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Wet Chemistry Data Package 04/2005
I A Analytical Data Package For TOWN OF SOUTHOLD, PART 360 BASELINE SDG NO: TSL001 Wafer Samples Received: 4/1/05 & 4/4/05 WET CHEMISTRY DATA PACKAGE APRIL 2005 I I U2M IL US, INC. TS i-oo► 0 TABLE OF CONTENTS I. SAMPLE REPORTS • II. Q.C. SUMMARY III. RAW DATA U2M I AUS, INC. • I. SAMPLE REPORTS .7 • . t 12M LADS, INCe 575BMWFb oov Road, Houle NY 11747 LABORATORY RESULTS (6 l)(%W3 O.FAX(631)420 M WSDOHm#10478 Sample Information... Town of Southold Landfill Lab No. : 0504024-001 Type: Groundwater Attn To : Origin: Client ID.: MW -3D Collected :4/1/2005 9:30:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameters} Results ualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 305 4 mg/L E310.1 04/06/2005 12:01 PM Biochemical Oxygen Demand 31 1 mg/L E405.1 04/01/2005 4:40 PM Bromide < 0.5 1 mg/L E320.1 04/13/2005 9:40 AM Chloride 198 10 mg/L E325.2 04/04/2005 1:05 PM Chemical Oxygen Demand 74.3 1 mg/L E410.4 04/08/200510:02 AM Color 30 1 units E110.2 04/02/2005 1:09 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/2005 1:42 PM Hardness (As CaCO3) 400 10 mg/L E130.2 04/07/2005 1:10 PM Nitrogen, Ammonia (As N) 23.5 20 mg/L E350.1 04/07/2005 11:44 AM Nitrate as N 39.0 20 mg/L E353.2 04/05/2005 2:25 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 04/12/2005 9:30 AM Sulfate 47.0 5 mg/L SW9038 04/08/200512:34 PM Total Dissolved Solids 938 2 mg/L E160.1 04/05/2005 3:06 PM Kjeldahl, Total 22.6 20 mg/L E351.2 04/12/2005 11:56 AM •Nitrogen, Total Organic Carbon 24.0 1 mg/L SW9060 04/06/2005 5:45 PM Qualifiers: E - Value above quantitation range is D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/21/2005 Page 1 of 9 Laboratory Manager U2A TAUS, INCe 575BrcadHcbN Roel W& W 11747 LABORATORY RESULTS (631)f4XIM.FAX (631)420. %NYSDOHID#10478 Sample Information... . Town of Southold Landfill Lab No.: 0504024-002 Type : Groundwater Attn To : Origin: Client ID. : MW -3S Collected :4/1/2005 9:10:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC 0 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/21/2005 Page 2 of 9 ? aws'.. )h Laboratory Manager 0 l C/) Parameters) Results Qualifler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 180 2 mg/L E310.1 04/06/2005 12:06 PM Biochemical Oxygen Demand 4 1 mg/L E405.1 04/01/2005 4:45 PM Bromide 0.6 1 mg/L E320.1 04/13/2005 9:45 AM Chloride 60.8 1 mg/L E325.2 04/06/2005 1:33 PM Chemical Oxygen Demand 54.3 1 mg/L E410.4 04/08/200510:03 AM Color 20 1 units E110.2 04/02/2005 1:10 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/2005 1:43 PM Hardness (As CaCO3) 450 10 mg/L E130.2 04/07/2005 1:15 PM Nitrogen, Ammonia (As N) 29.5 20 mg/L E350.1 04/07/200511:45 AM Nitrate as N 2.57 5 mg/L E353.2 04/05/2005 2:26 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/12/2005 9:35 AM Sulfate 16.2 1 mg/L SW9038 04/08/200512:36 PM Total Dissolved Solids 460 2 mg/L E160.1 04/05/2005 3:07 PM Kjeldahl, Total 28.7 20 mg/L E351.2 04/12/2005 11:56 AM •Nitrogen, Total Organic Carbon 20.1 1 mg/L SW9060 04/06/2005 6:10 PM 0 Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/21/2005 Page 2 of 9 ? aws'.. )h Laboratory Manager 0 l C/) IH2M "Uso INC. 575BroadH*w RDac, Mdvb NY 11747 LABORATORY RESULTS (631)6943000.FAX(6i1)42M436 NYSDO ID#10478 Sample Information... • Town of Southold Landfill Lab No. : 0504024-003 Type : Groundwater Attn To : Origin: Client ID.: MW -5D Collected :4/1/20051:30:00 PM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameter(s) Results ualifier —D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 487 4 mg/L E310.1 04/06/200512:11 PM Biochemical Oxygen Demand 21 1 mg/L E405.1 04/01/2005 4:50 PM Bromide 0.5 1 mg/L E320.1 04/13/2005 9:50 AM Chloride 374 10 mg/L E325.2 04/04/20051:07 PM Chemical Oxygen Demand 107 1 mg/L E410.4 04/08/200510:04 AM Color 30 1 units E110.2 04/02/2005 1:11 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/2005 1:44 PM Hardness (As CaCO3) 680 10 mg/L E130.2 04/07/20051:20 PM Nitrogen, Ammonia (As N) 45.1 20 mg/L E350.1 04/07/200511:45 AM Nitrate as N 8.22 5 mg/L E353.2 04/05/2005 2:26 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/12/2005 9:40 AM Sulfate 87.0 5 mg/L SW9038 04/08/200512:38 PM Total Dissolved Solids 1240 4 mg/L E160.1 04/05/2005 3:08 PM •Nitrogen, Kjeldahl, Total Total Organic Carbon 42.7 25.8 20 1 mg/L mg/L E351.2 SW9060 04/12/200511:57 AM 04/06/2005 6:34 PM Qualifiers: E - Value above quantitation range • D - Results for Dilution D.F.= Dilution Factor Date Reported : 4/21/2005 Page 3 of 9 Laboratory Manager 1-12M LA[3S, INC. 5758=dHda" Paid, M&M NY 11747 LABORATORY RESULTS (631)RX-3M - FAX(631)4208436 NYSDOH ID# 10478 Town of Southold Landfill Lab No. : 0504024-004 Type : Grroundound Sample Information... Attn To Origin: Client ID. : MW -5S Collected :4/1/20051:15:00 PM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Qualifiers: E - Value above quantitation range • D - Results for Dilution D.F. = Dilution Factor Date Reported : 421/2005 Page 4 of 9 Laboratory Manager Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 36.1 1 mg/L E310.1 04/07/2005 8:40 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/01/2005 4:55 PM Bromide < 0.5 1 mg/L E320.1 04/13/2005 9:55 AM Chloride 13.9 1 mg/L E325.2 04/04/20051:07 PM Chemical Oxygen Demand 29.3 1 mg/L E410.4 04/08200510:05 AM Color 80 2 units E110.2 04/0220051:14 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/022005 1:45 PM Hardness (As CaCO3) 68.0 2 mg/L E130.2 04/072005 1:25 PM Nitrogen, Ammonia (As N) 3.60 5 mg/L E350.1 04/072005 10:52 AM Nitrate as N 2.09 5 mg/L E353.2 04/052005 2:27 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 04/122005 9:45 AM Sulfate 14.2 1 mg/L SW9038 04/08200512:40 PM Total Dissolved Solids 106 1 mg/L E160.1 04/052005 3:11 PM Nitrogen, Kjeldahl, Total 4.34 10 mg/L E351.2 04/122005 11:58 AM Total Organic Carbon 33.1 1 mg/L SW9060 04/062005 6:59 PM Qualifiers: E - Value above quantitation range • D - Results for Dilution D.F. = Dilution Factor Date Reported : 421/2005 Page 4 of 9 Laboratory Manager U2 -At L US, INC. 575BroadFIOIDN Road, Mel b NY 11747 LABORATORY RESULTS (631)894,9040. FAX (631)42D 8K% NYSDOH ID# 10478 Sample Information... • Town of Southold Landfill Lab No. : 0504024-005 Type : Groundwater Attn To : Origin: Client ID.: MW -6D Collected :4/1/200511:20:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameter(s) Results Qualifler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 14.1 1 mg/L E310.1 04/07/2005 8:45 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/01/2005 5:00 PM Bromide < 0.5 1 mg/L E320.1 04/13/2005 10:00 AM Chloride 18.8 1 mg/L E325.2 04/04/2005 1:08 PM Chemical Oxygen Demand 11.8 1 mg/L E410.4 04/08/200510:06 AM Color 100 2 units E110.2 04/02/2005 1:15 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/2005 1:46 PM Hardness (As CaCO3) 252 4 mg/L E130.2 04/07/2005 1:30 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 04/07/200511:46 AM Nitrate as N 0.20 1 mg/L E353.2 04/05/2005 2:28 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/12/2005 9:50 AM Sulfate 38.5 5 mg/L SW9038 04/08/200512:42 PM Total Dissolved Solids 125 1 mg/L E160.1 04/05/2005 3:12 PM •Nitrogen, Kjeldahl, Total Total Organic Carbon 0.24 1.8 1 1 mg/L mg/L E351.2 SW9060 04/12/200511:58 AM 04/07/2005 9:56 AM is Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/21/2005 Page 5 of 9 Laboratory Manager F-4 U2M LABS, INCe MBroadHoloN Fkx4 McMla NY 11747 LABORATORY RESULTS (631)W4-3M-FAX(631)4208436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0504024-006 Type : Groundwater Attn To : Origin: Client ID.: MW -6S Collected :4/1/2005 11:00:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameterfsl Results Qualifler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 11.0 1 mg/L E310.1 04/07/2005 8:50 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/01/2005 5:05 PM Bromide < 0.5 1 mg/L E320.1 04/13/200510:05 AM Chloride 11.1 1 mg/L E325.2 04/04/20051:11 PM Chemical Oxygen Demand 11.8 1 mg/L E410.4 04/08/200510:07 AM Color < 5 1 units E110.2 04/02/20051:16 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/20051:47 PM Hardness (As CaCO3) 60.0 2 mg/L E130.2 04/07/20051:35 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 04/07/2005 11:47 AM Nitrate as N 3.65 5 mg/L E353.2 04/05/2005 2:28 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/12/2005 9:55 AM Sulfate 11.5 1 mg/L SW9038 04/08/200512:44 PM Total Dissolved Solids 104 1 mg/L E160.1 04/05/2005 3:13 PM Nitrogen, Kjeldahl, Total • Total Organic Carbon < 0.10 1.1 1 1 mg/L mg/L E351.2 SW9060 04/12/2005 11:59 AM 04/07/200510:22 AM • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/21/2005 Page 6 of 9 TORRE '"'"W 611im'"M Laboratory Manager 00 .-1 F-0 U2M LAUS, INC. 575BrcedHdav Road, M&Ila NY 11747 (631)634-M.FAX (631)42MM NYSDOHID#10478 Town of Southold Landfill Attn To : Collected :4/1/200510:16:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC LABORATORY RESULTS Lab No. : 0504024-007 Client ID.: MW -8D Sample Information... Type : Groundwater Origin: Parameterls) Results Qualffler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 376 4 mg/L E310.1 04/06/200512:21 PM Biochemical Oxygen Demand 31 1 mg/L E405.1 04/01/2005 5:10 PM Bromide < 0.5 1 mg/L E320.1 04/13/200510:10 AM Chloride 136 5 mg/L E325.2 04/04/20051:12 PM Chemical Oxygen Demand 69.3 1 mg/L E410.4 04/08/200510:08 AM Color 40 1 units E110.2 04/02/2005 1:17 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/02/2005 1:48 PM Hardness (As CaCO3) 530 10 mg/L E130.2 04/07/20051:40 PM Nitrogen, Ammonia (As N) 40.1 20 mg/L E350.1 04/07/200511:47 AM Nitrate as N 18.7 20 mg/L E353.2 04/05/2005 2:29 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 04/12/200510:00 AM Sulfate 78.0 5 mg/L SW9038 04/08/200512:46 PM Total Dissolved Solids 776 2 mg/L E160.1 04/05/2005 3:14 PM •Nitrogen, Kjeldahl, Total Total Organic Carbon 37.9 24.3 20 1 mg/L mg/L E351.2 SW9060 04/12/200512:00 PM 04/06/2005 8:15 PM Qualifiers: E - Value above quantitation range • D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/21/2005 Page 7 of 9 ? awr_ A 1-1164pc�* Laboratory Manager 1-12M L ES, INCe 57513foadHdlow Roel MEMIS NY 11747 LABORATORY RESULTS (631)6943040. FAX (631)42!}8436 NYSDOH ID# 10478 •Town of Southold Landfill Lab No. : 0504024-008 Sample Information... Type : Groundwater AMn To : Origin: Client ID.: MW -8S Collected :4/1/200510:00:00 AM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameter(sl Results Clualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 106 2 mg/L E310.1 04/06/200512:26 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/01/2005 5:10 PM Bromide 0.7 1 mg/L E320.1 04/13/2005 10:15 AM Chloride 18.5 1 mg/L E325.2 04/04/20051:13 PM Chemical Oxygen Demand 86.8 1 mg/L E410.4 04/08/2005 10:09 AM Color 30 1 units E110.2 04/0220051:18 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/022005 1:49 PM Hardness (As CaCO3) 96.0 2 mg/L E130.2 04/0720051:45 PM Nitrogen, Ammonia (As N) 43.6 5 mg/L E350.1 04/07200510:55 AM Nitrate as N < 0.10 1 mg/L E353.2 04/052005 2:30 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/122005 10:05 AM Sulfate 14.8 1 mg/L SW9038 04/082005 12:48 PM Total Dissolved Solids 151 1 mg/L E160.1 04/052005 3:15 PM Kjeldahl, Total 46.9 20 mg/L E351.2 04/122005 12:00 PM •Nitrogen, Total Organic Carbon 31.8 1 mg/L SW9060 04/062005 8:40 PM • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F.