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HomeMy WebLinkAboutMetals Data Package 09/2005i Analytical Data Package For T41AIN OF SDUTHOLD PART 360 ROUTINE SDG NO: TSL003 Water Samples Deceived: 9/16/05 METALS DATA PACKAGE U2M ILAUS, INC. 0 ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 ROUTINE WATER SAMPLES SAMPLES RECEIVED: 9/16/05 SDG NO.: TSI -003 I. NYS DEC SUMMARY FORMS II. SDG NARRATIVES III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY • U2M tAUS, INC. 0 NYS DEC SUMMARY FORMS • NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE IDENTIFICATION AND 01 ANALYTICAL REQUIREMENT SUMMARY 0 SDG: TSL003 Mal ical Requirements M M O CLP, - (Please indicate year of protocol) ASP 13 :o %q C/] TCUTAL, HSL, Priority Pollutant, SiW !ellt0.r Customer Laboratory Sample Sample ME we Code_ Code MW -1D __ 0509510-001 X X MW -1S 0509510-002 X X MW -3D --- — - — - --- - — 0509510-003 X I X MW -3S - 0509510-004 X X MW -4D 0509510-005 X X MW -4S 0509510-006 X X MW -5D 0509510-007 X X MW -5S 0509510-008 X X MW -6D 0509510-009 X i X MW -6S 0509510-010 X j X MW -8D 0509510-011 X X MW -8S 0509510-012 X X riEQPT BLANK 9/16 0509510-013 X X M M O CLP, - (Please indicate year of protocol) ASP 13 :o %q C/] TCUTAL, HSL, Priority Pollutant, SiW !ellt0.r 0 NEW YORK STATE DEPARTMENT OF EN ONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG : TSL003 INORGANIC ANALYSIS Laboratory Samp ID Client Sample ID Matrix Metals Requested DateRecd I at Lab Date Analyzed 0509510-001 MW -1D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-002 MW -1S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-002DUP MW -ISD WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-002MS MW -ISS WATER CA,CD,FE,K,MG,MN,NA,PB, 16-Scp-05 09/05 0509510-003 MW -3D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-004 MW -3S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-005 MW -4D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-006 MW -4S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-007 MW -5D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-008 MW -5S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-009 MW -6D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-010 MW -6S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-011 MW -8D WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-012 MW -8S WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 0509510-013 EQPT BLANK 9/16 WATER CA,CD,FE,K,MG,MN,NA,PB, 16 -Sep -05 09/05 TSL003 A4 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION • SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSI -003 INORGANIC ANALYSIS Laboratory j Samp ID ! Client Sample ID Matrix Tests DateRecd at Lab Date Analyze 0509510-001 MW -ID Groundwater SELECT WET CHEMISTRY'* 09/16/05 ' 09/05 0509510-002 MW -Is Groundwater SELECT WET CHEMISTRY *' 09/16/05 ! 09/05 0509510-002DUP MW-ISDUP Groundwater SELECT WET CHEMISTRY'* 09/16/05 09/05 0509510-002MS MW -ISMS i Groundwater j SELECT WET CHEMISTRY" 09/16/05 09/05 0509510-003 MW -3D Groundwater SELECT WET CHEMISTRY'* 09/16/05 09/05 0509510-004 MW -3S i Groundwater i SELECT WET CHEMISTRY'* 09/16/05 09/05 0509510-005 MW -4D ! Groundwater ! SELECT WET CHEMISTRY *' 09/16/05 09/05 0509510-006 MW4S Groundwater SELECT WET CHEMISTRY'* 09/16/05 09/05 0509510-007 MW -5D Groundwater i SELECT WET CHEMISTRY'* I 09/16/05 ! 09/05 0509510-008 MW -5S ! Groundwater SELECT WET CHEMISTRY" 09/16/05 09/05 - 10/05 0509510-009 MW -6D Groundwater SELECT WET CHEMISTRY" I 09/16/05 09/05 0509510-010 MW -6S Groundwater SELECT WET CHEMISTRY" 09/16/05 09/05 - 10/05 0509510-011 I MW -8D , Groundwater ! SELECT WET CHEMISTRY" 09/16/05 09/05 0509510-012 MW -8S Groundwater SELECT WET CHEMISTRY" 09/16/05 09/05 0509510-013 EQPT BLANK 9/16 i Blank SELECT WET CHEMISTRY " 09/16/05 09/05 • ** Alkalinity, Total (As CaCO3) ; Biochemical Oxygen Demand; Bromide; Chemical Oxygen Demand ; Chloride ; Hardness (As CaCO3) ; Nitrate as N ; Nitrogen, Ammonia (As N) ; Nitrogen, Kjeldahl, Total ; Phenolics, Total Recoverable ; Sulfate ; Total Dissolved Solids; Total Organic Carbon; • F12M UAUS, INC. 0 II. SDG NARRATIVES • U2M UAUS, INC. For Samples: NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 9/16/05 SDG#: TSL003 EQPT BLANK 9/16 MW -1D MW -1S MS/MSD MW -3D MW -3S MW -4D MW -4S MW -5D MW -5S MW -6D MW -6S MW -8D MW -8S Thirteen water samples were received by H2M Labs inc. on 9/16/05 for select metals analysis. • Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument. Sample MW -1S was utilized for QC analysis and reporting. No problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: October 4, 2005 o:\qc\narr2005\tsl\metals\ts1003.doc • ************************* Vincent Stancampiano Vice President U2M IA[3S, INC. SDG NARRATIVE FOR WET CHEMISTRY • SAMPLES RECEIVED: 9/16/05 SDG NO.: TSL003 For Samples: EQPT BLANK 9/16 MW -51) MW -ID MW -5S MW -1S MS/MSD MW -6D MW -3D MW -6S MW -3S MW -8D MW -4D MW -8S MW -4S Samples were prepared and analyzed using the following methods: PARAMETER Alkalinity BOD Bromide Chloride COD Hardness Ammonia METHOD # EPA 310.1 EPA 405.1 EPA 320.1 EPA325.2 EPA 410.4 EPA 130.2 EPA 350.1 PARAMETER Nitrate Phenols Sulfate TDS TKN TOC METHOD # EPA 353.2 EPA420.1 EPA 9038 EPA 160.1 EPA 351.2 EPA 9060 Sample MW -1S was utilized for duplicate and spike QC analysis and reporting. je results reported for BOD for samples MW -1D and MW -5D were derived from a calculation based on e COD reading due to BOD depletion. Several ammonia values exceeded the TKN concentration. All differences were within 20%RPD or ± the CRDL except for the following: Sample Ammonia mP/L TKN mQ/L RPD MW -5S 0.42 <0.1 200% MW -6S 0.23 <.01 200% Samples were diluted and reanalyzed as required to keep instrument readings within calibration ranges. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: October 7, 2005 o:\g6natr2005\ts1\wet chem\ts1003.doc • ************************* *****?in Joann Senior Vice President U2M [AUS., INC. E III. CHAIN OF CUSTODY DOCUMENTATION • • CN M O H U261 - INC. S7011. RF"d Nellew: Poo Mohdi/o_ NY 11747-5078. :1341 EXTERNAL: CHAIN ,fJF CUSTQDA r e: (51.0),.694-3"0, - Firxr (516) 420 -awe CLIENT:: /°C S C: JH SDG NO: P OJE. MBER L L Q nC �, NOTES: orpjivct Contact., wysaJFG C Ro vhrtie. Phone Number: 3(00 &sr/l/A6 CODS NH3 No Perls 7k1V ® 130- 5.� 8R r C L � ,SOt � ToTi4L X41 kA C J N r ?.D$ / MPLER$: (slgnsturayCllent . DELIVERABLES: -10— Q 16 . It ANALYSIS REQUESTED TURNAROUND TIME: ORGANIC J INORG. DATE '+TIME MATRIXFIELD.I.D. U LAB I.D. NOL I O REMARKS: w— i?JO /Ow— /.?40 mso Mw - W-1 112C MW S D �• t3�Q ubhed by (Slpnature) by slurs) Date to Tim o by. .( ) Date S LABORATORY USE ONLY Discrepancies Between Sample Cabala and COC Record? Y or N 1. Shipped or Hand delivered_ arbour 2. Ambient or Chilbd 3. Received In good o0ndilion: Y or N 4. PAY Prelarved: Y or N 3.3emples-mI mad to lob _ Hrs from collection. COC Taos wu: 1. Present on Oular peduge: Y or N 3. COC o c a dpresent & Complete upon "mPle Now, YorN RNlrqu4hed (Signature) Date Time Date' ReIMp1AsFNd by (Signature) Date TimeReoNwd ( Dal TWI#W69 ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATnRY U24 LA US, INC. .6. ' EXTERNAL CHAIN OGUST D Sys 6roed Hollow Rd. elvllld. NY 11747-5076 Toi: (510) 694-300Fixi Fix(s1 s o -a4 s CLIENT:, P X177 S L- HM SDG NO. PROJE NAME/NUMBER �.'Q At 7-0 90NY TOWN OF sou M.4Qi0zp c�T aa. 6 C�t3 �- $ ,e N _R 3 -. �? = ,� r i �` 3 Q c 6Cv - J NOTES: Project Contact: aEC C� R O c r hqr Phone Number: �1 x 1493 41 Ile -.0 C o D N H N© Phe n a I 3/ 3/ S sous, BR, C L SL TO TA L AL kq Z I N) , S SAMPLERS: (slgnatucey I ent H yw. DELIVERABLES: ANALYSIS REQUESTED : TURNAROUND TIME: a`. ORGANIC 1 INORG. DATE TIME MATRI FIELD I.D. ®As: v z LAB I.D:'NO. REMARKS: 4 is c63o �- W— I 3 3 Cna res s M s Z77 E Q PT 13 L4N Relinquish by: (Sipneture): Date Time s3 {S ) `�' (D u;1 Q LABORATORX'USE ONLY Discrepancies Between Sample Labels and C.Oe Record? Y or N d' 1. SNpped,_ or Hand Delivered_ Alrbill# 2 AmbW a. Y� 3. ReOdwd.in condition: Y or N 4. PmpwV preserved: Y or N S. Samples atumad to 4b _ Hrs from oolleclbn. COC Taor-w,ia: i t. Present on outer pecksps: Y or N 2 Unbmken on otrtar psdopa: Y or N 3. COC reowd presenl a cortpNte upon sample receipt: YarN n ul.trr tura) Date Time �? - lS ( Oatr 5'%!)n prra PAIImuWW by: (Siture)' Date Time ) Date RalinQuletted'by: (S"t") , Dab Time R.oNwd by: ( Date " TWhWcW - ORIGINAL YELLOW COPY - CLIENT PINK COPY - LABORATORY H2M LABS, INC. (L -T--s LC03' 0 Sample Receipt Checklist Client Name PCTSL Date and Time Receive 9/16/2005 9:53:00 AM Work Order Numbe10 Received by BGL Checklist completedb Reviewed by k I 0-w- Ns Ms Matrix Carrier name Hand Delivered Shipping container/cooler in good condition? Yes 0 No ❑ Not Applicable ❑ Custody seals iniad on shippping container/cooler? Yes ❑ No ❑ Not Applicable 0 Custody seals intact on sample bottles? Yes ❑ No ❑ Not Applicable 0 Chain of custody present? Yes 0 No ❑ Chain of custody signed when relinquished and received? Yes ® No ❑ Chain of custody agrees with sample labels? Yes ® No ❑ Samples in proper corgi iedbolOe? Yes B No D Sample containers intact? Yes 0 No D Sufficient sample volume for indicated test? Yes 0 No ❑ 4 amples received within holding time? Yes 0 No ❑ kainerfTemp Blank temperature in compliance? Yes 0 No ❑ Water - VOA vials have zero headspace? No VOA vials submitted 0 Yes ❑ No ❑ Water - pH acceptable upon receipt? Yes 0 No D Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section b --------------------------------------------- - — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — — - Cliient contacted Contacted by: Comments: Corrective Action Date contacted: Regarding Person contacted 1( j WA AADS, NCO INTERNAL CHAIN OF CUSTODY kov-,l - nd e%,Ahfc CUMiR-IS LDELIVERABLES: TURN AROUND TIME- zJ SDG CASE 0: MATRIX- pHCHECIaN REMARKS:- f'fl2_ RECEIVED BY: S)GNA7tWE--.�L&-DATE- METALS Fo 0043 NEVIN smomm IN im, 110111MEMINIMME! WIMMilml Emomm ROMP MEN mmb-q�blhm, MAIN �W- -ft�klc IMEMIMMIliffs- =.IMMl MENNEN IMEMIME METALS Fo 0043 U2A LAUS-9 WCo I L INTERNAL CHAIN OF CUSTODY METALS P 0044 MW . . . . . . . . .... 0.1m METALS P 0044 tom+► tAIES9 mac. • INTERNAL CHAIN OF CUSTODY cT.IExr: Mvlao L' ,IVERABi.ES. �n�xr/n�x,OUM TA t SDG #. '�C� CASE #:� MATRIX: `� I� V N REMARKS: . r a 1 .1 r : �C ,M lb W WET CHEMISTRY Ds -w P 0103. INN All I n no gal IN No -A ME iffivill NONE IN in Ml �EIMIM IN Ins 0 0 Now 1001400011 ME MEMO EMMMENES MIMMIN w Mill MA I MEMO UP MA V M, 0- f V WE MINE I N 1 N4 wAl WET CHEMISTRY Ds -w P 0103. HIA LAFS 9.11wa Vy sm I. -Mads INTERNAL CHAIN OF. CUSTODY RBLIHQUISHHD SAMPLE DATE TIME BY RECE IDy PURPOSE or DOT TLE cmuw= OF Typig CVSTOD'r IHI T IW@51 TV.-Pz> m SICU Mow slow maw vim slowslow. Blow 920w slow slow *sow slow allow slow Sim slicip allow ss" $200 sic" slow sicia slow sic" allow Sick$ slow sllc* slow sloU Slow slow allow SICIP allow slow . Slow silo" slow slow slow SICK slow sic)@ slow sic* slow sica -0 WET CHEMISTRY U2M I AUS, INC. 0 IV. ANALYTICAL DATA PACKAGE A. METALS B. WET CHEMISTRY • • 00 M O N IH2M ILAUS, INC. TT3EW3 s TABLE OF CONTENTS I. REPORTS 11. QC SUMMARY III. RAW DATA IV. DOCUMENTATION CJ • C: U.S. EPA - CLP COVER PAGE - INORGANIC ANALYSES DATA PACKAGE Lab Name: H2M LABS, INC. Lab Code: 10478 Case No SOW No.: ILM04.1 EPA Sample No. EQPT BLANK 9/16 MW -1D MW -1S MW-lSD MW-1SS L•lYY-JJ MW -4D MW -4S MW -5D MW -5S MW -6D MW -6S MW -8D MW -8S Were ICP interelement corrections applied? Were ICP backqround corrections applied? If yes -were raw data generated before application of background corrections? Comments: Date Reported: 9/28/05 Contract: SAS No.: SDG No.: TSL003 Lab Sample ID. 0509510-002 0509510-002DUP 0509510-002MS 0509510-003 0509510-004 0509510-005 0509510-007 V J V J J i V 0509510-009 0509510-010 Yes/No YES Yes/No YES Yes/No NO I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package and i the co ter -readable data submitted on diskette has been authorized by he La ra ry Manaqer or the Manaqer's desiqnee, as verified by the follow' g g e Signature: Z Name: Vincent Stancampiano Date: Title: Vice President • COVER PAGE - IN ILM04.1 U2M "US, INC. .7 REPORTS FOR METALS • • • • • U2M ILAUS, INC. QUALIFIERS FOR METALS ANALYSIS Q (Quality Control) Qualifiers E - The reported value is estimated because of the presence of interference. An explanatory note is included in the SDG narrative. M - Duplicate injection precision not met. N - Matrix spike sample recovery not within control limits. S- The "reported value was determined by the Method of Standard Additions (MSA). + - Correlation coefficient for the MSA is less than 0.995 W - Post digestion spike for Furnace AA analysis is out of control limits (85- 115%), while sample absorbance is less than 50% of spike absorbance. * - Duplicate analysis is not within control limits. C (Concentration) Qualifiers B - Entered if the reported value is less than the Contract Required Detection Limit (CRDL) but greater than the Instrument Detection Limit (IDL). U - Entered if the analyte was analyzed for but not detected, i.e., less than the IDL. M (Method) Qualifiers P - Analyzed by ICP. M - Analyzed by ICP -MS A - Analyzed by Flame AA. F - Analyzed by Furnace AA. CV - Analyzed by Manual Cold Vapor techniques. AV - Analyzed by Automated Cold Vapor techniques. C - Analyzed by Manual Spectrophotometric Method. CA- Analyzed by Midi -distillation Spectrophotometric Method. NR- Analyte not Required. U.S. EPA - CLP i1 Analyte Concentration C Q EPA SAMPLE NO 7440-43-9 Cadmium INORGANIC ANALYSIS DATA SHEET P 7440-70-2 Calcium 26200 P 7439-89-6 MW -1D 32.7 Lab Name: H2M LABS, INC. Contract: (Lead 1.2 U P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 P Matrix (soil/water): WATER Lab Sample ID: 0509510-001 P Level (low/med): LOW Date Received: 9/16/2005 P % Solids: 0.0 18400 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 26200 P 7439-89-6 Iron 32.7 B P 7439-92-1 (Lead 1.2 U P 7439-95-4 ;Magnesium 5480 P 7439-96-5 Manganese 7.2 B P 17440-09-7 Potassium 13200 P 7440-23-5 ISodium 18400 P Color Before: COLORLESS Clarity Before: • Color After: COLORLESS Clarity After: Comments: Date Reported: 9/28/05 • CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 M O E-4 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -1S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-002 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.59 B P 7440-70-2 Calcium 22500 P 7439-89-6 Iron 45.9 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4700 B P 7439-96-5 Manganese 7.91 B P 7440-09-7 Potassium 1530 B P 7440-23-5 Sodium 16900 P •Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 M O C/1 H U.S. EPA - CLP S1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET ME Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-003 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 23800 P 7439-89-6 Iron 21.2 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4670 B P ;7439-96-5 :Manganese 15.4 P 7440-09-7 lPotassium 1530 B P 7440-23-5 ISodium 16500 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 U.S. EPA - CLP • Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.37 U P 7440-7072 Calcium 22100 MW -3S Lab Name: H2M LABS, INC. Contract: B P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-004 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-7072 Calcium 22100 P 7439-89-6 Iron 24.2 B P 7439-92-1 Lead 1.2 U P 7939-95-4 IMagnesium 9300 B P 17439-96-5 'Manganese 14.7 B P 7440-09-7 'Potassium 1320 B P 7440-23-5 Sodium 15000 P Color Before: COLORLESS Clarity Before: •Color After: COLORLESS Clarity After: Comments: Date Reported: 9/28/05 �J CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 00 M O r� C/1 N U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -4D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-005 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 24100 P 7439-89-6 Iron 16.1 B P 7439-92-1 ILead 1.2 U P 7439-95-4 IMagnesium 4700 B P 7439-96-5 IManganese 14.8 B P 7440-09-7 Potassium 1770 B P 7440-23-5 Sodium 16800 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 U.S. EPA - CLP CAS No. Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET - U P 7440-70-2 MW -9S F Lab Name: H2M LABS, INC. Contract: 7439-89-6 Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-006 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 7439-96-5 'Manganese Concentration Units (ug/L or mg/kg dry weight): UG/L P CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 22700 P 7439-89-6 Iron 34.8 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4900 B P 7439-96-5 'Manganese 16.0 P 7440-09-7 jPotassium 1630 B P 7440-23-5 ISodium 15400 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 0 • O FORM I - IN ILM04.1 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -5D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-007 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 21700 P 7439-89-6 Iron 24.1 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 9810 B P 7439-96-5 Manganese 1 5.6 B P 7440-09-7 Potassium 6620 P 7440-23-5 Sodium 15900 P •Color Before: COLORLESS Clarity Before: CLEAR Color After: COLORLESS Clarity After: CLEAR Comments: Date Reported: 9/28/05 1 �J Texture: Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET �5S Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-008 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 22700 P 7439-89-6 Iron 18.3 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4690 B P 7439-96-5 ;Manganese 4.2 B P 7440-09-7 'Potassium 1430 B P 7440-23-5 Sodium 164001 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 U.S. EPA - CLP i1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -6D Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-009 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 22500 P 7439-89-6 Iron 43.2 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4510 B P 7439-96-5 Manganese 6.21 B I P 7440-09-7 Potassium 1330 B P 7940-23-5 Sodium 15300 P Color Before: COLORLESS Clarity Before • Color After: COLORLESS Clarity After: Comments: Date Reported: 9/28/05 CLEAR Texture: CLEAR Artifacts: FORM I - IN ILM04.1 U.S. EPA - CLP • Analyte 1 EPA SAMPLE NO M INORGANIC ANALYSIS DATA SHEET 0.37 U P 7440-70-2 Calcium 21100 MW -6S Lab Name: H2M LABS, INC. Contract: 18.1 B P Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-010 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 P i 17440-09-7 Concentration Units (ug/L or mg/kg dry weight): UG/L 1230 CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 21100 P 7439-89-6 Iron 18.1 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4290 B P 17439-96-5 Manganese 3.8i B P i 17440-09-7 Potassium 1230 B P 7440-23-5 Sodium 14400 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: • rted: 9/28/05 FORM I - IN ILM04.1 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET ::::�MW-=SD Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-011 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 23400 P 7439-89-6 Iron 14.3 B P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 4510 B P 7939-96-5 Manganese 11.3 B P 7440-09-7 Potassium 1320 B P 7440-23-5 Sodium 15000 P •Color Before: COLORLESS Clarity Before: CLEAR Texture: Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET MW -8 S Lab Name: H2M LABS, INC. Contract: F- -- Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-012 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 24200 P 7439-89-6 lIron 15.9 B P 7439-92-1 ILead 1.2 U P 7439-95-4 iMagnesium 4740 B P 7439-96-5 !Manganese 9.2 B P 7440-09-7 lPotassium 1390 B P 7440-23-5 Sodium 15700 P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 M O V1 FORM I - IN ILM04.1 [-4 U.S. EPA - CLP • 1 EPA SAMPLE NO INORGANIC ANALYSIS DATA SHEET EQPT BLANK 9/16 Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Matrix (soil/water): WATER Lab Sample ID: 0509510-013 Level (low/med): LOW Date Received: 9/16/2005 % Solids: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L CAS No. Analyte Concentration C Q M 7440-43-9 Cadmium 0.37 U P 7440-70-2 Calcium 141 B i P 7439-89-6 Iron 6.3 U P 7439-92-1 Lead 1.2 U P 7439-95-4 Magnesium 11.6 U, P 17439-96-5 Manganese 2.1 U P ' 7440-09-7 Potassium 32.3 B P 7440-23-5 Sodium 284 B P Color Before: COLORLESS Clarity Before: CLEAR Texture: • Color After: COLORLESS Clarity After: CLEAR Artifacts: Comments: Date Reported: 9/28/05 • FORM I - IN ILM04.1 U2M "US, INC. 0 Ii. QC SUMMARY FOR METALS A. INITIAL AND CONTINUING CALIBRATION VERIFICATION B. CRDL STANDARD FOR AA AND ICP C. METHOD BLANK D. ICP INTERFERENCE CHECK SAMPLE E. SPIKE SAMPLE RECOVERY F. POST DIGEST SPIKE SAMPLE RECOVERY G. DUPLICATES H. LABORATORY CONTROL SAMPLE I. STANDARD ADDITION RESULTS • J. ICP SERIAL DILUTIONS K. INSTRUMENT DETECTION LIMITS L. ICP INTERELEMENT CORRECTION FACTORS M. ICP LINEAR RANGES N. PREPARATION LOGS O. ANALYSIS RUN LOGS C7 U.S. EPA - CLP • 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L Analyte Initial Calibration True Found %R(1) True Continuing Calibration Found %R(1) Found %R(1) M Cadmium 2500.0 2499.63 100.0 2500.0 2526.89 101.1 2537.78• 101.5 P Calcium 50000.0 52045.53 104.1 50000.0 52670.61 105.3 52906.22 1 105.8 P Iron 50000.0 51116.23 102.2 50000.0 51540.91 103.1 51817.67 1 103.6 P Lead 500.0 502.43 100.5 500.0 509.13 101.8 509.84 102.0 P ,Magnesium Manganese 50000.0 2500.0-1 52947.94 2527.24 105.9 1 101.1 50000.0 2500.0 53658.48 2552.79 107.3 102.1 53816.98 12550.51 107.6 102.0 P P Potassium 80000.0 84029.31 105.0 80000.0 85646.42 107.1 84722.06 105.9 P Sodium 80000.0 82915.06 103.6 80000.0 84372.03 105.5 84391.73 105.5 P • (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 • FORM II (Part 1) - IN • U.S. EPA - CLP 2A INITIAL AND CONTINUING CALIBRATION VERIFICATION Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 Initial Calibration Verification Source: MV Labs/High Purity Continuing Calibration Verification Source: MV Labs/High Purity Concentration Units: ug/L • (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 • FORM II (Part 1) - IN Initial Calibration Continuing Calibration nalyte :Cadmium True Found %R(1) True Found %R(1) Found %R(1) M 2500.0 2547.09 101.9 2573.19 102.9 P Calcium 50000.0 52866.48 105.7 53261.97 106.5 P Iron 50000.0 52115.20 104.2 52768.73105.5 P Lead 500.0 510.35 102.1 511.94 102.4 P Magnesium 50000.0 53609.30 107.2 54093.65 108.2 P Manganese 2500.0 2541.86 101.7 2559.70 102.4 P Potassium 80000.0 82955.99 103.7 82995.65 103.7 P Sodium 180000.0 82843.20 103.6 82788.26 103.5 P • (1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115 • FORM II (Part 1) - IN • • U.S. EPA - CLP 2B CRDL STANDARD FOR AA AND ICP Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: AA CRDL Standard Source: ICP CRDL Standard Source: MV Labs/High Purity Concentration Units: ug/L SDG No.: TSL003 Analyte CRDL Standard for AA CRDL Standard Initial True Found %R True Found %R for ICP Final Found %R Cadmium 10.0 10.31 103.11 10.52 105.2 Lead 6.0 5.61 93.6 6.031 100.5 Manganese 30.0 30.15 100.5 30.63. 102.1 • FORM II (Part 2) - IN ILM04.1 • • U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL003 Analyte Initial Calib. Blank i (ug/L) C Continuing Blank 1 C Calibration (ug/L) 2 C 3 C Prepa- ration Blank C M Cadmium 0.5 B 0.4 B 0.6 B 0.4 1 U 0.365 U 1 P Calcium 41.2 B 54.7 B 51.0 B 36.4 B 18.022 U P Iron 8.4 B 12.6 B 9.4 B 6.3 U 6.302 U P Lead 1.2 U 1.2 U 1.2 U 1.2 U 1.159 U P Magnesium 11.6 U 18.4 B 11.6 U 11.6 U 11.554 U P Manganese 2.1 U 2.1 U 2.1 U 2.1 U 2.111 U P Potassium ! 70.4 B 65.5 B 67.2 B 57.4 B 36.200 B P Sodium 58.4 B 55.5 B 58.2 B 50.4 B 30.099 U P I • FORM III - IN ILM04.1 • • U.S. EPA - CLP 3 BLANKS Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: Preparation Blank Matrix (soil/water): WATER Preparation Blank Concentration Units (ug/L or mg/kg): UG/L SDG No.: TSL003 • FORM III - IN ILM04.1 Initial Calib. Continuing Calibration Prepa- Blank Blank (ug/L) ration Analyte (ug/L) C 1 C 2 C 3 C Blank C( Mi Cadmium 0.4 B P P Calcium 55.2 B P Iron 12.0 B P Lead 1.2 U Magnesium 19.8 B P Manganese 2.1 UP P Potassium 62.8 B P Sodium 65.5 B • FORM III - IN ILM04.1 U.S. EPA - CLP • 4 ICP INTERFERENCE CHECK SAMPLE • • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: ICP ID Number: TJA6IEA ICS Source SDG No.: TS1,003 MV Labs/High Purity Concentration Units: ug/L N M O FORM IV - IN ILM04.1 F-4 True Initial Found Final Found Sol. Sol. Sol. Sol. Sol. Sol. Analyte ( A AB A AB %R A AB %R Aluminum 500000 500000 „ 501303 496636.0 99.3 507030 503855.71 100.8 iCadmium 1000 952.4 95.2 i 976.0, 97.6 Calcium 500000 500000 514787 509677.3 101.9 526562 522928.0 104.6 Iron 200000 200000 203436 201773.5 100.9 210209 208757.0 104.4 Lead 1000 992.0 99.2 1010.0 101.0 Magnesium 500000 500000 512703 508821.1 101.8 521560 517408.7 103.5 Manganese 500 507.4 101.51 508.0 101.6 N M O FORM IV - IN ILM04.1 F-4 • C, Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 5A SPIKE SAMPLE RECOVERY Contract: SAS No.: EPA SAMPLE NO F ISS SDG No.: TSL003 Level (low/med): LOW Concentration Units (ug/L or mg/kg dry weight): UG/L Comments: • FORM V (Part 1) - IN ILM04.1 kn N M O Control Limit Spiked Sample Sample Spike Analyte %R Result (SSR) C Result (SR) C Added (SA) %R Q M Cadmium Iron 75-125 75-125 49.95001 992.5700 0.5900 45.9300 B B 50.00 1000.00 98.7 94.7 P P Lead 75-125 19.6078 513.6300 1.1592 7.9200 U i B: —7— 20.00 500.00 98.0 101.1 P P "Man Comments: • FORM V (Part 1) - IN ILM04.1 kn N M O • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER % Solids for Sample: 0.0 U.S. EPA - CLP 6 EPA SAMPLE NO DUPLICATES MW -1S Contract: SAS No.: SDG No.: TSL003 Level (low/med): LOW % Solids for Duplicate: 0.0 Concentration Units (ug/L or mg/kg dry weight): UG/L Analyte Control Limit Sample (S) C Duplicate (D) C RPD Q M Cadmium 5.0000 0.5900 B 0.3655 U 200.0 1PI Calcium 5000.0000 22465.7800 21673.2000 3.6 P Iron 1100.00001 1 45.9300 B 40.5400 B 12.5 P Lead 1.1592 U 1.1592 U P Magnesium 5000.0000 4698.8300 B 4523.6800 B 3.8 'P' Manganese 15.0000 7.9200 B 7.8000 B 1.5 P Potassium 5000.0000 1532.9900 B 1481.5300B 3.4 P Sodium 5000.0000 16926.0400 16106.6700 5.0 P r� • FORM VI - IN ILM04.1 • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Solid LCS Source: Aqueous LCS Source: U.S. EPA - CLP 7 LABORATORY CONTROL SAMPLE Contract: SAS No.: ERA MV Labs/High Purity SDG No.: TSL003 Analyte Aqueous (ug/L) True Found I Solid (mg/kg) %R True Found C Limits %R Cadmium 2500.0 2707.45 108.3 Calcium 50000.0 56371.86 112.7 Iron 50000.0 55894.86 111.8 Lead 500.0 547.81 109.6 Ma nesium 50000.0 57259.37 114.5 Man anese 2500.01 2750.20J 110.0 Potassium 80000.0 83655.16 104.6 Sodium 80000.0 90731.43 113.4 • • FORM VII - IN U.S. EPA - CLP • 8 STANDARD ADDITION RESULTS Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Contract: SAS No.: Concentration Units: ug/L SDG No.: TSL003 EPA Sample 0 ADD 1 ADD 2 ADD 3 ADD Final No. An ABS CON ABS CON ABS CON ABS Conc. r 4 • . FORM VIII - IN • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Matrix (soil/water): WATER U.S. EPA - CLP 9 ICP SERIAL DILUTIONS Contract: SAS No.: Concentration Units: ug/L MW -15 SDG No.: TSL003 Level (low/med): LOW Analyte Initial Sample Result (I) C Serial Dilution Result (S) C % Differ - ence Q M Cadmium 0.59 B 1.80 U 100.0 P Calcium 22465.78 22626.25 B 0.7ip?� Iron 45.93 B 41.50 B 9.6 Lead 1.20 U 5.80 U Ma nesium 4698.83 B 4582.70 B 2.5 Man anese 7.92 B 10.60 U, 100.0 ' P Potassium 1532.99 B 1555.95 B 1. 1 PI Sodium 16926.04 15485.05 BI 1 8.5 P • aFORM IX - IN ILM04.1 • r� U.S. EPA - CLP 10 INSTRUMENT DETECTION LIMITS (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. ICP ID Number: TJA6IEA Flame AA ID Number: Furnace AA ID Number: Comments: Contract: SAS No.: Date: 4/4/2005 SDG No.: TSL003 Analyte Wave- length Back- (nm) ground CRDL (ug/L) IDL (ug/L) M Cadmium 226.50 5.0 0.4 P Calcium 317.93 5000.0 18.0 P Iron 271.40 100.0 6.3 P Lead 220.35 3.0 1.2 P Ma nesium 279.08 5000.0 11.6 P Manganese 257.61 15.0 2.1 P Potassium 766.49 5000.0 20.4 P Sodium 330.20 5000.0 30.1 P • FORM X - IN ILM04.1 U.S. EPA - CLP • 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL003 ICP ID Number: TJA6IEA Date: 04/29/2005 • • Analyte Wave- length (nm) Interelement Al Ca Correction Factors for: Fe Mg Co Aluminum 308.22 0.0000000 0.0000000 0.0000000 0.0000000 -0.0170000 Antimony 206.84 0.0000000 0.00000001 0.0274000 0.0000000 0.0000000 Antimony 206.841 0.0000000, 0.0000000' 0.0380000 0.0000000 0.0000000 Arsenic 189.04 0.0127000 0.0000000 -0.0100000 0.0000000 -0.2470000 Barium 493.411 1 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Beryllium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Boron 249.68 0.0000000 0.0000000 -0.0004000 0.0000000 0.0017000 Cadmium 226.50 0.0000000 0.0000000 0.0001000 0.0000000 0.0000000 Calcium 317.93 0.00030001 0.0000000 0.0002000 0.0000000 0.0000000 Chromium 267.62 1 0.0000000' 0-00000001 0.0000000 0.0000000 0.0000000 Cobalt 228.62 0.00000001 0.00000001 0.0000200 0.0000000 0.0000000 Copper 324.75 0.0000000 0.0000000 -0.0000400 0.0000000 -0.0004000 Iron 259.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Iron 271.44 0.0000000 0.0000000 0.0000000 0.0000000 0.0920000 Lead 220.35 -0.2670000 0.0000000 0.0900000 0.0000000 0.0890000 _ Lead 220.35 1 0.4000000; 0.0000000 0.2200000 0.0000000 0.0900000 Magnesium 279.08 0.0000000E__0.0000000 0.0000000 0.0000000 0.0000000 Manganese 257.61 1 -0.00012001 0.0000000 0.0000400 0.0000000 -0.0002000 Molybdenum 202.03 1 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 -0.0004200 Potassium 766.490.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 -0.0063000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.0000000 0.0000000 0.3540000 Silicon 288.16 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Silver 328.07 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 330.23 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 589.00 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Strontium 407.77 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Thallium 190.86 0.0000000 0.0000000 -0.3600000 0.0000000 -0.5800000 Comments: FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP • 11A ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL003 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Al Interelement Ca Correction Fe Factors for: Mg Co Tin 189.99 0.0000000 0.0000000 -0.0004000 0.0000000 0.0000000 Titanium 334.94 0.0000000 0.0000000 0.0000000 0.0000000 0.0000500 Vanadium 292.40 0.0000000 0.0000000 0.0000200 0.00000001 0.0000000 Zinc 213.861i 0.0000000 0.0000000 0.0000250 0.00000001 0.0000000 • Comments: C7 FORM XI (PART 1) - IN ILM04.1 U.S. EPA - CLP 0 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL003 ICP ID Number: TJA6IEA Date: 04/29/2005 Fj • Analyte Wave- length (nm) Cr Interelement Cu Correction Mn Factors for: Ni V Aluminum 308.22 0.0000000 0.0000000 -0.0012000 0.0000000 0.0000000 AntimonV 206.84 7.1400000 0.0000000 -0.3830000 0.0000000 0.0000000 AntimonV 206.84 8.8100000 0.0000000 0.2510000 -1.0900000 -6.3000000 Arsenic 189.04 0.2500000 0.00000001 -0.2010000 0.0000000 0.0000000 Barium 493.41 0.0000000 0.0000000 0.00000001 0.0000000 0.0000000 Ber llium 313.04 0.0000000 0.0000000 0.0000000 0.0000000 0.0002000 Boron 249.68 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Cadmium 226.50 0.0000400 0.0000000 0.0000000 -0.0001800 0.0000000 Calcium 317.93 0.0000000 0.0000000 0.0000000 0.0000000 0.0019000 Chromium 267.62 0.0000000 0.0000000 0.0000000 0.0000000 0.0002960 Cobalt 228.62 0.0000000 0.0000000 0.0000000 0.00017001 0.0000000 Copper 324.75 0.0000000 0.00000001 0.0000000 0.00000001 0.0000360 Iron _ 259.94 0.0000000 0.00000001 0.0000000 0.0000000 0.0000000 Iron 271.44 0.0000000 0.0000000 -0.0038000 0.0000000 0.0000000 Lead 220.35 0.0000000 0.0000000 0.0000000 0.1500000 -0.1900000 Lead 220.35 0.0000000 0.0000000 0.0000000 0.3000000 -0.0200000 Magnesium 279.08 -0.0001000 0.0000000 0.1400000 -0.0001000 0.0000000 Manganese 257.61 0.0000000 0.0000000 0.0000000 0.0000000 -0.0001000 Mol bdenum 202.03 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Nickel 231.60 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Potassium 766.49 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.3250000 0.0000000 0.0000000 Selenium 196.03 0.0000000 0.0000000 0.4100000 0.0000000 0.0000000 Silicon 288.16 1 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Silver 328.07 0.0000000 0.0000000 0.1780000 0.0000000 -0.0433000 Sodium 330.23 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Sodium 589.00 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Strontium 1 407.77 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Thallium 1 190.86 0.1720000 0.0000000 -0.7417000 0.0000000 -0.9000000 Comments: FORM XI (PART 2) - IN ILM04.1 U.S. EPA - CLP • 11B ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: NRAS No.: SDG No.: TSL003 ICP ID Number: TJA6IEA Date: 04/29/2005 Analyte Wave- length (nm) Cr Interelement Cu Correction Mn Factors for: Ni V Tin Titanium 189.99 334.94 -0.0001100 0.0000000 -0.0001000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Vanadium 292.40 0.0000000 0.0000000 0.0000000 0.0000000 0.0000000 Zinc 213.86 0.0000000 0.00040001 0.0000000 0.0042000 0.0000000 .7 Comments: • FORM XI (PART 2) - IN ILM04.1 • • U.S. EPA - CLP 12 ICP LINEAR RANGES (SEMI ANNUALLY) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No. SAS No.: SDG No.: TSL003 ICP ID Number: TJA6IEA Date: 05/12/2005 Comments: Analyte Integ. Time (Sec.) Concentration (ug/L) M Cadmium 15.00 10000 P Calcium 15.00 750000P Iron 15.00 275000 P 'Lead 15.00 50000,P 'Magnesium 15.00 10000001P ;Man anese 15.00 20000 P Potassium 15.00 250000 P Sodium 15.001 500000 P • FORM XII - IN ILM04.1 • J Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Method: P U.S. EPA - CLP 13 PREPARATION LOG Contract: SAS No.: SDG No.: TSL003 EPA Sample No. Preparation Weight Date (gram) Volume (mL) LCSW 09/19/2005 50 MW -1D 09/19/2005 50 MW -is 09/19/2005 50 Mw-isD 09/19/2005 50 MW -ISS 09/19/2005 50 MW -3D 09/19/2005 50 MW -3S 09/19/2005 50 MW -4D 09/19/2005 50 MW -4S 09/19/2005 50 MW -5D 09/19/2005 50 MW -5S 09/19/2005 50 MW -6D 09/19/2005 ---5-O- 0MW-6S M-W--6S 09/19/2005 50 MW -8D 09/19/2005 50 MW -8S 09/19/2005 50 PBW 09/19/2005 50 QPT BLANK 9/16 09/19/2005 50 • FORM XIII - IN ILM04.1 C7 • Cl Lab Name: H2M LABS, INC. Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 09/28/2005 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.: Method: P End Date: SDG No.: TSL003 09/28/2005 FORM XIV - IN ILM04.1 O 0� MEN ■■■■MEN ■■■■■■■■■■■■■■ © • . 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Lab Code: 10478 Case No. Instrument ID Number: TJA6IEA Start Date: 09/28/2005 U.S. EPA - CLP 14 ANALYSIS RUN LOG Contract: SAS No.. Method: P End Date: SDG No.: TSL003 09/28/2005 EPA Sample No. D/F Time % R A L S A B B� C C C B S A E D A R Analytes C C F P M M 0 U E B G N H N K G I S A N T V Z C E G A L N N CCB 1.00 1059 X I X X I X I X X1 I Ix Ix CRI 1.00 1107 XI Ix X ICSA 1.00 1115 X X X X X X X ICSAB 1.00 1122 X X X X X X X cCv 1.00 1130%; X: X X X X X X CCB 1.00 1138 X X X X X X X X zzzzzz 1.00 1146 ZZZZZz 1.00 1154 zzzzzz 1.00 1201 zzzzzz 1.00 1209 zzzzzz 1.00 1217 zzzzzz 1.00 1225 zzzzzz 1.00 1232 zzzzzz 1.00 1243 zzzzzz 1.00 1251 zzzzzz 1.00 1259 zzzzzz 1.00 1307 zzzzzz 1.00 1314 zzzzzz 1.00 1322 zzzzzz 1.00 1330 zzzzzz 1.00 1338 zzzzzz 1.00 1346 zzzzzz 1.00 1353 zzzzzz 1.00 1401 0 FORM XIV - IN ILM04.1 00 M M O C/) H U2M UAUS, INC. • III. RAW DATA FOR METALS A. ICP DATA • • rn M M O F-� t P214 tA[3s, mac. CLIENT -rS ( p0? DATE TASK: C P RESULT FILE: PS 92._'}0'9' ANALYST _ # SAMPLE NOTES : # : SAMPLE NOTES ; • 1 1 1 26:0"frio - Wy ' r ; jri jet # i ; 15'Elva -00jG1 M-30 40 2 27;Os�i.Sw - �t'�G; L�Qr� �iA1Jlc'/ 16' -WM 1 • 1 3 ; C At 41: 28: 29: CZ 42'.C ' ' 18' CW 1, ; : 43' 1 1 191 1 . 1 - wl Jp 32,' SuJ►t r ; 1 8 : Ikb -14YLf : PQ w -1-33: CW • 1 9' ; Lt 1 KYLf - 22' 0 - M W - ' 47: • 1 10;or-O ll -it -Ooi-E ►MW -t S : 35:'1. I�t�P�'� : ��c��'t2 1 ' • 1 � ' 11bow 36' 24' O't -ol 4 e :�� Mj,-Mr: A 37: ' 1 1 e 13 0 -00 LC 4CA ' • 14� d -opt m vV--1 39: -W ' 15'Elva -00jG1 M-30 40 16' -WM kyj-3 ' 41: c4wr ; 42'.C ' ' 18' CW 1, ; : 43' ' ,F 191 1 . 1 - wl Jp ' 22' 0 - M W - ' 47: t9Oj ' ' 48: 00 O . 24' O't -ol 4 e :�� 49: A ` ' O V) C/1 1 , ; . 1 50 51 CC6� ` r page 1 Ca .0125 .0008 6.394 .0116 .0129 .0131 K .0071 .0004 5.359 .0067 .0075 .0071 2203/1 .01430 .00761 53.245 .01674 .02039 .00576 Sn .0046 .0003 6.171 .0045 .0044 .0049 M O H Standardization Rpt.s 06:46r .37 AM Method: CLP1 Standard: StdBLANK Run Time: 09/28/05 06:38:56 Ag Al As1890 B Ba Be -.00425 .0070 -.00146 .0024 .0004 -.0010 SDev .00010 .0003 .00085 .0001 .0000 .0000 %RSD 2.3421 3.944 58.068 2.769 10.65 2.493 #1 -.00426 .0067 -.00197 .0023 .0004 -.0010 #2 -.00434 .0071 -.00192 .0024 .0004 -.0009 #3 -.00414 .0071 -.00048 .0025 .0004 -.0010 Elem Cd Co Cr Cu Fe Fe Avge -.0005 .0001 .0004 .0032 .0000 .0358 SDev .0011 .0001 .0000 .0001 .0000 .0197 %RSD 234.9 138.9 11.17 2.926 49.80 54.89 #1 -.0018 -.0000 .0003 .0031 .0000 .0143 #2 .0003 .0002 .0004 .0032 .0001 .0404 #3 .0001 .0001 .0004 .0032 .0001 .0527 Elem Mg Mn Mo Na Na Ni Avge .0015 .0008 .0000 -.0189 .4048 .0003 SDev .0008 .0002 .0001 .0009 .0141 .0002 %RSD 53.73 22.56 433.9 4.959 3.495 61.62 #1 .0006 .0006 -.0000 -.0199 .3885 .0002 #2 .0020 .0010 -.0000 -.0181 .4128 .0005 .0018 .0009 .0001 -.0187 .4132 .0001 E em 2203/2 2068/1 2068/2 1960/1 1960/2 Si Avge .00007 -.00474 .00076 -.00806 .00100 .0551 SDev .00231 .00390 .00121 .00036 .00152 .0001 %RSD 3334.0 82.300 159.46 4.4277 151.79 .2494 #1 .00191 -.00482 .00036 -.00792 .00235 .0549 #2 -.00252 -.00860 .00212 -.00779 -.00065 .0551 #3 .00082 -.00080 -.00020 -.00846 .00130 .0552 Elem Sr Ti T11908 v Zn Avge .0009 .0003 -.00397 .0000 .0042 SDev .0001 .0000 .00094 .0000 .0001 %RSD 8.219 .7124 23.740 89.06 1.775 #1 .0009 .0003 -.00498 .0000 .0042 #2 .0010 .0003 -.00311 .0001 .0043 #3 .0009 .0003 -.00382 .0001 .0042 page 1 Ca .0125 .0008 6.394 .0116 .0129 .0131 K .0071 .0004 5.359 .0067 .0075 .0071 2203/1 .01430 .00761 53.245 .01674 .02039 .00576 Sn .0046 .0003 6.171 .0045 .0044 .0049 M O H Standardization Rpt. 09/28/05 06:52:50 AM Method: CLP1 Standard: StdAGSBH Run Time: 09/28/05 06:46:43 Ag 2068/1 2068/2 A .72538 3.0145 1.9199 SDev .01223 .0466 .0339 %RSD 1.6854 1.5463 1.7654 #1 .71346 2.9643 1.8849 #2 .73789 3.0565 1.9526 #3 .72479 3.0226 1.9222 • • page 1 Standardization Rpt. 09/28/05 06:58:16 AM page 1 Method: CLP1 Standard: StdICSH Run Time: 09/28/05 06:52:56 • Mg 70.86 .22 .3126 70.78 70.69 71.11 M d' cr1 O V) N Al Ca Fe A 30.28 52.18 .5996 SDev .12 .13 .0011 %RSD .3832 .2561 .1809 #1 30.42 52.11 .5998 #2 30.19 52.10 .5984 #3 30.25 52.34 .6005 • Mg 70.86 .22 .3126 70.78 70.69 71.11 M d' cr1 O V) N Standardization Rpt. 09/28/05 07:04:29 AM page 1 Method: CLP1 Standard: StdFURNH Run Time: 09/28/05 06:58:22 As1890 2203/1 2203/2 1960/1 1960/2 T11908 A 1.1829 4.1149 1.7609 .86298 .62206 1.0201 SDev .0065 .0170 .0091 .00631 .00321 .0083 %RSD .54979 .41243 .51542 .73117 .51683 .81529 #1 1.1852 4.1312 1.7625 .86849 .62241 1.0219 #2 1.1879 4.1161 1.7690 .86435 .62508 1.0273 #3 1.1755 4.0974 1.7511 .85610 .61868 1.0110 • M • O H Standardization Rpt. Method: CLP1 Standard: StdMULTH Run Time: 09/28/05 07:04:35 2.027 2.524 B Ba Be A e 1.672 5.129 6.756 SDev .020 .024 .075 %RSD 1.225 .4689 1.112 #1 1.649 5.101 6.671 #2 1.678 5.145 6.783 #3 1.688 5.141 6.813 Elem Mn Mo Ni Avge 17.38 1.964 2.085 SDev .17 .018 .013 %RSD .9658 .9361 .6125 #1 17.19 1.944 2.070 #2 17.44 1.969 2.090 #3 17.51 1.980 2.093 Elem v Zn Avge 1.229 4.643 SDev .011 .057 %RSD .9307 1.232 #1 1.216 4.579 #2 1.234 4.663 0 1.237 4.688 • 09/28/05 07:11:29 AM page 1 Cd Co Cr Cu 64.11 2.027 2.524 1.388 .49 .027 .024 .009 .7703 1.338 .9393 .6428 63.56 1.996 2.498 1.378 64.27 2.036 2.533 1.391 64.51 2.048 2.543 1.394 Si Sn Sr Ti 2.549 10.22 10.05 1.830 .041 .18 .07 .006 1.622 1.767 .6471 .3159 2.508 10.02 9.977 1.836 2.550 10.29 10.09 1.826 2.590 10.36 10.09 1.827 Standardization Rpt. 09/28/05 07:16:56 AM page 1 Hethod: CLP1 Standard: StdFENAL Stun Time: 09/28/05 07:11:36 E40 Fe Na A 42.52 45.20 SDev .10 .42 %RSD .2434 .9292 #1 42.42 45.49 #2 42.50 45.39 #3 42.63 44.72 is 1� Standardization Rpt. Kethod: CLP1 Standard: StdNAKH lun Time: 09/28/05 07:17:02 E# K Na Avge 9.331 2.147 SDev .039 .014 %RSD .4186 .6615 #1 9.375 2.163 #2 9.317 2.141 #3 9.300 2.137 • • 09/28/05 07:21:36 AM page 1 Standardization Report 09/28/05 07:21:36 AM page 1 4ethod: CLP1 Slope = Conc(SIR)/IR 31e t Wavelen High std Low std Slope Y -intercept Date Standardized kg 328.068 StdAGSBH StdBLANK 2741.11 11.6415 09/28/05 07:17:02 k1 308.215 StdICSH StdBLANK 16.5136 -.115356 09/28/05 07:17:02 ks1890 189.042 StdFURNH StdBLANK 844.360 1.22944 09/28/05 07:17:02 3 249.678 StdMULTH StdBLANK 3.00037 -.007233 09/28/05 07:17:02 3a 493.409 StdMULTH StdBLANK .974897 -.000397 09/28/05 07:17:02 3e 313.042 StdMULTH StdBLANK .740154 .000717 09/28/05 07:17:02 7a 317.933 StdICSH StdBLANK .937430 -.003957 09/28/05 07:17:02 226.502 StdMULTH StdBLANK .077976 .000038 09/28/05 07:17:02 -Nd -0 228.616 StdMULTH StdBLANK 2.46687 -.000216 09/28/05 07:17:02 ;r 267.716 StdMULTH StdBLANK 1.98145 -.000768 09/28/05 07:17:02 7u 324.754 StdMULTH StdBLANK 3.61030 -.011452 09/28/05 07:17:02 ?e 271.441 StdICSH StdBLANK 1.00568 .000008 09/28/05 07:17:02 ?e 259.940 StdFENAL StdBLANK .117697 -.004212 09/28/05 07:17:02 t 766.491 StdNAKH StdBLANK .857547 .000665 09/28/05 07:17:02 4g 279.079 StdICSH StdBLANK .883872 -.000705 09/28/05 07:17:02 4n 257.610 StdMULTH StdBLANK .287723 -.000244 09/28/05 07:17:02 40 202.030 StdMULTH StdBLANK 2.54564 -.000034 09/28/05 07:17:02 4a 330.232 StdNAKH StdBLANK .930871 -.011027 09/28/05 07:17:02 4a 588.995 StdFENAL StdBLANK .111620 -.045186 09/28/05 07:17:02 4i 231.604 StdMULTH StdBLANK 2.39795 -.000690 09/28/05 07:17:02 ?203/1 220.351 StdFURNH StdBLANK 243.867 -3.48632 09/28/05 07:17:02 ?203/2 220.352 StdFURNH StdBLANK 567.924 -.039355 09/28/05 07:17:02 ?068/1 206.831 StdAGSBH StdBLANK 662.426 3.13896 09/28/05 07:17:02 ?068/2 206.832 StdAGSBH StdBLANK 1042.15 -.791200 09/28/05 07:17:02 L960 1 196.021 StdFURNH StdBLANK 1148.05 9.25212 09/28/05 07:17:02 L9 196.022 StdFURNH StdBLANK 1610.16 -1.61188 09/28/05 07:17:02 Si 288.158 StdMULTH StdBLANK 1.98352 -.109268 09/28/05 07:17:02 Sn 189.989 StdMULTH StdBLANK .489097 -.002257 09/28/05 07:17:02 Sr 421.552 StdMULTH StdBLANK .497484 -.000465 09/28/05 07:17:02 ri 334.941 StdMULTH StdBLANK 2.73336 -.000712 09/28/05 07:17:02 011908 190.864 StdFURNH StdBLANK 976.544 3.87560 09/28/05 07:17:02 I 292.402 StdMULTH StdBLANK 4.06861 -.000191 09/28/05 07:17:02 ;n 213.856 StdMULTH StdBLANK 1.07780 -.004542 09/28/05 07:17:02 ?b2203 220.353 NONE NONE 1.00000 .000000 *NOT STANDARDIZED *NOT STANDARDIZED 33b2068 206.838 NONE NONE NONE 1.00000 1.00000 .000000 *NOT STANDARDIZED 3e1960 196.026 NONE .000000 • Standardization Readback Report 09/28/05 07:21:36 AM page 1 Method: CLP1 E1 nt Wavelength Standard A 328.068 StdBLANK StdAGSBH Element Wavelength Standard Al 308.215 StdBLANK StdICSH Element Wavelength Standard ks1890 189.042 StdBLANK StdFURNH Element Wavelength Standard 3 249.678 StdBLANK StdMULTH 3lement Wavelength Standard 3a 493.409 StdBLANK StdMULTH 3lement Wavelength Standard 3e• 313.042 StdBLANK StdMULTH 3lement Wavelength Standard -a 317.933 StdBLANK StdICSH ;lement Wavelength Standard 'd 226.502 StdBLANK StdMULTH :lement Wavelength Standard .0 228.616 StdBLANK StdMULTH :lement Wavelength Standard 'r 267.716 StdBLANK StdMULTH ;lement Wavelength Standard :u 324.754 StdBLANK • StdMULTH Known Concentration .000000 2000.00 Known Concentration .000000 500.000 Known Concentration .000000 1000.00 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Signal .007782 48.9123 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Known Concentration .000000 5.00000 Measured Concentration -.000000 2000.00 Measured Concentration -.000000 500.000 Measured Concentration -.000000 1000.00 Measured Concentration .000000 5.00840 Measured Concentration .000000 5.00000 Measured Concentration -.000000 5.00095 Measured Signal .012523 52.1813 Measured Concentration .000000 4.99930 Measured Concentration .000000 5.00000 Measured Concentration .000000 5.00108 Measured Concentration -.000000 4.99875 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration -.000000 -.008400 Residual Concentration -.000000 .000000 Residual Concentration .000000 -.000950 Residual Signal -.004741 -3.26896 Residual Concentration -.000000 .000700 Residual Concentration -.000000 .000000 Residual Concentration -.000000 -.001080 Residual �t Concentration .000000 M .001245 Cn H Standardization Readback Report Element Wavelength Standard F 271.441 StdBLANK e� StdICSH Element Wavelength Standard Fe 259.940 StdBLANK StdFENAL Element Wavelength Standard K 766.491 StdBLANK StdNAKH Element Wavelength Standard Mg 279.079 StdBLANK StdICSH Element Wavelength Standard Mn 257.610 StdBLANK StdMULTH Element Wavelength Standard Mo 202.030 StdBLANK • StdMULTH Element Wavelength Standard Va 330.232 StdBLANK StdNAKH Element Wavelength Standard Ja 588.995 StdBLANK StdFENAL Element Wavelength Standard Ji 231.604 StdBLANK StdMULTH 3lement Wavelength Standard ?203/1 220.351 StdBLANK StdFURNH 3lement Wavelength Standard ?203/2 220.352 StdBLANK ID StdFURNH 09/28/05 07:21:36 AM Known Measured Signal Signal .000055 .000047 .602976 .599560 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Signal Signal .006759 .007106 8.00205 9.33055 Known Measured Signal Signal .000584 .001459 62.6316 70.8613 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Signal Signal -.028601 -.018879 1.98779 2.14725 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.99790 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 page 2 Residual Signal .000008 .003416 Residual Concentration .000000 .000000 Residual Signal -.000348 -1.32850 Residual Signal -.000875 -8.22967 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Signal -.009722 -.159465 Residual Concentration .000000 .000000 Residual Concentration .000000 .002100 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000000 M O Cn F-4 Standardization Readback Report 09/28/05 07:21:36 AM Element Wavelength Standard 20 /1 206.831 StdBLANK StdAGSBH Element Wavelength Standard 2068/2 206.832 StdBLANK StdAGSBH Element Wavelength Standard 1960/1 196.021 StdBLANK StdFURNH Element Wavelength Standard 1960/2 196.022 StdBLANK StdFURNH Element Wavelength Standard 3i 288.158 StdBLANK StdMULTH Element Wavelength Standard 3n 189.989 StdBLANK • StdMULTH 3lement Wavelength Standard 3r 421.552 StdBLANK StdMULTH clement Wavelength Standard 'i 334.941 StdBLANK StdMULTH :lement Wavelength Standard '11908 190.864 StdBLANK StdFURNH :lement Wavelength Standard ' 292.402 StdBLANK StdMULTH ;lement Wavelength Standard n 213.856 StdBLANK StdMULTH U Known Measured Concentration Concentration .000000 .000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 -.000000 2000.00 2000.00 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 .000000 1000.00 1000.00 Known Measured Concentration Concentration .000000 .000000 5.00000 4.94713 Known Measured Concentration Concentration .000000 -.000000 5.00000 4.99870 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 1000.00 1000.000 Known Measured Concentration Concentration .000000 .000000 5.00000 5.00000 Known Measured Concentration Concentration .000000 -.000000 5.00000 5.00000 page 3 Residual Concentration -.000000 .000122 Residual Concentration .000000 -.000122 Residual Concentration .000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .052870 Residual Concentration .000000 .001300 Residual Concentration -.000000 .000000 Residual Concentration -.000000 .000000 Residual Concentration .000000 .000061 Residual Concentration -.000000 .000000 Residual Concentration ,f) .000000 .000000 M O C/1 H Standardization Readback Repo Element Wavelength Standard Pb�3 220.353 NONE NONE Element Wavelength Standard Sb2068 206.838 NONE NONE Element Wavelength Standard Se1960 196.026 NONE NONE C, • rt 09/28/05 07:21:36 AM Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 Known Measured Concentration Concentration .000000 .000000 .000000 .000000 page 4 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 Residual Concentration .000000 .000000 knalysis Report 09/28/05 07:29:22 AM page 1 Method: CLP1 Sample Name: ICV Operator: PES tun Time: 09/28/05 07:21:42 -0t: 40MCONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 996.41 51.43 516.00 2.512 2.562 2.548 52.05 SDev 5.39 .40 3.10 .023 .012 .017 .38 %RSD .54055 .7755 .60013 .9189 .4870 .6822 .7216 #1 990.36 51.01 512.42 2.487 2.548 2.530 51.63 #2 998.20 51.81 517.79 2.520 2.564 2.550 52.16 #3 1000.7 51.48 517.78 2.531 2.573 2.565 52.35 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge 2.500 2.541 2.520 2.584 51.12 84.03 52.95 SDev .011 .021 .016 .020 .26 1.08 .41 %RSD .4203 .8367 .6339 .7677 .5165 1.285 .7781 #1 2.490 2.518 2.503 2.561 50.84 83.00 52.49 #2 2.499 2.546 2.523 2.593 51.14 85.15 53.06 #3 2.511 2.560 2.534 2.597 51.37 83.94 53.29 E*s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.527 2.587 82.92 2.508 512.54 497.39 982.50 SDev .017 .019 1.07 .009 2.50 3.15 6.30 %RSD .6591 .7377 1.288 .3735 .48821 .63412 .64136 #1 2.509 2.571 81.79 2.499 509.73 493.91 976.11 #2 2.531 2.581 83.91 2.507 514.54 498.17 982.67 #3 2.542 2.608 83.05 2.517 513.34 500.07 988.71 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 961.23 512.78 512.15 2.503 2.549 2.542 2.564 SDev 3.16 1.40 1.76 .042 .028 .018 .004 96RSD .32908 .27310 .34287 1.669 1.111 .7025 .1595 # 957.79 513.15 510.92 2.457 2.519 2.522 2.569 #0 961.88 511.24 511.37 2.515 2.554 2.553 2.562 #3 964.02 513.97 514.16 2.537 2.575 2.552 2.562 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/28/05 07:29:22 AM page 2 High AEL Unit Avge SDev %RSD #1 #2 #3 Error High Low • d' • M O E-� T11908 v Zn Pb2203 Sb2068 Se1960 s ppb ppm ppm ppb ppb ppb 500.86 2.549 2.652 502.43 968.31 512.36 2.97 .017 .021 2.85 4.20 1.51 .59201 .6828 .7992 .56678 .43329 .29498 497.44 2.530 2.629 499.18 963.89 511.66 502.33 2.555 2.656 503.62 968.80 511.33 502.80 2.564 2.671 504.49 972.24 514.10 s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 550.00 2.750 2.750 550.00 1100.0 550.00 450.00 2.250 2.250 450.00 900.00 450.00 d' • M O E-� Analysis Report 09/28/05 07:37:09 AM page 1 Method: CLP1 Sample Name: ICB Operator: PES Run Time: 09/28/05 07:29:28 Co nt: M CONC Corr. Factor: 1 Eleni Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.11718 .0055 .96378 .0028 .0005 .0005 .0412 SDev .29049 .0069 .87461 .0009 .0002 .0002 .0039 %RSD 247.91 124.4 90.747 32.94 45.66 36.78 9.416 #1 .20138 .0128 1.8933 .0039 .0007 .0007 .0456 #2 -.36744 .0046 .84104 .0023 .0004 .0005 .0396 #3 -.18547 -.0008 .15704 .0023 .0003 .0003 .0383 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0005 .0002 .0002 .0006 .0084 .0704 .0051 SDev .0003 .0001 .0004 .0002 .0033 .0166 .0049 %RSD 63.80 57.22 221.1 33.46 39.55 23.62 97.50 #1 .0008 .0004 .0007 .0008 .0120 .0892 .0107 #2 .0004 .0002 -.0001 .0004 .0079 .0641 .0026 #3 .0002 .0001 -.0000 .0006 .0054 .0578 .0019 &rs LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0005 .0050 .0584 .0004 -.00153 -.43064 .44577 SDev .0002 .0021 .0215 .0003 2.50262 1.87454 .68986 %RSD 48.24 41.18 36.74 60.71 163690. 435.29 154.76 #1 .0007 .0073 .0815 .0006 -2.7499 1.3583 1.2147 #2 .0004 .0047 .0546 .0006 2.1458 -2.3804 -.11897 #3 .0003 .0031 .0391 .0001 .59951 -.26981 .24160 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.4804 .56682 -.61181 .0514 .0028 .0005 .0006 SDev 1.5690 2.2431 1.18627 .0143 .0006 .0002 .0002 %RSD 105.99 395.74 193.89 27.77 22.95 40.35 34.72 1.2002 -1.9747 -1.4823 .0660 .0021 .0007 .0009 3.1706 2.2700 .73937 .0509 .0034 .0004 .0006 .07032 1.4051 -1.0925 .0374 .0029 .0003 .0004 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/28/05 07:37:09 AM page 2 High Zn LAE Sb2068 Se1960 T11908 Units ppb Avge 3.1561 SDev 1.8715 %RSD 59.298 #1 4.3917 #2 4.0737 #3 1.0029 Errors LC Pass High 10.000 Low -10.000 • v Zn Pb2203 Sb2068 Se1960 ppm ppm ppb ppb ppb .0003 .0002 -.28771 1.1359 -.21933 .0003 .0002 .50720 .9757 1.44811 101.3 101.4 176.29 85.903 660.25 .0007 .0005 -.00971 1.2051 -1.6462 .0001 .0002 -.87313 2.0751 1.2491 .0001 .0000 .01972 .12736 -.26082 LC Pass LC Pass LC Pass LC Pass LC Pass .0500 .0200 3.0000 60.000 5.0000 -.0500 -.0200 -3.0000 -60.000 -5.0000 Analysis Report Method: CLP1 Sample Name: CRII Run Time: 09/28/05 07:37:15 ppm t: CoWCONC -.0001 .0105 .0013 MoCorr. Factor: 1 .7030 Elem Ag Al As1890 Units ppb ppm ppb Avge 19.311 -.0176 21.060 SDev .255 .0058 .254 %RSD 1.3185 33.00 1.2079 #1 19.479 -.0109 21.333 #2 19.436 -.0207 21.016 #3 19.018 -.0212 20.830 Elem Cd Co Cr Units ppm ppm ppm Avge .0103 .1010 .0200 SDev .0003 .0010 .0005 %RSD 2.615 .9673 2.692 #1 .0106 .1022 .0205 #2 .0103 .1007 .0200 #3 .0101 .1003 .0194 Eleni Mn Mo Na Units ppm ppm ppm Avge.0302 122.4 .0223 .0226 SYe .0004 .0006 .0075 % 1.400 2.748 33.19 #1 .0306 .0230 .0307 #2 .0300 .0218 .0211 #3 .0298 .0220 .0159 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 121.72 12.366 9.5627 SDev 1.94 1.789 1.1068 %RSD 1.5963 14.465 11.574 #1 122.08 13.390 10.840 #2 119.63 10.301 8.9677 #3 123.46 13.408 8.8807 Elem T11908 v Zn Units ppb ppm ppm Avge 21.055 .1010 .0434 SDev .406 .0009 .0006 %RSD 1.9278 .8670 1.339 #1 20.789 .1020 .0440 #2 21.522 .1007 .0431 #3 20.854 .1004 .0430 09/28/05 07:44:55 AM Operator: PES B Ba Be PPM ppm ppm .1833 -.0001 .0105 .0013 .0002 .0002 .7030 134.7 1.516 .1844 .0001 .0107 .1819 -.0002 .0104 .1837 -.0003 .0104 Cu Fe K PPM ppm ppm .0507 -.0001 .0485 .0003 .0022 .0168 .6900 2596. 34.67 .0511 .0024 .0649 .0506 -.0007 .0495 .0504 -.0019 .0313 Ni 2203/1 2203/2 PPM ppb ppb .0806 6.8883 4.9788 .0014 1.8522 .1972 1.782 26.889 3.9616 .0820 9.0100 4.9370 .0805 6.0605 4.8059 .0792 5.5944 5.1936 Si Sn Sr PPM ppm ppm .0529 .0823 -.0001 .0057 .0007 .0001 10.87 .8443 122.4 .0586 .0831 .0000 .0530 .0819 -.0001 .0471 .0819 -.0003 Pb2203 Sb2068 Se1960 ppb ppb ppb 5.6147 121.73 10.496 .5900 1.00 1.143 10.508 .82371 10.886 6.2934 121.83 11.689 5.2237 120.67 9.4115 5.3271 122.67 10.388 page 1 Ca PPM -.0012 .0022 183.8 .0009 -.0010 -.0034 Mg ppm -.0031 .0058 187.4 .0021 -.0021 -.0094 2068/1 ppb 121.73 .91 .74785 121.34 122.77 121.08 Ti PPM .0002 .0002 114.6 .0004 .0002 -.0000 Analysis Report 09/28/05 07:52:41 AM page1 Method: CLP1 Sample Name: ICSAI Operator: PES Run Time: 09/28/05 07:45:01 Coe t: MO CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .39051 501.3 -4.8697 -.0039 .0009 .0002 514.8 SDev .10947 2.8 1.2489 .0008 .0000 .0000 .8 %RSD 28.032 .5563 25.646 19.98 2.225 8.430 .1562 #1 .32440 504.4 -3.8312 -.0032 .0010 .0003 515.3 #2 .33027 500.5 -6.2555 -.0037 .0009 .0002 515.2 #3 .51687 499.0 -4.5225 -.0047 .0009 .0002 513.9 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass LC Pass LC Pass High 10.000 600.0 .2000 .0050 600.0 Low -10.000 400.0 -.2000 -.0050 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0012 .0004 .0031 -.0036 203.4 .0502 512.7 SDev .0001 .0001 .0002 .0004 .7 .0022 .7 %RSD 5.606 33.39 6.781 11.39 .3477 4.437 .1307 #1 .0011 .0004 .0031 -.0031 204.1 .0510 512.6 #2 .0012 .0003 .0029 -.0038 203.4 .0476 513.4 #3 .0011 .0006 .0033 -.0039 202.7 .0518 512.1 Es LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK LC Pass Hig .0050 .0100 240.0 600.0 Low -.0050 -.0100 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0140 -.0027 .0919 .0035 26.392 -15.364 .46829 SDev .0008 .0012 .0016 .0004 2.183 .967 2.6455 %RSD 5.584 43.35 1.756 12.91 8.2730 6.2909 564.92 #1 .0131 -.0013 .0935 .0030 24.052 -14.353 -.48306 #2 .0143 -.0035 .0920 .0035 28.374 -16.279 3.4579 #3 .0146 -.0032 .0903 .0039 26.751 -15.460 -1.5699 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .0150 .0400 Low -.0150 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .11651 -3.4080 .57983 -.0005 .0535 -.3186 .0029 SDev 4.4809 .6454 1.4285 .0015 .0008 .0039 .0000 %RSD 3845.9 18.936 246.36 286.0 1.445 1.222 .9979 #1 5.2456 -2.7948 2.2263 .0011 .0534 -.3231 .0029 #0 -1.8584 -3.3480 -.32969 -.0009 .0527 -.3171 .0029 # -3.0377 -4.0813 -.15710 -.0018 .0543 -.3157 .0029 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 M O L/1 F-+ Analysis Report 09/28/05 07:52:41 AM High Am T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge L-12.424 .0000 -.0094 -1.4592 .23367 -.74811 SDev .903 .0001 .0003 .0911 2.9566 1.12973 %RSD 7.2655 1426. 3.701 6.2444 1265.3 151.01 #1 L-12.552 .0000 -.0098 -1.5644 3.3380 .55426 #2 L-13.256 -.0001 -.0093 -1.4096 -.08808 -1.3348 #3 L-11.464 .0001 -.0092 -1.4037 -2.5489 -1.4638 Errors LC Low LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 6.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -6.0000 -60.000 -5.0000 • page 2 Analysis Report 09/28/05 08:00:27 AM page 1 Method: CLP1 Sample Name: ICSABI Operator: PES Run Time: 09/28/05 07:52:47 Co ent: MCONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 1055.5 496.6 1025.5 .9249 .5268 .5089 509.7 SDev .6 .5 2.9 .0002 .0002 .0012 1.3 %RSD .05731 .1011 .28116 .0225 .0309 .2326 .2600 #1 1056.0 496.8 1028.2 .9250 .5270 .5102 511.0 #2 1054.9 497.1 1022.5 .9246 .5266 .5078 508.4 #3 1055.7 496.1 1025.8 .9250 .5269 .5088 509.6 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1200.0 600.0 1200.0 1.200 .6000 .6000 600.0 Low 800.00 400.0 800.00 .8000 .4000 .4000 400.0 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .9524 .4826 .4963 .5395 201.8 .0305 508.8 SDev .0044 .0009 .0016 .0007 .9 .0028 1.1 %RSD .4578 .1932 .3331 .1225 .4482 9.021 .2096 #1 .9572 .4832 .4981 .5390 202.8 .0281 510.0 #2 .9488 .4816 .4948 .5394 201.1 .0300 507.9 #3 .9512 .4832 .4959 .5403 201.4 .0335 508.6 Ors LC Pass LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1.200 .6000 .6000 .6000 240.0 600.0 Low .8000 .4000 .4000 .4000 160.0 400.0 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .5074 1.000 .0354 .9454 1032.2 971.92 -8.0703 SDev .0007 .003 .0008 .0040 7.4 2.24 1.7639 %RSD .1319 .2677 2.226 .4258 .71713 .23092 21.857 #1 .5074 1.003 .0360 .9498 1038.9 972.75 -9.0252 #2 .5067 .9975 .0356 .9445 1024.3 973.62 -6.0348 #3 .5081 .9997 .0345 .9420 1033.5 969.37 -9.1509 Errors LC Pass NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK High .6000 1.200 Low .4000 .8000 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -8.7333 1015.5 1007.0 .4773 1.048 -.3177 .0023 SDev 1.8698 4.9 8.8 .0022 .004 .0021 .0001 %RSD 21.410 .48287 .87352 .4525 .3751 .6710 4.171 -7.0927 1019.2 1017.1 .4778 1.046 -.3201 .0022 io -10.769 1009.9 1003.0 .4792 1.046 -.3166 .0022 -8.3383 1017.3 1000.9 .4749 1.052 -.3163 .0024 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/28/05 08:00:27 AM High m T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 957.76 .5020 1.074 992.00 -8.5125 1009.8 SDev 2.89 .0006 .002 2.41 .7330 6.9 %RSD .30202 .1191 .1542 .24339 8.6104 .68450 #1 960.13 .5027 1.075 994.78 -7.7362 1017.8 #2 954.54 .5016 1.072 990.49 -9.1926 1005.3 #3 958.62 .5016 1.074 990.72 -8.6089 1006.3 Errors LC Pass LC Pass LC Pass LC Pass NOCHECK LC Pass High 1200.0 .6000 1.200 1200.0 1200.0 Low 800.00 .4000 .8000 800.00 800.00 • r� page 2 Analysis Report 09/28/05 08:08:13 AM page 1 Method: CLP1 Sample Name: CCV1 Run Time: 09/28/05 08:00:33 ppm Co ent: ppm 2.550 2.577 M� CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge 1005.0 52.01 518.38 SDev 3.9 .16 2.59 %RSD .38635 .3034 .50041 #1 1009.4 52.19 521.37 #2 1003.5 51.92 516.99 #3 1002.0 51.91 516.77 Errors LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 Low 900.00 45.00 450.00 Elem Cd Co Cr Units ppm ppm ppm Avge 2.527 2.569 2.545 SDev .016 .004 .008 %RSD .6406 .1590 .3104 #1 2.545 2.574 2.554 #2 2.520 2.567 2.542 #3 2.515 2.567 2.539 Ears LC Pass LC Pass LC Pass High 2.750 2.750 2.750 Low 2.250 2.250 2.250 Elem Mn Mo Na Units ppm ppm ppm Avge 2.553 2.606 84.37 SDev .006 .012 .07 %RSD .2365 .4620 .0849 #1 2.560 2.620 84.32 #2 2.550 2.599 84.34 #3 2.549 2.598 84.45 Errors LC Pass NOCHECK LC Pass High 2.750 ppm 88.00 Low 2.250 2.585 72.00 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 973.34 523.47 520.45 SDev .61 .54 1.85 %RSD .06317 .10349 .35481 # 972.95 523.91 521.88 973.02 523.62 521.12 # 974.05 522.86 518.37 Errors NOCHECK NOCHECK NOCHECK Operator: PES B Ba Be Ca ppm ppm ppm ppm 2.550 2.577 2.575 52.67 .003 .007 .006 .13 .1217 .2694 .2322 .2489 2.553 2.585 2.582 52.82 2.547 2.574 2.573 52.61 2.549 2.572 2.571 52.58 LC Pass LC Pass LC Pass LC Pass 2.750 2.750 2.750 55.00 2.250 2.250 2.250 45.00 Cu Fe K Mg . ppm ppm ppm ppm 2.609 51.54 85.65 53.66 .003 .23 .06 .12 .1094 .4426 .0742 .2302 2.613 51.80 85.63 53.80 2.607 51.44 85.59 53.60 2.609 51.38 85.72 53.58 LC Pass LC Pass LC Pass LC Pass 2.750 55.00 88.00 55.00 2.250 45.00 72.00 45.00 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb 2.529 519.07 504.16 993.06 .015 3.19 1.65 1.92 .5823 .61404 .32812 .19365 2.545 517.78 505.98 992.72 2.523 516.72 502.75 995.13 2.517 522.70 503.76 991.33 LC Pass NOCHECK NOCHECK NOCHECK 2.750 2.250 Si Sn Sr Ti ppm ppm ppm ppm 2.475 2.580 2.566 2.585 .039 .004 .002 .023 1.588 .1583 .0953 .8833 2.435 2.575 2.568 2.611 2.478 2.581 2.565 2.568 2.514 2.583 2.563 2.576 NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/28/05 08:08:13 AM High L E 16 Units Avge SDev %RSD #1 #2 #3 Error High Low • r] page 2 T11908 v Zn Pb2203 Sb2068 Se1960 ppb ppm ppm ppb ppb ppb 502.08 2.576 2.681 509.13 979.91 521.46 3.40 .004 .004 1.50 .43 1.41 .67641 .1452 .1344 .29378 .04437 .27074 506.00 2.581 2.685 509.91 979.53 522.55 499.97 2.574 2.678 507.40 980.38 521.95 500.27 2.574 2.679 510.07 979.80 519.86 s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 550.00 2.750 2.750 550.00 1100.0 550.00 450.00 2.250 2.250 450.00 900.00 450.00 r] page 2 Analysis Report 09/28/05 08:16:00 AM page 1 Method: CLP1 Sample Name: CCB1 Operator: PES Run Time: 09/28/05 08:08:19 Co ent: M CONC Corr. Factor: I Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.11494 .0153 .41411 .0033 .0004 .0004 .0547 SDev .36789 .0144 .73041 .0009 .0002 .0002 .0145 %RSD 320.06 94.27 176.38 28.73 48.22 54.68 26.57 #1 -.29386 .0311 -.36781 .0043 .0006 .0006 .0703 #2 -.35915 .0122 1.0788 .0029 .0003 .0004 .0523 #3 .30818 .0027 .53132 .0025 .0002 .0002 .0415 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0004 .0005 .0002 .0005 .0126 .0655 .0184 SDev .0003 .0001 .0002 .0001 .0074 .0110 .0134 %RSD 61.84 20.89 69.29 14.57 59.24 16.78 72.44 #1 .0007 .0006 .0003 .0005 .0204 .0782 .0335 #2 .0003 .0005 .0004 .0005 .0117 .0587 .0139 #3 .0002 .0004 .0001 .0006 .0056 .0597 .0079 Aa rs LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0004 .0051 .0555 .0001 -.15307 -.34573 .71967 SDev .0002 .0018 .0222 .0003 .73974 .69694 .98044 %RSD 51.58 35.25 39.99 315.2 483.26 201.58 136.23 #1 .0006 .0070 .0793 .0001 .50709 -.39366 1.1546 #2 .0003 .0047 .0521 .0004 -.01373 -1.0175 -.40300 #3 .0002 .0035 .0353 -.0002 -.95258 .37393 1.4074 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge -.48997 1.6624 -.20768 .0308 .0017 .0004 .0005 SDev 1.41310 .9392 2.30477 .0094 .0003 .0002 .0001 %RSD 288.41 56.500 1109.8 30.55 15.72 49.62 29.84 .52042 .65623 2.0362 .0407 .0016 .0006 .0006 .11443 1.8148 -2.5689 .0299 .0015 .0003 .0004 # -2.1048 2.5161 -.09028 .0219 .0020 .0002 .0004 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Analysis Report 09/28/05 08:16:00 AM High L m T11908 908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 2.7703 .0006 .0003 -.28154 -.08715 .41505 SDev .7864 .0001 .0003 .34808 .83380 1.3791 %RSD 28.387 21.29 86.89 123.64 956.71 332.28 #1 2.5356 .0005 .0006 -.09367 .73161 1.5766 #2 3.6474 .0007 .0002 -.68319 -.05786 -1.1091 #3 2.1280 .0006 .0001 -.06776 -.93521 .77763 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • • page 2 Analysis Report 09/28/05 08:23:47 AM page 1 Method: CLP1 Sample Name: MB -14825 Run Time: 09/28/05 08:16:06 Co ent: MCONC Corr. Factor: 1 fey% Operator: PES Elem Ag Al As1890 B Ba Units ppb ppm ppb ppm ppm Avge -.47748 -.0181 -.32913 -.0036 -.0003 SDev .08123 .0017 .83371 .0002 .0000 %RSD 17.012 9.147 253.31 5.660 9.037 #1 -.54048 -.0168 -.17529 -.0034 -.0002 #2 -.38580 -.0175 -1.2290 -.0038 -.0002 #3 -.50614 -.0200 .41696 -.0037 -.0003 Errors LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.0.00 .2000 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 Elem Cd Co Cr Cu Fe . Units ppm ppm ppm ppm ppm Avge -.0000 -.0001 -.0001 .0005 .0028 SDev .0001 .0001 .0003 .0001 .0005 %RSD 1237. 198.1 282.9 14.84 17.67 #1 .0000 .0000 -.0004 .0006 .0033 #2 .0000 -.0000 .0002 .0005 .0026 #3 -.0001 -.0002 -.0002 .0005 .0024 Drs LC Pass LC Pass LC Pass LC Pass LC Pass High .0050 .0500 .0100 .0250 .1000 Low -.0050 -.0500 -.0100 -.0250 -.1000 Elem Mn Mo Na Ni 2203/1 Units ppm ppm ppm ppm ppb Avge .0000 .0022 .0142 -.0003 1.3049 SDev .0001 .0004 .0025 .0001 .3062 %RSD 657.4 18.74 17.66 45.15 23.469 #1 -.0000 .0025 .0170 -.0003 1.5829 #2 .0001 .0017 .0133 -.0002 1.3552 #3 -.0000 .0022 .0122 -.0004 .97666 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Units ppb ppb ppb ppm ppm Avge .34639 -.16217 -.12085 -.0154 .0021 SDev .84758 1.43417 1.49291 .0033 .0002 %RSD 244.69 884.35 1235.4 21.57 8.589 ## -.21715 -1.7217 -1.8406 -.0125 .0023 -.06482 1.1001 .63603 -.0146 .0021 # 1.3211 .13504 .84202 -.0191 .0019 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Be Ca ppm ppm .0001 -.0144 .0000 .0003 60.23 1.739 .0001 -.0146 .0001 -.0141 .0000 -.0143 LC Pass .0050 -.0050 K ppm .0362 .0032 8.702 .0352 .0397 .0336 LC Pass 5.000 -5.000 2203/2 ppb -.40733 .86182 211.58 -1.3929 .20462 -.03368 NOCHECK Sr ppm -.0003 .0000 5.165 -.0003 -.0003 -.0003 NOCHECK LC Pass .2000 -.2000 Mg ppm .0012 .0008 65.76 .0021 .0008 .0007 LC Pass .2000 -.2000 2068/1 ppb .55001 .79688 144.88 1.2078 -.33610 .77830 NOCHECK Ti ppm .0005 .0001 21.47 .0005 .0006 .0004 NOCHECK Analysis Report 09/28/05 08:23:47 AM High Low E4 T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .21417 .0002 .0018 .16289 .41421 -.13461 SDev 2.0312 .0001 .0001 .50947 .66185 1.44606 %RSD 948.41 49.10 2.695 312.77 159.79 1074.3 #1 -.18585 .0001 .0018 -.40192 .25737 -1.8010 #2 2.4157 .0001 .0018 .58779 -.15514 .79057 #3 -1.5873 .0003 .0017 .30280 1.1404 .60660 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • r �J page 2 Analysis Report Method: CLP1 Sample Name: LCS-14825 Run Time: 09/28/05 08:23:53 Co ent• 09/28/05 08:31:33 AM M�WCONC Corr. Factor: 1 14)w Elem Ag Al As1890 B Units ppb ppm ppb ppm Avge 1083.0 55.88 556.65 2.994 SDev 6.0 .50 2.12 .008 %RSD .55417 .8944 .38150 .2522 #1 1089.9 56.46 557.89 H3.002 #2 1080.0 55.63 554.20 2.986 #3 1079.0 55.56 557.87 2.994 Errors LC Pass High 1200.0 Low 800.00 Elem Cd Units ppm Avge 2.707 SDev .013 %RSD .4618 #1 2.722 #2 2.699 #3 2.702 Errors NOCHECK LC Pass LC Pass Elas LC Pass High 3.000 Low 2.000 Elem Mn Units ppm Avge 2.750 SDev .010 %RSD .3651 #1 2.762 #2 2.743 #3 2.746 Errors LC Pass High 3.000 Low 2.000 Elem 2068/2 Units ppb Avge 1059.8 SDev 2.7 %RSD .25526 #1 1061.8 #.* 1056.7 if 1061.0 Errors NOCHECK LC Pass LC Pass LC Pass 60.00 600.00 3.000 40.00 400.00 2.000 Co Cr Cu ppm ppm ppm 2.765 2.741 2.852 .005 .011 .015 .1649 .3937 .5177 2.770 2.754 2.762 2.734 2.763 2.736 LC Pass LC Pass 3.000 3.000 2.000 2.000 Mo ppm 2.815 .011 .3939 2.828 2.809 2.808 NOCHECK 1960/1 ppb 548.51 1.02 .18673 549.66 547.70 548.17 NOCHECK Na ppm 90.73 .62 .6840 91.45 90.41 90.34 LC Pass 96.00 64.00 1960/2 ppb 546.92 3.17 .57967 550.51 544.52 545.73 NOCHECK 2.869 2.844 2.843 LC Pass 3.000 2.000 Ni ppm 2.709 .018 .6486 2.729 2.698 2.700 LC Pass 3.000 2.000 Si ppm 3.630 .053 1.447 3.575 3.636 3.679 NOCHECK Operator: PES Ba Be ppm ppm 2.781 2.863 .017 .009 .6115 .3187 2.801 2.874 2.771 2.856 2.772 2.861 LC Pass 3.000 2.000 Fe ppm 55.89 .30 .5441 56.24 55.69 55.75 LC Pass 60.00 40.00 2203/1 ppb 559.36 .75 .13378 560.23 558.98 558.88 NOCHECK Sn ppm 2.783 .002 .0747 2.781 2.785 2.783 NOCHECK LC Pass 3.000 2.000 K ppm 83.66 .79 .9437 84.56 83.29 83.11 LC Pass 96.00 64.00 2203/2 ppb 542.05 .87 .16109 541.11 542.19 542.84 NOCHECK Sr ppm 2.764 .014 .5235 2.780 2.754 2.757 NOCHECK page 1 Ca ppm 56.37 .19 .3357 56.59 56.23 56.30 LC Pass 60.00 40.00 Mg ppm 57.26 .15 .2587 57.43 57.16 57.19 LC Pass 60.00 40.00 2068/1 ppb 1078.7 2.8 .25990 1081.4 1075.8 1078.8 NOCHECK Ti ppm 2.792 .044 1.570 2.841 2.775 2.758 NOCHECK Analysis Report 09/28/05 08:31:33 AM High Low T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 540.30 2.777 2.859 547.81 1066.1 547.45 SDev 2.90 .011 .007 .35 2.7 2.46 %RSD .53585 .4119 .2610 .06466 .25364 .44852 #1 543.55 2.790 2.868 547.48 1068.3 550.23 #2 537.97 2.769 2.854 547.78 1063.1 545.58 #3 539.39 2.772 2.856 548.18 1066.9 546.54 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 600.00 3.000 3.000 600.00 1200.0 600.00 Low 400.00 2.000 2.000 400.00 800.00 400.00 • • page 2 Analysis Report 09/28/05 08:39:20 AM page 1 Method: CLP1 Sample Name: 0509510-002E Operator: PES Run Time: 09/28/05 08:31:39 Comment: M* CONC Corr. Factor: 1 y1n �-•� '�a Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.03678 .0636 .83147 .0206 .0006 .0005 22.47 SDev .07156 .0032 2.2937 .0009 .0001 .0001 .05 %RSD 194.56 5.029 275.86 4.274 8.880 11.64 .2445 #1 .02356 .0657 -.51070 .0214 .0006 .0005 22.46 #2 -.01806 .0653 3.4799 .0207 .0007 .0005 22.52 #3 -.11584 .0600 -.47478 .0196 .0006 .0004 22.41 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0002 .0041 .0017 .0459 1.533 4.699 SDev .0001 .0002 .0002 .0002 .0015 .015 .019 %RSD 18.48 86.99 4.278 11.79 3.269 .9753 .4055 #1 .0006 .0000 .0039 .0015 .0457 1.550 4.698 #2 .0007 .0003 .0043 .0019 .0475 1.529 4.718 #3 .0005 .0005 .0042 .0017 .0446 1.520 4.680 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0079 .0043 16.93 .0156 .61940 -.90011 1.5068 .0001 .0011 .08 .0005 .77721 .75537 1.0229 1.339 25.69 .4434 2.934 125.48 83.920 67.886 #1 .0079 .0054 17.01 .0161 .86977 -1.4373 1.4115 #2 .0080 .0042 16.89 .0156 1.2406 -1.2267 2.5740 #3 .0079 .0032 16.88 .0152 -.25213 -.03639 .53487 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 1.0425 2.7924 -.30410 3.489 .0020 .0326 .0015 SDev 1.0405 1.8758 .95744 .027 .0013 .0002 .0001 %RSD 99.807 67.177 314.84 .7688 64.61 .4926 6.783 #1 -.14946 4.5376 -.55019 3.513 .0015 .0324 .0015 #2 1.5079 .80876 .75236 3.493 .0034 .0327 .0015 #3 1.7691 3.0307 -1.1145 3.460 .0010 .0325 .0014 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.9376 .0011 .1378 -.39407 1.1971 .72703 SDev 1.3586 .0002 .0006 .28055 .7592 .44075 %RSD 70.118 17.78 .3975 71.193 63.419 60.624 #1 2.9263 .0013 .1377 -.66898 .37034 1.1441 #2 2.4980 .0012 .1385 -.40504 1.8629 .77114 #3 .38842 .0009 .1374 -.10820 1.3581 .26588 Analysis Report 09/28/05 08:47:06 AM page 1 Method: CLP1 Sample Name: 0509510-002EDUP Operator: PES Run Time: 09/28/05 08:39:26 Co ent: M* CONC Corr. Factor: 1 I `w - 15 fly Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.27002 .0598 1.3260 .0179 .0003 .0001 21.67 SDev .41977 .0033 .7790 .0006 .0001 .0000 .12 %RSD 155.46 5.457 58.748 3.124 30.29 53.09 .5726 #1 .21296 .0636 1.0302 .0186 .0004 .0000 21.78 #2 -.54691 .0575 2.2096 .0176 .0004 .0001 21.70 #3 -.47611 .0585 .73829 .0176 .0002 .0001 21.54 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0001 -.0001 .0030 .0009 .0405 1.482 4.524 SDev .0001 .0005 .0002 .0005 .0005 .013 .029 %RSD 44.57 343.3 6.810 59.71 1.224 .9013 .6450 #1 .0001 -.0001 .0031 .0010 .0405 1.497 4.551 #2 .0002 .0003 .0032 .0013 .0411 1.473 4.527 #3 .0001 -.0006 .0028 .0003 .0401 1.475 4.493 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0078 .0014 16.11 .0157 -.93171 .48344 .57554 .0002 .0003 .13 .0002 1.01340 1.0252 1.1758 2.656 20.57 .8048 1.266 108.77 212.06 204.30 #1 .0079 .0015 16.20 .0157 -1.4376 .98165 1.5118 #2 .0080 .0017 15.96 .0160 .23504 -.69564 -.74414 #3 .0076 .0011 16.16 .0156 -1.5925 1.1643 .95897 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .11037 2.6821 -.08474 3.325 .0004 .0310 .0014 SDev 1.7313 2.0189 1.19749 .028 .0005 .0006 .0002 %RSD 1568.6 75.275 1413.1 .8519 125.0 1.925 17.13 #1 -1.8569 .41966 .19032 3.358 -.0002 .0308 .0013 #2 1.4016 4.3003 .95128 3.312 .0007 .0305 .0017 #3 .78641 3.3264 -1.3958 3.306 .0006 .0317 .0012 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .32268 .0006 .1392 .01224 .26528 .83663 SDev .42425 .0001 .0008 .34640 .86993 1.0661 %RSD 131.48 9.012 .5664 2830.9 327.93 127.43 #1 -.04362 .0006 .1396 .17606 -.73514 .26669 #2 .22413 .0006 .1397 -.38568 .68708 2.0665 60 .78754 .0005 .1382 .24633 .84389 .17667 M O Cn N Analysis Report 09/28/05 08:54:53 AM page 1 Method: CLP1 Sample Name: 0509510-002EMS Operator: PES Run Time: 09/28/05 08:47:12 Cot: MoWCONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge 49.406 2.106 41.042 .0164 2.047 .0525 20.91 SDev .258 .010 .666 .0005 .006 .0002 .05 %RSD .52263 .4701 1.6228 2.909 .2889 .3098 .2487 #1 49.631 2.111 41.793 .0159 2.053 .0525 20.92 #2 49.124 2.113 40.523 .0169 2.041 .0523 20.86 #3 49.463 2.095 40.809 .0164 2.048 .0526 20.96 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0500 .5095 .2038 .2625 .9926 1.443 4.358 SDev .0002 .0013 .0005 .0005 .0027 .008 .013 %RSD .4587 .2529 .2346 .1857 .2671 .5331 .3058 #1 .0499 .5095 .2038 .2630 .9934 1.441 4.367 #2 .0498 .5083 .2033 .2622 .9896 1.452 4.342 #3 .0502 .5108 .2043 .2621 .9947 1.437 4.364 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Av e .5136 .0010 15.61 .5171 20.526 19.150 505.30 S .0015 .0004 .09 .0015 2.085 1.236 .98 % .2837 39.04 .5750 .2843 10.160 6.4535 .19390 #1 .5140 .0012 15.64 .5188 19.150 20.287 505.74 #2 .5120 .0013 15.68 .5161 22.925 17.835 504.17 #3 .5149 .0006 15.51 .5165 19.501 19.326 505.97 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 505.23 11.282 10.199 3.227 .0010 .0299 .0011 SDev 3.25 1.886 .479 .011 .0003 .0003 .0000 %RSD .64344 16.714 4.6931 .3482 29.16 1.153 2.975 #1 503.63 10.977 9.7449 3.239 .0009 .0303 .0010 #2 503.09 9.5673 10.699 3.223 .0008 .0297 .0011 #3 508.97 13.301 10.154 3.218 .0013 .0298 .0011 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 49.470 .5087 .6698 19.608 505.25 10.560 SDev .600 .0014 .0022 .271 2.40 .562 %RSD 1.2126 .2737 .3304 1.3798 .47442 5.3254 #1 48.895 .5088 .6709 19.909 504.33 10.155 #249.423 .5072 .6673 19.530 503.45 10.322 #0 50.092 .5100 .6713 19.385 507.97 11.202 Analysis Report 09/28/05 09:02:39 AM Method: CLP1 Sample Name: 0509510-002ESD Operator: PES Run Time: 09/28/05 08:54:59 Cot: MO CONC Corr. Factor: 1 �W- IS SD Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.17139 .0092 .15541 .0044 .0007 -.0000 SDev .35995 .0041 .28157 .0002 .0003 .0000 %RSD 210.02 44.65 181.18 4.062 46.13 224.8 #1 -.56951 .0139 -.00740 .0046 .0011 .0000 #2 .13106 .0067 .48053 .0044 .0006 .0000 #3 -.07572 .0069 -.00691 .0043 .0005 -.0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 -.0000 .0005 .0008 .0083 .3112 SDev .0001 .0001 .0004 .0001 .0007 .0081 %RSD 294.8 3292. 65.20 20.40 8.064 2.596 #1 .0002 .0000 .0009 .0009 .0090 .3205 #2 .0000 -.0001 .0003 .0006 .0082 .3073 #3 -.0001 .0001 .0004 .0007 .0077 .3058 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb Avge .0017 .0006 3.097 .0028 -.43870 -.34184 SM .0002 .0003 :035 .0005 2.73472 1.76279 11.32 45.03 1.128 17.01 623.37 515.68 #1 .0020 .0008 3.137 .0034 -2.1379 1.5913 #2 .0016 .0003 3.082 .0025 -1.8941 -.75642 #3 .0016 .0006 3.072 .0026 2.7159 -1.8604 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge 2.0248 1.4401 -1.1578 .6647 -.0008 .0059 SDev 1.7376 1.9593 1.4819 .0117 .0008 .0001 %RSD 85.818 136.06 127.99 1.753 97.52 1.714 #1 .13038 .62656 -.09398 .6779 -.0001 .0060 #2 2.3994 3.6751 -2.8504 .6559 -.0007 .0059 #3 3.5445 .01856 -.52902 .6603 -.0016 .0058 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge .38025 .0006 .0260 -.37407 1.7140 -.29271 SDev .51670 .0002 .0003 .74308 1.3668 .41433 %RSD 135.88 32.72 1.337 198.65 79.743 141.55 #1 .01933 .0005 .0264 .34948 .13584 .14596 #2 .97215 .0005 .0258 -1.1352 2.5164 -.67741 #3 • .14928 .0008 .0259 -.33645 2.4897 -.34668 page 1 Ca PPM 4.525 .049 1.094 4.581 4.486 4.508 Mg PPM .9165 .0127 1.387 .9310 .9070 .9116 2068/1 ppb 1.0916 1.4416 132.07 .14679 2.7509 .37705 Ti PPM .0004 .0001 30.97 .0005 .0003 .0004 Analysis Report 09/28/05 09:10:26 AM Method: CLP1 Sample Name: 0509510-001E Run Time: 09/28/05 09:02:45 Operator: PES Comment: I"1 : CONC Corr . Factor: 1 Kw - Ib em Units Ag ppb Al As1890 B Ba Be Avge -.07465 Ppm .0516 Ppb 1.1982 ppm .0224 ppm ppm SDev %RSD .25360 339.71 .0015 .8473 .0002 .0010 .0001 -.0000 .0000 2.870 70.709 .8823 7.142 37.04 #1 #2 -.09380 .0528 .38742 .0223 .0011 -.0000 #3 -.31814 .0521 1.1295 .0223 .0010 -.0000 .18798 .0500 2.0777 .0226 .0009 -.0000 Elem Cd Co Cr Cu Fe K Units Avge ppm .0001 ppm ppm ppm ppm p13.15 SDev .0001 .0002 .0001 .0046 .0002 .0014 .0327 %RSD 109.5 64.07 3.424 .0002 11.34 .0002 .5892 ,02 .1326 #1 #2 -.0000 .0003 .0045 .0013 .0325 13.14 #3 .0002 .0001 .0046 .0014 .0328 13.17 .0001 .0001 .0048 .0016 .0329 13.15 Elem Units Mn Mo Na Ni 2203/1 2203/2 Avge ppm .0072 Ppm .0010 Ppm 18.43 Ppm .0088 Ppb -.03228 Ppb -.73359 SDev .0001 .0002 .07 .0004 1.60675 .7961 21.77 .3607 4.820 4977.1 .57274 78.073 #1 #2 .0071 .0008 18.35 .0093 -.59014 -.55638 #3 .0072 .0012 18.47 .0085 1.7790 -1.3740 .0072 .0011 18.47 .0088 -1.2857 -,27040 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units Avge ppb .43779 Ppb 3.8621 Ppb 1.5953 ppm 3.371 Ppm ppm SDev .90059 1.8174 2.1664 .012 .0005 .0008 .0348 %RSD 205.71 47.057 135.80 .3680 162.3 .0004 1.076 #1 #2 1.4744 4.9675 -.89030 3.361 .0014 .0344 #3 -.00927 4.8543 2.5941 3.369 .0003 .0348 -.15180 1.7646 3.0821 3.385 -.0002 .0351 , Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb Ppb Avge .48716 .0011 .1195 -.49997 1.0729 2.3502 SDev 1.5278 .0001 .0008 .15381 .6996 1.1711 %RSD 313.61 7.826 .6727 30.763 65.207 49.829 #1 -1.2638 .0010 .1187 -.56754 1.8218 1.0604 #2 1.5488 .0011 .1195 -.32395 .43609 3.3468 #3 1.1765 .0012 .1203 -.60843 .96083 2.6434 • page 1 Ca ppm 26.22 .13 .4797 26.10 26.21 26.35 Mg ppm 5.478 .028 .5071 5.454 5.472 5.509 2068/1 ppb 2.3450 .9426 40.195 2.5174 1.3281 3.1894 Ti ppm .0006 .0001 14.32 0006 0005 0007 Analysis Report 09/28/05 09:18:12 AM Method: CLP1 Sample Name: 0509510-003E Run Time: 09/28/05 09.10 .32 Operator: PES Comment: a M: CONC Corr. Factor: 1 M� EfeE em Units Ag ppb Al As1890 B Ba Be Avge -.13397 •0578 pm .44397 .0216 .pm 0168 ppm SDev %RSD .01588 11.855 .0027 .96309 .0006 .0001 -.0000 .0000 4.604 216.93 2.856 .3074 429.2 #1 #2 -.13914 -.14663 .0603 .46659 .0209 .0168 .0000 #3 -.11615 .0581 1.3955 .0221 .0168 -.0000 .0550 -.53023 .0218 .0167 -.0000 Elem Units Cd Co Cr Cu Fe R Avge ppm .0001 ppm .0001.0022 ppm ppm ppm 1.531 SDev %RSD .0001 93.28 .0002 .0002 .0120 .0001 .0212 .0005 .008 244.9 10.06 1.139 2.465 .5385 #1 #2 .0001 .0001 .0023 .0119 .0213 1.524 #3 .0000 .0002 -.0001 .0020 .0120 .0217 1.540 .0002 .0024 .0122 .0206 1.528 Elem Units Mn Mo Na Ni 2203/1 2203/2 Avge ppm .0154 PPM .0007 ppm 16.52 PPM Ppb Ppb SDPv .0001 .0001 .18 .0020 .0007 .20155 .05151 -.83912 1.43340 .3133 10.73 1.069 34.44 25.559 170.82 #1 #2 .0154 .0008 16.38 .0025 .20903 -1.8686 #3 .0154 .0155 .0006 16.72 16.46 .0012 .14670 .79801 .0007 .0024 .24891 -1.4467 Elem 2068/2 1960/1 1960/2 Si Sn Sr Avges .38845 3.1609 .25000 3.393 .0002 .0403 SDev 2.0699 .6789 .69696 .025 .0003 %RSD 532.85 21.477 278.79 .7232 153.0 .0003 .7605 #1 #2 .93525 3.3054 .98919 3.377 -.0001 .0400 #3 2.1300 2.4214 -.39519 3.421 .0001 .0405 -1.8999 3.7559 .15599 3.380 .0006 .0405 Elem Units T11908 ppb v Zn Pb2203 Sb2068 Se1960 kvge 1.6217 ppm .0013 Ppm .0356 Ppb -.49254 Ppb .69004 Ppb 1.2193 SDev kRSD .6508 .0001 .0003 .94145 1.3956 .6200 40.131 10.11 .6966 191.14 202.25 50.851 #1 #2 1.2400 .0012 .0354 -1.1767 1.1481 1.7605 #3 2.3732 .0014 .0359 .58116 1.7991 .54277 1.2520 .0011 .0355 -.88205 -.87703 1.3548 • page 1 Ca ppm 23.78 .13 .5271 23.67 23.91 23.76 Mg ppm 4.668 .025 .5398 4.647 4.696 4.661 2068/1 ppb 1.2941 .2433 18.801 1.5743 1.1363 1.1717 Ti ppm _ .0008 .0001 6.406 .0009 .0008 .0009 Analysis Report 09/28/05 09:25:59 AM Method: CLP1 Sample Name: 0509510-004E Operator: PES Run Time: 09/28/05 09:18:19 CO ent: M CONC Corr. Factor: 1 3s Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.27674 .0302 .13611 .0156 .0099 -.0000 SDev .36472 .0020 .85357 .0001 .0000 %RSD 131.79 6.638 627.10 .5760 .3150 .0000 43.97 #1 .01285 .0324 -.77310 .0157 .0099 -.0000 #2 -.68634 .0293 .92025 .0155 .0098 -.0000 #3 -.15673 .0287 .26119 .0157 .0099 -.0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0000 -.0001 .0033 .0071 .0242 1.325 SDev .0002 .0002 .0001 .0002 .0001 .004 %RSD 19020. 167.0 3.409 2.223 .2402 .3089 #1 -.0002 -.0003 .0033 .0073 .0242 1.329 #2 .0002 -.0002 .0032 .0070 .0242 1.323 #3 -.0000 .0001 .0034 .0070 .0243 1.321 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb Avge .0147 .0009 14.96 .0020 -.70770 -.82190 .0000 .0000 .05 .0005 1.21652 .90953 .1788 3.291 .3575 27.71 171.90 110.66 #1 .0147 .0010 14.93 .0025 -2.1113 .22696 #2 .0147 .0009 15.02 .0019 -.05446 -1.3929 #3 .0147 .0010 14.93 .0015 .04267 -1.2998 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge 1.0328 2.7546 .99316 3.133 .0007 .0372 SDev .7373 1.7418 2.0508 .001 .0009 .0001 %RSD 71.388 63.230 206.49 .0273 117.8 .4058 #1 1.8175 1.1466 3.3017 3.133 .0006 .0371 #2 .35443 2.5126 -.61802 3.132 .0017 .0372 #3 .92654 4.6048 .29585 3.133 -.0001 .0374 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -.23153 .0009 .0410 -.78383 .93662 1.5797 SDev 1.88122 .0001 .0001 .20655 .82132 1.0877 $RSD 812.53 13.00 .1579 26.351 87.690 68.851 #1 -2.1488 .0011 .0410 -.55164 1.8278 2.5840 #2 -.15724 .0008 .0409 -.94714 .77204 .42447 #6 1.6115 .0009 .0410 -.85271 .21005 1.7307 page 1 Ca ppm 22.14 .03 .1411 22.12 22.11 22.17 Mg PPM 4.298 .002 .0549 4.295 4.298 4.300 2068/1 ppb .74385 1.7094 229.81 1.8482 1.6085 -1.2251 Ti PPM .0006 .0001 12.84 .0007 .0006 .0006 Analysis Report 09/28/05 09:33:46 AM Method: CLP1 Sample Name: 0509510-005E Operator: PES Run Time: 09/28/05 09:26:05 Comment: Mole M W M y CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge -.25565 .0605 .49276 .0216 .0055 -.0000 SDev .23296 .0016 .92113 .0003 .0001 .0000 %RSD 91.124 2.662 186.93 1.569 1.082 25.08 #1 -.11565 .0622 -.47263 .0218 .0055 -.0000 #2 -.52457 .0603 1.3621 .0212 .0055 -.0000 #3 -.12673 .0590 .58881 .0217 .0056 -.0000 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm ppm ppm Avge .0001 -.0001 .0015 .0055 .0161 1.767 SDev .0002 .0002 .0004 .0004 .0002 .014 $RSD 183.4 308.4 25.56 7.306 1.124 .7814 #1 -.0001 -.0001 .0011 .0051 .0162 1.767 #2 .0001 -.0003 .0015 .0058 .0159 1.781 #3 .0003 .0002 .0018 .0058 .0162 1.753 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm ppm ppm ppm ppb ppb Avge .0148 .0004 16.82 .0029 -.17258 -.93302 .0002 .0002 .23 .0003 2.52789 •1.59432 1.230 51.92 1.342 9.109 1464.8 170.88 #1 .0146 .0005 16.88 .0031 -2.2544 .67674 #2 .0147 .0006 17.00 .0026 -.90366 -.96435 #3 .0150 .0002 16.56 .0028 2.6403 -2.5114 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb ppm ppm ppm Avge .94903 .31738 1.1160 3.430 .0005 .0431 SDev 1.9109 1.2794 1.4445 .019 .0006 .0008 RSD 201.35 403.12 129.44 .5662 129.6 1.749 #1 1.0394 -1.0388 2.6325 3.441 -.0001 .0440 #2 -1.0054 .48803 -.24382 3.441 .0005 .0429 #3 2.8132 1.5029 .95927 3.407 .0012 .0425 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.0001 .0014 .0453 -.67971 .88900 .85004 SDev .7316 .0001 .0001 .33774 1.3829 .74850 %RSD 73.151 10.11 .1933 49.688 155.56 88.054 #1 1.8446 .0015 .0453 -.29924 2.0289 1.4099 #2 .56042 .0012 .0452 -.94406 -.64946 -.00011 #3 .59523 .0015 .0454 -.79584 1.2875 1.1403 page 1 Ca ppm 24.10 .03 .1044 24.13 24.09 24.08 Mg ppm 4.702 .009 .1836 4.710 4.704 4.693 2068/1 ppb .76872 2.9535 384.21 4.0110 .06360 -1.7684 Ti ppm .0009 .0003 28.01 .0007 .0008 .0012 Analysis Report 09/28/05 09:41:33 AM 1 page Method: CLP1 Sample Name: CCV2 Operator: PES Run Time: 09/28/05 09:33:52 Comment: Mole CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units Avge ppb 1000.1 ppm 51.97 Ppb 523.66 Ppm 2.558 ppm 2.552 Ppm 2.580 ppm SDev 1.2 .07 .66 .007 .001 52.91 %RSD .11798 .1324 .12688 .2895 .0198 .007 .2786 .16 .2987 #1 #2 999.48 52.02 523.75 2.549 2.552 2.571 52.73 #3 1001.5 51.99 522.95 2.561 2.552 2.583 52.97 999.34 51.89 524.27 2.563 2.551 2.585 53.02 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 Low 900.00 45.00 450.00 2.250 2.250 2.250 45.00 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm 2.538 ppm 2.574 ppm 2.547 ppm 2.592 ppm 51.82 ppm 84.72 ppm SDev .005 .011 .006 .002 .04 53.82 %RSD .1873 .4110 .2498 .0767 .0808 .20 .2361 .17 .3214 #1 2.532 2.562 2.540 2.591 51.78 84.83 53.62 #2 2.539 2.578 2.550 2.594 51.86 84.85 53.91 #3 2.542 2.582 2.552 2.591 51.82 84.49 53.93 E s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Hi 2.750 2.750 2.750 2.750 55.00 88.00 55.00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 2.551 2.609 84.39 2.526 520.19 504.68 988.78 SDev .006 .008 .18 .003 3.29 2.62 5.01 %RSD .2327 .3201 .2094 .1352 .63269 .51951 .50648 #1 2.544 2.600 84.52 2.522 516.45 501.99 984.38 #2 2.553 2.613 84.46 2.526 521.49 507.23 987.74 #3 2.555 2.615 84.19 2.529 522.63 504.82 994.23 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti 7nits ppb ppb ppb ppm ppm ppm ppm kvge 978.11 529.99 524.35 2.436 2.580 2.542 2.614 SDev 3.18 1.68 2.14 .047 .016 .002 .014 kRSD .32520 .31765 .40757 1.935 .6208 .0819 .5286 #1 974.68 529.23 526.79 2.389 2.562 2.540 2.630 # 978.70 528.81 522.81 2.436 2.588 2.544 2.606 # 980.97 531.91 523.45 2.483 2.591 2.543 2.606 srrors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK 00 r` M O C/1 H Analysis Report 09/28/05 09:41:33 AM page 2 High Low aT11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 499.60 2.570 2.686 509.84 981.67 526.23 SDev 4.39 .005 .008 2.70 3.74 1.40 %RSD .87968 .2061 .2991 .53006 .38053 .26579 #1 495.19 2.563 2.676 506.81 977.91 527.61 #2 499.64 2.572 2.690 511.98 981.71 524.81 #3 503.98 2.573 2.690 510.75 985.38 526.27 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 550.00 2.750 2.750 550.00 1100.0 550.00 Low 450.00 2.250 2.250 450.00 900.00 450.00 • Analysis Report 09/28/05 09:49:20 AM page 1 Method: CLP1 Sample Name: CCB2 Operator: PES Run Time: 09/28/05 09:41:39 Comment: M10: CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.56003 .0034 .34383 .0027 .0005 .0005 .0510 SDev .08861 .0084 .40016 .0013 .0001 .0001 .0024 %RSD 15.823 246.0 116.38 47.93 21.23 16.63 4.666 #1 -.65912 .0108 .03480 .0041 .0006 .0005 .0530 #2 -.48839 .0050 .79584 .0026 .0006 .0006 .0516 #3 -.53258 -.0057 .20084 .0015 .0004 .0004 .0484 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 .0050 .2000 Low -10.000 -.2000 -10.000 -.2000 -.2000 -.0050 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0006 .0005 .0002 .0009 .0094 .0672 .0069 SDev .0001 .0001 .0003 .0003 .0017 .0141 .0029 %RSD 13.58 31.84 161.1 36.72 18.51 20.97 42.06 #1 .0005 .0004 -.0001 .0009 .0105 .0748 .0067 #2 .0007 .0007 .0006 .0012 .0102 .0760 .0100 #3 .0006 .0004 .0002 .0005 .0074 .0510 .0042 rs LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass gh .0050 .0500 .0100 .0250 .1000 5.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge .0005 .0047 .0582 .0002 1.4287 -1.6090 -.71957 SDev .0002 .0016 .0182 .0003 .9374 .8374 .34818 %RSD 35.05 34.99 31.31 107.8 65.616 52.048 48.388 #1 .0005 .0063 .0770 -.0001 2.4585 -.65875 -.36713 #2 .0006 .0047 .0571 .0004 .62512 -2.2394 -1.0633 #3 .0003 .0030 .0406 .0004 1.2023 -1.9288 -.72826 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge .70907 3.2310 -.48568 .0322 .0016 .0005 .0008 SDev .42128 2.4853 .97605 .0104 .0009 .0001 .0003 %RSD 59.412 76.922 200.97 32.48 56.51 20.94 31.98 #1 .43152 6.0956 .11297 .0434 .0026 .0006 .0010 .50187 1.9486 .04197 .0302 .0016 .0006 .0010 1.1938 1.6488 -1.6120 .0228 .0007 .0004 .0005 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK O 00 M O V1 H nalysis Report 09/28/05 09:49:20 AM High Low E1* Units Avge SDev %RSD #1 #2 #3 Error High Low • • page 2 00 M O C/1 E-� T11908 v Zn Pb2203 Sb2068 Se1960 ppb ppm ppm ppb ppb ppb 3.1885 .0003 .0001 -.59739 .23333 .75197 1.4620 .0002 .0002 .86913 .29250 1.3173 45.853 71.98 115.5 145.49 125.36 175.18 4.8269 .0002 .0003 .37935 .16557 2.1052 2.7219 .0005 .0002 -1.2855 -.01934 .67689 2.0167 .0001 -.0000 -.88607 .55377 -.52616 s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 10.000 .0500 .0200 3.0000 60.000 5.0000 -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • page 2 00 M O C/1 E-� zalysis Report 09/28/05 09:57:07 AM �thod: CLP1 Sample Name: 0509510-006E Operator: PES in Time: 09/28/05 09:49:26 Mm t . M w - ee J �d#ONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Jnits ppb ppm ppb ppm ppm PPM kvge -.00687 .0691 .53687 .0217 .0100 .0002 3Dev .28503 .0027 1.2076 .0001 .0000 .0001 kRSD 4148.2 3.923 224.94 .3669 .4484 34.17 *1 .31774 .0718 -.69897 .0216 .0100 .0002 *2 -.21624 .0664 .59538 .0217 .0100 .0001 *3 -.12211 .0692 1.7142 .0216 .0100 .0002 Eleni Cd Co Cr Cu Fe K Jnits ppm ppm ppm ppm ppm PPM %vge .0002 .0001 .0026 .0108 .0348 1.628 30ev .0000 .0001 .0003 .0001 .0013 .008 9RSD 3.845 75.41 10.56 .6813 3.603 .4783 11 .0002 .0002 .0024 .0107 .0352 1.625 42 .0002 .0002 .0029 .0109 .0334 1.623 43 .0002 .0000 .0024 .0107 .0358 1.637 Elem Mn Mo Na Ni 2203/1 2203/2 Jnits ppm ppm ppm ppm ppb ppb %vge .01.60 .0018 15.43 .0021 -.18858 .02713 3D .0001 .0003 .13 .0004 1.69310 .85321 9R� .6202 17.88 .8486 17.34 897.80 3144.6 41 .0160 .0021 15.36 .0024 .93720 -.95744 �2 .0161 .0014 15.35 .0017 .63274 .54999 43 .0159 .0018 15.59 .0024 -2.1357 .48884 Elem 2068/2 1960/1 1960/2 Si Sn Sr Jnits ppb ppb ppb ppm ppm PPi11 kvge .62166 .49383 .73925 3.287 .0007 .0407 3Dev 2.1062 .61925 1.7828 .001 .0011 .0001 tRSD 338.81 125.40 241.17 .0173 146.3 .2669 �1 1.7101 .14682 1.0739 3.286 .0016 .0406 �2 1.9610 1.2088 2.3311 3.286 .0011 .0406 I3 -1.8061 .12589 -1.1872 3.287 -.0005 .0408 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Jnits ppb PPM PPM Ppb Ppb ppb kvge .93812 .0019 .0370 -.04466 1.0787 .65753 3Dev .0002 .0001 .53968 .5204 1.3568 kRSD .59833 63.779 8.543 .3692 1208.4 48.247 206.36 �1 1.3089 .0021 .0370 -.32649 1.5068 .76518 42 1.2576 .0018 .0371 .57759 1.2298 1.9574 R3 0 .24787 .0018 .0368 -.38509 .49941 -.74994 page 1 Ca PPM 22.68 .06 .2652 22.66 22.75 22.64 Mg ppm 4.398 .012 .2731 4.390 4.412 4.392 2068/1 ppb 1.9941 2.7858 139.70 1.0998 -.23473 5.1172 Ti ppm .0014 .0001 8.818 .0014 .0014 .0012 N 00 M O F-� zalysis Report 09/28/05 10:04:54 AM page 1 athod: CLP1 Sample Name: 0509510-007E Operator: PES in Time: 09/28/05 09:57:13 �d*ONC Corr. Factor: 1 31em Ag Al As1890 B Ba Be Ca Jnits ppb ppm ppb ppm .0182 ppm .0005 ppm -.0000 ppm . 21.66 kvge 3Dev -.16158 .13441 .0332 .0012 .15429 .30612 .0003 .0000 .0000 .04 WRSD 83.183 3.505 198.41 1.589 6.668 129.3 .1930 91 -.03501 .0345 -.08303 .0180 .0005 .0000 21.61 #2 -.14708 .0327 .49982 .0185 .0005 -.0000 21.68 93 -.30265 .0323 .04607 .0180 .0005 -.0000 21.69 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm -.0002 ppm ppm .0009 ppm .0241 ppm 6.619 ppm 4.811 kvge SDev .0001 .0001 .0003 .0035 .0002 .0002 .0001 .032 .008 %RSD 108.2 121.5 5.406 21.16 .6367 .4846 .1694 #1 .0001 -.0001 .0037 .0012 .0242 6.628 4.801 4.816 #2 .0000 -.0001 .0035 .0008 .0240 6.646 6.584 4.815 #3 .0000 -.0006 .0033 .0008 .0243 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm PPM 15.90 PPM .0047 Ppb -1.2775 Ppb -.17874 Ppb 1.0345 Avge SD .0056 .0007 .0002 .07 .0001 1.1094 1.61093 .5185 %Rio .0001 1.266 27.12 .4196 2.971 86.837 901.29 50.119 #1 .0057 .0005 15.86 .0048 -1.5378 -.96301 .60002 #2 .0056 .0007 15.98 .0046 -.06114 -2.2335 -1.2474 1.6742 .89497 1.6084 #3 .0055 .0008 15.87 .0046 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb 1.7343 PPM 3.279 PPM .0003 PPM .0365 PPM .0009 Avge SDev .09358 1.8417 .84414 1.3526 .8368 .006 .0006 .0000 .0001 %RSD 1968.1 160.24 48.249 .1806 185.8 .0758 13.72 #1 .18501 2.1099 1.0122 3.272 .0000 .0365 .0010 #2 1.8879 1.0036 1.5393 3.283 3.282 -.0001 .0365 .0365 .0008 .0008 #3 -1.7922 -.58116 2.6513 .0010 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM Ppb -.54458 Ppb .40691 Ppb 1.4379 Avge SDev .75605 .0010 .0002 .0743 .0003 .80883 1.1109 .1190 %RSD .82983 109.76 16.19 .3613 148.52 273.01 8.2751 #1 1.6942 .0008 .0740 -1.1544 .32323 1.3778 #2 .11805 .0011 .0744 -.85229 1.5573 1.3609 1.5749 #3 0 .45592 .0011 .0744 .37295 -.65977 M 00 M O N page 1 Ca PPM 22.65 .01 .0457 22.65 22.67 22.65 Mg PPM 4.693 .002 .0502 4.691 4.695 4.693 2068/1 ppb .86949 1.2649 145.48 1.5293 1.6680 -.58889 Ti PPM .0011 .0000 3.039 .0011 .0012 .0011 dt 00 M O F-+ 09/28/05 10:12:40 AM nalysis Report ethod: CLP1 Sample Name: 0509510-008E Operator: PES un Time: 09/28/05 10:05:00 ot: 1 IOW OWCONC Corr. Factor: Elem Ag Al As1890 B Ba Be Units ppb PPM Ppb PPM Ppm .0004 PPM .0001 Avge -.17531 .0478 .84940 1.0468 .0184 .0004 .0001 .0001 SDev %RSD .29502 168.29 .0021 4.479 123.24 2.307 17.26 64.01 #1 .16483 .0502 1.2939 .0180 .0003 .0001 #2 -.32901 .0473 -.34632 .0189 .0004 .0001 #3 -.36174 .0460 1.6006 .0184 .0003 .0000 Elem Cd Co Cr Cu Fe K Units ppm PPM PPM PPM PPM .0183 PPM 1.425 Avge .0002 .0002 .0022 .0000 .0009 .0003 .0008 .010 SDev %RSD .0000 1.296 .0003 147.5 1.739 34.61 4.115 .6889 #1 .0002 -.0001 .0022 .0005 .0180 1.436 1.418 #2 .0002 .0003 .0021 .0010 .0192 1.421 #3 .0002 .0005 .0022 .0011 .0178 Mo Na Ni 2203/1 2203/2 Elem Units Mn PPM PPM PPM PPM Ppb Ppb -1.1814 Av a .0042 .0011 16.37 .0154 .13455 1.9503 .4692 % .0001 2.001 .0001 4.415 .11 .6531 .0004 2.719 1449.5 39.713 #1 .0041 .0011 16.50 .0152 -.07912 -1.7231 -.90767 #2 .0043 .0010 16.30 16.32 .0151 -1.7001 2.1829 -.91341 #3 .0042 .0011 .0159 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb ppb ppb PPM 3.406 ppm .0009 PPM .0366 Avge .21411 .55749 .81756 .010 06 002 .0003 SDev %RSD 867574 172306 315239 .3034 72540 .8605 #1 -1.1361 -.55178 1.0461 3.418 .0003 .0368 #2 -.55456 1.0436 .86468 3.402 3.398 .0015 .0008 .0368 .0362 #3 2.3330 1.1807 .54188 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Ppb Units pp PPM m PPM Ppb -.74316 Ppb .43236 .73096 Avge .83238 .0009 .1035 .0004 .74552 .83220 .20613 SDev %RSD 1.8501 222.27 .0001 12.53 .3785 100.32 192.48 28.199 #1 .99545 .0008 .1031 -1.1756 -.24854 .51404 #2 -1.0939 .0009 .1039 -1.1715 .18559 1.3600 .92425 .75460 4) 2.5956 .0011 .1034 .11770 page 1 Ca PPM 22.65 .01 .0457 22.65 22.67 22.65 Mg PPM 4.693 .002 .0502 4.691 4.695 4.693 2068/1 ppb .86949 1.2649 145.48 1.5293 1.6680 -.58889 Ti PPM .0011 .0000 3.039 .0011 .0012 .0011 dt 00 M O F-+ analysis Report 09/28/05 10:20:27 AM page 1 4ethod: CLP1 Sample Name: 0509510-009E Operator: PES Zun Time: 09/28/05 10:12:46 :omment: Factor: 1 (06 IV CONC Corr. Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge -.30346 .0418 .59447 .0190 .0004 -.0000 22.49 SDev .15921 .0017 .76206 .0002 .0000 .0000 .08 %RSD 52.464 4.107 128.19 1.265 5.032 18.74 .3661 #1 -.46845 .0437 1.3094 .0192 .0004 -.0000 22.39 #2 -.29120 .0404 .68132 .0189 .0004 -.0000 22.52 #3 -.15074 .0412 -.20731 .0188 .0005 -.0000 22.54 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm PPM Avge .0000 -.0002 .0029 .0008 .0432 1.325 4.514 SDev .0001 .0000 .0001 .0002 .0003 .006 .020 %RSD 173.7 21.72 2.552 18.92 .7822 .4507 .4355 #1 -.0000 -.0003 .0028 .0007 .0429 1.332 4.492 #2 .0000 -.0002 .0029 .0009 .0434 1.320 4.527 #3 .0001 -.0002 .0030 .0010 .0435 1.323 4.524 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb Ppb Avge .0062 .0007 15.31 .0034 1.4276 -.11907 1.9139 S .0001 .0001 .03 .0006 1.2835 .92766 1.3379 jo1.507 10.96 .2026 17.27 89.902 779.09 69.907 #1 .0060 .0007 15.33 .0029 .10377 -1.1688 1.1572 #2 .0062 .0006 15.27 .0041 1.5126 .22087 3.4587 #3 .0062 .0007 15.32 .0032 2.6665 .59067 1.1258 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm PPM Avge -.34254 -.06434 .30213 3.300 .0001 .0386 .0012 SDev .12086 1.68637 1.2479 .009 .0004 .0002 .0001 %RSD 35.284 2621.2 413.03 .2759 454.5 .4557 7.330 #1 -.46985 -2.0098 -1.0949 3.291 -.0001 .0384 .0011 #2 -.22937 .98011 1.3064 3.301 .0006 .0387 .0012 #3 -.32840 .83671 .69485 3.309 -.0002 .0388 .0013 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb Ppb Avge .53436 .0011 .0835 .39606 .40887 .18010 SDev 1.3788 .0002 .0005 1.0373 .51260 1.3869 %RSD 258.03 14.84 .6308 261.89 125.37 770.04 #1 -1.0326 .0011 .0829 -.74493 .07196 -1.3996 #2 1.5621 .0012 .0836 .65111 .99878 1.1978 #3 1.0735 .0009 .0840 1.2820 .15586 .74211 U V) 00 M O E-� nalysis Report 09/28/05 10:28:14 AM page 1 ethod: CLP1 Sample Name: 0509510-010E Operator: PES un Time: 09/28/05 10:20:33 ont: Factor: 1 W - (Oro oW CONC Corr. Elem Ag Al As1890 B Ba Be Ca Units ppb -.52120 PPM Ppb 1.1687 ppm .0171 PPM .0003 PPM -.0000 PPM 21.13 Avge SDev .0406 .0018 .6635 .0003 .0001 .0000 .08 %RSD .25389 48.713 4.450 56.774 1.676 22.63 48.28 .3775 #1 -.63226 .0401 1.8890 .0170 .0003 -.0000 21.04 #2 -.23070 .0426 1.0351 .0169 .0002 -.0000 21.13 #3 -.70063 .0390 .58222 .0174 .0003 -.0000 21.20 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM -.0002 PPM PPM .0004 PPM .0181 PPM 1.230 PPM 4.285 Avge SDev .0000 .0003 .0014 .0001 .0000 .0000 .011 .014 %RSD .0001 331.4 121.2 7.721 9.259 .1730 .9232 .3232 #1 .0001 .0014 .0004 .0181 1.231 4.272 #2 .0001 .0000 -.0005 .0013 .0004 .0180 1.219 4.284 #3 -.0000 -.0003 .0014 .0004 .0181 1.241 4.300 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm PPM PPM 14.37 PPM Ppb -2.1922 Ppb -.02915 Ppb 1.9350 Avge .0038 .0008 .0004 .09 .0033 .0003 1.4595 .32760 1.1128 ° .0001 1.284 46.02 .6364 7.682 66.577 1123.9 57.511 #1 .0007 14.33 .0033 -.68873 -.33651 1.8667 #2 .0038 .0006 14.30 .0030 -3.6034 .31549 .85786 #3 .0038 .0039 .0013 14.47 .0035 -2.2846 -.06642 3.0804 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb 2.7598 Ppb -.14911 PPM 3.122 PPM -.0002 ppm, .0354 Ppm .0008 Avge SDev .17960 1.0521 2.0072 1.86238 .012 .0015 .0003 .0000 %RSD 585.80 72.729 1249.0 .3790 628.9 .8321 3.999 #1 1.2233 2.4703 1.8535 3.113 .0015 .0351 .0008 #2 -,88073 .91311 -1.8291 3.118 3.135 -.0010 -.0012 .0356 .0354 .0008 .0009 #3 .19626 4.8960 -.47173 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM Ppb -.74943 Ppb .76415 Ppb .81956 Avge SDev -.48058 .0008 .0002 .0629 .0003 .27216 .93374 1.5482 %RSD .59940 124.72 23.59 .4798 36.315 122.19 188.91 #1 -.48875 .0007 .0626 -.45376 1.4375 2.0589 #2 -1.0759 .0007 .0630 -.98949 -.30178 -.91594 16 .12286 .0010 .0632 -.80503 1.1567 1.3157 page 1 Ca PPM 23.38 .03 .1089 23.37 23.40 23.35 Mg PPM 4.510 .006 .1349 4.510 4.516 4.504 2068/1 ppb 2.9534 .5939 20.109 2.6315 2.5900 3.6388 Ti PPM .0008 .0001 12.83 .0009 .0007 .0009 r- 00 M O 09/28/05 10:36:01 AM ialysis Report �thod: CLP1 Sample Name: 0509510-011B Operator: PES in Time: 09/28/05 10:28:20 AONC Corr. Factor: 1 31em A9 Al As1890 B Ba PPM Be PPM Jnits ppb PPM ppb PPM .0196 .0006 -.0000 lege -.08555 .0408 .84971 0435 .001 0 SDev MSD .19649 226. 30743 90015 i?617 1945 80428 31042003 91 -.12440 .0424 -.10789 .0194 .0007 -.0000 -.0000 92 -.25707 .0408 1.3125 1.3445 .0199 .0006 .0006 -.0001 #3 .12482 .0393 .0195 Elem Cd Co Cr Cu FeK PPM PPM Units ppm -.0000 Ppm -.0002 PPM .0020 PPM .0009 .0143 1.315 Avge SDev .0001 .0000 .0001 .0001 .0001 .016 1.192 %RSD 600.5 22.10 5.519 8.555 .6448 #1 -.0000 -.0002 .0021 .0009 .0142 1.314 1.300 #2 .0001 -.0002 .0019 .0008 .0144 1.332 #3 -.0001 -.0003 .0021 .0009 .0143 Na Ni 2203/1 2203/2 Elem Mn Mo PPM Ppb Ppb Units PPM P M m P0005 ppm 15.01 .0030 -1.3353 -.70796 Av .16 .0003 .6646 .77564 S % 0 .0000 .3638 .0002 36.79 1.049 9.911 49.777 109.5 #1 .0114 .0008 14.92 .0030 -1.1242 -.80175 -.92221 -1.3540 #2 .0113 .0004 14.91 15.19 .0032 -2.0798 .15229 #3 .0113 .0005 .0026 Elem 2068/2 1960/1 1960/2 Si Sn Sr PPM Units ppb Ppb Ppb 1.8992 PPM 3.214 PPM .0006 .0395 Avge .83936 2.3376 1.0710 .007 .0004 .0003 SDev 1.3202 .7221 30.890 56.390 .2307 63.96 .7842 %RSD 157.29 #1 .60182 3.0166 .96799 3.210 .0009 .0391 #22.2623 1.5790 1.6601 3.0695 3.210 3.223 .0002 .0009 .0398 .0395 #3 -.34599 2.4173 Zn Pb2203 Sb2068 Se1960 Elem T11908 v pb ppb Ppb Units Ppb PP0012 PPM 0490 -.91677 1.5434 2.0452 Avge -.11558 .29629 .7323 .6990 SDev 1.87685 .0003 27.92 .0001 .2869 32.319 47.449 34.180 %RSD 1623.8 #1 -1.7568 .0015 .0491 -.98940 1.2777 2.3714 1.6502 1.6331 #2 -.52065 .0009 .0491 -1.1700 .98095 2.8523 0 1.9307 .0011 .0488 -.59092 page 1 Ca PPM 23.38 .03 .1089 23.37 23.40 23.35 Mg PPM 4.510 .006 .1349 4.510 4.516 4.504 2068/1 ppb 2.9534 .5939 20.109 2.6315 2.5900 3.6388 Ti PPM .0008 .0001 12.83 .0009 .0007 .0009 r- 00 M O ialysis Report 09/28/05 10:43:49 AM �thod: CLP1 Sample Name: 0509510-012E Operator: PES in Time: 09/28/05 10:36:08 �ddWONC Corr. Factor: 1 3lem Ag Al As1890 B Ba Be Jnits ppb -.40864 ppm Ppb -.04294 Ppm .0208 PPM .0007 PPM -.0001 kvge SDev .0452 .0016 1.34367 .0001 .0000 .0000 RSD .15666 38.337 3.593 3128.9 .6216 2.658 39.32 91 -.48409 .0447 1.0355 .0207 .0007 -.0000 92 -.22853 .0439 -1.5482 .0209 .0007 -.0001 93 -.51329 .0470 .38390 .0209 .0007 -.0001 Elem Cd Co Cr Cu Fe K Units ppm PPM PPM PPM .0011 PPM .0159 PPM 1.390 Avge SDev .0000 -.0001 .0001 .0016 .0002 .0002 .0004 .007 %RSD .0001 364.4 133.8 12.45 21.13 2.613 .4870 #1 #2 #3 Elem Units Av S %R #1 #2 #3 Elem Units Avge SDev %RSD #1 #2 #3 Elem Units Avge SDev %RSD .0001 .0000 -.0001 Mn PPM .0092 .0001 .7415 .0092 .0093 .0091 2068/2 ppb -.81779 2.99371 366.07 2.2822 -3.6925 -1.0431 T11908 ppb -.42418 .91208 215.02 .0000 -.0001 -.0002 Mo PPM .0007 .0006 83.46 .0001 .0013 .0008 1960/1 ppb -.22112 1.17636 532.00 -.41827 -1.2864 1.0414 v PPM .0013 .0001 9.186 #1 -1.2964 .0012 #2 .52313 .0013 V-.49928 .0015 .0017 .0018 .0014 Na PPM 15.75 .12 .7661 15.64 15.73 15.87 1960/2 ppb 1.0503 .8544 81.349 .95517 1.9484 .24748 Zn PPM .0550 .0001 .1785 .0550 .0551 .0549 .0008 .0011 .0013 Ni ppm .0031 .0001 3.749 .0032 .0030 .0031 Si PPM 3.332 .013 .3793 3.319 3.332 3.344 Pb2203 ppb -.13042 .33390 256.03 .00389 .11542 -.51056 .0154 .0160 .0162 2203/1 ppb -1.0633 .4566 42.945 -.97363 -1.5582 -.65818 Sn PPM -.0001 .0002 155.4 Sb2068 ppb .48826 1.7259 353.49 2.3166 -1.1127 .26091 1.383 1.391 1.396 2203/2 ppb .33532 .70705 210.86 .49189 .95095 -.43689 Sr ppm .0409 .0004 1.109 .0413 .0409 .0404 Se1960 ppb .62695 .21163 33.756 .49781 .87119 .51186 page 1 Ca ppm 24.15 .06 .2398 24.09 24.18 24.19 Mg PPM 4.743 .012 .2450 4.730 4.748 4.751 2068/1 ppb 3.1043 .8582 27.646 2.3855 4.0545 2.8729 Ti PPM .0014 .0000 2.023 .0014 .0014 .0014 00 00 M O F-+ ialysis Report 09/28/05 10:51:36 AM page 1 �thod: CLP1 Sample Name: 0509510-013E operator: PES in Time: 09/28/05 10:43:55 11&0 t: C-oi 61A-011- 3d ONC Corr. Factor: 1 3lem Ag Al As1890 B Ba Be Ca Jnits ppb PPM Ppb PPM PPM -.0003 PPM -.0001 PPM .1407 kvge SDev -.31904 .04931 -.0038 .0024 .27272 .67247 .0001 .0002 .0000 .0000 .0050 3.545 WRSD 15.457 62.49 246.58 154.6 10.17 32.44 41 -.26655 -.0048 1.0462 .0003 -.0003 -.0001 .1462 #2 -.32618 -.0011 -.05424 .0001 -.0003 -.0000 .1394 #3 -.36440 -.0056 -.17375 -.0001 -.0003 -.0001 .1365 Elem Cd Co Cr Cu Fe K Mg PPM Units ppm -.0000 PPM -.0001 PPM -.0003 PPM .0001 PPM .0042 PPM .0323 -.0001 Avge SDev .0001 .0003 .0001 .0003 .0003 .0061 .0019 2454. %RSD 737.4 266.9 46.75 530.9 6.147 18.78 #1 -.0000 -.0001 -.0003 .0001 .0042 .0378 .0013 -.0022 #2 -.0001 -.0005 -.0005 -.0003 .0044 .0258 .0333 .0007 #3 .0001 .0002 -.0002 .0003 .0039 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm PPM PPM PPM Ppb -.79031 Ppb -.70255 Ppb 1.2864 Av -.0000 '.0001 .0003 .2836 -.0003 .0001 1.42095 1.91746 1.2881 S % 2442. .0005 200.6 .0009 .3157 29.40 179.80 272.93 100.13 #1 -.0003 .2841 -.0004 -.94672 -.43392 .87976 2.7288 #2 .0000 -.0001 .0005 .2841 -.0003 -2.1266 1.0664 -2.7402 .25071 #3 .0000 .0007 .2825 -.0002 .70238 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb PPM PPM .0002 PPM -.0003 PPM .0002 Avge 1.3946 2.2078 1.2817 2.9154 -.09196 1.15427 .1711 18032 00 SDev %RSD 158.30 227.47 1255.1 20645 20005 B.0000 #1 .56832 -1.0850 -1.3257 .1678 .0001 -.0002 .0002 #2 -,28077 .39163 .96161 .1692 .0007 -.0002 -.0003 -.0003 .0002 .0001 #3 3.8964 4.5385 .08824 .1763 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM -.0016 Ppb -.73173 Ppb 1.3586 Ppb .36547 Avge -.66225 1.00884 .0002 .0001 .80603 1.1467 1.4512 SDev %RSD 152.34 .0003 166.5 4.890 110.15 84.402 397.07 #1 -1.7346 .0005 -.0015 -.60464 .67203 -1.2456 #20 000 -.0016 00 0320 -5938 .72141 2.6824 .77181 1.5702 * 268026 -0 0000 -.0016 zalysis Report 09/28/05 10:59:23 AM page 1 ethod: CLP1 Sample Name: CCV3 an Time: 09/28/05 10:51:42 991.21 C)Trmmt: LC Pass High 1100.0 odWCONC Corr. Factor: 1 Elem Eleni Ag Al As1890 Units ppb ppm ppb Avge 992.90 51.55 523.23 SDev 1.72 .27 2.22 %RSD .17311 .5318 .42493 #1 994.65 #2 992.85 #3 991.21 Errors LC Pass High 1100.0 Low 900.00 Elem Cd Units ppm Avge 2.547 SDev .008 %RSD .3036 #1 2.555 #2 2.540 # 2.546 • E ors LC Pass High 2.750 Low 2.250 Eleni Mn Units PPM Avge 2.542 SDev .004 %RSD .1726 #1 2.547 #2 2.538 #3 2.541 Errors LC Pass High 2.750 Low 2.250 Eleni 2068/2 Units ppb Avge 975.60 SDev 9.04 $RSD .92654 984.43 966.37 #3 976.01 51.48 51.85 51.31 LC Pass 55.00 45.00 Co PPM 2.561 .004 .1527 2.565 2.557 2.560 LC Pass 2.750 2.250 Mo ppm 2.606 .004 .1488 2.609 2.602 2.606 NOCHECK 1960/1 ppb 526.52 2.56 .48669 529.43 524.60 525.52 524.80 520.68 524.20 LC Pass 550.00 450.00 Cr PPM 2.544 .004 .1761 2.549 2.541 2.542 LC Pass 2.750 2.250 Na ppm 82.84 .85 1.027 82.38 83.82 82.33 LC Pass 88.00 72.00 1960/2 ppb 526.79 3.63 .68901 530.97 524.40 525.01 Errors NOCHECK NOCHECK NOCHECK B PPM 2.538 .001 .0348 2.538 2.539 2.537 LC Pass 2.750 2.250 Cu ppm 2.553 .005 .2115 2.553 2.558 2.547 LC Pass 2.750 2.250 Ni PPM 2.526 .008 .3055 2.534 2.518 2.527 LC Pass 2.750 2.250 Si ppm 2.453 .038 1.543 2.412 2.459 2.487 NOCHECK Operator: PES Ba PPM 2.524 .004 .1576 2.529 2.522 2.522 LC Pass 2.750 2.250 Fe ppm 52.12 .14 .2755 52.26 51.97 52.12 LC Pass 55.00 45.00 2203/1 ppb 518.02 1.35 .26034 519.19 516.55 518.33 NOCHECK Sn PPM 2.556 .002 .0653 2.558 2.555 2.557 NOCHECK Be ppm 2.580 .007 .2535 2.587 2.573 2.580 LC Pass 2.750 2.250 K PPM 82.96 .74 .8923 82.59 83.81 82.47 LC Pass 88.00 72.00 2203/2 ppb 506.51 1.44 .28473 507.93 505.04 506.58 NOCHECK Sr ppm 2.513 .002 .0907 2.515 2.513 2.511 NOCHECK Ca PPM 52.87 .07 .1355 52.95 52.82 52.83 LC Pass 55.00 45.00 Mg PPM 53.61 .06 .1069 53.67 53.60 53.56 LC Pass 55.00 45.00 2068/1 ppb 982.25 2.71 .27634 985.13 979.74 981.89 NOCHECK Ti PPM 2.676 .013 .4934 CD 2.692 2.669 2.669 p NOCHECK 51.48 51.85 51.31 LC Pass 55.00 45.00 Co PPM 2.561 .004 .1527 2.565 2.557 2.560 LC Pass 2.750 2.250 Mo ppm 2.606 .004 .1488 2.609 2.602 2.606 NOCHECK 1960/1 ppb 526.52 2.56 .48669 529.43 524.60 525.52 524.80 520.68 524.20 LC Pass 550.00 450.00 Cr PPM 2.544 .004 .1761 2.549 2.541 2.542 LC Pass 2.750 2.250 Na ppm 82.84 .85 1.027 82.38 83.82 82.33 LC Pass 88.00 72.00 1960/2 ppb 526.79 3.63 .68901 530.97 524.40 525.01 Errors NOCHECK NOCHECK NOCHECK B PPM 2.538 .001 .0348 2.538 2.539 2.537 LC Pass 2.750 2.250 Cu ppm 2.553 .005 .2115 2.553 2.558 2.547 LC Pass 2.750 2.250 Ni PPM 2.526 .008 .3055 2.534 2.518 2.527 LC Pass 2.750 2.250 Si ppm 2.453 .038 1.543 2.412 2.459 2.487 NOCHECK Operator: PES Ba PPM 2.524 .004 .1576 2.529 2.522 2.522 LC Pass 2.750 2.250 Fe ppm 52.12 .14 .2755 52.26 51.97 52.12 LC Pass 55.00 45.00 2203/1 ppb 518.02 1.35 .26034 519.19 516.55 518.33 NOCHECK Sn PPM 2.556 .002 .0653 2.558 2.555 2.557 NOCHECK Be ppm 2.580 .007 .2535 2.587 2.573 2.580 LC Pass 2.750 2.250 K PPM 82.96 .74 .8923 82.59 83.81 82.47 LC Pass 88.00 72.00 2203/2 ppb 506.51 1.44 .28473 507.93 505.04 506.58 NOCHECK Sr ppm 2.513 .002 .0907 2.515 2.513 2.511 NOCHECK Ca PPM 52.87 .07 .1355 52.95 52.82 52.83 LC Pass 55.00 45.00 Mg PPM 53.61 .06 .1069 53.67 53.60 53.56 LC Pass 55.00 45.00 2068/1 ppb 982.25 2.71 .27634 985.13 979.74 981.89 NOCHECK Ti PPM 2.676 .013 .4934 CD 2.692 2.669 2.669 p NOCHECK • • page 2 09/28/05 10:59:23 AM zalysis Report :sigh [,* Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm 2.673 ppb 510.35 ppb 977.82 ppb 526.70 Avge 504.05 2.25 2.558 .004 1.41 6.92 3.27 SDev %RSD .44614 .004 .1395 .1601 .27570 .70808 .62108 #1 501.99 2.562 2.678 511.68 984.66 530.46 #2 506.45 2.556 2.670 508.87 970.82 524.47 #3 503.70 2.555 2.672 510.49 977.97 525.18 Errors LC Pass LC Pass LC Pass LC Pass LC Pass 1100.0 LC Pass 550.00 High 550.00 2.750 2.750 2.250 550.00 450.00 900.00 450.00 Low 450.00 2.250 • • page 2 ialysis Report 09/28/05 11:07:10 AM page 1 �thod: CLP1 Sample Name: CCB3 Operator: PES in Time: 09/28/05 10:59:29 )ddWONC Corr. Factor: 1 slem Ag Al As1890 B Ba Be Ca Snits ppb -.45448 PPM Ppb PPM .0023 Ppm .0003 ppm .0003 ppm .0364 kvge 3Dev .11083 .0041 .0037 .08474 .77936 .0008 .0001 .0001 .0018 4.812 kRSD 24.386 91.81 919.68 33.75 36.28 29.44 �1 -.51957 .0073 .22272 .0031 .0003 .0003 .0361 �2 -.32651 .0049 -.75440 .0023 .0004 .0003 .0383 93 -.51735 -.0000 .78590 .0015 .0002 .0002 .0348 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 10.000 .2000 10.000 .2000 .2000 -.2000 .0050 -.0050 .2000 -.2000 Low -10.000 -.2000 -10.000 -.2000 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm .0002 ppm .0054 ppm .0574 ppm -.0001 Avge SDev .0004 -.0001 .0002 .0001 .0002 .0001 .0016 .0100 .0015 %RSD .0001 29.96 246.0 223.9 29.73 30.47 17.50 1296. #1 .0003 -.0001 .0000 .0003 .0062 .0669 -.0008 #2 .0005 .0001 .0002 .0001 .0064 .0586 .0469 .0017 -.0012 #3 .0003 -.0002 -.0001 .0002 .0035 EAs LC Pass LC Pass LC Pass LC Pass LC Pass LCPass High .0050 .0500 .0100 .0250 -.0250 .1000 -.1000 5C.000 -5.000 .2000 -.2000 Low -.0050 -.0500 -.0100 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm ppm ppm ppm Ppb -1.3643 Ppb .33746 Ppb 1.6604 Avge .0002 .0045 .0504 -.0000 .0004 .6322 .42399 1.5280 SDev %RSD .0001 46.69 .0019 41.13 .0137 27.10 13500. 46.341 125.64 92.027 #1 .0003 .0066 .0634 .0003 -1.5737 .78257 -.06165 3.0108 .00172 #2 .0003 .0038 .0515 .0001 -.0004 -1.8653 -.65395 .29148 1.9688 #3 .0001 .0031 .0362 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb ppm ppm ppm .0003 ppm .0006 Avge -.02056 3.7197 1.363622 .65456 .0360 .0007 02 SDev %RSD 1.65771 8064.6 620 235382 00 21078 66 13505 25001 85 28060 1.1639 4.0014 1.9441 .0435 .0018 .0004 .0007 .0006 0-1.9150 2.2387 1.0677 .0364 .0002 .0001 .0004 .0002 .0004 #3 .68945 4.9189 -1.0481 .0280 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Errors NOCHECK ialysis Report 09/28/05 11:07:10 AM sigh �o 31e Jnits kvge ;Dev $RSD 91 92 93 Errors High Low • • page 2 T11908 v Zn Pb2203 Sb2068 Se1960 ppb 2.6368 PPM PPM Ppb -.22919 Ppb .53923 Ppb 1.6752 1.8255 .0004 .0002 .0006 .0001 .37518 1.6073 .8659 69.231 43.70 24.34 163.70 298.07 51.685 4.4502 .0002 .0006 -.00202 1.7789 2.6292 .79948 .0005 .0007 -.66224 -1.2767 1.4576 2.6607 .0004 .0004 -.02331 1.1155 .93896 LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 10.000 .0500 .0200 3.0000 60.000 5.0000 -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • page 2 -ialysis Report 09/28/05 11:14:57 AM page 1 athod: CLP1 Sample Name: ORIF in Time: 09/28/05 11:07:16 t: AONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge 18.995 -.0115 22.587 SDev .459 .0029 .616 %RSD 2.4138 25.13 2.7285 #1 19.223 -.0120 22.751 #2 18.467 -.0141 21.905 #3 19.295 -.0084 23.104 Elem Cd Co Cr Units ppm ppm PPM Avge .0105 .1032 .0203 SDev .0001 .0012 .0005 %RSD 1.092 1.124 2.307 #1 .0105 .1021 .0200 #2 .0104 .1032 .0201 #3 .0106 .1044 .0209 Elem Mn Mo Na Units ppm PPM PPM A .0306 .0225 .0189 .0004 .0007 .0029 $ 1.186 3.135 15.61 #1 .0303 .0233 .0223 #2 .0306 .0219 .0174 #3 .0310 .0222 .0169 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 121.91 13.866 11.740 SDev 3.41 2.162 1.866 %RSD 2.7939 15.589 15.891 #1 119.92 11.498 12.270 ##2 119.97 14.366 13.282 #3 125.84 15.734 9.6663 Elem T11908 v Zn Units ppb ppm ppm Avge 22.261 .1026 .0443 SDev 1.579 .0008 .0003 %RSD 7.0929 .7352 .7928 #1 23.941 .1021 .0439 #2 20.807 .1023 .0443 is22.034 .1035 .0446 B PPM .1875 .0017 .8897 .1856 .1881 .1888 Cu PPM .0506 .0007 1.317 .0500 .0504 .0513 Ni PPM .0825 .0011 1.312 .0822 .0816 .0837 Si PPM .0502 .0013 2.670 .0507 .0512 .0487 Pb2203 ppb 6.0271 .6009 9.9697 6.5236 5.3591 6.1984 Operator: PES Ba PPM -.0002 .0001 33.02 -.0001 -.0002 -.0001 Fe PPM -.0004 .0006 148.1 .0002 -.0008 -.0005 2203/1 ppb 6.2580 .3505 5.6005 6.3085 5.8851 6.5806 Sn PPM .0841 .0015 1.791 .0829 .0835 .0858 Sb2068 ppb 122.11 2.88 2.3620 120.34 120.54 125.43 Be ppm .0107 .0000 .3733 .0106 .0107 .0107 K PPM .0361 .0084 23.24 .0358 .0279 .0447 2203/2 ppb 5.9116 .•7718 13.055 6.6309 5.0964 6.0075 Sr PPM -.0002 .0001 41.10 -.0001 -.0002 -.0001 Se1960 ppb 12.448 1.048 8.4205 12.013 13.643 11.687 Ca PPM -.0021 .0008 39.29 -.0016 -.0030 -.0016 Mg PPM -.0045 .0028 62.34 -.0039 -.0075 -.0020 2068/1 ppb 122.50 1.85 1.5117 121.19 121.70 124.62 Ti PPM .0001 .0001 190.8 .0001 -.0001 .0002 09/28/05 11:22:44 AM page 1 zalysis Report sthod: CLP1 Sample Name: ICSAF Operator: PES in Time: 09/28/05 11:15:03 t: �d CONC Corr. Factor: 1 ElemAgAl As1890 B Ba Be Ppm Ca ppm Units Unit ppb ppm Ppb ppm -.0005 Ppm . 0010 .0002 526.3 Avge .33888 507.0 1.5 -1.4532 1.3144 .0005 .0000 .0000 SDev %RSD .11791 34.794 .3022 90.449 100.8 3.117 8.098 .0546 #1 .21311 506.7 -.25600 .0001 .0010 .0002 526.7 #2 .44693 505.7 526.2 #3 .35661 508.7 -2,8598 -.001 0 .0010 .0002 Errors LC Pass LC Pass NOCHECK NOCHECK LC Pass L Pass C Pass High 10.000 600.0 .2000 -,2000 -.0050 400.0 Low -10.000 400.0 Elem Cd Co Cr Cu m Fe PP m K ppm Mg PPM Units ppm ppm ppm PP -.0023 210.2 .0327 521 �� Avge SDev .0005 .0001 -.0001 .0003 .0031 .0001 .0001 •2 ,0048 14.58 •0295 %RSD 18.49 367.1 2.908 6.133 .1076 #1 .0004 -.0003 .0032 -.0022 210.5 .0314 521.4 521.5 #2 .0006 .0003 .0031 -.0022 -.0024 210.1 210.0 .0380 .0288 521.7 # .0004 -.0002 .0030 LC Pass NOCHECK LC Pass NOCHECK LC Pass NOCHECK 600Pass E rs High .0050 .0100 240.0 160.0 400.0 Low -.0050 -,0100 Ni 2203/1 2203/2 2068/1 Elem Mn Mo Na Ppm ppb ppb ppb m •0064 m -•0036 ppm .0623 .0031 31.185 -18.683 -2.2500 2.6159 Avges SDev .0006 .0003 .0004 .0006 20.88 2.308 7.4015 .703 3.7604 116.26 %RSD 8.798 9.564 .6044 #1 .0059 -.0033 .0621 .0032 30.780 33.669 -19.335 -18.777 -2.1523 -4.9135 #2 .0065 -.0036 .0620 .0037 29.107 -17.939 .31568 #3 .0070 -.0040 .0627 .0024 NOCHECK NOCHECK LC Pass NOCHECK NOCHECK NOCHECK Errors LC Pass .0400 High .0150 -,0400 Low -.0150 Elem 2068/2 1960/1 19b0/2 Si Sn Sr PP m Ti ppm Units ppb ppb PP 3565 ppm ppm .0504 -.3255 .0031 Avge 1.3096 3.0375 -.52783 1.88570 -.5 .44006 .0013 .0012 .0013 .0009 .0002 5.356 SDev %RSD 231.94 357.25 82.154 96.65 2.636 .2710 4.5558 1.4303 -.65972 .0027 .0518 -.3264 -.3255 .0029 .0032 M 0 .83673 -.68215 -.04687 .0009 .0492 -.3247 .0032 O #3 -1.4637 -2.3316 -.90036 .0003 .0502 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Errors NOCHECK zalysis Report 09/28/05 11:22:44 AM page 2 High C,o0 Elem T11908 Units ppb Avge L-11.146 SDev .692 %RSD 6.2125 #1 L-11.924 #2 L-10.599 #3 L-10.914 Errors LC Low High 10.000 Low -10.000 • • V Zn Pb2203 Sb2068 Se1960 ppm ppm Ppb Ppb Ppb -.0005 -.0100 -2.0771 .12426 -.53304 .0002 .6883 1.9061 .74557 .0004 75.80 1.681 33.139 1534.0 139.87 -.0004 -.0099 -2.6465 2.3220 .03627 -.0002 -.0099 -1.3121 -1.0781 -.25842 -.0010 -.0102 -2.2726 -.87116 -1.3770 LC Pass LC Pass LC Pass LC Pass LC Pass .0200 6.0000 60.000 5.0000 .0500 -.0500 -.0200 -6.0000 -60.000 -5.0000 09/28/05 11:30:32 AM page 1 zalysis Report athod: CLP1 Sample Name: ICSABF Operator: PES in Time: 09/28/05 11:22:51 :)ddWONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be m Ca ppm Units nit1063.3 ppb PPM Ppb 1052.6 ppm PPM .5255 PP .5190 522.9 kvge 503.9 2.2 .9397 .0014 .0008 .0014 1.8 SDev %RSD 1.6 .14738 .2 .0475 .21109 .1437 .1489 .2768 .3360 #1 1063.5 503.6 1054.3 .9385 .5258 .5189 522.7 524.8 #2 1064.8 504.1 1053.4 .9412 .5261 .5204 521.3 #3 1061.7 503.8 1050.1 .9395 .5246 .5175 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 600.0 High 1200.0 600.0 L.200 1 8000 .6000 .6000 .4000 400.0 ow 800.00 400.0 800000 .4000 Elem Cd Co Cr Cu Fe KMg PPM PP m Units ppm ppm ppm ppm ppm 208.8 .0296 51?.4 Avge SDev .9760 .0028 .4874 .0016 .5061 .0014 .5382 .0005 .6 .0056 18.74 1.4 %RSD .2905 .3338 .2743 .0919 .3090 .2721 #1 .9758 .4866 .5061 .5377 208.9 .0262 517.0 519.0 #2 .9790 .4892 .5076 .5386 209.3 208.1 .0360 .0266 516.2 #3 .9733 .4863 .5048 .5383 LC Pass LC Pass LC Pass LC Pass LCPaass NOCHECK L6COOPass EjOrs High 1.200 .6000 .6000 .6000 240 160.0 400.0 Low .8000 .4000 .4000 .4000 Ni 2203/1 2203/2 2068/1 Elem Mn Mo Na pp Ppb Ppb Units ppm PP m 1.020 PPM ppm .9623 1045.8 991.84 2.2068 Avge .5080 .0496 .0030 SDev .0012 .003 .0008 1.645 .3072 .73644 .18522 24.599 %RSD .2343 .3331 #1 .5076 1.020 .0486 .9625 1044.1 1054.3 991.07 994.16 -7.7115 -11.519 #2 .5093 1.023 .0500 .9651 1039.2 990.89 -7.6820 #3 .5071 1.016 .0501 .9592 LC Pass NOCHECK NOCHECK LCPassNOCHECK NOCHECK NOCHECK Errors 1..8000 High .6000 Low .4000 Elem 2068/2 1960/1 1960/2 Si Sn Sr PPM Ti ppm Units pp b ppb ppb 1031.6 PPM ppm 1.005 -.3244 .0025 Avge -8.7800 1035.2 4.3 •4926 .0021 .0001 SDev 2.4053 6.8 .0019 .3850 .5159 .6326 2.432 %RSD 27.395 .65219 .41610 -7.9216 1037.4 1034.6 .4904 1.045 1.055 -.3228 -.3267 .0025 .0025 is-6.9216 1040.5 1033.5 .4937 1.048 -.3238 .0026 #3 -11.497 1027.6 1026.7 .4936 NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK Errors NOCHECK zalysis Report 09/28/05 11:30:32 AM Sigh Jowo 31 em 7nits kvge 3Dev WRSD 01 N2 #3 Errors High Low • I L - J page 2 00 M O E-+ T11908 v Zn Pb2203 Sb2068 Se1960 Ppb 980.21 Ppm Ppm 1.087 Ppb 1010.0 Ppb -8.8435 Ppb 1032.8 3.47 .5085 .0012 .003 3.8 1.2347 5.0 .35440 .2282 .2672 .37220 13.962 .48664 979.53 .5088 1.086 1008.7 -7.8517 1035.6 983.97 .5094 1.090 1014.2 -8.4525 1035.8 977.12 .5072 1.084 1007.0 -10.226 1027.0 LC Pass LC Pass LC Pass LC Pass NOCHECK LC 1200.0 .6000 1.200 1200.0 1200ass 800.00 .4000 .8000 800.00 800.00 I L - J page 2 00 M O E-+ ialysis Report 09/28/05 11:38:19 AM page 1 �thod: CLP1 Sample Name: CCV4 in Time: 09/28/05 11:30:38 Ppm 2.547 PPM 2.535 PPM 2.597 PPM 53.26 AONC Corr. Factor: 1 .007 3lem Ag Al As1890 Jnits ppb ppm ppb Avge 999.41 51.78 527.70 SDev .60 .24 2.11 $RSD .06000 .4681 .39983 #1 999.26 52.01 527.52 #2 1000.1 51.80 529.89 #3 998.90 51.53 525.69 Errors LC Pass LC Pass LC Pass High 1100.0 55.00 550.00 Low 900.00 45.00 450.00 Elem Cd Co Cr Units PPM ppm PPM Avge 2.573 2.569 2.565 SDev .006 .008 .005 %RSD .2173 .3113 .1808 #1 2.567 2.560 2.559 #2 2.577 2.574 2.568 # 2.576 2.573 2.566 EOro rs LC Pass LC Pass LC Pass High 2.750 2.750 2.750 Low 2.250 2.250 2.250 Elem Mn Mo Na Units ppm 2.560 PPM 2.629 PPM 82.79 Avge SDev .005 .010 508.00 %RSD .1801 .3685 .6379 #1 2.554 2.618 83.32 #2 2.563 2.636 82.78 #3 2.562 2.635 82.26 Errors LC Pass NOCHECK LC Pass High 2.750 2.554 88.00 Low 2.250 72.00 Elem 2068/2 1960/1 1960/2 Units ppb Ppb Ppb Avge 977.62 530.82 529.75 SDev 4.07 4.65 3.28 %RSD .41642 .87569 .61925 Ppm 2.562 975.04 527.63 527.51 2.485 982.31 536.15 533.51 #3 975.50 528.68 528.22 Errors NOCHECK NOCHECK NOCHECK Operator: PES B Ba Be Ca Ppm 2.547 PPM 2.535 PPM 2.597 PPM 53.26 .003 .007 .007 .2796 .1052 .2636 .2248 2.539 2.537 2.589 53.13 2.553 2.537 2.600 53.37 2.550 2.532 2.601 53.29 LC Pass LC Pass LC Pass LC Pass 2.750 2.750 2.750 55.00 2.250 2.250 2.250 45.00 Cu Fe K Mg PPM 2.554 ppm 52.77 ppm 83.00 PPM 54.09 .09 .68 .13 .003 .1275 .1722 .8165 .2472 2.557 52.68 83.71 53.95 2.555 52.86 82.93 54.21 2.551 52.76 82.36 54.12 LC Pass LC Pass LC Pass LC Pass 2.750 55.00 88.00 55.00 2.250 45.00 72.00 45.00 Ni 2203/1 2203/2 2068/1 ppm Ppb Ppb Ppb 2.551 519.85 508.00 982.84 2.39 1.95 4.78 .005 .1953 .46066 .38291 .48603 2.546 517.10 505.77 977.44 2.555 520.98 508.85 984.59 2.554 521.46 509.37 986.50 LC Pass NOCHECK NOCHECK NOCHECK 2.750 2.250 Si Sn Sr Ti ppm Ppm 2.562 ppm 2.522 ppm 2.706 2.485 .011 .004 .009 .035 1.417 .4115 .1430 .3469 CN 2.450 2.550 2.524 2.716 2.486 2.567 2.523 2.704 O 2.520 2.569 2.518 2.697 NOCHECK NOCHECK NOCHECK NOCHECK • • page 2 09/28/05 11:38:19 AM ialysis Report sigh �o0 31em T11908 v Zn Pb2203 Sb2068 Se1960 ppb Jnits ppb 513.57 Ppm 2.574 Ppm 2.686 Ppb 511.94 Ppb 979.36 530.10 %vge 3Dev RSD .26424 .1000 .2296 .40914 .36947 .70475 R1 512.82 2.572 2.679 509.54 975.84 527.55 534.39 92 51.75 2.573 2.691 2.689 512.89 513.40 9.577 #7 79.1 528.37 3 51226 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 550.00 High 2.750 2.750 2.250 550-00 450.00 .0 9000 00 450.00 Low 4550-00 .00 2.250 • • page 2 zalysis Report 09/28/05 11:46:07 AM page 1 athod: CLP1 Sample Name: CCB4 an Time: 09/28/05 11:38:26 t: Ba Be Ca CONC Corr. Factor: 1 PPM .0003 Elem Ag Al As1890 Units ppb PPM ppb Avge -.57692 .0260 1.4257 SDev .12496 .0030 .2847 %RSD 21.660 11.47 19.968 #1 -.71977 .0272 1.5574 #2 -.52316 .0226 1.0990 #3 -.48784 .0282 1.6208 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units PPM PPM ppm Avge .0004 .0003 -.0000 SDev .0001 .0002 .0001 %RSD 27.27 71.94 17430. #1 .0005 .0002 .0001 #2 .0004 .0006 -.0001 # .0003 .0002 -.0000 E ors LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem Mn Mo Na Units PPM PPM PPM Avge .0002 .0051 .0655 SDev .0000 .0018 .0129 %RSD 11.16 34.08 19.69 #1 .0003 .0070 .0783 #2 .0003 .0049 .0657 #3 .0002 .0035 .0525 Errors LC Pass NOCHECK LC Pass High .0150 1.1868 5.000 Low -.0150 -.22112 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge -.11726 -.08872 1.7443 SDev 1.12325 2.57227 .6055 %RSD 957.88 2899.3 34.715 .54496 -.52230 2.3316 PPM .0004 -1.4142 2.6728 1.1220 #3 .51743 -2.4166 1.7794 Errors NOCHECK NOCHECK NOCHECK Operator: PES B Ba Be Ca Ppm PPM .0003 Ppm .0003 PPM .0552 .0033 .0000 .0001 .0034 .0017 51.48 16.23 24.04 6.246 .0003 .0003 .0529 .0053 .0002 .0003 .0536 .0027 .0020 .0002 .0002 .0592 LC Pass LC Pass LC Pass LC Pass .2000 .0050 .2000 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K Mg PPM -.0000 PPM .0120 PPM .0628 PPM .0198 .0007 .0065 .0033 .0002 1058. 6.147 10.39 16.55 .0126 .0696 .0171 .0001 .0112 .0621 .0189 .0001 -.0002 .0122 .0566 .0235 LC Pass LC Pass LC Pass LC Pass .1000 5.000 .2000 .0250 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 PPM ppb ppb ppb -.19837 -.03551 1.6849 .0001 1.10616 .29441 .4358 .0001 125.1 557.63 829.02 25.867 -1.3459 -.18936 1.9962 .0001 -.0000 .86114 .30395 1.1868 .0002 -.11033 -.22112 1.8716 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti PPM PPM PPM .0002 PPM .0004 .0350 .0013 .0003 .0001 .0002 .0090 25.63 21.31 19.76 38.16 .0015 .0003 .0006 �O ,G .0447 .0014 .0002 .0004 O .0332 .0010 .0002 .0003 0 .0271 NOCHECK NOCHECK NOCHECK NOCHECK ialysis Report 09/28/05 11:46:07 AM sigh 3o* 31em T11908 v Zn Pb2203 Sb2068 Se1960 Jnits ppb 4.1609 ppm PPM -.0001 Ppb -.08971 Ppb .48286 Ppb 1.1339 wge 3Dev 1.6260 .0004 .0003 .0001 .53825 .89329 .6637 kRSD 39.078 79.68 79.75 600.02 185.00 58.529 91 6.0246 .0007 -.0000 -.57446 1.0282 1.3812 42 3.0316 .0005 -.0001 .48953 -.54804 1.6384 93 3.4267 .0000 -.0003 -.18419 .96839 .38210 Errors LC Pass LC Pass LC Pass LC Pass LC Pass 60.000 LC Pass 5.0000 High 10.000 .0500 .0200 -.0200 3.0000 -3.0000 -60.000 -5.0000 Low -10.000 -.0500 • • page 2 ialysis Report 09/28/05 11:53:55 AM page 1 !thod: CLP1 Sample Name: MB-14893 Operator: PES in Time: 09/28/05 11:46:14 )m )dEWONC Corr. Factor: 1 31em Ag Al As1890 B Ba Be Ca 7nits kvge ppb -.05163 PPM -.0015 Ppb -.61852 Ppm -.0029 PPM -.0001 Ppm .0001 PPM -.0109 SDev .0029 1.02964 .0003 .0000 .0000 .0013 kRSD .54265 1050.9 199.5 166.47 10.23 43.29 65.88 12.39 #1 .0007 -.81836 -.0029 -.0001 .0001 .-.0093 f2 .56171 -.24730 -.0003 -1.5336 -.0026 -.0001 .0000 -.0115 *3 -.46932 -.0048 .49639 -.0032 -.0000 .0000 -.0118 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass Sigh 10.000 .2000 10.000 .2000 -.2000 .2000 -.2000 .0050 -.0050 .2000 -.2000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Cu Fe K Mg Units ppm Ppm -.0003 PPM PPM -.0000 PPM .0087 PPM .0415 PPM -.0029 Avge SDev .0001 .0003 .0001 .0003 .0002 .0009 .0061 .0037 %RSD .0001 58.53 99.94 358.5 21230. 10.89 14.76 127.3 #1 .0000 -.0001 ..0003 -.0001 .0096 .0484 .0013 #2 .0001 -.0006 -.0003 -.0001 .0087 .0368 -.0056 #3 .0001 -.0002 .0002 .0002 .0077 .0394 -.0043 Ergs LC Pass LC Pass LC Pass LC Pass LC Pass L2000ss High .0050 .0500 .0100 .0250 .1000 5C.000 .2000 Low -.0050 -.0500 -.0100 -.0250 -.1000 -5.000 -.2000 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm PPM PPM PPM Ppb Ppb .02439 Ppb 1.6673 Avge SDev .0003 .0020 .0004 .0242 .0056 .0002 .0005 .94748 .93255 .93114 1.0594 %RSD .0001 37.18 17.94 23.10 294.7 98.424 3818.1 63.543 #1 .0025 .0300 .0001 -.12632 .53810 2.3249 #2 .0004 .0019 .0238 -.0003 1.4147 .58552 2.2319 #3 .0002 .0003 .0018 .0189 .0007 1.5541 -1.0505 .44513 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High .0150 5.000 .0400 Low -.0150 -5.000 -.0400 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb 1.1035 PPM -.0170 PPM .0113 PPM -.0003 PPM .0012 Avge 2.0595 -2.8113 1.6789 .0016 .0006 .0001 .0002 SDev %RSD .4187 20.330 .5278 18.774 152.14 9.621 4.927 24.76 14.89 # 1.8555 -2.3285 -.58926 -.0153 .0115 -.0002 .0014 $� 2.5411 -2.7306 1.1316 2.7683 -.0169 -.0186 .0107 .0117 -.0003 -.0003 .0010 .0013 #3 1.7819 -3.3748 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK zalysis Report 09/28/05 11:53:55 AM sigh ilo 3l0 snits kvge 3Dev 9RSD 41 42 43 3rror Sigh Low • [7 page 2 T11908 v Zn Pb2203 Sb2068 Se1960 ppb ppm ppm ppb ppb ppb .19609 .0003 .0040 .33182 1.9289 -.20010 .81344 .0003 .0001 .52256 .5553 .94635 414.82 99.14 3.119 157.48 28.790 472.93 -.16259 .0004 .0039 .31689 2.0118 -1.1684 -.37636 -.0000 .0038 .86168 2.4381 -.15450 1.1272 .0004 .0041 -.18312 1.3368 .72262 s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 10.000 .0500 .0200 3.0000 60.000 5.0000 -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 [7 page 2 09/28/05 12:01:42 PM page 1 ialysis Report !thod: CLP1 Sample Name: LCS-14893 Operator: PES in Time: 09/28/05 11:54:01 )m t : AWONC Corr. Factor: 1 31em Ag Al As1890 B Ba Be Ca PPM 7nits ppb PPM Ppb 1623.7 PPM PPM 2.526 PPM .9480 33.26 kvge 1394.7 64.64 .8143 kRSDDev �SRSD .28 747 .9513 .10640 .2169 .3633 .0606 .1661 11 1397.4 65.06 1622.9 .8133 2.535 .9483 33.28 33.20 #2 1390.1 63.93 1625.7 .8133 2.516 2.526 .9474 .9484 33.30 #3 1396.6 64.92 1622.6 .8164 Elem Cd Co Cr Cu Fe K PPM Mg PPM 7nits ppm PPM PPM PPM 1.464 PPM 124.5 18:33 98 20,03 kvge SDev 1.254 .001 .3434 .0002 .7008 .0007 .007 .2 WRSD .0744 .0670 .1052 .4647 .1512 1.766 .1660 91 1.255 .3432 .7014 1.468 124.7 18.86 18.26 20.96 20.96 #2 1.254.3436 .7000 1.456 1.468 124.3 124.5 18.80 21.02 #3 1.254 .3436 .7010 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm PPM PPM PPM Ppb 1423.7 Ppb 1406.9 ppb 30 585:46 Av a 3.922 .8502 4.514 1.444 9.8 2.0 S $ .005 .1366 .0008 .0943 .058 1.294 .003 .1964 .68660 .14155 .07783 #1 3.925 .8495 4.544 1.447 1414.3 1433.8 1407.9 1408.2 584.82 585.35 #2 3.916 .8500 4.447 4.552 1.441 1.444 1422.9 1404.6 585.73 #3 3.925 .511 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti PPM Units ppb ppb ppb 630.71 PPM 2.859 PPM .5503 PPM .7768 3.521 Avge 586.10 625.99 SDev $RSD 4'49 .76667 .69602 .15580 1.051 .3920 .5513 .5631 #1 582.37 626.74 630.86 2.892 .5480 .7805 3.543 3.504 #2 591.09 629.92 629.66 631.61 2.833 2.853 .5505 .5523 .7721 .7777 3.516 ##3 584.84 621.30 Elem T11908 v Zn Pb2203 Sb2068 Se11960 PP Units ppb PPM PPM 1.705 ppb 1412.5 ppb 585.83 629:184 Avge 875.66 2.18 .9576 .001 3.7 3.05 SDev %RSD .24839 .0024 .2504 .0682 .26142 .52141 .13370 #1 873.33 .9595 1.704 1410.0 583.19 589.17 629.49 629.75 #2 876.03 .9549 1.704 1.706 1416.7 1410.7 585.14 628.18 877.63 .9584 09/28/05 12:09:30 PM page 1 nalysis Report ethod: CLP1 Sample Name: 0509758-004A Operator: PES un Time: 09/28/05 12:01:49 pt: o CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca PPM Units ppb RPM 30.445 PPM PPM .5071 PPM .0023 166.2 Avge 2.0009 40.51 1.294 .0427 .0004 .0013 .0001 SDev %RSD .1381 6.8996 .15 .3625 4.2518 .9871 .2631 4.762 .1255 #1 2.1408 40.56 31.677 .0427 .5082 .0024 166.6 #2 1.9971 40.62 29.096 .0431 .5074 .0023 .166.9 166.5 #3 1.8648 40.34 30.562 .0422 .5056 .0022 Elem Cd Co Cr Cu Fe K PPM Mg PPM Units ppm PPM PPM PPM 1.112 PPM 193.5 7.155 77:20 Avge SDev .0107 .0001 .0482 .0005 .3270 .0003 .003 .4 .036 %RSD 1.235 .9463 .0963 .3012 .1986 .5028 .2637 #1 .0107 .0480 .3270 1.113 193.7 7.164 7.185 77.61 77.85 #2 .0109.0488 .3273 1.115 1.109 193.8 193.1 7.115 77.44 #3 .0106 _0479 .3266 Na Ni 2203/1 2203/2 2068/1 Elem Mn Mo PPM Ppb Ppb Ppb Units ppm 1.754 PPM PPM 3.510 .2693 3926.4 3911.6 20.085 A .002 .0237 .0008 .020 .0006 8.9 6.6 1.141 5.6790 .1419 3.162 .5612 .2081 .22652 .16878 #1 1.755 .0241 3.511 .2694 3917.7 3917.0 3913.6 20.761 18.768 #2 1.756 .0228 3.529 7 3935.4 3926.1 3904.2 20.725 #3 1.752 3.489 .268 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti PPM Units ppb Ppb Ppb 3.0667 PPM 3.031 PPM .2568 PPM .2294 2.614 Avge 20.501 -1.8591 0 .0021 14 106 .004 SDev %RSD 1 7.3277 35.499 329428 .20945 05 .8279 .66 .1609 #1 18.838 -1.8024 2.4855 3.035 .2547 .2288 2.619 2.613 #2 21.760 -1.2294 4.2151 3.035 3.024 .2590 .2310 .2284 2.611 #3 20.904 -2.5456 2.4997 .2568 Elem T11908 v Zn Pb2203 Sb2068 Se1960 ppb Units ppb PPM ppm 3.804 ppb 3916.5 ppb 20.362 1.4264 Avge -4.7711 .1972 533 SDev %RSD 3 4.4223 :0000 .1905 .04293 3.7641 598819 #1 -3.6120 .1976 3.803 3917.2 19.478 20.764 1.0576 2.4021 #2 -4.0508 .1971 3.811 3.797 3917.8 3914.6 20.845 .81960 0 -6.6505 .1968 O M O Cn F-4 09/28/05 12:17:17 PM page 1 zalysis Report �thod: CLP1 Sample Name: 0509758-004ADUP Operator: PES in Time: 09/28/05 12:09:36 DRIat: ANWONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca PPM Units ppb Ppm Ppb 24.568 PPM PPM .5819 PPM •0022 142.36 Avge .71941 50.55 1.319 .0254 .0010 .0017 .0000 SDev %RSD .13501 18.767 .56 1.109 5.3684 3.996 .2886 .1276 .4375 #1 .57430 50.64 25.973 .0256 .5801 .0022 141.6 142.6 #2 .74263 49.96 24.373 .0242 .5821 .0022 142.8 #3 .84130 51.07 23.357 .0262 .5835 .0022 Elem Cd Co Cr Cu Fe K PPM Mg PPM Units ppm PPM PPM PPM PPM 218.6 6.766 58.65 Avge SDev .0092 .0427 .0002 .2376 .0011 .9047 .0051 .9 .144 •27 %RSD .0001 .7934 .4973 .4496 .5645 .4212 2.123 .4587 #1 .0091 .0425 .2364 .9033 217.5 6.811 6.605 58.39 58.62 #2 .0091 .0429 .2377 .9005 219.1 219.2 6.881 58.93 #3 .0093 .0426 .2385 .9104 Na Ni 2203/1 2203/2 2068/1 Elem Mn Mo Ppb Ppb ppb Units ppm PPM PPM 3.022 PPM .1551 4222.0 4183.1 12.338 A S 2.107 .0108 911382 9 .009 .4225 30004 1.968 .2991 .54010 .42274 #1 2.097 .0113 3.034 .1546 4201.4 4246.5 4162.7 4192.1 11.452 13.607 #2 2.111.0106 2.958 3.075 .1555 4218.2 4194.4 11.955 #3 2.113 _0106 .1552 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti PP m Units ppb ppb ppb PPM 1.283 PP M .3217 PPM .4176 1.937 Avge 13.828 -1.5530 .78004 1.0549 .011 .0022 .0014 .003 SDev %RSD 1.075 7.7762 .5354 34.478 135.23 .8766 .6891 .3462 .1667 #1 13.245 -1.8935 1.0407 1.285 .3192 .4159 1.933 1.938 #2 13.170 -.93580 -.38071 1.271 1.293 .3235 .4182 .4186 1.940 #3 15.069 -1.8296 1.6801 .3224 Elem T11908 v Zn Pb2203 Sb2068 Se1960 ppb Units ppb PPM PPM 3.685 ppb 4196.0 ppb 13.332 .00316 Avge -7.2429 1.0649 .1678 .016 18.2 .692 .54102 SDev RSD 14.702 .0010 .6158 .4303 .43283 5.1917 17146. #1 -6.5385 .1669 3.667 4175.6 12.648 13.316 .06362 6 #2 -6.7223 .1678 3.691 3.697 4210.2 4202.3 14.032 .51141 0 -8.4679 _1689 O M O Cn F-4 00 O M O H 09/28/05 12:25:05 PM page 1 -ialysis Report sthod: CLP1 Sample Name: 0509758-004AMS Operator: PES 1n Time: 09/28/05 12:17:24 AONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca PPM Jnits ppb Ppm Ppb 79.591 PPM PPM 2.764 PPM .0524 233.7 kvge 53.597 52.03 .0375 762 $009 0 4.4 SDev RSD •705 49 1.311796 1.7207 214574 3.956 0233 1.012 149 1.900 #1 52.905 51.05 77.337 .0362 2.715 .0515 229.0 237.9 #2 54.314 52.81 80.598 .0386 2.812 2.7 67 .0533 .0525 234.1 #3 53.571 52.24 80.838 .0376 Elem Cd Co Cr Cu Fe K PPM Mg PPM Units ppm PPM PPM PPM 2.544 PPM 253.6 12.55 112.4 Avge SDev .0626 .5439 .0100 .6150 .0111 .046 4.9 .20 2.1 1.856 %RSD .0011 1.694 1.845 1.807 1.794 1.934 1.613 #1 .0614 .5335 .6035 2.495 248.7 12.32 12.68 110.2 114.4 #2 .0635.5535 .6257 2.586 2.549 258.5 253.8 12.65 112.6 #3 .0628 .5446 .6157 Na Ni 2203/1 2203/2 2068/1 Elem Mn Mo PPM Ppb Ppb Ppb Units ppm PPM PPM 4.328 .7252 5718.1 5686.4 279.30 Av S 2.787 .0180 .0005 .077 .0136 59.3 95.8 5.76 2.0631 %R .651 1.818 2.878 1.781 1.871 1.0369 1.6839 #1 2.735 .0177 4.241 .7110 5668.3 5783.7 5592.1 5783.5 273.53 285.05 #2 2.836 4.387 4.356 .7380 5702.4 5683.6 27 9.34 #3 2.790 _0186 8 .7266 Elem 2068/2 1960/1 1960/2 Si Sn Sr PPM Ti PPM Units pp ppb b Ppb 8.9822 PPM 2.234 PPM .2596 .2992 4.095 Avge 284.04 7.6654 .034 062 .064 SDev 3.26 .2638 3.4416 .6072 6.7603 1.508 10893 2049 .0%56 1.575 #1 281.33 7.4454 8.3948 2.198 .2547 .2927 4.029 4.158 #2 287.66 7.9579 9.6075 8.9443 2.264 2.239 .2645 .2596 .3048 .3002 4.096 #3 283.14 7.5929 Elem T11908 v Zn Pb2203 Sb2068 - Se1960 ppb Units ppb PPM PPM 8.136 Ppb 5696.9 Ppb 282.47 8.5437 Avge 37.612 2.362 .7344 .148 83.3 4.06 .4916 SDev %RSD 6.2809 10134 819 1.823 1.4620 1.4386 5.7541 #1 34.887 .7202 7.984 5617.4 278.73 286.79 8.0787 9.0582 #2 39.074 .7466 8.280 8.145 5783.6 5689.8 281.87 8.4943 0 38.877 .7366 00 O M O H Re ort 09/28/05 12:32:52 PM ►alysis p -thod: CLP1 Sample Name: 0509758-002A in Time: 09/28/05 12:25:11 >ONC Corr. Factor: 1 Clem Ag Al As1890 B hits ppb ppm ppb ppm kvge 3.1024 46.62 41.647 .0512 Mev .3108 .16 .616 .0003 MSD 10.019 .3467 1.4796 .6433 11 3.1005 46.74 41.334 .0512 #2 2.7925 46.43 41.249 .0516 #3 3.4142 46.68 42.356 .0509 3lem Cd Co Cr Cu Jnits ppm PPM PPM PPM kvge .0137 .0613 .4203 1.135 3Dev .0002 .0001 .0013 .003 $RSD 1.432 .2163 .3.177 .2208 41 .0137 .0614 .4202 1.134 92 .0135 .0611 .4190 1.133 93 .0139 .0613 .4217 1.138 Elem Mn Mo Na Ni Units ppm PPM ppm PPM Av 2.431 .0265 4.570 .2632 S .011 .0003 .004 .0018 $R .4374 1.010 .0962 .6854 #1 2.428 .0265 4.571 .2647 #2 2.422 .0262 4.565 .2612 #3 2.442 .0267 4.574 .2638 Elem 2068/2 1960/1 1960/2 Si Units ppb Ppb ppb PPM Avge 14.773 -4.8240 1.2852 2.104 SDev 2.680 .5736 2.5688 .009 %RSD 18.141 11.890 199.88 .4144 #1 15.643 -4.6559 -1.6807 2.109 ##2 16.910 -4.3533 2.7282 2.094 #3 11.766 -5.4629 2.8081 2.109 Elem T11908 v Zn Pb2203 Units ppb PPM ppm ppb Avge -5.2551 .2689 5.996 14981. SDev 1.9207 .0014 •027 82. %RSD 36.550 .5283 .4554 .54992 #1 -7.3960 .2691 5.987 14976. #2 -3.6833 .2673 5.974 14901. ie -4.6859 .2701 6.026 15065. Operator: PES Ba ppm .7919 .0027 .3409 .7914 .7895 .7948 Fe PPM 408.2 2.3 .5646 408.0 406.1 410.7 2203/1 ppb 14990. 99. .65733 14959. 14910. 15100. Sn PPM .4999 .0038 .7618 .4990 .4967 .5041 Sb2068 ppb 13.443 1.354 10.071 13.518 14.758 12.053 Be PPM .0017 .0000 1.468 .0017 .0017 .0017 K PPM 8.066 .044 .5495 8.114 8.026 8.058 2203/2 ppb 14976. 76. .50952 14984. 14896. 15048. Sr ppm .1955 .0024 1.217 .1944 .1939 .1982 Se1960 ppb -.74916 1.67220 223.21 -2.6714 .37007 .05385 page 1 Ca PPM 144.0 .7 .5127 144.0 143.3 144.8 Mg PPM 66.11 .26 .3862 66.05 65.89 66.39 2068/1 ppb 10.779 1.708 15.843 9.2614 10.447 12.628 Ti PPM 3.560 .015 .4298 3.565 3.543 3.572 ialysis Report 09/28/05 12:40:40 PM page 1 -thod: CLP1 Sample Name: CCV5 Operator: PES in Time: 09/28/05 12:32:59 AdWONC Corr. Factor.: 1 slem Ag Al As1890 B Ba Be Ca Jnits ppb Ppm Ppb Ppm PPM PPM PPM kvge 995.25 51.56 524.96 2.537 2.516 2.584 53.00 Mev .67 .31 2.31 .009 .002 .007 .11 kRSD .06755 .6050 .44085 .3483 .0786 .2607 .2032 11 994.73 51.33 523.15 2.527 2.514 2.582 52.92 12 996.01 51.91 524.15 2.540 2.517 2.579 52.96 13 995.01 51.43 527.57 2.544 2.518 2.592 53.12 3rrors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass sigh 1100.0 55.00 550.00 2.750 2.750 2.750 55.00 mow 900.00 45.00 450.00 2.250 2.250 2.250 45.00 3lem Cd Co Cr Cu Fe K Mg Jnits kvge ppm 2.565 PPM 2.550 PPM 2.553 PPM 2.532 PPM 52.73 PPM 82.16 PPM 53.78 3Dev .007 .004 .006 .08 .87 .09 RSD .006 .2281 .2676 .1524 .2292 .1442 1.055 .1696 91 2.565 2.546 2.550 2.527 52.69 81.56 53.71 R2 2.559 2.546 2.551 2.538 52.67 83.15 53.75 93 2.571 2.558 2.557 2.531 52.81 81.76 53.88 Erks LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass High 2.750 2.750 2.750 2.750 55.00 88.00 55- 00 Low 2.250 2.250 2.250 2.250 45.00 72.00 45.00 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm 2.619 PPM 82.35 PPM 2.542 Ppb 520.54 Ppb 511.58 ppb 971.19 Avge SDev 2.548 .006 .85 .004 2.89 .87 2.13 %RSD .005 .1777 .2453 1.037 .1499 .55542 .16997 .21881 #1 2.545 2.617 81.85 2.540 521.59 510.64 969.33 #2 2.546 2.614 83.34 2.539 517.27 511.75 970.73 #3 2.553 2.626 81.86 2.546 522.76 512.35 973.50 Errors LC Pass NOCHECK LC Pass LC Pass NOCHECK NOCHECK NOCHECK High 2.750 88.00 2.750 Low 2.250 72.00 2.250 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb 524.17 PPM 2.536 PPM 2.531 PPM 2.498 PPM 2.743 Avge 970.56 528.64 3.88 .027 .009 .005 .003 SDev %RSD 1.41 .14533 .73302 .63 .12108 1.064 .3430 .1931 .1116 968.93 525.28 523.44 2.505 2.527 2.493 2.744 2.740 971.39 527.77 524.61 2.550 2.526 2.502 2.500 2.746 #3 971.36 532.88 524.46 2.553 2.541 Errors NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK NOCHECK nalysis Report 09/28/05 12:40:40 PM page 2 High Pb2203 Sb2068 Loif Ppm Ppb Elem T11908 v Units ppb PPM Avge 506.26 2.558 SDev 2.46 .004 %RSD .48589 .1653 #1 505.63 2.554 #2 504.19 2.558 #3 508.98 2.563 Errors LC Pass LC Pass High 550.00 2.750 Low 450.00 2.250 • Zn Pb2203 Sb2068 Se1960 Ppm Ppb Ppb Ppb 2.670 514.56 970.77 525.66 1.14 1.54 1.61 .006 .2116 .22159 .15913 .30551 2.667 514.28 969.06 524.05 2.667 513.59 971.17 525.66 2.677 515.82 972.07 527.26 LC Pass LC Pass LC Pass LC Pass 2.750 550.00 1100.0 550.00 2.250 450.00 900.00 450.00 cn O zalysis Report 09/28/05 12:51:29 PM page 1 E!thod: CLP1 Sample Name: CCB5 in Time: 09/28/05 12:43:47 ppm .0003 Ppm .0001 ppm .0829 .0021 .0001 :)ONC Corr. Factor: 1 .0009 43.12 Elem Ag Al As1890 Units ppb ppm ppb avge .-.75234 .0001 .0098 1.4363 SDev .24870 .0071 1.5559 %RSD 33.056 72.76 108.33 #1 -.46521 .0171 3.0044 #2 -.89987 .0093 -.10723 #3 -.89195 .0029 1.4117 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge .0002 -.0000 -.0000 SDev .0001 .0001 .0003 %RSD 45.56 333.2 1153. #1 .0002 .0001 .0003 #2 .0001 -.0001 -.0002 #3 .0002 -.0001 -.0002 2.2789 1.8304 .73393 .0002 Er3brs LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Eleni Mn Mo Na Units ppm ppm PPM Avge SDev .0004 .0002 .0026 .0008 .0339 .0066 %RSD 64.79 29.09 19.53 #1 .0006 .0031 .0410 #2 .0003 .0030 .0329 #3 .0002 .0017 .0279 Errors LC Pass NOCHECK LC Pass High .0150 34.79 5.000 Low -.0150 .0012 -5.000 Elem 2068/2 1960/1 1960/2 Units ppb Ppb Ppb Avge .47921 1.1895 .34945 SDev 1.6589 .8555 1.2960 %RSD 346.17 71.916 370.87 1.6784 .21733 1.1518 0 -1.4140 1.8271 -1.1457 #3 1.1732 1.5242 1.0423 Errors NOCHECK NOCHECK NOCHECK Operator: PES B Ba Be Ca Ppm ppm .0003 Ppm .0001 ppm .0829 .0021 .0001 .0001 .0063 .0009 43.12 52.92 72.34 7.606 .0004 .0002 .0896 .0031 .0002 .0001 20 .0871 .0020 .0013 .0002 .0000 LC Pass LC Pass LC Pass LC Pass .2000 .0050 .2000 -.2000 -.2000 -.0050 _2000 2000 Cu Fe K Mg ppm -.0003 ppm .0303 ppm .0441 ppm .0057 .0108 .0065 .0054 .0002 79.27 35.67 14.82 94.96 -.0000 .0404 .0516 .0119 -.0004 .0316 .0396 .0036 -.0005 .0189 .0412 .0017 LC Pass LC Pass LC Pass LCPass .1000 5.000 .2000 .0250 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm Ppb Ppb Ppb 2.2789 1.8304 .73393 .0002 .4002 .5465 .55299 .0003 148.1 17.562 29.855 75.347 2.7175 1.9060 1.3630 .0003 2.1856 2.3352 .32472 .0003 -.0001 1.9335 1.2501 .51403 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti ppm Ppm ppm .0002 PPM .0009 .0249 .0006 .0002 .0001 .0003 .0055 22.20 37.99 63.13 34.79 .0008 .0003 .0012 .0302 .0005 .0001 .0009 .0253 .0192 .0004 .0001 .0006 NOCHECK NOCHECK NOCHECK NOCHECK lalysis Report 09/28/05 12:51:29 PM Sigh �o T11908 v Zn Pb2203 Sb2068 Se1960 31em Jnits ppb 2.3745 ppm ppm .0010 ppb 1.9798 ppb .56405 ppb .62920 kvge SDev 1.8264 .0000 .0004 .0002 .4382 1.2506 .70351 $RSD 76.917 970.3 21.52 22.135 221.71 111.81 #1 3.4173 .0005 .0013 2.1763 1.5734 .84062 #2 .26562 -.0003 .0011 2.2854 -.83496 -.15578 #3 3.4406 -.0000 .0008 1.4777 .95371 1.2028 Errors LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 5.0000 High 10.000 .0500 .0200 3.0000 -3.0000 60.000 -60.000 -5.0000 Low -10.000 -.0500 -.0200 page 2 M M O h ialysis Report 09/28/05 12:59:17 PM page 1 �thod: CLP1 Sample Name: CRI in Time: 09/28/05 12:51:35 )mt : )dONC Corr. Factor: 1 ;leen Ag Al As1890 Jnits ppb ppm ppb wge -.22997 .0505 2119.9 >Dev .14424 .0027 12.1 kRSD 62.721 5.416 .57153 #1 -.07465 .0530 2106.2 #2 -.25557 .0511 2124.8 *3 -.35970 .0476 2128.9 3lem Cd Co Cr Jnits ppm PPM PPM kvge .2128 .0068 2.079 SDev .0008 .0003 .008 $RSD .3878 5.147 .3952 R1 .2119 .0064 2.070 92 .2134 .0070 2.083 43 .2131 .0069 2.085 Elem Mn Mo Na Units ppm PPM PPM Av .0001 .0010 .1082 S .0001 .0003 .0014 $ 88.54 24.57 1.267 #1 .0001 .0008 .1093 #2 .0001 .0013 .1085 #3 .0000 .0011 .1066 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge .43004 214.50 212.80 SDev 1.0790 2.80 1.85 %RSD 250.90 1.3071 .86835 #1 1.6673 211.30 211.10 #2 -.31516 215.70 214.77 #3 -.06207 216.51 212.52 Elem T11908 v Zn Units ppb PPM ppm Avge 1.3775 .0003 .0007 SDev 1.3729 .0001 .0001 %RSD 99.669 35.82 20.50 #1 -.12325 .0004 .0008 #2 1.6854 .0002 .0006 0 2.5703 .0004 .0006 B ppm .1286 .0012 .9443 .1272 .1293 .1294 Cu PPM -.0011 .0001 7.693 -.0012 -.0011 -.0011 Ni PPM .0005 .0006 125.3 .0001 .0011 .0002 Si PPM .5957 .0009 .1545 .5964 .5961 .5947 Pb2203 ppb 2096.0 13.4 .63816 2082.6 2096.2 2109.3 Operator: PES Ba ppm 20.38 .03 .1329 20.35 20.38 20.40 Fe PPM .0070 .0051 72.67 .0125 .0061 .0024 2203/1 ppb 2091.2 9.7 .46492 2080.8 2092.8 2100.0 Sn PPM .0005 .0005 100.4 .0011 .0001 .0004 Sb2068 ppb 1.4503 1.0924 75.323 2.6994 .97837 .67319 Be PPM -.0000 .0000 130.4 -.0000 -.0000 -.0001 K PPM .0376 .0006 1.656 .0383 .0371 .0374 2203/2 ppb 2098.4 15.3 .72709 2083.5 2097.8 2114.0 Sr .0PPM 001 .0000 28.23 .0001 .0001 .0001 Se1960 ppb 213.37 2.00 .93700 211.17 215.08 213.85 Ca PPM .0461 .0027 5.971 .0491 .0453 .0438 Mg PPM -.0037 .0011 30.23 -.0046 -.0025 -.0041 2068/1 ppb 3.4939 1.3119 37.548 4.7664 3.5692 2.1459 Ti •0PPM 012 .0000 2.125 .0012 .0012 .0012 ialysis Report �thod: CLP1 Sample Name: MB -1489E in Time: 09/28/05 12:59:23 >nigot: AONC Corr. Factor: 1 3lem Ag Al As1890 Jnits ppb ppm ppb kvge -.47928 -.0156 1.2992 SDev .19597 .0009 .1858 kRSD 40.888 5.851 14.303 $1 -.25623 -.0161 1.4696 f2 -.62382 -.0161 1.3269 13 -.55780 -.0145 1.1011 3rrors LC Pass LC Pass LC Pass Sigh 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Jnits ppm ppm ppm kvge .0000 -.0003 -.0000 SDev .0001 .0001 .0003 WRSD 284.8 49.11 27600. al .0001 -.0003 .0001 ff2 -.0001 -.0005 -.0004 43 .0000 -.0002 .0002 LC Pass LC Pass LC Pass LC Pass EOrs LC Pass LC Pass LC Pass High .0050 .0500 .0100 Low -.0050 -.0500 -.0100 Elem Mn Mo Na Units ppm ppm ppm Avge -.0001 .0008 .0119 SDev .0001 .0005 .0006 $RSD 139.6 63.84 5.003 #1 -.0001 .0004 .0125 #2 -.0003 .0006 .0119 #3 .0000 .0014 .0113 Errors LC Pass NOCHECK LC Pass High .0150 5.000 Low -.0150 Sr -5.000 Elem 2068/2 1960/1 1960/2 Units ppb Ppb ppb Avge .84494 2.1744 .20937 SDev 1.6625 1.4471 .11798 %RSD 196.76 66.554 56.349 .0088 .0078 -.57492 1.7232 .18877 0 2.6738 1.0066 .33629 a., .43593 3.7934 .10305 Errors NOCHECK NOCHECK NOCHECK 09/28/05 01:07:05 PM page 1 Operator: PES B Ba Be Ca m m -.0001 PPM -.M 0021 •0028 -•0289 .0001 .0011 .0000 .0005 6.659 37.93 6.245 1.764 -.0022 .0040 -.0001 -.0286 -.0022 .0025 -.0001 -.0295 -.0019 .0019 -.0001 -.0286 LC Pass LC Pass LC Pass LC Pass .2000 .2000 .0050 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K Mg PPM PPM PPM PPM -.0005 -.0010 .0283 -.0073 .0001 .0009 .0092 .0032 15.24 88.88 32.68 43.54 -.0006 .0000 .0289 -.0090 -.0004 -.0016 .0187 -.0093 -.0005 -.0013 .0372 -.0036 LC Pass LC Pass LC Pass LC Pass .1000 5.000 .2000 .0250 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 PPM Ppb Ppb Ppb -.0004 4.5051 3.5015 .87653 .8361 .7784 1.3709 .0001 32.89 18.559 22.229 156.40 -.0005 3.7911 3.7671 1.6820 -.0003 4.2993 4.1122 1.6539 -.0003 5.4249 2.6251 -.70638 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti PPM PPM -.0006 PPM -.0004 PPM .0001 .0089 .0004 .0001 .0001 .0011 12.61 77.02 15.09 101.7 -.0001 -.0004 .0001 .0100 -.0009 -.0004 .0000 .0088 .0078 -.0008 -.0003 .0002 NOCHECK NOCHECK NOCHECK NOCHECK M O C/ F-4 malysis Report 09/28/05 01:07:05 PM High Low E& T11908 V Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge 1.1909 .0001 -.0001 H3.8357 .85548 .86373 SDev 1.3316 .0001 .0001 .3130 1.2820 .41150 %RSD 111.81 173.4 156.1 8.1597 149.86 47.643 #1 2.7278 .0002 .0000 H3.7752 .17667 .69972 #2 .46154 .0000 -.0002 H4.1746 2.3342 .55952 #3 .38333 -.0000 -.0000 H3.5575 .05556 1.3319 Errors LC Pass LC Pass LC Pass LC High LC Pass LC Pass High 10.000 .0500 .0200 3.0000 60.000 5.0000 Low -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • page 2 nalysis Report 09/28/05 01:14:53 PM page 1 :ethod: CLP1 Sample Name: MB1-14898 Operator: PES .un Time: 09/28/05 13:07:11 o t: ;ocwCONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm Ppb 10.306 PPM PPM PPM -.0000 PPM .0157 Avge SDev .24020 -.0059 .0013 .398 .0128 .0001 .0018 .0002 .0000 .0002 %RSD .12975 54.017 21.77 3.8654 .9294 12.98 221.1 1.223 #1 .11018 -.0047 10.303 .0128 .0020 .0000 .0155 #2 .24075 -.0072 10.706 .0130 .0017 -.0000 .0159 #3 .36968 -.0056 9.9096 .0127 .0016 -.0000 .0156 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM PPM .0116 PPM 1.109 PPM .0028 Avge SDev .0001 -.0002 .0001 .0005 .0002 .0007 .0000 .0001 .008 .0016 %RSD .0001 135.3 53.35 31.56 2.654 1.215 .7644 55.13 #1 .0000 -.0001 .0007 .0007 .0117 1.115 .0041 #2 -.0000 -.0002 .0003 .0007 .0115 1.113 1.100 .0011 .0033 #3 .0002 -.0004 .0005 .0007 .0116 Mo Na Ni 2203/1 2203/2 2068/1 Elem Units Mn ppm PPM PPM PPM PPb 3.3669 Ppb 3.3216 Ppb 1.0621 A v a .0002 .0005 1269. 5. .0009 .9679 .9350 2.6083' S $ .0001 23.09 .0003 52.93 .3795 .0005 52.06 28.749 28.150 245.57 #1 .0003 .0004 1274. .0014 3.3505 2.5042 4.3412 3.7428 #2 .0002 .0008 1269. .0009 2.4072 4.3429 3.1195 .91083 -1.4672 #3 .0002 .0003 1264. .0005 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb 10.090 PPM PPM -.0009 PPM -.0000 PPM .0005 Avge -1.2737 1.1053910 11.378 1.546 2.164 .0368 .0003 0 0 000 01 SDev $RSD 13.587 21.450 .8961 5 11701 350130 100 81 #1 -.81648 10.877 10.073 .0367 .0003 -.0017 -.0000 -.0000 .0005 .0005 #2 -.21273 13.113 10.145 12.263 7.9341 .0372 .0366 -.0015 -.0001 .0004 #3 -2.7919 Elem T11908 v Zn Pb2203 Sb2068 Se1960 ppb Units ppb PPM PPM .0015 ppb 3.3367 ppb -.49586 10.519 Avge SDev -1.7855 .0001 .0002 .0001 .4844 1.62896 1.944 %RSD .0932 5.2222 309.8 9.481 14.518 328.51 18.478 #1 -1.8839 .0001 .0014 2.7861 .70177 10.341 12.546 #2 -1.6984 .0002 .0015 3.6972 3.5269 .16142 -2.3508 8.6704 # i -1.7742 -.0001 .0017 nalysis Report =thod: CLP1 Sample Name: LCS-14898 an Time: 09/28/05 13:14:59 t: aONC Corr. Factor: 1 09/28/05 01:22:41 PM page 1 Operator: PES Elem Ag Al As1890 B Units ppb ppm ppb ppm Avge 941.29 48.58 490.95 2.229 SDev 1.73 .17 .66 .007 %RSD .18405 .3551 .13419 .3354 ##1 940.33 48.59 491.39 2.224 ##2 943.29 48.75 491.26 2.237 ##3 940.26 48.40 490.19 2.225 Errors LC Pass LC Pass LC Pass LC Pass High 1200.0 60.00 600.00 3.000 Low 800.00 40.00 400.00 2.000 Elem Cd Co Cr Cu Units ppm ppm ppm ppm Avge 2.413 2.402 2.422 2.399 SDev .003 .006 .003 .006 %RSD .1312 .2331 .1421 .2608 ##1 2.412 2.398 2.420 2.398 #2 2.416 2.408 2.426 2.406 #3 2.410 2.399 2.421 2.394 EAs LC Pass LC Pass LC Pass LC Pass High 3.000 3.000 3.000 3.000 Low 2.000 2.000 2.000 2.000 Elem Mn Mo Na Ni Units ppm PPM PPM ppm Avge 2.411 2.483 76.66 2.402 SDev .004 .008 .47 .003 %RSD .1566 .3073 .6088 .1434 #1 2.409 2.475 76.65 2.404 #2 2.416 2.490 77.13 2.403 #3 2.409 2.483 76.20 2.398 Errors LC Pass NOCHECK LC Pass LC Pass High 3.000 96.00 3.000 Low 2.000 64.00 2.000 Elem 2068/2 1960/1 1960/2 Si Units ppb Ppb Ppb PPM Avge 926.73 471.13 474.71 1.649 SDev 2.21 2.02 2.26 .025 %RSD .23878 .42948 .47545 1.527 924.44 473.40 476.27 1.622 *,,3 928.85 469.53 472.12 1.655 926.90 470.44 475.73 1.671 Errors NOCHECK NOCHECK NOCHECK NOCHECK Ba PPM 2.381 .004 .1661 2.381 2.384 2.376 LC Pass 3.000 2.000 Fe ppm 50.46 .07 .1444 50.41 50.55 50.43 LC Pass 60.00 40.00 2203/1 ppb 494.12 1.12 .22596 494.20 495.20 492.97 NOCHECK Sn PPM 2.398 .005 .2132 2.394 2.404 2.398 NOCHECK Be PPM 2.431 .003 .1383 2.428 2.435 2.430 LC Pass 3.000 2.000 K PPM 77.05 .30 .3897 77:14 77.29 76.71 LC Pass 96.00 64.00 2203/2 ppb 482.78 .95 .19678 481.68 483.34 483.31 NOCHECK Sr PPM 2.372 .004 .1515 2.373 2.374 2.368 NOCHECK Ca PPM 50.42 .09 .1703 50.35 50.51 50.38 LC Pass 60.00 40.00 Mg ppm 50.35 .14 .2821 50.25 50.51 50.28 LC Pass 60.00 40.00 2068/1 ppb 929.38 1.49 .16044 927.66 930.09 930.37 NOCHECK Ti PPM 2.626 .004 .1678 2.629 2.627 2.621 NOCHECK 00 M O E-� zalysis Report 09/28/05 01:22:41 PM Sigh Loo El em Units avge SDev WRSD #1 #2 #3 Error High Low • • page 2 M O V) H T11908 v Zn Pb2203 Sb2068 Se1960 Ppb 477.50 ppm 2.428 ppm 2.504 Ppb 486.55 Ppb 927.61 Ppb 473.52 3.36 .004 .005 •72 1.92 2.07 .70327 .1440 .2024 .14847 .20656 .43653 474.20 2.426 2.500 485.85 925.51 475.32 480.91 2.432 2.509 487.29 929.27 471.26 477.40 2.426 2.502 486.53 928.06 473.97 s LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 600.00 600.00 3.000 3.000 600.00 1200.0 800.00 400.00 400.00 2.000 2.000 400.00 • page 2 M O V) H nalysis Report 09/28/05 01:30:28 PM ethod: CLP1 Sample Name: 0509758-003A Operator: PES un Time: 09/28/05 13:22:47 ont: o4 CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Units ppb ppm ppb ppm ppm ppm Avge .48192 .5797 12.677 .1988 .3097 .0005 SDev .22043 .0044 .998 .0003 .0016 .0001 %RSD 45.741 .7557 7.8741 .1669 .5267 26.31 #1 .51855 .5772 12.086 .1985 .3079 .0006 #2 .24547 .5847 13.829 .1991 .3112 .0004 #3 .68175 .5771 12.114 .1989 .3099 .0004 Elem Cd Co Cr Cu Fe K Units ppm ppm ppm ppm .0334 ppm .8147 ppm 8.807 Avge SDev .0111 .0002 .0261 .0001 .0018 .0001 .0002 .0023 .078 %RSD 1.755 .2686 7.426 .6025 .2769 .8829 #1 .0113 .0261 .0019 .0332 .8138 8.720 #2 .0109 .0261 .0017 .0334 .8172 8.871 #3 .0109 .0260 .0017 .0336 .8130 8.830 Elem Mn Mo Na Ni 2203/1 2203/2 Units ppm 1.350 PPM PPM 1182. PPM .1024 Ppb 143.54 Ppb 144.42 Avge .0063 .0016 10. .0005 2.21 1.50 .006 .4093 24.99 .8770 .4753 1.5404 1.0392 #1 1.344 .0081 1170. .1019 141.16 146.13 #2 1.355 .0056 1189. .1026 145.53 143.81 #3 1.351 .0051 1186. .1028 143.94 143.32 Elem 2068/2 1960/1 1960/2 Si Sn Sr Units ppb 10.516 Ppb 2.1502 Ppb 4.2599 PPM 3.035 PPM -.0006 PPM .8083 Avge SDev 2.710 2.8811 1.6279 .052 .0006 .0059 %RSD 25.774 133.99 38.213 1.709 113.7 .7337 #1 7.3937 -.77216 6.0086 2.975 -.0003 .8020 #2 12.266 2.2345 2.7885 3.058 -.0001 .8139 #3 11.887 4.9882 3.9826 3.071 -.0013 .8089 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb 1.9657 PPM PPM 7.423 Ppb 144.13 Ppb 10.304 Ppb 3.5574 Avge SDev 1.5129 .0049 .0001 .033 .52 1.646 15.972 .8729 24.538 %RSD 76.963 1.878 .4502 .36393 #1 3.2720 .0048 7.386 144.48 8.4042 3.7506 #2 0807 .0048 7.451 144.39 11.285 2.6040 16 233171 .0050 7.432 143.53 11.224 4.3174 page 1 Ca ppm 229.2 .9 .4121 228.1 230.0 229.4 Mg PPM 25.79 .11 .4347 25.67 25.89 25.82 2068/1 ppb 9.8806 .5551 5.6184 10.428 9.3181 9.8957 Ti PPM .0022 .0002 9.404 .0023 .0020 .0024 nalysis Report 09/28/05 01:38:16 PM page 1 fethod: CLP1 Sample Name: 0509758-003ADUP Operator: PES :un Time: 09/28/05 13:30:35 'omment: [o* CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb ppm ppm ppm ppm Avge .52262 .6544 14.503 .2043 .3268 .0002 239.3 SDev .49814 .0026 .327 .0001 .0002 .0000 .1 %RSD 95.317 .3951 2.2539 .0354 .0713 13.56 .0245 #1 -.03804 .6565 14.858 .2043 .3270 .0003 239.3 #2 .69162 .6515 14.436 .2043 .3269 .0002 239.3 #3 .91427 .6551 14.214 .2042 .3265 .0002 239.4 Elem Cd Co Cr Cu Fe K Mg Units ppm ppm ppm ppm ppm ppm ppm Avge .0112 .0273 .0020 .0356 .8488 9.419 26.76 SDev .0001 .0002 .0001 .0002 .0006 .058 .02 %RSD .5896 .8760 3.275 .6800 .0660 .6161 .0604 #1 .0112 .0276 .0020 .0356 .8492 9.450 26.78 #2 .0112 .0271 .0019 .0353 .8491 9.352 26.74 #3 .0111 .0274 .0020 .0358 .8482 9.454 26.77 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm ppm ppm ppm ppb ppb ppb Avge 1.414 .0042 1239. .1069 150.15 150.26 11.567 .000 .0001 6. .0009 1.60 .26 1.513 ° .0163 3.425 .5215 .8613 1.0641 .17553 13.080 #1 1.415 .0044 1243. .1064 149.12 149.96 10.358 #2 1.414 .0042 1232. .1080 149.33 150.44 13.263 #3 1.414 .0041 1243. .1063 151.99 150.39 11.078 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb ppb ppm ppm ppm ppm Avge 12.639 1.8454 7.6641 3.221 -.0007 .8543 .0024 SDev 1.131 .5964 1.6360 .010 .0013 .0015 .0000 %RSD 8.9504 32.319 21.346 .3059 185.5 .1709 1.162 #1 12.291 1.9128 8.6500 3.232 -.0013 .8536 .0023 #2 11.723 1.2182 8.5666 3.213 .0008 .8533 .0023 #3 13.903 2.4053 5.7756 3.219 -.0015 .8559 .0024 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb ppm ppm ppb ppb ppb Avge -1.3953 .0046 7.691 150.22 12.282 5.7264 SDev 1.0077 .0005 .002 .64 .659 .9404 %RSD 72.219 11.55 .0246 .42292 5.3647 16.422 #1 -2.0580 .0042 7.692 149.68 11.647 6.4065 #2 -1.8922 .0052 7.692 150.07 12.236 6.1196 # -.23567 .0044 7.689 150.92 12.962 4.6533 nalysis Report 09/28/05 01:46:03 PM page 1 ethod: CLP1 Sample Name: 0509758-003AMS Operator: PES un Time: 09/28/05 13:38:23 omment: o*CONC Corr. Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb 15.262 ppm .1972 ppm .3151 ppm .0002 ppm 230.9 Avge SDev .58934 .5858 .0011 1.203 .0004 .0002 .0000 .4 %RSD .33978 57.654 .1930 7.8804 .2014 .0558 9.838 .1657 #1 .21902 .5856 14.596 .1968 .3151 .0002 230.7 #2 .88673 .5870 14.540 .1971 .3149 .0001 230.7 #3 .66226 .5848 16.650 .1976 .3152 .0002 231.3 Elem Cd Co Cr Cu Fe K Mg Units ppm PPM PPM PPM .0342 PPM .8207 PPM 8.981 Ppm 25.93 Avge SDev .0109 .0265 .0002 .0016 .0004 .0003 .0018 .022 .05 %RSD .0001 1.034 .7996 24.43 1.015 .2141 .2478 .1947 #1 .0263 .0012 .0338 .8198 8.987 25.92 #2 .0108 .0264 .0016 .0343 .8195 8.999 25.88 #3 .0108 .0110 .0267 .0020 .0345 .8227 8.956 25.98 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm 1.366 Ppm ppm 1201. PPM .1040 Ppb 1144.5 Ppb 1140.4 Ppb 11.028 Avge S .0032 .0002 1. .0003 2.2 2.9 1.773 % .002 .1478 6.191 .1096 .2957 .19359 .25014 16.075 #1 1.365 .0035 1202. .1042 1142.0 1137.6 9.1906 #2 1.364 .0032 1201. .1041 1146.2 1140.3 12.728 #3 1.368 .0031 1199. .1036 1145.3 1143.3 11.167 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb ppb 7.1025 ppb 8.5964 PPM 3.106 ppm -.0015 PPM .8209 PPM .0020 Avge SDev 11.145 1.459 .7369 3.3858 .004 .0013 .0014 .0001 %RSD 13.094 10.375 39.387 .1300 84.89 .1653 7.073 #1 9.8944 7.6991 4.7396 3.108 -.0019 .8225 .0021 #2 10.792 7.3296 9.9701 3.102 -.0025 .8202 .0018 .0020 #3 12.748 6.2787 11.080 3.109 -.0001 .8200 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM 7.470 ppb 1141.8 ppb 11.106 ppb 8.0989 Avge SDev -1.1703 .0046 .0001 .011 2.5 1.312 2.0650 %RSD .6770 57.853 2.076 .1485 .21885 11.817 25.497 #1 -1.5152 .0045 7.466 1139.0 9.6600 5.7251 #2 -.39023 .0046 7.462 1142.3 11.437 9.0908 #b -1.6053 .0047 7.483 1143.9 12.222 9.4809 analysis Report 09/28/05 01:53:51 PM page 1 4ethod: CLP1 Sample Name: 0509758-001A Operator: PES tun Time: 09/28/05 13:46:10 -omment: CONC Corr. 10 Factor: 1 Elem Ag Al As1890 B Ba Be Ca Units ppb ppm ppb 21.186 ppm .3669 ppm .4862 ppm .0001 ppm 243.8 Avge SDev .54819 .08146 .3942 .0016 .637 .0004 .0008 .0000 •4 %RSD 14.860 .4004 3.0046 .1217 .1628 13.31 .1571 ##1 .55254 .3960 21.514 .3674 .4871 .0001 244.2 #2 .46464 .3929 21.592 .3669 .4856 .0001 243.5 #3 .62738 .3937 20.452 .3665 .4858 .0001 243.6 Elem Cd Co Cr Cu Fe K Mg Units Avge ppm .0101 ppm .0321 PPM .0021 PPM .0097 PPM 1.228 PPM 10.04 PPM 34.78 SDev .0002 .0001 .0002 .002 .07 .08 %RSD .0000 .2280 .6276 4.055 2.328 .2002 .7296 .2169 #1 .0101 .0320 .0021 .0098 1.230 10.06 34.87 #2 .0101 .0323 .0020 .0099 1.225 10.11 34.73 #3 .0101 .0319 .0021 .0094 1.229 9.965 34.74 Elem Mn Mo Na Ni 2203/1 2203/2 2068/1 Units ppm 1.662 PPM PPM 1189. PPM .1530 Ppb 85.175 Ppb 81.656 Ppb 11.379 Avge S S .0043 .0005 7. .0006 .370 .228 1.402 .003 .1667 11.05 .5846 .3760 .43383 .27961 12.317 #1 1.665 .0048 1192. .1536 85.114 81.651 11.958 #2 1.660 .0039 1194. .1529 85.571 81.886 9.7811 #3 1.661 .0041 1181. .1525 84.839 81.430 12.399 Elem 2068/2 1960/1 1960/2 Si Sn Sr Ti Units ppb Ppb Ppb PPM PPM PPM PPM Avge 14.977 5.9936 10.946 4.580 -.0000 .8385 .0022 SDev 1.350 .4474 1.892 .007 .0011 .0015 .0000 %RSD 9.0141 7.4641 17.286 .1622 9043. .1830 1.583 #1 16.421 5.6855 9.6120 4.588 .0007 .8398 .0022 #2 13.746 5.7885 13.112 4.577 -.0013 .8389 .0021 #3 14.765 6.5067 10.115 4.575 .0006 .8368 .0022 Elem T11908 v Zn Pb2203 Sb2068 Se1960 Units ppb PPM PPM 7.961 Ppb 82.827 Ppb 13.779 Ppb 9.2970 Avge SDev -1.1030 .3198 .0042 .0003 .011 .275 1.266 1.2300 %RSD 28.991 5.887 .1429 .33179 9.1893 13.230 #1 -.88393 .0040 7.974 82.804 14.935 8.3045 #2 -.95514 .0045 7.951 83.113 12.426 10.673 #3 -1.4699 .0042 7.958 82.565 13.977 8.9135 F- -1 LJ nalysis Report [ethod: CLP1 Sample Name: CCV6 :un Time: 09/28/05 13:53:58 'omment: 1o0 CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge 996.90 51.70 528.64 SDev .74 .10 .61 %RSD .07434 .1929 .11598 #1 996.04 51.81 529.05 #2 997.33 51.61 528.93 #3 997.32 51.68 527.93 Elem Cd Co Cr Units ppm ppm ppm Avge 2.536 2.498 2.517 SDev .008 .007 .007 %RSD .2976 .2713 .2710 #1 2.528 2.491 2.510 #2 2.543 2.504 2.523 #3 2.539 2.500 2.519 Elem Mn Mo Na Units ppm ppm ppm Avge 2.509 2.588 81.47 .006 .009 .43 .2395 .3511 .5234 #1 2.503 2.577 81.90 #2 2.514 2.593 81.04 #3 2.511 2.593 81.46 Elem 2068/2 1960/1 1960/2 Units ppb ppb ppb Avge 977.27 529.78 525.03 SDev 7.19 4.95 3.59 %RSD .73533 .93376 .68349 #1 970.46 527.38 521.67 #2 984.78 535.47 528.81 #3 976.57 526.49 524.61 Elem T11908 v Zn Units ppb ppm ppm Avge 513.61 2.522 2.621 SDev 3.91 .005 .007 $RSD .76154 .1948 .2615 #1 509.14 2.517 2.613 #2 516.38 2.526 2.626 #3 515.31 2.524 2.623 r L_J 09/28/05 02:01:39 PM page 1 Operator: PES B PPM 2.330 .004 .1887 2.325 2.332 2.334 Cu PPM 2.479 .001 .0330 2.479 2.479 2.478 Ni PPM 2.514 .003 .1296 2.512 2.518 2.513 Si PPM 1.608 .010 .6122 1.598 1.606 1.618 Pb2203 ppb 509.20 2.70 .53091 506.19 511.42 509.99 Ba PPM 2.480 .002 .0722 2.479 2.483 2.480 Fe PPM 53.25 .15 .2830 53.08 53.35 53.33 2203/1 ppb 514.16 2.98 .57870 511.07 517.00 514.39 Sn PPM 2.488 .007 .2921 2.479 2.492 2.491 Sb2068 ppb 976.01 7.51 .76922 968.37 983.38 976.28 Be PPM 2.537 .008 .2964 2.528 2.543 2.539 K PPM 82.72 .26 .3135 83.00 82.50 82.65 2203/2 ppb 506.72 2.61 .51459 503.75 508.63 507.78 Sr PPM 2.464 .002 .0904 2.463 2.467 2.463 Se1960 ppb 526.61 3.91 .74330 523.57 531.03 525.23 Ca ppm 52.87 .14 .2606 52.71 52.97 52.91 Mg PPM 53.41 .11 .2026 53.29 53.48 53.47 2068/1 ppb 973.48 8.41 .86425 964.19 980.57 975.69 Ti PPM 2.745 .003 .1114 2.746 2.747 2.741 knalysis Report Method: CLP1 Sample Name: CCB6 tun Time: 09/28/05 14:01:46 7omment: 4040 CONC Corr. Factor: 1 Elem Ag Al As1890 Units ppb ppm ppb Avge -.12277 .0046 2.5656 SDev .18896 .0035 .2412 %RSD 153.92 77.11 9.4031 #1 .06478 .0084 2.4456 #2 -.11998 .0038 2.8433 #3 -.31310 .0015 2.4079 Errors LC Pass LC Pass LC Pass High 10.000 .2000 10.000 Low -10.000 -.2000 -10.000 Elem Cd Co Cr Units ppm ppm ppm Avge .0006 .0004 .0003 SDev .0002 .0003 .0004 %RSD 33.33 96.13 154.6 #1 .0009 .0007 .0006 #2 .0005 .0003 .0004 #3 .0005 .0001 -.0002 s LC Pass LC Pass LC Pass M� .0050 .0500 .0100 .,ow -.0050 -.0500 -.0100 3lem Mn Mo Na Jnits ppm ppm ppm kvge .0005 .0052 .6821 3Dev .0003 .0018 .0697 MSD 65.53 33.47 10.21 k1 .0008 .0072 .7566 k2 .0005 .0045 .6713 k3 .0002 .0039 .6185 .rrors LC Pass NOCHECK LC Pass [igh .0150 5.000 low -.0150 -5.000 lem 2068/2 1960/1 1960/2 'nits ppb ppb ppb vge 3.0472 3.9943 1.9275 Dev 1.1140 1.2792 .5860 RSD 36.559 32.026 30.402 1 3.2210 4.3354 2.5244 a4.0640 2.5791 1.9052 1.8565 5.0684 1.3530 rrors NOCHECK NOCHECK NOCHECK 09/28/05 02:09:28 PM Operator: PES page 1 B Ba Be Ca ppm ppm ppm ppm .0011 .0004 .0004 .0152 .0016 .0002 .0002 .0106 150.0 62.28 49.75 69.80 .0030 .0006 .0006 .0264 .0003 .0004 .0004 .0139 .0000 .0001 .0002 .0053 LC Pass LC Pass LC Pass LC Pass .2000 .2000 .0050 .2000 -.2000 -.2000 -.0050 -.2000 Cu Fe K Mg ppm ppm ppm ppm -.0003 .0070 .0720 .0049 .0005 .0036 .0211 .0063 197.1 51.67 29.34 127.8 .0002 .0109 .0943 .0115 -.0002 .0065 .0695 .0044 -.0008 .0037 .0523 -.0011 LC Pass LC Pass LC Pass LC Pass .0250 .1000 5.000 .2000 -.0250 -.1000 -5.000 -.2000 Ni 2203/1 2203/2 2068/1 ppm ppb ppb ppb .0004 -.98404 .39386 4.6962 .0003 1.92163 .53909 .2261 88.55 195.28 136.87 4.8153 .0004 1.2225 -.07272 4.6228 .0008 -2.2899 .27030 4.9499 .0001 -1.8847 .98400 4.5159 LC Pass NOCHECK NOCHECK NOCHECK .0400 -.0400 Si Sn Sr Ti ppm ppm ppm ppm .0366 .0006 .0003 .0007 .0095 .0010 .0003 .0003 25.84 155.6 96.50 45.46 .0467 .0016 .0005 .0010 .0353 .0007 .0003 .0006 .0279 -.0004 .0000 .0005 NOCHECK NOCHECK NOCHECK NOCHECK N M O Cn N knalysis Report 09/28/05 02:09:28 PM High Low A Units Avge SDev %RSD #1 #2 #3 Erro High Low • • page 2 T11908 v Zn Pb2203 Sb2068 Se1960 ppb ppm ppm ppb ppb ppb 2.0313 .0006 .0008 -.06494 3.5963 2.6158 .9908 .0004 .0005 .47736 .8124 .4994 48.779 59.82 63.20 735.05 22.589 19.094 2.8344 .0009 .0013 .35863 3.6879 3.1275 2.3353 .0008 .0007 -.58221 4.3590 2.1296 .92402 .0002 .0003 .02875 2.7421 2.5902 rs LC Pass LC Pass LC Pass LC Pass LC Pass LC Pass 10.000 .0500 .0200 3.0000 60.000 5.0000 -10.000 -.0500 -.0200 -3.0000 -60.000 -5.0000 • page 2 U2M IL US, INC. • IV. DOCUMENTATION FOR METALS A. DIGESTION LOG SHEETS B. REPORTING ANALYST SIGNATURE PAGE • • H2A Labs, inc_ CLP Digestion Loz Client:_ ��5� Analyst S' na re: SDG #: 1' Date: Matrix: Time Started/Ended: Comments:_ /1) - JPH: 'Description of colors: red, blue, yellow, green, orange, violet, white, colorless, brown, grey, black. 'Description of texture: fine, medium, coarse. 'Description of clarity: clear, cloudy, opaque. 'Description of artifacts: yes or no and describe 7 OJMMOOKS/CLPDigestwnlog D . 0175 N M O Cn H U2M LABS, INC. • SDG NO.: SCAN: ryi eT -1 S This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. S D 0 •