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HomeMy WebLinkAboutVolatiles Data Package 03/2006Analytical Data Package For TOWN OF SOUTHOLD PART 360 ROUTINE SDG NO: TSI.005 Water Samples Received: 3/16/06 \/x'11 AT11 17'0 DAl'A PACKAGE J F I A I-Ausm� Is Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 U2M "US, INC. ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 3/16/06 SDG NO.: TSI -005 I. NYS DEC SUMMARY FORMS II. SDG NARRATIVES III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. VOLATILES B. METALS C. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY U2M "USo INC. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE IDENTIFICATION AND ANALYTICAL REQUIREMENT SUMMARY SDG: TSL005 Anal ical Requirements M O O CLPNon-CLP lease indicate year of protocol) AS? 9 iolcW TCUTAL, HSL, Priority Pollutant, Customer Sample Code Laboratory Sample Code ME Msvoa we EQPT 0603561-001 X X X MW -11) 0603561-002 X X X MW -1S 0603561-003 X X X MW -31) 0603561-004 X X X MW -3S 0603561-005 X X X MW -41) 0603561-006 X X X MW -4S 0603561-007 X X X MW -51) 0603561-008 X X X MW -5S 0603561-009 X X X MW -61) 0603561-010 X X X MW -6S 0603561-011 X X X MW -813 0603561-012 X X X MW -8S 0603561-013 X X X TRIP BLANK 3116 0603561-014 X M O O CLPNon-CLP lease indicate year of protocol) AS? 9 iolcW TCUTAL, HSL, Priority Pollutant, NE�IV Y`ORtC':STA'fiE DEPARTIWE1"'F ENVIRONMENTAL CONSERVATION- SAMPLEPREPARATIONAND ANALYSIS SUMMARY VOLATILE (VOA) SDG: TSL005 ANALYSES Laboratory Analytical Date . . Da#eRecd Date Date Extraction Sam ID Client Sample ID , Matrix Protocol Collected at Lab Extracted Analyzed Method DF Level FAux Cleanup 0603561-OOIA 0603561-002A JEQPT MW -1D Aqueous Aqueous ASPB 8260 ASPB 8260 16 -Mar -06 16 -Mar -06 16 -Mar -06 16 -Mar -06 123 -Mar -0611 23 -Mar -06 1 LOW LOW 0 MW-1S W -1S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-004A MW -3D Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-005A MW -3S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -061 123 -Mar -061I LOW 0603561-006A MW -4D Aqueous ASPB 8260 16 -Mar -06 16 -Mar -061 123 -Mar -061 1 I LOW 0603561-007A MW -4S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -061 123 -Mar -061 I LOW 0603561-008A MW -5D Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-009A MW -5S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-009AMS MW-5SMS Aqueous ASPB 8260 16 -Mar -06 16 -Mu -06 23 -Mar -06 1 LOW 0603561-009AMSD MW-5SMSD Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -061 I LOW 0603561-OIOA MW -6D Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -061 1 LOW 0603561-011A MW -6S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-012A MW -8D Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-013A MW -8S Aqueous ASPB 8260 16 -Mar -06 16 -Mar -06 23 -Mar -06 1 LOW 0603561-014A TRIP BLANK 3/16 Aqueous ASPB 8260 1 16 -Mar -06 16 -Mar 061 123 -Mar -06 1 LOW TSL005 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSL005 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd at Lab Date Analyzed 0603561-001 EQPT WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-002 MW -1D WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-003 MW -1S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-004 MW -3D WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-005 MW -3S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-006 MW -4D WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-007 MW4S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-008 MW -5D WATER AG,AL,AS,B,BABE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-009 MW -5S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-009DUP MW-5SD WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-009MS MW-5SS WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-010 MW -6D WATER AG,ALAS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-011 MW -6S WATER AG AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-012 MW -8D WATER AG,ALAS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NANI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 0603561-013 MW -8S WATER AG AL AS,B,BA,BE,CA CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 16 -Mar -06 03/06 TSL005 A5 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSI -005 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Tests Date' Recd at Lab Date Analyze 0603561-001 EQPT Blank SELECT WET CHEMISTRY *' 03/16/06 03/06 0603561-002 MW -1D Groundwater SELECT WET CHEMISTRY ** 03/16/06 03/06 0603561-003 MW -IS Groundwater SELECT WET CHEMISTRY'* 03/16/06 03/06 0603561-004 MW -3D Groundwater SELECT WET CHEMISTRY `* 03/16/06 03/06 0603561-005 MW -3S Groundwater SELECT WET CHEMISTRY ** 03/16/06 03/06 0603561-006 MW -4D Groundwater SELECT WET CHEMISTRY'* 03/16/06 03/06 0603561-007 MW -4S Groundwater SELECT WET CHEMISTRY ** 03/16/06 03/06 0603561-008 MW -5D Groundwater SELECT WET CHEMISTRY *' 03/16/06 03/06 0603561-009 MW -5S Groundwater SELECT WET CHEMISTRY ** 03/16/06 03/06 0603561-009DUP MW-5SDUP Groundwater SELECT WET CHEMISTRY `* 03/16/06 03/06 0603561-009MS MW-5SMS Groundwater SELECT WET CHEMISTRY *' 03/16/06 03/06 0603561-010 MW -6D Groundwater SELECT WET CHEMISTRY *' 03/16/06 03/06 0603561-011 MW -6S Groundwater SELECT WET CHEMISTRY ** 03/16/06 03/06 0603561-012 MW -8D Groundwater SELECT WET CHEMISTRY *` 03/16/06 03/06 0603561-013 MW -8S Groundwater SELECT WET CHEMISTRY" 03/16/06 03/06 ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand; Chloride; Chromium, Hexavalent; Color; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total; Phenolics, Total. Recoverable ; Sulfate ; Total Dissolved Solids ; Total Organic Carbon ; U2M ILAI3S, INC. II. SDG NARRATIVES U2M "US, INC. SDG NARRATIVE FOR VOLATILE ANALYSES SAMPLE RECEIVED: 3/16/06 SDG#: TSL005 For Samples: EQPT MW -5D MW -1D MW -5S MS/MSD MW -IS MW -61) MW -3D MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S TRIP BLANK 3/16 The above samples were analyzed according to the requirements of the NYSDEC ASP 10/95 method 8260B for the part 360 baseline list of volatile organic analytes. All QC data and calibrations met the requirements of the method, and no problems were encountered with sample analysis. The following should be noted: • Sample MW -5S was analyzed as the matrix spike/matrix spike duplicate. • 4-Bromofluorobenzene had a 26.5% RSD in the initial calibration of 3/20/06, which exceeded 20.5% but met the acceptance limit of 40%. The response factor for trichloroethene was greater than 0.3 in the initial calibration of 3/20/06. Tetrachloroethene had a 34.8% D in the continuing calibration of 3/23/06, which exceeded 25% D but met the acceptance limit of 40%. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 3, 2006 ************************* M— J Slavin nior Vice President o:\gc\narr2006\pctsl\volatiles\ts]005.doc U2M "US, INC. For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 3/16/06 SDG#: TSL005 EQPT MW -5D MW -1D MW -5S MS/MSD MW -1S MW -61) MW -3D MW -6S MW -3S MW -813 MW -4D MW -8S MW -4S Thirteen water samples were received by H2M Labs, Inc. ' on 3/16/06 for cyanide and select metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument, method 7470A with a Leeman Hydra mercury analyzer and cyanide method 335.2. Sample MW -5S was utilized for QC analysis and reporting. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 3, 2006 * k �k�k�klk*�k ok#�k�k�k�k�k�k�k�k a*�k�k�ko Ie�k Vincent Stancampiano Vice President o:\qc\narr2006\pctsl\metals\tsIO05.doc U2M UAUS, INC. SDG NARRATIVE FOR WET CHEMISTRY SAMPLE RECEIVED: 3/16/06 SDG#: TSL005 For Samples: EQPT MW -5D MW -1D MW -5S MS/MSD MW -1S MW -613 MW -31) MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S EPA420.1 Thirteen water samples were received by H2M Labs, Inc. on 3/16/06 for select wet chemistry analysis. Samples were prepared and analyzed using the following methods: PARAMETER Alkalinity METHOD # EPA 310.1 PARAMETER METHOD # Ammonia EPA 350.1 BOD EPA 405.1 Nitrate EPA 353.2 Bromide EPA 320.1 Phenols EPA420.1 Chloride EPA325.2 Sulfate EPA 9038 COD EPA 410.4 TDS EPA 160.1 Color EPA 110.2 TKN EPA 351.2 Hexavalent Chromium STDM 3500 -CR D TOC EPA 9060 Hardness EPA 130.2 Sample MW -5S was utilized for duplicate and spike QC analysis and reporting Duplicate analysis did not reproduce within acceptance ranges for biochemical oxygen demand (BOD). Duplicate acceptance range for BOD is ± the CRDL of 2 mg/L. The difference between sample and duplicate values was 6 mg/L. Since the BOD values were low data usability should not be affected. Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 3, 2006 ************************* * Vincent Stancampiano 0 Vice President oAgc\narr2006\pcts1\wet chemsitry\ts1005.doc Lr) O O F-+ U2M LABS, INC. III. CHAIN OF CUSTODY DOCUMENTATION ELddwm so INC. 376 Broad Hallow Rd AftMV4 MY 11747-6076 1�5 VERNAL CHAIN OF CUSTODY Tak (631) 694-300F=. (631) 420-8436 PROJECT NAMEMIUMBER So HT'o 6 p / 710 wN ®l¢ jo&7MOL I 3 Pcr.� do a 2006 Q $us�lrh CLIENT: a � _♦ :3-� J O V rK Z s J J k G o O Z Q 4 Z ?� a � = J -J ,( a r o o — sicjl��Rrl H2M SDG .NO- NOTES: Pnyea! Comae CBR Bob s� , cc. ems' F oio R/ Rtd Siltf. Prron.Akanba: TdT Rt,K �S/ J ��4{� �( / � 8 g) c op NH3� A103 PriQuote# PHFgacs �f P r v� L m �r g 4s BORON N n,P ART 36O V ° C 710 RL N655 SAMPLERS: (t>ignafurey V S A DELIVERABLES: AHa-YSIS REQUESTEDGY TURNAROUND TIME: a 1 ,D19 -LIS ORGANIC DATE' TIME MA FIELD I.D. I� �a l9) o v LAB I.D. NO. . REMARKS: Sib 1: OD- L_ Of 7- 3. a 1 r F — L TR )P AL41Y K o 0TRIPBLS-NQS o L M rv- Is 1 3 a a I I I I 60 ab iLf. qo L MW— lb N 3 a CO 2. mw -23S. /} 3 z 12, 1 1 1 I Mw - 3D 11 3 a 1 I 11 OU jab 10.35 6610:55 /0w cb�D m w- 5S 33 9 6 3 3 3 3 659 /hsnaso by ) Date Tine itaoafrad Vs 6- 3 I6 06 f g 6?' ° 3•rb u T iT:cr] LABORATORY USE (*LY COC Re=d? Y or N Gln: ShWw or wea Detvaed arbor 2 Mrbiont or eta- Tamp & Raoeived in COW oond ' Y a N 4. PlWvly pre Wm& Y or N COC Taos waw 1.Pl a gan outer padmW YorN 2 unbratw an autr puJraprX Y or N &= eaoord praaarrt & oonplate upon sampb r000tpt YorN Rebqdshodptft h, i Tkne tteoeived by. ( +�) Dab -Date Ttme R ud bY• rSOaftwe) Deb Time Rao*.vd by: (sWimae) Dab Time PAWO te wd by: (SiOrratw) Dab Tkne lRsclhvdw-'moft") Dab Time WHI I E COPY - ORIGINAL YELLOW DOPY - CLIENT PINK COPY - LABORATORY TSL005 Al2 so INC• 16op EXTERNAL CHAIN OF CUSTODY • S,4 Broad fk tAow ft k NYIIM-WO Tee (631) 694-3040ftX. (WI) 4ZU-M5 CLIENT: L jH2M SDG NO: 51.. . PROJECT NAMEINUMBER g,0p1T06 Of %O� W/Y OF �S0!% V OL b aJ o� a o06 Q. P 360 O � Z -jz J Q J �' i � x J o � J c61 (n J 1 NOTES: Ph*wCo ttoct D� BR,CL Ccoc0 R CR+b Se � � �� 'bT +I g -M_S 4J �,�«,. I C-2) Cob). N H3 NO3 X / �-� $ Mlicl� T k N quote # C) PLoS f+) C WE S� F/41q 136 0 VO C (�) 7-07/-114L HIA i4bNESS SAMPLERS: (s)gnatwellCdent DELIVERABLES: 86-70 ANALYSIS REQUESTED TURNAROUND TIME: a / .64 Ys ORGANIC INORG. DATE TIME L% FIELD I.D. v LAB I.D. NO. REMARKS: �b n.20 L 14 W— o 1 Il `to L IN — 11 3 Z o f 1 1 a — S. 11 3 2 2 i f OQ •.5a L m w— g l 3 2 2 I r l l t2 Re�Z ) y s C— Dab 3 /b o� True i 8' b Dab 3•, Tkm � 9 M- 7 LABORATORY USE ONLY S eeMeen samae Labeis Ora COC Record? Y or N ExpW: somwn wasp l• sfrpped or Nrand Delvwed arbkV 2 AmWw t ar diMsd, lW* &R ch h good', --'r n: Y or N 4. PiWwly pr mm& Y orN COC Teom mw 1. PrMwrt on war peclugx Y or N 2 lhr6t c o AwaulF paJap� Y N N a COC rrcord pnsarl a I'm' up- sartpb moeipt YorN by (sloes) Time Reabhood by (mss) naa TNtle by ( ) Deb T& Rem IL by: (8l g*n) Dab Tkm PA* qu}dW by: (Sigrahm) Deb Tittle Reniwd by (si0r�)) Dab Time T009"EA99PY - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY H2M LABS, INC. Sample Receipt Checklist Client Name PCTSL Date and Time Receive Work Order Numbe 0603561 Checklist completed7b 7j l to p 1p Signature Date Matrix Carrier name Hand Delivered Shipping container/cooler in good condition? Yes Custody seals intact on shippping container/cooler? Yes ❑ Custody seals intact on sample bottles? Yes ❑ Chain of custody present? Yes Chain of custody signed when relinquished and received? Yes Chain of custody agrees with sample labels? Yes Samples in proper container/bottle? Yes Sample containers intact? Yes (] Sufficient sample volume for indicated test? 411 samples received within holding time? ;Dontainer/Temp Blank temperature in compliance Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? Yes Yes ❑Q ? Yes ❑d No VOA vials submitted ❑ Yes 0 Adjusted? Received by PS `CSL'0os 3/16/2006 6:07:00 PM Reviewed by 4— Initials' �e D7 a� No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ Yes 0 No ❑ Checked b Not Applicable ❑ Not Applicable R Not Applicable 0 No ❑ Any No and/or NA (not applicable) response must be detailed in the comments section b ---------------------------------------------- Client contactedyES Date contacted: 3 — Person contacted ! 1/� �1� Contacted by: J �:12AC-L Regarding Comments: ONdQ ' �j�� 0A K& -CA)(-, � Milo Corrective Actio �"i� mES���Ji bR By�U�' cJ�YJ H2AA tAUS, INCO INTERNAL CHAIN OF CUSTODY DELI VERADLES: TURN AROUND TDAE: SDG I: CASE 11: MATRIX: pH CHECK Y.(jN REMAMS: RECEIVED BY: -SIGNATURE- DATE: T WVA E:�N VOLATILE P 0419 ■ � s VOLATILE P 0419 12A U AUS, INC. INTERNAL CHAIN OF CUSTODY LTE TrME SAMPLE RELINQUISHED BY SAMPLE RECEIVED BY BOTTLE TYPE PURPOSE OF CHANGE OF CUSTODY INIT Biot Slow slow slow slow 3l0M slaw slow slaw slow slow BION al ow sI ON slow Slow Sloe/ SIGN slow SIGN ' 31 OW SIGN - - SIGN SIGN slow SIGN ' SIOY SIGN slew SIGN slow SIow slow 5I0I9 h' slow SIGN SIGN SIGN slow SIGN slow slow SIGN sic" SIGN t SIGN slow SIGN SIGN SIC" VOLATILE X20 V2AA LAUS9 INCe INTERNAL CHAIN OF CUSTODY CLIENT: TURN AROUND TIME: 91 -7 SDG #-. SL c� CASE #.MATRIX: Li pHOWC&N REMARKS.—('b �CZLC� REcErAm 13y. o� ���DA I? METALS P 0151 lH2A4 ILAUS9 INC. CL]IRNT: SDG INTERNAL CHAIN OF'CUSTODY METALS P 0152 00 LAIEs, isce INTERNAL CHAIN OF CUSTODY [LIENT: r 1��7 L DELIVERABLES -IK -10-D TURN AROUND TIIAE: SDG #:'FDWZ,C�' _ CASE #: MATRIX: pH CISCO or N NEMARKS: 09t �lb�5 �VFD BY: � SIGNATURE: DAIS: `b TOM WET CHEMISTRY w P Ois9 1 �44 W. ms im I IN WET CHEMISTRY w P Ois9 � I SD9 INTERNAL CHAIN OF CUSTODY WET CHEMISTRY P O170 PURPOSE.. "I CHARGE O. _CUSTODY ®�11WT TIN WET CHEMISTRY P O170 INC.N2� «►�s, ID��- I CLIENT: SDQ v INTERNAL CHAI DATE TIME 'SAMPLE RELINQUISHED B PURPOSE OF —] SAMPLE BOTTLE CHANGE OF RECEIVED BY TYPE CUSTODY IH IT 31 .fJ 1 1 SI� 167. —e4 Blow viola 1E so Aim Silas aim sIw alga" SIGN Blow .111op SIGN slow slow Slow Blow 3101 slow SIGN slow SzcN SIGIN SIGN SIG39 SIGN .91021 SIC" 5200 sic" • slow 31018 slow SIGN slow Stoll sign Blois 210K. slow SICU 11 "low SIGN slow SIC" LEE SIGN sic" WET CHEMISTRY $k V) p 0171 -7 I I 1�2M LABS, 1 N C. IV. ANALYTICAL DATA PACKAGE A. VOLATILES B. METALS C. WET CHEMISTRY lH2M LABS, INC. t j SL..Oos VOLATILE ORGANICS TABLE OF CONTENTS I. QC SUMMARY H. SAMPLE DATA PACKAGE III. STANDARDS DATA PACKAGE IV. RAW QC DATA PACKAGE V. DOCUMENTATION U2M "US, INC. I. QC SUMMARY FOR VOLATILE ORGANICS A. SYSTEM MONITORING COMPOUND RECOVERY FORM B. MS/MSD FORM C. MSB FORM D. METHOD BLANK FORM E. GC/MS TUNING FORM F. INTERNAL STANDARD AREA AND RT SUMMARY G. INSTRUMENT DETECTION LIMITS 2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 O1 02 03 04 OE OE 0 OE 05 1C 11 12 13 14 15 1E 17 IE 19 EPA SAMPLE NO. SMC1 DCE # SMC2 TOL # SMC3 OTHER BFB # TOT OUT VBLK032306 96 101 101 0 LFB032306 101 100 100 0 MSB032306 99 101 102 0 EQPT 96 100 101 0 MW -1D 97 99 101 0 MW-iS 96 99 100 0 MW -31) 96 99 100 0 MW -3S 96 100 100 0 MW -41) 96 100 101 0 MW -4S 95 99 100 0 MW -51) 95 100 100 0 MW -5S 94 99 99 0 MW-SSMS 95 100 99 0 MW-SSMSD 95 101 100 0 MW -6D 94 99 100 0 MW -6S 94 100 100 0 MW -81) 94 99 99 0 MW -8S 94 99 99 0 TRIP BLANK 3/16 92 99 99 0 QC Limit SMC 1 DCE = 1,2-Dichloroethane-d4 (76-114) SMC 2 TOL = Toluene -d8 (88-110) SMC3 BFB = 4-Bromofluorobenzene (86-115) # Column to be used to flag recovery values * Values outside of contract required QC limits page 1 of 1 FORM II VOA -1 OLM04.2 3A WATER VOLATILE MATRIX SPIRE/MATRIX SPIRE DUPLICATE RECOVERY Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix Spike - BPA Sample No.: MW -5S COMPOUND SPIKE ADDED (Ng/L) SAMPLE CONCENTRATION (Ng/L) MS CONCENTRATION (Ng/L) MS % REC # QC. LIMITS REC. 1,1-Dichloroethene 50 0 53 106 61-145 Benzene 50 0 55 111 76-127 Trichloroethene 50 0 52 104 71-120 Toluene 50 0 53 107 76-125 Chlorobenzene 50 0 54 108 75-130 COMPOUND SPIKE ADDED (N9/L) MSD CONCENTRATION (Ng/L) MSD % REC # % RPD # QC LIMITS RPD REG. 1,1-Dichloroethene 50 57 114 7 14 61-145 Benzene 50 61 121 9 11 76-127 Trichloroethene 50 57 114 9 14 71-120 Toluene 50 58 117 9 13 76-125 Chlorobenzene 50 59 119 10 13 75-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 5 outside limits Spike Recovery: 0 out of 10 outside limits COMMENTS: FORM III VOA -1 OLM04.2 3A SYSTEM MONITORING SPIKE RECOVERY Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Sample ID MSB032306 SDG No.: TSL005 Level:(low/med) LOW COMPOUND SPIKE ADDED (Ng/L) SAMPLE CONCENTRATION (Ng/L) SPIKE CONCENTRATION (Ng/L) SPIKE % REC # QC. LIMITS REC. 1,1-Dichloroethene 50 0 50 100 61-145 Benzene 50 0 54 108 76-127 Trichloroethene 50 0 51 102 71-120 Toluene 50 0 51 103 76-125 Chlorobenzene 50 0 52 104 75-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits Spike Recovery: 0 out of 5 outside limits COMMENTS: FORM III SW8260B 3A SYSTEM MONITORING SPIKE RECOVERY Lab Name: H2M LABS, INC. Lab Code: 10478 Contract: Case No.: PCTSL SAS No.: Sample ID LFB032306 SDG No.: TSL005 Level:(low/med) LOW COMPOUND SPIKE ADDED (Ng/L) SAMPLE CONCENTRATION (Ng/L) SPIKE CONCENTRATION (Ng/L) SPIKE % REC # QC. LIMITS REC. Chloromethane 50 0 53 106 70-114 Vinyl chloride 50 0 55 111 66-117 Bromomethane 50 0 54 109 50-136 Chloroethane 50 0 54 109 71-116 Acrylonitrile 50 0 58 116 74-122 Trichlorofluoromethane 50 0 55 109 64-124 1,1-Dichloroethene 50 0 53 105 67-120 lodomethane 50 0 54 108 70-122 Vinyl acetate 50 0 53 106 76-118 Acetone 50 0 63 125 71-125 Carbon disulfide 50 0 54 107 61-126 Methylene chloride 50 0 55 111 80-112 trans-1,2-Dichloroethene 50 0 54 108 74-115 1,1-Dichloroethane 50 0 55 110 77-114 cis-1,2-Dichloroethene 50 0 55 109 78-116 2-Butanone 50 0 58 117 74-121 Bromochloromethane 50 0 55 110 81-114 Chloroform 50 0 56 112 75-119 1,1,1 -Trichloroethane 50 0 55 110 66-126 Carbon tetrachloride 50 0 58 116 64-126 Benzene 50 0 55 111 77-116 1,2-Dichloroethane 50 0 57 115 76-120 Trichloroethene 50 0 56 112 72-121 1,2-Dichloropropane 50 0 56 112 81-115 Dibromomethane 50 0 56 113 82-114 Bromodichloromethane 50 0 57 113 78-118 cis-1,3-Dichloropropene 50 0 57 114 79-116 4-Methyl-2-pentanone 50 0 57 114 79-121 Toluene 50 0 56 111 70-125 trans-1,3-Dichloropropene 50 0 57 113 77-120 4 Column to ne used to slag recovery and RPD values with an asterisk * Values outside of QC limits Spike Recovery: COMMENTS: 0 out of 47 outside limits FORM III SW8260B 3A SYSTEM MONITORING SPIKE RECOVERY Lab Name: H2M LABS, INC. Lab Code: 10478 Sample ID LF] Contract: Case No.: PCTSL SAS No.: SDG No.: TSL005 Level:(low/med) LOW 1,12 -Trichloroethane 50 0 57 114 82-116 Tetrachloroethene 50 0 59 118 59-133 2-Hexanone 50 0 59 118 76-119 Dibromochloromethane 50 0 58 115 79-118 1,2-Dibromoethane 50 0 57 114 81-117 Chlorobenzene 50 0 56 111 72-124 trans-l,4-Dichloro-2-butene 50 0 55 110 47-135 Ethylbenzene 50 0 54 109 68-128 1,1,12 -Tetrachloroethane 50 0 57 114 76-119 Xylene (total) 150 0 160 109 70-125 Styrene 50 0 55 110 72-124 Bromoform 50 0 58 116 75-121 1,1,2,2 -Tetrachloroethane 50 0 57 113 77-120 1,2,3-Trichloropropane 50 0 57 113 78-118 1,4 -Dichlorobenzene 50 0 55 110 67-128 1,2 -Dichlorobenzene 50 0 56 112 71-123 1,2-Dibromo-3-chloropropane 50 0 57 114 1 74-123 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits Spike Recovery: 0 out of 47 outside limits COMMENTS: FORM III SWB260B 4A VOLATILE METHOD BLANK SUMMARY EPA SAMPLE NO. VBLK032306 Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Lab File ID: A\A45399.D Lab Sample ID: VBLK032306 Date Analyzed: 03/23/06 Time Analyzed: 10:34 GC Column: R-502.2 ID: .53 (mm) Heated Purge: (YIN) N Instrument ID: HP5971 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS., AND MSD: 0' 0; 0< 0� 0; 0( 0 O( 0S 1( 11 1: 1' 1� 1: 1E 11 1E COMMENTS: EPA SAMPLE NO. LAB SAMPLE ID LAB FILE ID TIME ANALYZED LFBO32306 LFB032306 A1A45400.D 11:05 MSB032306 MSB032306 AW45401.D 12:09 EQPT 0603561-001A A\A45402.D 12:49 MW -1D 0603561-002A A1A45403.D 13:21 MWAS 0603561-003A A\A45404.D 13:53 MW -313 0603561-004A AW45405.D 14:24 MW -3S 0603561-005A A1H45406.D 14:56 MW -4D 0603561-006A A1A45407.D 15:27 MW -4S 0603561-007A A1A45408.D 15:59 MW -5D 0603561-008A XA45409.D 16:30 MW -5S 0603561-009A A1A45410.D 17:02 MW-5SMS 0603561-009AMS A1A45411.D 17:34 MW-5SMSD 0603561-009AMSD A1A45412.D 18:05 MW -6D 0603561-010A A1A45413.D 18:36 MW -6S 0603561-011A A1A45414.D 19:08 MW -e1) 0603561-012A A1A45415.D 19:39 MW -6S 0603561-013A A\A45416.D 20:11 TRIP BLANK 3/16 0603561-014A AW45417.D 20:42 page 1 of 1 FORM IV VOA OLM04.2 m/e ION ABUNDANCE CRITERIA 5A 50 15.0 - 40.0% of mass 95 VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK 75 30.0 - 60.0% of mass 95 45.8 BROMOFLUOROBENZENE (BFB) Base peak, 100% relative abundance Lab Name: H2M LABS, INC. Contract: 6.9 Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Lab File ID: A\A45313.D BFB Injection Date: 03/20/06 Instrument ID: HP5971 BFB Injection Time: 17:47 GC Column: R-502.2 ID: .53 (mm) 5.2 (6.5)2 m/e ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 15.0 - 40.0% of mass 95 18.0 75 30.0 - 60.0% of mass 95 45.8 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.096 of mass 95 6.9 173 Less than 2.0% of mass 174 0.0 (0.0)1 174 Greater than 50.0% of mass 95 79.5 175 5.0 - 9.0% of mass 174 5.6 (7.1)1 176 95.0 - 101.0% of mass 174 80.2 (100.9)1 177 5.0 - 9.0% of mass 176 5.2 (6.5)2 1 -Value is % mass 174 2 -Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: 01 02 03 04 05 EPA SAMPLE NO. LAB SAMPLE ID LAB FILE ID DATE ANALYZED TIME ANALYZED VSTD010 VSTDO10 AVA45321.D 03/20/06 23:09 VSTD020 VSTD020 AVA45322.D 03/20/06 23:41 VSTD050 VSTD050 AV145323.D 03/21/06 0:12 VSTD100 VSTD100 AVA45324.D 03/21/06 0:44 VSTD200 VSTD200 A1A45325.D 03/21/06 1:16 page 1 of 1 FORM V VOA OLM04.2 O O H I m/e SAMPLE ID 5A % RELATIVE ABUNDANCE 50 VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK - 40.0% of mass 95 18.4 75 BROMOFLUOROBENZENE (BFB) - 60.096 of mass 95 Lab Name: H2M LABS, INC. Contract: peak, 100 relative abundance Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Lab File ID: A\A45397.D BFB Injection Date: 03/23/06 Instrument ID: HP5971 BFB Injection Time: 9:36 GC Column: R-502.2 ID: .53 (mm) 5.0 - m/e SAMPLE ID ION ABUNDANCE CRITERIA % RELATIVE ABUNDANCE 50 15.0 - 40.0% of mass 95 18.4 75 30.0 - 60.096 of mass 95 43.0 95 Base peak, 100 relative abundance 100.0 96 5.0 - 9.096 of mass 95 6.4 173 Less than 2.0% of mass 174 0.2 (0.2)1 174 Greater than 50.0% of mass 95 81.0 175 5.0 - 9.0% of mass 174 5.9 (7.2)1 176 95.0 - 101.0% of mass 174 79.0 (97.4)1 177 5.0 - 9.0% of mass 176 5.0 (6.4)2 1 -Value is W mass 174 2 -Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: 01 0' 0" 05 0E 0( 0' OF 05 1( 13 12 13 14 18 16 17 18 19 20 EPALAB SAMPLE NO. SAMPLE ID LAB FILE ID DATE ANALYZED TIME TIME VSTD050 VSTD050 AW45398.D 03/23/06 10:01 VBLK032306 VBLK032306 XA45399.1) 03/23/06 10:34 LFB032306 LFB032306 AW45400.1) 03/23/06 11:05 MSB032306 MSB032306 AV445401.0 03/23/06 12:09 EQPT 0603561-001A AW45402.D 03/23/06 12:49 MW -1D 0603561-002A A1A45403.D 03/23/06 13:21 MW -1S 0603561-003A AW45404.D 03/23/06 13:53 MW -313 0603561-004A AW45405.D 03/23/06 14:24 MW -3S 0603561-005A AW45406.D 03/23/06 14:56 MWAD 0603561-006A A1A45407.D 03/23/06 15:27 MW -4S 0603561-007A A1A45408.D 03/23/06 15:58 MW -5D 0603561 -008A A1A45409.D 03/23/06 16:30 MW -5S 0603561-009A A1A45410.D 03/23/06 17:02 MW-5SMS 0603561-009AMS A%A45411.13 03/23/06 17:34 MW-5SMSD 0603561-009AMSD AW45412.D 03/23/06 18:05 MW -613 0603561-010A A1A45413.D 03/23/06 18:36 MW -6S 0603561-011A A1A45414.D 03/23/06 19:08 MW -81) 0603561-012A AW45415.D 03/23/06 19:39 MW -8S 0603561-013A AW45416.D 03/23/06 20:11 TRIP BLANK 3/16 0603561-014A A1A45417.D 03/23/06 20:42 page 1 of 1 Ln FORM V VOA OLM04.2 C) O T 8A VOLATILE INTERNAL STANDARD AREA AND RT SUMMARY Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Lab File ID (Standard): A\A45398.D EPA Sample No.(VSTD050##): VSTD050 Instrument ID: HP5971 GC Column: R-502.2 ID: .53 (mm) 01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 18 19 Contract: SAS No.: Date Analyzed: Time Analyzed: SDG No.: TSL005 03/23/06 10:01 Heated Purge: (Y/N) N IS1 PFB = Pentafluorobenzene IS2 DFB = 1,4-Difluorobenzene IS3 CBZ = Chlorobenzene-d5 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = -50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM04.2 Ln O O F-� IS1 PFB AREA # RT # IS2 DFB AREA # RT # IS3 CBZ AREA # RT # 12 HOUR STD 586456 9.33 1028946 10.31 551788 14.14 UPPER LIMIT 1172912 9.83 2057892 10.81 1103576 14.64 LOWER LIMIT 293228 8.83 514473 9.81 275894 13.64 EPA SAMPLE VBLK032306 616006 9.34 1034999 10.32 564278 14.14 LFB032306 620227 9.34 1064787 10.32 572951 14.15 MSB032306 638865 9.35 1059479 10.31 576874 14.15 EQPT 630610 9.34 1059523 10.32 575055 14.15 MWA D 638271 9.35 1086018 10.33 586682 14.15 MWAS 645982 9.35 1100158 10.33 590866 14.15 MW -313 631089 9.35 1083471 10.33 579204 14.15 MW -3S 640291 9.34 1090108 10.32 578999 14.15 MW -413 639154 9.35 1080396 10.32 582678 14.15 MW4S 634098 9.35 1087438 10.32 584770 14.15 MW -513 629222 9.34 1081801 10.32 577365 14.15 MW -5S 653198 9.34 1111797 10.32 588688 14.15 MW-5SMS 644938 9.34 1091270 10.31 580223 14.15 MW-5SMSD 639677 9.34 1078024 10.31 573033 14.15 MW -61) 630012 9.34 1089440 10.32 579784 14.15 MW -6S 643327 9.34 1091979 10.32 581914 14.14 MW -81) 634884 9.34 1098220 10.31 583096 14.14 MW -8S 641422 9.34 1093396 10.31 581086 14.14 TRIP BLANK 3/16 634962 9.34 1091964 10.32 579971 14.14 IS1 PFB = Pentafluorobenzene IS2 DFB = 1,4-Difluorobenzene IS3 CBZ = Chlorobenzene-d5 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = -50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. * Values outside of QC limits. page 1 of 1 FORM VIII VOA OLM04.2 Ln O O F-� H2M LABS, INC. Date: 27 -Mar -06 Test Code: 8260_W 360B METHOD DETECTION / Test Number: SW8260B REPORTING LIMITS Test Name: PART 360 BASELINE VOLATILES WATER Matrix: Aqueous Units: µg/L Updated: 19 -Oct -01 Type Analyte MDL PQL A 1,1,1,2 -Tetrachloroethane 0.30 5 A 1,1,1 -Trichloroethane 0.24 5 A 1,1,2,2 -Tetrachloroethane 0.93 5 A 1,1,2 -Trichloroethane 0.63 5 A 1,1-Dichloroethane 0.34 5 A 1,1-Dichloroethene 0.64 5 A 1,2,3-Trichloropropane 1.1 5 A 1,2-Dibromo-3-chloropropane 1.6 5 A 1,2-Dibromoethane 0.68 5 A I.2 -Dichlorobenzene 1.0 5 A 1,2-Dichloroethane 0.93 5 A 1,2-Dichloropropane 0.32 5 A 1,4 -Dichlorobenzene 0.67 5 A 2-Butanone 2.2 5 A 2-Hexanone 2.4 5 A 4-Methyl-2-pentanone 0.61 5 A Acetone 3.8 5 A Acrylonitrile 2.1 5 A Benzene 0.26 5 A Bromochloromethane 0.51 5 A Bromodichloromethane 0.37 5 A Bromoform 1.8 5 A Bromomethane 1.2 5 A Carbon disulfide 0.58 5 A Carbon tetrachloride 0.31 5 A Chlorobenzene 0.42 5 A Chloroethane 1.9 5 A Chloroform 0.34 5 A Chloromethane 0.87 5 A cis-1,2-Dichloroethene 0.29 5 A cis-1,3-Dichloropropene 0.29 5 A Dibromochloromethane 0.49 5 A Dibromomethane 0.64 5 A Ethylbenzene 0.41 5 A Iodomethane 0.47 5 A Methylene chloride 0.58 5 A Styrene 0.35 5 A Tetrachloroethene 0.70 5 A Toluene 0.43 5 A trans-1,2-Dichloroethene 0.55 5 A trans-1,3-Dichloropropene 0.51 5 A trans-1,4-Dichloro-2-butene 1.2 5 1 of 2 112M LABS, INC. Date: 27 -Mar -06 Test Code: 8260_W 360B METHOD DETECTION / Test Number: SW8260B REPORTING LIMITS Test Name: PART 360 BASELINE VOLATILES WATER Matrix: Aqueous Units: gg/L Updated: 19 -Oct -01 Type Analyte MDL PQL A Trichloroethene 0.48 5 A Trichlorofluoromethane 0.48 5 A Vinyl acetate 0.69 5 A Vinyl chloride 0.91 5 A Xylene (total) 0.35 5 I 1,4 -Dichlorobenzene -d4 - 5 I 1,4-Difluorobenzene - 5 I Chlorobenzene-d5 - 5 I Pentafluorobenzene - 5 S 1,2-Dichloroethane-d4 3.6 5 S 4-Bromofluorobenzene 1.2 5 S Toluene -d8 1.4 5 X 1,1-Dichloropropene 0.49 5 X 1,2-Dichloroethene (total) 1.5 5 X m,p-Xylene 1.0 5 X o -Xylene 0.42 5 2 of 2 M r—+ O O CA N U2M "PS, INC. II. SAMPLE DATA PACKAGE FOR VOLATILE ORGANICS A. REPORTS B. RAW DATA U2M "US, INC. QUALIFIERS FOR REPORTING ORGANICS DATA Value - If the result is a value greater than or equal to the quantification limit, report the value. U - Indicates compound was analyzed for but not detected. The sample quantitation limit must be corrected for dilution and for percent moisture. For example, IOU for phenol in water if the sample final volume is the protocol -specified final volume. If a 1 to 10 dilution of extract is necessary, the reported limit is 100 U. For a soil sample, the value must also be adjusted for percent moisture. For example, if the sample had 24% moisture and a 1 to 10 dilution factor, the sample quantitation limit for phenol (330 U) would be corrected to: (300 U) 100%moisture x df where D = D 100 and df - dilution factor For example, at 24% moisture, D = 100-24 = 0.76 100 (300 Ln x 10 - 4300 U rounded to the appropriate number of significant figures .76 For semivolatile soil samples, the extract must be concentrated to 0.5 mL, and the sensitivity of the analysis is not compromised by the cleanup procedures. Similarly, pesticide samples subjected to GPC are concentrated to 5.0 mL. Therefore, the CRQL values in Exhibit C will apply to all samples, regardless of cleanup. However, if a sample extract cannot be concentrated to the protocol -specified volume. (see _ Exhibit C), this fact must be accounted for in reporting the sample quantitation limit. J - Indicates an estimated value. This flag is used either when estimating a concentration for tentatively identified compounds where a 1:1 response is assumed or when the mass spectral data indicates the presence of a compound that meets the identification criteria but the result is less than the specified quantification limit but greater than zero. (e.g.: If limit of quantification is 10 ug/L and a concentration of 3 ug/L is calculated, report as 3J.) The sample quantitation limit must be adjusted for dilution as discussed for the U flag. N - Indicates presumptive evidence of a compound. This flag is only used for tentatively identified compounds, where the identification is based on a mass spectral library search. It is applied to all TIC results. For generic characterization of a TIC, such as chlorinated hydrocarbon, the N code is not used. P - This flag is used for a pesticide/Aroclor target analyte when there is greater than 25% difference for detected concentrations between the two GC columns (see Form X). The lower of the two values is reported of Form I with a "P". C - This flag applies to pesticide results when the identification has been confirmed by GC/MS.. If GC/MS confirmation was attempted but was unsuccessful, do not apply this flag, instead use a Laboratory defined flag, discussed below. B - This flag is used when the analyte is found in the associated blank as well as in the sample. It indicates possible probable blank contamination and warns the data user to take appropriate action. This flag must be used for a TIC as well as for a positively identified target compound. F2M "US, INC. E - This flag identified compounds whose concentrations exceed the calibration range of the GUMS instrument for that specific analysis. If one or more compounds have a response greater than full scale, except as noted in Exhibit D, the sample or extract must be diluted and re -analyzed according to the specifications in Exhibit D. All such compounds with a response greater than full scale should have the concentration flagged with an "E" on the Form I for the original analysis. If the dilution of the extract causes any compounds identified in the fust analysis to be below the calibration ranges in the second analysis, then the results of both analyses shall be reported on separate copies of Form I. The Form I for the diluted sample shall have the "DU suffix appended to the sample number. NOTE: For total xylenes, where three isomers are quantified as two peaks, the calibration range of each peak should be considered separately, e.g. a diluted analysis is not required for total xylenes unless the concentration of the peak representing the single isomer exceed 200 ug/L or the peak representing the two coeluting isomers on that GC column exceed 400 ug/L. Similarly, if the two 1,2-Dichloroethene isomers coelute, a diluted analysis is not required unless the concentration exceed 400 ug/L. D - This flag identifies all compounds identified in an analysis at a secondary dilution factor. If a sample or extract is re -analyzed at a higher dilution factor, as in the "E" flag above, the "DU suffix is appended to the sample number on the Form I for the diluted sample, and all concentration values reported on that Form I are flagged with the "D" flag. This flag alerts data users that any discrepancies between the concentrations reported may be due to dilution of the sample or extract. A - This flag indicates that a TIC is a suspected aldol -condensation product. X - Other specific flags may be required to properly define the results. If used, they must be fully described and such description attached to the Sample Data Summary Package and the SDG narrative. Begin by using "X". If more than one flag is required use "Y" and "Z" as needed. If more than five qualifiers are required for a sample result, used the "X" flag to combine several flags as needed. For instance, the "X" flag might combine "A", "B", and "D" flags for some samples. The laboratory defined flags limited to the letters "X", "Y" and "Z". The combination of flags "BU' or "LIB" is expressly prohibited. Blank contaminants are flagged "B" only when they are detected in the sample. U2M "US, INC. CODES FOR MANUAL CORRECTIONS T: Transcription error CE: Calculation error CC: Changed per client request SC: Sample cancelled LB: Wrong spot in logbook MP: Missed peak MIP: Misintegrated peak WI: Wrong isomer TI: Total of isomers lA BPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET EQPT Lab Name: H2M LABS, INC. Contract: U Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-OOIA Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45402.D Level: (low/mad) LOW Date Received: 03/16/06 % Moisture: not dec. Trichlorofluoromethane Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 lodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLMO4.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. Ethylbenzene GC Column: R-502.2 ID: .53 Soil Extract Volume: (uL CAS NO COMPOUND Contract: EPA SAMPLE NO. EQPT SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-001A Lab File ID: A\A45402.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: (ua/L or ua/Ka) UGIL o 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET EQPT TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW W Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICs found: CAS NUMBER 0 COMPOUND NAME FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-001A Lab File ID: A\A45402.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. 4 FORM I VOA -TIC OLM04.2 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45402.D Vial: 1 Acq On : 23 Mar 2006 12:49 Operator: tm Sample : 0603561-001A Inst H5971 Misc : TSL005,EQPT,H2O,SAMP„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:15 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 Resnonse via : Continuina Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Abundance Tic: A45402.D 1400000 1350000 1300000 e 4 01 5 N e 1250000 N m � o r 1200000 o r 4 v 1150000 a d 1100000 ' d a 1050000 0 1000000 S 0 d � 950000- 900000 0 `o 850000 800000 750000 700000 ti 650000 a 0 `o 600000- 550000. a v d 500000- 00000450000 450000- s .2 400000 9 350000- 50000300000250000200000150000 300000- 250000- 200000- 150000 100000 50000 0 ime—> 6. 0 8.b0. 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45402.D PUHW0320.M Mon Mar 27 09:28:34 2006 H5971 Page 2 File Operator Acquired Instrument Sample Name: Misc Info . Vial Number: Quant File : LSC Report - Integrated Chromatogram C:\HPCHEM\1\DATA\MAR06\032306A\A45402.D tm 23 Mar 2006 12:49 using AcgMethod PUHW0320 H5971 0603561-001A TSL005,EQPT,H20,SAMP „ 1 PUHW0320.RES (RTE Integrator) Abundance TIC: A45402.13 10000.00- 800000- 10.32 600000 9.34 400000 9.88 200000 L6.27 6.69 10.700 Time--> 4. 0 &&6- 516 6.b6 6.H 7. 0 716 i.b6 8. 0 6.66 9. 0 10.00 10.50 11.00 un anceTIC: A45402.U--- 1 19 14.15 17.39 1000000 15.73 800000- 6000W 400000 200000 0 13.9 14.38 15.40 15.99 16.34 17 0.17 17= Time--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance 1000000 800000 600000 400000 200000 0 21.49 25.3 20.20IM77 Ime-> 18.50 19.00 19.50 20.00 50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 Ag04UL.1) ruhwu.3Lu.M Mon Mar 27 09:35:58 2006 H5971 Quant Time: Mar 23 13:15 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHWO320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1).Pentafluorobenzene Quantitation Report (QT Reviewed) 168 Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45402.D Vial: 1 Acq On 23 Mar 2006 12:49 Operator: tm Sample : 0603561-DOIA Inst H5971 Misc TSL005,EQPT,H2O,SAMP„ Multiplr: 1.00 MS Integration Params: RTEINT.P 50.00 UG/L Quant Time: Mar 23 13:15 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHWO320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1).Pentafluorobenzene 65 9.34 168 630610 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1059523 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 575055 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 513551 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -dB Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 9.88 65 402632 48.05 UG/L 0.00 Range 76 - 114 Recovery = 96.10% 12.19 98 1302089 49.85 UG/L 0.00 Range 86 - 115 Recovery = 99.70% 15.73 95 553796 50.43 UG/L 0.00 Range 88 - 110 Recovery = 100.86% Qvalue ----------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45402.D PUHW0320.M Mon Mar 27 09:28:32 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary perator ID: tm Date Acquired: 23 Mar 2006 12:49 Mita File: C:\HPCHEM\1\DATA\MAR06\032306A\A45402.D ivame: 0603561-001A Misc: TSL005,EQPT,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45402.D PUHW0320.M Mon Mar 27 09:35:59 2006 H5971 IA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case -No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: BPA SAMPLE NO. MW -1D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-002A Lab File ID: A\A45403.D Date Received: 03/16/&6 Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (AL) Soil Aliquot Volume (AL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 _ _ Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 8 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 3 J 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. Contract: EPA SAMPLE NO. MW -1D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-002A Lab File ID: A\A45403.D Date Received: 03/16/06 Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or Ag/Kg) UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane .5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 N O O Cn F-4 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -1D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICs found: 0 CAS NUMBER COMPOUND NAME FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-002A Lab File ID: A\A45403.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or gg/Kg) UG/L RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45403.D Vial: 2 Acq On 23 Mar -2006 13:21 Operator: tm Sample 0603561-002A Inst : H5971 Misc : TSL005,MW-1D,H2O,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:48 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 ResiDonse via : Continnina ral Fila- r-\i4pr.T-TFM\l\nAmA\mARnF\n-i,)-4nrA\Aargan n Abundance TIC: A45403.D 1450000 1400000 1350000 Y 1300000 b N N C c 1250000 a u e � 1200000 1150000 N d a 1100000 o 1050000 `o E 1000000 ° _ R 950000 900000 $ o` 850000 _ 9 800000 750000 700000 650000 N a 0 600000 c' G N 550000 a e 500000 0 450000 r Y 4 400000 350000 300000 250000 200000 150000 o 100000 ai 0p d = 50000 a N 0 ime-> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45403.D PUHW0320.M Mon Mar 27 09:29:53 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45403.D Operator : tm Acquired : 23 Mar 2006 13:21 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-002A Misc Info : TSL005,MW-1D,H20,SAMP „ Vial Number: 2 Quant File :PUHW0320.RES (RTE Integrator) Abundance FIG: A45403.13 1200000 - 1000000. 800000 10.33 600000 9:34 400000 9.89 200000 0 6.72 8.66.85 10.99 ime-> 4. 0 5. 0 un anceTIC: A45403.0 1200000 1 .20 14.15 17.39 1000000 15.74 800000 600000 400000- 00000200000 200 000 0 12.0 13.16 13.9t 14.34.55 14.97 15.42 16.75.95 ime--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance 1200000- 1000000. 800000 600000 400000 200000 0 ime-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 tSY JY VJ.IJ rvnwU.3cu.M Mon Mar G/ Uy:jb:L.i GUUb HSy/1 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45403.D Vial: 2 Acq On : 23 Mar 2006 13:21 Operator: tm Sample : 0603561-002A Inst H5971 Misc : TSL005,MW-1D,H2O,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:48 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 638271 50.00 UG/L 0.02 35) 1,4-Difluorobenzene 10.33 114 1086018 50.00 UG/L 0.02 57) Chlorobenzene-d5 14.15 82 586682 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 525457 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 8) Acetone 16) 2-Butanone 9.89 65 415941 48.42 UG/L 0.02 Range 76 - 114 Recovery = 96.84% 12.20 98 1322477 49.40 UG/L 0.00 Range 86 - 115 Recovery = 98.80% 15.74 95 566384 50.32 UG/L 0.00 Range 88 - 110 Recovery = 100.64% Qvalue 6.72 43 9309 8.04 UG/L 98 8.85 43' 5828 2.66 UG/L 85 ------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45403.D PUHW0320.M Mon Mar 27 09:29:51 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary Derator ID: tm Date Acquired: 23 Mar 2006 13:21 ita File: C:\HPCHEM\1\DATA\MAR06\032306A\A45403.D name: 0603561-002A Misc: TSL005,MW-lD,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST96.L TIC Top Hit name -------------------- A45403.D PUHW0320.M RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------- Mon Mar 27 09:36:23 2006 H5971 Re f50 0 rrdz--> Abundance Raw5o 0 z—> Abundance c Sub 50 0 z-> Abundance se Re f50 0 z-.> Abundance Raw50 0 rnlz-.> Abundance c: Sub 50 0 z-> #8 Acetone Concen: 8.04 UG/L RT: 6.72 min Scan# 272 Delta R.T. 0.03 min Lab File: A45403.D Acq: 23 Mar 2006 13:21 Tgt Ion: 43 Resp: 9309 Ion Ratio Lower Upper 43 100 58 31.4 12.5 52.5 2000 1500 1000 500 0 #16 2-Butanone Concen: 2.66 UG/L RT: 8.85 min Scan# 488 Delta R.T. 0.03 min Lab File: A45403.D Acq: 23 Mar 2006 13:21 Tgt Ion: 43 Resp: 5828 Ion Ratio Lower Upper 43 100 72 16..6 3.8 43.8 un ance on o 2000 1500 1000 500 0 > ! A45403.D PUHW0320.M Mon Mar 27 09:29:54 2006 H5971 N M O O H Page 3 lA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. MW -13 Lab Name: H2M LABS, INC. Contract: U Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45404.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Trichlorofluoromethane Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (,UL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or gg/Kg)UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U _ 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 8 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 3 J 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6. Trichloroethene 5 U- 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -1S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45404.D Level: (low/med) LOW Date Received: 03/16/06 Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (ua/L or uer/icer) Tin/T. n 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane _ 5 U FORM I VOA - 2 OLM04.2 Z j FORM I VOA -TIC M O O OLM04.2 i/1 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -1S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45404.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (ML) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or gg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q Z j FORM I VOA -TIC M O O OLM04.2 i/1 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45404.D Vial: 3 Acq On 23 Mar 2006 13:53 Operator: tm Sample 0603561-003A Inst : H5971 Misc TSL005,MW-1S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:49 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via . Cnntiniiincr Cal Filo• f'•\trprTT�M\�\namT\rrrDnc\nom-,�nrT�Tn���o ., un ance - - ------ - " 1500000 1450000 1400000 1350000 4 1300000 C C rda N 'a 1250000 u Q o s s 1200000 1150000 1100000 iv d 'o 1050000 0 1000000 0 d � 950000 N d " 900000 o` 850000 4�4 �t 800000 750000 700000 m 650000 $ `o 600000 y 550000 a Z. 500000 C f 0 450000 s u Q 400000 350000 300000 250000 200000 150000 100000 ° Y a � a 50000 0 .'Ime--> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45404.D PUHW0320.M Mon Mar 27 09:30:12 2006 H5971 Page 2 r LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45404.D Operator : tm Acquired : 23 Mar 2006 13:53 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-003A Misc Info : TSL005,MW-lS,H20,SAMP „ Vial Number: 3 Quant File :PUHW0320.RES (RTE Integrator) un ance 1200000 1000000 800000 10.33 600000 9.35 400000 9.89 200000 D 6.71 8.84 10JR98 ime-> 4. D 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 8. 0 8. D 9. 0 9. 0 10.00 10.50 11.00 un ance 1200000 1220 14.15 17.39 1000000 15.74 800000 600000 400000 200000 D 17.79 18.2 12.0 13.14 13.9 14.si.54 14.97 15.L6.O 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 '1'5.5 17.50 18.00 un ance TIC: A45404. 1200000 1000000 800000 600000 400000 200000 0 ime--> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 -2i2.00 22.50 23.00 23.50 24.00 24.50 25.00 T A T A 11 A n MT7-f -n n ---- - �� Vluli Leat c. i Uy: JO: Z) 10 6UUto M kn O O H Quant Time: Mar 23 16:49 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Quantitation Report (QT Reviewed) 168 Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45404.D Vial: 3 Acq On 23 Mar 2006 13:53 Operator: tm Sample 0603561-003A Inst H5971 Misc TSL005,MW-1S,H2O,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P 50.00 UG/L Quant Time: Mar 23 16:49 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 645982 50.00 UG/L 0.02 35) 1,4-Difluorobenzene 10.33 114 1100158 50.00 UG/L 0.02 57) Chlorobenzene-d5 14.15 82 590866 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 521819 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 8) Acetone 16) 2-Butanone 9.89 65 416343 47.85 UG/L 0.02 Range 76 - 114 Recovery = 95.70% 12.20 98 1346019 49.63 UG/L 0.00 Range 86 - 115 Recovery = 99.26% 15.73 95 567635 49.78 UG/L 0.00 Range 88 - 110 Recovery = 99.56% Qvalue 6.71 43 9034 7.71 UG/L 97 8.85 43, 5935 2.67. UG/L 92 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45404.D PUHW0320.M Mon Mar 27 09:30:09 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary -operator ID: tm Date Acquired: 23 Mar 2006 13:53 ata File: C:\HPCHEM\1\DATA\MAR06\032306A\A45404.D 'game: 0603561-003A Misc: TSL005,MW-1S,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45404.D PUHW0320.M Mon Mar 27 09:36:56 2006 H5971 Re f5D 0 Raw5o 0 Sub 50 0 me ance 58 96 #8 Acetone Concen: 7.71 UG/L RT: 6.71 min Scan# 271 Delta R.T. 0.02 min Lab File: A45404.D Acq: 23 Mar 2006 13:53 207 o Tgt Ion: 43 Resp: 9034 Ion Ratio Lower Upper 43 100 58 34.2 12.5 52.5 Abundance onoAd 2000 Ion 57.95 (57.65 to 58.65: A45 6.71 1500 1000 500 0 Ime--> 6. 0 #16 2-Butanone Concen: 2.67 UG/L RT: 8.85 min Scan# 488 Delta R.T. 0.03 -min Lab File: A45404.D Acq: 23 Mar 2006 13:53 Tgt Ion: 43 Resp: 5935 Ion Ratio Lower Upper 43 100 72 19.8 3.8 43.8 un ance on 42.95 2.65to43-.G3T*-AA5d 1600 Ion 71.95 71.65 to 72.65: A45 1400 8.85 1200- 1000 800 600- 400- 200 00400zoo dam" 0 O O Page 3 Ref50 0 Raw5o 0 Sub 50 0 A45404.D PUHW0320.M Mon Mar 27 09:30:19 2006 H5971 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/M,) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µL) CAS NO COMPOUND EPA SAMPLE NO. MW -3D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-004A Lab File ID: A\A45405.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: I.— /. 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 74-83-9 Bromomethane 5 U 5U 75-00-3 Chloroethane 5 / U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 1,1-Dichloroethene Iodomethane 5 U 5 U *67-64-1 Vinyl acetate 5 U Acetone 5 U Carbon disulfide 5 U 75-09-2 Methylene chloride 5 156-60-5 trans-1,2-Dichloroethene U 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U nzene 5 U EHE2-Dichloroethane 5 U U78-87-5 ichloroethene 5 U -Dichloropropane 5 U romomethane 5 U 75-27-4 Bromodichloromethane 5 U cis-1,3-Dichloropropene 1 4-Methyl-2-pentanone 5 U 5 U Toluene trans-1,3-Dichloropropene 5 U Q127-10061-01-5 1,1,2 -Trichloroethane 5 U 18-4 Tetrachloroethene 5 U 5 U 2-Hexanone Dibromochloromethane 5 U 5 U 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -3D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) s WATER Lab Sample ID: 0603561-004A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45405..D Level: (low/mad) LOW Date Received: 03/16/06 % Moisture: not dec. Xylene (total) Date Analyzed: 03/23/06 GC Colum-: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U U 106-46-7 1,4 -Dichlorobenzene 5 95-50-1 1,2 -Dichlorobenzene _ U 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET E MW -3D TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICs found: 0 CAS NUMBER COMPOUND NAME M d' tn O O FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-004A Lab File ID: A\A45405.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (ML) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q M d' tn O O FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45405.D Vial: 4 Acq On : 23 Mar 2006 14:24 Operator: tm Sample 0603561-004A Inst : H5971 Misc TSL005,MW-3D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:49 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Resbonse via _ Cnntimiinrr rAl Pilo - un ance - - ---- - - •---- --- ---___ 1450000 1400000 1350000 1300000 a o 1250000 Ir t i? 4 1200000 1150000 d 1100000 d 1050000 0 0 1000000 0 950000 900000 e 0 `o 850000 ¢ 800000 750000 700000 650000 H g` 0 600000 c D 550000 y am. 500000 or 0 450000 r Y 400000 K 350000 300000 250000 200000- 150000 100000 3 50000 u a L14-06 0 Time-> 6. 0 8. 0 10.00 12.00 16.00 20 18.00 .00 22.00 24.00 A45405.D PUHW0320.M Mon Mar 27 09:31:44 2006 H5971 Page 2 WE Ls' LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45405.D Operator : tm Acquired : 23 Mar 2006 14:24 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-004A Misc Info : TSL005,MW-3D,H20,SAMP „ Vial Number: 4 Quant File :PUHW0320.RES (RTE Integrator) Abundance TIC: A45405.13 1200000- 1000000. 800000 10.32 600000 9.34 400000 9.89 200000 0 4.78 6.69 Time-> 4. 0 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 8. 0 8. 0 9. 0 9. 0 10.00 10.50 11.00 u-n-cTance TIC: A45405.13 1200000 1220 14.15 17.39 1000000 15.73 800000 600000 400000 200000 0 2.36 13.15 13.t114.38 15.41ime--> 11.50 1200 12.50 1300 1350 140 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance 1200000- 1000000. 800000 600000 400000 200000 0 Time-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 11�J'Y VJ.1J rUn vv U JGU.PQ lvlon mar L / U`J' : J / : U`.1- 2 U U b HSy /1 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45405.D Vial: 4 Acq On : 23 Mar 2006 14:24 Operator: tm Sample : 0603561-004A Inst : H5971 Misc : TSL005,MW-3D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:49 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398,D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 631089 50.00 UG/L 0.02 35) 1,47Difluorobenzene 10.33 114 1083471 50.00 UG/L 0.02 57) Chlorobenzene-d5 14.15 82 579204 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 525700 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds }- Acetone 9.88 65 412760 48.17 UG/L 0.00 Range 76 - 114 Recovery = 96.34% 12.20 98 1323449 49.55 UG/L 0.00 Range 86 - 115 Recovery = 99.10% 15.73 95 561203 49.97 UG/L 0.00 Range 88 - 110 Recovery = 99.94% . Qvalue 6.71 43 2136 1.87 UG/L 72 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45405.D PUHW0320.M Mon Mar 27 09:31:42 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary operator ID: tm Date Acquired: 23 Mar 2006 14:24 data File:. C:\HPCHEM\1\DATA\MAR06\032306A\A45405.D __,fame: 0603561-004A Misc: TSL005,MW-3D,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area. IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45405.D PUHW0320.M Mon Mar 27 09:37:10 2006 H5971 Re f50 0 Raw50 0 Sub 50 0 #8 Acetone Concen: 1.87 UG/L RT: 6.71 min Scan# 271 Delta R.T. 0.02 min Lab File: A45405.D Acq: 23 Mar 2006 14:24 Tgt Ion: 43 Resp: 2136 Ion Ratio Lower Upper 43 100 58 16.9 12.5 52.5 400 300 200 100 0 me-> A45405.D PUHW0320.M Mon Mar 27 09:31:46 2006 H5971 00 O O Page 3 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) ML Level: (low/mad) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (µL) CAS NO. COMPOUND EPA SAMPLE NO. MW -3S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-005A Lab File ID: A\A45406.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µ9/L or uq/Kq) UG/L 0 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: EPA SAMPLE NO. MW -3S Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-005A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45406.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Xylene (total) Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 _ Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -3S TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-005A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45406.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45406.D Vial: 5 Acq On 23 Mar 2006 14:56 Operator: tm Sample 0603561-005A Inst : H5971 Misc TSL005,MW-3S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:50 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D 1450000 1400000 1350000 1300000 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 650000 600000 550000 500000 450000 400000 350000 300000 250000 200000 150000 100000 50000 0 limn-� A45406.D PUHW0320.M Mon Mar 27 09:32:01 2006 H5971 N O O 1-� Page 2 LSC Report - Integrated Chromatogram l' File C:\HPCHEM\1\DATA\MAR06\032306A\A45406.D Operator : tm Acquired : 23 Mar 2006 14:56 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-005A Misc Info : TSL005,MW-3S,H20,SAMP „ Vial Number: 5 Quant File :PUHW0320.RES (RTE Integrator) un ance 1200000- 2000001000000800000 1000000- 800000- 10.32 600000 9.34 400000 9.89 200000 5.43 0 ime-> 4. 0 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 8.b6 8. 0 9. 0 .9. 0 10.00 10.50 11.00 Okbundance 1200000 1 20 14.15 17.39 1000000 15.74 800000 600000 400000- 2000W 2.35 13.93 15.40 0 Time-> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Okbundance 1200000 1000000 800000- 600000. 400000 200000 24.08 0 ime-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 A45406.D PUHWU32U.M Mon Mar G7 Uy:J/:ZJ ZUUb r1c7il Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45406.D Vial: 5 Acq On : 23 Mar 2006 14:56 Operator: tm Sample : 0603561-005A Inst H5971 Misc : TSL005,MW-3S,H20,SAMP,, Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:50 2006 Quant Results File.: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 640291 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1090108 50.00 UG/L 0.01 57) Chlorobenzene-d5 14.15 82 578999 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 529551 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -dB Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 9.89 65 412703 47.87 UG/L 0.01 Range 76 - 114 Recovery = 95.74% 12.20 98 1337796 49.78 UG/L 0.00 Range 86 - 115 Recovery = 99.56% 15.73 95 562433 49.78 UG/L 0.00 Range 88 - 110 Recovery = 99.56% Qvalue ------------------------------------------------------------------------- J (4) = qualifier out of range (m) = manual integration A45406.D PUHW0320.M Mon Mar 27 09:31:59 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary erator ID: tm Date Acquired: 23 Mar 2006 14:56 to File: C:\HPCHEM\1\DATA\MAR06\032306A\A45406.D same: 0603561-005A Misc: TSL005,MW-3S,H2O,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45406.D PUHW0320.M Mon Mar 27 09:37:23 2006 H5971 kn kn O O V) F-+ lA BPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -4D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-006A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45407.D Level: (low/mad) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (ua/L or ua/Ka) UG/L O 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 6 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 2 J 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 2 J 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 IB VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) ML Level: (low/mad) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (µL) CAS NO. COMPOUND EPA SAMPLE NO. MW -4D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-006A Lab File ID: A\A45407.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or uQ/Ra)UG/L 0 108-90-7 Chlorobenzene 1 J 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5, U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -4D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICs found: 0 CAS NUMBER COMPOUND NAME 00 O O FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-006A Lab File ID: A\A45407.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (AL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q 00 O O FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45407.D Vial: 6 Acq On 23 Mar 2006 15:27 Operator: tm Sample 0603561-006A Inst : H5971 Misc TSL005,MW-4D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:55 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D un ance TIC: A45407.13 1450000 1400000- 40000013500001300000 1350000- 1300000 d a N 1250000 o a t o 1200000 cud 150000 1150000- N 1100000. 1100000 d 'o 1050000 1000000 E ' R 950000 N e 900000 a Q ' 850000 800000 750000 700000 , d 650000 d 0 600000 550000 N ad 500000 450000 2. z 400000 r 350000 300000- 250000 d 200000 0 a 150000~ 2 C o u 100000 d o a 4 50000 a 0 - ^ A45407.D PUHW0320.M Mon Mar 27 09:32:18 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45407.D Operator : tm Acquired : 23 Mar 2006 15:27 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-006A Misc Info : TSL005,MW-4D,H2O,SAMP,, Vial Number: 6 Quant File :PUHW0320.RES (RTE Integrator) 20 000- 1 I IC: A45407.13 -100000080000010.32 1000000- 800000- 10.32 600000 9.34 400000 9.89 200000- 5.81 5.81 6.25 6.71 7.337.57 8.18 8.54 8.89 9. 3 11.01 Ime-> 4. 0 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 8. 0 8.50 9.00 9. 0 10.00 10.50 11.00 undance TIC: A45407.13 1200000 1 20 14.15 17.39 1000000 15.74 800000 600000 400000 200000 0 13.14 13.9 14.39 14.97 15.40 16.33 16:1/.12 18.2 Time ->aa 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 1200000e 1000000 800000 600000- 400000 200000 0 Ime-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 A r n «z z L V1IVYVJGV .11 Lluii r1aL. Z/ UJ:j 1 :.3z) Luub HSy /1 O O O C/1 Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45407.D Vial: 6 Acq On 23 Mar 2006 15:27 Operator: tm Sample 0603561-006A Inst : H5971 Misc TSL005,MW-4D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:55 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 639154 50.00 UG/L 0.01 35) 1,4-Difluorobenzene 10.32 114 1080396 50.00 UG/L 0.01 57) Chlorobenzene-d5 14.15 82 582678 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 525684 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 408518 47.81 UG/L 0.01 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.62% 55) Toluene -d8 12.20 98 1325902 49.78 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 99.56% 56) 4-Bromofluorobenzene 15.74 95 565316 50.48 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.96% 'Target Compounds Qvalue 8) Acetone 6.71 43 6425 5.54 UG/L 96 16) 2-Butanone 8.84 43 4852 2.21 UG/ -L 85 43) 1,2-Dichloropropane 11.01 63 12463 1.53 UG/L #. 94 58) Chlorobenzene 14.20 112 21555 1.04 UG/L # 81 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45407.D PUHW0320.M Mon Mar 27 09:32:16 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary _nnerator ID: tm Date Acquired: 23 Mar 2006 15:27 ita File: C:\HPCHEM\1\DATA\MAR06\032306A\A45407.D _ffLme: 0603561-006A Misc: TSL005,MW-4D,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45407.p. PUHW0320.M Mon Mar 27 09:37:36 2006 H5971 N NO kn O O Cn E-+ ounaance Re f50 0 n-dz--> un ance Raw5o 0 Tllz—> Abundance Sub 5o 0 Re f50 0 Raw5o 0 Sub 50 0 #8 Acetone Concen: 5.54 UG/L RT: 6.71 min Scan# 271 Delta R.T. 0.01 min Lab File: A45407.D Acq: 23 Mar 2006 15:27 Tgt Ion: 43 Resp: 6425 Ion Ratio Lower Upper 43 100 58 30.2 12.5 52.5 1200 Ion 57.95 (57.65 to 5 6.71 1000- 800- 600. 000800600 400 200 0- #16 2-Butanone Concen: 2.21 UG/L RT: 8.84 min Scan# 487 Delta R.T. 0.01 min Lab File: A45407.D Acq: 23 Mar 2006 15:27 Tgt Ion: 43 Resp: 4852 Ion Ratio Lower Upper 43 100 72 16.2 3.8 43.8 1400 1200 1000 800 600 400 200 0 A45407.D PUHW0320.M Mon Mar 27 09:32:19 2006 H5971 M O O H Page 3 un ance r Re f50 0 rrdz-> Abundance Ra w50 0 nilz-> Abundance c Sub 50 0 z--> Abundance sce Ref50 0 z_> Abundance c Rawso 0 z-> un ance ------- zcai Sub 50 0 z-> A45407.D PUHW0320.M #43 1,2-Dichloropropane Concen: 1.53 UG/L RT: 11.01 min Scan# 708 Delta R.T. 0.01 min Lab File: A45407.D Acq: 23 Mar 2006 15:27 Tgt Ion: 63 Resp: 12463 Ion Ratio Lower Upper 63 100 112 1.8 0.0 23.8 41 54.8 0.0 20.0# un ance Ion o 63.70): A454 5000 Ion 112.00 (111.70 to 112.70): A lon 41.00 (40.70 to 41.70): A45 4000 11.01 3000 2000- 10W 0. Af, me-> 10.90 11.00 .11.10 #58 Chlorobenzene Concen: 1.04 UG/L RT: 14.20 min Scan# 1031 Delta R.T. 0.00 min Lab File: A45407.D Acq: 23 Mar 2006 15:27 Tgt Ion:112 Resp: 21555 Ion Ratio Lower Upper 112 100 77 91.9 49.9 89.9# 114 30.1 10.9 50.9 un ance Ion112o Ion 77.00 (V6' 71b 670 to 77.70): A45 10000 Ion 114.00 (113.70 to 114.70): A 5000 14.20 6000 4000 2000 0 me-> 14.10 14.20 14.30 Mon Mar 27 09:32:20 2006 H5971 d - O O CA H Page 4 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. Contract: BPA SAMPLE NO. MW -4S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-007A Lab File ID: A\A45408.D Date Received: 03/16/06 Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (AL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or Ag/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 2 J 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 2 J 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) ML Level: (low/med) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (AL) CAS NO. COMPOUND EPA SAMPLE NO. MW -4S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-007A Lab File ID: A\A45408.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: (ua/L or ua/Ka) UG/L O 108-90-7 Chlorobenzene 1 J 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -4S TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICs found: 0 CAS NUMBER I COMPOUND NAME FORM I VOA -TIC OLM04.2 l Lab Sample ID: 0603561-007A Lab File ID: A\A45408.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q FORM I VOA -TIC OLM04.2 l Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45408.D Vial: 7 Acq On : 23 Mar 2006 15:59 Operator: tm Sample : 0603561-007A Inst : H5971 Misc : TSL005,MW-4S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:54 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D 1450000 1400000 1350000 1300000 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 700000 850000 600000 550000 500000 450000 400000 350000 300000 250000 200000 150000 100000 50000 0 A45408.D PUHW0320.M Mon Mar 27 09:32:42 2006 H5971 00 O O Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45408.D Operator : tm Acquired : 23 Mar 2006 15:59 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-007A Misc Info : TSL005,MW-4S,H20,SAMP „ Vial Number: 7 Quant File :PUHW0320.RES (RTE Integrator) Abundance 1200000 1000000 800000 10.32 600000 9.34 400000 9.89 200000 0 6.25 6.72 7.57 8.18 8.56 8.89 9. 4 11.02 16 6.b6 6. 0 7. 0 7. 0 i.b6 8. 0 ;.bo 9. 0 10.00 10.50 11.00 Abundance 1200000 1 20 14.15 17.39 1000000 15.73 800000 600000 400000 200000 0 L2.36 13.14 13.9 14.37 14.97 15.41 16.33 16.0&11 L_� Time--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance I JG: A45408.13 1200000- 2000001000000800000 1000000- 800000. 600000 400000 200000 01, 18.66 Ime--> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.06 23.50 24.00 24.50 25.00 li43YUU.L eurinuizU.M Mon Mar z/ Uy:3-/:4b 2UUb Hb9/i Quant Time: Mar 23 16:54 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene Quantitation Report (QT Reviewed) 634098 • Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45408.D Vial: 7 Acq On : 23 Mar 2006 15:59 Operator: tm Sample : 0603561-007A. Inst H5971 - Misc : TSL005,MW-4S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P 70) 1,4 -Dichlorobenzene -d4 17.39 Quant Time: Mar 23 16:54 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 634098 • 50.00 UG/L 0.01 35) 1,4-Difluorobenzene 10.32 114 1087438 50..00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 584770 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 523660 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9:89 65 410005 47.67 UG/L 0.01 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.34% 55) Toluene -d8 12.20 98 1324184 49.40 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = .98.80% 56) 4-Bromofluorobenzene 15.73 95 564687 50.10 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.20% Target Compounds Qvalue 8) Acetone 6.71 43 6311 5.49 UG/L 99 16) 2-Butanone 8.85 43 4986 2.29 UG/L 89 43) 1,2-Dichloropropane 11.02 63 13376 1.63 UG/L # 95 58) Chlorobenzene 14.19 112 22575 1.08 UG/L # 80 ------------------------------------------------------------------------- - (#) = qualifier out of range (m) = manual integration A45408.D PUHW0320.M Mon Mar 27 09:32:40 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary erator ID: tm Date Acquired: 23 Mar 2006 15:59 to File: C:\HPCHEM\1\DATA\MAR06\032306A\A45408.D -ame: 0603561-007A Misc: TSL005,MW-4S,H2O,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top ---------------------------------------------------------------------------- Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc A45408.D PUHW0320.M Mon Mar 27 09:37:48 2006 H5971 Re f50 0 Raw50 0 Sub 50 0 Re f50 0 m ance 58 75 1 Raw5O 0 Sub 50 0 1400 1200 1000 800 600 400 200 0 A45408.D PUHW0320.M Mon Mar 27 09:32:43 2006 H5971 N O O H Page 3 #8 Acetone Concen: 5.49 UG/L RT: 6.71 min Scan# 271 Delta R.T. 0.01 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 207 Tgt Ion: 43 Resp: 6311 Ion Ratio Lower Upper 43 100 58 31.9 12.5 52.5 Okbundance Ion 42.95 42.65 to Ion 57.95 57.65 to 58.65 :A4 2107 1200 6.71 1000 800 O 600- AA 400 200 o. A 6. 0 -J 6. 0 6. 0 6.90 0 Ime--> #16 2-Butanone Concen: 2.29 UG/L RT: 8.85 min Scan# 488 Delta R.T. 0.02 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 o Tgt Ion: 43 Ion Ratio Resp: 4986 Lower Upper 43 100 72 18.6 3.8 43.8 1400 1200 1000 800 600 400 200 0 A45408.D PUHW0320.M Mon Mar 27 09:32:43 2006 H5971 N O O H Page 3 Re f5o 0 Ra W50 0 Sub50 41 0 Re f5o 0 Raw5o 0 Sub 0 0 76 49 97 112 can #43 1,2-Dichloropropane Concen: 1.63 UG/L RT: 11.02 min Scan# 708 Delta R.T. 0.01 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 Tgt Ion: 63 Resp: 13376 Ion Ratio Lower Upper 63 100 112 2.3 0.0 23.8 41 51.9 0.0 20.0# bundance Ion o 53.7 6000 Ion 112.00 (111.70 to 112.70): A Ion 41.00 (40.70 to 41.70): A45 5000 11.02 4000 3000 2000 1000 0 ime-> 10.90 11.00 11.10 11.20 #58 Chlorobenzene Concen: 1.08 UG/L RT: 14.19 min Scan# 1030 Delta R.T. -0.00 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 Tgt Ion:112 Resp: 22575 Ion Ratio Lower Upper 112 100 77 92.6 49.9 89.94f 114 32.9 10.9 50.9 un ance on o Ion 77.00 (76.70 to 77.70): A45 Ion 114.00 (113.70 to 114.70): A 10000 14.19 8000 6000 4000 2000 0 ime--> 14.10 14.20 14.30 A45408.D PUHW0320.M Mon Mar 27 09:32:44 2006 H5971 M O O H Page 4 76 41 49 I I 83 97 112 Sub50 41 0 Re f5o 0 Raw5o 0 Sub 0 0 76 49 97 112 can #43 1,2-Dichloropropane Concen: 1.63 UG/L RT: 11.02 min Scan# 708 Delta R.T. 0.01 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 Tgt Ion: 63 Resp: 13376 Ion Ratio Lower Upper 63 100 112 2.3 0.0 23.8 41 51.9 0.0 20.0# bundance Ion o 53.7 6000 Ion 112.00 (111.70 to 112.70): A Ion 41.00 (40.70 to 41.70): A45 5000 11.02 4000 3000 2000 1000 0 ime-> 10.90 11.00 11.10 11.20 #58 Chlorobenzene Concen: 1.08 UG/L RT: 14.19 min Scan# 1030 Delta R.T. -0.00 min Lab File: A45408.D Acq: 23 Mar 2006 15:59 Tgt Ion:112 Resp: 22575 Ion Ratio Lower Upper 112 100 77 92.6 49.9 89.94f 114 32.9 10.9 50.9 un ance on o Ion 77.00 (76.70 to 77.70): A45 Ion 114.00 (113.70 to 114.70): A 10000 14.19 8000 6000 4000 2000 0 ime--> 14.10 14.20 14.30 A45408.D PUHW0320.M Mon Mar 27 09:32:44 2006 H5971 M O O H Page 4 lA BPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -5D Lab Name: H2M LABS, INC. Contract: U Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-008A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45409.D Level: (low/mad) LOW Date Received: 03/16/06 % Moisture: not dec. Trichlorofluoromethane Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (AL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or u4/KQ) UG/L O 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 2 J 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 3 J 156-59-2 cis-1,2-Dichloroethene 3 J 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 1 J 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-l,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 1 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Ethylbenzene GC Column: R-502.2 ID: .53 Soil Extract Volume: (u CAS NO. COMPOUND Contract: (mm L) EPA SAMPLE NO. MW -5D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-008A Lab File ID: A\A45409.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (yL) CONCENTRATION UNITS: (µ9/L or µg/Rg) UG/L O 108-90-7 Chlorobenzene 3 J 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 H r C) 0 CN z'vowgO OII-VOA I WHOA VEM f OL 5Z'9 urnoumun ' T :SIINA NOIIVHINSONOO 0 ' ONOO' ISH Ili 3wKN GMOdw0O 2ISew[1N SKO VEM (bx/brl ao Z/bif) T :puno3 sOII aequinN :SIINA NOIIVHINSONOO ('Irf) 0 :awnTOA gonb?iK IToS:awnioA qOp3qxg i?oS 00'T :zojOe3 uo?gni?Q (wul) £S' :QI Z'ZOS-2i :uwnio0 OO 90/EZ/EO :PazATpuK aqua -Dap qou :eanis?ow % 90/9T/£0 :pan?aOag GIva b10'I (Paw/Moi) :ianaZ Q'60bSW\K :QI aTTa qpI iw (rim/5) y :TOA/qM aidwpS K800 -19S£090 :QI aidwpS qvq gHIKM (aGIPM/T?os) :x?.zgpw 90o'ISZ ON SCIS :,ON SKS 'TSIOd :'oN asvo 8Lb0T :apoo qvq :gDvajUOO 'DNI 'Sava WZH :awpN qpI SaMOdwOO =aIIN3QI )MAIIKINSI 1 QS -Mw IHSHS VJVCI SIS2IVNK SOINVE)HO S'IIIK'IOA 'ON S'IdKVS Kd3 3T Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45409.D Vial: 8 Acq On 23 Mar 2006 16:30 Operator: tm Sample 0603561-008A Inst H5971 Misc TSL005,MW-5D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:57 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuina Cal Fi_]Pe n Abundance TIC: A454US.D 1450000 1400000 1350000- 1300000 m "e 1250000 N d a C 2 `0 1200000 2 t u u 1150000 d 1100000 N 5 0 1050000 S 0 1000000 c 950000 a 900000 850000 o` 800000 750000 700000 d V 650000 d 0 600000 o C N 550000 a e 500000 0 450000 t 400000 n 350000 300000 250000 �- � 5a d ` F 0 200000 �" o c u o 150000 u o o N c K 100000 50000 01 - gime. 6.60 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45409.D PUHW0320.M Mon Mar 27 09:32:59 2006 H5971 Page 2 1� r Ln O O t4 File Operator Acquired Instrument Sample Name Misc Info Vial Number Quant File LSC Report -'Integrated Chromatogram : C:\HPCHEM\1\DATA\MAR06\032306A\A45409.D tm : 23 Mar 2006 16:30 using AcgMethod PUHW0320 H5971 : 0603561-008A : TSL005,MW-5D,H20,SAMP „ 8 :PUHW0320.RES (RTE Integrator) Abundance Tic: A45409.D 1600000 1400000 1200000 1000000 800000 10.32 600000 9.34 400000 9.89 200000 5.82 6.25 6.69 7.337.57 8.18 8.54 8.89 9. 3 11.02 0 Time-> 4. 0 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 6.66 8.50 9.00 9. 0 10.00 10.50 11.00 un ance VIC: A454091) 1600000 1400000 12.20 1200000 14.15 17.39 1000000 15.73 800000- 00000600000400000 600000- 400000 200000- 0 11.80 12.42.67 13.9 14.37 15.40 1613244 167!3112 11 .49 18.01 Time-> 11.50 12100 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance TIC: A4540.9- 1600000- 1400000 1200000 1000000 800000 600000 400000 200000 018.50 rime-> 19.00 19.50 20.00 20.50 21.00 21.50 22.00 _h'.5023.00 23.50 24.00 24.50 25.00 []Y JIY U7.L runnuo4u Ll mon roar G/ Uy:Jd:lU LUUb Hb /1 00 O O DO H Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45409.D Vial: 8 Acq On : 23 Mar 2006 16:30 Operator: tm Sample : 0603561-008A Inst H5971 Misc TSL005,MW-5D,H20,SAMP„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 16:57 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 629222 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1081801 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 577365 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 517673 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 407688 47.65 UG/L 0.02 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.300 55) Toluene -d8 12.20 98 1329835 49.86 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 99.72% 56) 4-Bromofluorobenzene 15.73 95 559107 49.86 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.72% Target Compounds Qvalue 5) Vinyl chloride 4.78 62 7006 1.82 UG/L 95 26) 1,1-Dichloroethane 8.18 63 40965 3.15 UG/L 97 30) cis-1,2-Dichloroethene 8.90 96 16884 2.52 UG/L # 80 40) 1,2-Dichloroethane 9.98 62 10608 1.22 UG/L 99 43) 1;2-Dichloropropane 11.02 63 40422 4.95 UG/L # 98 58) Chlorobenzene 14.19 112 69095 3.36 UG/L 95 A---------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45409.D PUHW0320.M Mon Mar 27 09:32:57 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary -^_,aerator ID: tm Date Acquired: 23 Mar 2006 16:30 1ta File: C:\HPCHEM\1\DATA\MAR06\032306A\A45409.D _:6me: 0603561-008A Misc: TSL005,MW-5D,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- Ethyl ether 6.25 9.6 UG/L 335412 ISTD01 9.34 1744910 50.0 A45409.D PUHW0320.M Mon Mar 27 09:38:11 2006 ' H5971 O 00 O O H ance Re f50 0 Ra W50 0 Sub 50 0 Re f5o 0 Ra W50 0 Sub 50 0 44 85 98 1 #5 Vinyl chloride Concen: 1.82 UG/L RT: 4.78 min Scan# 75 Delta R.T. 0.04 min Lab File: A45409.D Acq: 23 Mar 2006 16:30 Tgt Ion: 62 Resp: 7006 Ion Ratio Lower Upper 62 100 64 28.1 10.6 50.6 bundance Ion 62.00 161.70 to 62.70): A454 1000 14.10 800 600- 400. 200 0 ime-> 4.04.04.04.05.0 #26 1,1-Dichloroethane Concen: 3.15 UG/L RT: 8.18 min Scan# 420 Delta R.T. 0.01 min Lab File: A45409.D Acq: 23 Mar 2006 16:30 Tgt Ion: 63 Resp: 40965 Ion Ratio Lower Upper 63 100 65 29.8 11.4 51.4 83 8.6 0.0 30.4 un ance on 63.00 6Z.70tO63.70):A4W Ion 65.00 64.70 to 65.70 : A45 12000 Ion 83.00 182.70 to 83.70 : A45 Y07 10000 8.18 0 8000 6000 4000 2000 0 A45409.D PUHW0320.M Mon Mar 27 09:33:00 2006 H5971 -1 00 V) O O H Page 3 Re f50 0 z-> un anc Ra W50 0 z--> un ano Sub so 0 Re f50 0 Raw5o 0 Sub 50 0 A45409.D PUHW0320.M #30 cis-1,2-Dichloroethene Concen: 2.52 UG/L RT: 8.90 min Scan# 493 Delta R.T. 0.02 min Lab File: A45409.D Acq: 23 Mar 2006 16:30 Tgt Ion: 96 Resp: 16884 Ion Ratio Lower Upper 96 100 61 142.9 158.0 198.0# 98' 61.4 45.3 85.3 un ance on96.00 95.70 o 95.70 A45A Ion 61.00 60.70 to 61.70: A45 8000 Ion 98.00 197.70 to 98.70: A45 6000- 8. 0 4000 2000 0 ime--> #40 1,2-Dichloroethane Concen: 1.22 UG/L RT: 9.98 min Scan# 603 Delta R.T. 0.01 min Lab File: A45409.D Acq: 23 Mar 2006 16:30 Tgt Ion: 62 Resp: 10608 Ion Ratio Lower Upper 62 100 98 7.8 0.0 28.2 64 33.3 12.8 52.8 un ance ono Ion 98.00 197.70 to 98.70: A45 4000 Ion 64.00 63.70 to 64.70: A45 9.98 3000- 20001 000 2000 1000 _ 0 Mon Mar 27 09:33:01 2006 H5971 10: N 00 V) O O H Page 4 Re f50 0 Ra W50 0 76 41 111] 49 1�_�� . �111 63 97 112 3 4 5 6 7 8 9 1 0 1 0 i 6, Re f50 0 Raw5o 0 Sub 50 0 76 49 97 112 #43 1,2-Dichloropropane Concen: 4.95 UG/L RT: 11.02 min Scan# 708 Delta R.T. 0.02 min Lab File: A45409.D Acq: 23 Mar 2006 16:30 Tgt Ion: 63 Resp: 40422 Ion Ratio Lower Upper 63 100 112 3.2 0.0 23.8 41 47.3 0.0 20.0# bundance Ion o 53.70): A451 Ion 112.00 (111.70 to 112.70): A Ion 41.00 (40.70 to 41.70): A45 15000- 11.02 10000- 5000- 0 00005000D ...L Ime--> 10.90 11.00 11.10 11.20 #58 Chlorobenzene Concen: 3.36 UG/L RT: 14.19 min Scan# 1030 Delta R.T. -0.00 min Lab File: A45409.D Acq: 23 Mar. 2006 16:30 Tgt Ion:112 Resp: 69095 Ion Ratio Lower Upper 112 100 77 64.5 49.9 89.9 114 30.4 10.9 50.9 bundance ono Ion 77.00 ( 6.70 to 77.70): A45 Ion 114.00 (113.70 to 114.70): A 30000- 25000- 14.19 20000 15000 10000 5000 0 [me--> 14.10 14.20 14.30 A45409.D PUHW0320.M Mon Mar 27 09:33:01 2006 H5971 M DD O O N Page 5 Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45409.D Vial: 8 Acq On 23 Mar 2006 16:30 Operator: tm Sample 0603561-008A Inst : H5971 _ Misc TSL005,MW-5D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Library : C:\DATABASE\NIST98.L Peak Number 1 Ethyl ether Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 6.25 9.61 UG/L 335412 Pentafluorobenzene 9.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual -----------------------------------------------------------7--------- 1 Ethyl ether 74 C4H100 000060-29-7 90 2 Ethene, ethyloxy- 74 C4H100 1000221-95-9 90 3 Ethane, 1,2-diethoxy- 118 C6H1402 000629-14-1 64 4 Hydrazine, trimethvl- 74 C3H10N2 001741-01-1 47 Abundance scan 9.13 m/z 5905 100.00% 8000 59 45 6000 74 4000-. 2000 6. 0 6. 0 6.40 d.ho' 39 m/z 45.1 77.54% z-> 10 2 30 4 50 6 0 80 9 1 0 ''J46 1 0 Abundance ether 3 8000 6000 59 6.0 6. 0 6.40 6. 0 4000-:45 74 m/z 74.10 61.28% 2000 15 n-dz-> 10 26 30 40 50 6 70 8 9 1 0 1 0 1 0. L un ance3 ene, a oxy- 8000 59 6000 45- 74 6.bb6. 0 6.40 6. 0 m/z 43.15 20.22% 4000 2000 nilz-> 10 2 30 4 50 6 0 80 9 J66 AW 1 0 Abundance ane, a oxy- 3 59 6. 0 6. 0 s.40 6. 0 8000-1m/z 41.10 13.81% 6000 4000 45 74 2000 84 118 z-> 10 2 30 0"I 6 8 9 J66 ''JJ6 'Ah' 6. 0 6. 0 6.40 "6.60.' A45409.D PUHW0320.M Mon Mar 27 09:38:11 2006 H5971 Page 1 d' 00 O O H IA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) ML Level: (low/med) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (AL) CAS NO. COMPOUND EPA SAMPLE NO. MW -5S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-009A Lab File ID: A\A45410.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (ua/L or tza/Kal TT(:/T. n 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-5972 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,J-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 tran3-1,3-Dichloropropene 5 U 79-00-5, 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 V) 00 O O F-+ 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (9/m,) ML Level: (low/mad) LOW % Moisture: not dec. Ethylbenzene GC Column: R-502.2 ID: .53 Soil Extract volume: (UL CAS NO. COMPOUND Contract: (mm 1 EPA SAMPLE NO. MW -5S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-009A Lab File ID: A\A45410.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: (ua/L or ua/Ka) IIO/L n 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 00 O O V1 E'-4 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -5S j TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (Al) Number TICs found: 0 CAS NUMBER COMPOUND NAME FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-009A Lab File ID: A\A45410.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45410.D Vial: 9 Acq On 23 Mar 2006 17:02 Operator: tm Sample 0603561-009A Inst H5971 Misc TSL005,MW-5S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 24 11:49 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D ounaance TIC: A4541 0.13 1450000 1400000- 4000001350000 1350000- 1300000 1300000 N d 1250000 a `o ° = 1200000 r 1150000 N d d 1100000 a 0 1050000 ° o ' 1000000 ° e 950000 5 900000 0 0 850000 4 800000 750000 700000 d 650000 c `o 600000 d N 550000 ° 500000 0 450000 ° r 400000 u 4 350000 300000 250000 200000 150000 100000 50000 0 ime -> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45410.D PUHW0320.M Mon Mar 27 09:33:21 2006 H5971 Page 2 00 00 O O 1� H LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45410.D Operator : tm Acquired : 23 Mar 2006 17:02 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-009A Misc Info : TSL005,MW-5S,H20,SAMP „ Vial Number: 9 Quant File :PUHW0320.RES (RTE Integrator) un ance TIC: A45410.1) 1200000 1000000 800000 10.31 600000 9.34 400000 9.89 200000- 0 7.59 ime-> 4. 0 5. 0 5. 6 6. 0 6. 0 7. 0 7. 0 8. 0 8. 09. 0 9. 0 10.00 10.50 11.00 bundance 1200000 1220 14.15 . 17.39 1000000 15.73 800000 600000 J13.97 400000 200000 0 15.40 Time--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance 1200000 1000000 800000 600000 400000 200000 0 ime--> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 Il it g A 1 h n nrTiTr.Tn 7 -"- -- --"••�-�-�-� ••� +'+Uu rlcat 41 U7: JO:LJ L000 ri5y /1 00 O O H Quant Time: Mar 24 11:49 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Quantitation Report (QT Reviewed) 168 Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45410.D Vial: 9 Acq On : 23 Mar 2006 17:02 Operator: tm Sample : 0603561-009A Inst H5971 Misc : TSL005,MW-5S,H2O,SAMP„ Multiplr: 1.00 MS Integration Params: RTEINT.P 50.00 UG/L Quant Time: Mar 24 11:49 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 653198 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1111797 50.00 UG/L 0.01 57) Chlorobenzene-d5 14.15 82. 588688 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 531455 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 `,Target Compounds 9.89 65 413510 47.02 UG/L 0.01 Range 76 - 114 Recovery = 94.04% 12.20 98 1356411 49.49 UG/L 0.00 Range 86 - 115 Recovery = 98.98% 15.73 95 569276 49.40 UG/L 0.00 Range 88 - 110 Recovery = 98.80% Qvalue ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45410.D PUHW0320.M Mon Mar 27 09:33:18 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary operator ID: tm Date Acquired: 23 Mar 2006 17:02 ,ata File: C:\HPCHEM\1\DATA\MAR06\032306A\A45410.D -";ame: 0603561-009A Misc: TSL005,MW-5S,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45410.D PUHW0320.M Mon Mar 27 09:38:23 2006 H5971 i lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -6D Lab Name: H2M LABS, INC. Contract: U Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-010A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45413.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Trichlorofluoromethane Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (AL) Soil Aliquot Volume (AL) CONCENTRATION UNITS: CAS NO. COMPOUND 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 75-15-0 Carbon disulfide 5 U •75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichlorcethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 ib Dromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 N Cil O O C/1 F-+ 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -6D Lab Name: H2M LABS, INC. Contract: U Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-OIOA Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45413.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Styrene Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (gL) CONCENTRATION UNITS: CAS NO. COMPOUND 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U ' 96-12-8 1 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW-6D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (gl) Number TICS found: 0 CAS NUMBER COMPOUND NAME FORM I VOA -TIC OLM04.2 Lab Sample ID: 0603561-010A Lab File ID: A\A45413.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45413.D Vial: 12 Acq On 23 Mar 2006 18:36 Operator: tm Sample 0603561-010A Inst H5971 Misc TSL005,MW-6D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:07 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 ResAonse via _ Cnntinii'inri (:al Fila- r-\upruFNt\l\nnma\mAtDnc\n�,)incr\rnr:Ioo n 1400000 1350000 - 4 1300000 d 4 c N a ' 1250000 m o 1200000 .a o c U � 1150000 N 1100000 a 0 `o 1050000 0 1000000 ai a 950000 900000 a `o 850000 4 800000 750000 700000 N 650000 a 0 `o 600000 c' e 550000 a 500000 % 450000.s 400000 4 350000 300000 250000 200000 150000 u 100000 s` 50000 u Q 0 iflm( 6. 0 8. 0 10.00 12.00 14.00 1600 18.00 20.00 22.00 2400 A45413.D PUHW0320.M Mon Mar 27 09:34:13 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45413.D Operator : tm Acquired : 23 Mar 2006 18:36 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-010A Misc Info : TSL005,MW-6DfH2O,SAMPf, Vial Number: 12 Quant File :PUHW0320.RES (RTE Integrator) �eTic: A45413.L) 1000000 800000 10.32 600000 9.34 400000 9.88 200000 5.34 6.710 04/162 Ime--> 4. 0 5. 5. 6. 6. 0 7. 0 7. 0 . 8. 9. 0 9. 0 10.00 10.50 11.00 0 0 80 0 �e TIC: A45413.D 1 19 14.15 17.38 1000000 15.73 ' 800000 600000 400000 200000 0 12.0 13.9 14.0.54 15.40 16.32 17.11 18.2 Ime-> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 1000000 800000 600000 400000 200000 0 Time-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 t111 J41J.L rUn"U04U. V1 Mori Mar 'L/ U9:3b:42 2UUb H5971 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45413.D Vial: 12 Acq On : 23 Mar 2006 18:36 Operator: tm Sample : 0603561-010A Inst H5971 Misc : TSL005,MW-6D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:07 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 630012 50.00 UG/L 0.0,0 35) 1,4-Difluorobenzene 10.32 114 1089440 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 579784 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.38 152 523220 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.88 65 406188 47.14 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 94.28% 55) Toluene -d8 12.20 98 1333550 49.65 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 99.30%, 56) 4-Bromofluorobenzene 15.73 95 564449 49.99 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.98% Target Compounds Qvalue 8) Acetone 6.70 43 6191 5.42 UG/L 98 ------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45413.D PUHW0320.M Mon Mar 27 09:34:11 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary Pperator ID: tm Date Acquired: 23 Mar 2006 18:36 lata File: C:\HPCHEM\1\DATA\MAR06\032306A\A45413.D lame: 0603561-010A Misc: TSL005,MW-6D,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45413.D PUHW0320.M Mon Mar 27 09:38:43 2006 H5971 00 O O F-+ Re f50 ce Ra W50 0 Sub 50 0 A45413.D PUHW0320.M #8 Acetone Concen: 5.42 UG/L RT: 6.70 min Scan# 270 Delta R.T. 0.00 min Lab File: A45413.D Acq: 23 Mar 2006 18:36 Tgt Ion: 43 Resp: 6191 Ion Ratio Lower Upper 43 100 58 33.7 12.5 52.5 1200 1000 800 600 400 200 0 Mon Mar 27 09:34:15 2006 H5971 01 Page 3 IA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (9/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Contract: (amt Soil Extract Volume: (µL) CAS NO. COMPOUND BPA SAMPLE NO. MW -6S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-011A Lab File ID: A\A45414.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: (ua /L nr tiff/W-1 TTG /T. n 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 6 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: EPA SAMPLE NO. MW -6S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-011A Lab File ID: A\A45414.D Date Received: 03/16/06 Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (AL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 FORM I VOA -TIC OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -6S TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-011A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45414.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45414.D Vial: 13 Acq On : 23 Mar 2006 19:08 Operator: tm Sample : 0603561-011A Inst : H5971 Misc : TSL005,MW-6S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:37 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D 1400000 1350000 1300000 1250000 1200000 1150000 1100000 1050000 1000000 950000 900000 850000 800000 750000 '700000 650000 600000 550000 500000 450000 400000 350000 300000 250000 200000 150000 100000 50000 0 Ime-> A45414.D PUHW0320.M Mon Mar 27 09:34:28 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45414.D Operator : tm Acquired : 23 Mar 2006 19:08 using AcgMethod PUHW0320 Instrument : H5971 Sample Name: 0603561-011A Misc Info : TSL005,MW-6S,H20,SAMP „ Vial Number: 13 Quant File :PUHW0320.RES (RTE Integrator) A45414.D 2UHWUJ2U.M Mon Mar 27 09:38:55 2006 H5971 1000000- 800000. 10.32 600000 9.34 400000 9.88 200000 D 5.195.40 6.70 110.82 Time-> 4. 0 5. 0 5. 0 6.bb 6. 0 7.W 7. 0 i.66 B.ho 9.bo 9. 0 10.00 10.50 11.00 1 � . 1 19 14.15 17.38 1000000 15.73 800000- 600000. 400000 200000 01 12.0 13.9 14.1.54 15.40 16.32 17.11 18.2 Time--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 1000000 800000 600000 400000 200000 0 21.07 24.18 Ime--> 18.50 20. 19.00 19.50 00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 A45414.D 2UHWUJ2U.M Mon Mar 27 09:38:55 2006 H5971 Quant Time: Mar 23 19:37 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Quantitation Report (QT Reviewed) 168 Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45414.D Vial: 13 Acq On : 23 Mar 2006 19:08 Operator: tm Sample : 0603561-011A Inst : H5971 Misc : TSL005,MW-6S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P 50.00 UG/L Quant Time: Mar 23 19:37 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 643327 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1091979 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 581914 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.38 152 521281 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 8) Acetone 9.88 65 408084 47.25 UG/L 0.00 Range 76 - 114 Recovery = 94.500 12.19 98 1346944 50.04 UG/L 0.00 Range 86 - 115 Recovery = 100.08% 15.73 95 563976 49.83 UG/L ' 0.00 Range 88 - 110 Recovery = 99.66% Qvalue 6.71 43 6694 5.74 UG/L 92 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45414.D PUHW0320.M Mon Mar 27 09:34:26 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary onerator ID: tm Date Acquired: 23 Mar 2006 19:08 ;Lta File: C:\HPCHEM\1\DATA\MAR06\032306A\A45414.D ime: 0603561-011A Misc: TSL005,MW-6S,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45414.D PUHW0320.M Mon Mar 27 09:38:55 2006 H5971 Re fso 0 RawSo 0 Sub o 0 #8 Acetone Concen: 5.74 UG/L RT: 6.71 min Scan# 271 Delta R.T. 0.01 min Lab File: A45414.D Acq: 23 Mar 2006 19:08 Tgt Ion: 43 Resp: 6694 Ion Ratio Lower Upper 43 100 58 28.0 12.5 52.5 n 1400 1200 1000 800 600 400 200 0 A45414.D PUHW0320.M Mon Mar 27 09:34:30 2006 H5971 Page 3 E--+ lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Contract: EPA SAMPLE NO. MW -8D Case No.: PCTSL SAS No.: SDG No.: TSL005 WATER Lab Sample ID: 0603561-012A WML) ML Lab File ID: A\A45415.D LOW Date Received: 03/16/06 Date Analyzed: 03/23/06 ID: .53 (mm) Dilution Factor: 1.00 (µL) Soil Aliquot Volume (AL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 9 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 k.g 1 H 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: 112M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (AL) CAS NO. COMPOUND EPA SAMPLE NO. MW -8D SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-012A Lab File ID: A\A45415.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (gL) CONCENTRATION UNITS: (ua/L or as/Kal TTG/L A 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -BD Lab Name: H2M LABS, INC. Contract: L b C d a o e. 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-012A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45415.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (Al) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45415.D Vial: 14 Acq On 23 Mar 2006 19:39 Operator: tm Sample 0603561-012A Inst H5971 Misc TSL005,MW-BD,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 20:35 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuina Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Abundance TIC: A45415.D 1400000 1350000 e d 1300000 d N ` o 1250000 c u 1200000 0 t 0 N 1150000 d 1100000 ° `o 1050000 0 1000000 4 a 950000 d H 900000- a `o 850000 !E 800000- 00000750000700000 750000- 700000. N 650000- 50000600000 600000- 550000 550000 ad ° 500000 450000 s 400000- 00000 350000 350000'. 300000 250000 200000 150000 100000 e ° e a � 50000 0 � ;time--> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45415.D PUHW0320.M Mon Mar 27 09:34:45 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45415.D Operator tm Acquired 23 Mar 2006 19:39 using AcgMethod PUHW0320 Instrument H5971 Sample Name: 0603561-012A Misc Info : TSL005,MW-8D,H2O,SAMP „ Vial Number: 14 Quant File :PUHW0320.RES (RTE Integrator) kb �e 1000000 10.31 800000 600000 9.34 400000 9.88 200000 6.69 10.82 D Time--> s.8o 6 - bo 6. 0 7. 0 7. 0 8. 0 8. 0 9. 0 9. 0 10.00 10.50 11.00 12 19 17.38 14.15 1000000 15.73 800000 600000 400000 200000 12.0 13.14 13.9 14.14.54 15.40 16.32 16.715.86116 18.2 0 Time-> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 1000000 600000 600000 400000 200000 01.38 2129.44 Time-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 A45415 . V runwv3L V .M 111011 Lldi 4 1 U-7. 1�-1. U� � � . - I- Quant Time: Mar 23 20:35 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu May 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Quantitation Report (QT Reviewed) 168 Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45415.D Vial: 14 Acq On : 23 Mar 2006 19:39 Operator: tm } Sample : 0603561-012A Inst : H5971 - Misc : TSL005,MW-BD,H20,SAMP,, Multiply: 1.00 MS Integration Params: RTEINT.P 50.00 UG/L Quant Time: Mar 23 20:35 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu May 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 634884 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.31 114 1098220 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 583096 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.38 152 521652 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 8) Acetone -1-- 2-Butanone 9.88 65 406166 46.76 UG/L 0.00 Range 76 - 114 Recovery = 93.520 12.19 98 1341157 49.54 UG/L 0.00 Range 86 - 115 Recovery = 99.080 15:73 95 560890 49.27 UG/L 0.00 Range 88 - 110 Recovery = 98.54% Qvalue 6.70 43 10729 9.32 UG/L 96 8.84 43 2861 1.31 UG/L 67 ------------------------------------------------------------------------- (#) = qualifier out of range (m) =manual integration A45415.D PUHW0320.M Mon Mar 27 09:34:43 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary t�nerator ID: tm Date Acquired: 23 Mar 2006 19:39 Vita File: C:\HPCHEM\1\DATA\MAR06\032306A\A45415.D ,_ime: 0603561-012A Misc: TSL005,MW-8D,H20,SAMP,, Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45415.D PUHW0320.M Mon Mar 27 09:39:10 2006 H5971 Re f5o 0 n,dz-> Abundance IC Ra W50 0 z--> Abundance c Sub 50 0 ftvz—> Abundance bc Re f50 0 rrdz--> Abundance Raw50 0 z_> Abundance cl Sub 50 0 t—> #8 Acetone Concen: 9.32 UG/L RT: 6.70 min Scan# 270 Delta R.T. 0.00 min Lab File: A45415.D Acq: 23 Mar 2006 19:39 Tgt Ion: 43 Resp: 10729 Ion. Ratio Lower Upper 43 100 58 35.0 12.5 52.5 naanci 2000 1500 1000 500 0 #16 2-Butanone ` Concen: 1.31 UG/L RT: 8.84 min Scan# 487 Delta R.T. 0.01 min Lab File: A45415.D Acq: 23 Mar 2006 19:39 Tgt Ion: 43 Resp: 2861 Ion Ratio Lower Upper 43 100 72 7.5 3.8 43.8 700 600 500 400 300 200 100 0 me—> I A45415.D PUHW0320.M Mon Mar 27 09:34:46 2006 H5971 O O V1 Page 3 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (9/mL) ML Level: (low/med) LOW % Moisture: not dec. Bromomethane GC Column: R-502.2 ID: .53 Soil Extract Volume: NL CAS NO. COMPOUND Contract: (mm L) EPA SAMPLE NO. MW -8S SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-013A Lab File ID: A\A45416.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (ua/L or ua/Ka) IIG/L O 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 -U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 9 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Soil Extract Volume: (µ CAS NO.. COMPOUND Contract: BPA SAMPLE NO. MW -83 SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-013A Lab File ID: A\A45416.D Date Received: 03/16/06 Date Analyzed: 03/23/06 mm) Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: (µg/L or Ag/Kg)UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -BS TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) Number TICS found: 0 CAS NUMBER COMPOUND NAME Lab Sample ID: 0603561-013A Lab File ID: A\A45416.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L RT EST.CONC. Q FORM I VOA -TIC OLM04.2 00 O O Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45416.D Vial: 15 - Acq On 23 Mar 2006 20:11 Operator: tm Sample 0603561-013A Inst H5971 Misc : TSL005,MW-8S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 20:42 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 Roarnnnco via rnnt-iniiinrr r;;l Fila. r.\HPC.TiRM\l\nATA\MAR06\032306A\A45398.D Abundance TIC: A45416.13 1450000 1400000 1350000 m 1300000 b N d G D 1250000 o 1200000 m a r c r y 1150000 d N N 1100000 D D 1050000 a E o 1000000 d 950000 d 900000 a 0 cE 850000 800000- 00000750000700000 750000- 700000- 650000- 650000600000 600000 e d y 550000 d 500000 0 450000 t x 400000 n 350000 300000 250000 200000 150000 100000° A D Q N 50000 0 11 im, 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45416.D PUHW0320.M Mon Mar 27 09:35:04 2006 H5971 Page 2 _i File Operator Acquired Instrument Sample Name: Misc Info . Vial Number: Quant File : LSC Report - Integrated Chromatogram C:\HPCHEM\1\DATA\MAR06\032306A\A45416.D tm 23 Mar 2006 20:11 using AcgMethod PUHW0320 H5971 0603561-013A TSL005,MW-8S,H20,SAMP „ 15 PUHW0320.RES (RTE Integrator) 120 �o0eI IC: A45416.13 1000000- 800000- 10.31 .600000- 9.34 400000 9.88 200000 0 5.6618 6.70 10.9x.82 Time-> 4. 0 5.W 516 6.66 6. 0 7.W 7. 0 8. 0 8. 0 6.66 9 -To 10.00 10.50. 11.00 Ok 1n �00 TIC: A45416.13 20 1 19 14.14 17.38 1000000 15.73 800000- 00000600000400000200000 600000- 400000- 200000 O 12.0 13.14 13.9 14.54 15.40 16.32 16.97tPY)a 18.2 Time-> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.OD 15.50 16.06 16.50 17.00 17.50 18.00 1 0 Go- o -1000000800000600000400000 TIC: A454TU.EF- 1000000- 800000- 600000 - 400000. 200000 0 20.57 Time--> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.56 23.06 23.50 24.00 24.50 25.00 A45416.D PUHWU32U.M Mon Mar 2-1 09:39:26 2006 H5971 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45416.D Vial: 15 - Acq On : 23 Mar 2006 20:11 Operator: tm Sample : 0603561-013A Inst : H5971 Misc : TSL005,MW-BS,H2O,SAMP,, Multiplr: 1.00 MS Integration Params: RTEINT.P 0.00 70) 1,4 -Dichlorobenzene -d4 Quant Time: Mar 23 20:42 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 641422 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.31 114 1093396 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 581086 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.38 152 525782 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.88 65 406303 46.98 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.96% 55) Toluene -d8 12.19 98 1339943 49.71 UG/L .0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 99.42% 56) 4-Bromofluorobenzene 15.73 95 563300 49.70 UCS/L - 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.40% "Parget Compounds Qvalue 8) Acetone 6.70 43 10003 8.60 UG/L 95 -1-6-) 2-Butanone 8.84 43 2397 1.09 UG/L 67 ------------------------------------------------------------------------- �(#) = qualifier out of range (m) = manual integration A45416.D PUHW0320.M Mon Mar 27 09:35:02 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary -^rjerator ID• tm Date Acquired: 23 Mar 2006 20:11 ;ta File: C:\HPCHEM\1\DATA\MAR06\032306A\A45416.D 0603561-013A Misc: TSL005,MW-8S,H20,SAMP„ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc -------------------------------------=-------------------------------------- A45416.D PUHW0320.M Mon Mar 27 09:39:27 2006 H5971 i Re f50 0 z-> un aance Raw50 0 z-> un ance Sub 50 0 Re f50 0 RawSo 0 Sub 50 0 } A45416.D PUHW0320.M #8 Acetone Concen: 8.60 UG/L RT: 6.70 min Scan# 270 Delta R.T. 0.00 min Lab File: A45416.D Acq: 23 Mar 2006 20:11 Tgt Ion: 43 Resp: 10003 Ion Ratio Lower Upper 43 100 58 35.4 12.5 52.5 2000- 1500- 1000- 500 00015001000500 0 Ime--> 6.h—o---6Y6 6. 0 #16 2-Butanone Concen: 1.09 UG/L RT: 8.84 min Scan# 487 Delta R.T. 0.01 min Lab File: A45416.D Acq: 23 Mar 2006 20:11 Tgt Ion: 43 Resp: 2397 Ion Ratio Lower Upper 43 100 72 7.6 3.8 43.8 700 600 500 400 300 200 100 0 Ion 71.95 (71.65 to 72.65): A45 8.84 Mon Mar 27 09:35:06 2006 H5971 M N O O Page 3 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (AL) CAS NO. COMPOUND SPA SAMPLE NO. TRIP BLANK 3/16 SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-014A Lab File ID: A\A45417.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (u4/L or ua/Ka) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) ML Level: (low/med) LOW % Moisture: not dec. Contract: GC Column: R-502.2 ID: .53 (mm Soil Extract Volume: (AL) CAS NO. COMPOUND BPA SAMPLE NO. TRIP BLANK 3/16 SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-014A Lab File ID: A\A45417.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or u9/Ka) UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 _ trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 FORM I VOA -TIC N O O OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TRIP BLANK 3/16 1 /Lab TENTATIVELY IDENTIFIED COMPOUNDS Name: H2M LABS,.INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-014A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45417.D Level: (low/med) LOW Date Received: 03/16/06 % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (Al) Soil Aliquot Volume: 0 (AL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q FORM I VOA -TIC N O O OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45417.D Vial: 16 Acq On 23 Mar 2006 20:42 Operator: tm Sample 0603561-014A Inst : H5971 Misc TSL005,TB 3/16,H201SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 21:09 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 ,._—;-4 -- r- I L1; ie - r-\T41DrLiFM\1\nATz,\mAROfi\032306A\A45398.D A45417.D PUHW0320.M Mon Mar 27 09:35:21 2006 H5971 Page 2 N Ln O O un ance 1450000 1400000- 13500W - C N 1300000 d ° 1250000 iN Q ° e 1200000 v N 1150000- 1500001100000 1100000. a 0 1050000 o` E 1000000 a 950000 5 a 900000 ° `o 850000 800000 750000 700000 v 650000 `o 600000 � y 550000 0 500000 0 450000 t u 400000 r 350000 300000 250000 200000 150000 100000 50000 0 Ime—> 6.60' 8. 0 10.00 12.0 0 14.00 16.00 18.00 20.0 0 22.00 24.00 A45417.D PUHW0320.M Mon Mar 27 09:35:21 2006 H5971 Page 2 N Ln O O LSC Report - Integrated Chromatogram File : C:\HPCHEM\1\DATA\MAR06\032306A\A45417.D Operator tm Acquired 23 Mar 2006 20:42 using AcgMethod PUHW0320 Instrument H5971 Sample Name: 0603561-014A Misc Info : TSL005,TB 3/16,H20,SAMP „ Vial Number: 16 Quant File :PUHW0320.RES (RTE Integrator) Abundance 1200000 1000000- 800000 10.32 600000 9.34 400000 9.89 L 200000- i 5.45 7.30 0 Ime--> 4.50 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 8. 0 8. 0 9. 0 9. 0 10.00 10.50 11.00 Abundance 1200000 1 19 14.14 17.39 1000000 15.73 800000 600000 400000 200000 0�14 15.41 Time-> 11.50 12.00 12.50 13.00 13.50 .00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance 1200000 1000000 800000 600000 400000 200000 0 Ime-> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 A45417.D PUHWU3ZU.M Mon Mar 2/ U9:3y:3/ ZUUb ri5y/1 Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45417.D Vial: 16 Acq On 23 Mar 2006 20:42 Operator: tm Sample 0603561-014A Inst : H5971 Misc TSL005,TB 3/16,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 21:09 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 634962 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1091964 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 579971 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 524636 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55.) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 9.89 65 398664 46.16 UG/L 0.00 Range ..76 - 114 Recovery = 92.32% 12.19 98 1331556. 49.46 UG/L 0.00 Range 86 - 115 Recovery = 98.92% 15.73 95 560850 49.55 UG/L 0.00 Range 88 - 110 Recovery = 99.10% Qvalue ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45417.D PUHW0320.M Mon Mar 27 09:35:19 2006 H5971 Page 1 N O O Cn H Tentatively Identified Compound (LSC) summary -,aerator ID: tm Date Acquired: 23 Mar 2006 20:42 ;ta File: C:\HPCHEM\1\DATA\MAR06\032306A\A45417.D 0603561-014A Misc: TSL005,TB 3/16,H2O,SAMP „ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45417.D PUHW0320.M Mon Mar 27 09:39:37 2006 H5971 1-12M "US, INC. III. STANDARD DATA PACKAGE FOR VOLATILE ORGANICS A. INITIAL CALIBRATION FORM B. STANDARD GC/MS CHROMATOGRAMS C. DATA SYSTEM REPORT D. CONTINUING CALIBRATION FORM E. STANDARD GC/MS CHROMATOGRAMS F. DATA SYSTEM REPORT 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Lab Code: 10476 Case No.: Instrument ID: HP5971 Heated Purge: (YIN) N GC Column: R-502.2 Contract: PCTSL SAS No.: SDG No.: rsl,uuD Calibration Date(s): 03/20/06 03/21/06 Calibration Times: 23:09 1:16 ID: .53 (mm) LAB FILE ID: VSTD050 A45323.D VSTDO10 A45321.D VSTD100 A45324.D VSTD020 VSTD200 A45322.D A45325.D COMPOUND STDO1 STD02 STD05 STD10 STD20 RRF FRSD Chloromethane 0.319 0.290 0.284 0.278 0.272 0.289 6.3 Vinyl chloride 0.352 0.296 0.303 0.304 0.301 0.311 7.4 Bromomethane 0.268 0.222 0.213 0.222 0.221 0.229 9.6 Chloroethane 0.273 0.224 0.230 0.234 0.230 0.238 8.3 Acrylonitrile 0.222 0.149 0.151 0.170 0.159 0.170 17.8 Trichlorofluoromethane 0.433 0.336 0.422 0.413 0.435 0.408 10.1 1,1-Dichloroethene 0.338 0.293 0.303 0.292 0.294 0.304 6.4 lodomethane 0.598 0.518 0.507 0.553 0.557 0.547 6.6 Vinyl acetate 0.571 0.693 0.585 0.692 0.675 0.643 Acetone 0.152 0.114 0.100 0.105 0.102 0.115 8. 18.6 Carbon disulfide 1.613 1.388 1.352 1.470 1.468 1.458 6.9 Methylene chloride 0.533 0.470 0.463 0.454 0.448 0.474 7.3 trans-1,2-Dichloroethene 0.478 0.425 0.433 0.418 0.406 0.432 6.4 1,1-Dichloroethane 1.152 1.064 1.078 1.034 1.002 1.066 5.3 cis-1,2-Dichloroethene 0.606 0.540 0.539 0.514 0.483 0.536 8.5 2-Butanone 0.281 0.185 0.178 0.196 0.182 0.204 21.2 Bromochloromethane 0.243 0.219 0.207 0.201 0.194 0.213 9.0 Chloroform 1.095 0.980 0.955 0.935 0.903 0.974 7.5 1,1,1 -Trichloroethane 0.761 0.675 0.744 0.725 0.728 0.727 4.4 1,1-Dichloropropene 0.399 0.343 0.380 0.357 0.360 0.368 6.0 Carbon tetrachloride 0.364 0.314 0.374 0.354 0.373 0.356 7.0 Benzene 1.358 1.217 1.186 1.128 1.063 1.190 9.3 1,2-Dichloroethane 0.554 0.494 0.474 0.463 0.439 0.485 9.0 Trichloroethene 0.309 0.287 0.297 0.287 0.287 0.294 3.3 1,2-Dichloropropane 0.467 0.421 0.409 0.390 0.372 0.412 8.8 Dibromomethane 0.227 0.205 0.187 0.188 0.185 0.198 9.0 Bromodichloromethane 0.533 0.486 0.460 0.458 0.449 0.477 7.1 cis-1,3-Dichloropropene ' 0.726 0.655 0.618 0.603 0.582 0.637 8.9 4-Methyl-2-pentanone 0.454 0.282 0.262 0.297 0.274 0.314 25.3 Toluene 0.863 0.817 0.800 0.751 0.711 0.788 7.5 trans-1,3-Dichloropropene 0.666 0.592 0.547 0.536 0.519 0.572 10.4 1,1,2 -Trichloroethane 0.293 0.256 0.227 1 0.220 0.211 0.242 13.9 Tetrachloroethene 0.438 0.440 0.525 0.394 0.388 0.437 12.5 2-Hexanone 0.579 0.379 0.334 0.369 0.340 0.400 25.4 Dibromochloromethane 0.696 0.622 0.580 0.585 0.596 0.616 7.8 1,2-Dibromoethane 0.380 1 0.349 0.312 0.307 0.302 0.330 10.1 FORM VI VOA - 1 OLM04.2 6B VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Instrument ID: HP5971 Calibration Date(s) Heated Purge: (Y/N) N Calibration Times: GC Column: R-502.2 ID: .53 (mm) SDG No.: TSL005 03/20/06 03/21/06 23:09 1:16 LAB FILE ID: VSTDO50 A45323.1) VSTDO10 A45321.D VSTD100 A45324.1) VSTD020 VSTD200 A45322.1) A45325.D COMPOUND STDO1 STD02 STD05 STD10 STD20 RRF RSD Chlorobenzene 1.921 1.861 1.771 1.659 1.589 1.760 7.8 trans-1,4-Dichloro-2-butene 0.367 0.247 0.228 0.254 0.245 0.268 20.9 Ethylbenzene 0.952 0.909 0.878 0.791 0.732 0.852 10.5 1,1,1,2 -Tetrachloroethane 0.590 0.556 0.530 0.505 0.495 0.535 7.2 m,p-Xylene 1.207 1.160 1.109 0.982 0.912 1.074 11.5 o -Xylene 1.293 1.237 1.158 1.044 0.962 1.139 11.9 Xylene (total) 1.293 1.237 1.158 1.044 0.962 1.139 11.9 Styrene 2.190 2.172 1.981 1.796 1.646 1.957 12.1 Bromoform 0.513 0.484 0.440 0.442 0.451 0.466 6.9 1,1,2,2 -Tetrachloroethane 0.930 0.868 0.717 0.711 0.699 0.785 13.6 1,2,3-Trichloropropane 0.224 0.202 0.183 0.177 0.177 0.193 10.5 1,4 -Dichlorobenzene 1.564 1.493 1.410 1.335 1.284 1.417 8.0 1,2 -Dichlorobenzene 1.498 1.452 1.339 1.276 1.243 1.362 8.1 1,2-Dibromo-3-chloropropane 0.139 0.135 0.115 0.115 0.122 0.125 9.2 * Compounds with required minimum xxr, and maximum sxwli values. All other compounds must meet a minimum RRF of 0.010. FORM VI VOA - 2 OLM04.2 6B VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Instrument ID: HP5971 Calibration Date(s): 03/20/06 03/21/06 Heated Purge: (Y/N) N Calibration Times: 23:09 1:16 GC Column: R-502.2 ID: .53 (mm) LAB FILE ID: VSTDO50 A45323.D VSTD010 A45321.D VSTD100 A45324.D VSTD020 VSTD200 A45322.D A45325.1) COMPOUND �STD01 STD02 STD05 STD10 STD20� RSD RRF 1,2-Dichloroethane-d4 0.400 0.435 0.500 0.234 0.415 0.397 24.8 Toluene -d8 1.056 1.207 1.329 0.598 1.012 1.041 26.7 4-Bromofluorobenzene 0.468 0.540 1 0.592 0.267 0.462 0.466 26.5 * Compounds with required minimum RRF and maximum tRSD values. All other compounds must meet a minimum RRF of 0.010. FORM VI VOA - 3 OLM04.2 7t M O O H Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45321.D Vial: -9 Acq On : 20 Mar 2006 23:09 Operator: tm. Sample : VSTDO10 Inst : H5971 Misc : ,,,ICAL,, Multiplr:-1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2006 Quant -Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D Abundance 1300000 1250000 1200000 1150000 - e 1100000 1050000 1000000 950000 G ° 900000 E ° 850000 9 4 800000 750000 700000 0 650000 a 600000 E 6 550000 a ° 500000 450000 * z a . 400000 r- t O � 350000 F r k t� a Q § a F N 300000 6 �p 3 " 1 43. 250000 ' ' ~ 0 � r 2 w c . i a " ° o ° 200000• n E =.� {, e h CL s F 150000 :5E - $ c E �o o 3n E e a 100000 $r5 x�.c 4 05 °U F W8. 500000ie-> 10.00 12 00 14.00 16.00 18.00 20.00 Z A45321.D PUHW0320.M Mon Mar 27 10:07:03 2006 H5971 24.00 a Page 4 F-+ Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032006A\A45321:D Vial: 9 Acq On 20 Mar 2006 23:09 Operator: tm Sample VSTDO10 Inst H5971 Misc ,,,ICAL ,, Multiplr: 1:00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHWO320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\l\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev.(Min) 1) Pentafluorobenzene 9.35 168 641106 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10:32 114, 1075734 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15. 82 590747 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17:39 152 476370 50.00 UG/L 0.00 System Monitoring Compounds 36) --- -- 1,2-Dichloroethane-d4 9.89 65 86099 8.01 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery. = 16.02%# 55) Toluene -d8 12.20 98. 227169 ' '.7.'94 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery••= 15.88%# 56) 4-Bromofluorobenzene 15.74 95 100769 7.92 UG/L - 0.00 Spiked Amount 50.000 Range 86 -.115 Recovery = 15.84%# Target Compounds Qvalue 2) Chlorodifluoromethane 4.27 51 5457 6.32 UG/L # 79 3) Dichlorodifluoromethane 4.26 85 12673 11.30 UG/L 96 4) Chloromethane 4.53' 50• 40951 11.24-UG/L 99 5) Vinyl chloride 4.77 62 45131 11.62 UG/L 97 6) Bromomethane 5.38 94 .34309 12.57 UG/L 95 7) Chloroethane 5.54 64 34969 11.87 UG/L 99 8) Acetone. 6.72 43 19435 15.11 UG/L 95 9) Acetonitrile 7.14 41 141.188 56.93 UG/L 98 10) Allyl Chloride 7.14 41 141188 11.39 UG/L # 100 11) Acrolein 6.52 56 35072 59.95 UG/I; 96 12) Acrylonitrile 7.61 53 28505 14.70 UG/L 96 13) Iodomethane 6.94 142 76680 11.79 UG/L 99 14) Vinyl acetate 8.13 43• 73271. 9.76 UG/L 98 16) 2-Butanone 8.84 43 36026 15.83 UG/L 98 17) Tetrahydrofuran 9.24 42 18614 9.96 UG/L # 100 18) Freon -113 6.63 101 28444 8.41 UG/L 98 19) Carbon disulfide 7.06 76 206778 11:92 UG/L # 68 20) Trichlorofluoromethane 5.93 101 55570 10.26 UG/L 100 21) 1,1-Dichloroethene 6.67 96 .43302 11.16 UG/L 99 22) methyl tert-butyl ether 7.57 73 191793 11.56 UG/L 99 24) Methylene chloride 7.32 84 68372 11.51 UG/L 97 25) trans-1,2-Dichloroethene 7.64 96 61277 11.03 UG/L 99 26) 1,1-Dichloroethane 8.19 ' 63 147772 10.69 UG/L 99 27) Propionitrile 8.97 54 11398 16.97 UG/L 96 29) Methacrylonitrile 9.13 67 36112 15.80 UG/L 85 30) cis-1,2-Dichloroethene 8.89 96• 77739 11.24 UG/L 96 31) Bromochloromethane - - 9.21 128 ------------------------------- 31136 11.70 UG/L 97 -------------- --------------------- (#) = qualifier out of range (m) = manual integration A45321.D PUHW0320.M Mon Mar 27 10:06:56 2006 H5971 Page 1 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45321.D Vial: 9 Acq On : 20 Mar 2006 23:09 Operator: tm Sample : VSTDO10 Inst H5971 Misc : ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART3.60E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound R.T: QIon Response Conc Unit ------------------ Qvalue. ------------------------------------------ 32) 2,2-Dichloropropane 8.89 77 88245 10.70 UG/L 100 33) Chloroform 9.24 83 140377 11.46 UG/L 99 34) 1,1,1 -Trichloroethane 9.51 97 97568 10.22 UG/L 94 37) 1,1-Dichloropropene 9.68 75 85837 10.50 UG/L 98 38) Carbon tetrachloride 9.71 117 78391 9.73 UG/L 98 39) Benzene 9.97 78 292112 11.4.5 UG/L 100 40) 1,2-Dichloroethane 9.99 62 119246 11.69 UG/L 99. 41) Methyl Methacrylate 10.96 69. 67636 15.94.UG/L # 80 42) Trichloroethene 10.71 95 66561 10.43 UG/L 99 43) 1,2-Dichloropropane 11.01 63 .100563 11.42 UG/L # 34 44) Dibromomethane 11.21 93 48866 12.12 UG/L 97 47) Bromodichloromethane 11.33 83 114685 11.58 UG/L. 100 48) cis-1,3-Dichloropropene 11.85 75 156208 11.75 UG/L 99 49) Toluene 12.29 92 185728 10.79 UG/L 100 50) Ethyl Methacrylate 12.47 69 142871 16.49 UG/L 97 51) trans-1,3-Dichloropropene 12:53 75 143385 12.18 UG/L 100 52.) 1,1,2 -Trichloroethane 12.81 83 63113 12.93 UG/L 98 53) 1,2-Dibromoethane 13.61 107 81702 12.16 UG/L 100 54) 4-Methyl-2-pentanone 11.94 43 97703 17.33 UG/L 99 58) Chlorobenzene 14.20 112 227004 10.85. UG/L 98 59) 1,3-Dichloropropane 13.04 76 138072 12.71 UG/L 100 60) Tetrachloroethene 13.03 164 51705 8.34 UG/L 99 61) Dibromochloromethane 13.39 129 82291 12.00 UG/L 100 62) 2-Hexanone 13.00 43 68376 17.32 UG/L 97 63) 1,1,1,2 -Tetrachloroethane 14.27 131 69681 11.13 UG/L 97 . 64) Ethylbenzene 14.25 106 112440 10..84 UG/I, 99 65) m,p-Xylene 14.39 106 285101 .21.75 UG/L ..99 66) o -Xylene 14.97 106 152.745 11.16 UG/L 9.7 67) Xylene (total) 14.97 106 152745 11.16 UG/L 97 68) Styrene 14.98 104 258737 11.05 UG/L 99 69) Bromoform 15.38 173 60664 11.68 UG/L 98 71) trans-1,4-Dichloro-2-buten 15.93 53 34981 16.08 UG/L 93 72) 1,1,2,2 -Tetrachloroethane 15.87 83 88569 12.96 UG/L 100 73) Pentachloroethane 16.85 167 60704 19.31 UG/L 97 74) 1,2,3-Trichloropropane 12.53 112 21307 12.22 UG/L # 93 75) Isopropylbenzene 15.42 105 314098 10.93 UG/L 100 76) Bromobenzene 16.02 156 85271 11.54 .UG/L. 99 J- 77) n-Propylbenzene 15.99 91 386076 11.48 UG/L 100 M 78) 2-Chlorotoluene/4-Chloroto 16.37 91 540428m 22.13 UG/L T' tw_--Z14 � IY� stn 79) 1,3,5-Trimethbenz/P-ethylt 16.20 105 533766m 20.45 UG/L 80) tert-Butylbenzene 16.70 119 251380 11.19 UG/L 96 O O ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration V) A45321.D PUHW0320.M Mon Mar 27 10:06:58 2006 H5971 Page2 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45321.D Vial: 9 Acq On : 20 Max 2006 .23:09 Operator: tm Sample : VSTD010 Inst H5971 Misc . ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2.006 Quant Results.File: PUHW0320.*RES Quant Method.: C:\HPCHEM\1\METHODS\PUHW0320*.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 00 M O .------------------------------------------------------------------------- O (#) = qualifier out of range (m) = manual integration A45321.D PUHW0320.M Mon Mar 27 10:06:59 2006_' H5971 Page 3 [� Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 81) 1,2,4=Trimethylbenzene 16.77 105 308012 11.11 UG/L 99 82) sec-Butylbenzene 17.01 105 338988 10.67 UG/L 99 83) 4-Isopropyltoluene 17.18 119 264005 11.02 UG/L 100 84) 1,3 -Dichlorobenzene 17.31 146 149573 11.10 UG/L 99 85) 1,4 -Dichlorobenzene 17.43 146 149010 11.09 UG/L 99 86) 1,2 -Dichlorobenzene 18.02 146 142706 11.18 UG/L 99 87,) p-Diethylbenzene 17.73 119 111475 9.14 UG/L 99 88) n-Butylbenzene 17.78 91 282305 10.40 UG/L 92 89) 1,"2-Dibromo-3-chloropropan 19.24 75 13263• 12.12 UG/L 96 90) 1,2,4,5-Tetramethylbenzene 18.94 119 181004 9.17 UG/L 99 91) 1,2,4-Trichlorobenzene 20.61 180 94160• 10.56 UG/L 100 92) Hexachlorobutadiene 20.78 225 31548 8.40 UG/L 99 93)' Naphthalene 21.13 128 129769'" 10.78 UG/L 100 94) 1,2,3-Trichlorobenzene 21.59 180 55027 10..31 UG/L 99 00 M O .------------------------------------------------------------------------- O (#) = qualifier out of range (m) = manual integration A45321.D PUHW0320.M Mon Mar 27 10:06:59 2006_' H5971 Page 3 [� Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45322.D Vial: 10 Acq On : 20 Mar 2006 23:41 Operator: tm Sample : VSTD020 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00, MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS T,ast Update : Mon Mar 27 09:22:50 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\0320U6A\A4,)JZJ.0 1250000 1200000 1150000 ~_ Y 1100000 1050000 T ' a E 1000000 14 950000 4 qc 900000 850000 0 'f• 800000 0 f q MR 750000 N D Y 700000 ` T o C � Y . 650000 EC o y F 600000 C s "' a e �►- H~ r 550000 C. a o 5, a w Q a � 500000 r 2 S 450000 .; o `M. 4 K r $F S i o r o 400000 1i s e s F p Xs� o r F 350000 300000 i � c 250000 '' c r-� Eoo c t p 3 t a n f 200000ci N EOE O e. c E S x 150000 . H s — n 100000 � s 50000 • 0 iM_> 6. 0 8. 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45322.D PUHW0320.M Mon Mar 27 10:07:26 2006 H5971 Page 4 H Quantitation Report '- (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45322.D Vial: 10 Acq On : 20 Mar 2006 23:41 Operator: tm Sample : VSTD020 Inst : H5971 } Misc ,,, ICAL Multiplr: 1.00 MS Integration Params: RTEINT.P Chlorobenzene-d5 14.15 Quant Time: Mar 21 10:02-2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Internal Standards R. T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 604770 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.33 114 1018048 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 564967 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 458872 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 177005 17.40 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 34.80%# 55) Toluene -d8 12.20 98 491418 18.16 UG/L 0.00 Spiked Amount 50.000 Range -88 - 110 Recovery = 36.32%# 56) 4-Bromofluorobenzene 15.74 95 219871 18.26 UG/L' 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 36.52%# .Target Compounds Qvalue 2) Chlorodifluoromethane 4.25 51 14948 18.35 UG/L 79 3) Dichlorodifluoromethane 4.28 85 20643 19.51 UG/L 93 4) Chloromethane 4.53 50 70202 20.42 UG/L- 99 .5) Vinyl chloride 4.76 62 71659 19.56 UG/L 98 6) Bromomethane 5.38 94 53634 20.83 UG/L 97 7) Chloroethane 5.53 64 54145 19.48 UG/L 99 8) Acetone 6.71 43 27579 22.73 UG/L 98 9) Acetonitrile 7.13 41 243797 104.22 UG/L 99 10) Allyl Chloride 7.13 41 243797 20.84 UG/L .# 10 11) Acrolein 6.52 56 59681 ,108.14 UG/L 99 12) Acrylonitrile 7.61 53. 36030 19.70-UG/L 96 13) Iodomethane 6.94 142 125361 20.43 UG/L 99 14) Vinyl acetate 8.13 43 167667 23.68 UG/L .99 16) 2-Butanone 8.84 43 44716 20.83 UG/L 98 17) Tetrahydrofuran 9.24 42 30511 17.30 UG/L # 100 18) Freon -113 6.63 101 63388 19.86 UG/L 95 19) Carbon disulfide 7.05 76 335632 20.53 UG/L'# 68 20) Trichlorofluoromethane 5.92 101 81361 15.93 UG/L 98 21) 1,1-Dichloroethene 6.67 96 70910 19.37 UG/L 97 22) methyl tert-butyl ether 7.57 73 278837 17.82 UG/L 99 24) Methylene chloride 7.31 84 113667 20.29 UG/L 99 25). trans-1,2-Dichloroethene 7.64 96 102842 19.62 UG/L 99 26) 1,1-Dichloroethane 8.19 63 257299 19.73 UG/L 99 27) Propionitrile 8.96 54 12687 20.02 UG/L 99 29)-Methacrylonitrile 9.13 67 43545 20.20 UG/L 89 30) cis-1,2-Dichloroethene 8.69 96 130512 20.01 UG/L 97 31) Bromochloromethane 9.20 128 52887 21.07 UG/L 96 ------------------------------------------------------------------------- !(#) = qualifier out of range (m) = manual integration A4532'2.D PUHW0320.M Mon Mar 27 10:07:19 2006 H5971 - Page 1 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45322.D Vial: 10 Acq On : 20 Mar 2006 23:41 Operator: tm Sample VSTD020 Inst : H5971 Misc ,,,ICAL,l. Multiplr: 1.00 • RTEINT P 33) MS •Integration Params. Quant Time: Mar 21 10:02 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue ---------------------------- 32) -------------------------------------------- 2,2-Dichloropropane 8.89 77 148396 19.08 UG/L. 100 33) Chloroform 9.24 83 237149 20.53 UG/L 99 34) 1,1,1 -Trichloroethane. 9.51 97 163239 18.13 UG/L 9.7 37). 1,1-Dichloropropefte 9.67 75 139618 18.05 UG/L 99 38) Carbon tetrachloride 9.71 117 127762 16.76 UG/L 99 39) Benzene 9.96 78 495461 20.52 UG/L 99 40) 1,2-Dichloroethane 9.98 62 200999 20.82 UG/L 99 41) Methyl Methacrylate 10.96 69 81789 20.37 UG/L 97 42) Trichloroethene 10.71 95 117063 19.38 UG/L 99 43') 1,2-Dichloropropane 11.02 63 171573 20.59 UG/L # 34 44) Dibromomethane 11.20 93 83328 21.85 UG/L 99 47) Bromodichloromethane 11'.33 83 197728 21.09 UG/L 100 48) cis-1,3-Dichloropropene 11.85 75 266540 21.18 UG/L 100 49) Toluene 12.29 92 332633 20.43 UG/L 99 . 50) Ethyl Methacrylate 12.47 69 171949 20.97 UG/L 98 51) trans-1,3-Dichloropropene 12.52 75 241102 21.65 UG/L 99 52) 1,1,27Trichloroethane 12.81 83 104417 22.60 UG/L 99 53) 1,2-Dibromoethane 13.60 107 141923 22.32 UG/L 99 54) 4-Methyl-2-pentanone 11.94 43 114745 21.51 UG/L 99 58) Chlorobenzene 14.20 112 420473 21.01 UG/L 100 59) 1,3-Dichloropropane 13.05 76 23195.7 22.33 UG/L 98 60) Tetrachloroethene 13.03 164 99410 16.77 UG/L 100 61) Dibromochloromethane 13:39 129 140660 21.45 UG/L 99 62.) 2-Hexanone 13.00 43 85556 22.66 UG/L 99 63) 1,1,1,2 -Tetrachloroethane 14.27 131 125638 20.99 UG/L 98 64) Ethylbenzene 14.25 106 205529 20.72 UG/L 98 65) m,p-Xylene 14.39 106 524326 41.83 UG/L 98 66) o -Xylene 14.96 106 279443 21.35 UG/L 99 .67).Xylene (total) 14.96 106 279443 21.35 UG/L 99 68) Styrene 14.98 104. 490786 21.92 UG/L 99 69) Bromoform 15.38 173 109321 22.01 UG/•L 99 71) trans-l;4-Dichloro-2-buten 15.93 53 45285 21.61 UG/L 94 72) 1,1,2,2 -Tetrachloroethane 15.88 83 159241 24.19 UG/L 99 73) Pentachloroethane 16.85 167 82505 27.25 UG/L 98 74) 1,2,3-Trichloropropane 12.52 112 37150 22.12 UG/L # 89 75) Isopropylbenzene 15.42 105 518379 18.73 UG/L 100 76) Bromobenzene 16.02 156 158806 22.31 UG/L 99 77) n-Propylbenzene 15.99 91• 606660 18.72'-UG/L 99 d" 78) 2-Chlorotoluene/4-Chloroto 16.37 91 986252m 41.92 UG/L 79) 1,3,5-Trimethbenz/P-ethylt 16.20 105 967310m 38.48 UG/L 80) tent-Butylbenzene 16.70 119 367692 16.99 UG/L 100 CD ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration �- A45322.D PUHW0320.M Mon Mar 27 10:07:20 2006 H5971 Page 2 p -j Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A.\A45322.D Vial: 10 Acq On : 20 Mar 2006 23:41 Operator: tm Sample : VSTD020 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:02 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last.Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 81) 82) 83) 84) 85) 86) 87) 88) 89) 90) 91) 92) 93) 94) Compound 1,2,4-Trimethylbenzene .sec-Butylbenzene 4-Isopropyltoluene 1,3 -Dichlorobenzene 1,4 -Dichlorobenzene 1,2 -Dichlorobenzene p-Diethylbenzene n-Butylbenzene 1,2-Dibromo-3-chloropropan 1,2,4,5-Tetramethylbenzene 1,2,4-Trichlorobenzene Hexachlorobutadiene Naphthalene 1,2,3-Trichlorobenzene R.T. QIon Response 16.77 105 525171 17.01 105 449611 17.18 119 3598.82 17.31 146 272578 17.43 146 274022 18.02 146. 266540 17.73 119 224531 17.78 91 .394003 19.24 75 24845 18.93 119 367454 20.61 180 155162 20.77 225 35900 21.13 128 248777 21:58 160 96462 Conc Unit Qvalue 19.67 UG/L 98 14.69 UG/L 99 15.59 UG/L 99 21.01 UG/L_ 99 21.17 UG/L 99 21.69.UG/L 100 19.11 UG/L 97 15.07 UG/L # 62 23.57 UG/L 96 19.32 UG/L 99 18.06 UG/L 100 9.92 UG/L 99 21.46 UG/L 100 18.77 UG/L 98 ---------------------- 1(##) = qualifier out of range (m) = manual integration A45322.D PUHW0320.M Mon Mar 27 10:07:21-2006 H5971 Page 3 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D Vial: 11 Acq On : 21 Mar 2006 00:12 Operator: tm Sample VSTDO50 Inst H5971 Misc : ,,,ICAL „ Multiplr: 1.00 MS Integration Paxams: RTEINT.P Quant Time: Mar 21 9:58'2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 _\• i\�\r r\w i'!\/\!l ']rf !\1rT\TAC']7'i T\ fv:-op V115C V.La 1.V111. 111U 111j VCil Abundance TIC: A45323.0 2700000- 2600000- 2500000' 70000028000002500000 2400000 F 2300000 2200000 _f 2100000 4`E 2000000 1900000 1800000 e ~ M 1700000 • 1600000- 1500000 800000 1500000 F a 6- 0. U. cc ec o 1400000 ' o 1• w c 9L c • i °a o 1300000 B d Mc 1200000 ° 8 ` E y F F 3P. 1100000 N • C • F r 1000000 d K c 900000 a~ r ° c s 4 w 800000 �' r 6.2 { " 700000 c r• s i C• o 600000 O r _ C OA G O= L p 4.A F ~ O ~ aE a i t SL 500000 r v=E 4 9 400000 E •?- � 300000 0.2 200000 f o 100000 0 4 -AL—lui nn,pa 6_ a. D 10.00 12.00 11100 16.00 400 20.00 22.00 24.00 A45323:D PUHW032O.M Mon Mar 27 10:07:51 2006 H5971 Page 4 Quantitation Report (QT Reviewed). Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D Vial: 11 Acq On : 21 Mar 2006 00:12 Operator: tm Sample VSTD050 Inst H5971 Misc ,,,ICAL „ Multiplr:' 1.00 MS Integration Params: RTEINT.P Chlorobenzene-d5 14.15 Quant Time: Mar 21 9:58 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 09:54:28 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9:34 168 605212 50.00 UG/L 0.00 35) 1,4-Difluorobenzene .10.32. 114 1016422 50.00 UG/L 0.00 57') Chlorobenzene-d5 14.15 82 557357 50.00 UG/L 0.00 70) 1,.4 -Dichlorobenzene -d4 17.39 152 458982 50.00 U.G/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.88 65 507848 50.00 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery. = 100.000 55) Toluene -d8 12.20 98 1351127 50.00 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 10.0.00% 56) 4-Bromofluorobenzene 15.73 .95 601240 50.00 UG/L 0.00 Spiked Amount 50.000 Range. 86 - 115 Recovery = 100.00% Target Compounds Qvalue 2) Chlorodifluoromethane 4.27 51 40760 50.00 UG/L # 71 3) Dichlorodifluoromethane 4.,30 85. 52946 50.00 UG/L 94 4) Chloromethane 4.52 50 172001 50.00 UG/L 99 5) Vinyl chloride 4.77 62 183268 50.00 UG/L 97 6) Bromomethane 5.40 94 128867 50.00 UG/L 99 7) Chloroethane 5.53 64 139088 50.00 UG/L 99 8) Acetone 6.71 43 60720. 50.00 UG/L 98 9) Acetonitrile 7.13 41 585264 250.00 UG/L 100 10) Allyl Chloride 7.13 41 585264 50.00 UG/I; # 100 11) Acrolein 6.52 56 138073 250.00 UG/L 99 12) Acrylonitrile 7.' 61 53 91502 50.00 UG/L 95 13) Iodomethane 6.93 142 307018. 50.00 UG/L 100 14) Vinyl acetate 8..13 43 354238 50.00 UG/L 100 16) 2-Butanone .8.83 43 107437 50.00 UG/L 100 17) Tetrahydrofuran. 9.23 42 88234 50.00 UG/L # 100 18) Freon -113 6.63 101 159718 50.00 UG/L 97 19) Carbon disulfide 7.05 76 818532 50.00 UG/L # 68 20) Trichlorofluoromethane 5.91 101 255632 50.00 UG/L 100 21) 1,1-Dichloroethene 6.66 96 183142 50.00 UG/L 99 22) methyl tert-butyl ether 7.57 73 782975 50.00 UG/L 99 24) Methylene chloride 7.31 84 280315 50.00 UG/L 99 25) trans-1,2-Dichloroethene 7.64 96 262214 50.00 UG/L 100 26) 1,1-Dichloroethane 8.18 63. 652545 50.00 UG/L 100 27) Propionitrile 8.96. 54 31710 50.00 UG/L 98 29) Methacrylonitrile 9.13 67 107853 50.00 UG/L 94 30) cis-1,2-Dichloroethene 8.89 96 326350 50.00 UG/L 97 31) Bromochloromethane 9.21 128 125575 50.00 UG/L 98 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45323.D PUHW0320.M Mon Mar 27 10:07:45 2006 H5971 Page 1 d' 7t r-+ O O a V1 H Quantitation Report . (QT Reviewed) Data File : C:\HP.CHEM\1\DATA\MAR06\032006A\A45323..D Vial: 11 Acq On : 21 Mar 2006 00:12 Operator: tm Sample : VSTD050 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 MS Inte ration Params• RTEINT.P 33) Chloroform 9 Quant Time: Mar 21 9:58 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M '(RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 09:54:28 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue -----------------------------------------=-------------------------- 32.) 2,2-Dichloropropane 8.89 77 389254 50.00 UG/L 99 33) Chloroform 9.24 .83 578038 50..00 UG/L 100 34) 1,1,1 -Trichloroethane 9.50 97 450418 50.00 UG/L 99 37) 1,1-Dichloropropene 9.67: 75 386188 50.00 UG/L 99 38) Carbon tetrachloride 9.71 117 380475 50.00 UG/L 100 39) Benzene 9.96 78 1205162 50.00 UG/L 99 40) 1,2-Dichloroethane 9.98 62 481834 50.00-UG/L 100 41) Methyl Methacrylate 10.96 69 200487 50.00 UG/L 98 42) Trichloroethene 10.71 95 301582 50.00 UG/L 99 43) 1,2-Dichloropropane 11.02 63 415989 50.'00 UG/L # 34 44) Dibromomethane 11.20 93 190408 50.00 UG/L 98 47) Bromodichloromethane 11.33 83 467.974 50.00 UG/L 100 48) cis-1,3-Dichloropropene 11.84 75 628323 50.00 UG/L 100 49) Toluene 12.29 92 812875 50.00 UG/L 99 50) Ethyl Methacrylate 12.46 69 409289 50.00 UG/L 100 51,) trans-1,3-Dichloropropene 12.52 75 555991 50.00 UG/L 100 52) 1,1,2 -Trichloroethane. 12.81 83 230667. 50.00 UG/L 100 53) 1,2-Dibromoethane 13.60 107 317444 50.00 UG/L 99 54) 4-Methyl-2-pentanone 11.94 43 266333 50.00 UG/L 100 58) Chlorobenzene 14.19 112 987084 50.00 UG/L 99 59) 1,3-Dichloropropane 13.05 76 512324 50.00 UG/L 100 60) Tetrachloroethene 13.02 164 292378 50.00 UG/L 99 61) Dibromochloromethane 13.39 129 323511 50.00 UG/L 100 62) 2-Hexanone 12.99 43 186206 50._00 UG/L 99 63) 1,1,1,2 -Tetrachloroethane 14.27 131 295319 50'.00 UG/L 99 64) Ethylbenzene 14.24 106 489225 50.00 UG/L 99 65) m,p-Xylene 14.38 106 1236617 100.00 UG/L 99 66) o -Xylene 14.96 106 645520 50:00 UG/L 99 67) Xylene (total) 14.96 106 645520 50.O0.UG/L 99 68) Styrene 14.98 104 1104197 50.00 UG/L 100 69) Bromoform 15.38 173 244987 50.00 UG/L 99 71) trans-1,4-Dichloro-2-buten 15.92 53 104793 50.00 UG/L 93 72) 1,1,2,2 -Tetrachloroethane 15.88 83 329247 50.00 UG/L 100 73) Pentachloroethane 16.85 167 151449 50.00 UG/L 98 74) 1,2,3-Trichloropropane 12.52 112 83990 50.00 UG/L # 93 75) Isopropylbenzene 15.42 105 1384505 50.00 UG/L 100 76) Bromobenzene 16.02 156 355929 50.00 UG/L 100 77) n-Propylbenzene 15.99 91 1620695 50.00 UG/L 100 7t 78) 2-Chlorotoluene/4-Chloroto 16.37 91 2355172m 100.08 UG/LT-r- 79) 1;3,5-Trimethbenz/P-ethylt 16.20 105 2513662m 99.96 UG/L 80) tert-Butylbenzene 16'.70 119 1082331 50.00 UG/L 99 O O ----------------------------------------------------------------------- .(#) = qualifier out of range (m) = manual integration A45323.D PUHW0320.M Mon Mar 27 10:07:46 2006 H5971 Page 2' H Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D Vial: 11 Acq On : 21 Mar 2006 00:12 Operator: tm Sample : VSTDO50 Inst H5971 Misc : ICAL „ Multiplr: 1.00. MS'Integration Params: RTEINT.P Quant Time: Mar 21 9:58 2006 Quant Result's File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS'PLUS Last Update : Tue Mar 21 09:54:28 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 ----------------------=-------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45323.D PUHW032b.M Mon Mar 27 10:07:47 2006 H5971 .Page 3 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 81) 1,2,4-Trimethylbenzene 16.76 105 1335040 50.00 UG/L 100 82) sec-Butylbenzene 17.01 105 1530980 50.00 UG/L 100 83) 4-Isopropyltoluene 17.17 119 1154602 50.00 UG/L 99 84) 1,3 -Dichlorobenzene 17.31 146 648920 50.00 UG/L 100 85) 1,4 -Dichlorobenzene 17:43 146 647345 50.00 UG/L 99 86.) 1,2 -Dichlorobenzene 18.01 146 •614719 50.00 UG/L 100 87) p-Diethylbenzene 17:72 119 587459 50.00 UG/L 100 88) n-Butylbenzene 17.78 91 1307336 50.00 UG/L 96 89) 1,2-Dibromo-3-chloropropan 19'.24 75 52724 50.00 UG/L 99 90) 1,2,4,5-Tetramethylbenzene 18.93 119 951282 50.00 UG/L 100 .91) 1,2,4-Trichlorobenzene 20.61 180 429570 50.00 UG/L 99 92) Hexachlorobutadiene 20.77 225. 180914 5D.'00 UG/L 100 93) Naphthalene 21.13 128 579753 50•.00 UG/L 100 94,) 1,2,•3-Trichlorobenzene 21.58 180 257063 50.00 UG/L 99 ----------------------=-------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45323.D PUHW032b.M Mon Mar 27 10:07:47 2006 H5971 .Page 3 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45324.D Vial: 12 Acq On : 21 Mar 2006 00:44 Operator: tm Sample : VSTD100 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00, MS Integration Params: RTEINT.P Quant Time: Mar 21 10:03 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\l\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last'Update : Mon Mar 27 09:22:50 2006 I _ _ \ TTnnTTnIA\ \ TIT TT\TvIT D(1ti� (1 2i(1 flFZ1� DQ riii� _ f xesponse V.L ct l CJlll 111U1111, l Q1 L i ...� - — Nb—un—cra—ncee 4600000 4400000- �m . 4200000. SL � 2400000 F 4000000 n 1800000 a N C 3800000 -N O a a 0 2200000 F co 3600000 N 3400000 F� 3200000 ~ F t �} 3000000 ~ 2800000 Qs V 0 K A45324.D PUHW0320.M Mon Mar 27 10:08:16 2006 H5971 Page 4 F-+ zs00000 e i` o . �m . SL � 2400000 H [N n 1800000 o -N ~AL F 2200000 F co ~ ~ ~ S 2000000 ~ F Qs V 0 K A45324.D PUHW0320.M Mon Mar 27 10:08:16 2006 H5971 Page 4 F-+ � n 1800000 ~AL F a 0 Q P, F co 1600000 s F 1400000 e U2 F r 1200000 ' 'J e . ; -118� ° § ►- 1000000 r 4 = Q� i E '- o � R E 800000 E 4w�t A q e _ o � 600000 • a .0-00 e i $ 0' 200000 C 0 10.00 12 OD 14.00 16.00 18.00 Qs V 0 K A45324.D PUHW0320.M Mon Mar 27 10:08:16 2006 H5971 Page 4 F-+ Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\03:2006A\A45324.D Vial: 12 Acq On : 21 Mar'2006 00:44 Operator: tm Sample : VSTD100 Inst : H5971 Misc : ,,,ICAL ., Multiplr: 1.00 MS Integration Params: RTEINT.P 57) Quant Time: Mar 21 10:03 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene. 9.34 168 597037 50.00 UG/L 0.00 35)'1,4-Difluorobenzene 10.32 114 1002077 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 .546833 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 448319 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 469032 46.84 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.68% 55) Toluene -d8 12.20 98. 1199039 45.01 UG/L 0.00 . Spiked Amount 50.000 Range 88 - 110 Recovery' = 90.02% 56) 4-Bromofluorobenzene 15.73 95' 534352 45:07 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 90.14% Target Compounds Qvalue 2) Chlorodifluoromethane 4.29 51 79051 98.30 UG/L 91 3) Dichlorodifluoromethane 4.27 85 101426 97.09 UG/L 99 4) Chloromethane 4.53 50 331846 97.79 UG/L 100 5) Vinyl chloride 4.77 62 362588 100.28 UG/L 99 6.) Bromomethane 5.39 94 264900 104.19 UG/L 98 7) Chloroethane 5.54 64 279040 101.68 UG/L 99 8) Acetone 6.71 43 125257 104.56 UG/L 99 9)' Acetonitrile 7.13 .41 1211923 524.77. UG/L 98 10) Allyl Chloride 7.13 41 1211923 104.95 UG/L # 100 11).Acrolein 6.51 56 289263. 530.92 UG/L 100 12) Acrylonitrile 7.60 53- 203192 112:55 UG/L 97 13) Iodomethane 6.93 142 659824 108.93 UG/1- 97 14.) Vinyl acetate 8.12 43 826130 118.20 UG/L 100 16) 2-Butanone 8.84 43 234219 110.50 UG/L 99 17) Tetrahydrofuran 9.23 42 134521 77.27 UG/L # .100 18) Freon -113 6.63 101 301658 95.73 UG/L ' . 95 19) Carbon disulfide 7.05 76 1755860 108.73 UG/L'# 68 20) Trichlorofluoromethane 5.90 101 493578 97.86 UG/L 99' 21) 1,1-Dichloroethene 6.66 96 349066 96.60 UG/L 99 22) methyl tert-butyl ether 7.57 73 1597156 103.39 UG/L 98 24) Methylene chloride 7.31 84 541953 97.99 UG/L 98 25) trans-1,2-Dichloroethene 7.64 96 499085 96.47 UG/L 99 26) 1,1-Dichloroethane 8.18 63 1235074 95.93 UG/L 99 op 27) Propionitrile 8.96 54 74744 119.47 UG/L 99 29) Methacrylonitrile 9.13 67 254378 119.54 UG/L 96 30) cis-1,2-Dichloroethene 8.89 96 613324 95.25 UG/L 97 31) Bromochloromethane 9.20 128' 239817 96.80 UG/L 97 O --=---------------------------------------------------------------------- a (#) = qualifier out of range (m) = manual integration A45324.D PUHW0320.M Mon.Mar 2.7 10:08:08 2006 H5971 Page l [� Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032006A\A45324.D Vial: 12 Acq On 21 Mar 2006 00:44 Operator: tm Sample VSTD100 Inst H5971 Misc ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT-P Quant Time: Mar 21 10:03'2006 Quant Results File: PUHW0320.RES Quant Method : C:.\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART3.60E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue ---------------------------------------------------------------------- 32) 2,2-Dichloropropane 8.89 77 736962 95.96 UG/L 99 33) Chloroform 9.24_ 83.' 1116121 97.87 UG/L 99 34) 1,1,1 -Trichloroethane. 9.50 97 865934 97.44 UG/L 99 37) 1,1-Dichloropropene 9.67 75 716049 94.03 UG/L 98 38) Carbon tetrachloride 9.70 117 708664 94.45 UG/L 99 39) Benzene 9.96 78 2260809 95.14 UG/L 100 40) 1,2-Dichloroethane 9.98 62 928522 97.73 UG/L 100 41) Methyl Methacrylate 10.96 69 462144 116.91 UG/L. # 87 42) Trichloroethene 10,70 95 575409 96.76 UG/L 98 43) 1,2-Dichloropropane 11.01 63 761414 95.27 UG/L # 34 44) Dibromomethane. 11:20 93 376695 100.33 UG/L 99 47) Bromodichloromethane 11.33 83 918085 99.50 UG/L 99 48) cis-1,3-Dichloropropene .. 11.85 75 1208034 97.51-UG/L 100 49) Toluene 12.29 92 1504123 93:84 UG/L 100 50) Ethyl Methacrylate 12.46 69 936831 116.08 UG/L 98 51)'trans-l;3-Dichloropropene 12.52 75 1074158 97.98 UG/L 99 52) 1,1,2 -Trichloroethane 12.81 83 441295 :97.03 UG/Z 99 53) 1,27Dibromoethane 13.60 107 616172 98.44 UG/L 100 54') 4-Methyl-2-pentanone 11.94 43 595547 113.41 UG/L 99 58) Chlbrobenzene 14.19 112 1814285 93.67 UG/L 100 59) 1,3-Dichloropropane 13.05 76 968747 96.36 UG/L 100 60) Tetrachloroethene 13.02. 164 430637 75.06 UG/L. 10:0 61) Dibromochloromethane 13.39 129 640201 100.85 UG/L 100 . 62) 2-Hexanone 12.99 43. 403177 110.34• UG/L 98 63) 1,1,1,2 -Tetrachloroethane 14.27 131' 552286 95.31 UG/L 98 64) Ethylbenzene 14.24 106 864980 90.10 UG/L 98 65) m,p-Xylene 14.39 106 2148548 177.09 UG/L 98 66) o -Xylene 14.96 106 1142014 90.16 UG/L 98 67) Xylene (total) 14.96 106 1142014 90.16 UG/L 98 68) Styrene. 14.98 104 1963927 90.64 UG/L. 98 69) Bromoform 15.38 173 483006 100.48 UG/L' 99 71) trans-1,4-Dichloro-2-buten 15:92 53 227759 111.26 UG/L 93 72.) 1,1,2,2 -Tetrachloroethane 15.88 83 637298 99.08 UG/L 99 73) Pentachloroethane 16.85 167 469102 158.55 UG/L 99 74) 1;2,3-Trichloropropane 12.52 112 158613 96.67 UG/L # 91 75) Isopropylbenzene 15.42 105 2511954 92.87. UG/L 100 76) Bromobenzene 16.02 15.6 645962 92.90 UG/L 100 77).n-Propylbenzene 15.99 91 2897528. 91.52 UG/L 99 d' 78) 2-Chlorotoluene/4-Chloroto 16.37 91 4357732m 189.59 UG/L 79) 1,3,5-Trimethbenz/P-ethylt 16.14 105 4756438m 193.65 UG/I, 80.) tert-Butylbenzene 16.70 119 1957468 92.58 UG/L. 99 O O ----------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45324.D PUHW0320.M Mon Mar 27 10:08:09 2006 H5971 Page 2 Quantitation Report *(QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45324.D ..Vial: 12 Acq On : 21 Mar 2006 00:44 Operator: tm Sample : VSTD100 Inst : H5971 2464733 94.50 Multiplr: 1.00 Misc : ,,,ICAL „ sec-Butylbenzene 17.01 • RTEINT P 2749569 91.93 MS Integration Params. Quant Time: Mar 21 10:03 2006 Quant Results File: PUHW03.20.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART3609 ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue 81) ------------------------------------------- 1.,2,4-Trimethylbenzene 16..77 105 2464733 94.50 UG/L 99 82) sec-Butylbenzene 17.01 105 2749569 91.93 UG/L 99 83) 4=Isopropyltoluene 17.18 119 2099431 93.08 UG/L 99 84) 1,3 -Dichlorobenzene 17.31 146 1194964 94.26 UG/L 100 85) 1,4 -Dichlorobenzene 17.43 146 1196598 94.62 UG/L 99 86) -1,2 -Dichlorobenzene 18.01 146 1144100. 95..27 UG/L 99 87) p-Diethylbenzene 17.73 119. 1187702 103:49 UG/L 97 88) n-Butylbenzene 17.78 91 2414759 94.55 UG/L 97 89) 1,2=Dibromo-3-chloropropan 19.24 75 102860 99.87 UG/L 98 90) 1,2,4,5-Tetramethylbenzene 18.93 119 1912753 102.93 UG/L 99 91) 1,2,4-Trichlorobenzene 20.61 180 837672 99.82 UG/L 100 92) Hexachlorobutadiene 20.77 225 317353 89.79 UG/L 100 93) Naphthalene 21.13 128 1133212 100.06 UG/L 100 94) 1,2,3-Trichlorobenzene 21.58 180 505330 100.63 UG/L 100 O V� O . (#) =qualifier out of range (m) ----------------------------=------------ =manual integration CD A45324.D PUHW0320.M Mon Mar 27 10:08:10 2006 H5971 .Page 3 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45325.D Vial: 13 Acq.On : 21 Mar 2006 1:16 Operator: tm Sample : VSTD200 Inst : H5971 Misc : ,,,ICAL, Multiplr: 1..00' MS Integration Params: RTEINT:P Quant Time: Mar 21 10:03 2006 Quant.Results File: PUHW0320.RES Method C\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Continuina Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D 8500000 8000000• 7000000 6500000 6000000 5500000 5000000 4500000 4000000 3500000 3000000 2500000 2000000 1500000 1000000 500000 'rl7me-> D Y A45325.D PUHW0320.M Mon Mar 27.10:08:41 2006 H5971 O O CA Page 4 [--i Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\0320.06A\A45325.D Vial.: 13 Acq On : 21 Mar 2006 1:16 Operator: tm Sample : VSTD200 Inst H5971 Misc : ,,,ICAL,, Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:03 2006 Quant Results File:- PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth.: PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 620308 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1029504 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 551374 50.00 UG/L 0.00 70) 1,,4 -Dichlorobenzene -d4 17.40 152 447362 50.00 UG/L 0.00 System Monitoring Compounds 36). 1,2-Dichloroethane-d4 9..89 65 1708469 166.07 UG/L 0.00 Spiked Amount 50.000 Range 76 ='114 Recovery = 332.14%# 55) Toluene -d8 - 12.19 98 4169182 152.32 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 304.6.4%# 56) 4-Bromofluorobenzene 15.73 95 1902806 .15.6.23 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 312.46%# Target Compounds Qvalue 2) Chlorodifluoromethane 4.28 51 199705 239.01 UG/L 94 3) Dichlorodifluoromethane 4.25. 85 222966 205.44 UG/L 99 4) Chloromethane 4.53 50 675901 191.70 UG/L 98 5) Vinyl chloride 4.79 62 747816 199.06.UG/L 99 6) Bromomethane 5.39 94 547139 207.12 UG/L 98 7) Chloroethane 5.54 64 571246 200.36 UG/L 99 8) Acetone 6.70 ' 43 253141 203.38 UG/L 98 9) Acetonitrile 7.13 41 2383575 993.38 UG/L 96 10) Allyl Chloride 7.13 41 2383575 198.68 UG/L # 100 11) Acrolein 6.52 56 602341 1064.08 UG/L 100 12) Acrylonitrile 7.61 53 393848. 209.98 UG/L 97 13) Iodomethane 6.93 142 1382243 219.63 UG/L 96 14.) Vinyl acetate -8.12. 43 1675986 230.81 UG/L 99 16) 2-Butanone 8:83 43 451924 205.20 UG/L 96 17) Tetrahydrofuran 9.24 42 273302 151.10 UG/L # 100 18) Freon -113' 6'.62 .101 669663 204.54 UG/L 95 19) Carbon disulfide 7.05 76 3642868 217.11 UG/L # 68 20), Trichlorofluoromethane 5.89 101 1079980 206.10 UG/L 99 21) 1,1-Dichloroethene 6.65 96 728965 19.4.17 UG/L 98 22) methyl tent -butyl ether 7.57 73 3396909 211.64 UG/L 98 24) Methylene chloride 7.30 84 1110795 193.31 UG/L 95 25) trans-1,2-Dichloroethene 7.64 .96 1007944 187.52 UG/L 99 26) 1,1-Dichloroethane 8.18 63 2485551 185.82 UG/L 98 27) Propionitrile 8.96: 54 147128 226.34 UG/L 95 29) Methacrylonitrile 9.13 67 501881 227.01 UG/L 94 30) cis-1,2-Dichloroethene 8.88 .96 1197294 178.97 UG/L 97 31) Bromochloromethane 9.21 128 481228 186.95 UG/L 93 = qualifier out of range (m) = manual integration A45325.D PUHW0320.M Mon Mar 27 10:08:35 2006 H5971 Page 1 Quantitation Report (QT Reviewed) Data File.: C:\HPCHEM\1\DATA\MAR06\032006A\A45325.D Vial: 13' Acq On : 21 Mar 2006 1:16 Operator: tm Sample : VSTD200 Inst H5971 Misc . ,,kICAL,, Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 21 10:03 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 ------------------------------------------------------------------------- Compound R.T. QIon Response Conc Unit Qvalue 32) 2,2-Dichloropropane 8.88 77. 1462736 183.32 UG/L 99 33) Chloroform 9.24 83 2241111 189.14 UG/L. 99 34) 1,1,.1 -Trichloroethane 9.50 97 1806812 195.69 UG/L 98 37) 1,1-Dichloropropene 9.68 .75 1480738 189.28 UG/1 99 38) Carbon tetrachloride 9.71 117 1537341 199.46 UG/L 99 39) Benzene 9.97 78 4375429 179.22 UG/L 99 40) 1,2-Dichloroethane 9.99 62 1809457 185.38 UG/L 99 41) Methyl Methacrylate 10.95 69 900718 221.78 UG/L # 88 42) Trichloroethene 10..70 95. 1181637 193.42 UG/L 97 43) 1,2-Dichloropropane 11.01 63' 1533043 181.92 UG/L # 34 44) Dibromomethane 11.21 93 .759962 197.03 UG/L 98 47) Bromodichloromethane 11.33 83 1848754 195.02 UG/L 99 48) cis-1,3-Dichloropropene 11.85 75 2396509 188.28 UG/L 100 49) Toluene 12.29 92 2929290. 177.89 UG/L 58 50) Ethyl Methacrylate 12.47 69 1794429 216.43 UG/L 97 51) trans-1,3-Dichloropropene 12.53 75 2136807 189.72 UG/L' 99 52) 1,1,2 -Trichloroethane 12.80 83 869786 186.14 UG/L• 100 53) 1,2-Dibromoethane 13..60 107 1245247 193.64 UG/L 99 54) 4-Methyl-2-pentanone 11.94 43 1126455 208.79 UG/L 98 58). Chlorobenzene 14..19 112 3505128 179.48 UG/L 99 59) 1,3-Dichloropropane 13.04 76 1860237 183.52 UG/L 99 60) Tetrachloroethene 13.02 164 856197 148.01 UG/L 100 61) Dibromochloromethane 13.40 129 1313648 205..23 UG/L 100 62) 2-Hexanone 12.99 43' 750679 203.76 UG/L 97 63) 1,1,1,2 -Tetrachloroethane 14.27 131 1090776 186.68 UG/L 97 64) Ethylbenzene 14.24 10.6 1613905 166.73 UG/L 97 65) m,p-Xylene 14.38 106 4023147 328.•87 UG/L 99 66) o -Xylene 14.96 106 2120886 166.06 UG/L 97 67) Xylene (total) 14.96 106 2120886 166.06 UG/L 97 68) Styrene 14.98 104 3630645 166.19 UG/L' 97 69) Bromoform 15.38 173 993904 205.05 UG/L 99 71) trans-1,4-Dichloro-2-buten 15.93 53 437903 214.36 UG/L 89 72) 111,2,2 -Tetrachloroethane 15.88 83 1250100 194.77 UG/L 99 73) Pentachloroethane 16.86 167 925102 313..35 UG/L 96 74) 1,2,3-Trichloropropane 12.53 112 317262 193.77 UG/L # 93 75) Isopropylbenzene 15.43 105 4841959 179.40 UG/L 99 76) Bromobenzene 16.02 156 1226074 176.71 UG/L 98 77) n-Propylbenzene 16.00 91 5376156 170.17 UG/L 99 78) 79) 2-Chlorotoluene/4-Chloroto 16.37 91 8271792m 360.64 UG/L -rT- 1,3,5-Trimethbenz/P-ethylt 16.15 105 8820891m 359.89 UG/L 80) tert-Butylbenzene 16:71 119 3816483 180.89 UG/L 99 #) -------------------------------=---------- qualifier out of range (m) = manual integration a45325.D PUHW0320.M Mon Mar 27 10:08:36 200.6 H5971 Page 2 Quantitation Report- (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45325.D Vial: 13 Acq On : 21 Mar 2006 1:16 Operator: tm Sample : VSTD200 Inst H5971 Mi,sc • : , , , ICAL, , Multiple : 1.00 MS Integration Params: RTEINT.P. .Quant Time: Mar 21.10:03 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M ,(RTE Integrator) Title : WATER PART3609 ORGANICS PLUS Last Update : Tue Mar 21 10:00:31 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032006A\A45323.D DataAcq Meth : PUHW0320 Compound ------------------------------------------- R.T. QIon Response Conc Unit Qvalue 81) 1,2,4-Trimethylbenzene 16.78 105 -------- 4656223 ------------- 178.91 UG/L 9.8 82) sec-Butylbenzene 17.01 105 5308842 177..88 UG/L 99 83) 4-Isopropyltoluene_ 17.17 119 4056053 180.21 UG/L 99 84) 1,3 -Dichlorobenzene 17.32 146 2279582 180.21 UG/L 98 85) 1,4 -Dichlorobenzene 17.44 146 2297454 182.06 UG/L 98 86) 1,2 -Dichlorobenzene 18.02 146 2223710 185.57 UG/L 98 87) p-Diethylbenzene 17:72 119 2235132 195.18 UG/L 98 88) n-Butylbenzene 17.77 91 4621312 181.34 UG/L'# 49 89) 1,2-Dibromo-3-chloropropan 19.24 75 218394 212.49 UG/L 98 90) 1,.2,4,5-Tetramethylbenzene 18.94 119 3652402 196.96 U.G/L 98 91) 1,2,4-Trichlorobenzene 20.61 180 171010.6 204.22 UG/L 98 92) Hexachlorobutadiene 20.78 225 685.833 194.47 UG/L 100 93) Naphthalene 21.12 128 .2365501 209.31 UG/L 100 94) 1,2,3-Trichlorobenzene 21.59 180. 1026618 204_67 UG/L 100 ------------------------------ (#) = qualifier out of range (m) = manual integration A45325.D PUHW0320.M Mon Mar 27 10:08:37 2006 H5971. Page .3 7A VOLATILE CONTINUING CALIBRATION CHECK Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Instrument ID: HP5971 Calibration Date: 03/23/06 Time: 10:01 Lab File ID: A\A45398.D Init. Calib. Date(s): 03/20/06 03/21/06 EPA Sample No.(VSTD050##): VSTD050 Init. Calib. Times: 23:09 1:16 Heated Purge: (Y/N) N GC Column: R-502.2 ID: .53 (mm) COMPOUND RRF RRF50 MIN RRF WD MAX %D Chloromethane 0.289 0.276 -4.4 Vinyl chloride 0.311 0.306 0.100 -1.7 25.0 Bromomethane 0.229 0.203 0.100 -11.3 25.0 Chloroethane 0.238 0.220 -7.6 Acrylonitrile 0.170 0.144 -15.4 Trichlorofluoromethane 0.408 0.491 20.3 1,1-Dichloroethene 0.304 0.360 0.100 18.5 25.0 lodomethane 0.547 0.559 2.3 Vinyl acetate 0.643 0.639 -0.7 Acetone 0.115 0.091 -20.6 Carbon disulfide 1.458 1.575 8.0 Methylene chloride 0.474 0.448 -5.4 trans-1,2-Dichloroethene 0.432 0.452 4.6 1,1-Dichloroethane 1.066 1.034 0.200 -3.0 25.0 cis- 1,2-Dichloroethene 0.536 0.532 -0.8 2-Butanone 0.204 0.172 -15.8 Bromochloromethane 0.213 0.200 -6.0 Chloroform 0.974 0.880 0.200 -9.6 25.0 1,1,1 -Trichloroethane 0.727 0.772 0.100 6.2 25.0 Carbon tetrachloride 0.356 0.367 0.100 3.1 25.0 Benzene 1.190 1.128 0.500 -5.2 25.0 1,2-Dichloroethane 0.485 0.402 0.100 -17.1 25.0 Trichloroethene 0.294 0.302 0.300 2.9 25.0 1,2-Dichloropropane 0.412 0.377 -8.5 Dibromomethane 0.198 0.168 -15.3 Bromodichloromethane 0.477 0.408 0.200 -14.5 25.0 cis-1,3-Dichloropropene 0.637 0.551 0.200 -13.5 25.0 4-Methyl-2-pentanone 0.314 0.239 -23.8 Toluene 0.788 0.808 0.400 2.5 25.0 trans- 1,3-Dichloropropene 0.572 0.474 0.100 -17.1 25.0 1,1,2 -Trichloroethane 0.242 0.202 0.100 -16.4 25.0 Tetrachloroethene 0.437 0.589 0.200 34.8 25.0 2-Hexanone 0.400 0.296 -26.0 Dibromochloromethane 0.616 0.511 0.100 -17.1 25.0 1,2-Dibromoethane 0.330 0.279 -15.5 All other compounds must meet a minimum RRF of 0.010. FORM VII VOA - 1 OLM04.2 7B VOLATILE CONTINUING CALIBRATION CHECK Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Instrument ID: HP5971 Calibration Date: 03/23/06 Time: 10:01 Lab File ID: A\A45398.D Init. Calib. Date(s): 03/20/06 03/21/06 EPA Sample No.(VSTD050##): VSTD050 Init. Calib. Times: 23:09 1:16 Heated Purge: (YIN) N GC Column: R-502.2 ID: .53 (mm) COMPOUND RRF RRF50 MIN RRF %D MAX %D Chlorobenzene 1.760 1.783 0.500 1.3 25.0 trans-1,4-Dichloro-2-butene 0.268 0.208 -22.4 Ethylbenzene 0.852 0.945 0.100 10.9 25.0 1,1,1,2 -Tetrachloroethane 0.535 0.493 -7.9 Xylene (total) 1.139 1.192 0.300 4.7 1 25.0 Styrene 1.957 1.998 1 0.300 2.1 25.0 Bromoform 0.466 0.382 0.100 -18.0 25.0 1,1,2,2 -Tetrachloroethane 0.785 0.637 0.300 -18.8 25.0 1,2,3-Trichloropropane 0.193 0.166 -13.8 1,4 -Dichlorobenzene 1.417 1.405 -0.9 1,2 -Dichlorobenzene 1.362 1.319 -3.1 1,2-Dibromo-3-chloropropane 0.125 0.097 -22.5 110 All other compounds must meet a minimum RRF of 0.010. O O FORM VII VOA - 2 OLM04.2 E C/1 I= 7B VOLATILE CONTINUING CALIBRATION CHECK Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Instrument ID: HP5971 Calibration Date: 03/23/06 Time: 10:01 Lab File ID: A\A45398.D Init. Calib. Date(s): 03/20/06 03/21/06 EPA Sample No.(VSTD050##): VSTDO50 Init. Calib. Times: 23:09 1:16 Heated Purge: (Y/N) N GC Column: R-502.2 ID: .53 (mm) COMPOUND RRF RRF50 MIN RRF %D MAX %D' 1,2-Dichloroethane-d4 0.397 0.395 -0.4 Toluene -0 1.041 1.233 18.5 4-Bromofluorobenzene 0.466 0.518 0.200 11.2 25.0 All other compounds must meet a minimum RRF of 0.010. W) O O FORM VII VOA - 3 OLM04.2 i i Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Vial: 2 Acq On : 23 Mar 2006 10:01 Operator: tm Sample : VSTDO50 Inst : H5971 Misc : ,,,CCV„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 10:50 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 nesponse via : Continuing uai Flie: u:\riYGHt;M\i\DA'1'A\MARU6\U323UbA\A453yt3.D nunaance _T1ClV453 2700000 2600000 2500000 2400000 r d 2300000 e 2200000 My —n. 2100000 2000000 N€ k 1900000- 9000001800000 1800000. H 1700000 d � — 1600000 N d o� 8 i md 1500000 H k „� 8 1400000 u a'p U _y O p xi u e 1300000 5 ti O u $ a ,nE 1200000. 3 r 1100000 o17 1000000 a2 oNCNau RvoO Ui Fao0 C900000 ga $_ou c 800000 s " ~uo - 'arNa 700000 r~kma f►nd- `C e ad; � o Fai 60000 v C d Q' �s 50000 EE a Z CL no� 10 Z 400.000 +a E a 300000 1s e 4seu 200000 �r V� W7 100000G U 'B. ,rime—> 6.60' bo 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 00 O O A45398.D PUHW0320.M Mon Mar 27 09:25:10 2006 H5971 Page 4 F-+ Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Vial: 2 Acq On : 23 Mar 2006 10:01 Operator: tm Sample : VSTD050 Inst : H5971 Misc . ,,,CCV„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 10:50 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.33 168 586456 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.31 114 1028946 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 551788 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 463680 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.88 65 406918 50.00 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 100.00% 55) Toluene -d8 12.19 98 1268302 50.00 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.00% 56) 4-Bromofluorobenzene 15.73 95 533257 50.00 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.00% .Target Compounds Qvalue 2) Chlorodifluoromethane 4.26 51 51231 50.00 UG/L # 94 3) Dichlorodifluoromethane 4.24 85 57993 50.00 UG/L 97 4) Chloromethane 4.50 50 161750 50.17.UG/L 99 5) Vinyl chloride 4.74 62 179266 50.00 UG/L 100 6) Bromomethane 5.37 94 118963 49.89 UG/L 100 7) Chloroethane 5.51 64 129306 50.00 UG/L 99 8) Acetone 6.69 43 53162 50.00 UG/L 98 9) Acetonitrile 7.12 41 503083 250.00 UG/L 97 10) Allyl Chloride 6.77 41 1869 50.00 UG/L 78 12) Acrylonitrile 7.60 53 84384 50.00 UG/L 96 13) Iodomethane 6.92 142 327559 49.98 UG/L 94 14) Vinyl acetate 8.11 43 374531 50.01 UG/L 100 16) 2-Butanone 8.82 43 100796 50.00 UG/L 97 17) Tetrahydrofuran 9.23 42 57651 50.00 UG/L 97 18) Freon -113. 6.60 101 193653 49.80 UG/L 100 19) Carbon disulfide 7.04 76 923936 50.00 UG/L # 100 20) Trichlorofluoromethane 5.88 101 287747 49.98 UG/L 99 21) 1,1-Dichloroethene 6.64 96 211385 50.00 UG/L 96 22) methyl tert-butyl ether 7.56 73 627440 50.00 UG/L 97 24) Methylene chloride 7.29 84 263019 50.00 UG/L 95 25) trans-1,2-Dichloroethene 7.63 96 264910 49.95 UG/L 98 26) 1,1-Dichloroethane 8.17 63 606617 50.00 UG/L 100 27) Propionitrile 8.95 54 30285 50.00 UG/L 97 29) Methacrylonitrile 9.12 67 102492 50.00 UG/L 93 30) cis-1,2-Dichloroethene 8.88 96 312128 50.00 UG/L 97 31) Bromochloromethane 9.20 128 117081 50.00 UG/L 96 32) ------------------------------------------------------------------------- 2,2-Dichloropropane 8.87 77 397573 50.00 UG/L 99 (#) = qualifier out of range (m) = manual integration A45398.D PUHW0320.M Mon Mar 27 09:25:04 2006 H5971 Page 1 Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Vial: 2 Acq On 23 Mar 2006 10:01 Operator: tm Sample VSTDO50 Inst H5971 Misc ,,,CCV„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 10:50 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 33) Chloroform 9.24 83 516054 50.00 UG/L 34) 1,1,1 -Trichloroethane 9.49 97 452457 50.00 UG/L 37) 1,1-Dichloropropene 9.67 75 408215 50.00 UG/L 38) Carbon tetrachloride 9.70 117 377583 50.00 UG/L 39) Benzene 9.96 78 1160570 50.00 UG/L 40) 1,2-Dichlcroethane 9.98 62 413931 50.00 UG/L 41) Methyl Methacrylate 10.95 69 179154 50.00 UG/L 42).Trichloroethene 10.69 95 310799 50.00 UG/L 43) 1,2-Dichloropropane 11.00 63 388227 50.00 UG/L 44) Dibromomethane 11.20 93 172518 50.00 UG/L 47) Bromodichloromethane 11.33 83 420257 50.00 UG/L 48) cis-1,3-Dichloropropene 11.85 75 566916 50.00 UG/L 49) Toluene 12.28 92 830971 50.00 UG/L 50) Ethyl Methacrylate 12.46 69 370690 50.00 UG/L 51) trans-1,3-Dichloropropene 12.52 75 487977 50.00 UG/L 52) 1,1,2 -Trichloroethane 12.80 83 207664 50.00 UG/L 53) 1,2-Dibromoethane 13.60 107 286864 50.00 UG/L 54) 4-Methyl-2-pentanone 11.94 43 245745 50.00 UG/L 58) Chlorobenzene 14.19 112 983653 50.01 UG/L 59) 1,3-Dichloropropane 13.04 76 451512 50.00 UG/L 60) Tetrachloroethene 13.02 164 325168 50.00 UG/L 61) Dibromochloromethane 13.39 129 281806 50.00 UG/L 62) 2-Hexanone 12.98 43 163407 50.00 UG/L 63) 1,1,1,2 -Tetrachloroethane 14.26 131 271825 50.00 UG/L 64) Ethylbenzene 14.24 106 521316 50.00 UG/L 65) m,p-Xylene 14.38 106 1292854 100.06 UG/L 66) o -Xylene 14.95 106 657984 50.00 UG/L 67) Xylene (total) 14.95 106 657984 50.00 UG/L 68) Styrene 14.97 104 1102705 50.00 UG/L 69) Bromoform 15.38 173 210973 50.00 UG/L 71) trans-1,4-Dichloro-2-buten 15.93 53 96508 50.00 UG/L 72) 1,1,2,2 -Tetrachloroethane 15.87 83 295468 50.00 UG/L 73) Pentachloroethane 16.85 167 139412 50.00 UG/L 74) 1,2,3-Trichloropropane 12.52 112 77195 50.00 UG/L 75) Isopropylbenzene 15.42 105 1468462 50.00 UG/L 76) Bromobenzene 16.02 156 347803 50.00 UG/L 77) n-Propylbenzene 15.99 91 1747039 50.00 UG/L 78) 2-Chlorotoluene/4-Chloroto 16.36 91 2388581m 100.14 UG/L 79) 1,3,5-Trimethbenz/P-ethylt 16.20 105 2500673m 99.98 UG/L 80) tert-Butylbenzene 16.70 119 1115476 50.00 UG/L 81) 1,2,4-Trimethylbenzene 16.77 105 1358932 50.00 UG/L 99 99 97 100 99 100 93 98 100 99 100 99 99 98 99 98 100 99 99 99 100 99 99 99 96 97 98 98 99 99 92 99 99 94 99 99 100 jj 99 99 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45398.D PUHW0320.M Mon Mar 27 09:25:05 2006 H5971 Page 2 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Vial: 2 Acq On : 23 Mar 2006 10:01 Operator: tm Sample : VSTD050 Inst : H5971 Misc : ,,,CCV„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 2.3 10:50 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 ------------------------------------------------------------------ Compound R.T. QIon Response Conc Unit 82) sec-Butylbenzene 17.00 105 1638840 50.00 UG/L 83) 4-Isopropyltoluene 17.17 119 1188586 50.01 UG/L 84) 1,3 -Dichlorobenzene 17.31 146 650276 50.00 UG/L 85) 1,4 -Dichlorobenzene 17.43 146 651611 50.00 UG/L 86) 1,2 -Dichlorobenzene 18.02 146 611572 50.00 UG/L 87) p-Diethylbenzene 17.72 119 571578 50.00 UG/L 88) n-Butylbenzene 17.77 91 1347885 50.00 UG/L 89) 1,2-Dibromo-3-chloropropan 19.23 75 45117 50.00 UG/L 90) 1,2,4,5-Tetramethylbenzene 18.94 119 875551 50.02 UG/L 91) 1,2,4-Trichlorobenzene 20.60 180 411680 50.00 UG/L 92) Hexachlorobutadiene 20.78 225 155195 50.00 UG/L 93) Naphthalene 21.12 128 554563 50.00 UG/L 94) 1,2,3-Trichlorobenzene 21.58 180 257796 50.00 UG/L Qvalue 100 99 100 99 99 99 97 98 99 99 99 100 99 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45398.D PUHW0320.M Mon Mar 27 09:25:06 2006 H5971 Page 3 U2M ILAI3S, INC. IV. RAW QC DATA PACKAGE FOR VOLATILE ORGANICS A. TUNING B. BLANK C. MATRIX SPIKE BLANK D. SPIKE AND SPIKE DUPLICATE E. COPY OF CALCULATIONS BFB Data File : C:\HPCHEM\1\DATA\MAR06\032006A\A45313.D Vial: 1 Acq On : 20 Mar 2006 17:47 Operator:.tm Sample : 50 ng BFB Inst H5971 Misc . ,,,TUNE„ Multiplr: 1.00 MS Integration Params: RTEINT.P Method : C:\HPCHE14\1\METHODS\PUHW0320.M (RTE. Integrator) Title : WATER PART360E.ORGANICS PLUS AutoFind: Scans 256, 257, 258; Background Corrected with Scan 244 I Target I Rel. to I Lower I Upper I Rel. I Raw I Result I I Mass I Mass I Limit% I Limit% I Abn% I Abn I Pass/Fail I ---------------------------------------------------------------------- I 50 I 95 I 15 I 40 18.0 I 7475 I PASS' I I 75 I 95 I 30 I 60 I 45.8 18971 I PASS I I 95 I 95 I 100 I 100 1100.0 41432 I PASS I I 96 I 95 I 5 I 9 1 6.9 2855 I PASS I I 173 I 174 I 0.00 I 2 1 0.0 I 0 1 PASS I I 174 I 95 I 50 I 100 I 79.5 I 32936 I PASS I I 175 I 174 I 5 I 9 I 7..1 I 2327 I PASS I I 176 I 174 I 95 I 101 i 100.9 I 33216"I PASS I I 177 ------------------------------------------------------------- I 176 i 5 1 9 1 6.5 I 2151 I 'PASS I 7-------- A45313.D PUHW0320.M Mon Mar 27 10:10:13 2006 H5971 BFB Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45397.D Vial: 1 Acq On : 23 Mar 2006 9:36 Operator: tm Sample : 50 ng BFB Inst : H5971 Misc : ,,,TUNE„ Multiplr: 1.00 MS Integration Params: RTEINT.P I 40 I 18.4 I Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) I 95 I Title : WATER PART360E ORGANICS PLUS 43.0 I 9973 I AutoFind: Scans 270, 271, 272; Background Corrected with Scan 262 I Target I Rel. to I Lower I Upper I Rel. I Raw I Result I I Mass ---------------------------------------------------------------------- I Mass I Limit% I Limit% I Abn% Abn I Pass/Fail I I 50 I 95 I 15 I 40 I 18.4 I 4269 I PASS I I 75 I 95 I 30 I 60 I 43.0 I 9973 I PASS i I 95 I 95 I 100 I 100 1100.0 I 23208 I PASS 1 96 I 95 I 5 1 9 1 6.4 I 1493 I PASS I I 173 I 174 I 0.00 I 2 1 0.2 I 41 I PASS I I 174 1 95 I 50 I 100 I 81.0 I 18805 I PASS I I 175 1 174 I 5 1 9 1 7.2 I 1359 I PASS I I 176 I 174 I 95 I 101 I 97.4 I 18323 I PASS I i 177 ---------------------------------------------------------------------- I 176 I 5 1 9 1 6.4 1 1167 I PASS I A45397.D PUHW0320.M Mon Mar 27 09:21:46 2006 H5971 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/m,) M, Level: (low/med) LOW % Moisture: not dec. Contract: SAS No.: GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (AL) CAS NO. COMPOUND SPA SAMPLE NO. VBLX032306 SDG No.: TSL005 Lab Sample ID: VBLK032306 Lab File ID: A\A45399.D Date Received: Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: I — /T. -- — /V-1 ttn_ /T. 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53' Soil Extract Volume: (u CAS NO. COMPOUND Contract: (mm L) EPA SAMPLE NO. VBLX032306 SAS No.: SDG No.: TSL005 Lab Sample ID: VBLK032306 Lab File ID: A\A45399.D Date Received: Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 108-90-7 Chlorobenzene 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U . 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET FVBLK032306 TENTATIVELY IDENTIFIED COMPOUNDS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: VBLK032306 Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45399.D Level: (low/med) LOW Date Received: Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q J FORM I VOA -TIC OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45399.D Vial: 3 Acq On 23 Mar 2006 10:34 Operator: tm Sample VBLK032306 Inst H5971 Misc ,,,MBLK„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 11:15 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 ResiDonse via : Continuina Cal File' n un ante TIC: A45399.D 1400000 1350000- 1300000-' m 1250000 d N C N q 1; 1200000 N 1150000 c h Q o` a 1100000 v 1050000 a 0 e 1000000 0 °P 950000 d 900000 H 0 850000 `0 12 800000 750000- 700000 d 650000 d a 600000 550000 d a 500000 450000 0 s` 400000 4 N 350000 300000 250000- 50000200000150000 200000- 150000- 100000 50000 D . LIU I �A­ A)U rime—> i . . . 6.60' 8.60' 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45399.D PUHW0320.M Mon Mar 27 09:24:46 2006 H5971 Page 2 LSC Report - Integrated Chromatogram File C:\HPCHEM\1\DATA\MAR06\032306A\A45399.D Operator tm Acquired 23 Mar 2006 10:34 using AcgMethod PUHW0320 Instrument H5971 Sample Name: VBLK032306 Misc Info : ,,,MBLK„ Vial Number: 3 Quant File :PUHW0320.RES (RTE Integrator) AbundanceA45399.13 1000000- 800000. 10.32 600000 9.34 400000 9.88 200000 0 7.31 4. Time--> 0 5. 0 5. 0 6. 0 6. 0 7. 0 7. 0 i.b6 i.66 6.b6 9. 0 10.00 10.50 11.00 un anceA45399.13 1 19 14.14 17.38 1000000 15.73 800000 600000 400000 200000 0 13.02 13.9 14.38 14.97 15.41 15AR111111.36 11M7.VA.17 1YIM8.01 !me--> 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 Abundance , 1000000 800000 600000 400000 200000 18.93 20.10.77 21.13 21.58 0 ime--> 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 22.50 23.00 23.50 24.00 24.50 25.00 nsJJ��. u rVRVVVJGV .1"1 lion mar z1 U..l: jo: qU LUUb HSy71 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45399.D Vial: 3 Acq On : 23 Mar 2006 10:34 Operator: tm j Sample : VBLK032306 Inst : H5971 Misc : ,,,MBLK„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 11:15 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) Pentafluorobenzene 9.34 168 616006 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1034999 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.14 82 564278 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 495499 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 Spiked Amount 50.000 55) Toluene -d8 Spiked Amount 50.000 56) 4-Bromofluorobenzene Spiked Amount 50.000 Target Compounds 9.88 65 394877 48.24 UG/L 0.00 Range 76 - 114 Recovery = 96.48% 12.19 98 1282688 50.27 UG/L 0.00 Range 86 - 115 Recovery = 100.54% 15.73 95 539858 50.32 UG/L 0.00 Range 88 - 110 Recovery = 100.64% Qvalue ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45399.D PUHW0320.M Mon Mar 27 09:24:44 2006 H5971 Page 1 Tentatively Identified Compound (LSC) summary -,aerator ID: tm Date Acquired: 23 Mar 2006 10:34 ?ta File: C:\HPCHEM\1\DATA\MAR06\032306A\A45399.D �4ame: VBLK032306 Misc: ,,,MBLK„ Method: C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A45399.D PUHW0320.M Mon Mar 27 09:35:41 2006 H5971 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mod) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Contract: (mm Soil Extract Volume: (gL) CAS NO. COMPOUND EPA SAMPLE NO. MW-5SMS SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-009AMS Lab File ID: A\A45411.D Date Received: 03/16/06 Date Analyzed: 03/23/06 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 53 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochlorcmethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 55 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 52 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 53 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 IB VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Matrix: (soil/water) WATER Lab Sample ID: Sample wt/vol: 5 (g/mL) ML Lab File ID: Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: GC Column: R-502.2 ID: .53 (mm) Dilution Factor: EPA SAMPLE NO. MW-5SMS SDG No.: TSL005 0603561-009AMS A\A45411.D 03/16/06 03/23/06 1.00 Soil Extract Volume: (gL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 108-90-7 Chlorobenzene 54 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45411.D Vial: 10 Acq On 23 Mar 2006 17:34 Operator: tm Sample 0603561-009AMS Inst : H5971 Misc TSL005,MW-5SMS,H2O,MS„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:06 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via _ Cnntinnina Cal File- C-\HPCHEM\1\TATA\MApne\(]323f1FA\A4539R_n Abundance TIC: A45411.13 1500000- 50000014500001400000 1450000- 1400000- 1350000 1350000 8 a e 1300000 Co 1250000 a ° o` 1200000 h 1150000 a 1100000, a ° `o C 1050000 E 1000000 u y 950000 and 900000 0 850000 4E i 800000 750000 d 700000 a c � ° 650000 2 r° —Z° 600000 d ~ 550000 IL 500000 v 450000 d 400000 0 `o 350000 u 4 300000 250000 200000 150000 100000 50000 0 ime--> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45411.D PUHW0320.M Mon Mar 27 09:33:43 2006 H5971 Page 2 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45411.D Vial: 10 Acq On : 23 Mar 2006 17:34 Operator: tm Sample : 0603561-009AMS Inst H5971 Misc : TSL005,MW-5SMS,H2O,MS,, Multiplr: 1.00 MS Integration Params: RTEINT.P 0.00 Quant Time: Mar 23 19:06 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc UnitsDev(Min) ------------------------------------------------------------------------- 1) Pentafluorobenzene 9.34 168 644938 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.31 114 1091270 50.00.UG/L 0.00 57) Chlorobenzene-d5 14.15 82 580223 50.00 UG/L .0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 522667 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 411971 47.73 UG/L 0.01 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.460 55) Toluene -d8 12.20 98 1345425 50.01 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.02% 56) 4-Bromofluorobenzene 15.73 95 562427 4'9.72 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.44% Target Compounds Qvalue 21) 1,1-Dichloroethene 6.66 96 246595 53.04 UG/L 93 39) Benzene 9.96 78 1362095 55.33 UG/L 98 42) Trichloroethene 10.70 95 344140 52.20 UG/L 97 49) Toluene 12.29 92 940804 53.38 UG/L 98 58) Chlorobenzene 14.19 112 1116851 53.99 UG/L 88 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45411.D PUHW0320.M Mon Mar 27 09:33:41 2006 H5971 Page 1 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/mad) LOW % Moisture: not dec. Contract: EPA SAMPLE NO. MW-SSMSD SAS No.: SDG No.: TSL005 Lab Sample ID: 0603561-009AMSD Lab File ID: A\A45412.D Date Received: 03/16/06 Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (AL) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 57 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 61 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 57 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 58 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloroaiethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OL1404.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. MW-5SMSD Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: 0603561-009AMSD Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45412.D Level: (low/med) LOW Date Received: 03/16/06 Moisture: not dec. Styrene Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (gL) U 96-18-4 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 108-90-7 Chlorobenzene 59 110-57-6 trans-1,4-Dichloro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total)_ 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45412.D Vial: 11 Acq On 23 Mar 2006 18:05 Operator: tm Sample 0603561-009AMSD Inst : H5971 Misc TSL005,MW-5SMSD,H20,MSD „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:06 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 r,,i L�4I -. r- \ uDruFm\ 1 \ narA\mAPnr,\ n-�q-i lFA\A45398 _ D ter-•• -� — un ance IC: A45412.1) 1600000 1550000 1500000 1450000 1400000 ti e 4 1350000 1300000 d d 1250000 a 0 r 1200000 1150000 N= M 1100000 c 1050000 m E � 1000000 N m d 950000 iv d 900000 o `° ' 850000 r� 800000 5 750000 a 0 `o 700000.e c r 650000 ° G 600000 550000 a 500000 d 450000 4000000 0 t 350000L6. u 4 300000 250000 200000 150000 100000 50000 0 Time -->L11. 10.00 12.00 14.00 16.00L 18.00 20.00 22.00 24.00 A45412.D PUHW0320.M Mon Mar 27 09:33:58 2006 H5971 Page 2 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45412.D Vial: 11 Acq On : 23 Mar 2006 18:05 Operator: tm Sample : 0603561-009AMSD Inst : H5971 Misc : TSL005,MW-5SMSD,H20,MSD „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 19:06 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46.2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D Dat'aAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) ------------------------------------------- 1) Pentafluorobenzene 9.34 ----------------------------- 168 639677 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.31 114 1078024 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 573033 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 515527 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.88 65 404316 47.42 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 94.840 55) Toluene -d8 12.20 98 1335996 50.27 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.54% 56) 4-Bromofluorobenzene 15.73 95 557502 49.89 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.78% Target Compounds Qvalue _ 21) 1,1-Dichloroethene 6.67 96 263707 57.19 UG/L 95 39) Benzene 9.96 78 1474427 60.63 UG/L 98 42) Trichloroethene 10.70 95 372483 57.20 UG/L 96 49) Toluene 12.29 92 1017957 58.46 UG/L 98 58) Chlorobenzene 14.19 112 1211669 59.31 UG/L 87 ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A45412.D PUHW0320.M Mon Mar 27 09:33:56 2006 H5971 Page 1 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec.. Contract: BPA SAMPLE NO. MSB032306 SAS No.: SDG No.: TSL005 Lab Sample ID: MSB032306 Lab File ID: A\A45401.D Date Received: Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (AL) Soil Aliquot Volume (AL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 107-13-1 Acrylonitrile 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 50 74-88-4 Iodomethane 5 a U 108-05-4 Vinyl acetate 5 U 67-64-1 Acetone 5 U 75-15-0 Carbon disulfide 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 78-93-3 2-Butanone 5 U 74=97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 54 107-06-2 1,2-Dichloroethane 5 U 79-01-6 Trichloroethene 51 7B-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-88-3 Toluene 51 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 127-18-4 Tetrachloroethene 5 U 591-78-6 2-Hexanone 5 U 124-48-1 Dibromochloromethane 5 U 106-93-4 1,2-Dibromoethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO. MSB032306 Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL005 Matrix: (soil/water) WATER Lab Sample ID: MSB032306 Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A45401.D Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (na/L or ua/Kehr_/r. n 108-90-7 Chlorobenzene 52 110-57-6 trans-1,4-Dich1oro-2-butene 5 U 100-41-4 Ethylbenzene 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45401.D Vial: 6 Acq On : 23 Mar 2006 12:09 Operator: tm Sample : MSB032306 Inst : H5971 Misc . ,,,LCS„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:38 2006 Quant Results File: PUHW0320.RES Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update Mon Mar 27 09:22:50 2006 ResiDonse via : Conti_nuina Cal_ Fi1P- T) un ance TIC: A45401.D 1450000 1400000- 40000013500001300000 1350000- 1300000 g • a 1250000 =" 2 i � r 1200000 •- 1150000 w d d 1100000 N d a 0 1050000 c' 0 1000000 � a 950000 � 11 N 900000 d Q mo 850000 4 800000 750000 U 700000 d e 2 t 650000 ; o o 600000 d 550000 a 500000 450000 d 400000 0 350000 t 300000 4 250000 200000 150000 100000 50000 0 ime--> —6.60' 8. 0 10.00 12.00 14.00 16.00 16.00 20.00 22.00 24.00 A45401.D PUHW0320.M Mon Mar 27 09:27:12 2006 . B5971 Page 2 Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45401.D Vial: 6 Acq On 23 Mar 2006 12:09 Operator: tm Sample MSB032306 Inst H5971 Misc ,,,LCS„ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:38 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 638865 50.00 UG/L 0.01 35) 1,4-Difluorobenzene 10.31 114 1059479 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 576874 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 517656 50.00 UG/L 0.00 System Monitoring Compounds 36) 1,2-Dichloroethane-d4 9.89 65 414642 49.48 UG/L 0.01 Spiked Amount 50.000 Range 76 - 114 Recovery = 98.96% 55) Toluene -d8 12.20 98 1324356 50.71 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 101.42% 56) 4-Bromofluorobenzene 15.73 95 559124 50.91 UG/L 0.00 Spiked Amount 50.000. Range 88 - 110 Recovery = 101.82% Target Compounds Qvalue 21) 1,1-Dichloroethene 6.66 96 229395 49.81 UG/L 98 39) Benzene 9.96 78 1285940 53.80 UG/L 99 42) Trichloroethene 10.70 95 326810 51.06 UG/L 98 49) Toluene 12.29 92 877949 51.30 UG/L 99 58) Chlorobenzene 14.19 112 1068550 51.95 UG/L 89 ------------------------------------------------------------------------- W = qualifier out of range (m) = manual integration A45401.D PUHW0320.M Mon Mar 27 09:27:10 2006 H5971 Page 1 M 00 O O H Re fso 0 Raw50 0 Sub 50 0 Re f50 0 z-> Abundance Scan 601 (9 Raw50 51 39 63 rni0 z—> 3 4 50 6 Abundance Scan . Sub o 0 z--> 102 #21 1,1-Dichloroethene Concen: 49.81 UG/L RT: 6.66 min Scan# 266 Delta R.T. 0.01 min Lab File: A45401.D Acq: 23 Mar 2006 12:09 Tgt Ion: 96 Resp: 229395 Ion Ratio Lower Upper 96 100 61 199.5 183.6 223.6 63 64.0 43.6 83.6 100000 50000 60000 40000 20000 0 #39 Benzene Concen: 53.80 UG/L RT: 9.96 min Scan# 601 Delta R.T. 0.00 min Lab File:. A45401.D Acq: 23 Mar 2006 12:09 Tgt Ion: 78 Resp: 1285940 Ion Ratio Lower Upper 78 100 77 21.9 2.5 42.5 400000 350000 300000 250000 200000 150000 100000 50000 0 me--> A45401.D PUHW0320.M Mon Mar 27 09:27:13 2006 H5971 Re f50 60 35 47 0 67 74 82 Raw50 60 35 47 0 67 82 114 S u 90 60 35 47 0 70 82 114 Re f50 0 Raw50 0 Sub 0 0 500000 400000 300000 200000 10000[ A45401.D PUHW0320.M Mon Mar 27 09:27:14 2006 H5971 kn 00 O O V1 N Page 4 #42 130 Trichloroethene Concen: 51.06 UG/L RT: 10.70 min Scan# 676 Delta R.T. 0.00 min Lab File: A45401.D Acq: 23 Mar 2006 12:09 10 1 0 4 Tgt Ion: 95 `Resp: 326810 Ion Ratio Lower Upper 130 95 100 130 86.0 64.4 104.4 132 81.9 60.8 100.8 y� e Ion 130.00 129.70 to 130.70: A Ion 132.00 131.70 to 132.701: A 1[ 120000 10 1 0 100000-10.70 80000- 0000600004000020000 130 60000- 40000- 20000. 0 10.60 10.8011.00 11.20 T-10 'i46'Time--> 10.40 #49 Toluene Concen: 51.30 UG/L RT: 12.29 min Scan# 837 Delta R.T. 0.00•min Lab File: A45,401.D Acq: 23 Mar 2006 12:09 Tgt Ion: 92 Resp: 877949 Ion Ratio Lower Upper 92 100 91 152.1 131.1 171.1 Abundance Ion o 92.70): A454 500000 400000 300000 200000 10000[ A45401.D PUHW0320.M Mon Mar 27 09:27:14 2006 H5971 kn 00 O O V1 N Page 4 Re f50 0 Raw5o 0 Sub 50 0 #58 Chlorobenzene Concen: 51.95 UG/L RT: 14.19 min Scan# 1030 Delta R.T. -0.01 min Lab File: A45401.D Acq: 23 Mar 2006 12:09 Tgt Ion:112 Resp: 1068550 Ion Ratio Lower Upper 112 100 77 56.3 49.9 89.9 114 30.9 10.9 50.9 500000 Ion 77.00 (76.70 to 77.70): A4 Ion 114.00 (113.70 to 114.70): 400000 14.19 300000- 200000- 100000 00000200000100000 . o me--> 14.0014.2014.4014.6014.8( A45401.D PUHW0320.M Mon Mar 27 09:27:15 2006 H5971 110 00 O O V1 F-+ Page 5 lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: EPA SAMPLE NO. LFB032306 SAS No.: SDG No.: TSL005 Lab Sample ID: LFB032306 Lab File ID: A\A45400.D Date Received: Date Analyzed: 03/23/06 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (;&L) Soil Aliquot Volume (µL) CAS NO. COMPOUND CONCENTRATION UNITS: (µg/L or µg/Kg)UG/L Q 74-87-3 Chloromethane 53 75-01-4 Vinyl chloride 55 74-83-9 Bromomethane 54 75-00-3 Chloroethane 54 107-13-1 Acrylonitrile 58 75-69-4 Trichlorofluoromethane 55 75-35-4 1,1-Dichloroethene 53 74-88-4 Iodomethane 54 108-05-4 Vinyl acetate 53 67-64-1 Acetone 63 75-15-0 Carbon disulfide 54 75-09-2 Methylene chloride 55 156-60-5 trans-1,2-Dichloroethene 54 75-34-3 1,1-Dichloroethane 55 156-59-2 cis-1,2-Dichloroethene 55 78-93-3 2-Butanone 58 74-97-5 Bromochloromethane 55 67-66-3 Chloroform 56 71-55-6 1,1,1 -Trichloroethane 55 56-23-5 Carbon tetrachloride 58 71-43-2 Benzene 55 107-06-2 1,2-Dichloroethane 57 79-01-6 Trichloroethene 56 78-87-5 1,2-Dichloropropane 56 74-95-3 Dibromomethane 56 75-27-4 Bromodichloromethane 57 10061-01-5 cis-1,3-Dichloropropene 57 108-10-1 4-Methyl-2-pentanone 57 108-88-3 Toluene 56 10061-02-6 trans-1,3-Dichloropropene 57 79-00-5 1,1,2 -Trichloroethane 57 127-18-4 Tetrachloroethene 59 591-78-6 2-Hexanone 59 124-48-1 Dibromochloromethane 58 106-93-4 1,2-Dibromoethane 57 FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (q/m,) ML Level: (low/med) LOW % Moisture: not dec. 03/23/06 GC Column: R-502.2 ID: .53 Soil Extract Volume: (uL CAS NO. COMPOUND Contract: EPA SAMPLE NO. LFB032306 SAS No.: SDG No.: TSL005 Lab Sample ID: LFB032306 Lab File ID: A\A45400.D Date Received: Ethylbenzene Date Analyzed: 03/23/06 Dilution,Factor:. 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: iun/r. nr "MIT. 108-90-7 Chlorobenzene 56 110-57-6 trans-1,4-Dichloro-2-butene 55 100-41-4 Ethylbenzene 54 630-20-6 1,1,1,2 -Tetrachloroethane 57 1330-20-7 Xylene (total) 160 100-42-5 Styrene 55 75-25-2 Bromoform 58 79-34-5 1,1,2,2 -Tetrachloroethane 57 96-18-4 1,2,3-Trichloropropane 57 106-46-7 1,4 -Dichlorobenzene 55 95-50-1 1,2 -Dichlorobenzene 56 96-12-8 1,2-Dibromo-3-chloropropane 57 FORM I VOA - 2 OLM04.2 00 00 O O F-+ i Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45400.D Vial: 4 Acq On : 23 Mar 2006 11:05 Operator: tm Sample : LFB032306 Inst H5971 Misc : ,,,LFB „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:37 2006 Quant Results File: PUHW0320.RES Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via _ rnntintninn ral Fila• r•\T-TPrT-TTM\1\rnmmz,\maPnti\n�,)�ntin\aar,-4aP n Abundance - 3200000 3100000- 10000030000002900000 3000000- 2900000. k 2800000 2700000 2600000.d.2 2500000 2400000 2300000 2200000 ~ d 2100000 € w It ~ ai 2000000 d "c 1900000 o FtE 1800000 L ai o u � � e 1700000 � � e 1600000 v a o a a o y o 1500000 g a d 1400000 rfl $ _� 1300000 0 a e E S r 1200000 4 N C W y C C �V C 1100000' 1000000 �Uo Q m 0 S r v m a 900000 s Y § § 4 r C A IFC ~ d 800000:oicoN 700000OltCL600000 C "eF oF E o500000 1400000 �� 4 c E �u E 300000 . _ `o o s 4 N 200000 105 100000 0 Ime-> 6. 0 8. 0 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 A45400.D PUHW0320.M Mon Mar 27 09:25:59 2006 H5971 Page 4 Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAR06\032306A\A45400.D Vial: 4 Acq On 23 Mar 2006 11:05 Operator: tm Sample LFB032306 Inst : H5971 Misc ,,,LFB „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:37 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Internal Standards R.T. QIon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) Pentafluorobenzene 9.34 168 620227 50.00 UG/L 0.00 35) 1,4-Difluorobenzene 10.32 114 1064787 50.00 UG/L 0.00 57) Chlorobenzene-d5 14.15 82 572951 50.00 UG/L 0.00 70) 1,4 -Dichlorobenzene -d4 17.39 152 477710 50.00 UG/L 0.00 System Monitoring Compounds 7) Chloroethane 5.53 64 148682 8) 36) 1,2-Dichloroethane-d4 9.88 65 427336 50.74 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 101.48% 1134 55) Toluene -d8 12.20 98 1315985 50.13 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.26% 43 56) 4-Bromofluorobenzene 15.73 -95 551368 49.96 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.920 6.62 Target Compounds Qvalue 50.56 2) Chlorodifluoromethane 4.28 51 54787 3) Dichlorodifluoromethane 4.26 85 68195 4) Chloromethane 4.53 50 181250 5) Vinyl chloride 4.76 62 210065 6) Bromomethane 5.38 94 136906 7) Chloroethane 5.53 64 148682 8) Acetone 6.70 43 70468 9) Acetonitrile 7.13 41 567541 10) Allyl Chloride 6.53 41 1134 12) Acrylonitrile 7.61 53, 103222 13) Iodomethane 6.93 142 373775 14) Vinyl acetate 8.13 43 419594 16) 2-Butanone 8.84 43 124241 17) Tetrahydrofuran 9.23 42 66315 18) Freon -113 6.62 101 219198 19) Carbon disulfide 7.05 76 1045754 20) Trichlorofluoromethane 5.91 101 332891 21) 1,1-Dichloroethene 6.66 96 234855 22) methyl tert-butyl ether 7.57 73 757582 24) Methylene chloride 7.31 84 308466 25) trans-1,2-Dichloroethene 7.64 96 303727 26) 1,1-Dichloroethane 8.18 63 705172 27) Propionitrile 8.96 54 35066 29) Methacrylonitrile 9.13 67 117480 30) cis-1,2-Dichloroethene 8.89 96 361206 31) Bromochloromethane 9.20 128 136768 32) ----------------------------------------------------- 2,2-Dichloropropane 8.88 77 445579 (#) = qualifier out of range (m) = manual integration A45400.D PUHW0320.M Mon Mar 27 09:25:54 2006 H5971 Page 1 Qvalue 50.56 UG/L 98 55.59 UG/L 98 52.98 UG/L 99 55.40 UG/L 99 54.41 UG/L' 100 54.36 UG/L 99 62.67 UG/L 96 266.68 UG/L 98 28.69 UG/L 82 57.83 UG/L 98 53.95 UG/L 94 52.97 UG/L 100 58.27 UG/L 99 54.38 UG/L 98 53.51 UG/L 99 53.51 UG/L # 100 54.69 UG/L 99 52.53 UG/L 98 57.08 UG/L 97 55.45 UG/L 97 54.21 UG/L 97 54.96 UG/L 100 54.74 UG/L 98 54.19 UG/L 98 54.71 UG/L 98 55.23 UG/L 98 52.99 -------------------- UG/L 99 H5971 Page 1 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45400.D Vial: 4 Acq On : 23 Mar 2006 11:05 Operator: tm Sample : LFB032306 Inst : H5971 Misc . ,,,LFB „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:37 2006 Quant Results File: PUHW0320.RES Quant Method C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update Thu Mar 23 10:48:46 2006 Response via Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth PUHW0320 Compound R.T. QIon Response Conc Unit Qvalue 33) Chloroform 9.24 83 609110 55.80 UG/L 34) 1,1,1 -Trichloroethane 9.50 97 524657 54.82 UG/L 37) 1,1-Dichloropropene 9.67 75 467359 55.32 UG/L 38) Carbon tetrachloride 9.70 117 451823 57.82 UG/L 39) Benzene 9.96 78 1332095 55.46 UG/L 40) 1,2-Dichloroethane 9.98 62 491988 57.43 UG/L 41) Methyl Methacrylate 10.95 69 215131 58.02 UG/L 42) Trichloroethene 10.70 95 361376 56.18 UG/L 43) 1,2=Dichloropropane 11.01 63 451515 56.19 UG/L 44) Dibromomethane 11.20 93 201454 56.42 UG/L 47) Bromodichloromethane 11.33 83 492087 56.58 UG/L 48) cis-1,3-Dichloropropene 11.84 75 667149 56.86 UG/L 49) Toluene 12.29 92 955336 55.55 UG/L 50) Ethyl Methacrylate 12.46 69 441487 57.54 UG/L 51) trans-1,3-Dichloropropene 12.52 75 571723 56.61 UG/L 52) 1,1,2 -Trichloroethane 12.80 83 244682 56.93 UG/L 53) 1,2-Dibromoethane 13.60 107 338273 56.98 UG/L 54) 4-Methyl-2-pentanone 11.93 43 289503 56.92 UG/L 58) Chlorobenzene 14.19 112 1136523 55.64 UG/L 59) 1,3-Dichloropropane 13.04 '76 527362 56.24 UG/L 60) Tetrachloroethene 13.02 164 396707 58.75 UG/L 61) Dibromochloromethane 13.39 129 336836 57.56 UG/L 62) 2-Hexanone 12.99 43 199401 58.76 UG/L 63) 1,1,1,2 -Tetrachloroethane 14.27 131 321680 56.98 UG/L 64) Ethylbenzene 14.24 106 588842 54.39 UG/L 65) m,p-Xylene 14.38 106 1469376 109.46 UG/L 66) o -Xylene 14.96 106 752386 55.06 UG/L 67) Xylene (total) 14.38 106 2225867m 162.90 UG/L 68) Styrene 14.98 104 1259588 55.00 UG/L 69) Bromoform 15.37 173 253064 57.76 UG/L 71) trans-1,4-Dichloro-2-buten 15.92 53 109554 55.09 UG/L 72) 1,1,2,2 -Tetrachloroethane 15.88 83 345426 56.74 UG/L 73) Pentachloroethane 16.85 167 137248 47.78 UG/L 74) 1,2,3-Trichloropropane 12.52 112 89900 56.52 UG/L 75) Isopropylbenzene 15.42 105 1693674 55.97 UG/L 76) Bromobenzene 16.01 156 403823 56.35 UG/L 77) n-Propylbenzene 15.99 91 1988093 55.23 UG/L 78) 2-Chlorotoluene/4-Chloroto 16.36 91 2755806m 111.99 UG/L 79) 1,3,5-Trimethbenz/P-ethylt 16.19 105 2863314m 111.14 UG/L 80) tert-Butylbenzene 16.70 119 1281499 55.75 UG/L 81) 1,2,4-Trimethylbenzene 16.76 105 1555884 55.57 UG/L (#) = qualifier out of range (m) = manual integration A45400.D PUHW0320.M Mon Mar 27 09:25:55 2006 H5971 99 99 97 99 99 99 97 98 100 99 99 99 99 99 100 98 99 99 99 99 100 100 98 100 98 98 99 99 100 91 100 99 98 100 99 100 99 100 Page 2 Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45400.D Vial: 4 Acq On : 23 Mar 2006 11:05 Operator: tm Sample : LFB032306 Inst : H5971 Misc : ,,,LFB „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 23 13:37 2006 Quant Results File: PUHW0320.RES Quant Method : C:\HPCHEM\1\METHODS\PUHWO320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 23 10:48:46 2006 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\MAR06\032306A\A45398.D DataAcq Meth : PUHW0320 N Ln O O - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - a (#) = qualifier out of range (m) = manual integration FV) --i A45400.D PUHW0320.M Mon Mar 27 09:25:56 2006 H5971 Page 3 Compound R.T. QIon Response Conc Unit . Qvalue ------------------------------------------------------------------------- 82) sec-Butylbenzene 17.00 105 1866575 55.28 UG/L 100 83) 4-Isopropyltoluene 17.17 119 1354431 55.30 UG/L 100 84) 1,3 -Dichlorobenzene 17.30 146 753585 56.24 UG/L 100 85) 1,4 -Dichlorobenzene 17.42 146 741171 55.20 UG/L 100 86) 1,2 -Dichlorobenzene 18.01 146 704542 55.91 UG/L 99 87) p-Diethylbenzene 17.72 119 652860 55.43 UG/L 100 88) n-Butylbenzene 17.77 91 1539695 55.44 UG/L 99 89) 1,2-Dibromo-3-chloropropan 19.23 75 52934 56.94 UG/L 99 90) 1,2,4,5-Tetramethylbenzene 18.93 119 1001973 55.54 UG/L 99 91) 1,2,4-Trichlorobenzene 20.60 180 475580 56.06 UG/L 100 92) Hexachlorobutadiene 20.77 225 178976 55.97 UG/L 100 93) Naphthalene 21.12 128 625783 54.76 UG/L 100 94) 1,2,3-Trichlorobenzene 21.58 180 282355 53.15 UG/L 99 N Ln O O - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - a (#) = qualifier out of range (m) = manual integration FV) --i A45400.D PUHW0320.M Mon Mar 27 09:25:56 2006 H5971 Page 3 Quantitation Report Data File : C:\HPCHEM\1\DATA\MAR06\032306A\A45400.D Vial: 4 Acq On : 23 Mar 2006 11:05 Operator: tm Sample : LFB032306 Inst : H5971 Misc : ,,,LFB „ Multiplr: 1.00 Quant Time: Mar 23 13:37 2006 Quant Results File: temp.res Method : C:\HPCHEM\1\METHODS\PUHW0320.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Mar 27 09:22:50 2006 Response via : Single Level Calibration Abundance on o 105.70): A45400.13 1400000 Ion 91.00 (90.70 to 91.70): A45400.1) :on 105.00 (104.70 to 105.70): A45400.D 1200000- 1000000-, 800000 600000 1 .8 400000 200000 0 fine-> 13.40 13.60 13.80 14.00 14.20 14.40 14.60 14.80 15.00 15.20 15.40 15.60 15.80 16.00 Abundance can m n:10.13 9 106 500000 39 5165 77 LT 85 9;761f 117 133 163 207 z--> 3 4 50 60 0 80 90 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 2 0 2 0 bundance can4.953 min: A45398.D 9 106 5000 51 78 39 63 72 85 98 z--> 3 4 50 60 70 80 91 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 1 0 2 0 2 0 (67) Xylene (total) (T) 14.38m1n 162.90UG/L m response 2225867 Ion Exp% Act% 106.00 100 100 91.00 190.20 63.74# 105.00 51.30 17.15# 0.00 0.00 0.00 A45400.D PUHW0320.M Mon Mar 27 09:27:54 2006 H5971 U2M LABS, INC. WHERE: COMPUTATIONS FOR VOLATILE ORGANICS PERFORMED BY RTE DATA SYSTEM OF HP Ax Is CONC =-------- Ais x RRF W CONC = Concentration in sample (ug/L or ug/KG) Ax = Area of characteristic ion of compound Ais = Area of characteristic ion of internal standard RRF = Relative response factor as area per (ng) of compound, divided by area per ng of respective internal standard Is = Amount of internal standard injected (ng) W = Volume of sample in (ml) or dry.weight (g) Generally the amount of each internal standard injected is 250 ng. U28t "US. INC. V. DOCUMENTATION FOR VOLATILE ORGANICS A. LOG BOOK PAGES B. REPORTING ANALYST SIGNATURE PAGE mEll 0M0Me it r mm 00 U2M "US, INC. SDG # TSL005 SCAN: VOA This data package was reported by the undersigned. This reporting includes data calculations, manual edits, if necessary, and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature: 3-27-06