= Dilution Factor Date Reported : 421/2005 Page 8 of 9 Laboratory Manager U2A 1 AUS, INC. 575BIDadHObN RI)aCk Mdt41e NY 11747 LABORATORY RESULTS (631)6843040. FAX (631)42M436 WSOOH ID# 10478 Town of Southold Landfill Lab No. : 0504024-009 emple Information... • Type : Blank Attn To : Origin: Client ID. : EQUIPT. BLANK Collected :4/1/200512:00:00 PM Received :4/1/2005 4:20:00 PM Collected By VG Copies To :Original CC Parameterfs) Results Qualifier D.F.. Unfit Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 04/07/2005 8:55 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/01/2005 5:10 PM Bromide < 0.5 1 mg/L E320.1 04/13/200510:20 AM Chloride < 2.0 1 mg/L E325.2 04/04/20051:13 PM Chemical Oxygen Demand <10 1 mg/L E410.4 04/08/200510:10 AM Color < 5 1 units E110.2 04/02/20051:19 PM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/0220051:50 PM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 04/072005 1:50 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 04/07200510:57 AM Nitrate as N < 0.10 1 mg/L E353.2 04/052005 2:33 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 04/12200510:10 AM Sulfate < 5.0 1 mg/L SW9038 04/08200512:50 PM Total Dissolved Solids 16 1 mg/L E160.1 04/052005 3:16 PM Kjeldahl, Total < 0.10 1 mg/L E351.2 04/12200512:01 PM •Nitrogen, Total Organic Carbon < 1.0 1 mg/L SW9060 04/072005 10:47 AM • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 4/212005 Page 9 of 9 ? anvii,6 A Laboratory Manager U2M L US, INCe 5MBIDadHobN Road, W& NY 11747 LABORATORY RESULTS (631)694,3040.FAX (631)42t} M NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0504067-001 Type : Groundwater i Origin: Attn To Client ID. : MW -1D Collected :4/4/2005 4:00:00 PM Received :4/4/2005 5:00:00 PM Collected By VG Copies To :Original CC Parameterfsl Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 33.2 1 mg/L E310.1 04/07/2005 9:00 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/05/2005 3:20 PM Bromide < 0.5 1 mg/L E320.1 04/13/200510:25 AM Chloride 19.5 1 mg/L E325.2 04/06/20051:34 PM Chemical Oxygen Demand < 10 1 mg/L E410.4 04/08/200510:11 AM Color <5 1 units E110.2 04/05/2005 7:32 AM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/05/2005 7:02 AM Hardness (As CaCO3) 42.0 2 mg/L E130.2 04/07/20051:55 PM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 04/07/200511:48 AM Nitrate as N 1.17 5 mg/L E353.2 04/05/2005 2:36 PM Phenolics, Total Recoverable < 5.0 1 ug/L E420.1 04/12/200510:15 AM Sulfate 25.5 1 mg/L SW9038 04/08/200512:52 PM Total Dissolved Solids 131 1 mg/L E160.1 04/05/2005 3:18 PM Nitrogen, Kjeldahl, Total 0.18 1 mg/L E351.2 04/12/200512:03 PM • Total Organic Carbon < 1.0 1 mg/L SW9060 04/07/2005 11:13 AM Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 4/21/2005 Page 1 of 2 Laboratory Manager 1i2M LAUSO INC. 575BIoadH0110N Rued, MWIIS NY 11747 LABORATORY RESULTS (631)694.3040. FAX, (631)42D8436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No.: 0504067-002 Type: Groundwater Attn To Origin: Client ID.: MW -1S Collected :4/4/2005 4:10:00 PM Received :4/4/2005 5:00:00 PM Collected By VG Copies To :Original CC Parameters) Results Qualifler D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 33.8 1 mg/L E310.1 04/07/2005 9:05 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 04/05/2005 3:25 PM Bromide < 0.5 1 mg/L E320.1 04/13/200510:30 AM Chloride 20.6 1 mg/L E325.2 04/06/20051:35 PM Chemical Oxygen Demand <10 1 mg/L E410.4 04/08200510:14 AM Color < 5 1 units E110.2 04/052005 7:33 AM Chromium, Hexavalent < 0.02 1 mg/L M3500 -Cr D 04/052005 7:03 AM Hardness (As CaCO3) 40.0 1 mg/L E130.2 04/072005 2:10 PM Nitrogen, Ammonia (As N) 0.13 1 mg/L E350.1 04/07200511:49 AM Nitrate as N 1.15 5 mg/L E353.2 04/05/2005 2:36 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 04/12200510:20 AM Sulfate 47.5 5 mg/L SW9038 04/08200512:54 PM Total Dissolved Solids 236 1 mg/L E160.1 04/052005 3:19 PM Nitrogen, Kjeldahl, Total < 0.10 1 mg/L E351.2 04/12200512:04 PM • Total Organic Carbon 111 10 mg/L SW9060 04/06200510:46 PM M . Qualifiers: E - Value above quantitation range ,�f/�'L ',l - •--1 D - Results for Dilution 0 D.F. = Dilution Factor Laboratory Manager Date Reported: 4/21/2005 F"I Page 2 of 2 U2M "US, INC. .7 II. Q.C. SUMMARY • • HZM LABS, INC. SDG: TSL001 Date: 21 -Apr -05 QC SUMMARY REPORT Spike Sample Recovery RPDRsf %RPD Sample ID• Client Sample ID: Analyte Result Unita Amount Result %REC (.units Value %RPD UCL MBLK040705 MBLK040705 Alkalinity, Total (As CaCO3) < 1 mg/L LCSO40705 LCSO40705 Alkalinity, Total (As CaCO3) 21.8 mg/L 25 < 1 87 80 120 0504067-002bms MW -ISMS Alkalinity, Total (As CaCO3) 58.0 mg/L 25 33.8 97 75 125 0504067-002bdup MWASDUP Alkalinity, Total (As CaCO3) 33.3 mg/L 33.8 1.3 20 MBLK040605 IMBLK040605 JAIkalinity, Total (As CaCO3), High < 5 I mg/L 1 mg/L LCSO40505 LCSO40505 Biochemical Oxygen Demand LCSO40605 ILCS040605 lAlkalinity, Total (As CaCO3), High 1 126 1 mg/L 1 125 1 < 5 1 101 180 11201 1 93 MBLK040105 IMBLK040105 Biochemical Oxygen Demand <2 1 mg/L LCSO40505 LCSO40505 Biochemical Oxygen Demand 178 LCSO40105 ILCS040105 Biochemical Oxygen Demand 186 I mg/L 1 200 1 < 2 1 93 180 11201 Bromide MBLK040505 MB K040505 Biochemical Oxygen Demand < 2 mg/L LCSO40505 LCSO40505 Biochemical Oxygen Demand 178 mg/L 1 200 < 2 89 80 120 T-20 0504087-002bdup MWASDUP Biochemical Oxygen Demand < 4 mg/L I 1 1 <2 MB -041305 MB -041305 Bromide < 0.5 mg/L LCS-041305 LCS-041305 Bromide 4.9 mg/L 5 < 0.5 98 80 120 0504067-002BMS MW -ISMS Bromide 4.5 mg/L 5 < 0.5 90 75 125 0504067-002BDUP MW-1SDUP Bromide < 0.5 mg/L < 0.5 20 MBLK040805 MBLK040805 Chemical Oxygen Demand <10 mg/L LCSO40805 LCSO40805 Chemical Oxygen Demand 1100 mg/L 1000 < 10 110 80 120 0504067-002dms MW-1SMS Chemical Oxygen Demand 1090 myL 1000 < 10 109 75 125 0504067-002ddup MW-1SDUP Chemical Oxygen Demand <10 mg/L <10 20 MBI -040405 MBI -040405 IChWide <1 I myl LCS1-040405 LCSI-04W5 IChWide 50.5 1 mg/L 1 50 1 <11 1 101 180 11201 1 TSL001 W15 • QC SUMMARY REPORT SDG: TSL001 Spike Sample Recovery RPDRei %RPD Sample ID: Client Sample ID• Analyte Result Unita Amount Result %REC Limits Value %RPD UCL MS -040605 MB -040605 Chloride < 1 mg/L LCS-040605 LCS-040605 Chloride 50.8 m9/L 50 < 1 102 80 120 0504067-002BMS MWASMS Chloride 46.8 mg/L 25 20.6 105 75 125 0504067-002BDUP MWASDUP Chloride 20.3 mg/L 20.6 1.2 20 MBLK040205 IMBLK040205 lChromium, Hexavalent I < 0.02 1 mWL < 0.02 mg/L LCS-040505 LCS-040505 LCSO40205 ILCS040205 lChromium, Hexavalent 1 0.20 1 m9/L 1 0.2 1<0.021 100 180 11201 Chromium, Hexavalent 0.17 MB -040505 MB -040505 Chromium, Hexavalent < 0.02 mg/L LCS-040505 LCS-040505 Chromium, Hexavalent 0.17 m9/L 0.2 < 0.02 85 80 120 0504067-002BMS MW -ISMS Chromium, Hexavalent 0.17 mg/L 0.2 <0.02 85 75 125 0504067-002Bdup MWA SDUP Chromium, Hexavalent < 0.02 mg/L < 0.02 20 MB -R47906 MB -R47906 Color < 5 units LCS-R47906 LCS-R47906 Color 40 units 40 <5 100 80 120 D504067-002Bdup MW-1SDUP Color <5 units I I< 5 20 MBLK040205 IMBLK040205 IColor 1 <5 1 units < 5 mg/L LCSO40205 ILCS040205 IColor 1 40 1 units 1 40 1 < 5 1 100 180 11201 mg/L 1000 < 5 104 80 120 MBLK040705 MBLK040705 Hardness (As CaCO3) < 5 mg/L LCSO40705 LCSO40705 Hardness (As CaCO3) 1040 mg/L 1000 < 5 104 80 120 0504067-002ems MWASMS Hardness (As CaCO3) 144 mg/L 100 40.0 104 75 125 0504067-002edup MW -1 SDUP Hardness (As CaCO3) 40.0 mg/L 40.0 0 20 mb-040505 mb-040505 Nitrate as N < 0.1 m91L ICs -040505 ks-040505 Nitrate as N 1.12 mgtL 1.13 < 0.1 99 80 120 0504067-002DMS MWASMS Nitrate as N 3.52 mg/L 2.5 1.15 95 75 125 0504067-002DDUP MWASDUP Nitrate as N 1.12 m9/L 1.15 2.6 20 2 TSL001 W16 QC SUMMARY REPORT SDG: TSL001 Spike Sample Rsoovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Umits Value %RPD UCL MB1-13164 MBI -040705 Nitrogen, Ammonia (As N) < 0.1 mg/L Ica -13204 Ics-041205 Nitrogen, Kjeldahl, Total 4.44 mg/L 4.1 < 0.1 108 80 120 MS -13164 MB -040705 Nitrogen, Ammonia (As N) < 0.1 mg/L 0504067-002DDUP MW-1SDUP Nitrogen, Kjeldahl, Total -0.29 mg/L < 0.1 98.2 20 LCSI1-13164 LCSI1-040705 Nitrogen, Ammonia (As N) 0.55 mg/L 0.5 < 0.1 110 80 120 LCSI-13164 LCSI-040705 Nitrogen, Ammonia (As N) 0.52 mg/L 0.5 < 0.1 104 80 120 LCSh1-13164 LCSh1-040705 Nitrogen, Ammonia (As N) 2.74 mg/L 2.5 < 0.1 110 80 120 LCSh-13164 LCSh-040705 Nitrogen, Ammonia (As N) 2.68 mg/L 2.5 < 0.1 107 80 120 0504067-002DMS MWASMS Nitrogen, Ammonia (As N) 5.17 mg/L 5 0.13 101 75 125 0504067-002DDUP MW-1SDUP INKrogen, Ammonia (As N) I < 0.1 1 mg/L1 0.13 200 120 mb-13204 mb-041205 Nitrogen, Kjeldahl, Total < 0.1 mg/L Ica -13204 Ics-041205 Nitrogen, Kjeldahl, Total 4.44 mg/L 4.1 < 0.1 108 80 120 0504067-002DMS MWASMS Nitrogen, Kjeldahl, Total 4.30 mg/L 4.1 < 0.1 105 75 125 0504067-002DDUP MW-1SDUP Nitrogen, Kjeldahl, Total -0.29 mg/L < 0.1 98.2 20 MBLK-041205 MBLK-041205 Phenolics, Total Recoverable < 5 ug/l. LCS-041205 LCS-041205 Phenolics, Total Recoverable 27.7 ug/L 30 < 5 92 80 120 0504067-002DMS MWASMS Phenolics, Total Recoverable 18.8 ug/L 20 < 5 94 75 125 0504067-002Ddup MWA SDUP Phenolics, Total Recoverable < 5 ug/L <5 20 MB -040805 MB -040805 Sulfate <5 mg/L LCS-040805 LCS-040805 Sulfate 20.2 mg/L 20 <5 101 80 120 0504067-002BMS MW -ISMS Sulfate 148 mg/L 100 47.5 100 75 125 0504087-002Bdup MW-1SDUP Sulfate 47.0 mg/L 47.5 1.1 20 MBLK040605 MBLK040505 Total Dissolved Solids <10 mg/L LCS040505 LCS040505 Total Dissolved Solids 297 mg/L 300 <10 99 80 120 0504067-0021oms MW-1SMS Total Dissolved Solids 542 MWL 300 236 102 75 125 0504067-002bdup MW-1SDUP Total Dissolved Solids 245 mg/L 236 3.7 20 TSL001 W17 0 0 0 QC SUMMARY REPORT SDG: TSL001 Spike Sample Recovery RPDRef %RPD Sample ID: Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL MBLK-040605 MBLK-040605 Total Organic Carbon < 1 mg/L LCS-040605 LCS-040605 Total Organic Carbon 22.4 m9IL 25 < 1 90 80 120 0504067-002CMS MWA SMS Total Organic Carbon 202 r+ WL 100 111 91 75 125 0504067-002CDUP MWASDUP Total Organic Carbon 119 M91L 111 7.1 20 MBLK-040705 MBLK-040705 Total Organic Carbon <1 I mg/L LCS-040705 ILCS-040705 ITotal Organic Carbon 23.7 1 mg/l. 1 25 1 < 1 1 95 180 11201 TSL001 W18 U2M tAUS, INC. • III. RAW DATA • L` � f sem, 1 Si 001 i' c� G/e 6 Page 1 of 1 TSL001 W20 • �n,fLv�,1 D. TALK High 2 ICV TV=125MG/L 100 4/6/2005 9.95 2.53 126.25 4.46 101% 11:51:00 AM TALK High 2 ICB 100 4/6/2005 5.27 0.04 2.00 4.28 12:02:15 PM TALK High 2 0504024-001 b 25 4/6/2005 6.50 1.53 305.00 4.47 MW -3D 12:04:30 PM TALK High 2 0504024-002b 50 4/6/2005 6.75 1.81 180.50 4.44 MW -3S 12:10:47 PM TALK High 2 0504024-003b 25 4/6/2005 6.72 2.44 487.00 4.45 MW -5D 12:17:30 PM TALK High 2 0504024-004b 100 4/6/2005 5.97 0.84 42.00 4:44 6v -j MW -5S 12:24:28 PM TALK High 2 0504024-007b 25 4/6/2005 6.89 1.88 376.00 4.46 MW -8D 12:29:36 PM TALK High 2 0504024-008b 50 4/6/2005 6.32 1.06 106.00 4.41 MW -8S 12:36:43 PM TALK High 2 0504067-001 b 100 4/6/2005 6.60 0.72 35.75 4.37 dr o+r MWA D 12:42:40 PM TALK High 2 0504067-002b MWI 100 4/6/2005 6.54 4.66 232.75 3.84 is 12:49:09 PM TALK High 2 0504067-002bms 100 4/6/2005 9.63 3.41 170.50 4.45 -49.80% Mw -is 12:52:37 PM tv=125mg/I TALK High 2 0504067-002bdup 100 4/6/2005 6.69 0.85 42.50 4.45 rpd=138.24% MWA S 1:04:21 PM TALK High 2 CCV TV=25MG/L 100 4/6/2005 10.07 2.59 129.50 4.45 103.60% 1:10:28 PM TALK High 2 CCB 100 4/6/2005 5.55 0.05 2.50 4.42 1:21:05 PM TALK High 2 0504067-002b MW 100 4/6/2005 6.67 0.76 37.75 4.42 is 1:50:24 PM TALK High 2 0504067-002bms 100 4/6/2005 9.77 3.29 164.25 4.47 101.20% MW -1S 1:56:01 PM tv=125mgA TALK High 2 0504067.002bdup 100 4/6/2005 6.71 0.77 38.25 4.42 rpd=1.32% MW -1S 2:07:10 PM TALK High 2 ccv tv=125mg/I 100 4/6/2005 10.14 2.54 127.00 4.39 101.60% 2:13:27 PM TALK High 2 ccb 100 4/6/2005 5.43 0.04 2.00 4.36 2:24:29 PM � f sem, 1 Si 001 i' c� G/e 6 Page 1 of 1 TSL001 W20 • �n,fLv�,1 • • • O, oai►/ 'ya-�y TSL001 W21 �t"'r y�9ey Wac - Page 1 of 3 TSL QU t MW -1S 8:41:17 AM TALK low ICB 100 4/712005 5.18 0.08 0.07 4.18 0.10 96.80% Mw -is 8:58;00 AM TALK low 0504024.004b 100 417/2005 5.85 3.82 0.21 4.18 36.10 TALK' low MW -5S 100 8:56:27 AM 6.82 3.49 0:16 4.18 33.30 tpd=1.34% TALK low 0504024-005b 100 4/12005 6.03 1:55 0:14 4,1,8 14.10 TALK low MW -61) 50 $:02:2 AM 6.27 0.69 0.15 4.17 10.90 TALK low 0504024-006b 100 41712005 5.48 1.26 0:17 4:16 10.95 TALK low MW -BS 50 9:09:40 AM 6.42 1.01 0.17 4.14' 16.80 TALK low 0504024009b 100 41712005' 5.49 0.12 0:10 4.15 0.25 TALK low EQUIPT. ,BLANK 100 91$;10 AN1 9.39 2.58 0.14 4.17 24.45 " 97.80% TALK low 0604067-001b 100 4/7/2005 6.51 3.48 0.17 4:17 33.15 TALK low MW -ID 100 9:19:17 AM 5.67 0.15 0.13 4.16 0.20 TALK low 0504067-002b 100 4"{.12005' 6:67 3.53 0:18 4:48 `33:75 O, oai►/ 'ya-�y TSL001 W21 �t"'r y�9ey Wac - Page 1 of 3 TSL QU t MW -1S 9:21 AM TALK low 0504067-002bms 100 417/2005 8.88 5.99 0.20 4.18' 57.95 96.80% Mw -is 9:37:16 AM tv=25mgA TALK' low 0504067-002bdup 100 41712005 6.82 3.49 0:16 4.18 33.30 tpd=1.34% mw -Is 9:49:45AM TALK low 0504011-001 a 50 4/7/2005 6.27 0.69 0.15 4.17 10.90 9:58:15 AM TALK low 0504011-002a 50 4/7/2005 6.42 1.01 0.17 4.14' 16.80 10:04:52,AM TALK low CCV TV=25MG/L 100 4!7/2005 9.39 2.58 0.14 4.17 24.45 " 97.80% 10:12:29 AM TALK low CCB 100 4/7/2005 5.67 0.15 0.13 4.16 0.20 1023:55 AM TALK low 0504011-003a 50 4/7/2005 6.14 0.67 0.14 4.17 10.60 10:27:50 AM TALK low 0504012 -Ma 10' Al 6.42 7:33 0;7 4 I"T .Op 10.4 AAiI TALK low 0504012-0028 10 417/2005 5.50 ` 6.71 0:57 4.19 613.50 10:55:44 AM TALKlow 0504032-001 a 100 "+2t�1i5"" ` 5;50 4:28 04 " [, 1:1.01 AM " t O, oai►/ 'ya-�y TSL001 W21 �t"'r y�9ey Wac - Page 1 of 3 TSL QU t • • • Analysis ident Amount Dato initial pH mIs at 4.5 mls at 4.2 End value TALK TALK low 0504045-00la 100 417 6.24 0.62 - 0.18 4.16 4.40 11:10:09 AM TALK low 0504050-001a 100 4RI2005 6.23 4;64 0:21 4.17 44:35 1.1:16:23',AM TALK low 0504050-002a 100 4/7/2005 6.22 5.18 0.27 4.17 49.10 11:23:29 AM TALK low 0504050-003a 100 `4812005 6.11 2.57 0.20 4.18 23:75 11:30:47 AM TALK low 05040504004a 100 V712005 6.32 3:88 0.24 4:17 36.45' 11:37:35 AM TALK low 0504050.005a 100 4Il 6.42 2.61 0.24 4.13 23:70 1'144.58 AM TALK low ocv tv=25mgA 100 417/2005 9.57 2.67 0.16 4.17 25.10 100.401k 11:52:39 AM. TALK low ceb 100 4/78005 5:60 0.12 0:14 4.16 -0.20 12:0519 PM TALK low 0504050.006a 100' 417/2005 6.26 2.15 0:22 4113 19.30 12:0913.8 PM TALK IOW 0504050-007a 100 V12005 6.31 3.75'' 0.24 4,1!5 35.10 12:1,,7'-"-14,,,PM TALK low 0504050-008a 100 41712005' 6.35 4:64 0.27 4.15 43.70 12:24:26 PM TALK low 0504050.009a 100 "#14905 6.21 4:57 0.26` 4.18' 43.15 ' 12:31:'18; PM_ TALK low 0504050-010a 100 4/7/2005 6.69 2.45 0.19 4.20 22.60 12:38:01 PM TALK low 0504072-001a 100 4/7/2005 5.89 0.93 0.21 4.16 7.20 12:46:20 PM TALK low 0504146-001a 50 4/7/2005 6.35 0.71 0.22 4.14 9.90 12:52:32 PM TALK low 0504146-0028 50 41Y/2005' 6.18` 0.98 0.21' 4.14 151,40 " 12:51��0;F'M TALK low 0504146-003a 50 4/1/2005 6.35 0.72 0.19 4.18 10.70 1:WSO PM TALK low 0504146.004a 50 4/7 6.40 0:72 0.18 1.12:37'�1A` TALK low ccv tvx25mgA100 4/7/2005 9.59 2.74 0.18 4.16 25.80 102.40% 1:19:35 PM Page 2 of 3 TSL001 W22 Page 3 of 3 TSL001 W23 • U2M ANALYST DATE IN: DATE OU7 TRUE VALUE RESULT % RECOVERY n 1. 'DUPLICATE SAMPLE # RESULT DUPLICATE RPD B0175 CALIBRATION CHECK: IN OUT WINKLER METER ,1,7 0.27)( (4• 3 j= mL =' ' (� mL Chlorine ma r• r• r• ® r•mallow FARM Chlorine WIMNIVEN Chlorine 1 0"IP pr�� —_ :•• 9 00 r• r• r• r• :•r TSL001 W111 , TIM pH Adj.: Chlorine mg/L WWI mv .• •,.Emu�', =!1 Chlorine rng/L��m- cs�ffkt • ffno mm:Jw- umcf=��NRF &165� xER : W12w"1 1 WK07i��ci'`�:��� 5 -MMI Y 00c!) :.. r• r• r• ® r• :•r Y 00c!) V2 -A guse INC. BODS ANALYST: DATE IN: i k DATE OUT: STANDARD DUPLICATE TRUE VALUE SAMPLE # RESULT RESULT % RECOVERY DUPLTrATF e'er r� •• o - Chlorine MR/L Chlorine rn� :•. . 1 wwalwwww-20 '.���m. • •. a • r� . • _, : • • tiTi7� ,• ,. . ,• r�� ,• :•, TSL001 W25 CALIBRATION CHECK: IN OUT WINKLER METE f = mL ML MW 431 Chlorine m : Mes ,r., w 2 C .t, u. s• -n 912 �� �• KIM Chlorine MR/L KMT- M - .t, u. s• -n 912 �� �• :•• F U5,75 • 1-12M "IPS, INC. ANALYST: DATE IN: UK DATE OUT: STANDARD DUPLICATE TRUE VALUE SAMPLE # RESULT RESULT I • �i�' irk I • •Chlorineraw. momap"MWERIPIMH VIES= mIP M w & 10 b MM&" 60M' •Chlorine• AM L_3 il�G�iiv��tliii�►'�� BODS CALIBRATION CHECK: IN OUT WINKLER METER f= mL = ML M Jy Sal) b MM&" 60M' •Chlorine• il�G�iiv��tliii�►'�� cer��is'�■��� Ire � Chlorine mg/L il�G�iiv��tliii�►'�� VIM M!L'ml��•7����r _ wg Chlorine Mo. �=Wwp Mff. «ate,M ■� r�«riMIN w. a`3������ ►3t.w.l Chlorine mg/L min i AIMM EAMM IMMMM��� TSLOOI W26 P 0071 Chlorine :.. VIM M!L'ml��•7����r _ wg Chlorine Mo. �=Wwp Mff. «ate,M ■� r�«riMIN w. a`3������ ►3t.w.l Chlorine mg/L min i AIMM EAMM IMMMM��� TSLOOI W26 P 0071 STANDARD DUPLICATE TRUE VALUE SAMPLE #i RESULTRESULT ,• . ,• INWPA,. mmff:•, % RECOVERY TDUPLICATE •t- 1 RPD 6.J 6.J 6.J 6..A 6.J 6=d bond 6V BODS Chlorine irr���r�r Chlorine mg/L �. � i . mmmeow-4i 1LAI MINIM ARM TSL001 W27 CALIBRATION CHECK: IN OUT WINKLER METER , Y• j= mL c C ML P► cn k 5©o (Y�N> &Tllalbi Chlorine in Ism� ,• ,• . ,• INWPA,. mmff:•, I�1Mr��1�)�i»�� _R M�sa�r��r�i■Ir����� �17M s— &Tllalbi 1 2�rGt _ AA III. - ►n Chlorine-- MR/I, :•• Ism� ,• ,• . ,• INWPA,. mmff:•, _R M�sa�r��r�i■Ir����� �17M s— 1 2�rGt _ AA III. - ►n P mv. > Chlorine-- MR/I, :•• _R M�sa�r��r�i■Ir����� �17M s— P mv. > r.r `r `J Ind 6=d Lm d 6md 6ma P2M PS, INC. BODS ANALYST: DATE IN: DATE OUT: n STANDARD DUPLICATE TRUE VALUE SAMPLE # RESULT, ---RESULT �� �� sir■ �� �■�■�'� % RECOVERY DUPLICATE � RPD ell ►1._t � •. Chlorine:.. 1p � �� �� �� sir■ �� �■�■�'� � 4rw A V-NA10 —%� o; CALIBRATION CHECK: IN OUT WINKLER I= mL = ML --Chlorine mg/L Chlo:.. 1p � �� �� �� sir■ �� �■�■�'� � 4rw A o; CALIBRATION CHECK: IN OUT WINKLER I= mL = ML --Chlorine mg/L :.. IMWINVA .. .. �AChlorine �.173 P 0073 H2M LABS, INC. Pc i sb oo( BROMIDE DATE: i ANALYST: 44/1. A. ,TAS. rG H A = AsA E - AwANK Br (mg/L) = 13,320 x A x B _ D x E D = Ds�E -� � � C F AsuNx DBS = 1.0 mL B a E- NonuWi y of TitraaR = 0.0075 N MLS OF 0.0075N Na=S=O, TITRATED FOR LAB # CLIENT ID[ MLS USED DIFFERENCE G - H RESULT MG/L IODIDE + BR IODIDE C & F AsAmns Ds� o f g' l pp. o. 000 6 S •�0•-� ICB s o. 0000000 Nr ° • osvY3o6-oe,�3.l '0.0000010o.s �.eo•.'' Y• 3• o. 0000 0 I- 3. _ oold . 6 . oo 9007'x- .to -s - a o - oez __L2- 34 I • o..0vo Ys o 0.6 .s - d -6 0.00003 � o•S Alwof -S o _ 3.2 IV -0000500 eo.S . p� _ 3.3 o.'o0001t_�- Z0.S' 3. 0 0. 000 000 0 t o ..i 9.ply- 3•� 2- 0.0000/s^o .lo..� 10. 0000.Q o. q p. 6 /. 2 0.00036 Il' Y. 9 ccB' /. p -0.0000000 os"oY°zY�oo 3-.L 1. d o.OvoBo�,j' ,to•.S W`�G-I p o6 - 6 3•Y v.ovoo,tt -co•J� V.000000 0 �p 06 - oz 6 �• 6 ,e, o o v 33 ,� ..� 0.coo 00 .00.� 6. 7. N CCV 5.0 M91L Ac ccB too P 0010 re% gd/ pl�C BRAN+LUEBBE AACE 5.47 Post -run Report H2M LABS INC. Post -run report Name of Run : CL040405A Name of Analysis :cl.ANL Date of Report . 4/4/05 System No. :1 Date of Run 4/4/05 Type of System :TRAACS Operator : CP Start/Stop time :12:27 - 13:18 Comment mg/1 mg/l msl,gav, tsl Calibr. J d t4a OSO Ay 003 j sL off Corr. Coeff. 1.0000 Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/1 mg/l Calibr. Fit Quadratic Corr. Coeff. 1.0000 Base 62 Gain 18 Sensitivity 0.5420 Sample Limit 1 . Sample Limit 2 . • Value Pk Cup Sample Id 0 0 B Baseline 0.051 0 1 1 P Primer 100.876 1 2 1 D Drift 99.207 1 3 1 Hl High 99.420 1 4 0 Ll Low 0.302 1 5 0 Ll Low 0.302 1 6 1 C Cal. 100.090 1 7 2 C Cal. 74.603 1 8 3 C Cal. 50.516 1 9 4 C Cal. 19.782 1 10 5 C Cal. 9.880 1 11 0 C Cal. 0.078 1 12 9 QC3 CRA 2.0 1.031 1 ` 13 10 QC1 LCS 50 50.528 1,0% 1 14 0 QCIOMBLR -0.123 < 1.0 1 15 11 S 0504002-001A 115.604 5 p 1$8- C6- OW - %Z� 01,2.11 OC 16 12 S 0503771-001E 34.911 110 17 13 S 0504004-OO1C 7.637 1 V Ci- 49iO- DC71 --- *1700S 18 14 S 0504004-002C 9.251 1 -%2L- 0130K 19 15 S 0504004-003C 1.428 1 .0 O3300s - pG2 20 16 S 0504004-004C 5.634 1 -- 1V 0713 033000 •21 17 S 0504004-004CMST✓= 2 S 31.593 104 \/• 1 BRAN+LUEBBE RACE 5.47 QC 1 22 18 S 0504004-004CDUP 5.504 QQa 2 1 %a 1113 j)63- o33oos` 23 19 S 0504004-005C 1.525 1 iD& 41 - 03 ZI oC- 24 20 S 0504004-006C 1.325 1 pE,y,�- �p329v1� 25 2 QCl CCV75 75.208 (00)1. 1 26 0 QC1 ccb -0.064 < 1. J 1 5 Post -run Report F_ L 4 4 5 5 5 5 5 5 5 5 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused 4C 6 Unused QC 7 0 Unused 4 QC Limits Channel QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused 4C 6 Unused QC 7 0 Unused N BRAN+LUEBBE AACE 5.47 •0C 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel Baseline Drift Carry over ** <END OF REPORT> ** C7 2 Yes Yes Yes 1.2 Post -run Report BP"+LUEBBE AACE 5.47 0 Name of run :CL040405A.RUN Comment min Channel : 2 Method : Method 2 Unit : mg/l Base 62 Gain 18 Corr. 1.0000 H2M LABS INC. Post -run chart Post -run chart Name of analysis :cl.ANL Page 1 of 3 2 -------------- J ------------------ ----------------- ------------------' 4 -----------------------------------------------------4------------------I 8 ----------------- ------------------ ----------------- 1------------------� 10 -----------------4------------------------------------a------------------� i SOB 0.051 1P 100.876 12 ------------------------------------ Ir --------------i 2D 99.207 1-------------------- I 63H 99.420 '41, 0.302 14 --- -------------------------------------------------'- 0.302 15L :6C 100.090 ' :7C 74.603 Page 1 of 3 BRVI+LUZM AMM S. 47 Name of run :CL040405A.RUN Comment Post -run chart Name of analysis :cl.ANL Page 2 of 3 BRAN+IMMZ AUX 5.47 Name of run :CL040405A.RUN Comment Post -run chart Name of analysis :cl.ANL Page 3 of 3 :37QC175.257 r r 36 - - -- -------------------------------- r r � 38QC1-0.127 r r r r 39S 1.467 r r r r i r r r :40S 1.358 38 - ----------------'------------------ L - - - - - - - - - - - - - - - --------------- - - - - -' r41S -0.082 i � r r r � X425 198.491 r r r r 5142.623* 40 -- -------1------------- ----r--------- � --------y-------- - - - - -- X443373.934 i r i :455 13.900 r r r r r r r i i46S 18.812 r r r 42 ----------------------------------------------�- �----- ' ---------------- � :47S 45.828 r r r r 148S 18.097 i r i i r r �49QC175.883 r --- ------------J------------------ L ----------------- r i J ------------------ ' r r r r 50QC1-0. 002 r r r r r r r r :515 11.075 r r r r r r r r I 1525 136.054 r r r 46 r -----------------i-----------------r------------------ r r ------------------r X535 18.485 r r r r r r r r 154S -0.074 r r r r r r 1 i 155QCr74.665 r r 48----- ------------ r r r r r r i :57D 99.207, r r � r r r r r r r r i r r r r r r r 50 ---------------------------------- L ----------------- J ------------------ ' r r r r r r r r r r r r 'S8B 0.051 r r r r r r r r r r r r r r r r r r r r 52 r r ----------------- r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r Page 3 of 3 BRAN+LUMM AAC6 5.47 Calibration Curve H2M LABS INC. Calibration Curve •Name of run :CL040405A.RUN Comment Name of analysis :cl.ANL Page 1 of 1 �f BRAN+LOEBBE AACE 5.47 Post -run Report H2M LABS INC. Post -run report Name of Run c1040605 Name of Analysis :cl.ANL Date of Report . 4/6/05 System No. :1 Date of Run 4/6/05 Type of System :TRAACS Operator pw Start/Stop time :12:48 - 13:41 Comment pctsl -T C `(--)o Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/l mg/1 Calibr. Fit Quadratic Corr. Coeff. 1.0000 Base 62 Gain 18 Sensitivity 0.5610 Sample Limit 1 . Sample Limit 2 . r\ 1 Pk Cup Sample Id Value Vaj,de��� 0 0 B Baseline 0.036 �� 0 1 1 P Primer 99.586 1 2 1 D Drift 98.700 1 3 1 H1 High 98.434 1 4 0 L1 Low 0.347 1 5 0 L1 Low 0.347 1 6 1 C Cal. 100.154 1 7 2 C Cal. 74.502 1 8 3 C Cal. 50.480 1 9 4 C Cal. 20.045 1 10 5 C Cal. 9.636 1 11 0 C Cal. 0.147 1 12 9 QC3 CRA 2.0 1.935 1 13 10 QC1 LCS 50 50.785 102;1 1 14 0 QC10MBLK 0.040 1 (4'�v l 15 11 S 0504045-001A 10.358 1 \ / 16 12 S 0504050-001A 32.681 1 17 13 S 0504050-002A 26.771 1 18 14 S 0504050-003A 33.294 1 19 15 S 0504050-004A 23.102 1 M 20 16 S 0504050-005A 5.920 1 21 17 S 0504050-006A 28.345 1 _ • O BRAN+LUEBBE AACE 5.47 >10"/1 Post -run Report 22 18 S 0504050-007A 66.009 1 23 19 S 0504050-OOOA 32.388 1 \l 24 20 S 0504050-009A 27.235 1 25 2 QC1 ccv75 75.233 1007. 1 26 0 QC1 ccb 0.097 L Z.9 '(-1' \. 27 21 S 0504050-010A 34.112 1 28 22 S 0504054-001A 30.929 1 29 23 S 0504056-001A 20.684 1 30 24 S 0504059-001A 25.223 1 31 25 S 0504059-002A 8.354 1 32 26 S 0504059-003A 11.269 1 33 27 S 0504059-004A 12.465 1 34 28 S 0504072-OOIA 10.133 1 35 29 S 0504072-001AMS36.282 io,; , 1 36 30 S 0504072-001ADUP 10.045(VO- O.•1A 1 37 2 QC1 ccv75.. 74.785 IJOY. 1 38 0 QC1 ccb 0.061 ItZ.0 1(�� 1, 39 31 S 0504079-001A 21.834 1 40 32 S 0504079-002A 21.169 1 41 33 S 0504083-001A 138.754 CCCO^ 1 ovti- C04t. 42 34 S 0504083-002A 2.631 1, 1 (porl. 04& 43 35 S 0504084-001A 22.092 1 44 36 S 0504085-OOIA 9.622 1 45 37 S 0504086-001A 5.187 1 0 46 38 S 0504086-002A 5.260 1 47 39 S 0504086-003A 5.241 1 48 40 S 0504086-004A 5.246 1 49 2 QC1 ccv75 74.629 1Do % 1 50 0 QC1 ccb 0.046 t2.0 1 (( � . 0 51 41 S 0504087-001A 37.751 1 ` 52 42 S 0504024-002B V%-[- 3S 60.841 1 53 43 S 0504042-002A 100.798 1 54 44 S 0504067-001B Mv4-1 19.490 1 55 45 S 0504067-002B rnv4 -IS 20.556 1 56 46 S 0504067-002BMS -N>LS 46.757 105'/. 1 57 47 S 0504067-002BDUP 20.300 1.4 1 58 2 QC1 ccv75 74.414 1 59 0 QC1 ccb 0.138 L 2.0 1 (4 �> 60 1 D Drift 98.700 1 61 0 B FinalBase 0.036 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused 00 M C/� BRAN+LUEBBE AACE 5.47 isQC 5 Unused Yes QC 6 Unused Carry over QC 7 Unused 1.1 QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 1.1 ** <END OF REPORT> ** • • Post -run Report BRAN+LOEBBE AACE 5.47 •Name of run :cl04O6O5.RUN Comment • r� H2M LABS INC. Calibration Curve Calibration Curve Name of analysis :cl.ANL Channel :2 Method :Method 2 Curve fit :quadratic a= -2.2652E+000 b=9.7995E-004 c=1.7607E-008 Corr. coeff. :1.0000 Peak [$] 100 r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r i r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r i r r 80 -------L ------ r ------- r------- ------ I ------ L ------- r------- ------- ------ r-- --- r r r r r r r r r r r r r r r r r r r r i r r r r r r r r i r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r t r r r r r r r r r r r r r r i r r r r r r r r r r r r r r t r r r r r 60 ------ r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r r i r r r r r r r r r i r r r r r r r r r i r r i r r r r r r r i r r r r r r r r r r r r i r r r r r r r i r r r r r r r r r r i r r r r r r r r 40 ------r r r r ------r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r i r r r r r r r r r r r r r r r i r r r r r i r r r r r r r r r r i i r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r r i r r r r r r r r r r r r r r r r i r r r r r r r r r r r r 0 r r r r r r r r r r 0.00 10.00 20.00 30.00 40.00 50.00 60.00 70.00 80.00 90.00 100.00 110.00 Conc. [ mg/l ] Page 1 of 1 BRAN+LULBBB AACL 5.47 • Name of run :cl04O6O5.RUN Comment min Channel 2 Method Method 2 1 Unit mg/l 1 t 1 Base 62 Gain 18 Corr. 1.0000 H2M LABS INC. Post -run chart Post -run cbart Name of analysis :cl.ANL Page 1 of 3 I 1 1 1 1 I 1 1 1 t 1 1 I I 1 1 1 I 1 1 I 1 1 1 1 1 1 1 1 1 1 I 1 I 1 2 ----------------- J ------------------ L ----------------- I ------------------ I I I I 1 1 1 1 1 1 1 1 1 1 t I 1 I 1 1 1 I I 1 1 1 I I 1 I 1 1 1 1 i 1 1 t I 1 r 9 -----------------4------------------r------------------+------------------1 1 I I 1 I I 1 1 r I 1 r 1 r I r t 1 I 1 i 1 1 I I 1 1 1 I 1 1 I 1 1 1 1 1 1 I I 1 I I I I I 1 I I 1 1 1 i I 1 1 1 1 1 I I I I 1 I 1 I 1 I I I I 1 t I I 8 ------------------ j ------------------ ------------------I ------------------t I 1 1 1 I I 1 1 1 I 1 t 1 r r 1 i 1 1 1 I I 1 r I I 1 1 I I I r r I I I 10 ---------------- a - - - - - ------- ----- ------------- - - - - --------- ---------- -' 1 1 1 I 1 1 1 1 I i I 1 :OB 0.036 I 1 1 I 1 i1P 99.586 1 1 1 12 --------------� 98.700 1 � 12D 1 1 I i3H 98.434 1 I 1 1 1 '9L 0.347 i 1 1 1 14-- -------------- ------------------ L-----------------j------------------ I ' ' 1 r5L 0.347 1 1 I 1 I l6C 100.154 1 1 1 I 1 1 1 ' 17C 74.502 1 1 1 t I r Page 1 of 3 BRW+LUMM AACE 5.47 Post -run chart Name of run :cl04O6O5.RUN Name of analysis :cl.ANL Comment Page 2 of 3 I I I I I 1 ' :9C 20.045 I I 1 I I I 1 �10C 9.636 18 ---------- - - - - ------- 1 ------- - - - - - - ------------------------------------1 I 1 111C 0.147 I 1 1 1 1 1 1 1 '120C3 1.935 I I 1 I I 1 I 113QC150.785 1 1 20-- --------------J------------------L-----------------J------------------I114QC1�.040 I I 1 1 1 1 1 1 1 1 1 15S 10.358 1 t I 16S 32.681 I 22 ----------- - - - - -- - - - -- 1 I -- --------- -r- - -- --- ------------------i '---''-'-- 17S 26.771 I I i I I 1 i �18S 33.294 I I i I I 1 19S 23.102 I I I I 24 - - - - - ----------------------------------------------------------------1 I 120S 5.920 I I 1 I I I I :21S 28.345 I I 1 I I I 1 1 ' ' '22S 66.009 I I I 1 1 I 26 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ - -- -------- --- - - -J__ L------------___--J_-------____------I 32.388 1 � � 1235 I I 1 I I I ' �24S 27.235 I I ' 25QCD5.233 1 1 28-- ---------------------------------r-----------------y------------------126QC10.097 I 1 1 1 1 I 1 I I i 1 1 I 1 1275 34.112 1 1 1 I 1 1 :28S 30.929 I I 1 30 ---------------------------------------------------------------------I 1 I 1 129S 20.684 1 I 1 1 1 1 i :30S 25.223 1 t 1 I 1 1 1 131S 8.354 I I I 1 I I 1 1 32 - - - - - - - - - - - - - - - - J ------------------ L ----------------- J ------------------ ' 11.269 I 1 1 132S 1 1 I I I I I 1 33S 12.465 1 I 1 1 1 I 134S 10.133 1 I 1 I I I ----------------------I ----------------------------- --- -------- -----------------------------------135S 36.282 1 I I 136S 10.045 Page 2 of 3 BRAN+LULBBE AACE 5.47 Name of run :cl04O6O5.RUN Comment Post -nm chart Name of analysis :cl.ANL Invi '37QC174.785 36 ----------------------------------------------- --- �-� ------------------� i 380C10.061 �39S 21.834 ' 140S 21.169 i 38 -----------------'------------------L-----------------'�------------------ 5138.754* � � � '42S 2.631 :43S 22.092 90 ----------------ti------------------r-----------------y------------------'44S 9.622 i 145S 5.187 :46S 5.260 42 - - - - - ----- - - - - -------------------- � -----------------------------------� � � '47S 5.241 48S 5.246 ' :49Qcr74.629 ---------------J----------------- -L------ ---- ----- - -J- - ----------------' 0.046 � � � �SOQC1 �51S 37.751 152S 60.841 46 ---------- ---------------- -----------------+------------------r--- i---- - i 100.798 �53S i i54S 19.490 :55S 20.556 48----------------- --------- i ---------------- - -'i 56S 46.757- i57S 20.300 ' �580c174.414 50 - ---------------J----------------- - L - - - - - - - - - - - - - - ---------------- - - - - -' 0.138 � � � i59QCl :60D 98.700 -- - - - - - - - - - - -- :61B 0.036 Page 3 of 3 112M LABS, INC. • Anal st t Date:2 Start time: ) ; COD WS Calibration 1/6/2005 cont abs 0 0 10 0.01 25 0.016 50 0.025 125 0.055 250 0.105 375 0.153 500 0.202 625 0.257 750 0.305 8751 0.353 10001 0.404 Intercept (b) -10.742 slope (m) 2501 r 0.9999 COD Calibration 1/05/2005 1100- 1000- Y =2500.7x -10.742 900- 800- 700- 06 0080070006 600 • conc . 500 —Linear (conc) ci C 400- 300- 200- 100 00300200100 044 -100 GD 0.4242 Absorbance 9t,Ak 1001ST 0 Pag*1 0 1 1e • COLOR/ODOR DATE: I I2 6< COLOR STDS VERIFIED START TIME: 15100 5 TNRU 70: ✓ ANALYST:h; ; I P v4,n`n O N CLIENT ID LAB* ICV (40) COLOR UNITS a� DF ODOR UNITS NOTES f u c IuJ ;4 ICB - c 5 c0•au l CACI cx>zA FS OS 032 -aovA — lu- Wnw - 5n 3o CCV (40) CCB 6 v \-J ovi - 34 4051�— MW . ---- : � Z tAW l,\Ak CCV (40) CCB O N COLOR STDS VERIFIED 5 THRU 70: COLOR/ODOR r DATE: START TIME: : 30 P C ! Sb vv( ANALYST: CLIENT ID LAB* ICV (40) COLOR UNITS v p DF ODOR UNITS NOTES 1007 ICB �3� D ors-oo(fj a C3Oe( oso - 00m. v, oe/ oSi�- aZ .c.i o oe/ on-Mrs,r,i d, 0el Psv- 9 f �,�' V, to/ 94 -p -W ,c,� o, off CCV (40) CCB S- D �' ►� o.Soy p.%- v0 �S O Opl OP - 04YA zi Ol no 1 cot ofo -O/o �.� t7 0of 7 CCV (40) t7 Joe ' CCB f7 LAOS, INCo CR+6 DATE: eA1zIJS ANALYST: C iwr ID Lmm MLS USED ABS. DILUTIONS MG/L NOTES ICV (0.20 mg/L) �S V ��►� ac- 17-5-4 ICB - 3 2 7. -oa Oz- -$S -c�4fj 0,y > TJ=o. s.F b 0.11415' rr,,. r13. . CCV(0.20 mg/L) O, 1 53 14. CCB 17. 19. 20. 21. 22. 23. .. 25. CCV(0.20 mg/L) 5n b iS q� fpL = ��.5 %• CCB p.,J✓ <�.�Z P 0092 ]U2A LABS, INC. CR+6 DATE: Y- Pers,6 vol ANALYST: A-I&Ij AOPtfgf&OV 7:a0 r is 7.X,/X P CC94 i�►Jr .A lot", � � /_-�_, 7.X,/X P CC94 Calibration 116105 conc abs 0 0.000 0.02 0.017 0.04 0.034 0.1 0.082 0.2 0.16 0.3 0.245 0.41 0.321 Intercept (b) -0.0012 slope (m) 1.24 corr. Coeff. 0.9999 TSL001 W50 Cr+6 1/6/05 0,5- y 1.243 x - 0.0012 0.4 ,� ♦ cont J �6 0.3 —Linear (conc) E C 0.2- 0 V 0.1 0 0.000 0.050 0.100 0.150 0.200 0.250 0.300 0.350 Absorbance Page 1 of 1 • 1-12M 1135, INC. HARDNESS�- COIC Iun 64kZ7W,- . LofA R'IGWGU-/ DATE: _ •j�- � - oS c� �ja6 ANALYST: 00 HARDNESS = B x N x 100 0 TITRANT A= p. v/ Neor P 0022 •f BRAN+LUEBBE AACE 5.47 Post -run Report H2M LABS INC. Post -run report Name of Run NH3040705 Name of Analysis :NH3.ANL Date of Report 4/7/05 System No. :1 Date of Run 4/7/05 Type of System :TRAACS Operator CP Start/Stop time :10:28 - 11:06 Comment :#13164 1 TSL T SL ool Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 • Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 1 H1 High 4 0 L1 Low 5 0 L1 Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. 11 0 C Cal. 12 5 QC1 CRA 0.1 13 8 QC2 LCS 0.5 14 9 QC3 LCS 2.5 15 10 OC10MBLK 16 11 S 0503734-OOIA 17 12 S 0503734-002A 18 13 S 0504024-OO1D JJW - 3� 19 14 S 0504024-002D (iVj 35 20 15 S 0504024-003D KW - Si 21 16 S 0504024-004D 04 tj —576 • Real Data 2 2 NH3 Dilution mg/L mg/L Linear 0.9998 75 37 0.2937 i�o14 Value VAa X ��\dS 0.020 0 3.013 1 3.003 1 3.015 1 0.031 1 0.031 1 3.013 1 0.975 1 0.470 1 0.191 1 0.106 1 0.025 1 0.093 1 0.523 1 2.681 �J% �/, 1 0.024 <-O. ( 1 6.048 10 25.566 20 17.575 5 a4y - 17.315 � 5 17.325 5 3.600 5 BRAN+LUEBBE AACE 5.47 ��_ Qp Post -run Report • 22 17 S 0504024-005D n4� - c� 0.226 GtiC/K�u N 5 �� WX- 23 18 S 0504024-006D h W- C s 0.179 5 24 19 S 0504024-007D 11W - 17.742 5 OVelf L` 25 20 S 0504024-008D ii W 8S 8.713 5 X 26 2 QC4 CCV 1.0 0.980 '� pp 7• 1 27 0 QCl0CCB 0.043 <0.1 1 28 21 S 0504024-009D E QVIr. 8lkNK 0.096 1 29 22 S 0504067-001D WJ- ID 0.126 h 5 ttv-0k V c1Qt 30 23 S 0504067-002D h W - IS 0.208 1(i�N 5 31 24 S 0504067-002DMS Jtlf- S;O 5.052 10 r_p� 32 25 S 0504067-002DDUP 0.102 u 5 33 26 S lfb-13164 T1/Z. S.0 5.241 IQs%. 10 34 27 S lfbd-13164 5.312 VD 1x 10 35 2 QC4 CCV 1.0 0.971 14'? '/. 1 36 0 QCIOCCB 0.035 <.0.` 1 37 1 D Drift 3.003 1 38 0 B FinalBase 0.020 1 QC Limits Channel 2 QC 1 Cond. 1 Below Limit 1 0.080 Cond. 2 Above . Limit 2 0.120 QC 2 Cond. 1 Below Limit 1 0.400 Cond. 2 Above Limit 2 0.600 QC 3 Cond. 1 Below Limit 1 2.000 Cond. 2 Above Limit 2 3.000 OC 4 Cond. 1 Below Limit 1 0.800 Cond. 2 Above Limit 2 1.200 QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS • Channel 2 M 0 BRAN+LUEBBE AACE 5.47 Post -run Report •Baseline Yes Drift Yes Carry over Yes %: 2.4 ** <END, OF REPORT> ** [7 • BRAIHLUEBBE NICE 5.47 0 Name of run :NH3040705.RUN Comment :#13164 nun Channel 2 Method NH3 Unit mg/L Base 75 Gain 37 Corr. 0.9998 H2M LABS INC. Post -run chart Post -rum chart Name of analysis :NH3.ANL I I I I I 1 1 1 1 I I 1 1 1 1 1 1 1 I 1 I 1 1 1 I I 1 1 1 1 I 1 1 1 1 1 2 ---------------- J ------------------ L ----------------- ------------------1 1 1 1 I 1 t I I I 1 1 1 1 I 1 1 I 1 1 1 1 I 1 1 I 1 I 1 1 I I 1 i I 1 1 1 ------------------ ------ 1 1 1 1 1 1 1 1 1 1 1 1 1 I 1 1 1 1 1 I 1 I 1 1 I I 1 1 1 I I 1 1 1 1 1 1 1 1 1 1 1 1 I 1 I 1 1 1 I 1 I 1 I I 1 1 1 I I 1 1 S 8---------------------------------------------------------------------1 1 I 1 1 I 1 1 1 1 1 1 1 1 1 1 S 1 1 1 S 1 1 1 1 I 1 1 10L ---- 4 ------------------ 1� ------------------ 1 I 1 I S 1 I 1 S I 1 I SOB 1 1 1 I 1 1 I jlP ' 1 1 12 1 - - - - - -� 1 I , I 1 I 1 1 1 I 13H 1 1 1 ' 14L 19 --------- -------------------------- L-----------------�- 1 1 I -----------------151, 1 1 , 1 t 6C 1 , S 1 1 1 17C 1 , S Page 1 of 3 0.020 3.013 3.003 3.015 0.031 0.031 t/) 3.013 O 0.975 BRAN+LUEBBE RACE 5.47 Name of run :NH3040705.RUN Comment :#13164 Poet -run chert Name of analysis :NH3.ANL 1 1 1 1 19C 0.191 1 I I 1 �10C 0.106 1 1 r 1 1 1 1 1 18 ----------------j- ' 111C 0.025 1 1 1 1 1 1 1 1 :120C1 0.093 1 1 1 1 1 I I 1 1 1 1 113QC2 0.523 1 1 I 1 20------------------ �------------------- ---------------------- :140C3 2.681 1 I 1 1 1 1 15QC10J.024 1 1 I I 1 1 1 1 �16S 6.048 1 1 1 I 22 1 1 1 ----------------- 1 1 X175 25.566 r 1 1 S 17.575* 1 I 1 S 17.315* 1 29 ----------------- i ------------------- --------- ----------------- ' S 17.325* I 1 1 1 I 1 �21S 3.600 1 I 1 1 I 1 1 I 122S 0.226 1 1 1 1 r 1 1 1 26----------------J------------------L------------------------------------'23S 0.179, 1 r 1 1 1 1 I 1 1 1 I I S 17.742* 1 r 1 �25S 8.713 1 I 1 28 1 ------------- -----,-----------------�----------------- �------------------:26QC9 0.980 1 r 1 1 1 r 1 r27QC109.043 1 1 1 1 1 r 1 1 i :28S 0.096 1 1 r 1 30--------------------------------------------------- ------------------ 1 11295 0.126 1 1 1 1 I 1 I 1 �30S 0.208 1 r 1 1 r 1 r 1 131S 5.052 1 1 r 1 1 r 1 r 32 - - - - - - - - - - - - - - - - - J ------------------ L ----------------- J ------------------ I 132S 0.102 I 1 r 1 �33S 5.241 r 1 1 1 �34S 5.312 1 I 1 ----------------------------------r------------------------------------r , 135QC4 0.971 1 1 1 1 1 1 1 -360C10J.035 Page 2 of 3 BRAN+LUEBBE ALICE 5.47 Name of run :NH3040705.RUN Comment :#13164 Post -run chart Name of analysis :NH3.ANL I I 1 :37D ----- L ----------------- j - , 1 I 1 1 I I 1 I I I 1 1 1 1 I 1 I 1 r 1 I 1 r 1 1 1 1 138E 1 1 r 1 1 I r r 1 I 1 ----------1 1 1 1 1 1 1 1 1 1 1 r 1 r I 1 1 1 1 I r r I I 1 1 1 I 1 1 1 1 1 1 1 1 1 1 I 1 1 1 r 1 1 1 1 r 1 1 1 1 1 I 1 i 1 r I 1 1 I 1 1 1 i I I r 92 --- �- 1 - - - - - - --- -----------------1 ------------------------------- ------ r i -- I- 1 1 1 1 1 1 I 1 I I 1 1 I I r I I I I r I 1 I 1 1 I I 1 I I I 1 - - - - - - - - - - - - - - - - J ------------------ L ----------------- 1 ------------------ I I 1 i 1 1 1 t 1 1 I I 1 1 I 1 1 I 1 1 1 1 1 1 I 1 1 1 I I 1 I 1 1 1 I -----1 I 1 I 1 1 r I 1 1 r I I 1 I I I I 1 1 I 1 I 1 1 1 1 1 1 I I r I 48 I -------1 1 1 1 1 1 1 1 1 1 1 I I I I 1 I I 1 t 1 1 1 1 I 1 1 r 1 I r I 1 50 ----------------- J ------------------ L ----------------- j ------------------' 1 1 1 I 1 I 1 1 1 1 1 1 1 i r 1 1 1 I 1 I 1 I 1 I 1 1 1 1 I r 1 1 1 I r 1 r 52 ------------------ ------------------I-------- +------------------I 1 I 1 I I I 1 I I 1 i 1 I I 1 1 1 1 1 I 1 I 1 1 1 1 1 1 1 1 I Page 3 of 3 3.003 0.020 r - v> C/] BRAN+LUEBBE AACE 5.47 H2M LABS INC. Calibration Curve ame of run :NH3040705.RUN omment :#13164 Calibration Curve Name of analysis :NH3.ANL Page 1 of 1 00 O O H • BRAN+LUEBBE AACE 5.47 Name of Run : NH3040705A Date of Report , 4/7/05 Date of Run 4/7/05 Operator CP Comment :#13164 TSL H1 High Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 . Sample Limit 2 . is Pk Cup Sample Id H2M LABS INC. Post -run report 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 1 H1 High 4 0 L1 Low 5 0 L1 Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. 11 0 C Cal. 12 5 QC1 CRA 0.1 13 8 QC2 LCS 0.5 14 9 QC3 LCS 2.5 15 10 QC10MBLK 16 11 S 0504024-OO1D fiMi '3-b 17 12 S 0504024-002D MW -3'S 18 13 S 0504024-003D KW -S b 19 14 S 0504024-OOSD MW - 20 15 S 0504024-006D t(W - 6.S 21 16 S 0504024-007D MW- 8�10 Name of Analysis :NH3.ANL System No. :1 Type of System :TRAACS Start/Stop time :11:23 - 11:57 Real Data 2 2 NH3 Dilution mg/L mg/L Linear 0.041 0.9996 1 76 33 3.019 0.2873 1 ValueVa e V O �\\A 0 023 0 3.000 1 3.002 1 3.009 1 0.041 1 0.041 1 3.019 1 0.950 1 0.476 1 0.192 1 0.104 1 0.035 1 0.091 1 0.546 1 2.735 1 0.005 <0-1 1 23.496 20 29.523 20 45.147 20 0.055 1 0.058 1 40.132 20 Post -run Report CN C) 0 BRAN+LUEBBE AACE 5.47 2 2 QC 1 •22 17 S 0504067-001D tiia ' D 0.003 0.080 1 23 18 S 0504067-002D MW S 0.130 0.120 1 24 19 S 0504067-002DMS#- - 5.166 101 X 10 25 20 S 0504067-002DDUP 0.052 tJQ PC'. 1 26 2 QC4 CCV 1.0 0.997 2.000 27 0 QCl0CCB 0.034 3.000 QC 4 28 21 S lfbl-13164 0 5.348 i o7 �, 10 29 22 S lfbdl-13164 5.325 dJ-10 QC 5 30 2 QC4 CCV 1.0 0.945 Lf'/. 1 31 0 QC10CCB 0.037 O•� l 32 1 D Drift 3.002 1 33 0 B FinalBase 0.023 1 QC Limits Channel 2 2 QC 1 Cond. 1 Below Carry over Limit 1 0.080 3.3 Cond. 2 Above Limit 2 0.120 QC 2 Cond. 1 Below Limit 1 0.400 Cond. 2 Above •Limit 2 0.600 QC 3 Cond. 1 Below Limit 1 2.000 Cond. 2 Above Limit 2 3.000 QC 4 Cond. 1 Below Limit 1 0.800 Cond. 2 Above Limit 2 1.200 QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline yes Drift yes Carry over yes %: 3.3 C7 Post -run Report 0 C/) BRAN+LUEBBE AACE 5.47 • ** <END OF REPORT> ** • • Post -run Report 0 BRAN+LDEBBE AACE 5.47 H2M LABS INC. Post -run chart Names of run :NH3040705A.RUN Comment :#13164 Pott -tun chart Name of analysis :NH3.ANL Page 1 of 2 BP.AN+LUEBBE AACE 5.47 Name of run :NH3040705A.RUN Comment :#13164 Post -nm chart Name of analysis :NH3.ANL Page 2 of 2 BRAN+LUEBBE AACE 5.47 H2M LABS INC. Calibration Curve ame of run :NH3040705A.RUN comment :#13164 Calibration Curve Name of analysis :NH3.ANL Page 1 of 1 1-12M LA[3S, ilwo -Ts i-Oo ► • AMMONIA DISTILLATION NAME: PNI;` ► J Sf DATE: LAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE VOLUME_ MLS FINAL VOLUME MLS DATE ANALYZED SPIKE Z •`� 4 � �-�►Q GPS t � 056 OZA-Nl mw- 3 t> Mw - 3S mw -SD -•5S —ocrW vA vJ— (a mow_ vJ - 8 5 (6 -o-.A r> c.,,;o4. 1 k b7 -boli --002 r� vJ -• � S 5► D d� -cl�zD S, c7 p 0099 BRAN+LUEBBE AACE 5.47 • H2M LABS INC. Post -run report Name of Run no3040505R1 Name of Analysis :NO3.ANL Date of Report : 4/5/05 System No. :1 Date of Run 4/5/05 Type of System :TRAACS Operator cp Start/Stop time :13:37 - 14:42 Comment tsl Channel Type Channel Method Unit Calibr. Fit Corr. Coeff. Base Gain Sensitivity Sample Limit 1 Sample Limit 2 • Pk Cup Sample Id 0 0 B Baseline 1 1 P Primer 2 1 D Drift 3 6 H1 High/no2 4 0 L1 Low 5 0 L1 Low 6 1 C Cal. 7 2 C Cal. 8 3 C Cal. 9 4 C Cal. 10 5 C Cal. 11 0 C Cal. 12 5 QC1 cra0.1 13 10 QC1 lcsl.13 14 0 QC1 mblk 15 11 S 0504043-001A 16 12 S 0504043-003A 17 13 S 0504043-005A 18 14 S 0504043-007A 19 15 S 0504045-001A 20 16 S 0504050-001A •21 17 S 0504050-002A Real Data 1 2 NO3 Dilution mg/l mg/1 Linear 0.9997 90 12 0.8622 Value V� Va a , �\ 5 � , X9,0 �1 0.010 0 2.000 1 1.999 1 2.028 1 0.024 1 0.024 1 2.016 1 0.977 1 0.479 1 0.197 1 0.106 1 0.016 1 0.105 1 1.124 'RQ i. 1 0.008 46.1 1 15.116 10 9.984 10 15.854 10 15.798 10 3.545 10 5.268 10 3.633 10 Post -run Report O 0 S 0T'T 4;% M14 aZ00-L90i0S0 S 8S OL• S OLV T _ Mu aT00-LMOSO S LS 69 T ZE9'0 VZ00-0900090 S 99 89 J T T£0'0 VT00-090i0S0 S SS L9 S 09L'T vZ00-Z6060S0 S 6S 99 T £TO'0 �1Q -d,nb-3x600-eZ0i0S0 S £S S9 I A Q d� WS0'0 A anaa800-6ZOi0S0 S ZS t9 T *A 101 90S'0 S'0 , jilSFM800-6ZMSO S TS E9 T ('O> SOO'0 Q33 Too 0 Z9 T � ph 696-0 0' TAOo TOO Z T9 T L£O'0 s 8 _ MN a800-6206050 S OS 09 OZ £99'8T (18 - MLS aL00-6Z060SO S 66 6S S OWE SIJ - M1� x900-HMSO S 86 8S T S6T'0 Q� r1� aS00-6Z0i0S0 S L6 LS S E60'Z SS _ Mu a600-6ZOi0SO S 96 9S S OZZ'8 4ds _ Mu a£00-iZ060S0 S S6 SS S 89S'Z Slt - mu aZ00-6Z060S0 S 44 65 OZ OZO'6£ Qimli aT00-tMOSO S E6 £S T t90'T VZ00-6Z8EOSO S Z6 ZS T EL9'T KT00-6Z8£OSO S T6 TS T 1-P> ZT0'0 CPO TOO 0 OS I ',<CoI T00'T O'TAZ3 TOO Z 66 S LEE'6 VZ00-Z6L£OSO S 06 86 /1p� ►+�A- , T 080'0 VT00-Z6LEOSO S 6E 0 S h1 aJ L99'TT VZ00-06LEOSO S 8E 90 T SiZ'0 VT00-06LEOSO S LE S6 T S08'0 VZ00-SLLEOSO S 9E 66 T 6Z0'0 VT00-SLLEOSO S S£ E6 T T W O W00-6S060SO S 6E Z6 T 9ES'O YE00-6S060SO S EE Tb I 920'0 anaYZ00-6S060S0 S ZE 06 T 886'0 S10_/1_LSMZ00-6S060SO S TE 6£ T 07 L00' 0 CPO Tab 0 8E T ' / OQj 966'0 0'iLOa T30 Z LE T OEO'O VZ00-6SOi0SO S OE 9E T 8EE'0 VT00-6SOiOSO S 6Z SE S 609'9 `iT00-9SOiOSO S 8Z K S £6L'0 VT00-6S0i0S0 S LZ E£ S 900'T YTOO-£506050 S 9Z Z£ OT OZ91S VOTO-OSOi0SO S SZ T£ OT L99'E K600-OSOi0SO S 6Z OE OT EST'S V800-OSOi0SO S EZ 6Z OT SST'£ VL00-OSOi0SO S ZZ 8Z •yon ,Afp"kYY1 OT hffy4" 606'0 K900-0S0i0S0 S TZ LZ T ''0-7 600'0 Qoo TOO 0 9Z T %gl:, T86.0 O'TAoo 130 Z SZ OT 860'T vS00-OS060S0 S OZ 6Z OT SE£'S V000-OS040S0 S 6T EZ OT SZ6'S HE00-OS060S0 S 8T ZZO ;iodag utu-�sog LV S 3DYY 3HH3n I+Mg BRAN+LUEBBE AACE 5.47 K -W —1 S QC 1 71 59 S 0504067-002DMS i 2-r 3.520 5 72 60 S 0504067-002DDUP QC 5 1.117 Ob 3y' 5 73 2 QC1 ccv1.0 Unused 1.005�WC�11 1 74 0 QC1 ccb QC10 0.008 <0.1 1 75 1 D Drift 1.999 1 76 0 B FinalBase 0.010 1 QC Limits Channel 1 QC 1 Unused QC 2 Unused OC 3 Unused OC 4 Unused QC 5 Unused OC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS *Channel Baseline Drift Carry over ** <END OF REPORT> ** • 1 Yes Yes Yes 2.0 Post -run Report 00 Vi BRAN+LUEBBE Amz 5.47 • Name of run Comment no304O5O5R1.RUN H2M LABS INC. Post -run chart Post -run chart Name of analysis :NO3-ANL min Channel : 1 Method : NO3 Unit : mg/l Base 90 Gain 12 Corr. 0.9997 r r r r r r i r r r r r 2 ----------------- ------------------ L ----------------- J ------------------' r r r r r r r r r r r r r r r r ------------r------------------ ------------------r r r r r i r r --------------- ------------- r r r r r r r r r r r r r r r r r r r r � r r r e------------------ ------------------'------------------1------------------' r r r r r r r r r r r r r r r r r r r r r r r r r r t r r r i r r r r r 10 - ---------------4------------------------------------4------------------r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r r 12 r---------------� -----� r r r r i r r r r r r r r r r r r r r 10B 0.010 r r r 19 r ----------------- ------------------- r ' ---------61P r 2.000 r i r 2D 1.999 r r r r3H 2.028 r r r r i r Page 1 of 4 BRAN+LUMM AACE 5.47 Name of run :no304O5O5Rl.RUN Comment Post -run chart Name of analysis :NO3.ANL Page 2 of 4 r r r r r r r r5L 0.024 , r :6C 2.016 , r r '_ OC 0.977 18 ----------------- ---- r - - - - --L r r r r r r ' 8C 0.479 r r r r r r r r r r r r r 19C 0.197 r r r r r r r r 0.106 20 -------------a--- r --------------------------------r------------------ilOC r r r r r r r �11C 0.016 r r i r 12QC1 0.105 r r r r , r r 22 - - - - - - - - - ---------------4------------------i13QC11.124 - - - - - - - - - - - - - - - - - - - - - -- - -- r r r i14QC1 0.008 r r 15S 15.116 , r r 24 ------------------'-------------- L ----------------- -' ------------------ 116S 9.984 , r r :17S 15.854 , r r r r r i r r 118S 15.798 r r r r r r r :19S 3.545 26 ------------------------------------r------------------ ----- r r r r ' '20S 5.268 r r r r r r r :21S 3.633 r r r r r r 28 ------------------ ------------ r--------- -t------------------:22S 5.925 r r r r t23S 5.335 r r r r r r r :24S 1.048 r r r r r 30 - - - - - - - - - - - - - - - -- �-- -� r ----------------- r--------r25QC10.981 �- r r r 26QC1 0.009 r r r r '27S 0.409 r r r r r r r r 32 r ----- - - - - -------- r --------------- L- r --------------------------------- - - , r 28S 3.158 r r r r r r r r r ' 5.183 r r r'29S r r r r �30S 3.667 r r r r r r r r -- - - - - - - - - - - - - - -- ---- - - - - - - - - - -r- - - - - -t--------- :31S 5.624 ------------ - - - - - - - - - r :32S 1.005 r r r r r r r r Page 2 of 4 BRAN+LOEBBB AMZ 5.47 Name of run :no304O5O5Rl.RUN Comment Post -run chart Name of analysis :NO3.ANL 1 - 1 -----------------------------------------------------1---------------- S11.667- :47S 1.667 - 1 1 1 1 1 I 1 1 147S 0.080 1 1 1 1 1 I 1 1 1485 4.337 1 1 1 1 1 1 1 46-----------------i--------------f-----------------1------------------ i49QC11.001 1 1 1 I 1 150QC1 0.012 I I 1 1 1 1 151S 1.673 1 1 1 1 1 1 1 1I 'I1 1II 52S 1.064 ------------- ------48 ----------------- --------'------------------'53S 39.020 I 1 I 1 I 1 1 1 1 154S 2.568 I I 1 1 II 50 ----------------- J ------------------ L -------------- ------------------ 155S 8.220 1 1 1 1 1 i33S 0.793 I I 1 1 1 1 1 :56S 1 6.609 I - - - - - - - - -� - - ----- - - - - - - ------------------134S I 1 1 I 1 ' :35S 0.338 I 1 1 1 I I 1 157S 0.195 I 1 I i i I 136S 0.030 I I I 1 I I 1 38 - - - - - - - - - - - - - - - - - ------------- ------------ - - - - --------------------:37QC10.996 ---------F-----------------4 ------------------ I I 1 1 1 I I 1 1 1 I 1 1 i38QC1 0.007 I I 1 159S 18.663 I I 1 1 I 39S 0.488 1 1 1 I I I i 1 I I --r-----------------+------------------r40S 0.026 40 -_- ------___ ---- _ ----------- --- 1 1 1 1 I 1 I I I I 141S 0.536 I I I I 1 1 I '42S 0.031 143S 0.029 42 --------------------------------- ------------------------- I 1 1 :44S 0.805 1 1 1 145S 0.245' 1 1 1 I 1 - 1 -----------------------------------------------------1---------------- S11.667- :47S 1.667 - 1 1 1 1 1 I 1 1 147S 0.080 1 1 1 1 1 I 1 1 1485 4.337 1 1 1 1 1 1 1 46-----------------i--------------f-----------------1------------------ i49QC11.001 1 1 1 I 1 150QC1 0.012 I I 1 1 1 1 151S 1.673 1 1 1 1 1 1 1 1I 'I1 1II 52S 1.064 ------------- ------48 ----------------- --------'------------------'53S 39.020 I 1 I 1 I 1 1 1 1 154S 2.568 I I 1 1 II 50 ----------------- J ------------------ L -------------- ------------------ 155S 8.220 1 1 Page 3 of 4 Cid I I 1 1 - :56S 2.093 1 1 1 1 1 1 I 157S 0.195 I 1 I 1 1 1 1 i58S 3.650 52 ----------------- ------ ---------F-----------------4 ------------------ 1 1 1 1 I 1 1 1 1 1 159S 18.663 1 1 1 I 1 1 1 1 :60S 0.037 1 1 1 1 Page 3 of 4 Cid BRAN+LUZBU AMM 5.47 Name of run :no304O5O5Rl.RUN Comment Post -run chart Name of analysis :NO3.ANL Page 4 of 4 ----------- - - - - -------- - - - - -- ----------- - - - - ----_-- ----- r r �620C1 '768 0.010 , , r 0.005 66 ----------------- ---- ---------�---------� , '63S r 0.506 r , , r 56 ---- ----------j ------------------ L ----------------- ------------------'64S 0.054 1-----------------j- �65S 0.013 66S 1.760 70 - - - - - - - - - - - - - - - -------------------- L- - - - - - - - - - - - - - - - - - a - - - - - - - - - - - 58 --------------4------------------r-------------------------------------:67S 0.031 , , r ' 168S 0.632 , , r , , --------------- , �69S 1.170'i 60 --------- , , , 1.147 ------------'70S r r r r i71S 3.520 , r , 172S 1.117 62 -----------------1-------------- L ----------------- j ------------------ 173QC11.005 '740C1 0.008 r , , r 175D 1.999 r r r r , , Page 4 of 4 '---- - - - - - r , , '768 0.010 , , r 66 ----------------- ---- ---------�---------� , , r 1-----------------j- 70 - - - - - - - - - - - - - - - -------------------- L- - - - - - - - - - - - - - - - - - a - - - - - - - - - - - - - - - - - -' , , --------------- , Page 4 of 4 BRAN+LUEBBE AACE 5.47 H2M LABS INC. Calibration Curve •Name of run :no304O5O5Rl.RUN Comment Calibration Curve Name of analysis :NO3.ANL Page 1 of 1 � u u u �tm,t�QZ u Id2A I -AUS, INC. Phenols Method 420.1 Distillation Date: - 12 -OS Time: 1:10 i.pt.,O, . qu4,,-Kf e AV 003 pIS°!it o a ( Analyst: b0pvgo-oti Date: WI/ 0 Phen• P 00A 5-11 111-1il iii V,6^1,fA ■ � - ® �� err■■ . �, ■��■�■■■�■e� reTiMMIN WMIN 0 Phen• P 00A Calibration 1.24-05 cone abs 0 0 00 5 0.01 10 0.022 20 0.048 30 0.072 40 0.099 50 0,122 Intercept (b) 0.6708 slope (m) 402.96 r 0.9997 60 50 40 30 C V 20 10 0 0.000 Phenol Calibration 1124105 ., 0.050 0.100 0.150 Absorbance Page 1 of 1 0 0 96x + 0.6708 • cont —Linear (cone) sLrn 1001ST SULFATE PC / 5k of • Xt %�—PSS 0 �S DATE: ANALYST: Y- 8 - oS Si vK�toL It 3o CLIENT ID LAB# MLS USED ABS. MG/L (GRAPH) MG/L NOTES ICV (20.0 mg/L) is- U . 2 y I`B if- '0.010,0 iso ,r Oma - oor b 5-0 o• IM 9•Y )ts-: Y?. o M W, A PN- Vou aS 0-19Z IQ Me - S'ID OZ - 00h 3.0 t. Zo 8 g. Y xS'= 0 fly- l--or -ft CCV(20.0 nVX) z� 0.2 y . Z to CCB h wit- fly - vom a 0.193 Is b r,S: 790 jar -S Olt- 900 11� 0. I 2— / • 8 oly- 001A Js- 0.003 -1S . 0 ,t- of? .o- 3z 1 CCV(20.0 mg/L) 0. Z ' CCB I vS'v og -002h S'o o. 09f 9.S kr y7.s 1 06 -oo S- o o . 3 d o ,�� f.S, I YB s- • ra0 /,G 1 1F3^e0f,e S.0 10-Y3 �- &VIR S.O o-If 0 TZ !1 CCV(20.0 mg/L) CCB S o, 2 . z lotB. • jeCCV(20.0 mg/L) CCB 0077 Calibration 01120/0$ conc abs 0 0.000 5 0.03 10 0.091 15 0.16 20 0.23 25 0.306 30 0:375 35 0.464 40 0.544 Intercept (b) 2.6$63 slope (m) 70.96 corr. Coeff. 0.9957 0 LLAN t OO ISI SO4 01/20/05 y = 70.956x + 2.6553 40- 00OF 30 E 20 • • conc —Unear (conc) V 10- 0 0.000 0.100 0.200 0.300 0.400 0.500 0.600 Absorbance Page 1 of 1 • • IDS TD SS/ TS AIDITY: X. A 2,-I. l ;Vo TSLQ01 W78 CLIENT ID MOM TARE WEIGHT (G)-- RESULT 1 �• •A. •�, Ops • . �� _ � ® '�• � :a t1 � :� � saw• ®- �0.0-0 r . • ,� J • �_ I I • I I malls "a - mme mmmm ��sz MIA m M • M-AMMMMMM 00 a I mll, m MISM'.1 mm mmmmm A- �0-10 6 I= mo "I m 1•' � mm / • � �. � s ®m*4 a 1�. m ma.on malm �lb= Max m 910- M's M. -, "m* on MMMMM TSLQ01 W78 x -IDS kd Wtaa1 T liflt. (a11Yt d00 SS/ TS Sollds(ow)■ mL Sample ANALYST: � T DATE: tl GS STAR wuMielTv. TSL001 W79 99 A, E DRIED WT —TARE WEIP ®JMQJM1=K=w am Mk -1 i 10'' Proj b. . 1 1 MM MMMM-0-1 �-,: ®ter Put �O-twnl MOMFORS 1 W A W�*g - 7 m$y", M M, MMM M ®� � owes �-t • • Mm • • � � I a.. M�W.MMMMI imI � � onWAOMII"16-evMFOX01wasm, Jt. NMI N..k r one No Moo* FMIMM-1 MM10 'MMM �61 7t _ AS j tip _—la Is�' • �. .. _ 016,0M--11090 ...: _..-y�r -ter w ori w.n www IDS . D / S/ TS mL 84"yft ANALYST: TEMP. DATE: 4/3/0,S START• MIDITY: K= —m -mil -Il - �$�, 0, RllMULTIlrTirT-WUWT%r-l�= mow M, �s 46 6 �1-c -mom- mmmmm r• �` , S1 i11 �. oil ,a • 0 MO "som mo moPSAWN.AP �I= m m a.c mmmm� "Olommmmm •�' �A • 1"'4'affiveWoo *.'a �llas- �6.0-16® We mme mlitma. • M -a Pat m.m ===mom mmm 1.._ c mammm �► i� s � � _ - y 11 TKN Data Ok SampleiD � _ C Te -"t 001 r k L -s �l � Concentration listed after Optical Blank Correction. Preparation dilution factor not applied to results. SampTy Conc Units DF Conc z DF AnalDate AnalTime TestCod 1 Primer PRIM 2.987 mgIl 1 2.987 4/12/05 11:46:02 AM tkn w 1 0504165-002A SAMP 0.72905 mgIl 20 14.581 4/12/05 12:1923 PM tlm w 2 Drift DRIF 3.015 mgA 1 3.015 4/12/05 11:46:42 AM tlM w 3 High HIGH 3.029 mg/l 1 3.029 4/12/05 11:47:22 AM tlM w 4 Low LOW 0.039 mg4 1 0.03914/12/05 11:48:00 AM tim w 5 Low LOW 0.039 mg4 I 0.039 4/12/05 11:48:42 AM dM -w 6 Cal. CAM 3.016 mg/I 1 3.016 4/12/05 11.49:23 AM dM -w 7 Cal. CALB 0.964 mg/I 1 0.964 4/12/05 11:50:01 AM dM -w 8 Cal. CALB 0.473 mg/l 1 0.473 4/12/05 11:50:41 AM dM -w 9 Cal. CAM 0.192 mg/l 1 0.192 4/12/05 11:5120 AM tlM w 10 Cal. CALB 0.097 mg/l 1 0.097 4/12/05 11:52:02 AM dm w 11 Cal. CALB 0.03 mg/I 1 0.03 4/12/05 11:52:40 AM tlm w 12 optical bink QUAL 0.73 mg/l 1 0.73 4/12/05 11:53:23 AM dM -w 13 Ics-13204 Ics i V_ (! , 0.4442 mg/l 10 4.442 4/12/05 109 /• 11:54:03 AM tkn w 04 mb-13204 mblk -0.044 mg4 1 -0.044 4/12/05 e- 1 11:54.40 AM tkn w 15 0504023-002A SAW 0.148 mg/l 10 1.48 4/12/05 11:55:23 AM tlM w 16 0504024-OOID MW - 3b SAW 1.1295 mg/I 20 22.59 4/12/05 11:56:03 AM dal -W 17 0504024-002D ti W - 3 5 SAMP 1.4356 mg/l 20 28.712 4/12/05 11:56:43 AM dM -w 18 0504024-003D MW - S,i> SAMP 2.13585 mgA 20E---42.7117 4/12/05 11:57:23 AM tlM w 19 0504024-004D hW - SS SAMP 0.4341 mg/l 10 4.341 4/12/15 11:58:01 AM dM -w 20 0504024-005D M W - CID SAMP 0.238 mgA 1 0238 4/12/05 11:58:43 AM dM -w 21 0504024-006D % W - G6 SAMP 0.031 mg/I 1 0.031 4/12/05 11:5921 AM dM -w 22 0504024-007D SAMP 1.89655 mg4 20 37.931 4/12/05 12:00:03 PM dM -w 23 0504024-OOBD 11.1- is SAMP 2.3442 mg1l 20E---46.8941 4/12/05 12.00:43 PM dM -w 24 0504024-009D CQ V I PT. U g'br SAMP -0.015 mg/l IF------O-.OI-51 4/12/05 12:0120 PM dM -w 25 ccv1.0 ccv 0.956 mg/l 1 0.956 4112/05 4IG'I 12:02:03 PM dM -w 26 ccb ccb 0.027 mg/l 1 0.027 4/12/05 KO,' 12:02:41 PM dww 27 0504067-001 D M W - SAMP 0.176 mgtl 10.176 4/12/05 12:03:22 PM dM -w 28 0504067-002D n W - IS SAMP -0.021 mgA 1 -0.021 4/12/05 ` ` 12:04:02 PM dM -w 29 0504067-002DMS ms 1 �_ ' 0.4296 mg/l 10 4.296 4/12/05 t % , � 12:04:43 PM dm w 005 12:52:16 PM Page 1 of 2 Peak SampleID SampTy Conc Units DF Conc z DF AnalDate AnaMme TestCod �0 0504067-002DDUP Kt3 ` .S dup -0.293 mg/i 1 -0293 4/12/05 173 12:05:21 PM tkn w 31 0504060-001a SAMP 0.36075 mg/l 20 7.215 4/12/05 12:06:02 PM tknw 32 0504060-002a SAMP 1.11 mg/l 20 222 4/12/05 12:06:43 PM tlm w 33 0504134-OOIA SAMP 1.0274 mg/1l0 10274 4/12/05 12:07:22 PM tlm w 34 0504134-002A SAW 0.2038 mg/l 20 4.07614/12/05 12:08:01 PM dm—w 35 0504136.00IA SAW 1.6278 mg/l 10 16.278 4/12/05 12:08:43 PM tlm w 36 0504136-002A SAMP 0.18395 mg/1 20E----3.6719 4/12/05 12:09:21 PM tim w 37 ccvl.0 ccv 0.97 mgA 1 0.97 4/12/05 R7 12:10:03 PM dm—w 38 ccb ccb 0.027 mg/l 1 0.027 4/12/05 <0.1 12:10:41 PM tknw 39 0504148-OOIA SAMP 0.6401 mo 10 6.401 4/12/05 12:11:23 PM tim w 40 0504148-002A SAMP 1.4459 mgA 10 14.459 4/12/05 12:12:04 PM tlmw 41 0504149-OOIB SAMP 0.67565 mg/l 20E----13.5131 4/12/05 12:12:42 PM dm—w 42 0504144-001B 205 SIO —09 ( SAW 0.156 mg/l 1 0.156 4/12/05 12:13:22 PM dm—w 43 0504144-OOIBMS ms V •� 0.42 mgA 10 4.2 4/12/05 `�� 12:14:03 PM tknw 44 0504144-OOIBDUP dup 0.276 mg/l 1 0.276 4/12/05 le?11 STT 12:14:43 PM tkn w 45 0504209-001 B ZOCGO — 00 SAMP 0.362 mg/l 1 0-36214/12/05 12:15:23 PM dm—w �6 0504155-OOIA SAW 0.44055 mg/l 20 8.811 4/12/05 12:16:04 PM dm—w 47 0504155-002A SAMP 1.4309 mg/l 20E----28.6119 4/12/05 12:16:43 PM tim w 48 0504165-OOIA SAM? 02498 mg/l 20E---4.996 4/12/05 12:17:22 PM Om—w 49 ccvl.0 ccv 0.967 mg4 1 0.967 4/12/05 Q 7 %. 12:18:03 PM dm—w 50 ccb ccb 0.031 mg/l 1 0.031 4/12/05 p . ( 12:18:41 PM tim w 52 lfb-13204 lfb I i_ �'1 • ( 0.4077 mg/l 10 4.077 4/12/05 49 % 1220:02 PM dmw 53 Ifbd-13204 Ifbd 0.4316 mg/l 10 4.316 4/12/05 lith 6} 1220:43 PM dm—w 54 ccv 1.0 ccv 0.96 mg/l 1 0.96 4/12/05 �. 12:21:23 PM tkn w 55 ccb ccb 0.025 mg/l I 0.025 4/12/05 . O- t 12:22:01 PM tkn w 56 Drift DRIF 3.015 mg/l 1 3.015 4/12/05 12:22:43 PM dm—w 57 End END 0.029 mgA 1 0.029 4/12/05 1224.41 PM dm—w 005 12:52:16 PM Page 2 of 2 N 00 O O H BRAN+LDEBBE AACE 5.47 H2M LABS INC. Post -run Report Post -run report Name of Run tkn041205 Name of Analysis :tkn.ANL Date of Report . 4/12/05 System No. :1 Date of Run 4/12/05 Type of System :TRAACS Operator cp Start/Stop time :11:34 - 12:25 Comment tsl,bnls Channel Type Real Data Channel 2 2 Method tkn Dilution Unit mg/l Calibr. Fit Linear Corr. Coeff. 0.9997 Base 66 Gain 23 Sensitivity 0.4279 Sample Limit 1 Sample Limit 2 • Pk Cup Sample Id Value Va. e 0 0 B Baseline 0.029 0 1 1 P Primer 2.987 1 2 1 D Drift 3.015 1 3 1 H1 High 3.029 1 4 0 L1 Low 0.039 1 5 0 L1 Low 0.039 1 6 1 C Cal. 3.016 1 7 2 C Cal. 0.964 1 8 3 C Cal. 0.473 1 9 4 C Cal. 0.192 1 10 5 C Cal. 0.097 1 11 0 C Cal. 0.030 1 12 8 QC1 optical bink 0.730 1 13 9 QC1 lcs 4.1 5.172 10 14 10 QC1 mblk 0.686 1 15 11 S 0504023-002A 2.210 10 16 12 S 0504024-OOID 23.320 20 17 13 S 0504024-002D 29.442 20 18 14 S 0504024-003D 43.447 20 19 15 S 0504024-004D 5.071 10 20 16 S 0504024-005D 0.968 1 • 21 17 S 0504024-006D 0.761 1 M 00 0 C/1 F"� QC Limits BRAN+LUEBBE AACE 5.47 2 • 22 18 S 0504024-007D 38.661 20 Unused 23 19 S 0504024-008D 47.614 20 24 20 S 0504024-009D 0.715 1 QC 8 25 2 QC1 ccvl.0 0.956 1 26 0 QC1 ccb 0.027 1 27 21 S 0504067-001D 0.906 1 28 22 S 0504067-002D 0.709 1 29 23 S 0504067-002DMS 5.026 10 30 24 S 0504067-002DDUP 0.437 1 31 25 S 0504060-001a 7.945 20 32 26 S 0504060-002a 22.930 20 33 27 S 0504134-OOIA 11.004 10 34 28 S 0504134-002A 4.806 20 35 29 S 0504136-001A 17.008 10 36 30 S 0504136-002A 4.409 20 37 2 QC1 ccvl.0 0.970 1 38 0 QC1 ccb 0.027 1 39 31 S 0504148-001A 7.131 10 40 32 S 0504148-002A 15.189 10 41 33 S 0504149-001B 14.243 20 42 34 S 0504144-OOIB 0.886 1 43 35 S 0504144-OOIBMS 4.930 10 44 36 S 0504144-001BDUP 1.006 1 45 37 S 0504209-001B 1.092 1 •46 38 S 0504155-001A 9.541 20 47 39 S 0504155-002A 29.348 20 48 40 S 0504165-001A 5.726 20 49 2 QC1 ccvl.0 0.967 1 50 0 QC1 ccb 0.031 1 51 41 S 0504165-002A 15.311 20 52 42 S lfb 4.807 10 53 43 S lfbd 5.046 10 54 2 QC1 ccv 1.0 0.960 1 55 0 QC1 ccb 0.025 1 56 1 D Drift 3.015 1 57 0 B FinalBase 0.029 1 QC Limits Post -run Report Itt 00 Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused • QC 8 Unused Post -run Report Itt 00 BRAN+LUEBBE AACE 5.97 •QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 1.1 ** <END OF REPORT> ** • • Post -run Report BW +LUEBBE RACE 5.47 0 Name of run :tkn04l2O5.RUN Comment min Channel : 2 Method : tkn Unit : mg/l Base 66 Gain 23 Corr. 0.9997 H2M LABS INC. Post -run chart Post -run chart Name of analysis :tkn.ANL Page 1 of 3 110 00 1 1 1 r 1 I I 1 1 1 r 1 1 I I 1 i 1 r 1 1 i 1 I 1 1 I t 2 ----------------- J ------------------ L ----------------- J ------------------ 9-- ---------------+------------------------------------+------------------ 1 1 1 1 1 1 I I 1 1 I 1 1 r 1 1 1 1 r 1 1 1 r I 1 1 1 ------------------------------------ ---------------- r r r r 1 I I 1 1 r I I 1 1 1 r 1 1 i r 1 I 1 1 1 I 1 1 r 1 8 1 1 ------------------ J ------------------ L ----------------- i ------------------ I I 1 1 1 1 I i 1 1 1 I 1 1 1 1 1 1 1 1 t 1 1 1 r r 1 r 10 -----------------4------------------------------------a------------------r 1 1 1 1 r r I 1 i iOB 0.029 1 I I 1 r r r 1 --- ------- - - - - -r 1P 2.987 12 � 1 r 1 I � r 1 :2D 3.015 r � I I � i :3H 3.029 I 1 r 1 r r 19 ------- - - - - -- 1------------------�-----------------------------------'9L 0.039 1 I 1 1 i5L 0.039 1 r 1 r r r 6C 3.016 r 1 r r r r Page 1 of 3 110 00 BRAN+LUEBBE AACE 5.47 Post -run Chart Name of run :tkn04l2O5.RUN Name of analysis :tkn.ANL Comment Page 2 of 3 r- 00 O O E-+ BRAN+LUEBBE AACE 5.47 Name of run :tkn04l2O5.RUN Comment Post -run chart Name of analysis :tkn.ANL i36S 4.409 r i � r r r r 36 - - - - - - - - - - - - - ---- i- ---- - - - - - - - - - - - -- ------------------------------------- 37QC1 0.970 r i r38QC1 0.027 i39S 7.131 , r i r , r 38 - - - - - - - - - - - - - - - - - - J - - - -- - - - - - ------- '------------ - - - - - - ------------------'40S 15.189 :41S 14.243 , r r � , r r i 142S 0.886 � , r r r ' 90 - - - - - - - - -------- tir-- - - -- ------- - - - - -� -----------------�r ------------------r93S 4.930 r , r r :44S 1.006 r r r r r r � , r i 45 1.092 r , r 42 - - - - - - - - --------rrrrr'rrr',riiir'rrrrrrrr --irr'rr,r'rrrrrrr'r,rrriri -----------------rii'�rrrrrr�rr�'rrrr'ir�ii --r'iirir�ir''''r' 46S 9.541 r47S 29.348 :48S 5.726 -------------- - - ------------------- L - - - - - - - - - - - - - - - --- - - - - - - - - - - - - - - - - - :490C1 0.967 :50001 0.031 '51S 15.311 846 - - - - - - - -------1------------------f------------------+------------------:52S 4.07 53S 5.046 r54001 0.960 -----------48 - - - - - - - - - - - - - -r------------------r------------------------:550010.025 ''56D 3.015 50 ---------------------------------- L ------------------------------------r r r i i 57B 0.029 52------------------------------------r-----------------i------------- - - - - - � i r i r i r i r r r i r r r r r Page 3 of 3 00 00 BRAN+LUEBBE AACE 5.47 • Name of run :tkn04l205.RUN Comment • r� H21VI LABS INC. Calibration Curve Channel :2 Method :tkn Curve fit :linear a= -1.3395E-001 b=5.9634E-005 Corr. coeff. :0.9997 Peak [%] .LUU 80 60 40 20 0 Calibration Curve Name of analysis :tkn.ANL 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/l ] Page 1 of 1 00 O C/) 1-12M LABS, INC. '6rs'bo*l- • TOTAL P SITXN DIGESTIONS 34 NAME: V;C,.tf DATE • g;40 IAB NO. CLIENT ID SAMPLE WEIGHT SAMPLE VOIAM MIS I FINAL VOLUME MLS DATE ANALYZED SPI A lel P 0017 t12M LAOS, IMC. p N b s e/y • 33 3Y Li • TOTAL PRdS/TXN DIGESTIONS NAME: AIIVII ho W� DATE' Y - It - O LAB NO. CLIENT ID SAMPLE WEIGHT S= V MLS FINAL VOLUME DATE ANALYZED SPIKE 0 MAO mmo, M����mm�m Y 0018 Sample Results Report Print Date/Timdk 2 0/04/07 6'51!:Q25 Sample ID Result Std. Dev. RSD Mode ALT 0.2399 0.0325 13.53 UTILITY :S ZS( 15-W/ 22.4207 0.7564 3.37 TOC 'B X1.0 0.8823 0.0435 4.93 TOC ..................... 1.1775... 0.0594.. 5.05 ... TOC .. ;LK ll.0 0.6516 0.1144 17.56 TOC 04024-001C MW -3O 23.9766 3.9057 16.29 TOC 04024-002C. ................. 20.1390... 4.0118.. 19.92 ... TOC .. 04024-003C mW -550 25.7771 7.0449 27.33 TOC 04024-004C MW -S,933.1265 5.6577 17.08 TOC 04024-005C.MW: 60.••.••.••.••••••• 3.2436... 0.4028.. 12.42... TOC 04024-006C MW -CS 1.4040 0.2866 20.42 TOC�- 04024-007C 24.2803 7.4923 30.86 TOC 04024-008C.AAW:5 ................. 31.7897... 4.5878.. 14.43 ... TOC 04024-009C elviP1 &IL 2.5501 0.0963 3.78 TOC prof snit% 04067-001C MV -10 1.8450 0.3594 19.48 TOC 4, V ': A?4 f ................. Y9 ;LWX. 22.3491 ... 0.2 810.. 1.26 ... TOC . . B 1.0240 0.1403 13.70 TOC 04067-002C MC'i5 R:9�•�' ICA 11.111711) 0.3243 2.92 TOC 04067-002CMS,f:V =. Lo.Q.. �fp : �.A.x. .. 20.18231Ql 0.6115.. 3.03 ... TOC 04067-002CDU 11.930011 0.1484 1.24 TOC •. 03767-001A v/ 5.7229 0.2901 5.07 TOC V.Z'V?•%��1`............Ell X 21.2417... 0.4601.. 2.17 ... TOC .. B U L►.p 0.3133 0.2747 87.67 TOC SL_OC7 i N • O O F-� Sample Results Report Print Date/Time: 2005/04/07 6:57:25 • M OINO Cn E-4 Method ID Sample Type Vial Timestamp Message leaning Procedure Sample sp 2005/04/06 15:39 DC WATER Sample 1 2005/04/06 16:04 DC IOTE TE WATER Sample 2 2005/04/06 16:29 Low Sample Detect DC WASTE WATER ...Sample .. 3..2005/04/06 16:55 ..Low Sample Detect )C WASTE WATER Sample 4 2005/04/06 17:20 Low Sample Detect )C WASTE WATER Sample 5 2005/04/06 17:45 )C WASTE WATER ...Sample .. 6..2005/04/06 18:10 .. )C WASTE WATER Sample 7 2005/04/06 18:34 )C WASTE WATER Sample 8 2005/04/06 18:59 )C WASTE WATER ...Sample .. 9..2005/04/06 19:25 ..Low Sample Detect )C WASTE WATER Sample 10 2005/04/06 19:50 Low Sample Detect )C WASTE WATER Sample 11 2005/04/06 20:15 )C WASTE WATER ...Sample .. 12..2005/04/06 20:40 .. )C WASTE WATER Sample 13 2005/04/06 21:05 Low Sample Detect )C WASTE WATER Sample 14 2005/04/06 21:31 Low Sample Detect )C WASTE WATER ...Sample .. 15..2005/04/06 21:56 .. )C WASTE WATER Sample 16 2005/04/06 22:21 Low Sample Detect )C WASTE WATER Sample 17 2005/04/06 22:46 )C WASTE WATER ...Sample .. 18..2005/04/06 23:10 .. )C WASTE WATER Sample 19 2005/04/06 23:35 )C WASTE WATER Sample 20 2005/04/06 23:59 )C WASTE WATER ...Sample .. 21..2005/04/07 00:24 .. )C WASTE WATER Sample 22 2005/04/07 00:49 Low Sample Detect • M OINO Cn E-4 Detailed Analysis Report Print Date/Time: 2005/04/07 6:57:27 imple ID: DI Mode: UTILITY ?thod: Cleaning Procedure Filename: 04061514 itrve: TOC WW CURVE 40405 Timestamp: 2005/04/06 15:39 )e r ID: JASON SAMUEL Sample Type: Sample ?p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2530 0.1265 23950 10.461 10.660 144 2 0.2636 0.1318 24951 10.444 10.642 142 3 0.2435 0.1217 23045 10.432 10.631 139 4 0.2561 0.1281 24245 10.433 10.632 141 5 ---------------------------------------------------------------------------- 0.1833 0.0917 17355 10.435 10.635 123 :<Statistics>>> Mean: 0.2399 Std Dev: 0.0325 RSD: 13.53 imple ID: LCS Mode: TOC !thod: TOC WASTE WATER Filename: 04061514 .1. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 16:04 )erator ID: JASON SAMUEL Sample Type: Sample p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 23.5275 1.1764 222705 10.316 11.307 112 2 22.0731 1.1037 208938 10.326 11.325 112 3 21.8384 1.0919 206716 10.293 11.291 112 4 22.2436 1.1122 210552 10.271 11.259 112 -- ------------------------------------------------------------------ <0 istics>>> Mean: 22.4207 Std Dev: 0.7564 RSD: 3.37 mple ID: ICB Mode: TOC thod: TOC WASTE WATER Filename: 04061514 1. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 16:29 erator ID: JASON SAMUEL Sample Type: Sample P # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.9437 0.0472 8932 10.143 10.176 120 2 0.8568 0.0428 8111 10.146 10.146 120 3 0.8469 0.0423 8016 10.138 10.147 120 4 --------------------------------------------------------------------------- 0.8820 0.0441 8349 10.124 10.131 120 st Message: Low Sample Detected <Statistics>>> Mean: 0.8823 Std Dev: 0.0435 RSD: 4.93 nple ID: CRI thod: TOC WASTE WATER L. Curve: TOC WW CURVE 40405 srator ID: JASON SAMUEL • Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 16:55 Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Integration Baseline Baseline Time 1 1.2416 0.0621 11753 10.170 10.181 120 2 1.1685 0.0584 11061 10.170 10.210 120 3 1.1005 0.0550 10417 10.174 10.174 120 1.1992 -- --------------------------- 0.0600 11351--------10_152------10_164-------120----- 10.186 120 4 ---------------------------------------------------------------------------- ast Message: Low Sample Detected 6878 10.171 10.166 <<Statistics>>> Mean: 1.1775 Std Dev: 0.0594 RSD: 5.05 ample ID: MBLK sthod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 aerator ID: JASON SAMUEL Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 17:20 Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Baseline Baseline Time 1 0.6920 0.0346 6551 10.165 10.191 120 2 0.4813 0.0241 4556 10.187 10.191 120 3 0.7064 0.0353 6686 10.175 10.186 120 4 ---------------------------------------------------------------------------- 0.7266 0.0363 6878 10.171 10.166 120 ist Message: Low Sample Detected :<Statistics>>> Mean: 0.6516 Std Dev: 0.1144 RSD: 17.56 ample ID: 0504024-001C Mode: TOC !thod: TOC WASTE WATER Filename: 04061514 iurve: TOC WW CURVE 40405 Timestamp: 2005/04/06 17:45 �e or ID: JASON SAMUEL Sample Type: Sample !p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 29.5731 1.4787 279930 10.231 11.217 111 2 23.7206 1.1860 224532 10.245 11.241 110 3 21.5466 1.0773 203954 10.234 11.226 110 4 --------------------------------------------------------------------------- 21.0659 1.0533 199404 10.209 11.207 111 <Statistics>>> Mean: 23.9766 Std Dev: 3.9057 RSD: 16.29 mple ID: 0504024-002C thod: TOC WASTE WATER 1. Curve: TOC WW CURVE 40405 erator ID: JASON SAMUEL Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 18:10 Sample Type: Sample p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 25.7861 1.2893 244084 10.138 11.128 111 2 20.1716 1.0086 190939 10.134 11.117 109 3 17.6632 0.8832 167194 10.110 11.095 108 4 16.9352 --------------------------------------------------------------------------- 0.8468 160303 10.081 11.074 108 1Wistics>>> Mean: 20.1390 Std Dev: 4.0118 RSD: 19.92 ample ID: 0504024-003C athod: TOC WASTE WATER 3rve: TOC WW CURVE 40405 ?e Wor ID: JASON SAMUEL Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 18:34 Sample Type: Sample Bp # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 35.8778 1.7939 339609 10.024 11.020 112 2 25.2194 1.2610 238720 10.036 11.034 110 3 21.7201 1.0860 205596 10.004 11.000 111 4 20.2909 1.0145 192068 9.980 10.973 110 ---------------------------------------------------------------------------- ,<Statistics»> Mean: 25.7771 Std Dev: 7.0449 RSD: 27.33 ample ID: 0504024-004C Mode: TOC �thod: TOC WASTE WATER Filename: 04061514 al. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 18:59 )erator ID: JASON SAMUEL Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 38.8851 1.9443 368075 9.922 10.911 114 2 30.1462 1.5073 285355 9.964 10.957 113 3 26.7312 1.3366 253030 9.961 10.958 111 4 36.7437 1.8372 347805 9.932 10.924 115 --------------------------------------------------------------------=------- ;< tistics»> Mean: 33.1265 Std Dev: 5.6577 RSD: 17.08 ample ID: 0504024-005C Mode: TOC �thod: TOC WASTE WATER Filename: 04061514 il. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 19:25 )erator ID: JASON SAMUEL Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 3.7864 0.1893 35841 9.845 9.891 120 2 3.2847 0.1642 31092 9.831 9.851 120 3 3.0512 0.1526 28882 9.797 9.813 120 4 ---------------------------------------------------------------------------- 2.8519 0.1426 26996 9.766 9.784 120 ist Message: Low Sample Detected XStatistics>>> Mean: 3.2436 Std Dev: 0.4028 RSD: 12.42 imple ID: 0504024-006C !thod: TOC WASTE WATER i1. Curve: TOC WW CURVE 40405 >erator ID: JASON SAMUEL !p* ppm C ug C Raw Data Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 19:50 Sample Type: Sample Beginning Ending Integration Cr O Cn E-4 ample ID: 0504024-007C athod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 aerator ID: JASON SAMUEL 2!p # ppm C ug C Raw Data Mode: Filename: Timestamp: Sample Type: Beginning Baseline 1 35.3376 1.7669 334496 Baseline Baseline Time 1 1.8074 0.0904 17108 9.576 9.578 120 2 1.1510 0.0576 10895 9.544 9.521 120 3 1.2639 0.0632 11964 9.489 9.478 120 4 1.3936 0.0697 13191 9.426 9.428 120 ----------------------------------------------------------------------- 2.4346 0.1217 23045 9.582 9.627 120 as sage: Low Sample Detected <<Statistics>>> Mean: 1.4040 Std Dev: 0.2866 RSD: 20.42 RSD: 3.78 ample ID: 0504024-007C athod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 aerator ID: JASON SAMUEL 2!p # ppm C ug C Raw Data Mode: Filename: Timestamp: Sample Type: Beginning Baseline 1 35.3376 1.7669 334496 9.253 2 22.4330 1.1217 212344 9.288 3 19.2786 0.9639 182486 9.260 4 ---------------------------------------------------- 20.0719 1.0036 189994 9.277 ,<Statistics>>> Mean: 24.2803 Std Dev: 7.4923 ample ID: 0504024-008C ?thod: TOC WASTE WATER il. Curve: TOC WW CURVE 40405 )erator ID: JASON SAMUEL gip• ppm C ug C Raw Data TOC 04061514 2005/04/06 20:15 Sample Ending Integration Baseline Time 10.243 114 10.285 111 10.254 109 10.268 111 ------------------------ RSD: 30.86 1.8231 Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 20:40 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 1 34.9310 1.7465 330647 9.370 10.362 112 2 28.5602 1.4280 270342 9.376 10.376 112 3 36.4620 1.8231 345139 9.388 10.385 115 4 27.2055 •--------------------------------------------------------------------------- 1.3603 257519 9.428 10.425 113 X Statistics>>> Mean: 31.7897 Std Dev: 4.5878 RSD: 14.43 2.5129 ample ID: 0504024-009C !thod: TOC WASTE WATER 1. Curve: TOC WW CURVE 40405 lerator ID: JASON SAMUEL Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 21:05 Sample Type: Sample !p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 2.5996 0.1300 24607 9.467 9.542 120 2 2.6534 0.1327 25116 9.517 9.579 120 3 2.5129 0.1256 23786 9.566 9.637 120 4 --------------------------------------------------------------------------- 2.4346 0.1217 23045 9.582 9.627 120 st Message: Low Sample Detected <Statistics>>> Mean: 2.5501 Std Dev: 0.0963 RSD: 3.78 ample ID: 0504067-001C ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 pe0r ID: JASON SAMUEL ep # ppm C ug C Raw Data Mode: Filename: Timestamp: Sample Type: Beginning Baseline 1 2.3053 0.1153 21821 9.612 2 1.9225 0.0961 18198 9.635 3 1.4642 0.0732 13859 9.687 4 1.6879 0.0844 15977 9.663 -------------------------------------------- ast Message: Low Sample Detected -<Statistics>>> Mean: 1.8450 Std Dev: ample ID: CCV �thod: TOC WASTE WATER 31. Curve: TOC WW CURVE 40405 )erator ID: JASON SAMUEL TOC 04061514 2005/04/06 21:31 Sample Ending Integration Baseline Time 9.654 120 9.688 120 9.710 120 9.686 -------------------------- 120 0.3594 RSD: 19.48 Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 21:56 Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 22.5294 1.1265 213257 9.621 10.615 112 2 22.3541 1.1177 211598 9.679 10.679 112 3 21.9505 1.0975 207777 9.708 10.700 112 4 ---------------------------------------------------------------------------- 22.5623 1.1281 213568 9.684 10.683 113 :< istics>>> Mean: 22.3491 Std Dev: 0.2810 RSD: 1.26• ample ID: CCB Mode: TOC !thod: TOC WASTE WATER Filename: 04061514 il. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 22:21 )erator ID: JASON SAMUEL Sample Type: Sample :p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 1.0965 0.0548 10379 9.676 9.701 120 2 1.0808 0.0540 10230 9.706 9.712 120 3 1.1048 0.0552 10458 9.691 9.748 120 4 ---------------------------------------------------------------------------- 0.8141 0.0407 7706 9.685 9.686 120 .st Message: Low Sample Detected *<Statistics>>> Mean: 1.0240 Std Dev: 0.1403 RSD: 13.70 .mple ID: 0504067-002C -thod: TOC WASTE WATER .1. Curve: TOC WW CURVE 40405 erator ID: JASON SAMUEL p o ppm C ug C Raw Data Mode: TOC Filename: 04061514 Timestamp: 2005/04/06 22:46 Sample Type: Sample Beginning Ending Integration 00 a\ O Baseline Baseline Time 1 11.2986 0.5649 106949 9.667 10.656 106 2 11.4478 0.5724 108362 9.712 10.703 107 3 10.9744 0.5487 103881 9.705 10.695 106 4 10.7259 0.5363 101528 9.684 10.672 106 - ------------------------------------------------------------------ < tistics»> Mean: 11.1117 Std Dev: 0.3293 RSD: 2.92 ample ID: 0504067-002CMS Mode: TOC ethod: TOC WASTE WATER Filename: 04061514 al. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 23:10 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 20.7049 1.0352 195986 9.717 10.705 110 2 20.6954 1.0348 195896 9.742 10.734 110 3 19.8209 0.9910 187619 9.717 10.708 110 4 19.5079 0.9754 184656 9.672 10.663 110 ---------------------------------------------------------------------------- <<Statistics>>> Mean: 20.1823 Std Dev: 0.6115 RSD: 3.03 ample ID: 0504067-002CDUP Mode: TOC athod: TOC WASTE WATER Filename: 04061514 al. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 23:35 Derator ID: JASON SAMUEL Sample Type: Sample a* ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 11.9303 0.5965 112929 9.643 10.642 107 2 12.0633 0.6032 114188 9.635 10.624 107 3 11.7229 0.5861 110966 9.599 10.592 106 4 12.0037 0.6002 113624 9.575 10.566 106 ---------------------------------------------------------------------------- ,<Statistics>>> Mean: 11.9300 Std Dev: 0.1484 RSD: 1.24 ample ID: 0503767-001A Mode: TOC sthod: TOC WASTE WATER Filename: 04061514 al. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/06 23:59 )erator ID: JASON SAM ;L Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 6.0270 0.3013 57050 9.587 10.574 101 2 5.4685 0.2734 51764 9.571 10.563 101 3 5.4813 0.2741 51885 9.550 10.539 101 4 5.9148 0.2957 55988 9.522 10.521 102 ---------------------------------------------------------------------------- XStatistics>>> Mean: 5.7229 Std Dev: 0.2901 RSD: 5.07 • ample ID: CCV ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 perator ID: JASON SAMUEL Mode: Filename: Timestamp: Sample Type: TOC 04061514 2005/04/07 00:24 Sample efflF ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 21.2001 1.0600 200674 9.527 10.519 111 2 20.9075 1.0454 197904 9.505 10.505 110 3 20.9548 1.0477 198352 9.430 10.429 111 4 21.9045 1.0952 207342 9.333 10.323 111 ---------------------------------------------------------------------------- <<Statistics>>> Mean: 21.2417 Std Dev: 0.4601 RSD: 2.17 ample ID: CCB Mode: TOC ethod: TOC WASTE WATER Filename: 04061514 al. Curve: TOC WW CURVE 40405 Timestamp: 2005/04/07 00:49 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.7158 0.0358 6775 8.784 8.743 120 2 0.2558 0.0128 2421 8.699 8.660 120 3 0.1687 0.0084 1597 8.599 8.540 120 4 0.1130 0.0057 1070 8.498 8.454 120 ---------------------------------------------------------------------------- ast Message: Low Sample Detected <<Statistics>>> Mean: 0.3133 Std Dev: 0.2747 RSD: 87.67 _----------- - ------------------------------------------ • Calibration Report Print Date/Time: 2005/04/07 6:57:33 al. Curve ID: TOC WW CURVE 40405 reated: 2005/04/04 18:18 alibration Factor (m): 1.893e+05 (b): 8697 _,Srcept red: 0.99852 Standard ID Y X Expected Measured Message Raw Data ug C ug C I 12025 0.000 0.018 Low Sample De .5PPM 14900 0.025 0.033 Low Sample De .OPPM 18657 0.050 0.053 Low Sample De .OPPM 53646 0.250 0.237 O.OPPM 89582 0.500 0.427 5.OPPM 249262 1.250 1.271 O.OPPM 500784 2.500 2.599 5.OPPM 706762 3.750 3.687 • Date & Time 2005/04/04 15:48 2005/04/04 16:10 2005/04/04 16:31 2005/04/04 16:52 2005/04/04 17:13 2005/04/04 17:34 2005/04/04 17:55 2005/04/04 18:16 Sample Results Report Print Date/TimeT-.20"'O"31AW AW. 22 Sample ID Result Std. Dev. RSD Mode ALT IS � 1.tis �B <! ................... AU 3LK L% D 504024-005C W -10 504024-006CJ � �1 �............. 504024-009C CSO 504067-001C 14V-10 41.0 FB.'--1�Ccs o:�%...... w-AOyEBDTy (oQ w-ry- zS PIF� �B............................4/.JQ i SLQOI 0 • V.Lrog'J V.Vlo'! Q.7 7 V1.L.0 .L .3.7386 1.4658 6.17 TOC 0.9078 0.1035 11.40 TOC 1.1100... 0.2996.. 26.99 ... TOC .. 0.5813 0.3233 55.62 TOC 1.8003 0.2141 11.89 TOC 1.1367... 0.1342.. 11.81 ... TOC .. 0.7135 0.2272 31.84 TOC 0.9559 0.2299 24.05 TOC 9.3411... 0.0472.. 0.51 ... TOC .. 9.3222 0.2004 2.15 TOC ?2.4777 0.4284 1.91 TOC 0.5948... 0.1173.. 19.72 ... TOC .. Sample Results Report Print Date/Time: 2005/04/07 13:07:22 • • M O 0 Method ID Sample Type Vial Timestamp Message leaning Procedure Sample sp 2005/04/07 07:50 O*TE WATER Sample 1 2005/04/07 08:15 O TE WATER Sample 2 2005/04/07 08:40 Low Sample Detect OC WASTE WATER ...Sample .. 3..2005/04/07 09:05 ..Low Sample Detect OC WASTE WATER Sample 4 2005/04/07 09:31 Low Sample Detect OC WASTE WATER Sample 5 2005/04/07 09:56 Low Sample Detect OC WASTE WATER ...Sample .. 6..2005/04/07 10:22 ..Low Sample Detect OC WASTE WATER Sample 7 2005/04/07 10:47 Low Sample Detect OC WASTE WATER Sample 8 2005/04/07 11:13 Low Sample Detect OC WASTE WATER ...Sample .. 9..2005/04/07 11:37 .. OC WASTE WATER Sample 10 2005/04/07 12:01 OC WASTE WATER Sample 11 2005/04/07 12:26 OC WASTE WATER ...Sample .. 12..2005/04/07 12:52 ..Low Sample Detect • • M O 0 Detailed Analysis Report Print Date/Time: 2005/04/07 13:07:24 ample ID: DI Mode: UTILITY ethod: Cleaning Procedure Filename: 04070730 a4urve: TOC WW CURVE 40405 Timestamp: 2005/04/07 07:50 p or ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2552 0.1276 24155 10.798 10.997 126 2 0.2451 0.1225 23197 10.748 10.947 124 3 0.2872 0.1436 27190 10.732 10.932 130 4 ---------------------------------------------------------------------------- 0.2705 0.1353 25605 10.748 10.946 129 <<Statistics>>> Mean: Mean: 0.2645 Std Dev: 0.0184 RSD: 6.95 XStatistics>>> ample ID: LCS Bthod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 aerator ID: JASON SAMUEL Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 08:15 Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 23.0299 1.1515 217994 10.664 11.654 111 2 23.4416 1.1721 221891 10.672 11.671 112 3 22.6061 1.1303 213982 10.685 11.684 112 4 ---------------------------------------------------------------------------- 25.8769 1.2938 244943 10.688 11.676 113 ti.stics>>> Mean: 23.7386 Std Dev: 1.4658 RSD: 6.17 XStatistics>>> Mean: 0.9078 Std Dev: 0.1035 imple ID: ICB tthod: TOC WASTE WATER il. Curve: TOC WW CURVE 40405 )erator ID: JASON SAMUEL Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 08:40 Sample Type: Sample !p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.9456 0.0473 8951 10.485 10.514 120 2 1.0352 0.0518 9799 10.502 10.544 120 3 0.8055 0.0403 7625 10.512 10.527 120 4 •--------------------------------------------------------------------------- 0.8447 0.0422 7996 10.495 10.513 120 ist Message: Low Sample Detected XStatistics>>> Mean: 0.9078 Std Dev: 0.1035 RSD: 11.40 mple ID: CRI thod: TOC WASTE WATER 1. Curve: TOC WW CURVE 40405 erator ID: JASON SAMUEL plo ppm C ug C Raw Data Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 09:05 Sample Type: Sample Beginning Ending Integration ample ID: MBLK 1.9027 0.0951 Mode: Baseline Baseline Time 1 0.7509 0.0375 7108 10.382 10.325 120 2 1.0155 0.0508 9613 10.312 10.311 120 3 1.2174 0.0609 11523 10.274 10.285 120 4 1.4561 0.0728 13783 10.279 10.321 120 ------------------------------------------------------------------------ 2 0.4785 0.0239 4529 10.137 10.109 120 3se ssage: Low Sample Detected 10.082 10.118 120 ,<Statistics>>> 0.0495 Mean: 1.1100 Std Dev: 0.2996 RSD: 26.99 ist Message: Low ample ID: MBLK 1.9027 0.0951 Mode: TOC 10.092 �thod: TOC WASTE WATER 2 Filename: 04070730 0.0900 il. Curve: TOC WW CURVE 40405 10.025 Timestamp: 2005/04/07 09:31 )erator ID: JASON SAMUEL 1.9960 Sample Type: Sample 9.975 �p # ppm C ug C Raw Data Beginning Ending Integration 14222 10.022 10.032 Baseline Baseline Time 1 0.2166 0.0108 2051 10.218 10.169 120 2 0.4785 0.0239 4529 10.137 10.109 120 3 0.6406 0.0320 6064 10.082 10.118 120 4 0.9893 ---------------------------------------------------------------------------- 0.0495 9365 10.129 10.175 120 ist Message: Low Sample Detected ;<Statistics»> Mean: 0.5813 Std Dev: 0.3233 RSD: 55.62 imple ID: 0504024-005C !thod: TOC WASTE WATER il. Curve: TOC WW CURVE 40405 >e1Wr ID: JASON SAMUEL !p # ppm C ug C Raw Data Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 09:56 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 1 1.9027 0.0951 18011 10.081 10.092 120 2 1.8002 0.0900 17040 10.025 10.037 120 3 1.9960 0.0998 18893 9.975 10.033 120 4 ---------------------------------------------------------------------------- 1.5024 0.0751 14222 10.022 10.032 120 .st Message: Low Sample Detected <Statistics>>> Mean: 1.8003 Std Dev: 0.2141 RSD: 11.89 .mple ID: 0504024-006C thod: TOC WASTE WATER .1. Curve: TOC WW CURVE 40405 �erator ID: JASON SAMUEL p # ppm C ug C Raw Data 1 1.3125 0.0656 12423 2 0.9866 0.0493 9339 3 1.1123 0.0556 10528 4 1.1355 0.0568 10748 sjessage: Low Sample Detected Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 10:22 Sample Type: Sample Beginning Ending Baseline Baseline 9.947 9.974 9.944 9.950 9.961 9.971 9.964 ----------------------- 9.962 Integration Time 120 120 W) 120 O 120 4 ----------- O r� N <<Statistics>>> Mean: 1.1367 Std Dev: 0.1342 RSD: 11.81 ample ID: 0504024-009C Mode: TOC e TOC WASTE WATER Filename: 04070730 al urve: TOC WW CURVE 40405 Timestamp: 2005/04/07 10:47 Derator ID: JASON SAMUEL Sample Type: Sample ap # ppm C ug C Raw Data Beginning Ending Integration 0.0399 7559 9.909 9.885 Baseline Baseline Time 1 0.7302 0.0365 6912 10.062 10.091 120 2 0.4772 0.0239 4517 10.056 10.026 120 3 1.0164 0.0508 9621 10.008 10.022 120 4 0.6301 0.0315 5964 10.037 10.044 120 ---------------------------------------------------------------------------- ast Message: Low Sample Detected thod: TOC :<Statistics>>> Filename: 04070730 Mean: 0.7135 Std Dev: 0.2272 RSD: 31.84 ample ID: 0504067-001C ?thod: TOC WASTE WATER i1. Curve: TOC WW CURVE 40405 )erator ID: JASON SAMUEL ?p # ppm C ug C Raw Data Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 11:13 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 1 1.2955 0.0648 12263 9.933 9.924 120 2 0.7985 0.0399 7559 9.909 9.885 120 3 0.8953 0.0448 8474 9.848 9.843 120 4 --0_8342 0.0417 0.4700 88969 9.833 10.832 105 -------------- ist Message: Low ------7896---------9_820-------9_823-------120- Sample Detected 0.4644 87909 9.840 ---- XStatistics>>> Mean: 0.9559 Std Dev: 0.2299 RSD: 24.05 10.829 ample ID: LFB !thod: TOC WASTE WATER .1. Curve: TOC WW CURVE 40405 ,erator ID: JASON SAMUEL Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 11:37 Sample Type Sample p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 9.3252 0.4663 88270 9.812 10.803 105 2 9.3991 0.4700 88969 9.833 10.832 105 3 9.2871 0.4644 87909 9.840 10.839 105 4 --------------------------------------------------------------------------- 9.3531 0.4677 88533 9.836 10.829 105 <Statistics>>> Mean: 9.3411 Std Dev: 0.0472 RSD: 0.51 mple ID: LFBD Mode: TOC thod: TOC WASTE WATER Filename: 04070730 l0rve: TOC WW CURVE 40405 Timestamp: 2005/04/07 12:01 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration �thod: TOC WASTE WATER Baseline Baseline Time 1 9.5450 0.4772 90350 9.876 10.869 105 2� 9.0934 0.4547 86076 9.887 10.886 104 3 9.2291 0.4615 87360 9.903 10.894 104 4 ---------------------------------------------------------------------------- 9.4212 0.4711 89179 9.893 10.884 105 <<Statistics>>> Mean: 9.3222 Std Dev: 0.2004 RSD: 2.15 4323 ample ID: CCV ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 40405 Aerator ID: JASON SAMUEL Mode: TOC Filename: 04070730 Timestamp: 2005/04/07 12:26 Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration �thod: TOC WASTE WATER Baseline Baseline Time 1 22.9100 1.1455 216859 9.992 10.980 113 2 22.0672 1.1034 208881 10.048 11.036 112 3 22.1545 1.1077 209708 10.023 11.022 111 4 ---------------------------------------------------------------------------- 22.7790 1.1390 215620 9.986 10.985 112 "<Statistics>>> Mean: 22.4777 Std Dev: 0.4284 RSD: 1.91 4323 ample ID: CCB Mode: TOC �thod: TOC WASTE WATER Filename: 04070730 itrve: or TOC WW CURVE 40405 Timestamp: 2005/04/07 12:52 )e ID: JASON SAMUEL Sample Type: Sample �p # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.6739 0.0337 6379 9.874 9.870 120 2 0.4567 0.0228 4323 9.850 9.821 120 3 0.7087 0.0354 6708 9.787 9.797 120 4 ---------------------------------------------------------------------------- 0.5401 0.0270 5113 9.779 9.771 120 ist Message: Low Sample Detected :<Statistics>>> Mean: 0.5948 Std Dev: 0.1173 RSD: 19.72 • • 00 O O F-, Calibration Report Print Date/Time: 2005/04/07 13:08:04 al. Curve ID: TOC WW CURVE 40405 reated: 2005/04/04 18:18 alibration Factor (m): 1.893e+05 (b): 8697 _I*cept s ed: 0.99852 Standard ID Y X Expected Measured Message Date & Raw Data ug C ug C Time I 12025 0.000 0.018 Low Sample De 2005/04/04 15:48 .SPPM 14900 0.025 0.033 Low Sample De 2005/04/04 16:10 .OPPM 18657 0.050 0.053 Low Sample De 2005/04/04 16:31 .0PPM 53646 0.250 0.237 2005/04/04 16:52 ).OPPM 89582 0.500 0.427 2005/04/04 17:13 5.OPPM 249262 1.250 1.271 2005/04/04 17:34 ).OPPM 500784 2.500 2.599 2005/04/04 17:55 5.OPPM 706762 3.750 3.687 2005/04/04 18:16 • 00 O O F-, • • • U2M LABS, INC. SDG NO.: -` 00I SCAN: WO (4-� This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge.