88 15.124 15.948 #2 124.39 12.973 7.4585 #3 130.90 19.160 18.032 Elem Pb2203 Se1960 Un i. t s ppb ppb Avge 4.5887 14.459 SDev .9530 4.676 %RSD 20.768 32.341 #1 4.4329 15.674 #2 3.7232 9.2953 #3 5.6100 18.408 06/28/06 03:48:13PM page 1 Operator: CO B Ba Be Ca Ppm PPM ppm ppm .2008 .0001 .0108 .0170 .0018 .0000 .0001 .0008 .9185 38.04 .7336 4.849 .2014 .0001 .0108 .0169 .1987 .0001 .0107 .0179 .2022 .0001 .0109 .0162 Cu Fe K Mg PPM PPM PPM PPM .0545 -.0015 .0241 -.0034 .0010 .0002 .0098 .0014 1.817 16.28 40.75 41.83 .0544 -.0013 .0352 -.0020 .0536 -.0014 .0164 -.0034 .0555 -.0018 .0208 -.0048 Ni P 2203/1 2203/2 PPM PPM ppb ppb .0795 .0085 5.1063 4.3296 .0009 .0053 2.5191 .9735 1.169 62.10 49.333 22.486 .0805 .0093 -6.7225 3.2892 .0786 .0134 2.2038 4.4811 .0793 .0029 6.3927 5.2185 Sn T11908 V Zn PPM ppb ppm ppm .0822 22.340 .1064 .0460 .0008 2.861 .0009 .0003 .9231 12.806 .8781 .5844 .0827 25.639 .1060 .0458 .0813 20.833 .1056 .0463 .0826 20.548 .1074 .0459 Analysis Report 06/28/06 03:58:53 PM page 1 hod: DVCLPI Sample Name: ICSAF Operator: CO Time: 06/28/06 15:48:21 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .74889 538.1 -2.2748 .0482 .0007 .0002 529.0 SDev .34142 .3 2.0102 .0005 .0000 .0000 1.3 %RSD 45.591 .0582 88.369 1.030 5.603 8.845 .2381 #1 .36399 538.0 -1.3486 .0477 .0007 .0002 528.1 #2 .86747 537.8 -.89464 .0483 .0007 .0002 528.5 #3 1.0152 538.4 -4.5811 .0487 .0007 .0002 530.5 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0013 .0026 .0067 .0013 212.1 .0065 533.8 SDev .0001 .0005 .0003 .0004 .1 .0084 .7 %RSD 11.97 17.93 4.038 33.25 .0523 128.8 .1370 #1 .0012 .0023 .0067 .0011 212.0 .0015 533.2 4,)0014 .0025 .0070 .0017 212.1 .0018 533.6 3 .0012 .0032 .0065 .0010 212.2 .0162 534.6 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni P 2203/1 2203/2 Unitas ppm ppm ppm ppm ppm ppb ppb Avge .0087 .0005 .0153 .0019 .0012 -4.1430 -.44850 SDev .0001 .0006 .0009 .0007 .0181 3.3157 4.94983 %RSD .9390 106.7 6.140 34.15 1570. 80.033 1103.6 #1 .0087 -.0001 .0154 .0014 .0072 -.61038 -6.1608 #2 .0086 .0007 .0161 .0027 -.0192 -7.1878 2.2413 #3 .0086 .0010 .0143 .0017 .0155 -4.6307 2.5740 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 8.3160 2.5816 1.2783 -.0109 H19.286 .0042 .0032 SDev 2.4947 10.476 4.0034 .0010 5.907 .0003 .0011 0 -.RSD 29.999 405.80 313.18 8.811 30.629 6.818 35.93 41 8.2762 7.9533 5.7947 -.0098 H23.729 .0040 .0039 2 5.8414 -9.4908 -1.8339 -.0115 H21.547 .0040 .0018 3 10.830 9.2823 -.12583 -.0114 H12.583 .0045 .0038 Errors LC Pass NOCHECK NOCHECK NOCHECK LC High LC Pass LC Pass Analysis Report —gh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb ppb Avge -1.6783 1.7128 SDev 2.3432 5.5628 %RSD 139.62 324.78 #1 -4.3120 H6.5140 #2 -.89809 -4.3832 #3 .17532 3.0076 Errors LC Pass LC Pass High 6.0000 5.0000 Low -6.0000 -5.0000 06/28/06 03:58:53 PM page 2 10.000 .0500 .0200 -10.000 -.0500 -.0200 06/28/06 04:09:33 PM page 1 Analysis Report hod: DVCLPI Sample Name: ICSABF Operator: CO xun Time: 06/28/06 15:59:01 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm ppm ppm 534.6 Avge 1095.8 543.7 1102.8 1.146 .5361 .5373 •8 SDev .6 1.2 4.3 .38923 .001 .1304 .0006 .1063 .0005 .0869 .1497 %RSD .05583 .2147 #1 1096.4 545.0 1098.4 1.144 .5361 .5379 535.5 #2 1095.2 543.2 1107.0 1.147 .5355 .5372 534.2 #3 1095.8 542.8 1102.8 1.146 .5367 .5370 534.0 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 600.0 High 1200.0 600.0 1200.0 1.200 .6000 .6000 400.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm Ppm ppm 213.6 ppm .0072 ppm 538.3 Avge 1.016 .5044 .5348 .5463 .5 .0066 .6 SDev .002 .0009 .0013 .2416 .0009 .1682 .2178 91.73 .1135 %RSD .1921 .1696 #1 1.018 .5054 .5358 .5455 214.1 .0142 539.0 "2 1.016 .5039 .5352 .5461 213.6 .0064 538.2 3 1.014 .5040 .5333 .5473 213.2 .0010 537.7 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 400.0 Low .8000 .4000 .4000 .4000 160.0 Na Ni P 2203/1. 2203/2 Elem Mn Mo ppm ppm ppm Ppb ppb Unitsppm 5382 ppm 1.042 .0090 .9296 .0090 1008.4 973.48 Avge SDev .0006 .004 .0019 .0044 .0169 9.6 5.08 %RSD .1024 .3918 21.21 .4699 188.1 .95218 .52149 #1 1.039 .0108 .9289 .0141 1012.1 971.37 #2 .5388 1.040 .0091 .9257 .0227 1015.6 969.80 #3 .5382 .5377 1.047 .0070 .9343 -.0099 997.50 979.27 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb 1042.5 ppm Ppm .9969 Avge 5.1575 1104.6 1078.5 1.071 4.7 .5364 SDev .6042 6.3 10.5 .008 .7371 .45086 .0005 .0893 .0011 .1150 %RSA 11.715 .57345 .97520 #1 4.9200 1110.6 1066.6 1.077 1037.7 .5369 .9979 {$2 5.8444 1105.3 1082.7 1.074 1047.1 .5362 .9972 43 4.7082 1098.0 1086.3 1.062 1042.6 .5360 .9957 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 04:09:33 PM page 2 1200.0 .6000 1.200 Hugh 800.00 .4000 .8000 Low Elem Pb2203 Se1960 Units ppb ppb Avge 985.11 1087.2 SDev .21 5.2 %RSD .02124 .47714 #1 984.94 1081.2 #2 985.05 1090.2 #3 985.34 1090.2 Errors LC Pass LC Pass High 1200.0 1200.0 Low 800.00 800.00 Analysis Report 06/28/06 04:20:12 PM page 1 hod: DVCLPI Sample Name: CCV4 Operator: CO Time: 06/28/06 16:09:40 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1003.9 51.40 526.11 2.556 2.541 2.572 52.36 SDev 11.2 .57 4.93 .028 .028 .025 .47 %RSD 1.1175 1.112 .93799 1.077 1.117 .9578 .9031 #1 1013.3 51.83 528.98 2.575 2.564 2.591 52.75 #2 991.47 50.75 520.42 2.524 2.509 2.544 51.83 #3 1007.0 51.63 528.95 2.567 2.549 2.581 52.50 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.551 2.538 2.545 2.503 52.38 77.75 50.70- SDev .024 .019 .025 .031 .48 .90 .51 %RSD .9567 .7472 .9808 1.243 .9199 1.156 1.009 #1 2.571 2.560 2.565 2.529 52.74 78.55 51.15 #2 2.524 2.528 2.517 2.468 51.83 76.78 50.14 2.557 2.527 2.552 2.512 52.56 77.94 50.81 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb Avge 2.550 2.572 77.19 2.374 .0099 499.88 488.51 SDev .026 .022 .77 .025 .0053 7.95 7.12 %RSD 1.010 .8639 .9978 1.033 53.78 1.5903 1.4571 #1 2.569 2.588 77.57 2.396 .0161 507.46 496.35 #2 2.521 2.547 76.31 2.348 .0069 500.57 482.45 #3 2.560 2.582 77.70 2.379 .0068 491.61 486.74 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge 1021.6 539.13 518.24 2.563 515.92 2.565 2.515 SDev 11.4 12.71 4.16 .023 3.66 .026 .024 %RSD 1.1143 2.3574 .80209 .9155 .71036 .9948 .9424 #1 1021.3 548.20. 522.05 2.581 519.94 2.585 2.535 1010.4 544.58 513.81 2.537 512.76 2.536 2.489 3 1033.2 524.60 518.85 2.572 515.06 2.573 2.522 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report 06/28/06 04:20:12 PM page 2 —gh 1100.0 Low 900.00 Elem Pb2203 Se1960 Units ppb ppb Avge 492.30 525.19 SDev 6.71 5.09 %RSD 1.3639 .97001 #1 500.05 530.76 #2 488.48 524.05 #3 488.36 520.76 Errors LC Pass LC Pass High 550.00 550.00 Low 450.00 450.00 550.00 2.750 450.00 2.250 2.750 2.250 Analysis Report :hod: DVCLPI Sample Name: CCVL4 �LL�z Time: 06/28/06 16:20:20 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge .05405 .0050 1.6163 SDev .63615 .0077 .6644 %RSD 1176.9 152.5 41.109 #1 -.67958 .0069 2.1429 #2 .38885 .0116 .86976 #3 .45288 -.0034 1.8361 Errors NOCHECK NOCHECK NOCHECK High Low Elem Cd Cc Cr Units ppm ppm ppm Avge .0007 .0005 .0005 SDev .0001 .0004 .0004 %RSD 13.76 88.52 76.01 #1 .0007 .0001 .0001 42 .0008 .0003 .0008 :3 .0006 .0009 .0007 Errors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo ppm .0108 .0048 44.64 .0161 .0099 .0065 NOCHECK 1960/1 ppb 4.0898 7.1062 173.76 -.99039 12.210 Na ppm 2.429 .055 2.255 2.493 2.395 2.401 LC Pass High 2.750 Low 2.250 1960/2 ppb 2.3009 5.4397 236.42 8.3799 .63073 -2.1079 Errors NOCHECK NOCHECK NOCHECK 06/28/06 04:30:52 PM Operator: CO B ppm .0074 .0009 12.50 0084 0071 0066 NOCHECK Cu ppm .0026 .0004 13.71 .0023 .0030 .0026 NOCHECK Ni ppm -.0014 0003 23.59 -.0017 -.0010 -.0015 NOCHECK Sn ppm .0007 .0007 91.87 .0000 .0014 .0009 NOCHECK Ba ppm .0005 .0001 32.62 .0004 .0006 .0004 NOCHECK Fe PPM 2.493 .004 .1500 2.489 2.496 2.493 LC Pass 2.750 2.250 P ppm -.0032 .0024 76.70 -.0024 -.0059 -.0012 NOCHECK T11908 ppb -.92409 4.44435 480.94 -5.8757 .38406 2.7194 NOCHECK Be ppm .0005 .0001 28.23 .0006 .0005 .0003 NOCHECK K ppm .0207 .0211 102.3 -.0027 .0384 .0263 NOCHECK 2203/1 ppb -.77794 .47916 61.594 -.22717 -1.0077 -1.0990 NOCHECK v ppm .0007 .0001 14.21 .0006 .0007 .0008 NOCHECK page 1 Ca ppm .0463 .0083 17.84 .0507 .0515 .0368 NOCHECK Mg ppm .0209 .0071 33.88 .0194 .0286 .0147 NOCHECK 2203/2 ppb .98510 .84324 85.599 .83338 1.8939 .22803 NOCHECK Zn ppm -.0008 .0003 44.95 -.0010 -.0010 -.0004 NOCHECK Analysis Report ...ugh Low Elem Pb2203 Se1960 Units ppb ppb Avge .39845 2.8970 SDev .57519 3.4453 %RSD 144.36 118.93 #1 .48064 5.2600 #2 .92811 4.4871 #3 -.21342 -1.0562 Errors NOCHECK NOCHECK High Low 06/28/06 04:30:52 PM page 2 Analysis Report 06/28/06 04:41:32 PM page 1 :hod: DVCLPI Sample Name: CCB4 Operator: CO ...::.i Time: 06/28/06 16:31:00 Comment: Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge' -.08346 -.0194 .64332 .0018 .0001 .0001 .0113 SDev .18997 .0011 2.2301 .0010 .0001 .0000 .0023 %RSD 227.61 5.715 346.65 56.07 61.99 30.38 20.10 #1 -.07993 -.0207 .34642 .0027 .0001 .0001 .0138 #2 -.27518 -.0191 -1.4234 .0019 .0002 .0001 .0106 #3 .10472 -.0185 3.0070 .0007 .0000 .0001 .0095 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .0200 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.0200 -.2000 -.0050 -.2000 Eleni Cd Co - Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0001 -.0006 .0022 -.0016 .0113 .0060 SDev .0001 .0002 .0003 .0004 .0013 .0045 .0014 %RSD 21.19 145.0 44.01 20.81 81.56 39.47 22.71 #1 .0002 -.0000 -.0007 .0017 -.0003 .0084 .0058 42 .0004 .0004 -.0008 .0025 -.0015 .0165 .0048 3 .0003 .0001 -.0003 .0023 -.0029 .0091 .0075 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni P 2203/1 2203/2 Units ppm ppm ppm ppm ppm ppb ppb Avge -.0003 .0018 .0304 -.0015 .0067 -.32784 -.34734 SDev .0000 .0001 .0011 .0002 .0061 .73054 2.24985 %RSD 11.01 7.421 3.582 14.44 91.07 222.83 647.73 #1 -.0003 .0019 .0310 -.0015 .0106 .41494 -2.2570 #2 -.0003 .0016 .0310 -.0017 -.0003 -.35298 2.1329 #3 -.0004 .0019 .0291 -.0012 .0098 -1.0455 -.91793 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem Sb2068 1960/1 1960/2 Sn T11908 V Zn Units ppb ppb ppb ppm ppb ppm ppm Avge -1.5156 3.8554 .34419 -.0021 1.1593 .0005 .0010 SDev 1.3046 4.4557 .42155 .0014 2.1827 .0002 .0008 %RSD 86.077 115.57 122.48 67.47 188.29 38.02 80.21 #I -3.0130 8.3396 .78118 -.0017 .67922 .0004 .0002 2 -.90874 3.7979 -.06000 -.0009 3.5421 .0007 .0009 .3 -.62496 -.57116 .31139 -.0036 -.74350 .0004 .0018 Errors LC Pass NOCHECK NOCHECK NOCHECK LC Pass LC Pass LC Pass Analysis Report —gh 60.000 Low -60.000 Elem Pb2203 Se1960 Units ppb ppb Avge -.34044 1.5138 SDev 1.43987 1.6593 %RSD 422.95 109.61 #1 -1.3668 3.2985 #2 1.3055 1.2251 #3 -.96002 .01789 Errors LC Pass LC Pass High 3.0000 5.0000 Low -3.0000 -5.0000 06/28/06 04:41:32 PM page 2 10.000 .0500 .0200 -10.000 -.0500 -.0200 U2M "US., 1 N C. IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE it N l f'. H2 C -as., inc. CLP Digestion Loi . jient: �l 1 Analyst Signature:_*LkL SDG #: S L nMo Date: Matrix: C Time Started/Ended: 1 O .(on 19 o. Method: . Description Sample ID # Lab # Dig Type Initial VoI/Wt Final Comments: PH:_ G 2,- I / IUMC/BOOKS/Cl-Migestionlog 'Description of colors: red, blue, yellow, green, orange, violet, Vol. Spike Sol Lot # Volume Before After AQP T 5-D.DmL SD.omL Colones C' (e- M ►—tD D 3S — S - h�Mvini+� sa�5 0.5mL D COS,'- �D S LCS-ni Y�U Comments: PH:_ G 2,- I / IUMC/BOOKS/Cl-Migestionlog 'Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. 'Description of texture: fine, medium, coarse. `Description of clarity: clear,:cloudy, opaque_ `Description of artifacts: yes or no and describe P 0165 U2/4 "US -9 INC. SDG NO.:-MLO(D(o SCAN: t -t ET0LS This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature Date: ReviE Date: