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Home My WebLink AboutMetals Data Package 03/2006IH2M ILAI3S9 INC. rSLOOS METAL TABLE OF CONTENTS I. REPORTS II. QC SUMMARY III. RAW DATA IV. DOCUMENTATION U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. SOW No.: ILM04.1 EPA Sample No. EQPT MW -1D MW -1S MW -3D MW -3S MW -4D MW -4S MW -5D MW -5S MW-5SD MW-5SS MW -6D MW -6S MW -8D MW -BS Were ICP interelement corrections applied? Were ICP background corrections applied? If yes -were raw data generated before application of background corrections? Comments: Date Reported_ 3/29/06 Contract: SAS No.: SDG No.: TSL005 Lab Sample ID. 0603561-001 0603561-002 0603561-003 0603561-004 0603561-005 0603561-006 0603561-007 0603561-008 0603561-009 0603561-009DUP 0603561-009MS 0603561-010 0603561-011 0603561-012 0603561-013 Yes/No YES Yes/No YES Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the condition detailed above. Release of the data contained in this hardcopy data package and i the computer -readable data submitted on diskette has been authorized byhe Laboratory Manager or the Manager's designee, as verified by the follow'ng[III ign Signature: A# kA-4-iATANA) Name: Vincent Stan(-amniAnn Date: Title: Vice President COVER PAGE - IN ILM04.1 U2M "US, 1NG REPORTS FOR METALS U2AA LABS, INC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO Q M INORGANIC ANALYSIS DATA SHEET 21.0 B P Lab Name: H2M LABS, INC. Contract: U EQPT Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-001 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 P 7440-42-8 7440-43-9 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 21.0 B P 7440-36-0 Antimony 2.9 U P 7440-38-2 Arsenic 1.8 U P 7440-39-3 Barium1.5 U P 7440-41-7 Beryllium_ 0.23 U P 7440-42-8 7440-43-9 Boron Cadmium 2.2 0.12 B U P P 7440-70-2 Calcium 68.5 B P 7440-47-3 Chromium 1.2 B P 7440-48-4 _ Cobalt —1.2—U P 7440-50-8 Copper 0.96 U P 57-12-5 Cyanide 10.0 U CA 7439-89-6 Iron 17.8 U P 7439-92-1 Lead 1.1 U P 7439-95-4 Magnesium 20.3 B P 96-5 Manganese 3.4 B P 97-6 Mercury 0.10 U Cv 02-0 V Nickel 1.0 U P 09-7 Potassium 162 B P 9-2 7440-22-4 Selenium _ Silver _ 1.9 0.45 U U P P 7440-23-5 Sodium 118 B P 7440-28-0 Thallium 2.4 U P 7440-62-2 Vanadium__ 1.4 U P 7440-66-6 Zinc 13.81 BI P Color Before_ COLORLESS Clarity Before: Color After: COLORLESS Clarity After: Comments: Date Reported: 3/29/06 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID Level (low/med): LOW Date Received % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 41.6 B P 7440-36-0 Antimony 2.9 U p 7940-38-2 Arsenic 1.8 U P 7440-39-3 Barium_ 14.7 B P 7940-41-7 7990-92-8 7990-43-9 Beryllium_ Boron Cadmium —.—_- -- 0.23 0.15 U B P P 7440-70-2 Calcium _ 3730 B P Chromium 2.7 B P t40-47-3 0-48-4 jCobalt 1.4 B P. 7440-50-8 ICopper 2.8 B p 57-12-5 Cyanide 10.0 U CA 7439-89-6 Iron 97.1 B P 7439-92-1 Lead 1.1 U P 7439-95-4 Magnesium 1120 B P 7439-96-5 Manganese 357 P 7939-97-6 Mercury 0.10 U CV 7440-02--0 Nickel _ 1.6 B P 7_440-09-7 Potassium 12500 _ P 7782-49-2 Selenium 1.9 U P 7440-22-4 Silver 0.45 U P 7_440-23-5 Sodium 14500 P 7440-28-0 Thallium 2.4 U P 7940-62-2 Vanadium 1.4 U P 7940-66-6 Zinc 31.4 p Color Before: COLORLESS Clarity Before Color After: COLORLESS Clarity After: Comments: Date Reported:_3/29/06 EPA SAMPLE NO MW -1D SDG No.: TSL005 0603561-002 3/16/2006 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L No. V Analyte 1 EPA SAMPLE NO Q M INORGANIC ANALYSIS DATA SHEET T—_ 30.1 2.9 - - ^- -- - 1.8 B U U. -P p ---- P Lab Name: H2M LABS, INC. Contract: B MW -1S Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-003 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L No. V Analyte Concentration C Q M -90-5 ----- -- - 17440-36-0 7440-38-2 Aluminum Antimony Arsenic T—_ 30.1 2.9 - - ^- -- - 1.8 B U U. -P p ---- P 7440-39-3 Barium----- ------ -- 14.5 B P 7440-41-7 Beryllium 0d.O U P 7440-42-8 Boron 4B p 7440-43-9 Cadmium 0U P 7440-70-2 Calcium 3B P 7440-47-3 Chromium B p 7440-48-4 Cobalt 1.2 B p 7440-50-8 Copper 3.3B P 57-12-5 Cyanide 10.0 U CA 7439-89-6 Iron 47.2 B _ P 7439-92-1 !7439-95-4 :_ - _...------- 7439-96-5 7439-97_-6 Lead ,Magnesium - - Manganese Mercury 1.1 1080 . ------------ - _ 346 0.10 B B -- U p -- P P CV 7440-02-0 Nickel 1.6 B P 7440-09-7 Potassium _ 12200 P 7782-49-2 _ Selenium 1.9 U P 7440-22-4 Silver 0.45 U P 7440-23-5 Sodium 14100 P 7440-28-0 Thallium _ 2.4 U p 7440-62-2 Vanadium 1.4 U P 7440-66-6 Zinc 37.7 p Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date ed: 3/29/06 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L 1 CAS No. r Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 50.0 B P- Lab Name: H2M LABS, INC. Contract: U MW -3D Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water) : WATER Lab Sample ID: 0603561-004 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L 1 CAS No. r Analyte concentration c Q M 7429-90-5 Aluminum 50.0 B P- 7440-36-0 Antimony 2.9 U P 7440-38-2 Arsenic 1.8 U P 7440-3-9-3 Barium 41.9 B P 7_440-41-7 Beryllium 0.23 U P 7440-42-8 Boron 82.7 B P 17440-43-9 Cadmium 0.12 U P .7440-70-2 Calcium 10500 P 40-47-3 '7440-48-4 Chromium Cobalt 3.5 3.6 B B P P i7440-50-8 57-12-5 Copper Cyanide 6.0 10.0 B U P CA '7439-89-6 Iron 75.4 B P 7939-92-1 Lead 1.4 B P 7439-95-4 Magnesium 2870 B P 7939-96-5 Manganese 1070 P 7439-97-6 743 9- 9 7 - 6 - Mercury 0.10 U Cv 7440-02-0 7 E 0 44 0-0 E2 Nickel 4.1 B P 7440-09-7 744 0-0 9 - 7 Potassium 8860 P 7782-49-2 Selenium 1.9 U P 7440-22-4 Silver--_- 0.45 U P 7440-23-5 17440-28-0 Sodium Thallium 5030 2.6 B P P 17440-62-2 7940-66 -6 Vanadium Zinc 1.4 26.3. U P P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04. 1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET — Lab Name: H2M LABS, INC. Contract: MW -3S Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-005 Level (low/med): LOW Date Received: 3/16/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7929-90-5 Aluminum 72.4 B P 7940-36-0 Antimony 2.9 U P 7440-38-2 Arsenic 1.8 U P 7440-39-3 Barium 47.0 B P 7440-41-7 Beryllium_ 0.23 U P 7440=42-8 Boron 89.7 B P 7440-_43-9__cadmi_um 7440-70-2Cal 7440-47-3 7440-48-4 I cium Chrom Chromium _ Cobalt _ _ _ _ 0.24 11800 2,q _ 2.4 B B_ _ B P p p P 7440-50-8 Copper _ 2.7 B P 57-12-5 Cyanide _ 10.0 U CA 7439-899=6 Iron _ 92.6 B P 7939-92-1 Lead 1.1 U P 7939-95-9 Magnesium _ 3220 B P 743_9_-96-5 Manganese _ _ 1150 P 743_9-97-6 Mercury 0.10 U CV 7440-02-0 INickel 3.6 B P _ 7440-_09-7 !Potassium_ --- —+- -- 7782-49-2 JSeAenium 9900 -- 1.9 U P P 7990-22-9 7440-23-5 Silver Sodium 0.45 U P P 7490-28-0 Thallium _5440 2,4 U p 7440-62-2 Vanadium 1.9 U P 7440-66-6 Zinc 39.8 P Color Before_ COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L 1 EPA SAMPLE NO No. INORGANIC ANALYSIS DATA SHEET C Q M ACAS Lab Name: H2M LABS, INC. Contract: MW -4D Lab Code: 10478 Case No. SAS No.: � SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-006 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04.1 No. Analyte Concentration C Q M ACAS 17929-90-5 Aluminum 117 B P 7_940-36-0 Antimony — 2.9 U p 7490-38-2 Arsenic U P 17440-39-3- Barium - -------51.4 B P 17440-41-7 Beryllium 0.23 U P 7440-42_-8 Boron-- - P 799_0-93-9 Cadmium _ - — — _238 0.17 B _ P 7490-70-2 Calcium __ 31700 P 7.440-47-3 Chromium 5.2 B P 7440-48-4 Cobalt 8.4 B p 7440-50-8 Copper 22.8 B P 57-12-5 Cyanide 10.0 U CA 7439-89-6 Iron 230 P 7439-92-1 Lead3.8 p 7939-95-4 -- - -- Magnesium_ — -- 21900 P 7939--96-5— Manganese -- ---- 4560 p ;7439-97-6 Mercury 10 U CV X7440-02-0 - -, Nickel Potassium - -- - -0_ 18.6 51500 B P P .7440-09-7 7782-49-2 Selenium 1.9 U P 7440-22-9 Silver --- - ---- -- 0.95 U P 7440-23-5 Sodium 73900 P 7440-28-0 Thallium 2.7 B P 7440-62-2 Vanadium _ 1.4 U P 7440-66-6 Zinc _ _ 20.2 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -4S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-007 Level (low/med): LOW Date Received: 3/16/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L [CAS No. 7429-90-5 Analyte Aluminum_ Concentration 112 C B Q M P 7440-36-0 7440-38-2 Antimony2.9 Arsenic 1.8 U U P P 7440 -39 -3 --Barium — 50.3 B P 7440-41-7 Beryllium 0.23 U P 7490-42-8 Boron 234 P 7440-93-9 Cadmium 0.22 B P 74_4_0_-70-2 Calcium - 31100 P 744_0-47-3 Chromium -- 5.2 B P 7440-48-4 7440-50-8 Cobalt Copper - 8.6 22.1 B B p P '57-12-5 17939-89-6 Cyanide Iron -- -- 10.0 -_- --- 123 U CA P 17439-92-1 1__ 7439-95-T Lead _ Magnesium 3.6 21500 P P 7939-96-5 Manganese 4480 P 7439-97-6 Mercury 0.10 U CV 7440-02-0 INickel 18.3 B P 7440-09-7 Potassium 49600 P 7782-49-2 Selenium 1.9 U P 7440-22-4 Silver 0.45 U P 7440-23-5 Sodium 72300 P 7440-28-0 Thallium 2.4 U P 7440-62-2 Vanadium 1.4 U P 7490-66-6 Zinc 17.4 B P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 -- FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte 1 EPA SAMPLE NO Q M INORGANIC ANALYSIS DATA SHEET 80.9 B — Lab Name: H2M LABS, INC. Contract: U �_ MW -5D Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-008 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 80.9 B P 7990-36-0 Antimony 2,g U P 7440-38-2 Arsenic 1.8 U P 7440-39-3 Barium 134 B P 7440-41-7 Beryllium 0.23 U P 7940-42-8 Boron -- — 631 P 7940-43-9 Cadmium 0.38 B P 7440-70-2 Calcium 81800 P 7440-47-3 -Chromium--_ — 5.8 B P 7440-48-4 Cobalt _ 20.5 B P 7440-50-8 157-12-5 7439-89-6 -- Copper_ - -- Cyanide Iron - --- -- ----- 22.0 10.0 -- ---- 80.7 B U B P CA P 7439-92-1 Lead _ __ 2,8 —B -----p 17439-95-9 Magnesium 56500 P x793_9-96-5 Manganese 12500 P (7439-97-6 Mercury_ 0.10 U CV 7940-02-0 Nickel _ 41.4 p 7940-09-7 Potassium Selenium _ 137000 1.9 U p P 744�7782-49-2 0-22_-4 Silver _--- 0.84 B P .74i 40-23-5 Sodium _ 196000 P 7940-28-0 7440-62-2 Thallium Vanadium _ 5.1 1.4 B U P P 7440-66-6 Zinc 15.3 B P _ Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: -3/29/06 FORM I - IN ILM04.1 U.S. EPA - CLP % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. I Analyte 1 EPA SAMPLE NO Q M INORGANIC ANALYSIS DATA SHEET 64.6 B P Lab Name: H2M LABS, INC. Contract: U MW -5S Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-009 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. I Analyte Concentration C Q M 7429-90-5 Aluminum 64.6 B P 7440-36-0 Antimony 2,9 U p 7440-38-2 Arsenic 1.8 U P 7440-39-3 Barium 85.8 B p 7490-41-7 Beryllium 6,82 g p 7440-42-6 !7990743-9 7440-70-2 7940_47 _3 7440-48-4 !7440-50-8 JBoron 1Cadmium 1,Calcium Chromium — Cobalt_ Copper _ 115 1.1 13400 8.5 — — -- 2.7 10.8 B B B B p P P P P P 57-12-5 Cyanide 10.0 U CA 7439-89-6 Iron 113 P 7439-92-1 Lead 2.6 B p 7439-95-4 Magnesium 9740 p 7439-96-5 Manganese 1370 P 7439-97-6 Mercury 0.10 U CV 74_40-02-0 Nickel 9.7 B p 7440-09-7 Potassium 13000 P 7782-49-2 Selenium — --- -- U P 744_0-2_2_-4_ Silver _1.9 ----0.54 B — P 17440-23-5 — - -- Sodium-.--- ---- 14800 -- P 7440-28-0 Thallium 2.4 U p 17440-62-2 Vanadium 1.4 U P 7440-66-6— Zinc 17.4 B p Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Resorted: 3/29/06 Texture: Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Matrix (soil/water): WATER Lab Sample ID: Level (low/med): LOW Date Received: % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7929-90-5 Aluminum 42.0 B P 7940-36-0 !7440-38-2 7990-39-3 47440-41-7 .Beryllium •7440-42-8 7440-43-9 Antimony 2.9 U P jArsenic 1.8 U jBarium - _ - 44.2 B — _ 0.23 UP Boron 88.8 B ----_---- P P -- - P Cadmium 0.15 B P 7990-70-2 Calcium 11200 P 7990-47-3 _ Chromium 2.3 B P 7990-48-4 Cobalt 2.7 B P 7440-50-8 Copper 5.7 BI P 57-12-5 Cyanide 10.0 U CA 7939-89-6 Iron 57.6 B P- [7439-92-1 �----...------ Lead 1.5 B P 17439-95-4 X7939-96-5 :7439-97-6 17_440-02-0 Magnesium-F—," agnesium [Manganese Mercury Nickel _ 3020 _ - -- -1090 _ 0.10 I 3.7 B P P U CV B P 7440-09-7 Potassium 8900 P 7782-49-2 Selenium _ 1.9 U P 7440-22-4 Silver 0.45 U P 7440-23-5 Sodium 5110 P 7440-28-0 Thallium 2.4 U P 7440-62-2 Vanadium 1.4 U P 7990-66-6 Zinc 24.1 P EPA SAMPLE NO MW -6D SDG No.: TSL005 0603561-010 3/16/2006 Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE N0 INORGANIC ANALYSIS DATA SHEET MW -6S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-011 Level (low/med): LOW Date Received: 3/16/2006 Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No.Analyte i 17429-90-5 7440-36-0_Antimon Aluminum iConcentration ------------------- 66.3 - - -- 2.9 C B U Q M P P 7440-38-2 Arsenic 1.8 U P 7440-39-3 Barium _ 46.0 B P 7440-41-7 Beryllium 0.23 U P 7940-42-8 Boron 94.1 B P 7440-43-9 Cadmium 0.29 B P 7440-70-2 Calcium 11900 P 7440-47-3 Chromium 3.1 B P 744_0-48-4 Cobalt -- --_ 4.6 _ B P 17440-50-8 X57-12-5 '7439-89-6 7439-92-1 74_3_9_-95-4 Copper Cyanide Iron IL_ead Magnesium _ 4.8 10.0 87.6 1.6 -- -- - 3140 B U B B B P CA P P P 7439-96-5 Manganese 1250 P 7439-97-6 _ Mercury 0.10 U Cv 7440-02-0 Nickel 3.9 B P 7440-09-7 Potassium 10200 P 7782-99-2 Selenium 1.9 U P 7490-22-9 Silver 0.45 U P 7440-23-5 '7440-28-0 !7440-62-2 .1____*___-_-_____ .,---- !7440-66-6 Sodium _ Thallium Vanadium-- --- Zinc 5040 2.4 -- ----- 1.4 17.4 U U --- B P P P P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 - - — O 0� FORM I - IN ILM04.1 H U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: MW -8D Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-012 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L - — - jCAS No. 7_429-90-5 Analyte Aluminum - -- - Concentration C1 Q ------- 60.2 B M P r7490-36-0 Antimony 2.9 U P [7440-38-2 --Arsenic 1.8 U P 7440-39-3 _ Barium_____ 44.6 B P 7440-41-7 Beryllium _ 0.23 _ _ U P 7440-42-8 !7440-43-9 Boron _ 114 P Cadmium 7440-70-2 Calcium 7440-47-3 Chromium r -'-------.- -i_'---------'------4---- 7940-48-4 Cobalt [7440-50-8 Copper 57-12-5 _ Cyanide --.--- _ _ 0.18 B P 11900 2.8 B - ----'--'-- - --- _3.3 B P P P 4.9 B P 10.0 U CA 7439-89-6 7439-92-1 ILead Iron ---- — 73.7 1.6 BI B I P P 7439-95-4 Magnesium 3600 B P 7439-96-5 Manganese 1120 P 7439-97-6 Mercury 0.10 U CV 7440-02-0 Nickel 4,0 B P 7990-09-7 Potassium _ 41300 P 7782-49-2 7_490_-22_-9 Selenium Silver _ 1.9 0.45 U U I P P 17440-23--5 790- 928-0 k7440-62-2 7440-66-6 Sodium_ _ _ 46900 T_halliu_m 2.4 Vanadium _ 1.4 Zinc —_ - — 45.2 U U P P P P Color Before:_ COLORLESS_ Clarity Before Color After: COLORLESS Clarity After: Comments: Date Resorted: 3/29/06 _ CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -8S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Lab Sample ID: 0603561-013 Level (low/med): LOW Date Received: 3/16/2006 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7429-90-5 Aluminum 63.5 B P 7440-36-0 --Antimony 2.9 U P 7440-38-2 Arsenic 1.8 U P .7440-39-3 ..-Barium __45. 3 B P 7440-41-7 " - Beryllium 0.23 U P 2____ 7 440-4 8 17440-43-9 11,1440-70-2 i7440-47-3 Fi4146-E8-_ Boron Cadmium ;Calcium Chromium Cobalt 116 0.27 2 2' 0 0 3.0 B B P - P P P 3.6 B P 17440-50-B Copper 5.1 B P 57-12-5 --Cyanide 10.0 79.2 U B CA P 7439-89-6 Iron 7439-92-1 Lead 1.8 B P 7439-95-4 -Magnesium _7_ 3700 BI P J.9-96-5 Manganese 1150 P 7439-97-6 ___1�ii_ckel Mercury_ 0.10 U Cv 7990-02-0 17440-09-7 7782-49-2 �7440-22-4_ 'FS'_i_1v`e'_ Potassium Selenium r' 4.2 B 43500 1. 91 B 0.46 B P P P P 7440-23-5 Sodium49300 P 7440-28-0 ha11ium_ Thallium_ 2.4 U P 7440-62-2 Vanadium 1.4 U P 7440-66-6 Zinc 45.5 P Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: -COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 3/29/06 FORM I - IN ILM04. 1 U2M LABS, INC. II. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS - J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES . N. PREPARATION LOGS O. ANALYSIS RUN LOGS U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Analyte True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Aluminum (Antimony 50000.0 48802.16 97.6 50000.0 48942.75 97.9 49139.58 98.3 P 1000.0 979.73 98.0 1000.0 986.16 98.6 987.89 98.8 P Arsenic 500.0 501.00 100.2 500.0 507.92 101.6 509.92 102.0 1 P (Barium 2500.0 2627.09 105.1 2500.0 2621.86 104.9 2609.9.3 104.4 P !Beryllium 2500.0 t- Boron 2500.0 Cadmium 2500.0 2623.39 - -- - 2621.51 2583.60 _104.9 - 104.9 2500.0 --- 2500.0 2659.46 ----- 2652.85 106.4 106.1 2657.15 2654.13 106.3 106.2 P P 103.3 2500.0 2621.66 2638.48 105.5 P Calcium Chromium 50000.0 2500.0 48843.22 2586.57 97.7 50000.0 49634.45 _104.9 99.3 49523.27 99.0 P 103.5 2500.0 2615.53 104.6 2608.59 104.3 P Cobalt 2500.0 2509.47 100.4 2500.0 2536.60 101.5 2514.36 100.6 P _ Copper 2500.0_ 2668.93 106.8 2500.0 2667.89 106.7 2650.54 106.0 P ,Iron 50000.0 Lead 500.0 48173.35 96.3 50000.0 48807.83 97.6 49039.43 98.1 P 482.09 96.4 500.0 486.40 97.3 485.65 97.1 P iMagnesium :50000.0 502_46.66 100.5 50000.0 50933.84 101.9 50605.66 101.2 P (Manganese Nickel i 2500.0 1 2500.0 2497.03 99.9 2500.0 2520.65 100.8 2512.65 100.5 P 2468.77_ 98.8 2500.0 2493.31 99.7 2506.02 300.2 P Potassium 80000.0 82913_ 45 103.6 80000.0 82748.91 103.4 82258.77 102.8 P jSelenium- - Silver - 500.0 1000.0 499.39 979.82 99.9 500.0 507.59 101.5 516.67 103.3 P 98.0 1000.0 985.16 98.5 983.66 98.4 P ,._....-- - - Sodium -- - --- 80000.0_ -- --- 80676.87_ 100.8 80000.0 80880.47 101.1 80669.45 100.8 P aiL--un- Thll 500.0 495.17 99.0 500.0 500.83 100.2 500.27 100.1 P _ Vanadium 2498.03 99.9 2500.0 2516.91 100.7 2502.90 100.1 P Zinc _2500.0 2500.0 2625.10 105.0 2500.0 2660.67 106.4 2657.81 106.3 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 C� FORM II (Part 1) - IN ILM04.1 00 O� a U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O FORM II (Part 1) - IN ILM04.1 07 H Initial Calibration Continuing Calibration j Analyte True Found %R(1) True Found %R(1) Found %R(1) M I-..- - um 50000._0 49358.77 98.7 49446.09 98.9 AntimonyP !_---...---. _ . _ 1000. 0 983.62 98•. 4 986.25 98.6 P Arsenic ! 500.0 -- 510.17 102.0 512.51 102.5 P Barium_ _ - 2500.0 2500.0 2605.20 2648.21 104.2 2611.93 2669.28 104.5 106.8 P P Beryllium _ (Boron - 2500.0 2634.25 _105.9 105.4 2646.35 105.9 P Cadmium 2500.0 2654.98 106.2 2683.96 107.4 P Calcium - 50000.0 49280.21 98.6 49719:69 99.4 P Chromium 2500.0 2599.64 104.0 2620.60 104.8 P Cobalt 2500.0 2480.55 99.2 2491.76 99.7 P Copper -- 2500.0 2632.38 105.3 2632.91 105.3 P Iron_ --- _ 50000.0 49211.95 98.4 99707.62 99.9 P Lead __ 500.0 481.96 96.4 984.97 96.9. P Magnesium 50000.0 50250.39 100.5 50685.51 101.4 P Manganese _ _ _ _ _ 2500.0 2504.73 100.2 2523.59 100.9 P Nickel - -_ -_ 2500.0 2520.17 100.8 2544.55 101.8 P Potassium _ 80000.0. 81769.61 102.2 81677.64 102.1 P ,'Selenium 500.0 513.76 102.8 517.87 103.6 P Silver 1000.0 983.55 98.4 989.29 98.9 P Sodium_ 80000.0 80348.07 100.4 80438.22 100.5 P !Thallium ___ - _ 500.0 500.70 100.1 506.24 101.2 P Vanadium __ 2500.0 2487.22 99.5 2500.07 100.0 P Zinc 2500.0 2645.89 105.8 2669.16 106.8 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 O N O FORM II (Part 1) - IN ILM04.1 07 H U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte I True Found %R(1) True Found %R(1) Found %R(1) M Iron _ 2500.0 — 2427.97_ 97.1 2500.0 2422.85 96.9 2416.16 96.6 P. Sodium 2500.0 2988.9999.6 2500.0 2450.53 98.0 2399.33 96.0 P (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N FORM II (Part 1) - IN ILM09.1 O F-+ U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity . Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M 2500.0 2433.48 97.3 2453.11 98.1 P �Sodium 2500.0 2393.62 95.7 2399.59 96.0 P - -- - - - (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N N FORM II (Part 1) - IN ILM04.1 O 07 U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte i True Found %R(1) True Found %R(1) Found %R(1) M !Mercury _ _ 6.0 _6.1_2_ 102.0 5.0 5.09 101.8 4.96 99.2 CV (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 M N Ln FORM II (Part 1) - IN ILM04.1 O O H U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L initiai Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M yercury 5.0 4.98 99.6 CV (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 d' N FORM II (Part 1) - IN ILM04.1 p C/� U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Lab code: 104'78} Case No. Sao No.: Initial Calibration Verification Source: MV Labs/High Purit Continuing Calibration Verification Source: MV Labs/High Purit Concentration Units: og/L Initial Calibration Continuing Calibration Analyte True Found %R(l) True Found %R(l) Found SDG No. : TSL005 (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 FORM zz (Part I) - IN ILM04.I U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Initial Calibration Continuing Calibration Analyte True Found %R(1) True Found %R(1) Found %R(1) M Cyanid— 100.0 98.40 98.4 1 1 CA (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 N FORM II (Part 1) - IN ILM04.1 O O C/� H U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AA CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purity Concentration Units: ug/L SDG No.: TSL005 CRDL Standard for AA CRDL Standard for ICP i Analyte True Found An Arsenic iBeryllium Boron `Cadmium - Cobalt Copper Lead - ---�- Initial %R True Found 27 %R Final Found 120.0 ---19.29 117.18 97.7-- 117.64 20.0 (Selenium 5 19.87 10. 0 200.0 --19.29---96.5- 10.84 204.51 __96. 108.4 102.3 10.99 - 204.08 - - _ 10.0 _ 10.77 _ 107.7 10.88 18.80 21.05 105.3 _ 20.68 _- 100.0 101.27 101.3 99.50 50.0 6.0 30 0 52.08 5.16 30 34 104.2 86.0 101 1 49.97 5.17 30 Nickel 80.0 80.80 101.0 82.04 (Selenium 10.0 11.53 115.3 9.98 Silver i.. _..._ --F -- -- -- --- 20.0 -- -- 18.80 94. 0 18.89 'Thallium Vanadium f 20.0 20.36 101.8 20.52 100.0 100.57 100.6 99.85 Zinc_ 40.01 _ 43.63 109.1 46.95 %R 98.0 99.4 109.9 102.0 108.8 103.4 99.5 99.9 86.1 100.9 102.6 99.8 94.4 102.6 99.9 117.4 FORM II (Part 2) - IN ILM04.1 r` N Ln O O C/1 E-1 U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 AA CRDL Standard Source: MV Labs/High Purity ICP CRDL Standard Source: Concentration Units: ug/L 00 N FORM II (Part 2) - IN ILM04.1 O O cin F-+ CRDL Standard for AA CRDL Standard for ICP Initial Final Analyte True Found %R True Found %R Found %R Mercury _ 0_2 0.21 7 104.0 00 N FORM II (Part 2) - IN ILM04.1 O O cin F-+ U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 AA CRDL Standard S'ource: MV Labs/High Purity ICP CRDL Standard Source: Concentration Units: ug/L CRDL Standard for AA CRDL Standard for ICP Initial Final Analyte True Found %R True Found %R Found %R Cyanide 10.01 9.451 94.5 Cr N Ln FORM II (Part 2) - IN ILM04.1 O O H Lab Name: H2M LABS, INC. U.S. EPA - CLP 3 BLANKS Contract: Lab Code: 10478 Case No. Preparation Blank Matrix (soil/water): SAS No.: WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL005 FORM III - IN ILM04.1 j Initial i Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M iAluminum- 9.9 U 9.9 U 9.9 U 16.0 B 9.921 U P Antimony 2.9 U 2.9 U 2.9 U1 2.9 U 2.918 U P Arsenic_ 1.8 U 1.8 U 1.8 U 1.8 U 1.768 U P Barium 1.5 U 1.5 U 1.5 U 1.5 U 1.511 U P Beryllium 0.2 UT 0.2 U 0.2 U 0.2 U 0.230 U P Boron----.-.. 1.3 U 1.5 B 1.3 U 1.3 U 1.310 B P Cadmium 0.3 B 0.2 B 0.2 B 0.1 U 0.122 U P Calcium-._.-. 7.4 U 7.8 B 7.4 U 7.4 U 9.420 B P Chromium 0.3 U 0.3 U 0.3 U 0.3 U 0.930 B P ,Cobalt 1.2 U 1.2--U 1.2 U 1.2 U 1.198 U P Copper 1.0 U -1.2 B -1.8 B 0.964 U P ,Iron 17.8 U 17.8 U 17.8 U 17.8 U 25.100 B P Lead - _ 1.1 U 1.1 U 1.1 U 1.1 U 1.126 U P Magnesium - - 8.2 U 8.2 U 8.2 U 8.2 U 8.230 U P Manganese - 0.4 U 0.4 U _0A U 0.4 U 0.376 U P Nickel 1.0 U 1.0 U 1.0 U 1.0 U 1.042-u P Potassium 49.8 B 36.7 B 37.0 B 34.4 B 37.600 B P Selenium-__ 1.9 U 1.9 U 2.0 B 1.9 U 1.910 U P Silver _ 0.4 U 0.4 U 0.4 U 0.4 U 0.449 U P Sodium 15.0 U 1-5.0 U 15.0 U 15.0 U 14.979 U P Thallium 2_4'U -- 2.4 U 2.4 U 2.4 U 2.416 U P Vanadium 1 1_4 U 1.4 U 1,.4 U 1.4 U 1.355 U P Zinc 114;U 1.4� U 1.4 U 1.4 U 3.790 B P FORM III - IN ILM04.1 Lab Name: H2M LABS, INC. U.S. EPA - CLP 3 BLANKS Contract: Lab Code: 10478 Case No. Preparation Blank Matrix (soil/water): SAS No.: WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL005 i I Initial I Calib. Continuing Calibration Prepa- I I Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M !Aluminum jAntimony_..... senic .... . —.-.. ------ - 26.1 2.9 P ...- 1.8 P VB --!Barium 1.5 p rtlBeryllium 0.2 p----- .._... 1.3 P E'Cadmium -- --...- - Calcium -- I — --- - - - --- --- -- - �- - ----I-- — - ----- — t 0 1 U p I ----- -- - — --- — - 7.4 �- Chromium Cobalt--.,.------ 0.3 U ---- - — P 1.2 U1 P Copper -- -1.9 B P Iron_---- — - 17.8 U P Lead Magnesium Manganese INickel _ --- - — 1.1 U P 8.8 B P 0.4 U P 1.0 U IP - --- [Potassium - -- - ---- - 34.6 B 1P Selenium 1.9 U P Silver L_ 0.4 U P Sodium 15.0 U Thallium 2.4 U P Vanadium _ — 1.4 U P fZinc ---.--- - B P — - -3.2 FORM III - IN ILM04.1 U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Initial Calib. Continuing Calibration Prepa- Blank j Blank (ug/L) ration Analyte (ug/L) C1 1 C 2 C 3 C Blank C M Mercury - 0.11U 0.1 161 0.11 U 0.1 U 0.1001 U CV FORM III - IN U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C M ,Cyanide 10._01 U 10. q! U 10. 0_I U 10.0 1 U _ 10. 0001 U CA FORM III - IN ILMG4.1 U.S. EPA - CLP 4 ICP INTERFERENCE CHECK SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA ICS Source: MV Labs/High Purity Concentration Units: ug/L I Analyte L-_ True Sol. Sol. A AB Initial Found Sol. Sol. A AB %R Final Found Sol. Sol. A AB %R Aluminum Arsenic ----------- 500000 �_ 500000 1000 495587 498752.5 1039.3 99.8 103.9 482429 49103.4.6 1019.7 98.2 102.0 Barium 500 560.6 112.1 544.9 109.0 Beryllium Boron - C 500 546.7 109.3 535.5 107.1 _ 1000 982.9 98.3 954.9 95.5 Cadmium 1000 1017.2 101.7 1014.7 101.5 Calcium Chromium Cobalt_ 500000 500000 500 500 496.061 503171.8 _ 528.3 495.4 100.6 105.7 99.1 482260 489300.4 515.7 474.1 _ 97.9 103.1 9'4.8 _ Copper_ _ 500 588.2 117.6 563.6 112.7 Iron 200000 200000 199109 201354.8 100.7 196700 199867.4 99.9 Lead 1000 986.7 98.7 957.9 95.8 Magnesium _ 5_0.0_000 500000 498050 502959.2 100.6 481270 489154.0 97.8 Manganese 500 497.2 99.4 476.0 95.2 Nickel Selenium Silver _ 1000 959.6 96.0 953.9 95.4 1000 1033.2 103.3 1017.9 101.8 1000 1068.1 106.8 1043.7 104.4 Thallium _ I 1000 _ 1011.5 101.2 995.3 99.5 Vanadium Zinc _ --- 500 _ 508.8 101.8 493.0 98.6 _ 1000 1114.8 111.5 1 1082.21 108.2 7t M O FORM IV - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO MW-5SS SDG No.: TSL005 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L (Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M !Aluminum175-125_ _ _ 1993.6700 _ 64.6200 B 2000.00 96.5 P nt Aimony __ 75-125 _ 498.1016 2.9176 U 500.00 99.6 P Arsenic 75-125_ 39.0805 1.7682 U 40.00 97.7 P Barium _75-125 Ber�lium _ 2186.3000 52.8500 _ __ 85.8200 B 2000.00 105.0 P _75-125 0.8200 B 50.00 104.1 P LBoron 75-125 - . ------ - - -L._. _ 714.8800 115.9000 500.00 119.9 P Cadmium - 75-125_ 52.4800 1.1200 B 50.00 102.7 P Chromium_ 75-125 216.3200 8.4800 B 200.00 103.9 P Cobalt 75-125 _ 498.6100 2.7300 B 500.00 99.2 P Copper 75-125 276.4900 10.8300 B 250.00 106.3 P Cyanide 75-125 81.2692 _ 10.0000 U 100.00 81.3 CA Iron75-125 rLead 1002.5300 113.0800 1000.00 88.9 P 75-125 _ 21.6229 2.5965 B 20.00 95.1 P M_an anese 75-_12_5 _ 1866.1300 1367.5400 500.00 99.7 P Mercua 75-125 Nickel 75-12_5 --..--.---505. - 1.0700 2700 _ _ 0.1000 9.6800 U B500.00 1.00 107.0 99.1 CV P Selenium_ 75-125 11.0318 1.9100 U ___ 10.00 110.3 P Silver 75-125 Thallium 75-125 48 _.6932 _ 48.3492 _ _ 0.5414 2.4157 B U 50.00 50.00 96.3 96.7 P P Vanadium 75-125 500.95001.3551 JU 500.00 100.2 P Zinc 75-125 551.0800 17.3600 B 500.00 106.7 P Comments: FORM V (Part 1) - IN ILM04.1 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES MW -5S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 Matrix (soil/water): WATER Level (low/med): LOW % Solids for Sample: 0.0 % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q M Aluminum iAnt imony Arsenic 200.0000 _- _ 64.6200 B 36.8800 B 54.7 P 2. 917 6 U 2. 9176 U 1.7682 U 1.7682 U P P -------- - iBarium 200.0000 85.8200 B _ 67.9200 B 2.4 P Beryllium -- - 5_.0000 - -.. 0.8200 B 0.2297 U 200.0 P I'Boron .._ . (100.0000 - -- ----- 115.4000 --- -- ---- -117.4000 1.7 P Cadmium 5.0000 1.1200 B 0.2500 B 127.0 1 P Calcium 5000.0000 13422.3500 13768.2200 2.5 P c(Chromium 10.0000 _ 8.4800 B 7.3900 B 13.7 P obalt 50.0000 2.7300 B 2.3000 B 17.1 P Copper- 25.0000 10.8300 B 10.3800 B 4.2 P Cyan ide -------- --------- ------------ -- 10.0000 U - 10.0000 U CA J:ron iLead 100.0000 3.0000 ---- 113.0800 -------- 55.7100 B 68.0 P 2.5965 B 2.4671 B 5.1 P Magnesium 5000.0000 _ 9735.9200 10018.7000 2.9 P Manganese 1367.5400 _ 1405.5300 2.7 P Mercury 0.1000 U 0.1000 U CV Nickel 40.0000 _ 9.6800 B 9.0300 B 6.9 P Potassium 5000.00 00 13017.5800 13970.9100 7.1 P (Selenium 1.9100 U 1.9100 U P Silver 10.0000 0.5414 B 0.4485 U 200.0 P Sodium 5000.0000 14805.0400 15351.0900 3.6 P Thallium _ 2.4157 U 2.4157 U P Vanadium 1.3551 U 1.3551 U P Zinc 20.0000 17.3600 B 18.9000 B 8.5 P FORM VI - IN ILM04.1 S U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Solid LCS Source: ERA Aqueous LCS Source: MV Labs/High Purity SDG No.: TSL005 i i Analyte Aqueous (ug/L) True Found Solid (mg/kg) %R True Found C Limits %R Aluminum 50000.0 49245.24 98.5 Anti.mo Arsenic Barium Be_rylliu_m 1000._0 500.0 2500.0 _2500.0 966.68 _ 500.49 2645.49 2684.15 96.7 100.1 105.8 107.4 Boron. _ 2500.0 2742.87 109.7 Cadmium 2500.0 2629.28 105.2 Calcium 50000.0 49727.78 99.5 iChromium 2500.0 2644.54 105.8 !Cobalt 1 2500.0 2550.29 102.0 Copper I :Iron 2500.0 50000.0 2706.45 49081.72 108.3 98.2 (Lead 500.0 485.93 97.2 Magnesium 1 50000.0' 50503.38 101.0 Man anese 1 2500.0 2544.48 101.8 Nickel 2500.0 2509.35 100.4 Potassium 80000.0 81805.69 102.3 Selenium 500.0 485.26 97.1 Silver 1000.0 976.52 97.7 Sodium 80000.0 81299.77 101.6 Thallium 500.0 496.45 99.3 Vanadium 2500.0 2544.36 101.8 Zinc 2500.0 2646.18 105.8 FORM VII - IN M O ILM04.1 O Cn F-+ 4 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No U.S. EPA - CLP 8 STANDARD ADDITION RESULTS Contract: SAS No.: Concentration Units: ug/L SDG No.: TSL005 j EPA Sample 0 ADD 1 ADD 2 ADD 3 ADD Final No. �An ABS CON ABS CON ABS CON ABS Conc. r Q FORM VIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Contract: SAS No.: Concentration Units: ug/L MW -5S SDG No.: TSL005 Level (low/med): LOW -- . -- -- Analyte i i lAluminum ----- Initial Sample Result (I) C Serial Dilution Result (S) C % Differ - ence Q M _64.62 B __. 49.60 U- 100.0 P Antimony _ __ �_ 2.90 U 14.60 Ul P Arsenic_ 1.80 U 8.80 U1 P Barium Beryllium_ 85.82 B 88.35 BI 1 2.9 P 0.82 B 1.10 U 100.0 P Boron 115.40 121.15 B 5.0 P Cadmium _ _ 1.12 B 0.61 U 100.0 P Calcium (Chromium Cobalt-- Copper _-_13422_ 35 8.48 - -- -_ B ____ 13675.50 8.55 B B 1.9 0.8 P P I- ---- - 2.73 B 6.00 U 100.0 i� - - -10.83-B 6.75 B 37.7 P P Iron Lead 113.08 2.60 B _---......_,_ 109.00 5.60 B U 3.6 100.0 P P Ma nesium 9735.92 9825.00 B 0.9 P manganese 1367.54 1394.85 2.0 P Nickel 9.68 B 8.80 B 9.1 P Potassium 13017.58 I 12376.40 B 4.9 P Selenium 1.90 U 9.50 U P Silver _ 0.54 B 2.20 Ul 100.0 P Sodium 14805.04 14268.70 B 3.6 P Thallium 2.40 U - 12.10 _U P Vanadium Zinc _ _ _ _ 1.40 _ _ _ 17.36 U B ._ 6.80 32.20 U B 85.51 P P FORM IX - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: TJA6IEA Flame AA ID Number: Furnace AA ID Number: Comments: Contract: SAS No.: Date: 3/15/2006 SDG No.: TSL005 Analyte Wave- length Back- (nm) ground CRDL (ug/L) IDL (ug/L) M Aluminum 308.21 200.0 9.9 P Antimony 206.84 60.0 2.9 P Arsenic 189.04 10.0 1.8 P Barium 493.411 200.0 1.5 P Beryllium 313.04 5.0 0.2 P Boron 249.68 100.0 1.3 P Cadmium 226.50 5.0 0.1 P Calcium 317.93 5000.0 7.4 P Chromium 267.62 10.0 0.3 P Cobalt 228.62 50.0 1.2 P Copper 324.75 25.0 1.0 P Iron 259.90 100.0 17.8 P Lead 220.35 3.0 1.1 P Magnesium 279.08 5000.0 8.2 P Manganese 257.61 15.0 0.4 P Nickel 231.60 40.0 1.0 P Potassium 766.49 5000.0 16.0 P Selenium 196.03 5.0 1.9 P Silver 328.07 10.0 0.4 P Sodium 588.90 5000.0 15.0 P Thallium 190.86 10.0 2.4 P Vanadium 292.40 50.0 1.4 P Zinc 213.86 20.01 1.4 P FORM X - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: Flame AA ID Number: HYDRA Furnace AA ID Number: Comments: Contract: SAS No.: Date: 1/23/2006 SDG No.: TSL005 -- -... --- I Wave- -- --- �— i length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Mercur 253.66 0.2 0.1 CV FORM X - IN ILM04.1 U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: Flame AA ID Number: SPEC20D+ CN Furnace AA ID Number: Comments: Contract: SAS No.: Date: 12/2/2005 SDG No.: TSL005 Wave- length Back- CRDL IDL Analyte (nm) ground (ug/L) (ug/L) M Cyanide 578.30 10.0 10.0 CA FORM X - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA Date: 12/19/2005 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Aluminum 308.22 0.0000000 -------------- 0.0000000 0.0000000 0.0000000 -0.0163000 Antimony _ 206.84 _0.0000000 ---- 0 .0000000 --- 0.0200000 0.0000000 0.0000000 Antimony 206.84 0.0000000 0.0000000 0.0320000 0.0000000 0.0000000 Arsenic_ Barium 189.04 493.41 0.0000000 0.0000000 0.0000000 0.0000000 -0.0100000 0.0000000 0.0000000 0.0000000 -0.2040000 0.0000000 Beryllium_ 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Boron_ 249.68 0.000000' 01 0.0000000 -0.0003400 0.0000000 0.0014300 Cadmium 226.50 0.00000001 0.0000000 0.0001130 0.0000000 0.0000000 Cal_ciu_m _ 317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 :Chromium __267.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cobalt Copper !Iron 'Iron 228.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 324.75 _ 0.0000000 0.0000000 -0.0000400 0.0000000 ;_259.94 0.00000000.0000000 0.0000000 0.0000000 271.44 0.0000000 0.0000000 0.0000000 0.0000000 -0.0003670 0.0000000 0.0000000 Lead_ - 220.35 -0.2720000 0.0000000 0.0420000 0.0000000 0.0000000 Lead 220.35 0.5260000 0.0000000 0.0830000 0.0000000 -0.7550000 Magnesium 279.08 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Manganese 257.61 -0.0001400 0.0000000 0.0000230 0.0000000 -0.0004900 Mol bdenum 202.03 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 -0.0004500 Potassium 766.49 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.0000000 0.0000000 0.4080000 Sil_ico_n_328. _ 288.16 0.0000000 0.0000000 0.0000000 0.0000000 silver _ _07 Sodium - _0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 _ 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium _330.23 589.00 _0.0000000 _ 0.0000000 0.0000000 0.0000000 0.0000000 Strontium Thallium_ 0._0000000 0.0000000 0.0000000 0.0000000 0.0000000 _40_7.77 190.86 0.0000000 0.0000000 -0.3320000 0.0000000 -0.5310000 Comments: M Ln O O V1 FORM XI (PART' 1) - IN ILM04.1 U.S. EPA - CLP 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA Date: 12/19/2005 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Tin 189.99 0.0000000 0.0000000 -0.0002040 0.0000000 0.0000000 _ Titanium 334.94 0.00000001 0.0000000 0.0000000 0.0000000 0.0000500 Vanadium_ 292.40 0.00000001 0.0000000 0.0000200 0.0000000 0.0000000 Zinc 213.86 0.00000001 0.0000000 0.0001580 0.0000000 0.0000000 Comments: FORM XI (PART 1) - IN ILM04.1 H U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA Date: 12/19/2005 Analyte Wave- length (nm) Cr Interelement Cu Correction Mn Factors for: Ni V Aluminum 308.22 0.0000000 0.0000000 -0.0003880 0.0000000 0.0170000 Antimony 206.84 8.5710000 0.0000000 0.0000000 0.0000000 0.0000000 Antimony . 20684 9.8570000 0.0000000 0.0000000 -1.1020000 -6.4900000 Arsenic 189. 04 0.2450000 0.0000000 -0.2700000 0.0000000 0.0000000 Barium 493.411 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium Boron 313.04 249.681 r 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0002000 -0.0002500 Cadmium_ - 226.501 0.0000610 0.0000000 0.0000000 -0.0001840 0.0000000 Calcium _317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Chromium 267.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0005100 Cobalt 228.62 0.0000000 0.0000000 0.0000000 0.0002040 0.0000000 Copper 324.75 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 259.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 271.44 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Lead 220.35 0.0000000 0.0000000 0.1550000 0.1430000 -0.1570000 Lead 220.35 0.0000000 0.0000000 0.0000000 0.3140000 0.0000000 Magnesium 279.08 -0.0001000 0.0000000 -0.0035000 0.0000000 0.0000000 Manganese_ 257.61 'Molybdenum 202.03 rNickel �-231.60 0.0000000 0.0000000 0.0000000 0.0_000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 -0.0001000 0.0000000 0.0000000 Potassium 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium _766.49 196.03 0.0000000 0.0000000 0.2750000 0.0000000 0.0000000 :,Selenium 196.03 0.0000000 0.0000000 0.4450000 0.0000000 0.2350000 Silicon 288.16 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 _ Silver 328.07 0.0000000 0.0000000 0.1850000 0.0000000 0.0000000 Sodium 330.23 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 589.00 0.00000001 0.0000000 0.0000000 0.0000000 0.0000000 Strontium 407.77 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 (Thallium _ 190_86 t___19 0.20000001 0.0000000 -0.65000001 0.0000000 -0.8430000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA Date: 12/19/2005 Anal I . T_in Tita Mana Zinc yte nium 3ium Wave- length (nm) 189.99 334.94 292.40_ Cr Interelement Cu Correction Mn Factors for: Ni V 0.00_00000 0.0000000 0.0000000 0.0000000 0.0000000 _ 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 213.86 0.0000000 0.0004000 0.0000000 0.0050400 0.0000000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL005 ICP ID Number: TJA6IEA Date: 11/12/2005 Comments : Analyte Integ. Time (Sec.) Concentration (ug/L) M Aluminum 15.00 1000000P Antimony 15.00 10000P Arsenic 15.00 20000P Barium 15.00 20000P Beryllium 15.00 10000P Cadmium _ Calcium 15.00 15.00 20000P 1000000P Chromium 15.00 50000P Cobalt 15.00 50000P Copper 15.00 50000P Iron 15.00 250000P Lead 15.00 50000P Magnesium 15.00 1000000P Manganese 15.00 20000P Nickel 15.00 50000P Potassium 15.00 250000P Selenium 15.00 20000P Silver 15.00 5000P Sodium 15.00 500000P Thallium 15.00 50000P Vanadium 15.00 50000P Zinc 15.00 10000P FORM XII - IN d' ILM04.1 CD O UD Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract; SAS No.: SDG No.: TSL005 EPA Sample I No. Preparation Weight Date (gram) Volume (mL) EQPT 03/21/2006 50 LCSW 03/21/2006 50 MW -1D 03/21/2006 50 Mw -is 03/21/2006 so MW -3D 03/21/2006 so MW -3S MW -4D Mw -4S Mw -5D Mw -5S 03/21/2006 50 03/21/2006 50 03/21/2006 I 03/21/2006 03/21/2006 50 50 50 03/21/2006 50 MW-5SS 03/21/2006 50 MW -6D 03/21/2006 50 Mw -6S 03/21/2006 50 M W 03/21/2006 50 MW -BS 03/21/2006 50 PBW 03/21/2006 50 00 FORM XIII - IN ILM04.1O Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: CV U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL005 EPA Sample No. --- -- ...------- EQPT Mw -1D Mw -is Preparation Weight Date (gram) Volume (mL) ...-------- 03/21/2006 100 _ 03/21/2006 100 03/21/2006 100 MW -3D 03/21/2006 100 Mw -3S 03/21/2006 100 14W -4D 03/21/2006 100 Mw -4S 03/21/2006 100 MW -5D 03/21/2006 100 Mw -5s 03/21/2006 100 _ MW-5S_D____ MW-5SS MW -6D MW -6S 03/21/2006 03/21/200_6 03/21/2006 — --- ----- 100 100 -- 100 03/21/2006 100 _ MW -8D 03/21/2006 100 _ Mw -8S 03/21/2006 100 PBw 03/21/2006 100 FORM XIII - IN ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: CA U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL005 EPA Sample No. Preparation Weight Date (gram) Volume (mL) EQPT 03/21/2006 50 _ Mw -1D 03/21/2006 50 Mw -is 03/21/2006 50 MW -3D 03/21/2006 50 MW -3s _ 03/21/2006 50 MW -4D 03/21/2006 50 MW -4S 03/21/2006 50 MW -5D 03/21/2006 50 Mw -5s 03/21/2006 50 _ Mw-5SD 03/21/2006 50 MW-5Ss 03/21/2006 50 _ MW_ -6D _ 03/21/2006 50 _ Mw -6s _ 03/2_1/2006 50 MW -8D —_--+— 03/21/2006 -- - 50 MW -8S 03/21/2006 50 PBw _ 03/21/2006 50 FORM XIII - IN Q ILM04.1 Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 03/22/2006 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL005 03/22/2006 EPA i Analytes Sample D/F Time % R A S A B B C C C C C F P M M H N K S A N T V Z C No. L B S A E D A R 0 U E B G N G I E G A L N N !so 1.00 0655 X X X X X X X X X X X I X I X I X I X X X X X X X X Is 1.00 0702 X X s 1.00 0708 X X X X !s I 1.00 0713 X X X X is 1.00 0719 X X X X X X X X X X X X X S1.00 0731 X X ICv 1.00 0735 + X X X X X X X X X X X X X X X X X X X X X X IcV 1.00 0743 X X i 0750 ICB _ 1.00 X X XIX X X X X XIX X XIX X X X X X X X X X CRI 1.00 0757 X X X X X X X X X X X X X X X ICSA _ 1.00 0805_ X X X X X X X X X X X X X X X X X X X ICSAB 1.00 0812 X X X X X XIX X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X X CCv --1.00- 1.00 0820 CCv _ 1.00 0827 _ X X ICCB_ _ _ 1.00 0835_ X X X X X X X X X X X X X X1 Ix X XIX X X X X rPBW 1.00 0842 X X X X X X X X X X X X X X X X XIX X X X X LCSW 1.00 0849 X X X X X X X X X X X X X X X X X X X X X X Mw -5s 1.00 0857 X X X X X X X X X X X X X X X X X X X X X X MW -5s D 1.00 0904 _ X X X X X X X X X X X X X X X X X X X X X X MW-5ss 1.00_ 0912_ X X X X X X X X X X X X X X X X X X X X X X .Mw --5-9L ---.--...-5.00 0919 X X X X X X X X X X X X X X X X X X X X XIX MW -61D - _ 1.00 0927 X X X X X X X XIX X X XIX X X X X X X X X X MW- iD 1.00 0934 X X X X X X X X X X X XIX X X X X X X X X X Mw -1s 1.00 0942 X X X X X X X X XIX X X X X X X X X X X X X MW 3D._..00 0949 X X X X X X X X X X X X X X X XIX X X X X X ICCV 1.00 0956 X X X X X X X X X X X X X X X X X X X X X X !CCv 1.00 1004 _ X X !CCB1.00 1011 X X X X X X X X X X X X X X X X X X X XIX X Mw -3S 1.00 1019 X X X X X X X X X X X X X X X X X X X X X X MW -41D 1.00 1026 _ X X X X X X X X X X X X X X X X X X X X XIX MW -9S _ 1.00 1034 X X X X X X X X X X X X X X X X X X X X X -� X MW -51D 1.00 1041 X XIX X X X X XIX X X X X X X X X X X X X X EQPT 1.00 1049 X X X X X X X X X X X X X X X X X X X X X X Mw -5s 1.00 1056 X X X X X X X X X X X X X X Ix X X x X X X x FORM XIV - IN ILM04.1 O Q� Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA61EA Start Date: 03/22/2006 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSI,005 03/22/2006 EPA I Analytes Sample D/F Time % R A S A B 3 C C C C C F P M M H N K S A N T V Z C No. L B S A E D A R 0 U E B G N G I E G A L N N MW -8D 1.00 1103 xlxlxlxlx xlxlxlxlxlxlx x I x I I x I x x x xjxjx x MW -8S 1._00_ - lill x xjxjx x x x x x x x x x x x x x x x x x x ccv 1.0 1118 x x x x x x x x x x x x x x x x x x x x x x ccv_ 1,00 1126 x x !CCB 1.00 1133 x x x x x x x x x x x x x x x x x x x x x x 1141 CRI 1.00 x x x x x x x x x x X X x x x 1148 115 6 JCSA 1.00 "ICSAB 1.-0 x x x x x 1� x x -X x X x X x X x X x X x X x X x X x x x x x x X x X x X x _qc ccv 1 00 -- 1203 —x x x x x x x x x x x x x x x x X x ccv 1 00 1211 X x dx ix CCB 1. 00-f 1218 x x x x x x x x x x x x x x x x x x X xx x N FORM XIV - IN ILM04.1O Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: HYDRA Start Date: 03/21/2006 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: CV End Date: SDG No.: TSL005 03/21/2006 ---EPA -- -- ---_- ---- Analytes ' Sample D/F Time I RA S A B B C C C C C F P M M H N K S A N T V z C No. L B S A E D A R 0 U E B G N G I E G A L N N! � --....-1.0 _J j s D 0 1 1306 X 50.2 1.00 1308 x IS1 --- -1.00 1309-f------- - - X S2 1 1.00 1312 I X S5 1.00 1314 X S10 _ _ 1.00 1315 X 1.00 1317 Icv X ICB 1.00 1320 _ X Ccv 1.00 1322 X CCB 1.00 1324 X CRA 1.00 1327 x PBW _ 1.00 1329 X EQPT - _ 1.00 1330 X MW -1D 1.00 --------- 1332 -- _ _ X Mw-is 1.00 1334 X MW -3D 1.00 1336 X MW -3S 1.00 1338 _ X MW -4D _ 1.00 1340 X MW -4S 1.00 1342 X Mw -5D 1.00 1344 x CCV 1.00 1345 Ix CCB _ 1.00 1347 Ix MW -5S _ 1.00 1349_ Ix Mw-5SD 1.00 1351 x Mw-5SS 1.00 1354 X !MW -6D 1.00 1356 x 1MW-6S 1.00 1357_ X I D_ _ 1.00_ 1359 X MW -8S 1.00 1902 X zzzzzz 1.00 1404 zzzzzz 1.00 1406 zzzzzz 1.00 1408 CCV 1.00 1412 X CCB _ 1.00 1414 X zzzzzz 1.00 1415 FORM XIV - IN ILM04.1 CD 0n Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: SPEC20D+ CN Start Date: 03/21/2006 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: CA End Date: SDG No.: TSI,005 EPA Analytes 7 Sample D/F Time % R A S B B C C C j C C F P M M H N K S A N T V Z C 1 No. i I L B S �A A E D A R 0 U E B G N G I E G A L N N � SO_ 1.00 0800 1 .00 0801 X S50 1.00 -1.00 0802 x 6100 0803 x 1.00 0804 x ICV .00 0830 X- ICB 1.00 0831 X CRI 1.00 0832 x CCv 1.00 0833 x CCB 1.00 0834 PBW 1.00 0835 EQPT 1.00 0836 X MW 1D 1.00 0837 X Mw -is 1.00 0838 X M.W-.3. D X. MW -3S 1.00 0840 -- X Mw -4D 1.00 0841 x MW -4S 1.00 0842 X MW -3D 00 0843 X MW -5s 1.00 0844 0845 MW-5SS 1.00 C C v - . .1- XB --.. _0 --- 1.00 0847 0848 x yW-5SD 1.00 0849 x AW -6D 1.00 0850 X 4W -6s 1.00 0851 x .4W -8D1.00 -------T—oo 0852 x K—w--8—s 08-53 X 7,Z ZZZZ 1.00 0854 Cv 1.00 0856x -7yo ,CB 1 08 T 57 1-1-1---Tx— FORM XIV - IN ILM04.1 U2M I AUS, INC. III. RAW DATA FOR METALS A. ICP DATA B. HG DATA C. CYANIDE DATA 112M LA[ -3S9 INC. J CLIENT ' JL Cy j DATE 17 ooze Nlu -� �� t -3 TASK: RESULT FILE: HO3--Qt:(,e- ANALYST Oit6 ; Hw-(o5 43: ; # ; SAMPLE NOTES ; # ; SAMPLE ; NOTES___ ; 20: Cc VZ ; 26, �L.1- CO� '�i ' &a * 45; ; PT Alb+�� a /u ; J 22; - 23 H ml 7 , 24: Ob (r�, ; �� • �1 �� ; 49.' ; 25i pnz C, ; KW -`t S ; 50: � �- P 0001 17 ooze Nlu -� �� t -3 28; Oit6 ; Hw-(o5 43: ; ' 19; 4AW 3D 441 20: Cc VZ ; ; 45; ; 30: C -i136 ; i'iw - es 6 CC -\i 3 ; 7 i ctv i 32 8 ; CC ii ; ; 33: Cc 1% 9 34; e- it ; 10 ; M -5-I bLi is i'Pw,/ ; 35; 16411 ; i 11; 1-(S'!bLig5 ;Lt.5 cS�*r 12; O(piS SWI-OCIG ; iAw-5S L 37; Cc- v4 38 i CC VL -4 22; - 23 H ml 7 , 24: Ob (r�, ; �� • �1 �� ; 49.' ; 25i pnz C, ; KW -`t S ; 50: � �- P 0001 17 ooze Nlu -� �� t 42 43: ; ' 19; 4AW 3D 441 20: Cc VZ ; ; 45; ; 22; - 23 H ml 7 , 24: Ob (r�, ; �� • �1 �� ; 49.' ; 25i pnz C, ; KW -`t S ; 50: � �- P 0001 :W- #I-- o\o m '� [r1 *1: 4# :4-- ao w �ro N 4:1- 0\0 Cl] '� LT1 W CO o\o 10 wNN pdt7C H wNH :uu-� - FA �t7� N wNH ?dt7C F+ wNH Cn cD lQ N Cn (D W (D M (D LQ (D Cl) (D LQ (D M (D CQ (D (D F3 U (D (D9 U74(DEl U-4(DF1 HO a Ea pi a Ul CA I I I 00 I NI (7 N 0 0 0 -1 0 0 Fj N 0 0 0 H O C) CQ •I •I • j. I� I I . I O r N 000 00 000 H000 000 • 00 000 • 00a 000 uloo� W F% Crt 000 N 0 0 000 U100 W 000 1A00 000 1D00 000 000 \ FJ- NH0 IPI HH 000 0001-1 1P, PA. \D F- W 000 \DO0 www �7oLA) N p 00 lD l0 o 1D N 01 FA. H Ul Ul Ul O Ul 01 <N a7 N Ul OD \ Q �J 0) F, y I I I N I N Ca) • 3 I iA I 000 NOO- p '• 0 0 o 000 -10 C) 0• \D 0 ~' ' O 0 0 0 • O O rn N 000 00 000 oorn 000 00 000 rnoo 000 MOO..w000 F-Ioo 000 kDOOOD 000 UI U H00 000 • 0o UI I lDOCil 7 rt FAUNA UIHiA NNW UION\ ll -1 W wtom ONO 0100 0OH ONO U10) HUIFA 0101 ]N N NO .� N-IUI 00 N �, N 0) ti i I I FA I y 00. N N.�+ • F--' 000 N000 000 J000 000 coo0CD11 •I ,I O 00- .I 03 .. 000 0 o O O N 000 • 0 001 0 0 0 • 00 0 0 0 • 0 0 000 N O O H Cn 000 H 0 0 w ONO 000000 000 H00 000 0100 OOH 0000 rt FA FA W 000�A0 lOHO %D 017\ W NN CYN HW FA FAN H1HW NHO NN0ID ¢, HNOD (3)N00o lOU1FA 00 W N H�1N H�IlDO aj N Co lD O WFA H N FA C I I H I H I I FA I Z H (1 Ul x 000 W0C) . . . o. to b7 fv 000 00� 000 00 000 00 000 0001 000 FP. 00 000 NC3 000 X100 000 W 00 OHO 01000 NNN -40N w W w Now 000 FA00 O HHo FAOH 000OD 00W\ 00N FAON H00 OlOO FA FA FA 010FA W OD N FA ID ID N N' 00 L I N W N \ co C> `3 00 N N N N H . . . N.7a W . . F� N 0 000 00 S 000 00010 W W W O WSL 000 W 00(D 000 0000) i 000 0100 000 0001 FA wUl FA OFA 000 00 000 00 0 000 Oo00 W NH HHN0 NOD UI lD W CII 000 0000 000 0100 �l J W co 1D000 NU70 $4HN\ O101H OlO1FA 000 0100 wNN Ol W N 0 F;s O N W . N ��'' � Faj I 1 � FA I b7 NHH ooHl+ 000 l)NlooN 000 Oo(D (D N N N N O N 0 0 0 00 O O Cl N 0 o 0 0 0 W O o N� H HN U10 H 000 X100 ODC:)< Ul01000 000 FA 00 p 0161 OD001 W W N <NN WHUl FA FAO 000 ODOO OD OD 00 O OD Q• W Cr) . . . N N H • 000 W OO x' 0 • ' ' ',S 000 FAOON 000 POO 000 W 000)o 000 0 0 H H H OH O 000 0 0 000 01 0 0 b NW N NON NWID 0WUIW UI UI FA FA0UI FA FA FA OOFA O) H l T1 O Ol OD 0l lD N W FA Ol H \ FA W FA Ol 01 O W lD W Ol O 1p LQ Ul 01 -1 U1 FA 01 H (D H TSL005 M57 Standardization Rpt. -hod: CLP1 Standard: StdAGSBH i Time: 03/22/06 07:02:39 Elem Ag 2068/1 2068/2 Avge .64224 2.4220 1.5444 SDev .00011 .0061 .0044 %RSD .01754 .25000 .28588 #1 .64211 2.4151 1.5393 #2 .64230 2.4245 1.5461 #3 .64231 2.4264 1.5477 03/22/06 07:08:25 AM page 1 00 O O Standardization Rpt. 03/22/06 07:13:31 AM page 1 thod: CLP1 Standard: StdICSH n Time: 03/22/06 07:08:31 Elem Al Ca Fe Avge 28.59 38.45 .4860 SDev .04 .08 .0009 %RSD .1488 .2065 .1770 41 28.63 38.54 .4870 #2 28.55 38.38 .4853 #3 28.59 38.42 .4857 Mg 54.76 .10 .1906 54.87 54.67 54.74 Standardization Rpt. 03/22/06 07:19:23 AM ;thod: CLP1 Standard: StdFURNH n Time: 03/22/06 07:13:37 Elem As1890 2203/1 2203/2 1960/1 1960/2 T11908 Avge .90319 3.1665 1.2588 .67015 .48804 .74291 SDev .00352 .0160 .0039 .00279 .00177 .00278 %RSD .39010 .50485 .30852 .41688 .36181 .37421 #1 .89917 3.1553 1.2543 .66944 ..48674 .74308 #2 .90573 3.1593 1.2616 .66778 .48734 .74005 #3 .90468 3.1848 1.2604 .67323 .49005 .74560 page 1 Standardization Rpt. thod: CLP1 Standard: StdMULTH n Time: 03/22/06 07:19:29 1.454 Elem B Ba Be Avge 1.192 4.746 4.970 SDev .001 .003 .008 %RSD .1071 .0695 .1541 #1 1.191 4.750 4.961 #2 1.193 4.744 4.976 #3 1.193 4.745 4.972 Elem Mn Mo Ni Avge 13.50 1.340 1.444 SDev .02 .003 .002 %RSD .1462 .1989 .1205 #1 13.47 1.337 1.442 #2 13.51 1.342 1.445 #3 13.50 1.342 1.445 Elem v Zn Avge 1.013 3.386 SDev .001 .006 %RSD .0781 .1904 #1 1.012 3.379 1.013 3.391 1.013 3.388 03/22/06 07:26:03 AM page 1 Cd 1.083 1.082 1.080 Co Cr Cu 40.24 1.454 1.835 1.281 .07 .003 .003 .001 .1671 .1729 .1782 .0961 40.16 1.452 1.831 1.282 40.29 1.456 1.837 1.280 40.26 1.456 1.836 1.281 Si Sn Sr Ti 1.082 6.817 9.544 1.663 .002 .009 .003 .001 1509 .1317 .0276 .0658 6.808 9.547 1.662 6.826 9.543 1.664 6.816 9.543 1.664 O O Standardization Rpt. thod: CLP1 Standard: StdFENAL _n Time: 03/22/06 07:26:09 Elem Fe Na Avge 33.56 43.42 SDev .03 .05 %RSD .0815 .1096 #1 33.53 43.42 #2 33.56 43.37 43 33.58 43.47 03/22/06 07:31:09 AM page 1 P FM Standardization Rpt. thod: CLP1 Standard n Time: 03/22/06 07:31:16 Elem. K Na Avge 8.691 1.861 SDev .019 .005 %RSD .2219 .2722 #1 8.683 1.862 #2 8.713 1.865 #3 8.677 1.855 StdNAKH 03/22/06 07:35:28 AM page 1 Standardization Report 03/22/06 07:35:28 AM page 1 thod: CLP1 Slope = Conc(SIR)/IR Element Wavelen High std Low std Slope Y -intercept Date Standardized Ag 328.068 StdAGSBH StdBLANK 3096.82 11.0980 03/22/06 07:31:16 Al 308.215 StdICSH StdBLANK 17.4911 -.088017 03/22/06 07:31:16 As1890 189.042 StdFURNH StdBLANK 1106.03 1.04262 03/22/06 07:31:16 B 249.678 StdMULTH StdBLANK 4.20230 -.001653 03/22/06 07:31:16 Ba 493.409 StdMULTH StdBLANK 1.05356 -.000230 03/22/06 07:31:16 Be 313.042 StdMULTH StdBLANK 1.00607 .000804 03/22/06 07:31:16 Ca 317.933 StdICSH StdBLANK 1.49856 -.002069 03/22/06 07:31:16 Cd 226.502 StdMULTH StdBLANK .124247 .000060 03/22/06 07:31:16 Co 228.616 StdMULTH StdBLANK 3.43779 .000089 03/22/06 07:31:16 Cr 267.716 StdMULTH StdBLANK 2.72635 -.000951 03/22/06 07:31:16 Cu 324.754 StdMULTH StdBLANK 3.91205 -.011795 03/22/06 07:31:16 Fe 271.441 StdICSH StdBLANK 1.24069 .000016 03/22/06 07:31:16 Fe 259.940 StdFENAL StdBLANK .149037 -.001190 03/22/06 07:31:16 K 766.491 StdNAKH StdBLANK .920495 .002114 03/22/06 07:31:16 Mg 279.079 StdICSH StdBLANK 1.14374 .000264 03/22/06 07:31:16 Mn 257.610 StdMULTH StdBLANK .370464 -.000221 03/22/06 07:31:16 Mo 202.030 StdMULTH StdBLANK 3.73188 -.000954 03/22/06 07:31:16 Na 330.232 . StdNAKH StdBLANK 1.07149 -.005918 03/22/06 07:31:16 Na 588.995 StdFENAL StdBLANK .116080 -.040097 03/22/06 07:31:16 Ni 231.604 StdMULTH StdBLANK 3.46172 -.000841 03/22/06 07:31:16 2203/1 220.351 StdFURNH StdBLANK 317.329 -4.81033 03/22/06 07:31:16 2203/2 220.352 StdFURNH StdBLANK 793.855 .733681 03/22/06 07:31:16 2068/1 206.831 StdAGSBH StdBLANK 824.837 2.23863 03/22/06 07:31:16 2068/2 206.832 StdAGSBH StdBLANK 1295.64 -.940718 03/22/06 07:31:16 0/1 196.021 StdFURNH StdBLANK 1472.03 13.5198 03/22/06 07:31:16 0/2 196.022 StdFURNH StdBLANK 2058.57 -4.67425 03/22/06 07:31:16 Si 288.158 StdMULTH StdBLANK 5.15315 -.626532 03/22/06 07:31:16 Sn 189.989 StdMULTH StdBLANK .733576 -.001875 03/22/06 07:31:16 Sr 421.552 StdMULTH StdBLANK .523871 -.000059 03/22/06 07:31:16 Ti 334.941 StdMULTH StdBLANK 3.00673 -.001313 03/22/06 07:31:16 T11908 190.864 StdFURNH StdBLANK 1338.68 5.48041 03/22/06 07:31:16 v 292.402 StdMULTH StdBLANK 4.93700 -.000369 03/22/06 07:31:16 Zn 213.856 StdMULTH StdBLANK 1.47694 -.001134 03/22/06 07:31:16 Pb2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Sb2068 206.838 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Se1960 196.026 NONE NONE 1.00000 .000000 *NOT STANDARDIZED Standardization Readback Report thod: CLP1 Element Wavelength Standard Ag 328.068 StdBLANK StdAGSBH Element Wavelength Standard Al 308.215 StdBLANK StdICSH Element Wavelength Standard As1890 189.042 StdBLANK StdFURNH Element Wavelength Standard B 249.678 StdBLANK StdMULTH Element Wavelength Standard Ba 493.409 StdBLANK StdMULTH !meet Wavelength Standard 313.042 StdBLANK StdMULTH Element Wavelength Standard Ca 317.933 StdBLANK StdICSH Element Wavelength Standard Cd 226.502 StdBLANK StdMULTH Element Wavelength Standard Co 228.616 StdBLANK StdMULTH Element Wavelength Standard Cr 267.716 StdBLANK StdMULTH Element Wavelength Standard Cu 324.754 StdBLANK StdMULTH 03/22/06 07:35:28 AM Known Concentration .000000 2000.00 Known Concentration .000000 500.000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .005266 57.6118 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration .000000 500.000 Measured Concentration .000000 1000.00 Measured Concentration -.000000 5.00840 Measured Concentration -.000000 5.00000 Measured Concentration .000000 5.00095 Measured Signal .004894 38.4461 Measured Concentration .000000 4.99930 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00108 Measured Concentration -.000000 4.99875 page 1 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 -.000061 Residual Concentration .000000 -.008400 Residual Concentration .000000 -.000000 Residual Concentration -.000000 -.000950 Residual Signal .000371 19.1658 Residual Concentration -.000000 .000700 Residual Concentration -.000000 .000000 Residual Concentration -.000000 -.001080 Residual' Concentration .000000 O .001245 H Standardization Readback Report 03/22/06 07:35:28 AM .006759 .005046 Known Measured ement Wavelength Standard Signal Signal Fe 271.441 StdBLANK .000055 .000031 Known StdICSH .602976 .485989 .000000 -.000000 Known Measured Element Wavelength Standard Concentration Concentration Fe 259.940 StdBLANK .000000 .000000 Known StdFENAL 5.00000 5 00000 Element Wavelength Standard K 766.491 StdBLANK StdNAKH Element Wavelength Standard Mg 279.079 StdBLANK StdICSH Element Wavelength Standard Mn 257.610 StdBLANK StdMULTH Element Wavelength Standard 202.030 StdBLANK StdMULTH Element Wavelength Standard Na 330.232 StdBLANK StdNAKH Element Wavelength Standard Na 588.995 StdBLANK StdFENAL Element Wavelength Standard Ni 231.604 StdBLANK StdMULTH Element Wavelength Standard 2203/1 220.351 StdBLANK StdFURNH Element Wavelength Standard 2203/2 220.352 StdBLANK StdFURNH Known Measured Signal Signal .006759 .005046 8.00205 8.69091 Known Measured Signal Signal .000584 .000280 62.6316 54.7602 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Signal Signal -.028601 -.021169 1.98779 1.86068 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.99790 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.000 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 page 2 Residual Signal .000024 .116987 Residual Concentration -.000000 .000000 Residual Signal .001713 -.688854 Residual Signal .000304 7.87143- Residual .87143Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Signal -.007432 .127107 Residual Concentration -.000000 .000000 Residual Concentration .000000 .002100 Residual Concentration .000000 .000061 Residual � Concentration -.000000 V) .000000 0 0/) H Standardization Readback Report 03/22/06 07:35:28 AM ement Wavelength Standard 2068/1 206.831 StdBLANK StdAGSBH Element Wavelength Standard 2068/2 206.832 StdBLANK StdAGSBH Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNH Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNH Element Wavelength Standard Si 288.158 StdBLANK StdMULTH Element Wavelength Standard 189.989 StdBLANK StdMULTH Element Sr Element Ti Element T11908 Element V Wavelength Standard 421.552 StdBLANK StdMULTH Wavelength Standard 334.941 StdBLANK StdMULTH Wavelength Standard 190.864 StdBLANK StdFURNH Wavelength Standard 292.402 StdBLANK StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 2000.00 Known Concentration .000000 1000.00 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Element Wavelength Standard Concentration Zn 213.856 StdBLANK .000000 StdMULTH 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration .000000 2000.00 Measured Concentration -.000000 1000.00 Measured Concentration -.000000 1000.000 Measured Concentration -.000000 4.94713 Measured Concentration .000000 4.99870 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 Measured Concentration -.000000 1000.00 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00000 page 3 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.000061 Residual Concentration .000000 .000061 Residual Concentration .000000 .052870 Residual Concentration -.000000 .001300 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual � Concentration' .000000 kn .000000 O O V1 E' -i Standardization Readback Report 03/22/06 07:35:28 AM ement Wavelength Standard Pb2203 220.353 NONE NONE Element Wavelength Standard Sb2068 206.838 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Analysis Report 03/22/06 07:42:55 AM page 1 thod: CLP1 Sample Name: ICV Operator: MAG n Time: 03/22/06 07:35:35 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm . ppm ppm ppm Avge 979.82 48.80 501.00 2.622 2.627 2.623 48.84 SDev .98 .03 2.36 .002 .000 .002 %RSD .10021 .0674 .47069 .0641 .0186 .0836 .06 .1293 41 980.95 48.82 499.01 2.620 2.628 2.624 48.86 #2 979.34 48.83 503.61 2.623 2.627 2.625 48.90 #3 979.16 48.76 500.39 2.621 2.627 2.621 48.77 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm Ppm Ppm Ppm Ppm Avge 2.584 2.509 2.587 2.669 48.17 82.91 50.25 SDev .003 .003 .003 .002 .06 .03 .06 %RSD .1352 .1230 .0988 .0759 .1246 .0402 .1128 #1 2.585 2.508 2.587 2.671 48.19 82.95 50.26 #2 2.586 2.513 2.589 2.670 48.23 82.89 50.30 2.580 2.507 2.584 2.667 48.11 82.90 50.18 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.497 2.645 80.68 2.469 486.93 479.67 982.94 SDev .002 .005 .12 .002 1.28 .20 2.77 %RSD .0736 .1824 .1535 .0876 .26357 .04100 .28140 #1 2.498 2.639 80.68 2.467 486.27 479.65 981.90 42 2.498 2.649 80.80 2.471 488.41 479.49 980.84 #3 2.495 2.646 80.55 2.468 486.12 479.88 986.07 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 978.13 500.41 498.88 3.158 2.512 2.553 2.695 SDev 3.41 2.49 1.18 .005 .002 .001 .001 %RSD .34877 .49662 .23559 .1566 .0781 .0370 .0365 #1 980.35 497.89 497.56 3.153 2.511 2.554 2.696 979.85 502.86 499.82 3.162 2.510 2.552 2.695 974.20 500.47 499.25 3.159 2.514 2.552 2.694 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 07:42:55 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 495.17 2.498 2.625 482.09 979.73 499.39 SDev 3.22 .001 .002 .32, 1.41 1.60 %RSD .64962 .0585 .0882 .06705 .14376 .32000 41 498.71 2.499 2.626 481.86 980.87 497.67 #2 494.38 2.499 2.627 482.46 980.18 500.83 #3 492.42 2.496 2.622 481.96 978.16 499.66 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 03/22/06 07:50:21 AM page 1 thod: CLP1 Sample Name: ICVL Operator: MAG n Time: 03/22/06 07:43:01 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm Ppm Ppm Avge .32849 .0124 .55535 .0052 .0009 .0009 .0182 SDev .22491 .0056 .77737 .0009 .0003 .0003 %RSD 68.468 45.18 139.98 17.88 34.66 37.60 .0065 35.53 #1 .55061 .0185 .44153 .0060 .0012 .0012 #2 .33396 .0114 -.15884 .0054 .0009 .0008 .0250 #3 .10089 .0074 1.3833 .0042 .0006 .0006 .0176 .0121 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0010 .0009 .0010 .0007 2.427 .0805 .0167 SDev .0003 .0003 .0004 .0005 .003 .0140 .0063 %RSD 27.12 37.87 39.04 73.90 .1058 17.40 37.74 #1 .0012 .0012 .0012 .0011 2.429 .0955 .0233 #2 .0009 .0007 .0011 .0008 2.429 .0780 .0159 1 .0007 .0007 .0005 .0001 2.425 .0679 .0108 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0008 .0067 2.489 .0004 -.75319 -.05227 .99363 SDev .0003 .0031 .019 .0004 1.07140 1.50469 1.2864 %RSD 38.04 46.88 .7602 108.9 142.25 2878.7 129.47 #1 .0011 .0103 2.509 .0005 -1.3778 1.0373 2.4131 #2 .0008 .0055 2.486 -.0001 -1.3657 .57502 .66305 #3 .0005 .0043 2.472 .0007 .48394 -1.7691 -.09523 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.55135 4.0538 .03559 .0182 .0023 .0009 .0010 SDev 1.72957 .8220 1.2674 .0091 .0011 .0003 .0004 %RSD 313.70 20.278 3561.5 49.97 49.23 36.75 39.97 #1 .27589 3.1714 .47184 .0281 .0015 .0012 .0015 -2.5392 4.1920 1.0272 .0102 .0035 .0008 .0010 .60925 4.7980 -1.3923 .0164 .0017 .0006 .0006 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 07:50:21 AM page 2 igh Zn Low Sb2068 Elem T11908 Units ppb Avge 2.8563 SDev 1.1117 %RSD 38.921 #1 4.1015 #2 2.5034 #3 1.9638 Errors NOCHECK High 3475.5 Low .0013 v Zn Pb2203 Sb2068 Se1960 Ppm PPM Ppb Ppb Ppb .0009 .0011 -.28565 -.03685 1.3737 .0003 .0003 .65293 1.28079 .7060 34.90 28.50 228.58 3475.5 51.396 .0013 .0014 .23310 .98759 1.3708 .0008 .0010 -.07121 -1.4728 2.0811 .0007 .0008 -1.0188 .37468 .66908 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 07:57:47 AM page 1 thod: CLP1 Sample Name: ICB Operator: MAG n Time: 03/22/06 07:50:27 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.03477 -.0006 .16783 .0012 .0002 .0001 .0040 SDev .26442 .0006 1.6374 .0002 .0000 .0001 .0012 %RSD 760.52 100.6 975.62 13.98 26.00 41.21 30.57 #1 .18785 .0000 1.3608 .0013 .0002 .0002 .0054 #2 -.32704 -.0012 .84160 .0010 .0001 .0001 .0036 #3 .03488 -.0007 -1.6989 .0013 .0001 .0001 .0031 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0002 .0001 -.0003 .0040 .0498 .0051 SDev .0001 .0003 .0001 .0001 .0013 .0018 .0004 %RSD 27.20 146.9 53.66 31.30 31.41 3.629 7.155 #1 .0003 .0004 .0001 -.0003 .0053 .0518 .0056 #2 .0003 -.0002 .0000 -.0003 .0038 .0484 .0049 s .0002 .0005 .0001 -.0002 .0028 .0491 .0049 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0001 .0016 .0073 -.0000 .15609 -.82392 -.29874 SDev .0000 .0005 .0041 .0002 .72800 .67471 1.13485 %RSD 20.50 31.37 56.20 3521. 466.39 81.890 379.88 #1 .0001 .0019 .0117 .0002 -.58962 -.35223 -.68492 #2 .0001 .0018 .0066 -.0001 .86498 -.52277 .97880 #3 .0001 .0010 .0036 -.0001 .19292 -1.5968 -1.1901 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.03650 2.5917 .44625 -.0291 .0015 .0002 .0002 SDev .61696 .4044 2.2832 .0055 .0002 .0000 .0000 %RSD 1690.5 15.603 511.64 19.04 12.01 24.84 12.01 #1 .64197 2.1422 -1.3441 -.0350 .0016 .0002 .0003 -.18757 2.9258 -.33451 -.0284 .0014 .0001 .0002 -.56389 2.7070 3.0174 -.0240 .0017 .0001 .0003 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 07:57:47 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .80619 -.0001 .0001 -.49756 -.12381 1.1607 SDev 2.0660 .0002 .0001 .47356 .56170 1.5887 %RSD 256.27 270.0 74.04 95.178 453.69 136.88 #1 3.1256 -.0003 .0001 -.43126 .20013 -.18319 #2 .13018 -.0000 .0001 -.06063 .20085 .75120 #3 -.83716 .0001 .0000 -1.0008 -.77240 2.9141 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 03/22/06 08:05:13 AM 1 page -thod: CLP1 Sample Name: CRII Operator: MAG a Time: 03/22/06 07:57:53 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm ppm Ppm Avge 18.804 .0002 19.294 .2045 .0001 .0108 SDev .095 .0012 1.006 .0006 .0000 .0000 .0033 %RSD .50521 701.5 5.2131 .2709 13.60 .0784 .0006 19.88 #1 18.722 -.0004 18.862 .2039 .0001 .0109 #2 18.782 .0015 20.444 .2050 .0001 .0040 #3 18.908 -.0006 18.577 .2047 .0001 .0108 .0108 .0028 .0031 Errors LC Pass NOCHECK LC Pass NOCHECK NOCHECK LC Pass NOCHECK High 26.000 26.000 Low 14.000 14.000 .0130 .0070 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm ppm ppm ppm ppm ppm Avge .0108 .1013 .0211 .0521 .0003 .0470 SDev .0001 .0004 .0002 .0003 .0004 .0018 .0032 %RSD 1.386 .4165 1.072 .4794 145.7 3.725 .0015 48.86 #1 .0107 .1009 .0209 .0'518 .0008 .0465 #2 .0109 .1013 .0210 .0521 .0001 .0455 .0050 .0024 .0107 .1017 .0213 .0523 -.0000 .0489 .0022 r;rrors LC Pass LC Pass LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0130 .1300 .0260 .0650 Low .0070 .0700 .0140 .0350 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0303 .0228 .0012 .0808 3.9165 5.7849 116.51 SDev .0001 .0005 .0024 .0003 1.9207 .5229 %RSD .1966 2.146 206.6 .4358 49.040 9.0396 .94 .80544 #1 .0303 .0223 .0039 .0804 3.0824 6.0559 116.52 #2 .0303 .0231 .0004 .0810 6.1132 6.1167 115.57 #3 .0304 .0231 -.0007 .0810 2.5539 5.1821 117.44 Errors LC Pass LC Pass NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0390 .0260 .1040 Low .0210 .0140 .0560 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 117.52 12.533 11.025 .0798 .0801 .0001 .2174 SDev 1.48 1.097 .635 .0267 .0008 .0000 .0004 %RSD 1.2596 8.7558 5.7573 33.53 .9702 14.51 .1760 #1 115.92 12.383 10.298 .1104 .0805 .0001 .2173 117.79 13.698 11.469 .0675 .0793 .0001 .2171 118.85 11.519 11.308 .0613 .0807 .0001 .2178 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Ln O O E-+ Analysis Report 03/22/06 08:05:13 AM ;figh .1040 Low .0560 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 20.359 .1006 .0436 5.1628 117.18 11.527 SDev .336 .0002 .0000 .9082 1.13 %RSD 1.6481 .1975 .0719 17.592 .96727 .623 5.4046 #1 20.746 .1005 .0437 5.0657 116.12 10.992 #2 20.141 .1008 .,0436 6.1156 117.05 12.211 #3 20.191 .1004 .0436 4.3069 118.38 11.378 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 30.000 .1300 .0520 9.0000 180.00 13.000 Low 10.000 .0700 .0280 3.0000 60.000 7.0000 page 2 Analysis Report 03/22/06 08:12:39 AM page 1 thod: CLP1 Sample Name: ICSAI Operator: MAG a Time: 03/22/06 08:05:19 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .45047 495.6 -1.1210 -.0040 .0020 .0003 496.1 SDev .20959 3.2 2.8809 .0006 .0001 .0000 2.0 %RSD 46.525 .6451 257.00 14.02 2.715 4.057 .3960 #1 .22530 498.3 -1.4495 -.0036 .0020 .0003 497.2 #2 .48627 496.4 -3.8236 -.0039 .0021 .0003 497.2 #3 .63986 492.1 1.9101 -.0047 .0020 .0003 493.8 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0018 -.0012 .0042 .0007 199.1 .0458 498.0 SDev .0001 .0003 .0004 .0001 1.1 .0029 2.3 %RSD 5.479 24.91 9.099 15.56 .5439 6.328 .4562 #1 .0017 -.0014 .0039 .0008 199.9 .0426 499.7 #2 .0019 -.0014 .0046 .0007 199.6 .0482 499.0 .0018 -.0009 .0041 .0005 197.9 .0466 495.5 Errors LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass High .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0074 -.0045 .0303 .0019 2.8623 -3.7449 -4.4289 SDev .0002 .0002 .0003 .0001 1.0578 1.9327 3.5903 96RSD 2.501 4.923 .8907 5.815 36.956 51.609 81.066 #1 -.0074 -.0044 .0305 .0018 1.6517 -5.9311 -8.5552 #2 -.0073 -.0043 .0304 .0020 3.3271 -2.2632 -2.0178 #3 -.0077 -.0047 .0300 .0020 3.6080 -3.0405 -2.7137 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 2.5084 6.4356 -3.5159 -.0170 .0323 -.2926 .0023 SDev .9048 4.8596 3.8631 .0057 .0014 .0011 .0001 %RSD 36.070 75.511 109.88 33.28 4.392 .3904 1.996 #1 2.0009 11.692 -6.2827 -.0112 .0337 -.2931 .0023 3.5529 2.1057 .89768 -.0173 .0322 -.2934 .0024 1.9712 5.5094 -5.1626 -.0224 .0309 -.2913 .0023 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 08:12:39 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 8.0742 .0004 .0015 -1.5447 .19827 -.20202 SDev 2.2350 .0002 .0001 1.6259 1.6166 1.45671 %RSD 27.681 63.91 4.417 105.26 815.38 721.06 #1 8.4864 .0005 .0015 -3.4059 -1.5143 -.29726 #2 5.6618 .0001 .0016 -.40154 1.6979 1.3000 #3 H10.074 .0005 .0015 -.82650 .41116 -1.6088 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 00 O O Analysis Report 03/22/06 08:20:05 AM page 1 ;thod: CLP1 Sample Name: ICSABI Operator: MAG n Time: 03/22/06 08:12:45 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1068.1 498.8 1039.3 .9829 .5607 .5467 503.2 SDev .7 .2 .1 .0014 .0006 .0008 1.2 %RSD .06296 .0434 .01213 .1427 .1098 .1367 .2323 #1 1068.9 499.0 1039.2 .9823 .5613 .5458 501.9 #2 1067.6 498.6 1039.3 .9820 .5605 .5470 503.4 #3 1067.8 498.7 1039.4 .9845 .5602 .5472 504.2 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 1.017 .4955 .5283 .5882 201.4 .0479 503.0 SDev .002 .0008 .0009 .0011 .3 .0032 .4 %RSD .1532 .1634 .1711 .1879 .1508 6.681 .0802 #1 1.015 .4945 .5273 .5895 201.0 .0443 502.5 #2 1.018 .4958 .5286 .5879 201.4 .0504 503.0 1.018 .4960 .5291 .5873 201.6 .0489 503.3 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .4972 1.066 .0328 .9596 993.98 983.02 -12.293 SDev .0003 .002 .0005 .0015 3.74 1.69 1.359 %RSD .0646 .2220 1.450 .1608 .37665 .17180 11.057 #1 .4968 1.066 .0324 .9580 990.70 982.38 -12.096 #2 .4974 1.064 .0326 .9596 998.06 981.74 -13.740 #3 .4973 1.069 .0333 .9610 993.19 984.93 -11.043 Errors LC Pass- NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -5.4103 1042.5 1028.5 .8515 1.067 -.2956 .0025 SDev 4.5037 4.9 7.8 .0030 .004 .0004 .0013 %RSD 83.242 .47419 .75823 .3545 .3780 .1523 52.38 #1 -10.026 1036.8 1037.5 .8485 1.066 -.2951 .0017 -1.0272 1045.5 1023.8 .8515 1.063 -.2958 .0040 -5.1783 1045.3 1024.1 .8545 1.071 -.2960 .0018 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 08:20:05 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1011.5 .5088 1.115 986.67 -7.7023 1033.2 SDev 5.3 .0009 .001 1.34 2.7717 3.6 %RSD .52031 .1741 .1094 .13559 35.986 .34411 #1 1006.3 .5084 1.113 985.15 -10.715 1037.3 #2 1016.9 .5082 1.115 987.17 -5.2606 1031.0 #3 1011.4 .5098 1.116 987.68 -7.1313 1031.2 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 Analysis Report 03/22/06 08:27:31 AM page 1 :thod: CLP1 Sample Name: CCV1 Operator: MAG Ln Time: 03/22/06 08:20:11 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 985.16 48.94 507.92 2.653' 2.622 2.659 49.63 SDev 1.28 .02 1.56 .005 .001 .004 .04 %RSD .12956 .0396 .30802 .1832 .0538 .1623 .0767 #1 983.80 48.95 507.28 2.647 2.621 2.655 49.59 #2 985.36 48.92 509.70 2.654 2.622 2.661 49.64 #3 986.33 48.96 506.77 2.657 2.623 2.663 49.67 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.622 2.537 2.616 2.668 48.81 82.75 50.93 SDev .006 .005 .004 .001 .05 .01 .01 %RSD .2155 .2007 .1669 .0528 .1056 .0176 .0269 #1 2.615 2.531 2.611 2.667 48.75 82.74 50.92 #2 2.624 2.538 2.617 2.668 48.81 82.74 50.95 3 2.626 2.541 2.619 2.669 48.86 82.77 50.94 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.521 2.664 80.88 2.493 492.46 483.37 989.90 SDev .004 .007 .10 .006 1.02 2.68 3.57 %RSD .1523 .2692 .1212 .2357 .20643 .55421 .36020 #1 2.516 2.656 80.77 2.487 492.27 480.33 985.92 #2 2.522 2.666 80.94 2.496 491.55 484.38 992.79 #3 2.524 2.669 80.94 2.498 493.56 485.39 991.00 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 984.29 513.46 504.59 3.217 2.533 2.556 2.709 SDev .72 2.58 1.23 .050 .005 .001 .003 %RSD .07272 .50320 .24421 1.556 .2017 .0523 .1088 #1 984.16 510.75 503.25 3.176 2.528 2.554 2.706 983.64 513.74 505.67 3.202 2.538 2.556 2.710 985.06 515.90 504.84 3.273 2.533 2.557 2.711 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 O O F-+ Analysis Report 03/22/06 08:27:31 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 500.83 2.517 2.661 486.40 986.16 507.54 SDev 1.93 .002 .004 1.93 1.23 1.56 %RSD .38446 .0806 .1386 .39669 .12501 .30684 #1 501.75 2.515 2.657 484.31 984.75 505.75 #2 502.13 2.517 2.661 486.77 986.69 508.36 #3 498.62 2.519 2.664 488.11 987.04 508.52 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 03/22/06 08:34:58 AM page 1 :hod: CLP1 Sample Name: CCVL1 Operator: MAG Z Time: 03/22/06 08:27:37 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .39072 .0313 -.36822 .0045 .0008 .0007 .0374 SDev .35544 .0157 .83669 .0009 .0003 .0003 .0184 %RSD 90.971 50.16 227.22 19.09 43.23 47.94 49.25 #1 .77969 .0487 .56413 .0055 .0012 .0011 .0576 #2 .08282 .0273 -.61511 .0042 .0007 .0007 .0330 #3 .30965 .0181 -1.0537 .0039 .0005 .0004 .0216 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0009 .0006 .0006 .0000 2.423 .0662 .0356 SDev .0004 .0002 .0002 .0003 .002 .0156 .0185 %RSD 41.35 34.77 42.66 874.5 .0982 23.59 51.85 #1 .0013 .0009 .0008 .0004 2.426 .0840 .0557 #2 .0008 .0006 .0006 -.0000 2.421 .0601 .0318 .0006 .0004 .0003 -.0003 2.421 .0546 .0194 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0006 .0062 2.451 .0006 -1.4748 .36122 -.27395 SDev .0003 .0026 .010 .0004 .9373 .94211 .23888 %RSD 49.80 42.47 .3969 66.74 63.554 260.82 87.199 #1 .0010 .0091 2.456 .0008 -.40992 -.50319 -.06604 #2 .0005 .0058 2.456 .0010 -1.8398 .22143 -.53488 #3 .0004 .0038 2.439 .0002 -2.1747 1.3654 -.22092 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.41936 3.7023 .74689 -.0619 .0011 .0007 .0008 SDev 1.30620 .9707 .51812 .0238 .0003 .0003 .0004 %RSD 311.47 26.218 69.370 38.39 29.54 45.81 49.07 #1 .43455 4.7964 .96080 -.0349 .0010 .0010 .0013 -1.9230 3.3663 1.1238 -.0713 .0009 .0006 .0008 .23038 2.9443 .15607 -.0795 .0015 .0004 .0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK M 00 Ln O O UD E-{ Analysis Report 03/22/06 08:34:58 AM page 2 igh Zn Low Sb2068 Elem T11908 Units ppb Avge 2.7319 SDev 1.7208 %RSD 62.989 #1 3.9948 #2 3.4290 #3 .77192 Errors NOCHECK High 255.71 Low .0012 v Zn Pb2203 Sb2068 Se1960 PPM PPM ppb Ppb Ppb .0007 .0008 -.25015 -.37092 1.7311 .0004 .0004 .37824 .94848 .5893 52.18 51.68 151.21 255.71 34.040 .0012 .0013 -.47210 .26787 2.2381 .0006 .0008 -.46493 -1.4608 1.8706 .0005 .0004 .18659 .08012 1.0846 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 7t 00 O O Analysis Report 03/22/06 08:42:24 AM page 1 thod: CLP1 Sample Name: CCB1 Operator: MAG n Time: 03/22/06 08:35:04 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm Ppm ppm Ppm Avge .01299 .0036 -.94423 .0015 .0001 .0001 .0078 SDev .18089 .0019 .91746 .0002 .0000 .0001 %RSD 1392.9 52.04 97.164 15.61 53.80 88.35 .0023 29.46 #1 -.08756 .0049 -.61529 .0017 .0001 .0001 #2 .22181 .0044 -1.9808 .0015 .0001 .0001 .0101 #3 -.09530 .0014 -.23659 .0012 .0001 .0000 .0078 .0055 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 .2000 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0001 -.0001 -.0007 .0051 .0367 .0069 SDev .0001 .0001 .0001 .0001 .0015 .0031 %RSD 71.25 70.01 69.52 8.317 29.98 8.546 .0013 19.11 #1 .0003 .0001 -.0001 -.0006 .0066 .0403 #2 .0002 .0000 -.0003 -.0007 .0053 .0349 .0084 .0065 .0000 .0002 -.0001 -.0007 .0035 .0348 .0058 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge -.0000 .0018 .0002 -.0002 -1.6164 -.33846 -.67893 SDev .0000 .0005 .0028 .0003 .0651 .33360 .88380 %RSD 15640. 24.87 1721. 228.1 4.0285 98.565 130.17 #1 .0000 .0023 .0031 -.0005 -1.6430 .04524 -.20423 #2 -.0000 .0015 -.0001 -.0002 -1.6639 -.55985 -.13392 #3 -.0000 .0017 -.0025 .0002 -1.5421 -.50076 -1.6986 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.23774 2.7414 .44871 -.1082 .0003 .0001 .0001 SDev 1.20268 .7417 .46824 .0080 .0008 .0000 .0001 %RSD 505.88 27.054 104.35 7.370 295.8 45.98 74.73 #1 1.1186 3.0190 .75360 -.1003 -.0006 .0001 .0002 -.65760 1.9010 -.09042 -.1078 .0005 .0000 .0000 -1.1742 3.3043 .68295 -.1163 .0010 .0001 .0000 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 08:42:24 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.5056 -.0001 -.0002 -.76398 -.38464 1.2122 SDev 1.1013 .0003 .0001 .21767 1.01706 .5543 %RSD 73.145 219.3 23.15 28.491 264.42 45.727 #1 2.7764 .0001 -.0003 -.51692 .67811 1.5080 #2 .83035 -.0000 -.0002 -.92749 -.48320 .57274 #3 .91003 -.0005 -.0002 -.84752 -1.3488 1.5559 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 03/22/06 08:49:51 AM page 1 thod: CLP1 Sample Name: MB -16445 Operator: MAG Time: 03/22/06 08:42:30 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .17950 .0033 .03739 .0013 .0000 -.0000 .0094 SDev .13671 .0006 .41937. .0002 .0000 .0000 .0017 %RSD 76.160 16.86 1121.5 17.18 23.25 66.93 17.71 #1 .06250 .0034 .38879 .0015 .0001 -.0000 .0112 #2 .14622 .0027 -.42685 .0011 .0001 -.0000 .0091 #3 .32977 .0038 .15025 .0014 .0000 -.0000 .0079 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0001 .0009 -.0005 .0251 .0376 .0055 SDev .0002 .0001 .0001 .0001 .0008 .0001 .0007 %RSD 203.9 138.4 5.975 18.46 3.239 .3675 13.06 #1 -.0001 .0001 .0009 -.000.6 .0259 .0376 .0063 ? .0003 .0002 .0009 -.0006 .0250 .0377 .0056 I .0001 -.0000 .0010 -.0004 .0243 .0374 .0048 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -,0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0001 .0009 -.0012 -.0002 -1.9830 -.31059 .24549 SDev .0000 .0003 .0008 .0001 .8370 .24728 .,56400 %RSD 47.87 34.50 65.41 67.31 42.208 79.616 229.75 #1 .0000 .0006 -.0003 -.0000 -1.2545 -.46596 .51936 #2 .0001 .0012 -.0014 -.0002 -2.8973 -.44037 -.40315 #3 .0001 .0007 -.0019 -.0002 -1.7973 -.02544 .62026 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.3362 .03278 -.60251 -.1212 -.0000 .0000 .0001 SDev 1.0771 .87780 2.30639 .0024 .0004 .0000 .0001 %RSD 80.607 2677.8 382.79 2.015 1729. 20.90 38.28 R 1.83'73 .25957 -2.2045 -.1188 -.0003 .0001 .0001 .09988 -.93616 -1.6440 -.1212 ..0005 .0000 .0001 2.0715 .77494 2.0409 -.1237 -.0002 .0000 .0002 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 08:49:51 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.4217 .0002 .0038 -.86748 .97304 -.39094 SDev 1.1601 .0000 .0000 .34331 .90621 1.74104 96RSD 81.598 .4167 .9998 39.576 93.132 445.34 #1 1.5393 .0002 .0038 -.72851 1.3985 -1.3839 #2 .20729 .0002 .0038 -1.2585 -.06761 -1.4083 #3 2.5184 .0002 .0038 -.61544 1.5883 1.6194 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 00 O O H Analysis Report 03/22/06 08:57:17 AM page 1 thod: CLP1 Sample Name: LCS-16445 Operator: MAG n Time: 03/22/06 08:49:57 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 976.52 49.25 500.49 2.743 2.645 2.684 49.73 SDev 1.23 .06 .77 .003 .004 .001 .03 %RSD .12589 .1145 .15323 .0939 .1667 .0439 .0588 #1 977.93 49.29 501.13 2.745 2.649 2.686 49.74 42 975.68 49.18 499.64 2.740 2.641 2.683 49.75 #3 975.95 49.26 500.70 2.744 2.647 2.684 49.70 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 60.00 600.00 3.000 3.000 3.000 60.00 Low 800.00 40.00 400.00 2.000 2.000 2.000 40.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.629 2.550 2.645 2.706 49.08 81.81 50.50 SDev .001 .002 .001 .005 .02 .14 .03 %RSD .0262 .0667 .0496 .1712 .0372 .1737 .0526 #1 2.630 2.552 2.646 2.711 49.09 81.95 50.53 #2 2.629 2.551 2.644 2.701 49.09 81.67 50.49 2.629 2.548 2.644 2.707 49.06 81.79 50.48 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 3.000 3.000 3.000 3.000 60.00 96.00 60.00 Low 2.000 2.000 2.000 2.000 40.00 64.00 40.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.544 2.700 81.30 2.509 492.10 482.85 969.49 SDev .001 .002 .05 .002 .60 1.87 1.89 %RSD .0452 .0784 .0577 .0730 .12141 .38659 .19485 41 2.546 2.699 81.28 2.511 491.59 481.30 971.66 42 2.544 2.699 81.27 2.510 491.96 484.92 968.52 #3 2.544 2.703 81.35 2.507 492.76 482.34 968.28 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 3.000 96.00 3.000 Low 2.000 64.00 2.000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 965.28 485.28 485.24 4.717 2.555 2.580 2.754 SDev 2.66 2.29 .15 .028 .004 .004 .003 %RSD .27598 .47151 .03062 .5880 .1742 .1642 .1189 #1 965.31 482.75 485.40 4.723 2.559 2.585 2.757 967.93 487.20 485.22 4.742 2.556 2.576 2.750 962.60 485.91 485.11 4.687 2.550 2.580 2.754 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 08:57:17 AM .gh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 496.45 2.544 2.646 485.93 966.68 485.26 SDev 1.10 .003 .002 1.27 1.93 .69 %RSD .22176 .1173 .0648 .26224 .19933 .14136 #1 496.89 2.548 2.648 484.73 967.42 484.52 #2 495.19 2.542 2.646 487.27 968.13 485.88 #3 497.26 2.544 2.645 485.81 964.49 485.37 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 600.00 3.000 3.000 600.00 1200.0 600.00 Low 400.00 2.000 2.000 400.00 800.00 400.00 page 2 Analysis Report 03/22/06 09:04:43 AM page 1 thod: CLP1 Sample Name: 0603561-009G Operator: MAG n Time: 03/22/06 08:57:23 Comment: TSL005 F^IAJ Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .54139 .0646 -1.3425 .1154 .0858 .0008 13.42 SDev .30744 .0185 2.2365 .0006 .0002 .0004 .05 %RSD 56.787 28.68 166.58 .5010 .2591 54.82 .4033 #1 .63009 .0599 -.15722 .1160 .0861 .0012 13.41 #2 .79474 .0851 .05176 .1153 .0857 .0009 13.48 #3 .19935 .0489 -3.9222 .1149 .0857 .0003 13.38 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0011 .0027 .0085 .0108 .1131 13.02 9.736 SDev .0006 .0006 .0009 .0008 .0101 .05 .027 %RSD 51.26 22.09 10.17 7.293 8.896 .4101 .2812 #1 .0016 .0031 .0086 .0113 .1159 13.00 9.722 #2 .0013 .0031 .0093 .0112 .1214 12.97 9.767 #3 .0005 .0020 .0076 .0099 .1019 13.08 9.719 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb age 1.368 .0047 14.81 .0097 2.0678 2.8604 .66623 Iev .001 .0019 .06 .0010 .8246 1.3219 1.0507 %RSD .0900 40.75 .3924 10.71 39.877 46.215 157.70 #1 1.367 .0067 14.79 .0099 1.6910 3.4588 .45421 #2 1.369 .0046 14.76 .0106 3.0135 3.7773 1.8067 #3 1.367 .0029 14.87 .0086 1.4990 1.3451 -.26226 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.4443 .86471 1.0499 5.180 .0019 .0807 .0026 SDev .7891 2.5768 3.0487 .010 .0022 .0003 .0007 %RSD 54.636 297.99 290.38 .2010 114.0 .4104 26.30 #1 -.93629 2.1607 -1.0612 5.191 .0009 .0811 .0029 #2 -2.3534 -2.1028 4.5451 5.172 .0044 .0804 .0030 #3 -1.0432 2.5362 -.33426 5.175 .0004 .0807 .0018 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.7343 .0009 .0174 2.5965 -.74148 .98825 SDev 1.6531 .0007 .0005 1.0894 .25003 1.2025 96RSD 95.315 77.34 2.723 41.956 33.720 121.68 ##1 3.3743 .0016 .0177 2.8702 -.47324 .01176 #2 1.7604 .0010 .0176 3.5230 -.96805 2.3314 43 .06840 .0002 .0168 1.3964 -.78315 .62161 Analysis Report 03/22/06 09:12:09 AM page 1 :hod: CLP1 Sample Name: 0603561-009GDUP Operator: MAG z Time: 03/22/06 09:04:49 Comment: TSL005 14 W - S's CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .27459 .0369 -.57618 .1174 .0879 .0001 13.77 SDev .16808 .0015 .50026 .0001 .0004 .0000 .07 %RSD 61.209 4.059 86.823 .1227 .4531 32.99 .5028 #1 .24796 .0362 -.69710 .1174 .0880 .0001 13.75 #2 .12142 .0358 -.02655 .1173 .0875 .0001 13.71 #3 .45440 .0386 -1.0049 .1176 .0883 .0000 13.85 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0003 .0023 .0074 .0104 .0557 13.97 10.02 SDev .0001 .0004 .0001 .0002 .0006 .07 .04 %RSD 28.29 19.17 1.477 1.722 1.166 .4875 .4038 #1 .0002 .0026 .0073 .0105 .0563 13.97 10.01 #2 .0003 .0025 .0075 .0102 .0550 13.90 9.985 #3 .0003 .0018 .0074 .0104 .0558 14.04 10.06 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ge 1.406 .0014 15.35 .0090 2.0962 2.6522 -.64921 ev .007 .0001 .08 .0002 2.0067 .7347 .79314 %RSD .4700 4.745 .4956 2.299 95.730 27.702 122.17 #1 1.404 .0014 15.36 .0088 2.2183 2.8118 -1.2629 #2 1.400 .0014 15.27 .0092 4.0391 1.8507 -.93104 #3 1.413 .0013 15.42 .0091 .03123 3.2939 .24636 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .14318 .77744 .32697 5.340 .0008 .0825 .0015 SDev 1.9688 2.2419 .28782 .024 .0004 .0004 .0001 %RSD 1375.0 288.37 88.027 .4543 54.13 .5133 6.003 #1 2.1462 1.3715 .12793 5.338 .0010 .0825 .0016 #2 .07300 2.6624 .65698 5.317 .0003 .0821 .0015 #3 -1.7896 -1.7017 .19598 5.366 .0011 .0830 .0015 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .67603 -.0001 .0189 2.4671 -.12066 .47699 SDev .94019 .0001 .0001 .2255 1.06826 .88217 %RSD 139.08 83.16 .2927 9.1403 885.31 184.94 #1 -.40285 -.0002 .0188 2.6143 1.0110 .54207 #2 1.3203 -.0001 .0189 2.5795 -.26133 1.3248 #3 1.1106 -.0000 .0189 2.2075 -1.1116 -.43591 N O O V/ H Analysis Report 03/22/06 09:19:35 AM page 1 hod: CLP1 Sample Name: 0603561-009GMS Operator: MAG Time: 03/22/06 09:12:15 Comment: TSL005 MW -ES JAS Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 48.693 1.994 39.080 .7149 2.186 .0529 13.42 SDev .349 .003 .705 .0022 .005 .0001 .03 %RSD .71610 .1701 1.8042 .3084 .2197 .2909 .2590 #1 48.395 1.992 38.327 .7123 2.184 .0527 13.38 #2 48.608 1.991 39.724 .7163 2.183 .0529 13.43 #3 49.077 1.998 39.190 .7160 2.192 .0530 13.45 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0525 .4986 .2163 .2765 1.003 13.23 9.745 SDev .0002 .0017 .0008 .0005 .002 .02 .024 %RSD .3198 .3405 .3835 .1824 .2437 .1184 .2474 #1 .0523 .4968 .2154 .2761 1.000 13.23 9.721 #2 .0525 .4988 .2165 .2763 1.002 13.21 9.745 #3 .0527 .5002 .2170 .2771 1.005 13.24 9.769 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 TTnits ppm ppm ppm ppm ppb ppb ppb ge 1.866 .0009 14.87 .5053 21.437 21.716 494.51 ev .005 .0001 .01 .0012 1.034 .913 1.17 %RSD .2534 10.81 .0502 .2356 4.8212 4.2025 .23605 #1 1.861 .0010 14.88 .5041 21.380 22.336 493.46 #2 1.866 .0009 14.86 .5052 22.498 20.668 494.30 #3 1.871 .0008 14.88 .5065 20.433 22.143 495.77 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 499.89 12.218 10.439 5.224 -.0007 .0800 .0012 SDev 2.18 .881 .415 .014 .0013 .0002 .0001 %RSD .43590 7.2117 3.9800 .2593 196.0 .2459 7.138 #1 497.46 11.564 10.035 5.210 .0003 .0800 .0011 #2 500.55 11.871 10.418 5.225 -.0002 .0798 .0012 #3 501.67 13.220 10.865 5.237 -.0022 .0802 .0012 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 48.349 .5010 .5511 21.623 498.10 11.032 SDev 1.429 .0016 .0011 .373 1.82 .564 %RSD 2.9547 .3238 .2078 1.7240 .36448 5.1130 #1 47.753 .4996 .5499 22.018 496.13 10.544 #2 47.315 .5006 .5511 21.277 498.47 10.902 #-4 49.979 .5027 .5522 21.574 499.71 11.650 Analysis Report 03/22/06 09:27:01 AM page 1 thod: CLP1 Sample Name: 0603561-009GS15 Operator: MAG z Time: 03/22/06 09:19:42 Comment: TSL005 N(tgf - S SD Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .10804 .0073 -.49103 .0242 .0177 -.0000 2.735 SDev .23575 .0005 1.85208 .0004 .0003 .0000 .004 %RSD 218.21 6.901 377.18 1.764 1.434 507.1 .1558 #1 .37816 .0078 -1.8136 .0247 .0180 .0000 2.735 #2 -.05629 .0072 -1.2852 .0239 .0176 -.0000 2.731 #3 .00225 .0068 1.6257 .0241 .0175 .0000 2.739 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0000 .0006 .0017 .0014 .0218 2.475 1.965 SDev .0002 .0002 .0003 .0001 .0001 .005 .004 %RSD 364.9 33.12 15.46 5.871 .3638 .2072 .2020 #1 .0002 .0008 .0018 .0014 .0219 2.479 1.966 #2 -.0001 .0004 .0014 .0013 .0218 2.469 1.961 #3 .0001 .0008 .0019 .0014 .0218 2.478 1.968 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ge .2790 .0003 2.854 .0018 .44002 .78422 .21706 ev .0003 .0005 .000 .0004 .87841 .88494 1.3982 %RSD .1206 176.0 .0106 21.92 199.63 112.84 644.13 #1 .2790 .0001 2.854 .0015 -.55266 .71908 -.71178 #2 .2786 .0008 2.853 .0015 1.1168 -.06635 -.46210 #3 .2793 -.0001 2.854 .0022 .75594 1.6999 1.8251 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.25745 2.2657 .05906 .9428 .0004 .0159 .0003 SDev 1.22601 .8236 1.5265 .0042 .0010 .0000 .0000 %RSD 476.22 36.351 2584.6 .4489 278.8 .0488 9.699 #1 -1.4866 3.0250 -1.3092 .9445 .0009 .0159 .0003 #2 .96535 1.3902 -.21918 .9380 -.0008 .0158 .0003 #3 -.25104 2.3818 1.7055 .9459 .0011 .0159 .0003 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.8215 .0003 .0064 .66964 -.09942 .79388 SDev .2558 .0003 .0001 .62027 .97821 .98879 %RSD 14.043 93.59 1.713 92.628 983.95 124.55 #1 2.0332 .0004 .0065 .29562 -1.2286 .13414 #2 1.5373 -.0000 .0065 .32766 .49003 .31674 #3 1.8939 .0005 .0063 1.3856 .44032 1.9308 Analysis Report 03/22/06 09:34:28 AM page 1 thod: CLP1 Sample Name: 0603561-4"0 Operator: MAG n Time: 03/22/06 09:27:08 Comment: TSL005 Mode: CONC Corr. Factor: 1- Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm Ppm PPn► Avge .24359 .0420 -1.0583 .0888 .0442 .0000 11.19 SDev .04791 .0007 1.4861 .0007 .0001 .0000 96RSD 19.670 1.636 140.42 .7388 .2120 35.19 .02 .1405 #1 .20786 .0419 .59906 .0893 .0443 .0000 11.19 #2 .22488 .0414 -1.5019 .0880 .0442 .0000 11.17 #3 .29804 .0427 -2.2721 .0890 .0442 .0000 11.20 Elem Cd Cc Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0027 .0023 .0057 .0577 8.905 3.017 SDev .0000 .0001 .0000 .0001 .0002 .008 .000 %RSD 24.52 2.714 1.004 1.738 .2694 .0848 .0151 #1 .0002 .0028 .0023 .0058 .0577 8.913 3.016 #2 .0002 .0026 .0023 .0056 .0575 8.899 3.017 #3 .0001 .0028 .0023 .0056 .0578 8.902 3.017 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ge 1.092 .0006 5.109 .0037 .63958 1.8734 -.38408 ev .001 .0004 .006 .0003 1.0973 .9587 .60155 %RSD .1176 71.10 .1174 6.692 171.56 51.172 156.62 #1 1.092 .0006 5.116 .0039 1.2609 .77260 -.98935 #2 1.090 .0002 5.107 .0038 1.2852 2.3228 -.37656 #3 1.093 .0010 5.105 .0034 -.62738 2.5248 .21367 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .03755 3.6036 -.50409 5.783 .0001 .0289 .0016 SDev .10305 2.4623 1.26923 .011 .0007 .0000 .0000 %RSD 274.41 68.328 251.79 .1871 690.4 .0726 2.129 41 .01481 6.3965 -.96536 5.792 .0004 .0289 .0017 #2 .15007 1.7460 -1.4782 5.771 .0006 .0289 .0016 #3 -.05223 2.6684 .93127 5.787 -.0007 .0289 .0017 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .97555 .0002 .0241 1.4626 -.10283 .86380 SDev .45353 .0001 .0001 .5211 .19020 1.0985 %RSD 46.490 63.27 .3115 35.630 184.96 127.17 V) 41 1.4169 .0003 .0241 .93529 -.31956 1.4861' #2 .99907 .0001 .0241 1.9773 -.02528 -.40452 #3 .51072 .0003 .0242 1.4752 .03633 1.5098 O O H Analysis Report 03/22/06 09:41:55 AM page 1 thod: CLP1 Sample Name: 0603561-002G Operator: MAG ___n Time: 03/22/06 09:34:34 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .19134 .0416 -.44698 .0427 .0147 .0000 3.731 SDev .20019 .0005 .51369 .0001 .0001 .0000 .016 %RSD 104.62 1.188 114.92 .3593 .3322 50.52 .4218 #1 .36179 .0416 -.18960 .0426 .0147 .0000 3.722 #2 .24135 .0421 -1.0385 .0428 .0147 .0000 3.749 #3 -.02911 .0411 -.11286 .0428 .0146 .0000 3.722 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0002 .0014 .0027 .0028 .0971 12.51 1.117 SDev .0001 .0002 .0001 .0002 .0004 .03 .002 %RSD 30.10 13.31 3.558 6.345 .3857 .2389 .2137 #1 .0002 .0015 .0028 .0028 .0970 12.48 1.118 #2 .0002 .0014 .0027 .0030 .0975 12.54 1.120 #3 .0001 .0012 .0026 .0026 .0968 12.51 1.115 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ,ge .3572 .0017 14.51 .0016 .84760 .21541 -1.1670 __iev .0013 .0003 .04 .0003 .84229 1.1576 .8280 %RSD .3508 18.33 .2655 19.10 99.374 537.43 70.95.3 #1 .3564 .0017 14.47 .0014 -.02889 -.05552 -1.1669 #2 .3587 .0020 14.55 .0020 .92077 1.4845 -.33900 #3 .3567 .0013 14.50 .0015 1.6509 -.78275 -1.9950 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.5539 2.5681 1.2914 1.613 .0005 .0085 .0032 SDev .3921 1.3505 2.4278 .009 .0008 .0000 .0001 %RSD 25.230 52.589 188.00 .5302 162.5 .4587 2.051 #1 -1.8655 4.1221 3.9337 1.608 .0015 .0085 .0032 #2 -1.1137 1.9032 .78148 1.623 -.0000 .0086 .0033 #3 -1.6825 1.6789 -.84093 1.609 .0001 .0085 .0031 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .33833 .0001 .0314 .42600 -1.4250 1.7165 SDev 2.4108 .0001 .0001 .75509 .4990 2.0574 %RSD 712.58 41.78 .4845 177.25 35.018 119.86 #1 -.48629 .0001 .0313 -.04658 -1.6328 3.9964 #2 3.0533 .0002 .0316 1.2968 -.85570 1.1550 4PI -1.5520 .0002 .0313 .02773 -1.7866 -.00182 O O Analysis Report 03/22/06 09:49:21 AM :hod: CLP1 Sample Name: 0603561-003G Operator: MAG ____i Time: 03/22/06 09:42:01 Comment: TSL005 MW_0 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .17823 .0301 -.81857 .0437 .0145 .0000 SDev .23795 .0005 .93536 .0006 .0001 .0000 %RSD 133.51 1.740 114.27 1.411 .3425 89.26 #1 -.02965 .0300 -1.4708 .0434 .0145 .0000 #2 .12657 .0307 -1.2380 .0444 .0145 .0000 #3 .43775 .0297 .25308 .0433 .0144 .0000 Elem Cd Cc Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0000 .0012 .0020 .0033 .0472 12.17 SDev .0000 .0001 .0001 .0001 .0001 .03 %RSD 162.9 9.617 5.094 2.750 .2886 .2521 #1 -.0000 .0012 .0020 .0032 .0473 12.21 #2 .0001 .0011 .0021 .0034 .0472 12.17 #3 .0000 .0014 .0019 .0034 .0470 12.14 Elem Mn Mo Na Ni 2203/1 2203/2 TTnits ppm ppm ppm ppm ppb ppb -ge .3464 .0015 14.05 .0016 1.7857 .81076 __iev .0006 .0006 .04 .0006 .4849 1.0890 %RSD .1589 39.15 .2559 40.50 27.153 134.32 #1 .3468 .0010 14.09 .0022 1.5257 .21742 #2 .3465 .0013 14.05 .0009 2.3451 .14728 #3 .3458 .0021 14.02 .0016 1.4863 2.0676 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .36172 1.9765 -.49047 1.533 -.0008 .0083 SDev 1.3305 1.0615 1.58816 .005 .0005 .0000 %RSD 367.82 53.703 323.81 .3421 71.20 .1548 #1 .12741 2.7662 .56640 1.537 -.0013 .0083 #2 -.83603 2.3936 .27899 1.535 -.0008 .0083 #3 1.7938 .76989 -2.3168 1.527 -.0002 .0083 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.4471 -.0000 .0377 1.1354 -.11434 .33107 SDev .7018 .0002 .0001 .6496 .85113 1.4118 %RSD 48.499 841.4 .1493 57.208 744.41 426.44 #1 -1.8611 -.0002 .0377 .65309 -.51449 1.2989 #2 -1.8435 -.0000 .0378 .87918 -.69164 .98316 4z -.63676 .0002 .0377 1.8740 .86313 -1.2889 page 1 Ca ppm 3.635 .005 .1440 3.640 3.636 3.630 Mg ppm 1.078 .003 .2543 1.080 1.079 1.074 206.8/1 ppb -1.0679 .7013 65.670 -1.8003 -.40248 -1.0010 Ti ppm .0017 .0001 6.783 .0017 .0018 .0016 Analysis Report 03/22/06 09:56:48 AM page 1 :hod: CLP1 Sample Name: 0603561-004G Operator: MAG ,.-.1 Time: 03/22/06 09:49:27 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .11070 .0500 -.53859 .0827 .0419 .0000 10.55 SDev .16614 .0023 1.16141 .0001 .0001 .0000 .04 %RSD 150.07 4.577 215.64 .1432 .1996 34.65 .3685 #1 -.02849 .0476 -.00624 .0825 .0419 .0000 10.50 42 .29463 .0502 .26123 .0828 .0418 .0000 10.56 #3 .06598 .0522 -1.8707 .0827 .0420 .0000 10.58 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 .0036 .0035 .0061 .0754 8.857 2.872 SDev .0002 .0003 .0002 .0004 .0006 .027 .009 %RSD 169.9 7.951 5.266 5.987 .7368 .3021 .3010 #1 -.0000 .0034 .0033 .0057 .0748 8.879 2.863 #2 .0004 .0039 .0037 .0064 .0755 8.827 2.872 #3 .0000 .0034 .0034 .0061 .0759 8.866 2.881 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 TT..lits ppm ppm ppm ppm ppb ppb ppb rge 1.072 .0003 5.030 .0041 2.0129 1.0946 -1.9454 -Jev .003 .0003 .023 .0006 .2984 .3931 .7135 %RSD .2751 117.8 .4664 13.46 14.824 35.914 36.675 #1 1.069 .0002 5.052 .0037 2.0993 1.4280 -1.4934 #2 1.073 .0006 5.005 .0047 2.2587 .66111 -2.7679 #3 1.075 -.0000 5.033 .0039 1.6809 1.1948 -1.5749 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.2497 2.9497 -1.1989 5.394 .0003 .0273 .0019 SDev 1.4862 2.8401 1.4915 .013 .0007 .0001 .0001 %RSD 118.92 96.285 124.41 .2470 230.6 .3751 5.028 #1 .58916 .03678 -.49961 5.385 -.0002 .0273 .0019 ##2 2.9516 5.7110 -.18551 5.389 .0010 .0272 .0020 #3 .20829 3.1.014 -2.9115 5.409 .0001 .0274 .0019 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.5750 -.0001 .0263 1.4005 .18573 .18262 SDev 1.2589 .0001 .0001 .2323 ).75902 1.4126 %RSD 48.888 63.77 .4860 16.589 408.66 773.52 ##1 1.1884 -.0001 .0262 1.6516 -.10430 -.32097 #2 2.8904 -.0001 .0264 1.1932 1.0470 1.7780 -� 3.6462 -.0000 .0264 1.3568 -.38551 -.90920 00 O O H Analysis Report 03/22/06 10:04:14 AM page 1 :hod: CLP1 Sample Name: CCV2 Operator: MAG ____i Time: 03/22/06 09:56:54 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 983.66 49.14 509.92 2.654 2.610 2.657 49.52 SDev 1.97 .09 5.42 .008 .005 .010 .20 %RSD .19999 .1786 1.0631 .2976 .1944 .3824 .3980 #1 981.79 49.08 503.67 2.648 2.605 2.647 49.35 ##2 983.49 49.10 512.77 2.652 2.610 2.656 49.48 ##3 985.71 49.24 513.32 2.663 2.615 2.668 49.74 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.638 2.514 2.609 2.651 49.04 82.26 50.61 SDev .011 .008 .009 .003 .19 .09 .15 %RSD .4117 .3075 .3603 .1232 .3959 .1056 .3005 #1 2.628 2.507 2.600 2.648 48.85 82.22 50.48 ? 2.637 2.514 2.607 2.650 49.02 82.19 50.57 t 2.650 2.522 2.619 2.654 49.24 82.36 50.77 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.513 2.664 80.67 2.506 488.89 .484.04 981.09 SDev .009 .015 .12 .010 2.60 1.61 3.99 %RSD .3395 .5659 .1462 .3807 .53263 .33231 .40641 #1 2.505 2.649 80.66 2.497 485.90 482.21 976.81 #2 2.511 2.664 80.56 2.505 490.11 485.24 981.77 ##3 2.522 2.679 80.79 2.516 490.65 484.66 984.70 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 991.29 520.90 514.56 3.047 2.497 2.539 2.704 SDev 2.55 4.41 2.96 .058 .008 .005 .008 %RSD .25738 .84570 .57603 1.902 .3090 .2026 .2845 4f1 988.88 516.47 511.94 3.114 2.492 2.535 2.697 991.02 525.28 513.96 3.018 2.493 2.539 2.703 993.96 520.96 517.77 3.010 2.506 2.545 2.712 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 10:04:14 AM Lgh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 500.27 2.503 2.658 485.65 987.89 516.67 SDev 2.66 .007 .008 1.92 3.01 2.85 %RSD .53073 .2887 .3168 .39540 .30455 .55096 #1 497.30 2.496 2.651 483.44 984.86 513.45 #2 501.09 2.502 2.655 486.86 987.94 517.73 #3 502.42 2.510 2.667 486.65 990.88 518.84 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report -thod: CLP1 Sample Name: CCVL2 in Time: 03/22/06 10:04:21 NOCHECK -)mment: TSL005 High Mode: CONC Corr. Factor: 1 Low Elem Ag Al As1890 Units ppb ppm ppb Avge .21139 .0155 .70530 SDev .18621 .0031 .46963 %RSD 88.089 19.68 66.585 #1 .26700 .0181 .82883 #2 .36346 .0163 .18626 #3 .00371 .0121 1.1008 Errors NOCHECK NOCHECK NOCHECK High NOCHECK LC Pass High Low 2.750 Low Elem Cd Co Cr Units ppm ppm ppm Avge .0006 .0006 .0004 SDev .0003 .0003 .0002 %RSD 51.68 53.42 45.89 #1 .0009 .0009 .0006 #2 .0006 .0005 ul 5.8266 -.29166 .0004 03/22/06 10:11:41 AM page 1 Operator: MAG B ppm .0043 .0007 16.58 .0050 .0042 .0036 NOCHECK Cu ppm -.0006 .0004 58.77 -.0002 -.0007 -.0009 NOCHECK Ni ppm .0002 .0003 122.9 .0006 .0000 .0001 NOCHECK Si ppm -.1354 .0154 11.38 -.1194 -.1368 -.1501 NOCHECK Ba ppm .0006 .0002 39.03 .0008 .0006 .0004 NOCHECK Fe ppm 2.416 .003 .1268 2.418 2.417 2.413 LC Pass 2.750 2.250 2203/1 ppb -1.0787 .5557 51.517 -1.4022 -.43702 -1.3968 NOCHECK Sn ppm .0003 .0002 85.83 .0001 .0001 .0005 NOCHECK Be ppm .0006 .0002 38.61 .0008 .0006 .0004 NOCHECK K ppm .0597 .0138 23.04 .0742 .0581 .0468 NOCHECK 2203/2 ppb -.34525 .70457 204.07 .42672 -.50883 -.95364 NOCHECK Sr ppm .0005 .0002 43.71 .0008 .0005 .0003 NOCHECK Ca ppm .0096 .0052 54.58 .0152 .0087 .0048 NOCHECK Mg ppm .0112 .0050 44.62 .0168 .0097 .0072 NOCHECK 2068/1 ppb -.42004 .95456 227.25 .57973 -1.3218 -.51803 NOCHECKCA Ti ppm .0007 .0004 52.15 .0011 .0008 .0003 NOCHECK .00D3 .0003 .0002 --rors NOCHECK NOCHECK NOCHECK High Low Elem Mn Mo Na Units ppm ppm ppm Avge .0005 .0062 2.399 SDev .0003 .0024 .013 %RSD 57.22 38.87 .5235 #1 .0008 .0089 2.414 #2 .0005 .0052 2.392 #3 .0002 .0045 2.392 Errors NOCHECK NOCHECK LC Pass High 2.750 Low 2.250 Elem 2068/21960/1 1960/2 Units ppb ppb ppb Avge -.07523 4.4125 -.07884 SDev 1.28271 1.5921 1.46004 %RSD 1705.1 36.082 1852.0 #1 -1.2841 4.7227 1.4759 1.2704 5.8266 -.29166 -.21201 2.6881 -1.4208 Errors NOCHECK NOCHECK NOCHECK 03/22/06 10:11:41 AM page 1 Operator: MAG B ppm .0043 .0007 16.58 .0050 .0042 .0036 NOCHECK Cu ppm -.0006 .0004 58.77 -.0002 -.0007 -.0009 NOCHECK Ni ppm .0002 .0003 122.9 .0006 .0000 .0001 NOCHECK Si ppm -.1354 .0154 11.38 -.1194 -.1368 -.1501 NOCHECK Ba ppm .0006 .0002 39.03 .0008 .0006 .0004 NOCHECK Fe ppm 2.416 .003 .1268 2.418 2.417 2.413 LC Pass 2.750 2.250 2203/1 ppb -1.0787 .5557 51.517 -1.4022 -.43702 -1.3968 NOCHECK Sn ppm .0003 .0002 85.83 .0001 .0001 .0005 NOCHECK Be ppm .0006 .0002 38.61 .0008 .0006 .0004 NOCHECK K ppm .0597 .0138 23.04 .0742 .0581 .0468 NOCHECK 2203/2 ppb -.34525 .70457 204.07 .42672 -.50883 -.95364 NOCHECK Sr ppm .0005 .0002 43.71 .0008 .0005 .0003 NOCHECK Ca ppm .0096 .0052 54.58 .0152 .0087 .0048 NOCHECK Mg ppm .0112 .0050 44.62 .0168 .0097 .0072 NOCHECK 2068/1 ppb -.42004 .95456 227.25 .57973 -1.3218 -.51803 NOCHECKCA Ti ppm .0007 .0004 52.15 .0011 .0008 .0003 NOCHECK ! i Analysis Report 03/22/06 10:11:41 AM igh .uow Elem Units T11908 ppb v Zn Pb2203 Sb2068 Se1960 Avge 4.4108 PPM .0006 PPM Ppb Ppb Ppb SDev 1.4461 .0001 .0007 .0003 -.589.45 -.19003 1.4168 %RSD 32.786 17.81 43.11 .46828 79.444 .54594 287.29 1.3356 94.267 #1 #2 4.8824 5.5622 .0006 .0009 -.18229 -.66341 2.5571 #3 2.7877 .0006 .0005 :0007 -.48488 .40720 1.7457 .0004 -1.1012 -.31390 -.05251 Errors High NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Low page 2 Analysis Report 03/22/06 10:19:07 AM page 1 thod: CLP1 Sample Name: CCB2 Operator: MAG n Time: 03/22/06 10:11:47 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units Avge ppb .25362 Ppm Ppb Ppm Ppm Ppm Ppm SDev .25352 .0071 .0022 .89328 .80874 .0006 .0001 .0001 -.0015 %RSD 99.959 31.70 90.536 .0005 72.45 .0001 75.48 .0000 62.20 .0010 64.34 #1 #2 .46556 .0093 1.6852 .0012 .0002 .0001 -.0004 #3 .32253 .0048 .92594 .0003 .0000 .0001 -.0020 -.02723 .0072 .06870 .0005 .0000 .0000 -.0022 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 .2000 -.2000 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm .0002 ppm ppm Ppm Ppm Ppm Ppm SDev .0001 .0002 .0002 .0001 .0002 -.0012 .0003 .0021 .0370 .0030 %RSD 79.01 114.6 296.4 23.93 .0011 51.36 .0053 14.32 .0032 106.6 #1 #2 .0003 .0004 .0002 -.0009 .0033 .0427 .0059 .0002 .0000 -.0000 -.0015 .0018 .0323 -.0003 .0000 .0001 -.0000 -.0012 .0012 .0361 .0033 Errors High LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass .0050 .0500 .0100 .0250 .1000 5.000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 .2000 -.2000 Elem Units Mn Mo Na Ni 2203/1 2203/2 2068/1 Avge ppm .0000 ppm .0017 ppm -.0043 ppm -.0004 Ppb -1.3754 Ppb -.04679 Ppb SDev .0001 .0007 .0023 .0002 .2353 .54622 .70826 %RSD 336.0 38.83 52.83 50.99 17.111 1167.4 .57618 81.351 #1 #2 .0001 .0023 -.0018 -.0003 -1.6182 .00852 .81265 #3 -.0001 .0017 -.0050 -.0007 -1.1483 -.61856 1.2251 .0000 .0010 -.0062 -.0003 -1.3596 .46967 .08702 Errors High LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.5640 3.7791 1.1583 -.1575 .0005 .0001 SDev .6168 1.4237 .9059 .0026 .0010 .0001 .0002 %RSD 39.440 37.672 78.205 1.633 205.7 70.48 .0001 73.21 #1 -1.7637 2.9710 2.1397 -.1554 .0015 .0001 .0003 -2.0562 5.4229 .35423 -.1568 .0005 .0001 .0001 -.87202 2.9433 .98098 -.1604 -.0005 .0000 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 10:19:07 AM :igh Low Elem Units T11908 ppb v Zn Pb2203 Sb2068 Se1960 Avge 1.6259 Ppm -.0000 Ppm .0000 Ppb -.48916 Ppb -.80730 Ppb 2.0310 SDev %RSD .7488 .0003 .0001 .32994 .22242 .3912 46.054 1216. 251.3 67.449 27.551 19.259 #1 #2 1.8527 -.0000 .0001 -.53312 -.90577 2.4166 #3 2.2349 .0002 .0000 -.79492 -.96348 2.0421 .78988 -.0003 -.0000 -.13945 -.55264 1.6345 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 Analysis Report 03/22/06 10:26:34 AM t page 1 thod: CLP1 Sample Name: 0603561-005G Operator: MAG n Time: 03/22/06 10:19:13 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Units Ag ppb Al As1890 B Ba Be Ca Avge .11375 PPM .0724 Ppb .60661 Ppm Ppm Ppm PPM SDev .06810 .0014 .07267 .0897 .0003 .0470 .0000 .0001 11.79 %RSD 59.871 1.893 11.980 .3198 .0252 .0000 25.82 .02 .2112 #1 42 .05458 .0740 .68970 .0895 .0470 .0001 11.82 #3 .18819 .0715 .55487 .0900 .0470 .0001 11.78 .09847 .0718 .57528 .0896 .0470 .0001 11.78 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm .0002 PPM PPM PPM PPM PPM PPM SDev .0001 .0024 .0005 .0025 .0003 .0027 .0002 .0926 9.898 3.215 %RSD 26.94 18.85 13.91 7.547 .0006 .6302 .022 .2240 .006 .1863 #1 #2 .0003 .0029 .0028 .0029 .0932 9.885 3.222 #3 .0003 .0025 .0022 .0027 .0921 9.885 3.214 .0002 .0020 .0023 .0025 .0923 9.923 3.210 Elem Units Mn Mo Na Ni 2203/1 2203/2 2068/1 ppm Ppm PPM PPM Ppb Ppb Ppb ge 1.151 .0005 5.441 .0036 1.1400 -.37449 -.57891 ev %RSD .001 .0003 60.92 .015 .0006 .6650 .19626 .45087 .1082 .2823 17.81 58.332 52.406 77.882 #1 #2 1.152 .0007 5.432 .0043 .75062 -.24181 -1.0837 #3 1.150 .0002 5.432 .0032 .76158 -.28173 -.43686 1.150 .0007 5.459 .0032 1.9079 -.59994 -.21618 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units Avge ppb .54459 ppb 3.4474 Ppb -.43213 PPM 6.069 ppm PPM PPM SDev 1.8307 1.2216 1.97745 .008 -.0007 .0010 .0310 .0027 %RSD 336.17 35.436 457.60 .1280 146.0 .0000 .0562 .0002 6.121 #1 #2 .67467 2.2114 1.7950 6.075 .0003 .0309 .0029 #3 -1.3477 3.4768 -1.1096 6.060 -.0007 .0309 .0026 2.3068 4.6541 -1.9818 6.073 -.0016 .0310 .0027 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .21446 .0000 .0398 .12986 .17048 .85977 SDev .27221 .0001 .0001 .09193 1.2575 .93485 %RSD 126.93 2629. .3233 70.794 737.63 108.73 V) O_ #1 -.08699 .0002 .0400 .08869 .08915 1.9337 42 .44227 -.0001 .0398 .06571 -1.0444 .41767 V) #3 .28809 -.0000 .0397 .23518 1.4667 .22797 O O H Analysis Report 03/22/06 10:34:00 AM page 1 -�thod: ;in CLP1 Sample Name: 0603561-006G Operator: MAG Time: 03/22/06 10:26:40 Comment: TSL005 Mode: CONC Corr. Factor: 1 k% -y -b Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb ppm Ppm PPM Ppm Avge -.00741 .1171 .54892 .2378 .0514 .0,001 31.66 SDev .19624 .0004 .63588 .0008 .0001 .0000 %RSD 2649.2 .3439 115.84 .3225 .1580 12.10 .14 .4412 #1 .18464 .1174 -.14617 .2376 .0514 31.72 #2 .00072 .1172 1.1014 .23.87 .0514 .0001 .0001 31.76 #3 -.20758 .1166 .69154 .2372 .0513 .0001 31.50 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm PPM PPM PPM PPM ppm Avge .0002 .0084 .0052 .0228 .2304 51.53 21.90 SDev .0001 .0001 .0001 .0002 .0011 .06 %RSD 59.36 1.062 2.733 .9444 .4879 .1073 .07 .3420 #1 .0003 .0084 .0054 .0229 .2308 51.51 21.92 #2 .0001 .0085 .0052 .0230 .2312 51.59 21.96 #3 .0001 .0084 .0051 .0226 ..2291 51.49 21.81 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb age 4.559 .0008 73.88 .0186 3.3920 3.9973 -2.1681 )ev .018 .0002 .12 .0001 .5522 .8079 96RSD .3915 22.51 .1601 .2994 16.279 20.211 .4945 22.808- 2.808#1 #1 4.567 .0008 73.85 .0186 2.8234 4.5152 -2.0256 #2 4.572 .0006 74.01 .0186 3.4264 4.4103 -2.7182 43 4.539 .0009 73.78 .0187 3.9262 3.0664 -1.7605 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.0865 .86747 -1.4034 1.829 .0002 .2387 .0039 SDev 1.1604 1.0122 1.7338 .010 .0012 .0006 %RSD 106.80 116.68 123.54 .5714 635.4 .2302 .0001 3.235 #1 .65662 1.5164 -1.3270 1.836 .0007 .2390 #2 .20246 -.29885 -3.1741 1.835 .0011 .2391 .0040 #3 2.4005 1.3849 .29092 1.817 -.0012 .2381 .0038 .0038 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.6645 .0006 .0202 3.7958 .00277 -.64717 SDev .4723 .0002 .0001 .3892 .91624 1.45443 96RSD 17.724 39.48 .5915 10.254 33127. 224.74 110 O #1 2.3902 .000.8 .0202 3.9519 -.23652 -.38012 #2 3.2098 .0004 .0203 4.0827 -.77008 -2.2166 #3 2.3935 .0005 .0201 3.3528 1.0149 .65523 O O V) H Analysis Report 03/22/06 10:41:28 AM thod: CLP1 Time: Sample Name: 0603561-007G Operator: MAG n 03/22/06 10:34:07 Comment: TSL005 Mode: CONC Corr. Factor: 1 14W-45 Elem Ag Al As1890 B Ba Be Units Avge ppb .18394 ppm Ppb ppm ppm ppm SDev .29974 .1116 .0066 .34794 .2336 .0503 .0002 %RSD 162.96 5.903 .16691 47.970 .0006 .2786 .0003 .4890 .0002 102.1 #1 #2 .31113 .1085 .31250 .2332 .0501 .0001 #3 .39911 .1191 .52972 .2333 .0506 .0004 -.15843 .1071 .20160 .2344 .0503 .0001 Elem Cd Co Cr Cu Fe K Units. Avge Ppm .0002 Ppm ppm ppm ppm ppm SDev .0002 .0086 .0006 .0053 .0004 .0221 .1234 49.58 %RSD 84.66 6.983 7.926 .0004 2.033 .0051 4.112 .11 .2274 #1 #2 .0001 .0083 .0050 .0216 .1203 49.55 #3 .0005 .0092 .0057 .0225 .1293 49.48 .0001 .0082 .0050 .0220 .1207 49.70 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm Ppm ppm Ppb ppb ge 4.478 .0006 72.29 .0183 4.1306 3.3806 ev 96RSD .010 .0004 .12 .0010 .4570 .4247 .2340 72.05 .1640 5.460 11.065 12.564 #1 #2 4.467 .0011 72.19 .0173 3.9837 2.8904 #3 4.488 .0002 72.25 .0193 4.6431 3.6401 4.479 .0005 72.42 .0183 3.7651 3.6111 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .43529 2.2689 .39335 1.799 .0009 SDev 1.1701 2.5069 1.0913 .023 .0016 .2342 %RSD 268.80 110.49 277.44 1.261 184.1 .0002 .1018 #1 -.08921 3.2767 -.86652 1.781 .0003 #2 1.7758 4.1150 1.0009 1.824 .0026 .2340 #3 -.38075 -.58508 1.0456 1.790 -.0003 .2341 .2345 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .88652 .0006 .0174 3.6304 -.15906 1.0179 SDev .52354 .0003 .0002 .3609 .83960 %RSD 59.056 41.37 1.242 9.9414 527.85 .8834 86.782 #1 .60515 .0004 .0172 3.2545 -.57001 #2 1.4906 .0009 .0176 3.9742 .80685 .51318 2.0379 #3 .56383 .0006 .0173 3.6625 -.71402 .50264 page 1 Ca ppm 31.11 .11 .3382 31.01 31.22 31.08 Mg ppm 21.52 .05 .2112 21.47 21.56 21.54 2068/1 ppb -1.3496 .2014 14.925 -1.5331 -1.1341 -1.3816 Ti ppm 0039 0003 6.924 0038 0042 0038 Analysis Report 03/22/06 10:48:55 AM 1 page !thod: CLP1 Sample Name: 0603561-008G Operator: MAG [n Time: 03/22/06 10:41:34 Comment: TSL005 Mode: CONC Corr. Factor: 1 w Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb Ppm Ppm PPM Ppm Avge .84415 .0809 1.4969 .6310 .1340 .0001 81.78 SDev .19249 .0021 .6136 .0018 .0004 .0000 %RSD 22.803 2.641 40.990 .2914 .3147 19.47 .32 .3944 #1 .83246 .0786 2.0235 .6289 .1335 .0001 81.43 #2 1.0422 .0813 .82311 .6321 .1342 .0001 82.06 #3 .65778 .0828 1.6441 .6319 .1342 .0002 81.84 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM PPM PPM Avge .0004 .0205 .0058 .0220 .0807 137.3 56.55 SDev .0001 .0003 .0001 .0001 .0002 .4 %RSD 32.80 1.334 .8347 .5506 .2378 .3179 .18 .3126 #1 .0005 .0207 .0057 .0219 .0805 136.8 •56.36 #2 .0003 .0207 .0058 .0222 .0809 137.6 56.71 #3 .0003 .0202 .0058 .0220 .0806 137.5 56.58 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb age 12.47 -.0004 195.8 .0414 2.6509 2.7999 -3.9694 )ev .04 .0003 .6 .0008 .7610 1.3051 %RSD .3572 78.57 .3058 1.954 28.708 46.613 .9252 23.309 #1 12.42 -.0005 195.2 .0407 3.1914 4.0493 -4.3220 #2 12.51 -.0001 196.4 .0410 1.7806 1.4454 -4.6665 #3 12.48 -.0008 195.9 .0423 2.9808 2.9049 -2.9197 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 3.5087 2.2003 -.48585 4.808 .0000 .6675 .0028 SDev 1.7328 1.1201 .60405 .013 .0007 .0020 .0001 %RSD 49.386 50.906 124.33 .2787 8484. .3040 3.612 #1 3.8748 1.5288 -.40681 4.794 -.0007 .6652 .0028 #2 1.6221 1.5788 -1.1255 4.821 .0006 .6691 .0028 #3 5.0293 3.4933 .07478 4.808 .0001 .6682 .0030 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 5.0599 .0003 .0153 2.7503 1.0185 .40865 SDev .7432 .0002 .0002 1.1142 1.4313 .73416 %RSD 14.687 78.99 1.207 40.513 140.53 179.66 00 O #1 5.7773 .0003 .0151 3.7637 1.1453 .23776 #2 4.2934 .0005 .0154 1.5571 -.47197 -.22499 43 5.1090 .0001 .0153 2.9302 2.3823 1.2132 V) H Analysis Report 03/22/06 10:56:22 AM page 1 thod: CLP1 Sample Name: 0603561-@I:E))S03u36'- Operator: MAG Z Time: 03/22/06 10:49:02 Comment: TSL005 C QFC Mode: CONC Corr. Factor: 1 U;lzabc Elem Ag Al As1890 B Ba Be Ca Units Avge ppb .09009 ppm Ppb ppm Ppm Ppm Ppm SDev .28692 .0210 .0006 .17582 1.0125 .0022 .0009 .0001 .0685 %RSD 318.49 2.901 575.85 .0003 16.05 .0001 5.906 .0000 13.59 .0121 17.69 #1 .42128 .0217 1.2923 .0023 .0010 #2 -.06802 .0208 -.68290 .0025 .0009 .0001 .0821 #3 -.08300 .0205 -.08190 .0018 .0009 .0001 .0001 .0644 .0590 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm Ppm PPM Ppm Ppm Avge .0000 -.0001 .0012 -.0006 .0090 .1617 SDev .0001 .0004 .0002 .0002 .0002 .0304 .0203 %RSD 270.0 394.3 18.29 39.21 2.500 18.79 .0097 47.78 #1 #2 .0001 .0003 .0014 -.0004 .0091 .1964 .0315 .0001 -.0004 .0009 -.0009 .0092 .1487 #3 -.0001 -.0001 .0012 -.0006 .0088 .1399 .0150 .0145 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ge .0034 .0000 .1184 .0000 .58680 .09241 -1.0196 ev .0020 .0005 .0355 .0003 2.3991 1.0849 1.0471 %RSD 58.22 2271. 29.99 829.5 408.84 1174.0 102.70 #1 .0056 -.0005 .1574 .0004 -2.1201 1.1352 #2 .0028 .0003 .1098 -.0001 1.4300 .17233 .11905 -1.9412 #3 .0018 .0002 .0880 -.0002 2.4504 -1.0303 -1.2366 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb Ppm Ppm Ppm Ppm Avge .88092 2.3717 .88762 -.1682 -.0000 .0003 SDev .73329 1.3893 .26599 .0014 .0005 .0001 .0007 %RSD 83.242 58.577 29.967 .8461 1014. 47.59 .0001 9.079 #1 1.6590 1.9611 .85136 -.1698 -.0000 .0004 #2 .20271 3.9201 .64162 -.1678 -.0005 .0002 .0008 #3 .78100 1.2340 1.1699 -.1671 .0004 .0002 .0007 .0008 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .12072 -.0002 .0138 .25709 .24808 1.3818 SDev .99176 .0003 .0002 .29192 .83740 .3048 %RSD 821.56 156.1 1.528 113.55 337.55 22.056 #1 1.1530 .0001 .0138 .05123 1.1462 1.2209 _O #2 .03407 -.0005 .0136 .59118 -.51118 1.7334 #3 -.82488 -.0003 .0141 .12886 .10917 1.1913 O O Analysis Report 03/22/06 11:03:49 AM 1 page thod: CLP1 Sample Name: 0603561-011G Operator: MAG n Time: 03/22/06 10:56:28 Comment: TSL005 Mw -&S Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb Ppm ppm Ppm ppm Avge .39784 .0663 -.31209 .0941 .0460 .0001 11.93 SDev .21257 .0017 .87343 .0001 .0001 .0000 %RSD 53.432 2.497 279.87 .1564 .1907 9.760 .03 .2561 #1 .50572 .0682 -.63572 .0939 .0459 11.96 #2 .53484 .0657 -.97751 .0940 .0459 .0001 11.90 #3 .15296 .0651 .67697 .0942 .0461 .0001 .0001 11.92 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm ppm PPM ppm ppm PPM ppm SDev .0003 .0000 .0046 .0001 .0031 .0048 .0877 10.18 3.139 %RSD 10.23 3.084 .0001 3.979 .0002 4.825 .0004 .5151 .03 .2893 .004 .1408 #1 .0003 .0047 .0033 .0049 .0882 10.15 3.144 #2 .0003 .0045 .0030 .0045 .0873 10.17 3.136 #3 .0003 .0047 .0031 .0050 .0875 10.21 3.138 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb ge 1.247 .0003 5.041 .0039 .54353 2.0642 .17151: ev .002 .0004 .011 .0005 .76132 1.0817 %RSD .1685 141.3 .2157 12.73 140.07 52.401 .19853 115.76 #1 1.249 .0005 5.033 .0044 1.1267 1.1908 #2 1.245 -.0002 5.038 .0034 -.31774 3.2742 .26889 #3 1.247 .0005 5.053 .0040 .82161 1.7277 .30255 -.05691 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -1.2790 3.4324 .73885 6.043 -.0002 .0301 SDev 1.0157 1.1748 2.1234 .010 .0011 .0001 .0020 %RSD 79.416 34.229 287.40 .1594 541.3 .1995 .0002 11.91 #1 -1.0925 3.0389 -.80673 6.044 -.0006 .0301 #2 -2.3751 2.5048 -.13680 6.033 -.0010 .0302 .0023 #3 -.36949 4.7534 3.1601 6.052 .0010 .0301 .0018 .0020 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .26314 .0002 .0174 1.5579 -.79597 1.6358 SDev .93222 .0001 .0001 .4684 .62399 1.7847 %RSD 354.27 75.91 .4412 30.069 78.394 109.10 O #1 -.38287 .0003 .0175 1.1695 -.63911 .47386 #2 1.3318 .0001 .0174 2.0781 -1.4834 #3 -.15955 .0001 .0174 1.4261 -.26538 .74286 3.6907 O O F-+ Analysis Report 03/22/06 11:11:16 AM thod: CLP1 Sample Name: 0603561-012G Operator: MAG n Time: 03/22/06 11:03:55 Comment: TSL005 Mode: CONC Corr. Factor: 1 O, Elem Ag Al As1890 B Ba Be Units ppb Ppm ppb PPM Ppm ppm* Avge .16903 .0602 -.25365 .1137 .0446 .0001 SDev .13357 .0009 1.04142 .0006 .0001 %RSD 79.021 1.445 410.58 .4888 .1222 .0000 9.511 #1 .01501 .0605 -.53240 .1140 .0447 .0001 #2 .23912 .0592 .89878 .1131 .0446 .0001 #3 .25297 .0608 -1.1273 .1141 .0446 .0001 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0002 .0033 .0028 .0049 .0737 41.26 SDev .0001 .0003 .0001 .0001 .0001 .05 %RSD 39.01 7.472 4.344 2.753 .1586 .1126 #1 .0003 .0035 .0030 .0050 .0738 41.31 #2 .0001 .0033 .0029 .0050 .0736 41.22 #3 .0002 .0030 .0027 .0047 .0737 41.24 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb ge 1.115 .0038 46.86 .0040 2.4205 1.2030 rev .001 .0003 .05 .0001 .9778 .5223 %RSD .0513 6.683 .1040 2.645 40.398 43.416 #1 1.116 .0039 46.92 .0039 1.3288 1.5460 #2 1.115 .0039 46.82 .0041 2.7168 .60192 #3 1.115 .0035 46.85 .0039 3.2158 1.4612 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .48934 3.1788 .83895 5.573 -.0001 .0278 SDev 1.1134 1.0408 .58713 .004 .0008 .0000 %RSD 227.54 32.742 69.984 .0801 648.9 .1198 #1 1.7426 1.9776 1.3716 5.576 -.0010 .0279 #2 .11121 3.8120 .93590 5.568 .0006 .0278 #3 -.38578 3.7468 .20938 5.575 .0000 .0279 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.26922 .0003 .0452 1.6085 .33812 1.6181 SDev .42485 .0001 .0000 .3877 .73082 .2561 %RSD 157.81. 49.98 .0167 24.101 216.14 15.826 #1 -.15739 .0001 .0452 1.4737 1.1232 1.5734 #2 -.73879 .0002 .0452 1.3062 .21373 1.8937 43 .08853 .0004 .0451 2.0455 -.32252 1.3874 page 1 Ca ppm 11.93 .01 .0562 11.94 11.92 11.93 Mg PPM 3.604 .004 .1138 3.608 3.603 3.-600 2068/1 ppb .0352G .33471 950.83. -.11756 .41904 -.19587 Ti ppm .0028 .0001 2.011 .0028 .0028 .0029 Analysis Report 03/22/06 11:18:43 AM thod: CLP1 Sample Name: 0603561-013G Operator: MAG n Time: 03/22/06 11:11:22 Comment: TSL005 Mode: CONC Corr. Factor: 1 Kw- �S Elem Ag Al As1890 B Ba Be Units ppb PPM ppb ppm Ppm Ppm Avge .45818 .0635 .71845 .1161 .0453 SDev .04046 .0008 1.0125 .0005 .0002 .0001 %RSD 8.8300 1.315 140.92 .4129 .4153 .0000 9.773 #1 #2 .41146 .0630 .45386 .1156 .0452 .0001 #3 .48135 .0645 -.13546 .1166 .0455 .0001 .48172 .0631 1.8370 .1161 .0452 .0001 Elem Cd Co Cr Cu Fe K Units Avge ppm .0003 ppm ppm ppm ppm ppm SDev .0001 .0036 .0002 .0030 .0001 .0051 .0001 .0792 .0003 43.55 96RSD 49.14 6.133 2.189 1.961 .3599 .13 _2889 #1 #2 .0002 .0035 .0030 .0050 .0794 43.52 #3 .0004 .0036 .0029 .0052 .0793 43.69 .0002 .0039 .0030 .0051 .0789 43.44 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm Ppb Ppb ge 1.149 .0042 49.28 .0042 1.3375 2.0444 ev .003 .0003 .17 .0001 1.2246 =cxSD .3018 5.966 .3444 2.720 91.560 .1969 9.6331 41 #2 1.149 .0040 49.35 .0042 1.4285 2.2343 #3 1.153 .0045 49.41 .0041 .06994 2.0578 1.146 .0041 49.09 .0043 2.5141 1.8411 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .29656 3.0329 1.3926 5.694 .0007 SDev .51698 .6449 .6898 .016 .0011 .0281 %RSD 174.32 21.262 49.530 .2837 168.1 .0002 .5547 #1 .76808 3.7419 1.7399 5.689 -.0006 #2 -.25624 2.4814 .59823 5.712 .0014 .0281 43 .37785 2.8754 1.8397 5.681 .0012 .0283 .0280 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb Ppb Ppb Avge .26137 .0004 .0455 1.8091 .13597 1.9388 SDev 1.0828 .0001 .0001 .3612 .46945 %RSD 414.28 26.68 .3295 19.968 345.27 .6278 32.381 #1 1.3744 .0003 .0454 1.9660 .67803 2.4066 #2 .19816 .0005 .0457 1.3959 -.13780 1.2253 #3 -.78845 .0003 .0454 2.0653 -.13233 2.1846 page 1 Ca ppm 12.20 .04 .3107 12.20 12.23 12.16 Mg ppm 3.700 .012 .3213 3.698 3.712 3.689 2068/1 ppb -.18575 .86208 464.11 .49764 .09938 -1.1543 Ti ppm .0028 .0000 .3929 0028 0028 0028 Analysis Report 03/22/06 11:26:10 AM page 1 thod: CLP1 Sample Name: CCV3 Operator: MAG n Time: 03/22/06 11:18:50 Comment:•TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 983.55 49.36 510.17 2.634 2.605 2.648 49.28 SDev .39 .02 1.05 .002 .001 .001 %RSD .03981 .0307 .20592 .0593 .0567 .0500 .00 .0076 #1 983.63 49.37 509.29 2.636 2.606 2.650 49.28 #2 983.13 49.37 511.33 2.633 2.606 2.647 49.28 #3 983.90 49.34 509.90 2.633 2.604 2.648 49.28 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.655 2.481 2.600 2.632 49.21 81.77 50.25 SDev .001 .001 .001 .002 .01 .06 .00 %RSD .0266 .0438 .0559 .0590 .0149 .0713 .0063 #1 2.656 2.482 2.601 2.634 49.22 81.78 50.25 #2 2.655 2.481 2.599 2.633 49.21 81.82 50.25 2.654 2.479 2.598 2.631 49.21 81.71 50.25 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.505 2.669 80.35 2.520 483.48 481.20 .965.92 SDev .001 .006 .06 .001 2.09 .09 2.14 %RSD .0202 .2150 .0770 .0584 .43254 .01913 .22131 #1 2.505 2.662 80.36 2.522 484.46 481.24 964.91 #2 2.504 2.674 80.40 2.519 484.91 481.09 964.48 #3 2.504 2.670 80.28 2.520 481.08 481.26 968.38 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 992.45 519.58 510.85 2.941 2.449 2.523 2.701 SDev 2.13 2.81 .91 .008 .004 .002 .001 %RSD .21469 .54102 .17741 .2789 .1683 .0661 .0482 #1 990.18 516.86 511.89 2.934 2.445 2.524 2.702 992.77 522.48 510.44 2.938 2.452 2.523 2.702 994.41 519.40 510.23 2.950 2.451 2.521 2.700 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 11:26:10 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 500.70 2.487 2.646 481.96 983.62 513.76 SDev 2.04 .001 .000 .66 2.00 .61 %RSD .40671 .0428 .0095 .13596 .20340 .11883 41 498.75 2.488 2.646 482.31 981.77 513.55 #2 502.81 2.486 2.646 482.36 983.35 514.45 #3 500.53 2.488 2.646 481.20 985.74 513.28 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 03/22/06 11:33:38 AM page 1 thod: CLP1 Sample Name: CCVL3 Operator: MAG ,n Time: 03/22/06 11:26:17 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units Avge ppb .26620 ppm .0251 Ppb Ppm Ppm Ppm ppm SDev .20328 .0036 .97246 1.8950 .0041 .0006 .0006 .0002 .0006 .0056 %RSD 76.365 14.17 194.86 14.25 30.95 .0002 32.56 .0033 59.46 #1 #2 .09986 .0292 3.1218 .0047 .0008 .0008 .0088 #3 .20593 .0232 .25290 .0039 .0005 .0006 .0057 .49280 .0230 -.45736 .0036 .0004 .0004 .0022 Errors High NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Low Elem Cd Co Cr Cu Fe K Mg Units Avge ppm .0007 Ppm Ppm Ppm ppm ppm Ppm SDev .0002 .0005 .0004 .0006 .0001 -.0010 .0002 2.433 .0603 .0110 %RSD 30.82 84.59 23.66 17.39 .006 .2624 .0075 12.47 .0023 21.02 #1 42 0009 .0004 .0007 -.0009 2.426 .0663 .0134 .0006 .0009 .0007 -.0010 2.435 .0627 .0005 .0001 .0004 -.0012 2.439 .0519 .0108 .0088 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm Ppm Ppb Ppb Ppb Avge .0005 .0066 2.394 .0001 -1.8928 -.51305 -.28554 SDev .0001 .0025 .014 .0004 .8425 .74067 %RSD 29.54 37.87 .5769 339.9 44.510 144.37 .38586 135.13 #1 #2 .0006 .0093 2.407 .0004 -1.8421 -.56998 -.18120 #3 .0005 .0060 2.394 .0004 -1.0768 -1.2236 -.71284 .0003 .0044 2.379 -.0004 -2.7594 .25444 .03742 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.88279 5.3040 -.97263 -.1048 .0003 .0005 SDev 1.43172 2.3907 .45039 .0013 .0006 .0002 .0007 96RSD 162.18 45.073 46.306 1.274 220.5 29.28 .0003 36.14 #1 -1.4625 2.9867 -.51735 -.1033 -.0001 .0007 .0010 .74788 5.1635 -.98258 -.1050 .0009 .0005 .0007 -1.9337 7.7619 -1.4180 -.1060 -.0001 .0004 .0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 11:33:38 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 3.4023 .0007 .0007 -.97246 -.68389 1.1175 SDev .8476 .0001 .0002 .21355 .82757 .4969 %RSD 24.912 12.41 29.83 21.960 121.01 44.463 #1 2.8537 .0007 .0008 -.99357 -1.0358 .64951 #2 2.9747 .0008 .0006 -1.1747 .26148 1.0641 #3 4.3785 .0006 .0005 -.74914 -1.2773 1.6389 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low page 2 Analysis Report 03/22/06 11:41:05 AM 1 page :hod: CLP1 Sample Name: CCB3 Operator: MAG i Time: 03/22/06 11:33:44 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb ppm Ppm Ppm Ppm Avge .02261 .0160 .67075 .0008 .0001 .0001 -.0050 SDev .04417 .0012 .71181 .0001 .0000 .0000 %RSD 195.38 7.636 106.12 15.14 22.89 14.76 .0006 11.11 #1 .06919 .0174 .15867 .0009 .0001 .0002 -.0044 #2 -.01869 .0151 1.4836 .0009 .0001 -.0055 #3 .01733 .0156 .37001 .0007 .0001 .0001 .0001 -.0050 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 .2000 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm Ppm Ppm Ppm Ppm Ppm Avge .0001 .0001 -.0000 -.0018 .0020 .0344 SDev .0001 .0002 .0001 .0002 .0007 .0021 .0015 %RSD 130.8 327.1 329.7 8.421 32.86 6.020 .0022 147.5 #1 .0002 .0003 -.0001 -.0017 .0027 .0341 #2 -.0000 -.0000 -.0001 -.0020 .0019 .0325 .0019 -.0009 .0001 -.0001 .0001 -.0017 .0014 .0366 .0033 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 .2000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0000 .0013 -.0028 -.0002 -1.1727 -.52549 -1.2849 SDev .0001 .0003 .0016 .0002 .9568 .86914 96RSD 136.1 24.06 55.84 87.84 81.591 165.39 .2886 22.459 #1 .0001 .0017 -.0011 -.0004 -.54486 -.66905 -1.0428 #2 -.0000 .0011 -.0033 -.0003 -2.2739 -1.3139 -1.2077 #3 .0001 .0012 -.0041 .0000 -.69928 .40648 -1.6043 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .88805 5.0765 -.87305 -.1239 .0002 .0001 .0000 SDev 1.4039 2.1409 1.52268 .0020 .0005 .0000 .0001 %RSD 158.09 42.173 174.41 1.590 188.2 28.97 205.0 #1 .25318 4.4158 .26089 -.1216 .0000 .0001 -.0000 2.4972 7.4698 -2.6037 -.1248 .0008 .0001 -.0000 -.08627 3.3437 -.27632 -.1252 -.0001 .0001 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 11:41:05 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm, ppb ppb ppb Avge 1.6314 -.0001 -.0002 -.74098 .16447 1.1082 SDev .6515 .0003 .0000 .84166 .97398 %RSD 39.933 229.9 25.07 113.59 592.20 .4730 42.682 #1 2.2729 -.0001 -.0002 -.62766 -.17837 1.6445 #2 1.6510 .0001 -.0001 -1.6336 1.2635 #3 .97036 -.0004 -.0002 .03828 -.59174 .75079 .92917 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 00 O O H Analysis Report 03/22/06 11:48:32 AM 1 page thod: CLP1 Sample Name: CRIF Operator: MAG a Time: 03/22/06 11:41:12 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm Ppm Ppm Avge 18.889 .0194 19.873 .2041 .0000 .0110 -.0059 SDev .107 .0014 .580 .0004 .0000 .0000 %RSD .56434 7.321 2.9165 .1823 191.3 .1753 .0008 13.05 #1 18.810 .0180 20.138 .2041 .0000 .0110 -.0051 #2 18.848 .0209 19.208, .2044 -.0000 .0110 -.0067 #3 19,010 .0193 20.272 .2037 .0000 .0110 -.0060 Errors LC Pass NOCHECK LC Pass NOCHECK NOCHECK LC Pass NOCHECK High 26..000 26.000 .0130 Low 14.000 14.000 .0070 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm Ppm ppm Ppm Ppm Ppm Avge .0109 .0995 .0207 .0500 -.0002 .0305 -.0007 SDev .0000 .0003 .0001 .0003 .0001 .0054 %RSD .2071 .2541 .6062 .5084 69.01 17.83 .0008 109.7 #1 .0109 .0998 .0207 .0503 -.0003 .0325 -.0007 #2 .0109 .0993 .0205 .0498 -.0000 .0243 -.0016 .0109 .0995 .0208 .0499 -.0003 .0346 .0000 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0130 .1300 .0260 .0650 Low .0070 .0700 .0140 .0350 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0303 .0227 -.0027 .0820 5.1024 5.1999 115.48 SDev ,0001 .0003 .0004 .0006 1.6152 .9850 1.55 %RSD .2673 1.319 15.94 .7203 31.655 18.943 1.3416 #1 .0303 .0231 -.0024 .0824 6.6109 4.0740 115.26 #2 .0302 .0226 -.0026 .0814 5.2979 5.9022 114.06 #3 .0303 .0225 -.0032 .0824 3.3984 5.6237 117.13 Errors LC Pass LC Pass NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0390 .0260 .1040 Low .0210 .0140 .0560 Elem 2068/2 196.0/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 118.72 14.850 7.5510 .0172 .0774 -.0000 .2182 SDev .69 2.425 1.9903 .0030 .0004 .0000 .0004 %RSD .58447 16.332 26.3.58 17.31 .5626 184.3 .1826 #1 118.05 17.587 6,.9785 .0145 .0778 -.0000 .2187 118.67 12.967 5.9097 .0204 .0772 -.0001 .2181 119.43 13.997 9.7648 .0167 .0770 .0000 .2179 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK Analysis Report 03/22/06 11:48:32 AM igh .1040 Low .0560 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 20.524 .0999 .0470 5.1675 117.64 9.9817 SDev .513 .0003 .0003 .4624 .89 1.5277 %RSD 2.4982 .2902 .6048 8.9477 .75646 15.305 #1 19.997 .1001 .0473 4.9188 117.12 10.511 #2 20.553 .0995 .0467 5.7010 117.13 8.2597 #3 21.022 .1000 .0469 4.8827 118.67 11.174 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 30.000 .1300 .0520 9.0000 180.00 13.000 Low 10.000 .0700 .0280 3.0000 60.000 7.0000 page 2 Analysis Report 03/22/06 11:56:00 AM f page 1 thod: Time: CLP1 Sample Name: ICSAF Operator: MAG n 03/22/06 11:48:39 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units Avge ppb .65057 Ppm 482.4 Ppb -2.0762 Ppm ppm Ppm Ppm SDev .26793 2.0 .6947 -.0029 .0020 .0005 482.3 %RSD 41.183 .4115 33.462 .0006 20.31 .0000 .3984 .0000 3.313 2.8 .5787 #1 #2 .60127 484.3 -1.4486 -.0026 .0020 .0006 484.9 #3 .93973 482.7 -1.9574 -.0026 .0020 .000.5 482.5 .41072 480.3 -2.8227 -.0036 .0020 .0005 479.4 Errors High LC Pass 10.000 LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass Low -10.000 600.0 400.0 .2000 .0050 600.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm -.0000 ppm -.0019 ppm .0045 ppm -.0010 ppm 196.7 ppm ppm SDev .0001 .0001 .0002 .0003 1.0 .0288 481.3 2.1 96RSD 341.8 6.720 3.854 26.87 .5075 .0012 4.079 .4293 #1 #2 -.0001 -.0019 .0044 -.0007 197.7 .0294 483.3 .0001 -.0018 .0044 -.0011 196.7 .0296 481.4 -.0001 -.0020 .0047 -.0012 195.7 .0275 479.1 Errors High LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass Low .0050 -.0050 .0100 240.0 600.0 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm Ppb Ppb Ppb Avge L-.0159 -.0049 .0106 .0023 -.07303 -3.4631 -1.6509 SDev .0001 .0002 .0007 .0001 1.22710 .5812 2.6115 %RSD .7030 3.660 6.764 2.497 1680.2 16.781 158.19 #1 #2 L-.0158 -.0047 .0114 .0023 -1.3463 -3.2383 .95595 #3 L-.0160 -.0051 .0104 .0022 .02531 -3.0280 -1.6415 L-.0158 -.0048 .0100 .0024 1.1019 -4.1231 -4.2.670 Errors LC Low NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb ppm ppm ppm ppm Avge -.54089 5.8152 -3.9407 -.0683 .0264 -.2795 N SDev 3.40200 4.4420 3.3805 .0080 .0013 .0017 .0021 �+ %RSD 628.96 76.385 85.786 11.74 5.003 .6181 .0001 6.353 #1 -3.2904 3.8622 -.05633 -.0591 .0278 -.2802 .0022 O 3.2636 10.899 -5.5483 -.0736 .0264 -.2807 .0022 O -1.5959 2.6843-6.2174 -.0722 .0251 -.2775 .0020 V) Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 11:56:00 AM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 6.5559 .0011 -.0041 -2.3342 -.91049 -.69195 SDev 1.1255 .0001 .0001 .3015 2.22130 2.31411 %RSD 17.168 12.61 2.785 12.918 243.97 334.43 #1 7.8414 .0010 -.0040 -2.6083 -1.8763 1.2486 #2 6.0789 .0011 -.0042 -2.0112 1.6302 -.07133 #3 5.7474 .0012 -.0041 -2.3831 -2.4854 -3.2531 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 page 2 Analysis Report 03/22/06 12:03:27 PM 1 page thod: CLP1 Sample Name: ICSABF Operator: MAG n Time: 03/22/06 11:56:07 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb PPM Ppm Ppm Ppm Avge 1043.7 491.0 1019.7 .9549 .5449 .5355 489.3 SDev 1.0 .2 3.1 .0012 .0005 .0003 %RSD .09463 .0409 .30648 .1254 .0979 .0589 .3 .0671 41 1043.3 491.3 1019.2 .9537 .5454 .5358 488.9 42 1043.0 490.9 1016.9 .9561 .5449 .5357 489.5 #3 1044.9 490.9 1023.1 .9549 .5444 .5352 489.5 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM PPM PPM Avge 1.015 .4741 .5157 .5636 199.9 .0424 489.2 SDev .000 .0003 .0003 .0008 .1 .0019 %RSD .0384 .0649 .0652 .1394 .0357 4.589 .1 .0107 #1 1.014 .4742 .5161 .5645 199.8 .0417 489.2 #? 1.015 .4737 .5154 .5632 199.9 .0410 489.1 1.015 .4743 .5157 .5631 199.9 .0446 489.1 Errors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .4760 1.049 .0230 .9539 956.24 958.72 -9.4934 SDev .0003 .003 .0001 .0008 1.70 4.11 %RSD .0562 .2550 .5454 .0808 .17784 .42885 .7870 8.2898 #1 .4763 1.046 .0230 .9530 954.53 954.73 -8.9235 #2 .4760 1.050 .0231 .9540 957.93 958.50 -10.391 #3 .4758 1.052 .0229 .9546 956.26 962.94 -9.1653 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -9.2569 1033.3 1010.2 .7939 1.005 -.2824 .0015 SDev 1.7089 3.8 3.8 .0027 .003 .0004 .0001 %RSD 18.461 .37212 .37941 .3356 .3105 .1315 9.127 #1 -7.4156 1037.2 1011.1 .7934 1.008 -.2820 .0014 -9.5629 1033.2 1013.4 .7968 1.004 -.2825 .0017 _10.792 1029.5 1005.9 .7916 1.002 -.2828 .0014 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK' NOCHECK NOCHECK Analysis Report 03/22/06 12:03:27 PM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 995.29 .4930 1.082 957.90 -9.3356 1017.9 SDev 1.29 .0005 .001 3.05 1.2451 3.5 %RSD .12994 .0947 .0573 .31822 13.337 .34737 #1 994.38 .4925 1.082 954.66 -7.9177 1019.8 #2 996.77 .4934 1.083 958.31 -9.8387 1020.0 #3 994.71 .4933 1.082 960.72 -10.250 1013.8 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 page 2 Analysis Report 03/22/06 12:10:54 PM 1 page thod: CLP1 Sample Name: CCV4 Operator: MAG n Time: 03/22/06 12:03:34 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm Ppm Ppm Avge 989.29 49.45 512.51 2.646 2.612 2.669 49.72 SDev 1.30 .03 1.80 .001 .001 .006 %RSD .13133 .0630 .35195 .0515 .0559 .2120 .11 .2262 #1 988.71 49.48 510.43 2.645 2.611 2.665 49.65 #2 988.39 49.42 513.63 2.646 2.611 2.667 49.66 #3 990.78 49.44 513.48 2.648 2.614 2.676 49.85 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm Ppm Ppm Ppm Ppm Avge 2.684 2.492 2.621 2.633 49.71 81.68 50.69 SDev .007 .005 .005 .001 .10 .05 %RSD .2599 .2020 .1910 .0466 .2056 .0598 .06 .1190 #1 2.678 2.488 2.618 2.633 49.62 81.73 50.67 #2 2.682 2.490 2.618 2.632 49.68 81.67 50.64 2.692 2.498 2.626 2.634 49.82 81.64 50.75 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.524 2.694 80.44 2.545 485.09 484.16 968.24 SDev .005 .006 .05 .007 3.00 .63 5.02 %RSD .1894 .2183 .0614 .2637 .61942 .13090 .51816 #1 2.520 2.688 80.49 2.541 483.01 484.45 967.19 #2 2.522 2.693 80.42 2.540 483.72 483.43 963.82 #3 2.529 2.700 80.40 2.552 488.53 484.60 973.69 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 995.25 525.36 514.13 3.081 2.453 2.529 2.717 SDev 3.72 2.53 2.44 .013 .008 .001 .003 %RSD .37379 .48187 .47532 .4377 .3313 .0522 .1217 #1 990.97 524.51 512.01 3.079 2.446 2.528 2.715 997.04 523.36 513.58 3.069 2.453 2.528 2.715 997.74 528.20 516.80 3.096 2.462 2.530 2.721 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Ln N Ln O O C/1 Analysis Report 03/22/06 12:10:54 PM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 506.24 2.500 2.669 484.47 986.25 517.87 SDev .94 .004 .005 1.27 3.35 2.39 %RSD .18652 .1473 .1822 .26129 .33943 .46108 #1 506.35 2.497 2.666 483.97 983.05 516.17 #2 505.25 2.499 2.666 483.53 985.98 516.83 #3 507.13 2.504 2.675 485.91 989.73 520.60 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 page 2 Analysis Report 03/22/06 12:18:20 PM page 1 thod: CLP1 Sample Name: CCVL4 Operator: MAG n Time: 03/22/06 12:11:00 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm Ppm Ppm Avge .53122 .0439 2.3172 .0045 .0006 .0007 SDev .13963 .0087 1.7816 .0007 .0002 .0002 .0172 %RSD 26.285 19.73 76.886 16.13 33.28 30.94 .0103 59.49 #1 .66659 .0527 3.6287 .0053 .0008 .0009 #2 .53939 .0435 3.0342 .0039 .0006 .0007 .0281 #3 .38768 .0354 .28883 .0042 .0004 .0005 .0158 .0078 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK High Low Elem Cd Co Cr Cu Fe K Mg Units ppm ppm Ppm Ppm Ppm Ppm Ppm Avge .0007 .0008 .0006 -.0013 2.453 .0600 SDev .0003 .0003 .0002 .0003 .006 .0094 .0247 %RSD 46.50 32.08 28.25 24.61 .2611 15.60 .0093 37.60 #1 .0009 .0008 .0008 -.0011 2.459 .0678 42 .0009 .0011 .0007 -.0011 2.454 .0624 .0341 .0247 .0003 .0006 .0004 -.0017 2.447 .0496 .0155 Errors NOCHECK NOCHECK NOCHECK NOCHECK LC Pass NOCHECK NOCHECK High 2.750 Low 2.250 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0005 .0064 2.400 .0005 -2.8649 -.11774 .96531 SDev .0002 .0029 .009 .0004 .6373 .63430 1.1522 %RSD 35.60 45.38 .3894 80.35 22.244 538.74 119.36 41 .0007 .0095 2.409 .0005 -3.1511 .47920 1.5418 #2 .0006 .0061 2.399 .0010 -2.1347 -.04867 1.7155 #3 .0003 .0037 2.391 .0001 -3.3090 -.78375 -.36137 Errors NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK NOCHECK High 2.750 Low 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .-1.1383 5.7593 1.1270 -.0910 .0006 .0005 .0008 SDev 1.2492 3.6026 .0166 .0107 .0010 .0002 .0003 %RSD 109.74 62.553 1.4689 11.71 176.1 34.12 34.91 #1 -1.9162 6.0670 1.1458 -.0795 -.0002 .0007 .0010 .30262 2.0127 1.1204 -.0929 .0002 .0006 .0008 -1.8014 9.1982 1.1147 -.1006 .0018 .0003 .0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 12:18:20 PM page 2 igh Zn Low Sb2068 Elem T11908 Units ppb Avge 3.5334 SDev 1.4640 %RSD 41.434 #1 4.2873 #2 4.4668 #3 1.8461 Errors NOCHECK High 247.84 Low .0009 v Zn Pb2203 Sb2068 Se1960 PPM ppm ppb ppb ppb .0007 .0050 -1.0325 -.43779 2.6696 .0004 .0002 .5128 1.08505 1.1986 53.46 3.689 49.667 247.84 44.900 .0009 .0051 -.72964 -.76468 2.7846 .0010 .0050 -.74329 .77312 1.4176 .0003 .0048 -1.6246 -1.3218 3.8065 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 12:25:45 PM page 1 thod: CLP1 Sample Name: CCB4 Operator: MAG n Time: 03/22/06 12:18:26 Comment: TSL005 Mode: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb Ppm Ppb Ppm Ppm Ppm Ppm Avge .31099 .0261 -.10134 .0011 .0001 .0002 -.0004 SDev .11124 .0047 .91101 .0003 .0001 .0001 96RSD 35.769 18.20 898.95 27.64 43.39 28.09 .0047 1218. #1 .40010 .0316 -.70326 .0014 .0002 .0003 #2 .34655 .0235 .94676 .0008 .0001 .0002 .0049 -.0021 #3 .18632 .0233 -.54753 .0011 .0001 .0002 -.0039 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 .2000 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm Ppm Ppm Ppm Ppm Ppm Avge .0001 .0002 .0002 -.0019 .0058 .0347 .0088 SDev .0001 .0002 .0001 .0001 .0025 .0055 %RSD 171.8 124.1 84.78 7.803 43.33 15.78 .0060 68.25 #1 .0002 .0004 .0003 -.0017 .0086 .0406 42 .0001 -.0000 .0001 -.0019 .0050 .0334 .0146 .0089 -.0001 .0001 .0001 -.0020 .0038 .0299 .0027 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0000 .0014 -.0045 -.0002 -2.7482 .49655 -.58815 SDev .0001 .0002 .0026 .0001 1.3294 1.1562 .92688 96RSD 304.1 17.85 57.39 57.53 48.373 232.85 157.59 #1 .0002 .0013 -.0016 -.0001 -3.9883 1.3246 .47330 #2 -.0000 .0016 -.0053 -.0002 -1.3447 -.82444 -1.2376 #3 -.0000 .0011 -.0066 -.0004 -2.9115 .98947 -1.0001 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.66057 3.9944 .68705 -.1306 -.0005 .0001 .0001 SDev .87046 1.2425 .48544 .0073 .0004 .0001 .0001 %RSD 131.77 31.105 70.655 5.588 77.31 66.01 46.24 #1 .32995 2.6514 .12669 -.1231 -.0004 .0002 .0002 -1.0080 5.1028 .97923 -.1377 -.0008 .0001 .0001 -1.3036 4.2290 .95525 -.1310 -.0001 .0000 .0001 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 03/22/06 12:25:45 PM igh Low Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.8972 .0000 .0032 -.58391 -.63644 1.7884 SDev .3941 .0001 .0001 .36461 .88025 .7274 %RSD 20.774 2891. 2.645 62.443 138.31 40.672 #1 1.9409 .0002 .0033 -.44455 .37771 .96742 #2 1.4830 -.0000 .0031 -.99764 -1.0845 2.3524 #3 2.2676 -.0001 .0033 -.30953 -1.2025 2.0454 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 page 2 T2M LA US, INC. 3 cal. Stds. Prep: 3A zt Ty,- Source:_ ��ahPur�, G20a Z- o J Instrument I.D. L-ctyranVk4 at t>P 1 MERCURY (Hg) " ANALYST S IGNATIIRE : j ;,, 1 RESULT DIL. SAMPLE # SPK LAB NO. (IIG/L) FACTOR WEIGHT % TS I MG -$Z. `5k. 2uk 2 •-,gyl tzt,o5 t3:o� DATE • 3 z A oc• SAMPLE G ID/NOTES L 00 =s.00 M c. v (o • 1 z - M5 "L IcC> Lo.I 3 ccvl S. >g c c 431 < 5 c Yl -N 0.2 -os - (o Mtb-IVIf1(1 40. 1 0 g - oo1(r L o • 1 Do 10 -- po4� < a. • I I Z - cw6 < t3 -� < �. 35Ca l - o04 PL I — WgC. f O Zo -pko(, Lo.l ZI `a1�cr <'� • j 22 ' oIzcr X 0.1 Z3 -03 F < Z) ) Ll 4`I i o l0�1 S live>% -IL q,,/ -L t3:o� DATE • 3 z A oc• SAMPLE G ID/NOTES L 00 =s.00 M -Dv - M5 Lo 1, _ Q i> —�5 0 0 Do P 0127 mw S00'ISZ MERCURY STANDARDS AND '.R EAGENTc 1.x "U2A LABS, INC. Cal. Stds. Prep: 3 z,rt, Source: %ti Qvv%�, ERfa Instrument I.D_-eerrukh k^p1.�o- A4� MERCURY (Hg) ANALYST SIGNATIIRE•C"-)1rUL �OA-e, ,., a /� DATE • 31z�, o co P 0129 Folder: HG032106 Page 1 Protocol: MERCURY ***POST -RUN REPORT*** Line Conc. Units SD/RSD 1 2 3 4 5 ------------------------------------------------------------ I *** Standard: 1 Rep: 1 Seq: 1 13:06:04 21 Mar 06 HG Hg .000 ug/L -82 *** Standard: 2 Rep: 1 Seq: 2 13:08:11 21 Mar 06 HG { Hg .200 ug/L 656 *** Standard: 3 Rep: 1 Seq: 3 13:09:53 21 Mar 06 HG Hg 1.00 ug/L 2612 *** Standard: 4 Rep: 1 Seq: 4 13:12:12 21 Mar 06 HG Hg 2.00 ug/L 4841 *** Standard:'5 Rep: 1 Seq: 5 13:14:09 21 Mar 06 HG Hg 5.00 ug/L 12605 *** Standard: 6 Rep: 1 Seq: 6 13:15:47 21 Mar 06 HG Hg 10.0 ug/L 25226 *** Sample ID: ICV Seq: 7 13:17:34 21 Mar 06 HG Hg 6.12 ug/L 15416 *** Sample ID: ICB Seq: 8 13:20:40 21 Mar 06 HG Hg .061 ug/L 151 -------------------------- *** Sample ID: CCV1 ____________________________________________ Seq: 9 13:22:51 21 Mar 06 HG Hg 5.09 ug/L 12838 *** Sample ID: CCB1 Se 10 13.24.31 21 Mar 06 HG Hg -.002 ug/L -9 *** Sample ID: CRA Seq: 11 13:27:20 21 Mar 06 HG Hg .208 ug/L 522 *** Sample ID: MB -16441 Seq: 12 13:29:09 21 Mar 06 HG PBW Hg -.002 ug/L -9 *** Sample ID: 03561001G Seq: 13 13:30:58 21 Mar 06 HG M Hg . 015 ug/L 34 Q p ---------------------------------- ____________________________ -- CD CD V] [� Folder: HG032106 Page 2 Protocol: MERCURY ***POST -RUN REPORT*** Line Conc. Units SD/RSD 1 2 3 4 5 ----------------------------------------------------------------------- *** Sample ID: 03561002G Seq: 14 13:32:37 21 Mar 06 HG Hg -.043 ug/L -113 I__AW _ 17 *** Sample ID: 03561003G Seq: 15 13:34:15 21 Mar 06 HG Hg . 015 ug/L 35 M w - i S *** Sample -------------------------------- ID: 03561004G Seq: 16 13:36:42 21 Mar 06 -____ HG Hg . 005 ug/L 8 Nk *** Sample ID: 03561005G Seq: 17 13:38:35 21 Mar 06 HG Hg -.021 ug/L -57 *** Sample ID: 03561006G Se 18 13:40:45 21 Mar 06 HG Hg -.002 ug/L -9 *** Sample ID: 03561007G Seq: 19 13.42.35 21 Mar 06 HG Hg . 023 ug/L 55 M �'- y S *** Sample ID: 03561008G Seq: 20 13.44.11 21 Mar 06 HG Hg -.012 ug/L -34 M W _ S *** Sample ID: CCV2 Se 21 13:45:59 21 Mar 06 HG Hg 4.96 ug/L 12491 *** Sample ID: CCB2 Se 22 13:47:48 21 Mar 06 HG Hg .014 ug/L 31 *** Sample ID: 03561009G Seq: 23 13:49:30 21 Mar 06 HG Hg . 039 ug/L 96 M *** Sample ID: 03561009GD Se Hg -.014 ug/L -38 *** Sample ID: 03561009GS Seq: 25 Hg 1.07 ug/L 2698 ------------- 13:51:11 21 Mar 06 HG --------------- 13:54:14 21 Mar 06 HG Folder: HG032106 Page 3 Protocol: MERCURY ***POST -RUN REPORT*** Line Conc. Units SD/RSD 1 2 3 4 5 ---------------------------------------------------------- *** Sample ID: 0356101OG Seq: 26 13:56:06 21 Mar 06 HG Hg . 006 ug/L ' 12 *** Sample ID: 03561011G Se 27 13:57:45 21 Mar 06 HG Hg .014 ug/L 32 *** Sample ID: 03561012G Seq: 28 13:59:48 21 Mar 06 HG Hg .033 ug/L 81 *** Sample ID: 03561013G Seq: '29 14:02:19 21 Mar 06 HG Hg -.010 ug/L -28 *** Sample ID: MB -16492 Se 30 14:04:35 21 Mar 06 HG PBW Hg .104 ug/L 258 *** Sample ----------------------------------------------------- ID: MBI -16492 Seq: 31 14:06:26 21 Mar 06 HG MBLKTCLP Hg .025 ug/L 59 *** Sample ID: 03420002A Seq: 32 14:08:23 21 Mar 06 ---------- HG Hg .067 ug/L 166 *** Sample ID: CCV3 Seq: 34 14.12.27 21 Mar 06 HG Hg 4.98 ug/L 12542 *** ---------------------------------- Sample ID: CCB3 Seq: 35 19.14.03 21 Mar 06 HG Hg -.058 ug/L -149 *** Sample ID: 03358001B Seq: 36 14:15:46 21 Mar 06 HG Hg .027 ug/L 64 *** Sample ID: 03358001BD Se 37 14:19:19 21 Mar 06 HG Hg -.033 ug/L •-86 I *** Sample ID: 0335800lBS Seq: 38 19:21:12 21 Mar 06 HG Hg .994 ug/L 2503 Folder: HG032106 Page 4 Protocol: MERCURY *** Line Conc. Units SD/RSDPOSREPORT*** T -RUN 2 3 4 5 -------------------------------------------- *** Sample ID: 03626001A Seq: 39 14:23:09 21 Mar 06 HG Hg 1.07 ug/L- 2699 *** Sample ID: 03626002A I Se 40 14:24:51 21 Mar 06 HG Hg .209 ug/L 523 * _______________________________ Sample ID: 03626003A Seq: 41 14:27:12 21 Mar 06 HG Hg .122 ug/L 303 *** Sample ID: 03626004A Seq: 42 14.29.22 21 Mar 06 HG Hg .342 ug/L 859 *** Sample ----------------- ID: CCV9 __ q: 44 14:33:10 21 Mar 06 HG Hg 4.84 ug/L 12187 *** Sample ID: CCB4 Seq: 45 14:34:57 21 Mar 06 HG Hg .043 ug/L 106 M O O V1 F-4 0 • CLIENT ID#• IH2M LAB# Mil-�D MW -IS n V/ FWD mv- 5P nw-�s . CCV2 CCB2 �l�l3S • G rtw ss SJJG � TSL vaS CN, UG/L = A x DAF ANALYS B DATE: 3 - CN, MG/KG = A X D X F WxE 0.000. CO TSL005 M139 - •GRAMS • • USED NOTES CULATIONS mss!! �!!!!�l��!!"�a!!!�!!��•��! loan n, 7 ZP,MIN ![J��! KIM 0.000. CO TSL005 M139 U2M LABS' INC. IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE J H2M Labs, Inc. �� CLP Di estion In Client: L -SDG #:_ Analyst Signature: TC L— _ D��_ ate:_ Matrix:�S Time Started/Ended: Method: I PH: 91 < 2 O:/QC/BOOKS/Cl-Migestionlog of colors: 'Description of texture: 'Description of clarity: 'Description of artifacts red, blue, yellow, green, orange, violet white, colorless, brown, grey, black. fine, medium, coarse. clear, cloudy, opaque. yes or no and describe P �� 112M LA I3S, INC. 1 i 1 � SL Oo5 NAME: �� ►..,� ��,,,� DATE • 1 - AG TTf-.WemTwn _ P 0034 N 'd' O O V) Eq U2M LABS, INC. . J l 1 !I 1 NA M:L. DATE: �1LAiy- HG DIGESTIONS d/, lH2A LAUS9 NUO CYANIDE DISTILLATION LOG DATE: ANALYST VOLUMEI1 KI TEST jPb ACETATE SAMPLE VESSEL LAB. CLIENT OF PAPER TEST PAPER NO. I. D. I. D. ISAMPLE IDU J:cv 2 1 ISM, I TES C KI ��T Pb ACETATE SEL / TEST I VES CLIENT VOLUME SAMPLE PAPER TEST PAPER D. S PH + floso-356V -co,7,41 f 6 rSL Sp COM evlA 4 5 6 016A 7 0l;L& 9 613A' lo.1,�rM SZo -XIA A Amount' oof ascorbic acid used Amount f Cd Co used * 1 3 NDARDS.PREPARED FOR THIS RUN: 0 CONC. T -n elt &N Ard SO *751,5"G ITY DISTILLED: YES No LOT # AND SOURCE Id -00 C/o J(,V F2M "USo INC. SDG NO.: jsL ooS SCAN: f+ `Tl*\S This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature: Date: 3 Reviewed By Signatu Date: