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Water Chemistry Data Package 03/2006
Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDC NO: TSL005 Water Samples Received: 3/16/06 `",�-r �'"='1�IISTRY DATA PACKAGE V I A I-Auso� Is C'm Environmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 U2M KAUS, INC. TS L O 0-5 TABLE OF CONTENTS I. SAMPLE REPORTS II. Q.C. SUMMARY III. RAW DATA U2M "US, INC. SAMPLE REPORTS 1-2M "US, INC. 575BrcadFdoN Rued, MO& NY 11747 LABORATORY RESULTS (631)643W)-FAX(631)420&W NYSDOHJD#10478 Town of Southold Landfill Lab No. : 0603561-001 Attn To Collected :3/16/2006 1:00:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original cc Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Color Chromium, Hexavalent Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate ' Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Client ID. : EQPT Sample Information... Type : Blank Origin: Results Qualifier D.F.. Units Method Number Analyzed < 1.0 1 mg/L E310.1 03/20/2006 11:00 AM < 2 1 mg/L E405.1 03/16/2006 4:28 PM < 0.5 1 mg/L E320.1 03/23/2006 9:30 AM < 2.0 1 mg/L E325.2 03/27/2006 1:54 PM <10 1 mg/L E410.4 03/21/2006 10:02 AM < 5 1 units E110.2 03/17/2006 1:02 PM < 0.02 1 . mg/L M3500 -Cr D 03/17/20061:10 PM < 5.0 1 mg/L E130.2 03/17/2006 1:20 PM < 0.10 1 mg/L E350.1 03/27/2006 11:23 AM < 0.10 1 mg/L E353.2 03/25/2006 11:27 AM < 5.0 1 pg/L E420.1 03/27/2006 10:30 AM < 5.0 1 mg/L SW9038 03/28/2006 1:34 PM <10 1 mg/L E160.1 03/20/2006 11:40 AM 0.26 1 mg/L E351.2 03/28/2006 1:33 PM < 1.0 1 mg/L SW9060 03/22/2006 3:04 PM Page 1 of 13 &K11- Laboratory Laboratory Manager "/*A "Uso INC. 5756foedHdw Road, Mdvle NY 11747 LABORATORY RESULTS (631)691,9040. FAX (631)42N3436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0603561-002 Type : Groundwater Attn To : Origin: Client ID.: MW -1D Collected :3/16/2006 2:40:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 03/20/2006 11:05 AM Biochemical Oxygen Demand 17 1 mg/L E405.1 03/16/2006 4:32 PM Bromide < 0.5 1 mg/L E320.1 03/23/2006 9:45 AM Chloride 26.4 1 mg/L E325.2 03/27/2006 1:55 PM Chemical Oxygen Demand 38.7 1 mg/L E410.4 03/21/2006 10:03 AM Color < 5 1 units E110.2 03/17/2006 1:03 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:15 PM Hardness (As CaCO3) 16.0 1 mg/L E130.2 03/17/2006 1:25 PM Nitrogen, Ammonia (As N) 0.68 1 mg/L E350.1 03/27/2006 11:24 AM Nitrate as N 1.56 5 mg/L E353.2 03/25/2006 11:28 AM Phenolics, Total Recoverable 27.0 1 pg/L E420.1 03/27/2006 10:45 AM Sulfate 39.9 1 mg/L SW9038 03/28/2006 1:36 PM Total Dissolved Solids 130 1 mg/L E160.1 03/20/2006 11:42 AM Nitrogen, Kjeldahl, Total 23.4 10 mg/L E351.2 03/28/2006 4:09 PM Total Organic Carbon 21.7 1 mg/L SW9060 03/22/2006 3:33 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 2 of 13 Q/� I4l Laboratory Manager d' CA P-4 F2M "US, INC. 575 Broad Hollow Road, Mdvie NY 11747 LABORATORY RESULTS (631AA-3110. FAX (631)4204K% NYSDOH ID#10478 Town of Southold Landfill Lab No. : 0603561-003 Attn To : Collected :3/16/2006 2:10:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(sl Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Color Chromium, Hexavalent Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID. : MW -1S Sample Information... Type : Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed < 1.0 1 mg/L E310.1 03/20/2006 11:10 AM 16 1 mg/L E405.1 03/16/2006 4:36 PM < 0.5 1 mg/L E320.1 03/23/2006 10:00 AM 29.7 1 mg/L E325.2 03/27/2006 1:56 PM 48.7 1 mg/L E410.4 03/21/2006 10:04 AM < 5 1 units E110.2 03/17/2006 1:04 PM < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:20 PM 17.0 1 mg/L E130.2 03/17/2006 1:30 PM 0.65 1 mg/L E350.1 03/27/2006 11:25 AM 1.37 5 mg/L E353.2 03/25/2006 11:29 AM 26.1 1 pg/L E420.1 03/27/2006 11:00 AM 63.0 2.5 mg/L SW9038 03/28/2006 1:38 PM 138 1 mg/L E160.1 03/20/2006 11:44 AM 25.1 10 mg/L E351.2 03/28/2006 4:09 PM 22.1 1 mg/L SW9060 03/22/2006 4:03 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 3 of 13 Laboratory Manager U2M ILAUSO INC. 575BtcadHdl0v Road, Mdvie NY 11747 LABORATORY RESULTS (631)684,3010.FAX (631)42084W NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0603561-004 Type : Groundwater Attn To : Origin: Client ID. : MW -31) Collected :3/16/2006 1:45:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 7.0 1 mg/L E310.1 03/20/2006 11:15 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 03/16/2006 4:40 PM Bromide 0.6 1 mg/L E320.1 03/23/2006 10:15 AM Chloride 10.3 1 mg/L E325.2 03/27/20061:56 PM Chemical Oxygen Demand 13.5 1 mg/L E410.4 03/21/2006 10:05 AM Color < 5 1 units E110.2 03/17/2006 1:05 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:25 PM Hardness (As CaCO3) 43.0 1 mg/L E130.2 03/17/2006 1:35 PM Nitrogen, Ammonia (As N) 0.20 1 mg/L E350.1 03/27/2006 11:25 AM Nitrate as N 3.91 5 mg/L E353.2 03/25/2006 11:29 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 11:15 AM Sulfate 21.7 1 mg/L SW9038 03/28/20061:40 PM Total Dissolved Solids 101 1 mg/L E160.1 03/20/2006 11:46 AM Nitrogen, Kjeldahl, Total 4.51 20 mg/L E351.2 03/28/2006 1:35 PM Total Organic Carbon 3.0 1 mg/L SW9060 03/22/2006 4:34 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 4 of 13 Laboratory Manager li U214 UAIUS, INC. 575B(ced Hollow Road, Wale NY 11747 LABORATORY RESULTS (631)aW3M - FAX (631)4aR9W NYSDDHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0603561-005 Type : Groundwater Attn To Origin: Client ID.: MW -3S Collected :3/16/2006 1:15:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 25.2 1 mg/L E310.1 03/20/2006 11:20 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 03/16/2006 4:44 PM Bromide < 0.5 1 mg/L E320.1 03/23/2006 10:30 AM Chloride 8.8 1 mg/L E325.2 03/27/2006 1:57 PM Chemical Oxygen Demand <10 1 mg/L E410.4 03/21/2006 10:06 AM Color < 5 1 units E110.2 03/17/2006 1:06 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:30 PM Hardness (As CaCO3) 48.0 2 mg/L E130.2 03/17/2006 1:40 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 03/27/2006 11:26 AM Nitrate as N 4.33 10 mg/L E353.2 03/25/2006 11:30 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 11:30 AM Sulfate 10.4 1 mg/L SW9038 03/28/2006 1:42 PM Total Dissolved Solids 101 1 mg/L E160.1 03/20/2006 11:48 AM Nitrogen, Kjeldahl, Total 0.42 1 mg/L E351.2 03/28/2006 1:36 PM Total Organic Carbon 3.0 1 mg/L SW9060 03/22/2006 5:05 PM Qualifiers: E . Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 5 of 13 Laboratory Manager U2M 1. US' INCe 575 BroadHdav Road, Mtdvile W 11747 (631)694-,'3W-FAX(631)42084W NYSDOHID#10478 - Town of Southold Landfill Attn To : Collected :3/16/2006 10:55:00 AM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original cc LABORATORY RESULTS Lab No. : 0603561-006 Client ID. : MW4D Sample Information... Type : Groundwater Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 250 2 mg/L E310.1 03/20/2006 11:25 AM Biochemical Oxygen Demand 5 1 mg/L E405.1 03/16/2006 4:48 PM Bromide 2.6 1 mg/L E320.1 03/23/2006 10:45 AM Chloride 117 5 mg/L E325.2 03/27/2006 1:58 PM Chemical Oxygen Demand 33.6 1 mg/L E410.4 03/21/2006 10:07 AM Color < 5 1 units E110.2 03/17/2006 1:07 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:35 PM Hardness (As CaCO3) 205 5 mg/L E130.2 03/17/2006 1:45 PM Nitrogen, Ammonia (As N) 22.3 20 mg/L E350.1 03/27/2006 12:37 PM Nitrate as N 1.32 5 mg/L E353.2 03/25/2006 11:30 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 11:45 AM Sulfate 38.8 1 mg/L SW9038 03/28/2006 1:44 PM Total Dissolved Solids 450 2 mg/L E160.1 03/20/2006 11:50 AM Nitrogen, Kjeldahl, Total 28.8 10 mg/L E351.2 03/28/2006 1:36 PM Total Organic Carbon 8.5 1 mg/L SW9060 03/22/2006 5:34 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 4/3/2006 Page 6 of 13 i U2/4 "144, INC. 5756roadHollotry Roes' Mdvie NY 11747 (631)694.3040.FAX' (631)420-84W WSDOHID#10478 LABORATORY RESULTS Town of Southold Landfill Lab No. : 0603561-007 Sample information... Type : Groundwater Attn To Origin: Client ID.: MW -4S Collected :3/16/2006 10:25:00 AM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 295 2 mg/L E310.1 03/20/2006 11:30 AM Biochemical Oxygen Demand 4 1 mg/L E405.1 03/16/20064:52 PM Bromide 2.4 1 mg/L E320.1 03/23/2006 11:00 AM Chloride 116 5 mg/L E325.2 03/27/2006 1:58 PM Chemical Oxygen Demand 28.6 1 mg/L E410.4 03/21/2006 10:08 AM Color < 5 1 units E110.2 03/17/2006 1:08 PM Chromium, Hexavalent < 0.02 1 mg/l- M3500 -Cr D 03/17/2006 1:40 PM Hardness (As CaCO3) 190 5 mg/L E130.2 03/17/20061:50 PM Nitrogen, Ammonia (As N) 22.3 20 mg/L E350.1 03/27/2006 12:37 PM Nitrate as N 1.01 5 mg/L E353.2 03/25/2006 11:31 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 12:00 PM Sulfate 38.5 1 mg/L SW9038 03/28/2006 1:46 PM Total Dissolved Solids 526 2 mg/L E160.1. 03/20/2006 11:52 AM Nitrogen, Kjeldahl, Total 26.9 50 mg/L E351.2 03/28/2006 1:37 PM Total Organic Carbon 8.5 1 mg/L SW9060 03/22/2006 6:04 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 7 of 13 �(. Laboratory Manager U2M "US, INC. 575 Broad Hollow Road, Movie NY 11747 LABORATORY RESULTS (631)694-3040. FAX 436 (631)4208NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0603561-008 Type : Groundwater Attn To Origin: Client ID.: MW -5D Collected :3/16/2006 9:55:00 AM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 686 4 mg/L E310.1 03/20/2006 11:35 AM Biochemical Oxygen Demand 3 1 mg/L E405.1 03/16/2006 4:56 PM Bromide 6.5 1 mg/L E320.1 03/23/2006 11:15 AM Chloride 301 10 mg/L E325.2 03/27/2006 1:59 PM Chemical Oxygen Demand 94.0 1 mg/L E410.4 03/21/2006 10:09 AM Color 5 1 units E110.2 03/17/2006 1:09 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:45 PM Hardness (As CaCO3) 490 10 mg/L E130.2 03/17/2006 1:55 PM Nitrogen, Ammonia (As N) 24.2 50 mg/L E350.1 03/27/2006 1:15 PM Nitrate as N 1.65 5 mg/L E353.2 03/25/2006 11:32 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 12:15 PM: Sulfate 103 10 mg/L SW9038 03/28/2006 1:48 PM Total Dissolved Solids 1100 4 mg/L E160.1 03/20/2006 11:54 AM Nitrogen, Kjeldahl, Total 73.1 50 mg/L E351.2 03/28/2006 4:10 PM Total Organic Carbon 27.5 1 mg/L SW9060 03/22/2006 6:30 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 8 of 13 QiwK r`3c . Laboratory Manager U2M "US, INC. 575 BroadH*w Road, Mdv le NY 11747 LABORATORY RESULTS (631)694.33M.FAX (631)42M436 WSDOHID#10478 Town of Southold Landfill Lab No. : 0603561-009 Attn To Collected :3/16/2006 9:30:00 AM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Color Chromium, Hexavalent Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Client ID. : MW -5S Sample Information... Type: Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed 63.5 1 mg/L E310.1 03/20/2006 11:40 AM 9 1 mg/L E405.1 03/16/2006 5:00 PM 0.8 1 mg/L E320.1 03/23/2006 11:30 AM 23.8 1 mg/L E325.2 03/27/2006 2:00 PM <10 1 mg/L E410.4 03/21/2006 10:10 AM < 5 1 units Ell 10.2 03/17/2006 1:10 PM < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:50 PM 85.0 5 mg/L E130.2 03/17/2006 2:00 PM 4.85 5 mg/L E350.1 03/27/2006 11:29 AM 1.70 5 mg/L E353.2 03/25/2006 11:33 AM < 5.0 1 pg/L E420.1 03/27/2006 12:30 PM 33.8 2.5 mg/L SW9038 03/28/2006 1:50 PM 167 1 mg/L E160.1 03/20/2006 11:56 AM 5.77 10 mg/L E351.2 03/28/2006 4:11 PM 6.8 1 mg/L SW9060 03/22/2006 7:04 PM Qualifiers: E- Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 9 of 13 Q/ww /RI�Jd Laboratory Manager U2/4 "US, INC. , 575BMdFUM Road, Mdule NY 11747 (631) O.FAX' (631)420.84W NYSDOHID#10478 LABORATORY RESULTS Sample Information... Town of Southold Landfill Lab No. : 0603561 -01 O Type : Groundwater Attn To Origin: Client ID. : MW -6D Collected :3/16/2006 11:40:00 AM Received :3/1612006 6:07:00 PM Collected By VSG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 03/20/2006 12:15 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 03/16/2006 5:08 PM Bromide < 0.5 1 mg/L E320.1 03/23/2006 12:15 PM Chloride 11.4 1 mg/L E325.2 03/27/2006 2:03 PM Chemical Oxygen Demand <10 1 mg/L E410.4 03/21/2006 10:13 AM Color < 5 1 units E110.2 03/17/2006 1:11 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 1:55 PM Hardness (As CaCO3) 52.0 2 mg/L E130.2 03/17/2006 2:15 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 03/27/2006 11:32 AM Nitrate as N 3.83 5 mg/L E353.2 03/25/2006 11:36 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 1:15 PM Sulfate 28.1 1 mg/L SW9038 03/28/2006 1:56 PM Total Dissolved Solids 117 1 mg/L E160.1 03/20/2006 12:02 PM Nitrogen, Kjeldahl, Total 1.18 10 mg/L E351.2 03/28/2006 1:42 PM Total Organic Carbon 17.6 1 mg/L SW9060 03/22/2006 9:33 PM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 10 of 13 Laboratory Manager U2M ILAUS, INC. 575 Broad Hollow Road, MdAle NY 11747 LABORATORY RESULTS (631)694-3=.FAX (631)42MW WSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0603561-011 Type : Groundwater Attn To : Collected :3/16/2006 11:20:00 AM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC Client ID. : MW -6S Origin: Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 28.6 1 mg/L E310.1 03/20/2006 12:20 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 03/16/2006 5:12 PM Bromide < 0.5 1 mg/L E320.1 03/23/2006 12:30 PM Chloride 7.9 1 mg/L E325.2 03/27/2006 2:04 PM Chemical Oxygen Demand <10 1 mg/L E410.4 03/21/2006 10:14 AM Color < 5 1 units E110.2 03/17/2006 1:12 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 2:00 PM Hardness. (As CaCO3) 47.0 1 mg/L E130.2 03/17/2006 2:20 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 03/27/2006 11:33 AM Nitrate as N - 3.32 5 mg/L E353.2 03/25/2006 11:37 AM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 03/27/2006 1:30 PM Sulfate 10.7 1 mg/L SW9038 03/28/2006 1:58 PM Total Dissolved Solids 103 1 mg/L E160.1 03/20/2006 12:04 PM Nitrogen, Kjeldahl, Total 2.19 20 mg/L E351.2 03/28/2006 1:42 PM Total Organic Carbon 40.8 1 mg/L SW9060 03/22/2006 10:04 PM Qualifiers: E . Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 11 of 13 Laboratory Manager U2M LABS, INC. 575 BroadHdlav Road, Movie NY 11747 LABORATORY RESULTS (631)691,=1-FAX(631)420.8436 WSDOHID#10478 Town of Southold Landfill Lab No. : 0603561-012 Attn To Collected :3/16/2006 12:50:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original Cc Parameter(s) Alkalinity, Total (As CaCO3) Biochemical Oxygen Demand Bromide Chloride Chemical Oxygen Demand Color Chromium, Hexavalent Hardness (As CaCO3) Nitrogen, Ammonia (As N) Nitrate as N Phenolics, Total Recoverable Sulfate Total Dissolved Solids Nitrogen, Kjeldahl, Total Total Organic Carbon Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Client ID. : MW -8D Sample Information... Type: Groundwater Origin: Results Qualifier D.F.. Units Method Number Analyzed < 1.0 1 mg/L E310.1 03/20/2006 12:25 PM 55 1 mg/L E405.1 03/16/2006 5:16 PM < 0.5 1 mg/L E320.1 03/23/2006 12:45 PM 84.8 2 mg/L E325.2 03/27/2006 2:05 PM 152 1 mg/L E410.4 03/21/2006 10:15 AM < 5 1 units El 10.2 03/17/2006 1:13 PM < 0.02 1 mg/L M3500 -Cr D 03/17/2006 2:05 PM 52.0 2 mg/L E130.2 03/17/2006 2:25 PM 2.18 1 mg/L E350.1 03/27/2006 11:34 AM 3.82 5 mg/L E353.2 03/25/2006 11:37 AM 49.3 1 pg/L E420.1 03/27/20061:45 PM 47.8 2.5 mg/L SW9038 03/28/2006 2:00 PM 385 1 mg/L El 60.1 03/20/2006 12:06 PM 71.1 50 mg/L E351.2 03/28/2006 4:13 PM 40.0 1 mg/L SW9060 03/22/2006 10:30 PM Page 12 of 13 Laboratory Manager U2M "US, INC. 575 &mad Fd3N Road, Mtivie NY 11747 (631)6911- 1 -FAX(631)42(1 M NYSDOH ID# 10478 Town of Southold Landfill Attn To : Collected :3/16/2006 12:25:00 PM Received :3/16/2006 6:07:00 PM Collected By VSG03 Copies To :Original CC LABORATORY RESULTS Lab No. : 0603561-013 Client ID. : MW -8S Sample Information... Type : Groundwater Origin: Qualifiers: E. Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 13 of 13 Laboratory Manager Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 03/20/2006 12:30 PM Biochemical Oxygen Demand 38 1 mg/L E405.1 03/16/2006 5:20 PM Bromide < 0.5 1 mg/L E320.1 03/23/2006 1:00 PM Chloride 82.7 1 mg/L E325.2 03/27/2006 2:05 PM Chemical Oxygen Demand 154 1 mg/L E410.4 03/21/2006 10:16 AM Color < 5 1 units E110.2 03/17/2006 1:14 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 03/17/2006 2:10 PM Hardness (As CaCO3) 54.0 2 mg/L E130.2 03/17/2006 2:30 PM Nitrogen, Ammonia (As N) 2.12 1 mg/L E350.1 03/27/2006 11:34 AM Nitrate as N 4.07 10 mg/L E353.2 03/25/2006 11:38 AM Phenolics, Total Recoverable 47.2 1 pg/L E420.1 03/27/2006 2:00 PM Sulfate 48.2 2.5 mg/L SW9038 03/28/2006 2:02 PM Total Dissolved Solids 363 1 mg/L E160.1 03/20/2006 12:08 PM Nitrogen, Kjeldahl, Total 71.7 50 mg/L E351.2 03/28/2006 4:13 PM Total Organic Carbon 56.7 1 mg/L SW9060 03/22/2006 11:04 PM Qualifiers: E. Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/3/2006 Page 13 of 13 Laboratory Manager U2M LABS, INC. II. Q.C. SUMMARY H2M LABS, INC. SDG: TSL005 Date: 30 -Mar -06 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analvte Result Units Amount Result %REC Limits value %RPD UCL MB -032006 MB -032006 Alkalinity, Total (As CaCO3) < 1 mg/L LCS-032006 LCS-032006 Alkalinity, Total (As CaCO3) 21.3 mg/L 25 < 1 85 80 120 0603561-009fms MW-5SMS Alkalinity, Total (As CaCO3) 90.6 m91L 25 63.5 108 75 125 0603561-009fdup MW-5SDUP Alkalinity, Total (As CaCO3) 62.1 mg/L 63.5 2.2 20 MB -03-16-06 MB -03-16-06 Biochemical Oxygen Demand <2 mg/L LCS-032306 LCS-03-16-06 LCS-03-16-06 Biochemical Oxygen Demand 196 mg/L 200 < 2 98 1 80 11201 MW-5SMS 0603561-009FDUP MW-5SDUP Biochemical Oxygen Demand 3 mg/L 9 100 20 MB -032306 MB -032306 Bromide < 0.5 mg/L LCS-032306 LCs -032306 Bromide 4.9 mg/L 5 < 0.5 98 80 120 0603561-009FMS MW-5SMS Bromide 5.6 mg/L 5 0.8 96 75 125 0603561-00917dup MW-5SDUP Bromide 0.8 mg/L 0.8 0 20 MB -03-21-06 MB -03-21-06 Chemical Oxygen Demand <10 mg/L LCS-03-21-06 LCS-03-21-06 Chemical Oxygen Demand 993 mg/L 1000 <10 99 80 1120 0603561-009CMS MW-5SMS Chemical Oxygen Demand 1020 mg/L 1000 < 10 102 75 125 0603561-009CDUP MW-5SDUP Chemical Oxygen Demand <10 mg/L < 10 20 MB -032706 MB -032706 Chloride < 2 mg/L LCS-032706 LCS-032706 Chloride 47.8 mg/L 50 < 2 1 80 1120 0603561-009FMS MW-5SMS Chloride 51.1 mg/L 25 23.8 109 175 1125 0603561-009FDUP MW-5SDUP Chloride 25.1 mg/L 1 1 23.8 5.5 20 MB -031706 MB -031706 Chromium, Hexavalent < 0.02 mg/L LCS-031706 LCS-031706 Chromium, Hexavalent 0.18 mg/L 0.2 < 0.02120 0603561-009FMS M-5SMS W Chromium, Hexavalent 0.17 mg/L 0.2 < 0.02E!85f75125 d2O 0603561-009FDUP MW-5SDUP Chromium, Hexavalent <0.02 mg/L <0.02 TSL005 W17 SDG: TSL005 QC SUMMARY REPORT Sample ID: Client Sample ID: Analyte Result Spike Sample Recovery RPDRef %RPD Units Amount Result %REC Limits Value %RPD UCL MB -031706 MB -031706 Color <5 units 1040 605 90.0 LCS-031706 ILCS-031706 Color 40 0603561-009FDUP MW-5SDUP Color <5 units 40 <5 100 80 11201 units < 5 20 FB -036 17031706 MB -031706 Hardness (As CaCO3) < 5 mg/L 561-009Dms E06O3 561-009Ddup LCS-031706 MW-5SMS MW-5SDUP Hardness (As CaCO3) Hardness (As CaCO3) Hardness (As CaCO3) 1040 605 90.0 mg/L 1000 < 5 104 80 120 mg/L 500 85.0 104 75 125 mg/L 5-7 20 MB -032506 MB -032506 Nitrate as N < 0.1 mg/L LCS-032506 LCS-032506 Nitrate as N 1.12 mg/L 1.13 <0.1 99 80 120 0603561-009CMS MW-5SMS Nitrate as N 4.11 mg/L 2.5 1.70 96 75 125 0603561-009CDUP MW-5SDUP Nitrate as N 1.70 mg/L 1.70 0 20 MB3-16478 MB3-032706 Nitrogen, Ammonia (As N) < 0.1 mg/L MB -16488 MB -032806 Nitrogen, Kjeldahl, Total < 0.1 mg/L M132-16478 MB2-032706 Nitrogen, Ammonia (As N) < 0.1 mg/L 0603561-009CMS MW-5SMS Nitrogen, Kjeldahl, Total 10.2 mg/L 4.1 5.77 108 75 125 MB1-16478 MBI -032706 Nitrogen, Ammonia (As N) < 0.1 mg/L LCS3-16478 LCS3-032706 Nitrogen, Ammonia (As N) 1.04 mg/L 1 < 0.1 104 80 120 LCS2-16478 LCS2-032706 Nitrogen, Ammonia (As N) 1.03 mg/L 1 < 0.1 103 80 120 LCS1-16478 LCS1-032706 Nitrogen, Ammonia (As N) 1.03 mg/L 1 < 0.1 103 80 120 0603561-009CMS MW-5SMS Nitrogen, Ammonia (As N) 11.0 mg/L 5 4.85 123 75 125 0603561-009CDUP MW-5SDUP INitrogen, Ammonia (As N) 5.36 mg/L 4.85 1 10 20 MBI -16488 MBl-032806 Nitrogen, Kjeldahl, Total < 0,1 mg/L MB -16488 MB -032806 Nitrogen, Kjeldahl, Total < 0.1 mg/L LCS1-16488 LCS-16488 LCS1-032806 LCS-032806 Nitrogen, Kjeldahl, Total Nitrogen, Kjeldahl, Total 4.60 4.53 mg/L 4.1 < 0.1 112 80 120 mg/L 4.1 < 0.1 110 80 120 0603561-009CMS MW-5SMS Nitrogen, Kjeldahl, Total 10.2 mg/L 4.1 5.77 108 75 125 0603561-009CDUP NMI-5SDUP INitrogen, IGeldahl, Total 6.01 mg/L 5.77 4.1 20 2 TSL005 W18 SDG: TSL005 QC SUMMARY REPORT Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MB -0327066 MB -0327066 Phenolics, Total Recoverable < 5 ug/L LCS-032706 0603561-009CMS LCS-032706 MW-5SMS Phenolics, Total Recoverable Phenolics, Total Recoverable 29.1 19.8 ug/L 30 < 5 97 80 120 u9/L 20 < 5 99 75 125 0603561-009Cdup MW-5SDUP Phenolics, Total Recoverable . 5 --'ug—/L < 5 20 MB -032806 MB -032806 Sulfate < 5 mg/L LCS-032806 LCS-032806 Sulfate 19.7 mg/L 20 < 5 98 80 120 0603561-009FMS MW-5SMS Sulfate 84.5 r WL 50 33.8 102 75 125 0603561-009Fdup MW-5SDUP Sulfate 34.2 mg/L 33.8 1.5 20 MB -03-20-06 MB -03-20-06 Total Dissolved Solids <10 mg/L LCS-03-20-06 LCS-03-20-06 Total Dissolved Solids 336 mg/L 300 _ < 10 112' 80 120 0603561-009FMS MW-5SMS Total Dissolved Solids 490 mg/L 300 167 108 75 125 0603561-009FDUP MW-5SDUP Total Dissolved Solids 171 mg/L 167 2.4 20 MB -032203 MB -032203 Total Organic Carbon <1 rncyl LCS-032203 LCS-032203 Total Organic Carbon 26.4 mg/L 25 < 1 106 80 120 0603561-009BMS MW-5SMS Total Organic Carbon 16.8 m9/L 10 6.8 100 75 125 0603561-009BDUP MW-5SDUP Total Organic Carbon 5.9 mg/L 6.8 14.2 20 TSL005 W19 U2M LAOS, INC. III. RAW DATA TSL005 W21 Si?C-pl-- I S bGC6 TSL005 W22 I&MIMIRT"I U2M LA13S9 INC. ANALYST: DATE IN: DATE OUT: STANDARD DUPLICATE TRUE VALUE 2Qb SAMPLE # RESULT fi RESULT %RECOVERYq W,e3 DUPLICATE RPD 3.Q - I l BODS CALIBRATION CHECK: IN OUT . l ul rj05 wINKLER , p METER •-- Chlorine• Elm M N:eM' 1 ;%-)EVVD W/--,+ f= mL o,iY�. 3,g _ 0- 2� mL :10f, 50, IN , WIN.11.111.1 E• �e �e ® �e :•� KIM vs�r�c�����■■��a 1 ;%-)EVVD W/--,+ f= mL o,iY�. 3,g _ 0- 2� mL :10f, 50, IN , WIN.11.111.1 E• �e �e ® �e :•� vs�r�c�����■■��a W��,d &wriOTA �i Chlorine M2 L vs�r�c�����■■��a &wriOTA r 11U01 Chlorine r 11U01 J� U2M 1AI3S9 INC. ANALYST: 4-j DATE IN: c6 DATE OUT: 112-110(o STANDARD DUPLICA TRUE VALUE S RESULT SULT % RECOVERY DUPLICATE RPD BODS rr'::-� MAV wax=omm �. : I 1 W -mm �r���■� K'AM��������rl-a■ rr'::-� CALIBRATION CHECK: IN WINKLER METER .f= mL = mL 01410 "— l,_ Wr- Chlorine:.. ® �. : I 1 W -mm �r���■� K'AM��������rl-a■ CALIBRATION CHECK: IN WINKLER METER .f= mL = mL 01410 "— l,_ WAWX WUMA m gwr, o B.s z' d H Ad'.: AVG LAR# 07ln=f--n7dl n TSL005 W25�1 os� !nl C�9,N/ro�l 'aNI3J2� QOlb ■ Wr- Chlorine:.. ® �. : I 1 WAWX WUMA m gwr, o B.s z' d H Ad'.: AVG LAR# 07ln=f--n7dl n TSL005 W25�1 os� !nl C�9,N/ro�l 'aNI3J2� QOlb ■ A".■ - 112M LABS, INC. BODS ANALYST: Qyj CALIBRATION CHECK: IN UT DATE IN: 3 WINKLER DATE OUT: OC METER STANDARD DUPLICATE TRUE VALUE S # RESULT $ULT % RECOVERY DUPLICATE RPD .,?Ae r� . "1 ,-rPH Adj.: AVG Chlorine BOD—M 11 I• . 1• r�� 1• I1 1• _, 1160 OP PH Ad'.: AVG LAB# 0061-0b►,40Chlorine m BOD % SAMP. DOt DOF A DO S.C. DO -SC BOD ®,S i�0- D11 I LL I 14.1 1 1 1 q.1m j= mL = ML ,, -. .E • .�� .,h . . 0 OWN 1• 1• •1• ® 1• •1 TSL005 W26 P 0019 1• 1• •1• ® 1• •1 TSL005 W26 P 0019 qp� wompum 1 r �1� ■ir Wpb Mr.. U2M "IBS, INC. BODS ANALYST: 4Kew DATE IN: 36 DATE OUT: 6 STANDARD D LATE TRUE VALUE AMPLE # RESULT RESULT % RECOVERY DUPLICATE RPD �4 CALIBRATION CHECK: IN WINKLER METER f= mL = ML Chlorine mg/L WEm �4 CALIBRATION CHECK: IN WINKLER METER f= mL = ML Chlorine mg/L EDAM IFR� VA �4 CALIBRATION CHECK: IN WINKLER METER f= mL = ML EWA* Chlorine mg/L EDAM IFR� wjtmw�wlmmm � EWA* Chlorine mg/L TSL005 W27 P 002:0 112AIAI3S., iNc. ANALYST: DATE IN: DATE OUT: STANDARD DUPLIC ; 'TRUE VALUE SAbOlff# RESULT u -- LT % PECOVFRV 192- BODS CALIBRATION CHECK: IN WINKLER METER !!TML f= mL U244tAJUS, INC. BODS ANALYST: 6tfj CALIBRATION CHECK: IN OUT DATE IN: -340d -P WINKLER DATE OUT: �./V/0& METER STANDARD DUPLICATr TRUE VALUE S E # RESULT SULT % RECOVERY DUPLICATE RPD .A 1./ .t S WMA" MWAY�16. 1 1 Chlorine TSL005 W29 I f= ' mL = ML m In/ -KV :.� ml„ MK,, .,, rkv� „ :,, ®� sr.�r.������®■�� WMA" MWAY�16. 1 1 Chlorine TSL005 W29 I f= ' mL = ML m In/ -KV :.� ®� ,. MWAY�16. 1 1 Chlorine TSL005 W29 I f= ' mL = ML m In/ -KV ���[Chlorine ML :.� ®� ,. ���[Chlorine ML :.� I' P 00ti2 ri- H2M LABS, INC. .. Tstoos BROMIDE DATE: s 0 (10 ANALYST: Ah 1-1'kr G H A = AsA E - ABuwx Br (mg/L) =13,320 x A x B_ D x E D:= Ds - DB,� C F ABUNx = mL DBLANK = �. mL B & E = NomiWity of r&mt — 0.0075 N x a•o/ I 11 MIS OF II • TITRATED FOR I • •III •III II • �.' .- SON III+ l + ■EN . E31M �.,f.. ' M- CIE mot 0 � 10- ®� Tom r 1 EMN �,CM' ' •A'.`1 0� - T 0 Ml CIE I • -- ®WMEM � f br d a WMEM dtlIf— /.WOOME MEN _ MMMM AjlPPF — MENIMMINIME ,'MOOMMINIME MEN MEN •� i _ SCE ���SON IMMOMEM.. i r f� r x a•o/ L Author, mad2 Original Run FNename: Original Run Author's Signature: Current Run Filename: Current Run Author's Signature: Description: 1-12M Lams. Inc. Date: 3/27/2006 OM 3-27-2006 01-39-09PM.OMN created 3127120061:39:09 PM [mad2) OM 3-27-2006 01-39-09PM.OMN last modified 3/2712006 2:14:00 PM [ms;R) Default New Run �G. fiS UJB Sample Cup No. Channell chloride Conc. m ADF Area s MDF CalStd 5:icaF5:d dw S1 100.ODO 19.085 CalStd 4:Ica%:d dw S2 75.000 15.596 Ca1Std 3:1ca19:d dw S3 50.000 11.678 CalStd 2:ical2:cI dw S4 20.000 5.374 CalStd 1:hudl:d dw S5 10.000 2.826 CalStd O:i=M:d dw S16 0.000 0.007 CRA:CRA:CL dw 32 2.226 0.596 Known Calc: 2.000 Calibration: Table/Fig. 1 LCS:LCS:CL dw 33 47.841 11.174 Known Conc: 50.000 MB-:MBLKCL dw I S16 0.534 0:022 Known Conc: 0.000 "0603792-001A:SAMP:Cl- DW" "0503794-001A:SAMP:CL DW" 1 2 14.664 .10.837 4.190 3.176 "060.3794-00?A:SAMPLC DW" 3 27.748 7.253 "0603803-W1A:SAMP:CL DW 4 10.927 3.201 "06038034002A:SAMP:CL DW' 1 10.627 3.119 "0603803403A:SAMP:CL DW B 1 10.988 3.218 70603841-001A:SAMP:CL DW' 122.123 21.919 "0603854-001A:SAMP:CL DW" 8 5.632 1.676 "0603855-001A:SAMP:CL DW" 9 4.985 1.477 "0603771-001A:SAMP:CL W' 10 1.121e+3 12.596 20.00 CCV:CCV:CL DW S2 75.006 15.597 Known Conc: 75.000 CCB:CCB:CL DW I S16 0.5571 0.030 Known Conn 0.000 "0603561401F:SAMP:CL W 11 0.604 0.047 "0603561-=F:SAMP:CL W" 12 26.427 6.966 "0603561-003F:SAMP:CL W" 13 29.712 7.671 "06035614)04F:SAMP:CL W 14 10.328 3.036 "0603561-005F:SAMP:CL W" "06035614006F:SAMP:CL W "08D3561-007F:SAMP:CL W 17 15 16 .776 116:992 ---1-T6-.469 2.601 6.292 6.269 1 5.00 5.00 "0603561-008F:SAMP:CL W" 18 300.991 7.752 10.00 "0603561-009F:SAMP:CL W* 19 23.757 6.373 "0603561-009FMS:MS:CL W 20 51.085 11.746 CCV.CCV:CL DW S2 68.482 14.603 Known Cone: 75.000 CCB:CCB:CL DW 1 S16 0.445 -0.008 Known Cons 0.000 "0603561-OWFDUP:DUP:CL W" -2-1 25.109 6.676 "0603561-01OF:SAMP:CL W" "0603561-011F:SAMP:CL W 23 22 11.392 7.894 3.328 2.347 "0603561-012F:SAMP:CL W" 24 84.829 10.184 2.00 "0603561-013F:SAMP:CLW 25 82.703 16.726 "LFB:LFB:CL W" 26 25.552 6.774 "LFBD:LFBD:CL W 27 25.210 6.698 "0603841-001A:SAMP:CL DW" 7 116.625 3.401 10.00 CCV.CCV:CL DW S2 75.263 15.636 Known Conc: 75.000 CCB:CCB:CL DW S16 0.535 0.023 Known Conc: o_nao i Run: OM_3-27-2006 01-39-09PM 'Vi.5v-I�u/O L Q.O JQ-jur; 0, -erj Tv= as 109 0000 D . vm> - 9 rnw-3q yv�a - 3S rnw-4S 1-"Lj-SS jr.w 617 Mw -6S mw -B9 rv.LJ-4 -5 1- Py O O F'+ o Vqp rn j M g CalStd 5:ical5:d dw S? CalStd 4:ical4:c! dw ra CalStd 3:ical3:cl dw o CalStd $2: 2:c dw o CalStd 1:icall:c dw CalStd O:lcalO:cl dw J CRkCRA CL dw LCS:LCS:CL dw MB-AkKCL dw A "0603792-001A:SAMP:CL DW' EX0603794-001A:SAMP:CL DW' m. v "0603794-002A:SAMP:CL DW" c "0603803-001A SAMP:CL_DW' o "0603803-002A:SAMP:CL DW' b� N o '0603803-003A:SAMP:CL DW' so w "0603841-001A:SAMP:CL_D "060385"01A:SAMP:CL DW' N 3 '61"0603855-001A:SAMRCL DW' o "0603771-0O1A:SAMP:CL W' w CCV:CCV:CL DW 3 TSL005 W32 m3 010 N g o z 3 n T C gNg c co s w 8 $ ZT 20) m CL .. I� 0 J N • z 3 n Z TSL005 W33 n VRP A V J CCB:CCB:CL DW "0603561-00IF:SAMP:CL W W "0603561-002F:SAMP:CL W' A "0603561-003F:SAMP:CL W' "0603561-006F:SAMP:CL W' "0603561-007F:SAMP:CL W' 5' "0603561-MF:SAMP:CL W' B "0603561-009FMS:MS:CL W' 3 $; CCV:CCV:CL DW CCB:CCB:CL%W 3 "0603561AFDUP:DUP:CL W "0?03561-010F:SAMP:CL W is 3 -60&3561-011 F:SAMP:CL W' it "0603561-012F:SAMP:CL_W' A B V "0603561-013F:SAMP:CL W Un "&:LFB:& W' "LFBD:LFS%:CL W 3 J Co N w N -71 Author: mad2 H2M Labs. Inc. Date: 3/27/2006 Table 1: chloride Figure 1: chloride 19.08 Area = - 8.247e-4 • Cone2 + 0.271 • Conc + 0.144 „ Conc = 0.122' Area"2 + 2.876 • Area + 0.470 Z Correlation Coefficient (r) = 0.99981 LD �o No Weighting Y f0 m CL chloride concentration, mg/L 100.000 Run: OM_3-27-2006 019-09PM -4- Lr) 4- Conc. (mg/L) Rep Peak Area (Volt -s) Peak Height (Volts) % Residual Detection Date Detection Time 1 100.000 1 19.085 2.651 -0.6 3/27/2006 1:40:43 PM 2 75.000 1 15.596 2.211 1.4 3127/2006 1:41:24 PM 3 50.000 1 11.678 1.698 -0.5 3427/2006 1:42:06 PM 4 20.0001 1 1 5.3741 0.805 -2.7 3/27/2006 1 1:42:47 PM 5 10.0001 1 1 2.8261 0.427 -2.0 327/2006 1 1:43:30 PM 6 0.0001 1 1 0.0071 0.002 3272006 1 1:44:13 PM Figure 1: chloride 19.08 Area = - 8.247e-4 • Cone2 + 0.271 • Conc + 0.144 „ Conc = 0.122' Area"2 + 2.876 • Area + 0.470 Z Correlation Coefficient (r) = 0.99981 LD �o No Weighting Y f0 m CL chloride concentration, mg/L 100.000 Run: OM_3-27-2006 019-09PM -4- Lr) 4- 4 112M LABS, INC. Anal st: Date: Start time: COD �s6,00-5 OV, Calibration 12/2912005 cone 0 abs 0 10 0.007 25 0.011 50 0.018 125 0.06 250 0.109 375 0.158 500 0.209 625 0.263 750 0.303 87510.345 10001 0.396 Intercept (b) -11.624 slope (m) 2514 r 0.9992 J E C 0 u s. 1100 1000 900 800 700 600 500 400 300 200 100 0 -100 COD Calibration 12/29/05 Absorbance ............... - Page' -,?1 • conc —Linear (conc) 9EM 9001SZ TsLoos COLOR. STD;S V IFIED 5 THRU 70: COLOR/ODOR DATE: 311-406 13� START TIME: 13 00 ANALYST: ,-mr CLIENT ID LAB# COLOR UNITS DF ODOR UNITS f NOTES ICV (40) Ics L s. EQU G03jeC/- QQ& cS Mw- Io t < s Ui- -003F -yoCOG F L s �W S -00 f C . >�w ss -ocr) -IL79f p/c CCV ( 0) CCB MuJ-6p s6' - old < McrJ`�o —t1 Zf _g `s CCV (40) CCB VIA LABS, INC. CR+6 DATE: 06 ANALYST: e ;i P C 027 1 HIM a MI 1 ■- 1 f r i .r ■- ' MTRUNI MOM ■- l i r l 11, ■- i !f 1� .mm m n, IMMF RWmff { e ;i P C 027 Calibration 12128/05 conc abs 0 0.000 0.02 0.018 0.04 0.032 0.1 0.081 0.2 0.171 0.3 0.263 0.41 0.33 Intercept (b) 0.0001 slope (m) 1.18 corr. Coeff. 0.9991 Cr+6 12/28/06 0.5 = 1. 18 38x + E-05 0.4 -j ♦ cont J tm 0.3 —Linear (conc) E v 0 0.2 V 0.1 0 0.000 0.050 0.100 0.150 0.200 0.250 0.300 0.350 Absorbance Page 1 of 1 6£rn 9001SI I 610 f -I i i p " 'Ir 12- 1.: P . 0 U2AA UAUS9 'NCO HARDNESS 50,1r ---vs vlc,-1 HARDNESS = B x N x 100,000 A DATE: ANALYST: TITRANT N CLIENT ID LAB#SED J�TA) MLS. I MG/L NOTES TITRATED�(Bj) ICV(I o0o mgh�— 10 IC8 LI)y < i0o i) loo El -317 L C. � .19 100 3 3 6. a. Ll q? 7. 9. /41 W- 6) 10 — Zo -, joy CCV(I 000 mg/1) CCB /41 Uj )to 3541 .- c;.i oa� z. m 0 -6"1) 3. 01100 , so -M a C;ip -j i 00 Li. 7 50 2,6 5. -7 6. 7. i. 9. 10. CCV(1000 mg/1) 10 — J0q0 Ec—B BRAN+LUEBBE RACE 5.48 Z�lh "IL 4_L_�, H2M Labs Inc. Post -run report Name of Run NH3032706a Name of Analysis :NH3.ANL Date of Report 3/27/2006 System No. :1 Date of Run 3/27/2006 Type of System :TRAACS Operator and Start/Stop time :11:03 - 11:41 Comment Base 67 #16478 C O J 39 Post -run Report Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/l s mg/l Calibr. Fit Linear Corr, Coeff, 0.9993 Base 67 Gain 39 Sensitivity 0.2341 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value Va e`u 0 0 B Baseline 0.02 0 1 1 P Primer 3.01 1 2 1 D Drift 3.00 1 3 1 H1 High 3.03 1 4 0 L1 Low 0.06 1 5 0 L1 Low 0.06 1 6 1 C Cal. 3.02 1 7 2 C Cal. 0.95 1 8 3 C Cal. 0.44 1 9 4 C Cal. 0.21 1 10 5 C Cal. 0.12 1 11 0 C Cal. 0.05 1 12 5 QC1 CRA 0.1 0.09 1 13 9 QC1 LCS1-16478 1.03 J031 -a 1 19 10 QC1 MB1-16978 -0.02 er 3/a�/ob 15 11 S 0603561-001C 0.02 1 16 12 S 0603561-002C 0.68 1 17 13 S 0603561-003C 0.65 1 ( S 18 14 S 0603561-004C 0.20 19 15 S 0603561-005C 0.06 NH3.ANL / NH3032706a.run Page 1 BRAN+LUEBBE AACE 5.48 20 16 S 0603561-006C 23.46 Unused 21 17 S 0603561-007C 22.25 Unused 22 18 S 0603561-008C 22.99 Unused 23 19 S 0603561-009C 4.85 1 24 20 S 0603561-009CMS 'Tv = 5 11.02 1 25 2 QCl CCV 1.0 0.93 cl J/ o 26 0 QCl CCB 0.07 LO 27 21 S 0603561-009CDUP 5.36 1 28 22 S 0603561-010c 0.08 1 29 23 S 0603561-011C 0.08 30 24 S 0603561-012C 2.18 31 25 S 0603561-013C 2.12 32 26 S 0603719-004A 0.01 33 27 S LFB1-16478 TV -:�_ 57•10 5.16 34 26 S LFBD1-16478 4.96. 35 2 QCl CCV 1.0 0.93 q 31- 36 0 QC1 CCB 0.06 •L O' 1 37 1 D Drift 3.00 38 0 B FinalBase 0.02 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS `A Channel 2 Baseline Yes Drift Yes Carry over Yes %c 4.3. ** <END OF REPORT> ** NH3.ANL / NH3032706a.run Page 2 Post -run Report Yr1w -W, -55 5 s S 10 1 1 5 r.p-9 /L✓0 r w— s S 1 —6-9 1 -6S 1 — wy 1 ._ $ S' 1 10 103 JIu 10 9 7� 1 1 1 1 NH3.ANL / NH3032706a.run Page 2 BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Calibration Curve Name of run :NH3032706a.RUN Comment Calibration Curve Name of analysis :NH3.ANL Channel :2 Method :Method 2 Curve fit :linear a= -1.1710E-001 b=7.4590E-005 Corr. coeff. :0.9993 eak [$] 100 80- 060402000.00 60- 40- 20- Oz - 0.000.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ] Page 1 of 1 M 3 BRAN+LUEBBE AACL 5.48 H2M Labs Inc. Post -run chart Post -run chart Name of run :NH3032706a.RUN Name of analysis :NH3.ANL Comment min Channel 2 Method Method 2 Unit : mg/l Base fi7 Gain 34 Corr. 0.9993 2 4 6 8 10 OB 0.02 12 1P 3.01 2D 3.00 3H 3.03 19 4L 0.06 SL 0.06 6C 3.02 7C 0.95 Page 1 of 3 ►Si ON BRAN+LUEBBE AACE 5.48 *lame of run :NH3032706a.RON j'omment Post -run chart Name of analysis :NH3.ANL min 8C 0.44 9C 0.21 10C 0.12 18 11C 0.05 12QC1 0.09 20 13QC1 1.03 14QC1 -0.02 15S 0.02 22 16S 0.68 17S 0.65 18S 0.20 24 19S 0.06 20S 23.46 21S 22.25 26 S 22.99* 23S 4.85 24S 11.02 28 25QC1 0.93 26QC1 0.07 27S 5.36 30 28S 0.08 29S 0.08 30S 2.18 31S 2.12 12 32S 0.01 33S 5.16 34S 4.96 4 35QC1 0.93 Page 2 of 3 kn BRAN+LVEBBE AACE 5.48 Name of run :NH3032706a.RUN --,Name Poat-run chart Name of analysis :NH3.ANL Run 36 37D 3.00 38 40 38B 0.02 42 44 46 48 50 52 Page 3 of 3 l (DO 91 BRAN+LUEBBE AACE 5.48 Name of Run NH3032706b Date of Report 3/27/2006 Date of Run 3/27/2006 Operator and Comment Unit H2M Labs Inc. Post -run report Name of Analysis :NH3.ANL System No. :1 Type of System :TRAACS Start/Stop time :12:16 - 12:43 #16478 eurS V 0 N -- Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/l mg/l Calibr. Fit Linear 2 Corr. Coeff. 0.9990 2.99 Base 67 Gain 34 H1 High Sensitivity 0.2300 1 Sample Limit 1 . 4 0 Sample Limit 2 . 0.06 Pk Cup Sample Id Value V e ( V tv 0 0 B Baseline 0.06 0 1 1 P Primer 3.01 1 2 1 D Drift 2.99 1 3 1 H1 High 3.02 1 4 0 L1 Low 0.06 1 5 0 L1 Low 0.06 1 6 1 C Cal. 3.03 1 7 2 C Cal. 0.94 1 8 3 C Cal. 0.43 1 9 4 C Cal. 0.20 1 10 5 C Cal. 0.11 1 11 0 C Cal. 0.04 1 12 5 QC1 CRA 0.1 0.09 1 13 9 QC1 LCS2-16478r✓r- 1. p 1.03 Io3%- 1 14 10 QCl MB2-16478 -0.02 G 0. j 1 15 11 S 0603561-006C 22.28 20 9 16 12 S 0603561-007C 22,32 20 —Lf 17 13 S 0603561-008C 66.68 20 Re - r-, 18 2 QC1 CCV 1.0 0.83 -Z-f-j%-, 1 19 0 QCl CCB 0.08 /9,1 1 NH3.ANL / NH3032706b.run Page 1 Post-run Report BRAN+LUEBBE AACE 5.98 Post -run Report 20 1 D Drift 2.99 1 21 0 B FinalBase 0.06 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused OC 3 Unused OC 9 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline yes Drift s yes Carry over Yes %: 4.9 ** <END OF REPORT> ** NH3.ANL / NH3032706b.run Page 2 BRAN+LUEBBE RACE 5.40 H2M Labs Inc. Calibration Curve Name of run :NH3032706b.RUN Comment Calibration Curve Name of analysis :NH3.ANL Channel :2 Method :Method 2 Curve fit :linear a= -1.8436E-001 b=7.4945E-005 Corr. coeff. :0.9990 eak [�] 100 80- 06040200 60- 40- 20- 0) 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ] Page 1 of 1 BR M+LUEBBE MCE 5.48 H2M Labs Inc. Post -run chart Name of run :NH3032706b.RUN Comment Poet -run chart Name of analysis :NH3.ANL min Channel 2 Method Method 2 Unit mg/l Base 67 Gain 39 Corr. 0.9990 2 9 6 8 10 12 19 OB 0.06 iP 3.01 2D 2.99 3H 3.02 9L 0.06 5L 0.06 6C 3.03 7C 0.99 Page 1 of 2 BRAN+LQEBBE MACE 5.48 -'came of run :NH3032706b.RUN omment Post -run chart Name of analysis :NH3.ANL Bin 8C 0.43 9C 0.20 10C 0.11 18 11C 0.04 12QC1 0.09 13QC1 1.03 20 14QC1 -0.02 15S 22.28 16S 22.32 22 17S 66.68 18QC1 0.83 190C1 0.08 29 20D 2.99 26 21B 0.06 28 30 32 34 Page 2 of 2 P q/o? BRAN+LDEBBE AACE 5.48 H2M Labs Inc. Post -run report Name of Run NH3032706c Date of Report 3/27/2006 Date of Run 3/27/2006 Operator and Comment #16478 Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 1 ki High 4 0 L1 Low 5 0 L1 Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. it 0 C Cal. 12 5 QC1 CRA 0.1 13 9 QCl LCS3-16478 T V = 1 0 14. 10 QCl MB3-16478 15 11 S 0603561-0080 16 2 QCl CCV 1.0 17 0 QCl ccs 18 1 D Drift 19 0 B FinalBase Name of Analysis :NH3.ANL System No. :1 Type of System :TRAACS Start/Stop time :12:54 - 13:19 V,3 S, Real Data 2 2 Method 2 Dilution mg/l ^" mg/l Linear 0.9992 67 34 0.2319 Value Va e 0.03 0 3.00 1 2.99 1 3.01 1 0.07 1 0.07 1 3.02 1 0.95 1 0.43 1 0.20 1 0.11 1 0.05 1 0.09 1 1.04 -0.02 G �' • i 1 24.15 50 M h3 J 5 0.91 0.07 L o 1 2.99 1 0.03 1 NH3.ANL / NH3032706c.run Page 1 Post -run Report BRAN+LUEBBE AACE 5.98 QC Limits Channel QC 1 Unused QC 2 Unused QC 3 Unused QC 9 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC•8 Unused QC 9 Unused QC10 Unused CORRECTIONS 2 Channel 2 Baseline yes Drift yes Carry over Ye3 8c 4.6 ** <END OF REPORT> ** NH3.ANL / NH3032706c.run Page 2 Post -run Report M V7 O O V) E-� BPJW+LUEBBE AACE 5.48 H2M Labs Inc. Calibration Curve Name of run :NH3032706c.RUN Comment Calibration Curve Name of analysis :NH3.ANL Channel :2 Method :Method 2 Curve fit :linear a= -1.8876E-001 b=7.4662E-005 Corr. coeff. :0.9992 Peak [%] 100 80- 06040200 60- 40- 20- 0 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ] Page 1 of 1 BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Post -run chart Post -run chart Name of run :NH3032706c.RUN Name of analysis :NH3.ANL Comment min Channel 2 Method Method 2 Unit mg/1 Base 67 Gain 34 Corr. 0.9992 2 4 6 B 10 OB 0.03 1P 3.00 12 2D 2.99 3H 3.01 4L 0.07 14 SL 0.07 6C 3.02 _ 7C 0.95 Page 1 of 2 kn O O BBAN+LUEBBE AACE 5.48 Vame of run :NH3032706c.RUN .'�omment Post -run chert Name of analysis :NH3.ANL min r 8C 0.43 9C 0.20 10C 0.11 18 11C 0.05 120C1 0.09 13QC1 1.04 20 140C1 -0.02 15S 24.15 160C1 0.91 22 17QC1 0.07 18D 2.99 24 19B 0.03 26 28 30 32 34 Page 2 of 2 U2A► LADS IMC. PC 7,&k 00S, - * os * (6 Y ? 9 AMMONIA DISTILLATION NAME: N� boeyg -w DATE: 3-2Y-06 f -* 00 — 13:00 vr LAB NO. CLIENT ID SAWLE WEIGHT GRAMS SAMPLE VOLUME MLS FINAL VOLUME MLS DATE ANALYZED SPIKE 1 �A�tk Sd SO -o SO /. 0 3 obn S .00 g Q PT Y S -vat tx-I � 6 S-61- oorc Dl- v0S - 8. sk- tKte - YA S11-0 W _ 561- 003 S - 009 �b!-ott Mtr- 6 S6- o!z kv,- sm S - o! *it - es V. 11-vo bF ,,; so Pt 1h J;o ; i I P 0038 IJI07 BRAN+LUEBBE RACE 5.48 I H2M Labs Inc. Post -run report Name of Run no3032506RI Name of Analysis :NO3.ANL Date of Report 3/25/2006 System No. :1 Date of Run 3/25/2006 Type of System :TRAACS' Operator Cmo Start/Stop time :11:04 - 11:43 Comment Base 89 pctsl Gain 11 Channel Type Real Data Channel 1 2 Method Method 1 Dilution Unit mg/l mg/1 Calibr. Fit Linear Corr. Coeff. 0.9998 Base 89 Gain 11 Sensitivity 0.9030 Sample Limit 1 Sample Limit 2 • Pk Cup ample S Id Value Va a \1 3+ 0 0 B Baseline 0.01 0 1 1 P Primer 2.01 1 2 1 D Drift 2.02 1 3 6 H1 High NO2 2.07 1 4 0 L1 Low 0.02 1 5 0 Ll Low 0.02 1 6 1 C Cal. 2.02 1 7 2 C Cal. 0.97 1 8 3 C Cal. 0.49 1 9 4 C Cal. 0.20 1 10 5 C Cal. 0.10 1 11 0 C Cal. 0.01 1 12 5 QC1 CRA 0.1 0.10 1 13 10 QC1 LCS-032506 i i.13 1.12 44°It 1 14 0 QC1 MB -032506 0.01 1-0.1 1 15 11 S 0603561-001C 0.03 1 16 12 S 0603561-002C KW -113 1.56 5 17 13 S 0603561-003C MW -15 1.37 5 18 14 S 0603561-004C M1.)'= !o% 3.91 5 19 15 MIV ` S 0603561-0050 IS 4.33 10 NO3-ANL / no3032506Rl.run Page 1 Post -run Report 00 O O H BRAN+LUEBBE RACE 5.48 1 QC 1 Unused 20 16 S 0603561-006C M(,J- H J Unused QC 4 Unused 21 17 S 0603561-007C M VJ - " 1,32 1.01 QC 7 5 5 22 18 S 0603561 -008C -.KW- 5b 1.65 QC10 5 23 19 S 0603561-009C MW - 5 S 24 20 S 0603561-009CMS1V=215 1.70 4.11 �J�" 5 5 25 2 QC1 CCv 1.0 0.99 Q i �� 1 26 0 QC1 CCB 0.02 LZ-' 1 27 21 S 0603561-009CDUP K I.J 55 1.70 2P1) ' O� 28 22 S 0603561-OIOC 'H w' -L 3.83 5 5 29 23 S 0603561-011C ��� s 3.32 5 30 24 S 0603561-012C M w - 3.82 5 31 25 S 0603561-013C X91%;._ � 5 4.07 10 32 26 S LFB-032506 -rvr-)O-� s 5 0.47 Q &io(, 1 33 27 S LFBD-032506 V a 0.50 00, 34 2 QC1 CCv 1.0 0.99 ;Q cto& 1 35 0 QC1 CCB 0.01 36 1 D Drift 2.02 1 37 0 B FinalBase 0.01 1 QC Limits Channel 1 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 1 Baseline yes Drift yes Carry over yes %= 1.9 ** <END OF REPORT> ** NO3,ANL / no3032506R1.run Page 2 Post -run Report BRAN+LOEBBE AACE 5.48 H2M Labs Inc. Calibration Curve Name of run :no3032506R1.RUN Comment 09rn A01, SCuzve Name of analysis :NO3.ANL Channel :1 Method :Method 1 Curve fit :linear a= -8.7100E-002 b=3.9976E-005 Corr. coeff. :0.9998 eak [�] 100 80- 0604020 60- 40- 20. 0 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 Conc. [ mg/1 ] Pages 1 BRAN*LUEBBE RACE 5.48 H2M Labs Inc. Post -run chart Post -run chart Name of run :no3032506Rl.RUN Name of analysis :NO3.ANL Comment min Channel 1 Method : Method 1 Unit : mg/l Base 89 Gain 11 Corr. 0.9998 2 4 1, 6 8 10 12 L14 OB 0.01 h r r 1P 2.01 t4 C 2D 2.02 F 3H 2.07 E Page 1 of 3 L BRAN♦LUEBBE RACE 5.48 Name of run :no3032506R1.RUN Comment Post -run chart Name of analysis :NO3.ANL min 4L 0.02 5L 0.02 6C 2.02 18 7C 0.97 8C 0.49 9C 0.20 20 10C 0.10 11C 0.01 120C1 0.10 22 13QC1 1.12 14QC1 0.01 24 15S 0.03 16S 1.56 17S 1.37 18S 3.91 26 19S 4.33 20S 1.32 21S 1.01 28 22S 1.65 23S 1.70 24S 4.11 30 25QC1 0.99 26QC1 0.02 27S 1.70 32 26S 3.83 29S 3.32 po 30S 3.62 � 34 � 31S 4.07 G E Page 2 of 3 L BRAN+LUEBBE RACE 5.48 Name of run :no3032506Rl.RUN Comment Post -run chart Name of analysis :NO3.ANL . min 32S 0.47 33S 0.50 36 34QC1 0.99 35QC1 0.01 38 36D 2.02 37B 0.01 40 42 44 46 48 50 C 52 r r E Page 3 of 3 `. j .I..J R✓ �I �...� 1✓ `a iii. {ter 6.W U2/4 I AUS, INC. Phenols Method 420.1 Distillation Dater Time: --/t?. p P(f T Sk vos er AlY 009 Analyst: ' ' 9 lo Date: Phenols P 0004 Calibration 1-4-06 conc abs 0 0.000 5 0.012 10 0.025 20 0.048 30 0,068 40 0.095 50 0.12 Intercept (b) -0.0069 slope (m) 421.33 r 0.9994 Phenol Calibration 1/4/06 60 50 - y - t2l.33x - 0.0069 40 - ' - J 30 ♦ conc c—Linear (conc) v 20 10 — 0 0.000 0,050 0.100 0.150 Absorbance Page 1 of 1 S9A S00'IS.L 70 1 SULFATE PC T � k 00S- DATE: 3 -z f -0-6 ANALYST: 13�� CLIENT ID LAB# MLS USED ABS. MG/L (GRAPH) MG/L NOTES ICV (20.0 mg/L)�• 9 . S , ICB 0.0042 r a, r 03 S,6f- 00/p as e. on 2 �s. 0 ,K lz W-1 �6-vo Io x!j: 63•o 74 CCV(20.0 mg/L) �J A• 2 3O (�• 9 d° �^ CCB ��� �J• o0 0 .ls': o 0 ,o3.S - VOW s o. Y g0 3e. 8 Mir- S,6/- oo ll. o. Y 3r.-C m%x- 9p s6/- 00F9 J.r V. 106 10.5xto_ M3 AAW-S S-6/- o to V. 8 /I.�xIS- 33.8 NtiS 41- 009 (0 0. yl 3�•Q gY +ee^lol•Y CCV(20.0 mg/L) �� O • z f 9. 9�'..t^ CCB U. 060J -0Qy4= 10 0. rSl /3.� x,?•� 3�.3 PPIDZ/.Y? v, - I -F61- olop jr o. 35 t•3 I V,- �� S61'- 96rF t 0 0.2 2 2 g. ( y-2-�'=Y7. g m tx - s6 - 0 3,P to S= Y8. CCV(20.0 mg/L) O • % %e• s,. ly LJ.�, CCB 13 0.000 ZI ,7 - a(as. zs0 696'�t z o• �Y6 /3.3 fp v 71s -on/ s. oo g /SO PR I% - aot 9S O . oa 6 '� S� O CCV(20.0 mg/L) CCB js- Q.00 0 1s,0 0r/6 I• ir•v6 Y/yl- P 0063 110 Ln V) H Calibration 12/29/05 conc abs 0 0.000 5 0.034 10 0.089 15 0.149 20 0.229 25 0.298 30 0.351 35 0.44 401 0.510 Intercept (b) 2.3217 slope (m) 75.76 corr. Coeff. 0.9964 SO4 12/29/05 y = 75.764x + 2.3217 40 30 J E20 • conc —Linear (con c) 0 v 10 0 0.000 0.100 0.200 0.300 0.400 0.500 0.600 Absorbance Page 1 of 1 • • Page 1 of 1 • S0& • f(Dried WL(a) - Tare Wt. (g))x1000N1000 � / SS/ TS T SOlids(mgll)= mL Sample GTS L' - 1 S Coc6 � Gmoo2G ANALYST: TEMP. t //.. --n DATE: 2 0 0 START: // U HUMIUI I Y: LAB # CLIENT ID PANT CRUC. SAMPLE ML DRIED WT G TARE WEIGHT G SOLID WEIGHT G RESULT MG1L DRIED . WT G IGNITED WT G VOL. WT G COND. C✓ 6? In /of! 115 2/4 0.0336 336 Q oV : I/z 7 /n o L / 105, / O. 000 /-/0 35 -ill -0 Lf -F 261 /e'o /051555 23 d.00 o 30 06o3511 - al,4. KCC /1 L l�'° / 87iEq6 o• oo6'o 60 41/ L v 5 ..6 V& 1. . toc o, o 6 6G 656 ~nig QbUV 2O /60 1,0Y110f to / / / 0,0060 66 -a24 -13G fTD //?./37 /I 9 7 oo 96 916 yG l� /Uy 621 /b 93 00 8Y" -kV �� 0.0 09/ Pa'o ov / 0,09 1 -6b7 10-V77 d . oog y �sl 26 TSL005 W68 0 OLS - 4L D ffDried Wt.(al .Tare Wt an ,nnn+, Solids(mg/I)= mL Sample GTO SS/ T$ TEMP. 2% TSL005 W69 M [!Dried Wt.(ol -Tare Wt rnnr Innn,..,nnn IDS Solids(mg/I)= mL sample (TPs S/ TS TEMP. NbMIDITY: 28 TSL005 W70 OLIDS f{Dried Wt.(a) - Tare Wt. (c)WOOON1000 TD / SS/ TS Solids(mgA)= mL Sample ANALYST: &AW TEMP. DATE: START- w*uiniTv. LAB # CLIENT ID PAN/ CRUC. SAMPLE ML DRIED WT G TARE WEIGHT G SOLID WEIGHT G RESULT MG/L DRIED WT G IGNITED WT G VOL. WT G COND. 10 v oo X MD /oy, 0 86`� y, p5yZ 0,032o azo ex.: le,3.0020 o. 000 4-/0 LIJ/5 l - Al w 16D/04! 61/G /Oy 0-0/03 /o 3 7-'v0356 144� -o12F W -$D —d -&4Y Igo%3 /03.7/00 0, o3 SS 3 r5�Sm7 -613F MO -95 /a 11. XZ' 05 //2-7:� .o.3 (3 363 �,SS� D 8 / EF • CuTf-A(16a1 r'ai26°T D /oc Sd` i o, o 2.3y P ' + y TV.1 QD z �� . X319 /2 5 y996 0,032-3 90 coy /07.7 CB 93 ieD /o 7. 97Z Boz yew o, oo os 4/0 29 TSL005 W71 T sw 212A O 3282006 2:12:58 PM Page 1 of 3 I4 c)D 5 -(rte TKN Data Concentration listed after Optical Blank Correction. Preparation dilution factor not applied to results. Peak SampleID SampTy Conc Units DF Conc x DF AnalDate AnalTime TestCod 1 Primer PRIM 3 mg/I 1 3/28/2006 01:23:37 PM tkn_w 2 Drift DRIF 3 mg/I 1 3/28/2006 01:24:17 PM tkn_w 3 High HIGH 3.01 mg/I 13.0 l 3/28/2006 01:24:57 PM tkn_w 4 Low LOW 0.03 mg/I 1 0.03 328/2006 01:25:37 PM tIM w 5 Low LOW 0.03 mg/I l 0.03 3/282006 01:26:17 PM tkn_w 6 Cal. CALB 3.02 mg/I 1 3.02 3282006 01:26:58 PM tkn_w 7 Cal. CALB 0.96 mg/I 1 0.96 3282006 01:27:37 PM tkn_w 8 Cal. CALB 0.48 mg/1 1 0.48 3282006 01:28:18 PM tkn w 9 Cal. CAM 0.2 mg/I I 0.2 3/282006 01:28:58 PM tkn w 10 Cal. CALB 0.11 mg/I I O.l l 3/282006 01:29:38 PM tkn_w I Cal. CALB 0.01 mg/I 1 0.01 3/282006 01:30:18 PM tkn w 12 OPTICAL BLK QUAL 0.71 mg/I l 0.71 3/28/2006 01:30:59 PM tkn_w 13 LCS-16488 'T✓,- q.1 ICS 0.453 mg/I 10 4.53 3282006 110% 01:31:39 PM tkr _w 14 MB -16488 mblk 0.02 mg/I 1 0.02 3/282006 ZO•1 01:32:18 PM tkn_w 15 0603180-002A SAMP 0.03 mg/I l 0.03 3/28/2006 01:32:58 PM tkn_w 16 0603561-001C S QPT SAMP 0.26 mg/I 1 0.26 3282006 01:33:33 PM tkn w 17 0603561-002C 14w- 1 1) SAMP 3.29 mg/I 1 3.29 328/2006 01:34:20 PM tkn w &I A 18 0603561-003C MW- 15 SAMP 3.26 mg/I 1 3.26 328/2006 01:35:00 PM tkn_w a v, �' � �• 19 0603561-004C 14 - 3 i SAMP 0.2255 mg/I 20 4.51 3/282006 01:35:36 PM tkn_w 20 0603561-005C NA 35 SAMP 0.42 mg/1 1 0.42 3/282006 01:36:17 PM am w 21 0603561-006C F'I W ' SA IP 2.882 mg/I 10 28.82 328/2006 01:36:58 PM tkn_w 22 0603561-007C M L` l - 5 SAMP 0.5386 mg/I 50 26.93 3/282006 01:37:37 PM tkn_w 23 0603561-008C µuJ _ 5� SAMA 3.28 mg/1 l 3.28 3/28/2006 01:38:20 PM tko_w,'�„n &xx"4 24 0603561-009C Mw - i S SAMP 3.25 mg/I 1 3.25 3282006 01:39:00 PM tkn_w j -tA c>ju-(,(. 25 CCV 1.0 ccv 1.2 mg/I 1 1.2 3/28/2006 1?R% 01:39:36 PM tkn_w 26 CCB ccb 0.15 mg/l 1 0.15 3/282006 01:40:16 PM tkn_w 27 0603561-009CMS MIA) -!55 ms 1.097 mg/l 10 10.97 3/28/2006 01:40:57 PM tkn_w 28 0603561-009CDUP MW'- i �% d.p 3.26 mg/I 1 326 3/282006 01:41:40 PM tkn_w&r.A "- 29 0603561-01OC MW " (7 SAMp 0.118 mg/I 10 1.18 3282006 01:42:16 PM tkn_w 30 0603561-011C MtJ " 6 S SAMA 0.1095 mg/I 20 2.19 328/2006 01:42:59 PM tkn_w O O 3282006 2:12:58 PM Page 1 of 3 I4 Peak SampleID SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod 31 0603561-012C SAMp 3.27 mg/l I 3.27, 3/28/2006 01:43:40 PM tkn_w ATIm. (AX 32 0603561-013Ct"'� - �s SAMP 3.23 mg/l I j 3.23; 3/28/2006 01:44:20 PM tkn_w 33 0603013-OOIA SAMP 1.294 mg/l 20 �2 8 3/28/2006 01:44:56 PM tkn_w 34 0603626-003A SAMP 0.9598 mg/l 50 47.99 3/28/2006 01:45:36 PM tkn_w 35 0603626-004A SAMP 2.464 mg/l 10 24.64 3/28/2006 01:46:18 PM tkn_w 36 0603628-OOIA SAMP 0.75 mg/1 1 0.75 3/28/2006 01:46:49 PM tkn_w 37 CCV 1.0 ccv 1.04 mg/1 1 1.04 3/28/2006 INW. 01:47:38 PM tkn w 38 CCB ccb 0.08 mg/l 1 0.08 3/28/20060.1 01:48:17 PM tkn_w 39 0603628-002A SAMP 0.53 mg/l 1 0.53 3/28/2006 01:48:58 PM tkn_w 40 0603628-003A SAMP 0.51 mg/l 1 0.51 3/28/2006 01.49:38 PM tkn_w 41 0603637-OOIA SAMP 0.8665 mg/l 20 17.33 3/28/2006 01:50:18 PM tkn_w 42 0603637-002A SAMP 1.653 mg/l 20 33.06 3/28/2006 01:50:58 PM tkn_w 43 0603702-OOIA SAMP 0.672 mg/l 10 6.72 3/28/2006 01:51:38 PM tkn_w 44 0603702-002A SAMP 1.607 mg/l 10 16.07 3/28/2006 01:52:18 PM tkn_w 45 0603706-OOIA SAMP 0.82 mg/l 1 0.82 3/28/2006 01:52:58 PM tkn_w 46 0603707-OOIA SAMP 0.39 mg/l 1 0.39 3/28/2006 01:53:38 PM tkn _w 47 0603707-002A SAMP 0.58 mg/l I 0.58 3/28/2006 01:54:18 PM tkn_w 48 0603707-003A SAMP 0.66 mg/l 1 0.66 3/28/2006 01:54:57 PM tkn_w 49 CCV 1.0 ccv 0.98 mg/l 1 0.98 3/28/2006 01:5538 PM tkn_w 50 CCB ccb 0.04 mg/l 1 0.04 3/28/2006 01:56:17 PM tkn_w 51 0603708-OOIA SAMP 0.547 mg/l 20 10.94 3/28/2006 01:56:58 PM tkn_w 52 0603708-002A SAMP 1:83 mg/l 20 36.6 3/28/2006 0(:57:38 PM tkn_w 53 0603738-OOIA SAMP 0.209 mg/l 10 2.09 328/2006 01:58:17 PM ikn_w 54 0603738-002A SAMP 0.466 mg/l 10 4.66 3/28/2006 01:58:58 PM tkn_w 55 0603741-002A SAMP 0.162 mg/l 10 1.62 328/2006 01:59:37 PM tkn_w 56 0603752-OOIA SAMP 1.132 mg/l 10 11.32 3282006 02:00:18 PM tkn_w 57 LFB-16488 T1s Ifb 0.412 mg/l 10 4.12 328/2006 16D t..�"02:00:58 PM tkn w 58 LFBD-16488, Ifbd 0.417 - mg/l 10 4.17 3282006 9M= 1 '02:01:39 PM tkn_w 59 CCV 1.0 ccv 0.96 mg/l 10.96 3/282006 CA% 02:02:19 PM tkn _w 60 CCB ccb 0.02 mg/I 1 0.02 328/2006 LO•t 02:02:57 PM tkn_w M 61 Drift DR1F 3 mgfl 1 L- 3282006 02:03:39 PM tkn-w ;28/2006 2:12:58 PM O O Page 2 of 3 Peak SampleID SampTy Cone Units DF Conc x DF AnalDate AnalTime ' TestCod 62 End END 0.02 mg/I I 1 0.02 3/28/2006 02:04:54 PM tkn_w 3/28/2006 2:12:58 PM O O Page of BRAN+LUEBBE AACE 5.48 Name of Run tkn032806 Date of Report 3/28/2006 Date of Run 3/28/2006 Operator cmo Comment 1 pctsl 1 Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 1 H1 High 4 0 L1 Low 5 0 Ll Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. it 0 C Cal. 12 8 QC1 OPTICAL BLK 13 9 QC1 LCS-16488 14 10 QC1 MB -16488 15 11 S 0603180-002A 16 12 S 0603561-001C 17 13 S 0603561-002C 18 14 S 0603561-003C 19 15 S 0603561-004C H21W Labs Inc. Post -run report Name of Analysis :TKN.ANL System No. :1 Type of System :TRAACS Start/Stop time :13:12 - 14:05 Real Data 2 2 Method 2 Dilution mg/l mg/l Linear 1 0.9997 1 72 1 22 1 0.4182 1 Value Value 0.02 0 3.00 1 3.00 1 3.01 1 0.03 1 0.03 1 3.02 1 0.96 1 0.48 1 0.20 1 0.11 1 0.01 1 0.71 1 5.24 10 0.73 1 0.74 1 0.97 1 4.00 1 3.97 1 5.22 20 TKN.ANL / tkn032806.run Page 1 Post -run Report BRAN+LUEBBE AACE 5.48 20 16 S 0603561-005C 1.13 21 17 S 0603561-006C 29.53 22 18 S 0603561-007C 27.64 23 19 S 0603561-008C 3.99 24 20 S 0603561-009C 3.96 25 2 QC1 CCV 1.0 1.20 26 0 QC1 CCB 0.15 27 21 S 0603561-009CMS 11.68 28 22 S 0603561-009CDUP 3.97 29 23 S 0603561-010c 1.89 30 24 S 0603561-011C 2.90 31 25 S 0603561-012C 3.98 32 26 S 0603561-013C 3.94 33 27 S 0603013-001A 26.59 34 28 S 0603626-003A 48.70 35 29 S 0603626-004A 25.35 36 30 S 0603628-001A 1.46 37 2 QC1 CCV 1.0 1.04 38 0 QC1 CCB 0.08 39 31 S 0603628-002A 1.24 40 32 S 0603628-003A 1.22 41 33 S 0603637-001A 18.04 42 34 S 0603637-002A 33.77 43 35 S 0603702-001A 7.93 44 36 S 0603702-002A 16.78 45 37 S 0603706-001A 1.53 46 38 S 0603707-001A 1.10 47 39 S 0603707-002A 1.29 48 40 S 0603707-003A 1.37 49 2 QC1 CCV 1.0 0.98 50 0 QC1 CCB 0.04 51 41 S 0603708-001A 11.65 52 42 S 0603708-002A 37.'31 53 43 S 0603738-001A 2.80 54 44 S 0603738-002A 5.37 55 45 S 0603741-002A 2.33 56 46 S 0603752-001A 12.03 57 47 S LFB-16488 4.83 58 48 S LFBD-16488 4.88 59 2 QC1 CCV 1.0 0.96 60 0 QC1 CCB 0.02 61 1 D Drift 3.00 62 0 B FinalBase 0.02 QC Limits 1 10 50 1 1 1 1 10 1 10 20 1 1 20 50 10 1 1 1 1 1 20 20 10 10 1 1 1 1 1 1 20 20 10 10 10 10 10 10 1 1 1 1 TKN.ANL / tkn032806.run Page 2 Post -run Report kn 0 C) BRAN+LUEBBE RACE 5.98 Post -run Report Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 9 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 0.9 ** <END OF REPORT> ** F__q TKN.ANL / tkn032806.run Page 3 BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Calibration Curve Name of run :tkn032806.RUN Comment Calibration Curve Name of analysis :TKN.ANL Page 1 of 1 BPAN-LUEBBE RACE 5.48 H2M Labs Inc. Post—run chart Post -run chart Name of run :tkn032806.RUN Name of analysis :TKN.ANL Comment min Channel 2 Method : Method 2 Unit mg/l Base 72 Gain 22 Corr. 0.9997 2 9 6 8 10 OB 0.02 1P 3.00 12 2D 3.00 3H 3.01 c 9L 0.03 19 t t 5L 0.03 c 6C 3.02 F 1 7C z 0.96 Page 1 of 3 >T n D D BRAN+LUEBBE AACE 5.48 Name of run :tkn032806.RUN Comment Post -run chart Name of analysis :TKN.ANL Page 2 of 3 BRANaLUEBBE RACE 5.40 Name of run :tkn032806.RUN Comment Post -run chart Name of analysis :TKN.ANL Page 3 of 3 3/28/2006 4:24:27 PM N 00 O O Page l of I F- H -S TK` ` Data Concentration listed after Optical Blank Correction. Preparation dilution factor not applied to results. Peak SampleID SampTy Conc Units DF Conc a DF AnalDate AnalTime TestCod 1 Primer PRIM 3.01 mg/I 1 3.01 3/28/2006 03:59:50 PM tkn_w 2 Drift DRIF 3.01 mg/I 1 3.01 3/28/2006 04:00:30 PM tkn_w 3 High HIGH 3.02 mg/I 1 3.02 3/28/2006 04:01:10 PM dM-w 4 Low LOW 0.02 mg/I 1 0.02 3/28/2006 04:01:49 PM tlrn_w 5 Low LOW 0.02 mg/I 1 0.02 3/28/2006 04:02:30 PM tkn w 6 Cal. CALB 3.02 mg/I 1 3.02 3/28/2006 04:03:10 PM tkn_w 7 Cal. CALB 0.96 mg/I I 0.96 3/28!2006 04:03:49 PM tkn_w 8 Cal. CALB 0.48 mg/I 1 0.48 3/28/2006 04:04:30 PM tkn_w 9 Cal. CALB 0.21 mg/I 1 0.21 3/28/2006 04:05:12 PM dm 10 Cal. CALB 0.11 mg/I I O.l 1 3/28/2006 04:05:50 PM -w tkn w 1 I Cal. CALB 0.02 mg/I 1 0.02 3/28/2006 04:06:30 PM tkn_w 12 OPTICAL BLK QUAL 0.72 mg/1 1 0.72 3/28/2006 04:07:11 PM tkn_w 13 LCSI-1648$x1/0 a/. 1cs 0.46 mg/I 10 4.6 3/28/2006 tIZ°/' 04:07:51 PM tkn_w -_ 14 MBI-16488 mblk 0.02 mg/I 1 0.02 3/28/2006 04:08:31 PM tkn_w 15 0603561-002C MIJ - t l) SAMP 2344 mg/1 10 23.44 3/28/2006 04:09:11 PM tkn_w 16 0603561-003C KW SAMP 2.513 mg/I 10 25.13 3/28/2006 04:09:50 PM tkn_w 17 0603561-008C M k/ - 5 SAMA 1.4614 mg/1 50 73.07 3/28/2006 04:10:30 PM 18 ' S 5 tkn_w 0603561-009C )4W SAMA 0.577 mg/I 10 5.77 3/28/2006 04:11:10 PM tkn w 19 0603561-009CMS'�V-,H. ms 1.018 mg/l 10 10.18 3/28/2006 10$�G 04:11:51 PM tkn_w 20 0603561-009CDUP dup 0.601 mg/1 10 6.O1 328/2006 q*Y0=04;12:30 PM tkn 21 0603561-012C A W-- 16 i SAMP 1.4216 mg/I 50 71.08 328/2006 04:13:11 PM w tkn_w 22 0603561-013C SAMP 1.4338 mg/I 50 71.69 328/2006 04:13:51 PM tkn_w 23 CCV 1.0 ccv 0.96 mg/I 1 0.96 3282006 96°4 04:14:30 PM tln_w 24 CCB ccb 0.02 mg/1 1 0.02 3282006 LD 04:15:11 PM tkn_w 25 Drift DRIF 3.01 mg/I 1 3.01 3282006 04:15:51 PM tlm_w 26 End END 0.02 mg/I 1 0.02 3282006 04:17:15 PM tkn_w 3/28/2006 4:24:27 PM N 00 O O Page l of I F- H BRAN+LUEBBE'AACE 5.48 Name of Run tkn032806a Date of Report 3/28/2006 Date of Run 3/28/2006 Operator =0 Comment Unit pctsl mg/l H2M Labs Inc. Post -run report Name of Analysis :TKN.ANL System No. :1 Type of System :TRAACS Start/Stop time :15:48 - 16:17 Channel Type Real Data Channel 2 2 Method Method . -2 Dilution Unit mg/1 mg/l Calibr. Fit Linear P Corr. Coeff. 0.9998 1 Base 74 D Gain 23 1 Sensitivity 0.4257 Sample Limit 1 Sample Limit 2 Pk Cup Sample Id Value Value 0 0 B Baseline 0.02 0 1 1 P Primer 3.01 1 2 1 D Drift 3.01 1 3 1 H1 High 3.02 1 4 0 L1 Low 0.02 1 5 0 '' Ll Low 0.02 1 6 1 C Cal. 3.02 1 7 2 C Cal. 0.96 1 8 3 C Cal. 0.48 1 9 4 C Cal. 0.21 1 10 5 C Cal. 0.11 1 11 0 C Cal. 0.02 1 12 8 QC1 OPTICAL BLK 0.72 1 13 9 QC1 LCS1-16488 5.32 10 14 10 QC1 MBI -16488 0.74 1 15 11 S 0603561-002C 24.16 10 16 12 S 0603561-0030 25.85 10 17 13 S 0603561-008C 73.79 50 18 14 S 0603561-009C 6.49 10 19 15 S 0603561-009CMS 10.90 10 TKN.ANL / tkn032806a.run Page 1 Post -run Report BRAN+LUEBBE RACE 5.48 20 16 S 0603561-009CDUP 6.73 21 17 S 0603561-012C 71.80 22 18 S 0603561-013C 72.41 23 2 QC1 CCV 1.0 0.96 24 0 QC1 CCB 0.02 25 1 D Drift 3.01 26 0 B FinalBase 0.02 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 0.7 ** <END OF REPORT> ** TKN.ANL / tkn032806a.run 10 50 50 1 1 1 1 Page 2 Post -run Report BRAN+LUEBBE RACE 5.48 H2M Labs Inc. Calibration Curve Calibration Curve Name of run :tkn032806a.RUN Name of analysis :TKN.ANL Comment Channel :2 Method' :Method 2 Curve fit :linear a= -2.0447E-001 b=6.0620E-005 Corr. coeff. :0.9998 Peak [�] 100 80- 06040206 60- 40- 20-- 0 r r V C 0 C H 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 CO Conc. [ mg/l ] F Page 1 of 1 BRAN+LUEBBE RACE 5.48 Post -run Chart H2M Labs Inc. Post -run chart Name of run :tkn032806a.RUN Name of analysis :TKN.ANL Comment min Channel : 2 Method Method 2 Unit mg/l Base 79 Gain 23 Corr. 0.9998 2 4 I 6 8 10 OB 0.02 12 1P 3.01 2D 3.01 3H 3.02 14 4L 0.02 5L 0.02 �r C ` C 6C 3.02 v. 16, 7C 0.96 Page 1 of 2 BRANaLUEBBE RACE 5.48 Post-run chart Name of run :tkn032806a.RUN 1 Comment Name of analysis :TKN.ANL Page 2 of 2 V2AM LABS, INC. Pc lb oo� ke(ify 6S 9% eXP I -,F -V6 TOTAL/TRN DIGESTIONS g' �" ��o O vr AA�! ryK °l NO. CLIENT ID SAMPLE WEIGHT GRAM SAMPLE FINAL VOLUME MLS DATE YZED SPIKE WIN FIE 0110011010110 FIE iU�011EMENE1101MENEMMENEM MENEM MENEM ME MEN SEE MEN SEE MEN MAIN MEN 0110 0110 P 0070 00 00 0 0 IH2AA LABS, INC. TOTAL/TXN DIGESTIONS NAM: Al"llH ✓Cr -oV . DATE • 3-19 -d � LAB NO. CLIENT ID-1WEIGHT SAMPLE GRAMS SAMPLE VOLUME MIS FINAL VOLUME MLS DATE ANALYZED SPIKE .oeo cwt Its ,t,s Im S o z -tet k 7o -0/ Alr— C Ai s 38- ASIS 1s S, 0. 79.004 ^Y. Y. l P 0071 sC 00S ; `' (-x� goo-isi 14 � 03 I, Multiple Analysis Report Print Date/Time: 2006/03/23 9:26:48 ID --- _ _ _ Result a -a -e Std. Dev. RSD Mode ALT Method Method ID Sample P Type Vial Timestamp Message ID1 LCB-itc ti ^^ 10,r/ 0.1824 26.3760 0.0157 0.6007 8.62 2.28 UTILITY Cleaning _ ProcedureSample SOm===aQ6sp�2006/03/22a12:290 ICB tj,p 0.0551 0.1494 271.47 TOC TOC TOC TOC WASTE WASTE WATER WATER Sample 1 2006/03/22 12:56 -0 Det Detected CRI ed 3.%,'.......... Sample 2 2006/03/22 13:30 Low Sample -0 Detected r , 0.8533... 0.1494.. 17.50...TOC TOC WASTE WATER ...Sample 3..2006/03/22 19:01.Low Sample MBLK -O Detected 4.6 -0.1089 0.2228 -204.72 TOC TOC WASTE WATER Sample 4 2006/03/22 14:29 Low Sample 0603561-001B EiPr -0 Detected G/ 0 0.0617 0.4543 735.73 TOC TOC WASTE WATER Sample 5 2006/03/22 15:09 Low Sample 0603561-002B. Oh -JA 0603561-0038 14W -1S ..... 21.7237... 22.0974 0.2780.. 0.4753 1.28 ... TOC TOC WASTE WATER ...Sample 6..2006/03/22 15:33. 0603561-004B MW- 30 3.0051 0.1178 2.15 3.92 TOC TOC TOC WASTE WATER Sample 7 2006/03/22 16:03 -D-Detected TOC WASTE WATER Sample 8 2006/03/22 16:34 Low Sample 0603561-00513. W:!?...... 2.9550... -c Detected 0.1430.. 4.84...TOC TOC WASTE WATER ...Sample 9..2006/03/22 17:05.Low Sample 0603561-006B VAW -40 0603561-007B fY�W-L{s 8.5469 8.5343 1.4277 0.8544 16.70 10.01 TOC TOC WASTE WATER Sample 2006/03/22 17:34 0603561-0088. ...... 5S 27.5232... 4.3150.. 15.68... TOC TOC TOC TOC WASTE WASTE WATER WATER Sample it 2006/03/22 18:04 0603561-009B JAW- 6.7925 0.3212 4.73 TOC TOC ...Sample 12..2006/03/22 18:30. 0603561-009BMS'I'ys10 1tlOX, 16.7989 0.6946 4.13 TOC TOC WASTE WASTE WATER Sample 13 2006/03/22 19:04 CCV.7j/t1;rgFr..........IJP 27.8504... 0.1884.. 0.68... TOC TOC WASTE WATER WATER. Sample 14 2006/03/22 19:33 a e p 0.2099 6 0:239 114.13 TOC TOC WASTE Sample Sample 15..2006/03/22 16 20:03. Detected d .WATER. 2006/03/22 20:34 Low Sample 0603561-009BDUP :. 060j861-01013. "90-46 Rp=h2 5.8909 .0,4342 7.37 TOC TOC WASTE WATER .' Sample 17 2006/03/22 21:.09 0603561-011B . 17.5753... 40.8477 0.3606.. 0.2388 2.05...TOC 0.58 TOC WASTE WATER ...Sample 18..2006/03/22 21:33. 0603561-012B MW -D40.0250 7.9998 19.99 TOC TOC TOC WASTE WATER Sample 19 2006/03/22 22:04 0603561-�013B.NW.-. s.. -N, 56.7498... 0.6890.. 1.21 ... TOC TOC TOC WASTE WASTE WATER WATER Sample 20 2006/03/22 22:30 SGP1 26.9951 0.3270 1.21 TOC TOC ...Sam le 21..2006/03/22 23:04. CCBCCV Ct. 0.9617 0.2593 55.07 TOC TOC WASTE WASTE WATER WATER Sample Sample 22 2006/03/22 23:34 -0 Detected 23 2006/03/23 00:05 Low Sample Printed: 3/23/06 9:26:49 AM AM Page 1 of 1 a Detailed Analysis Report Print Date/Time: 2006/03/23 9:26:52 Sample ID: ID1 Mode: UTILITY Method: TOC WASTE WATER Method: Cleaning Procedure Filename: 03221205 Operator ID: JASON Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 12:29 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 11.232 12.223 107 2 25.7717 Baseline Baseline Time 1 0.2003 0.1002 20858 11.130 11.328 116 2 0.1663 0.0832 18149 11.168 11.367 117 3 0.1726 0.0863 18654 11.139. 11.338 115 4 --------------------------------------------------=-------------------------- 0.1906 0.0953 20086 11.172 11.369 117 <<<Statistics>>> Mean: 0.1824 Std Dev: 0:0157 RSD: 8.62 Sample ID: LCS Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 12:56 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 27.2066 1.3603 221674 11.232 12.223 107 2 25.7717 1.2886 210240 11.335. 12.320 106 3 26.2323 1.3116 213911 11.302 12.284 106 4 26.2935 ----------------------------------------------------------------------------- 1.3147 214398 11.252 12.252 106 <<<Statistics>>> Mean: 26.3760 Std Dev: 0.6007 RSD: 2.28 Sample ID: ICB Mode:;, TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 13:30 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.1201 0.0060 5855 11.211 11.169 120 2 -0.1659 -0.0083 3577 11.204 11.159 120 3 0.1630 0.0082 6197 11.267 11.241 120 4 0.1030 ----------------------------------------------------------------------------- 0.0052 5719 11.280 11.252 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.0551 Std Dev: 0.1494 RSD: 271.47 Sample ID: CRI Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 14:01 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning;: Ending Integration Baseline Baseline Time 1 1.0049 0.0502 12905 11.236 11.228 120 2 0.8770 0.0439 11886 11.214 11.202 120 3 0.6473 0.0324 10056 11.244 11.225 120 4 0.8840 ----------------------------------------------------------------------------- 0.0442 11942 11.194 11.160 120 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.8533 Std Dev: 0.1494 RSD: 17.50 Sample ID: MBLK Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Tiinestamp: 2006/03/22 14:29 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline' Baseline Time 1 0.0184 0.0009 5045 11.16..9., 11.197 120 2 0.0113 0.0006 4988 11.198 11.228 120 Printed: 3/23/06 9"26:53 AM AM Page 1 of 6 3 -0.0231 -0.0012 4714 11.193 11.189 120 4 -0.4420 -0.0221 1377 11.226 11.224 120 ----------------------------------------------------------------------------- Last Message: Low Sample Detected <<<Statistics>>> Mean: -0.1089 Std Dev: 0.2228 RSD: -204.72 Sample ID: 0603561-001B Method: TOC WASTE WATER Cal. Curve: TOC WW CURVE 021606 Operator ID: JASON SAMUEL Rep # ppm C ug C Raw Data Mode:. TOC Filename: 03221205 Timestamp: 2006/03/22 15:04 Sample Type: Sample Beginning Ending Integration Baseline' Baseline Time 1 -0.5562 -0.0278 467 11.279 11.232 120 2 0.0071 0.0004 4955 11.144 11.134 120 3 0.3342 0.0167 7561 11.153 11.177 120 4 0.4619 ----------------------------------------------------------------------------- 0.0231 8579 11.101 11.076 120 Last Message: Low Sample Detected Baseline Time 1 2.8337 <<<Statistics>>> Mean: 0.0617 Std Dev: 0.4543 RSD: 735.73 2 3.0662 Sample ID: 0603561-002B 10.967 Mode:. TOC 3 3.0951 Method: TOC WASTE WATER Filename: 03221205 11.025 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 15:33 Operator ID: JASON SAMUEL Sample Type: Sample Last Message: Low Rep # ppm C ug C Raw Data Beginning Ending Integration <<<Statistics>>> Mean: 3.0051 Std Baseline. . Baseline Time 1 21.4297 1.0715 175645 11.121. 12.110 105 2 21.6195 1.0810 177157 11.090 12.084 105 3 21.7564 1.0878 178248 11.0.61 12.046 105 4 22.0890 ------------------------------------------------- 1.1045 180898 11.062'• ---------------------------- 12.052 106 <<<Statistics>>> Mean: 21.7237 Std Dev: 0.2780 RSD: 1.28 Sample ID: 0603561-003B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 16:03 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 21.8477 1.0924 178975 10.971 11.970 104 2 22.7268 1.1363 185980 10.927 11.911 105 3 22.1787 1.1089 181612 10.957 11.946 105 4 21.6364 . ----------------------------------------------------------------------------- 1.0818 177291 10.944 11.930 105 <<<Statistics>>> Mean: 22.0974 Std Dev: 0:4753 RSD: 2.15 Sample ID: 0603561-004B Mt I ode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 16:34 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 2.8337 0.1417 27477 10.991 11.002 120 2 3.0662 0.1533 29329 10.967 11.020 120 3 3.0951 0.1548 29559 10.979 11.025 120 4 3.0254 ----------------------------------------------------------------------------- 0.1513 29004 11.022 11.078 120 Last Message: Low Sample Detected _ <<<Statistics>>> Mean: 3.0051 Std Dev: 0.1178 RSD: 3.92 Sample ID: 0603561-005B Method: TOC WASTE WATER Cal. Curve: TOC WW CURVE 021606 Operator ID: JASON SAMUEL Mode: TOC Fijename: 03221205 Timestamp: 2006/03/22 17:05 Sample Type: Sample Printed: 3/23/06 9:26:53 AM AM Page 2 of 6 Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline.' Baseline Time 1 3.1527 0.1576 30018 11.134 12.132 94 2 2.9573 0.1479 28461 11.085 11.085 120 3 2.8215 0.1411 27380 11.020 11.022 120 4 2.8886 0.1444 27914 ------------------------------------------------- 11.019 11.045 120 Last Message: Low Sample Detected --------------------------- <<<Statistics>>> Mean: 2.9550 Std Dev: 0.1430 ASD: 4.84 Sample ID: 0603561-006B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal: Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 17:34 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 10.2236 0.5112 86357 11.184 12.167 100 2 9.2412 0.4621 78530 10.991 11.986 100 3 7.2874 0.3644 62962 10.948 11.933 100 4 7.4355 0.3718 64142 ----------------------------------------------------------------------------- 11.060 12.054 99 <<<Statistics>>> Mean: 8.5469 Std Dev: 1.4277 RSD: 16.70 Sample ID: 0603561-007B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Time§tamp: 2006/03/22 18:04 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 7.9692 0.3985 68394 11.065 12.053 99 2 9.3572 0.4679 79454 11.044 12.037 100 3 9.1670 0.4584 77939 10.997 11.987 100 4 7.6436 0.3822 65800 ----------------------------------------------------------------------------- 10.980 11.973 100 <<<Statistics>>> Mean: 8.5343 Std Dev: 0.8544 RSD: 10.01 Sample ID: 0603561-008B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 18:30 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline... Baseline Time 1 33.8043 1.6902 274242 11.253 12.244 105 2 26.8036 1.3402 218462 10.981.. 11.969 106 3 25.2021 1.2601 205702 10.941 11.941 106 4 24.2829 1.2141 198378 ----------------------------------------------------------------------------- 10.897 11.879 106 <<<Statistics>>> Mean: 27.5232 Std Dev: 4.3150 RSD: 15.68 Sample ID: 0603561-009B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 19:04 Operator ID: JASON SAMUEL Sample Type: 'Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 7.1083 0.3554 61535 10.917 11.914 98 2 6.5186 0.3259 56837 10.853 11.838 98 3 7.0302 0.3515 60913 10.819 11.806 99 4 6.5128 0.3256 56791 ----------------------------------------------------------------------------- 10.817 11.811 99 <<<Statistics>>> Mean: 6.7925 Std Dev: 0.3212 ASD: 4.73 Sample ID: 0603561-009BMS Mode: TOC Printed: 3/23/06 9:26:53 AM AM Page 3 of 6 Method: TOC WASTE WATER Filename: 03221205 TOC Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 19:33 Operator ID: JASON SAMUEL Sample'Type: Sample Timestamp: 2006/03/22 21:04 Rep # ppm C ug C Raw Data Beginning Ending Integration Type: Sample Rep # ppm C Baseline.:_ Baseline Time 1 15.7679 0.7884 130532 10.701.. 11.700 103 2 17.0280 0.8514 140573 10.652 '. 11.638 104 3 17.1273 0.8564 141364 10.636' 11.623 104 4 17.2723 ----------------------------------------------------------------------------- 0.8636 142519 10.625 11.611 104 <<<Statistics>>> Mean: 16.7989 Std Dev: 0.6946 RSD: 4.13 11.319 99 Sample ID: CCV 5.6006 Mode: TOC 11.314 Method: TOC WASTE WATER Filename: 03221205 Mean: 5.8909 Std Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 20:03 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 28.1131 1.4057 228896 10.746 11.734 107 2 27.8562 1.3928 226849 10.787 11.784 107 3 27.7431 1.3872 225948 10.822 11.813 106 4 27.6893 ---------------------------------------------- 1.3845 225519 10.776 11.772 107 <<<Statistics>>> Mean: 27.8504 Std --------------------------- Dev: 0.1884 RSD: 0.68 Sample ID: CCS Mode• TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WN CURVE 021606 Timestamp: 2006/03/22 20:34 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 -0.0023 -0.0001 4880 10.644 10.569 120 2 0.4640 0.0232 8595 10.551 10.547 120 3 0.0133 . 0.0007 5004 10.548 10.561 120 4 0.3647 ----------------------------------------- 0.0182 7805 10.501. 10.495 120 Last Message: Low Sample Detected --------------- <<<Statistics>>> Mean: 0.2099 Std Dev: 0.2396 RSD: 114.13 Sample ID: 0603561-009BDUP Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 21:04 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline' Baseline Time Baseline Baseline Time 1 5.4452 0.2723 48284 10.472 11.471 98 2 6.1830 0.3092 54163 10.379 11.362 98 3 6.3350 0.3167 55374 10.327 11.319 99 4 ----------------------------------------------------------------------------- 5.6006 0.2800 49523 10.321 11.314 98 <<<Statistics>>> Mean: 5.8909 Std Dev: 0.4342 RSD: 7.37 Sample ID: 0603561-010B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 21:33 Operator ID: JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration Baseline' Baseline Time 1 17.8212 0.8911 146893 10.222" 11.209 104 2 17.1955 0.8598 141907 10.216 11.215 104 3 17.9392 0.8970 147833 10.186 11.170 103 4 17.3454 ----------------------------------------------------------------------------- 0.8673 143102 10.175 11.168 104 <<<Statistics>>> Mean: 17.5753 Std Dev: 0.3606 RSD: 2.05 Printed: 3/23/06 9:26:53 AM AM Page 4 of 6 Sample ID: 0603561-0116 Mode: TOC TOC Method: TOC WASTE WATER Filename: 03221205 TOC WASTE WATER Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 22:04 Operator ID: JASON SAMUEL Sample Type: Sample Operator Rep # ppm C ug C Raw Data Beginning Ending Integration 1 40.9983 2.0499 331562 Baseline 10.170 Baseline 11.166 Time 108 2 40.5329 2.0266 327853 10.157 11.145 109 3 41.0635 2.0532 332082 10.119 11.111 108 4 40.7961 2.0398 329951 ------------------------------------------ 10.104 11.099 109 <<<Statistics>>> Mean: 40.8477 Std -------------------------- Dev: 0.2388 RSD: 0.58 3 Sample ID: 0603561-012B Mode: TOC Filename: Method: TOC WASTE WATER Filename: 03221205 2006/03/22 23:04 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 22:30 Operator ID: JASON SAMUEL Sample Type: Sample 2.8643 461335 Rep # ppm C ug C Raw Data Beginning Ending Integration 1 36.3221 1.8161 294303 Baseline 10.041_ . Baseline 11.034 Time 108 2 36.3607 1.8180 294611 10.013 11.001 108 3 52.0066 2.6003 419274 10.483 11.476 108 4 35.4107 ---------------------------------------------------- 1.7705 287041 9.956 10.946 108 <<<<Stati6•stics>>>-Mean:- 400250 ---Std Dev: ---7_9998--- ----------------- RSD: -19_99-�- ------ Sample ID: 0603561-013B Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/22 23:04 Operator ID: JASON'SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 1 57.2857 2.8643 461335 Baseline 9.913 Baseline Time 10.906 111 2 56.3878 2.8194 454181 9.925_ 10.909 111 3 55.9590 2.7979 450765 9.887' 10.877 111 4 57.3667 ----------------------------- 2.8683 461981 9.921 '' 10.915 111 <<<Statistics>>> --------------------------------------- Mean: 56.7498 Std Dev: 0.6890 RSD: 1.21 Sample ID: CCV Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp; 2006/03/22 23:34 Operator ID. JASON SAMUEL Sample Type: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 1 27.1805 1.3590 221465 Baseline 9.959 Baseline Time 10.950 107 2 26.5209 1.3260 216210 10.035 11.027 107 3 27.0394 1.3520 220341 10.040 11.037 106 4 27.2394 ------------------------------------------=---- 1.3620 221935 10.027 11.020 107 <<<Statistics>>> Mean: 26.9951 Std Dev: 0.3270 ---------------------- RSD: 1.21 Sample ID: CCB Mode: TOC Method: TOC WASTE WATER Filename: 03221205 Cal. Curve: TOC WW CURVE 021606 Timestamp: 2006/03/23 00:05 Operator ID: JASON SAMUEL Sample Type: ype: Sample Rep # ppm C ug C Raw Data Beginning Ending Integration 1 0.5295 0.0265 9117 Baseline 9.995 Baseline Time 10.018 120 2 0.6466 0.0323 10050 9.973 9.995 120 3 0.0871 0.0044 5593 9.993 9.977 120 --4------0_5837 ---------- 0.0292------9549 -------------------------------------------- 9.958 9.991 120 Printed: 3/23/06 9:26:53 AM AM Page 5 of 6 Last Message: Low Sample Detected <<<Statistics>>> Mean: 0.4617 Std Dev: 0:2543 RSD: 55.07 Printed: 3/23/06 9:26:53 AM AM Page 6 of 6 14 0l H Calibration Report Print Date/Time: 2006/03/23 9:27:24 Cal. Curve ID: TOC WW CURVE 021606 Created: 2006/03/09 09:12 Calibration Factor (m): 1.594e+05 Y Intercept (b): -122 r -squared: 0.99958 Standard ID Y X Expected Measured Message Date s Raw Data ug C ug C Time DI 1370 0.000 0.009 Low Sample De 2006/03/08 17:27 0.5PPM 7650 0.025 0.049 Low Sample De 2006/03/08 17:50 l.OPPM 14608 0.050 0.092 Low Sample De 2006/03/08 18:13 S.OPPM 35761 0.250 0.225 2006/03/08 18:35 10.OPPM 73270 0.500 0.461 2006/03/08 18:58 25.OPPM 196089 1.250 1.231 2006/03/08 19:20 50.OPPM 395860 2.500 2.485 2006/03/08 19:43 75.OPPM 601041 3.750 3.772 2006/03/08 20:06 Printed: 3/23/06 9:27:25 AM AM Page 1 of 1 U2M LABS, INC. SDG NO.:�" 06 SCAN: " "+N P�' This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. I Signature:, Date: