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HomeMy WebLinkAboutVolatiles Data Package 04/2005ail= U2A LAUS • Onvironmental Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 0 • • u2A "usINC. ANALYTICAL DATA PACKAGE TABLE OF CONTENTS TOWN OF SOUTHOLD PART 360 BASELINE WATER SAMPLES SAMPLES RECEIVED: 4/1/05 & 4/4/05 SDG NO.: TSI -001 I. NYS DEC SUMMARY FORMS 11. SDG NARRATIVES III. CHAIN OF CUSTODY DOCUMENTATION IV. ANALYTICAL DATA PACKAGE A. VOLATILES B. METALS C. WET CHEMISTRY DATA PACKAGE FOR CLIENT INFORMATION PURPOSES ONLY • 1-i2M "13%. INC. NYS DEC SUMMARY FORMS NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION SAMPLE IDENTIFICATION AND • ANALYTICAL REQUIREMENT SUMMARY SDG: TSL001 Anal ical Requirements Customer Laboratory Sample Sample ME MSvoA We Code Code X X X MW -31) 0504024-001 MW -3S 0504024-002 X X X MW 5D 0504024-003 X X X MW -5 S ; 0504024-004 X X X MW -61) 0504024-005 X X X 'MW -6S 0504024-006 X X X MW -8D 0504024-007 X - X - - - X - 'MW -8S 0504024-008 X X X EQUIPT. BLANK 0504024-009 X X t X 'TRIP BLANK 4/1/05 0504024-010 X MW -1D i 0504067-001 X X X Mw -Is i 0504067-002 X X I X TB 4-4-05 0504067-003 X • CLP, on -C (Please indicate year of protocol) ASS TCUTAL, HSL, Priority Pollutant, kn uj2� M O O 1.4 Cn H • SDG: TSL001 NEW YORK STATE DEPARTMENT OF ENVISMENTAL CONSERVATION • SAMPLE PREPARATION AND ANALYSIS SUMMARY VOLATILE (VOA) ANALYSES Laboratory Analytical i Date DateRecd Date ' Date 1 Extraction j SamP ID_ Client Sample ID Matrix Protocol Collected'; at Lab 'Extracted Analyzed! —Method DF Level Aux Cleanup 0504024-OOIA 'MW -3D Aqueous ASP 95-1 1 O1 -Apr -05 01 -Apr -05 04 -Apr -05 I I LOW 0504024-002A MW -3S Aqueous ASP 95-1 O1 -Apr -05 O1 -Apr -05 04 -Apr -05 1 LOW 0504024-003A MW -5D Aqueous ASP 95-1 O1 -Apr -05 01 -Apr -05 ! '04 -Apr -05 1 LOW 0504024-004A MW -5S Aqueous ; ASP 95-1 01 -Apr -05 O1 -Apr -05 1 04 -Apr -05 l LOW 0504024-005A MW -6D Aqueous ASP 95-1 01 -Apr -05 i O1 -Apr -05 1 04 -Apr -05 l LOW 0504024-006A MW -6S AqueousASP 95-1 O1 -Apr -OS O1 -Apr -OS 04 -Apr -05 j 1 LOW 0504024-007A iMW-8D Aqueous ASP 95-1 O1 -Apr -05 j O1 -Apr -05 I 04 -Apr -05 I LOW 0504024-008A !MW -8S 1 Aqueous ASP 95-1 01 -Apr -05 O1 -Apr -05 ! ( 04 -Apr -05 I LOW� 0504024-009A �EQUIPT. BLK I Aqueous ASP 95-1 01 -Apr -05 ! O1 -Apr -05 i 04 -Apr -05 I LOW 0504024-01 OA tB 411/05 Aqueous ASP 95-1 O1 -Apr -05 01 -Apr -05 04 -Apr -05 i 1 LOW !0504067-00IA !MW -ID Aqueous ASP 95-1 04 -Apr -05 04 -Apr -05I 04 -Apr -05 1 LOW 0504067-002A �,MW-1S Aqueous I ASP 95-1 104 -Apr -05 04 -Apr -05 04 -Apr -05I 1 LOW 0504067-002AMS MW -ISMS Aqueous ASP 95-1 104 -Apr -05 04 -Apr -05 104 -Apr -051 1 LOW 0504067-002AMSD MW-ISMSD Aqueous I ASP 95-1 04 -Apr -05 ! 04 -Apr -05 104 -Apr -05 I LOW 0504067-003A iTB 44-05 Aqueous ASP 95-1 04 -Apr -05 04 -Apr -05 j 04 -Apr -05 ! 1 LOW TSL001 A4 • NEW YORK STATE DEPARTMENT OF ENSONMENTAL CONSERVATION SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSL001 INORGANIC ANALYSIS Laboratory Samp ID I Client Sample IDI Matrix Metals Requested DateRecd I Date at Lab I Analyzed 0504024-001 MW -3D WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 i 04/05 0504024-002 ,MW -3S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504024-003 �MW-5D WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 j 04/05 0504024-004 BMW -5S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,K,MG.MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504024-005 ;MW -6D 1 WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504024-006 MW -6S WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504024-007 MW -8D WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -OS 04/05 0504024-008 MW -8S WATER AG,AL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504024-009 JEQUIPT. BLANK WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE.HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 01 -Apr -05 04/05 0504067-001 MW -ID WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 04 -Apr -05 04/05 0504067-002 MW -IS WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 04 -Apr -05 04/05 0504067-002DUP MW -ISD WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 04 -Apr -05 04/05 0504067-002MS MW -ISS WATER AGAL,AS,B,BA,BE,CA,CD,CN,CO,CR,CU,FE,HG,K,MG,MN,NA,NI,PB,SB,SE,TL,V,ZN, 04 -Apr -05 04/05 TSL001 A5 NEW YORK STATE DEPARTMENT OF ENVIRONMENTAL CONSERVATION . SAMPLE PREPARATION AND ANALYSIS SUMMARY SDG: TSI -001 INORGANIC ANALYSIS Laboratory Samp ID !, Client Sample ID Matrix Tests iDateRecd ; at Lab Date Analyze 0504024-001 MW -313 Groundwater SELECT WET CHEMISTRY** 04/01/05 i 04/05 0504024-002 MW -3S Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-003 MW -51) Groundwater SELECT WET CHEMISTRY ** I 04/01/05 , 04/05 0504024-004 MW -5S Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-005 MW -613 Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-006 MW -6S i Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-007 MW -813 Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-008 MW -8S Groundwater SELECT WET CHEMISTRY ** 04/01/05 04/05 0504024-009 j EQUIPT. BLANK Blank SELECT WET CHEMISTRY ** 04/01/05 j 04/05 0504024-010 ! TRIP BLANK 4/1/05 Blank SELECT WET CHEMISTRY ** 04/01/05 04/05 0504067-001 MW -1D Groundwater SELECT WET CHEMISTRY ** 04/04/05 04/05 0504067-002 i MW -IS Groundwater SELECT WET CHEMISTRY ** 04/04/05 04/05 0504067-003 : TB 4-4-05 Trip Blank SELECT WET CHEMISTRY ** 04/04/05 04/05 • ** 1,1,1,2 -Tetrachloroethane ; 1,1,1 -Trichloroethane ; 1,1,2,2 -Tetrachloroethane ; 11,11,2 - Trichloroethane; 1,1-Dichloroethane ; 1,1-Dichloroethene ; 1,2,3-Trichloropropane ; 1,2- Dibromo-3-chloropropane ; 1,2-Dibromoethane ; 1,2 -Dichlorobenzene ; 1,2- Dichloroethane ; 1,2-Dichloroethane-d4 ; 1,2-Dichloropropane ; 1,4 -Dichlorobenzene ; 2- Butanone ; 2-Hexanone ; 4-Bromofluorobenzene ; 4-Methyl-2-pentanone ; Acetone ; Acrylonitrile ; Alkalinity, Total (As CaCO3) ; Alkalinity, Total (As CaCO3), High ; uminum ; Antimony; Arsenic ; Barium ; Benzene ; Beryllium ; Biochemical Oxygen an ; Boron ; Bromide ; Bromochloromethane ; Bromodichloromethane ; Bromoform ; Bromomethane ; Cadmium ; Calcium ; Carbon disulfide ; Carbon U2M "US, INC. 0 SDG NARRATIVES • U2AA "U%S INC. SDG NARRATIVE FOR VOLATILE ANALYSES SAMPLE RECEIVED: 4/1/054/4/05 SDG#: TSL001 For Samples: MW -3D MW -6S TRIP BLANK 4/1/05 MW -3S MW -8D MW -1D MW -5D MW -8S MW -1S MS/MSD MW -5S EQUIPT. BLANK TB 4-4-05 MW -6D The above samples were analyzed according to the requirements of the NYSDEC ASP 10/95 method 8260B for the part 360 baseline list of volatile organic analytes. All QC data and calibrations met the requirements of the method, and no problems were encountered with sample analysis. The following should be noted: • Sample MW -IS was analyzed as the matrix spike/matrix spike duplicate. 4-Bromofluorobenzene had a 20.8% RSD in the initial calibration of 4/4/05, which exceeded 20.5% but met the acceptance limit of 40%. Carbon tetrachloride had a 26.7% D in the continuing calibration of 4/4/05, which exceeded 25% D but met the acceptance limit of 40%. • I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 19, 2005 o:\qc\naiT2005\irr\voa\ts 1001.doc • ***** ********** ****** **** * * ** *********** Joa Slavin Senior Vice President 00 C U2M I U%3 INC. . NARRATIVE FOR METALS ANALYSES SAMPLE RECEIVED: 4/1/05 & 4/4/05 SDG#: TSL001 For Samples: MW -3D MW -8D MW -3S MW -8S MW -5D EQUIPT. BLANK MW -5S MW -ID MW -6D MWAS MS/MSD MW -6S Eleven water samples were received by H2M Labs inc. on 4/1/05 and 4/4/05 for cyanide and TAL metals analysis. Samples were prepared and analyzed using EPA method 6010B with a TJA61E Trace ICP instrument, method 7470A with a Leeman HYDRA mercury analyzer and cyanide method 335.2. Sample MW -IS was utilized as the QC sample for QC analysis and reporting. Spike analysis did not recover within acceptance ranges for cyanide. The sample was post • spiked, reanalyzed and recovered acceptably. Cyanide data was reported flagged "N" on forms 1 and 5A. ICP serial dilution analysis did not reproduce within acceptance ranges for sodium. Sodium data was reported flagged "E" on forms 1 and 9. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 19, 2005 Valent Stancampiano Vice President 0 • U2M INC. For Samples: SDG NARRATIVE FOR WET CHEMISTRY SAMPLES RECEIVED: 4/1/05 & 4/4/05 SDG NO.: TSL001 MW -3D MW -813 MW -3S MW -8S MW -513 EQUIPT. BLANK MW -5S MW -11) MW -6D MW -IS MS/MSD MW -6S Samples were prepared and analyzed using the following methods: PARAMETER Alkalinity BOD Bromide Chloride COD Color Hexavalent chromium Hardness Ammonia Nitrate Phenols Sulfate TDS TKN TOC METHOD # EPA 310.1 EPA 405.1 EPA 320.1 EPA325.2 EPA 410.4 EPA 110.2 STDM 3500- CR D EPA 130.2 EPA 350.1 EPA 353.2 EPA420.1 EPA 9038 EPA 160.1 EPA 351.2 EPA 9060 Sample MW -1 S was utilized for duplicate and spike QC analysis and reporting. Duplicate analysis did not reproduce within acceptance ranges for total kjeldahl nitrogen. The initial analysis was <0.10 mg/L. The duplicate aliquot was a negative 0.29 mg/L. Matrix interferences were suspected. Batch acceptance was based on ICV, CCV and LCS recoveries. No other problems were noted during the analysis of this sample group. I certify that this data package is in compliance with the terms and conditions of the contract, both technically and for completeness, for other than the conditions detailed above. Release of the data contained in this hardcopy data package has been authorized by the Laboratory Manager or his designee, as verified by the following signature. Date Reported: April 21, 2005 ** ********************** wvk C �- , x* • n�� Vincent Stancampiano Vice President • o:\qc\narr2005\irr\we1 chem\ts1001.doc u2M I AU%4, INC. • III. CHAIN OF CUSTODY DOCUMENTATION • 0 0 cn NIAI3S 575 lr&ollow Rd, Melville, N INC. (11747-5076 EXTERNAL CHAIN OF CUSTODO Tel: (516) 694-3040 Fax: (516) 420-8436 CLIENT: So v7NOt H2M SDG NO: 00 PROJECT NAME/NUMBER '�0w o C4o Q(!. ��00 .c o-ct 0 .0 CL Eo - ©. `� i -� r ; . � .... ( NOTES: Project Contact: Or Gi, �,� S IJfr- (u , � C. D / Phone Number: ( DSI x/623 / x lbaS SAMPLERS: (signature)/Client DELIVERABLES: o c ` c Z ro B 8 1 ANALYSIS REQ U ED TURNAROUND TIME: ORGANIC .`� INORG. DATE TIME MATRIXFIELD I.D. O > fl 2 m oV ° a n4 "� N Z V LAB I.D. NO. REMARKS: 4/1/602'0210 vJ M— I a 1 ��4014- a 0130 i/11 Uy 3,6 Gam, 3 i M -- 5-5 - i33a MW — 15L) 100 -- S —CATs /040 M G _ 2bNV /zoo E- _ ; Relinquished by: (Signature) Date i ime 1 Received by; (Signal re) a e l Time .� I LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y or N Explain: Samples were: f Shipped_ or Hand Delivered_ Airbill# 2. Ambient or chilled 3. Received in good condition: Y or N 4. Properly preserved: la or N 5. Samples resumed to lab _ Hrs from collection. COC Tape was: 7. Present on outer package Y or N 2. Unbroken on outer package: Y or N 3. COC record present & complete upon sample receipt: YorN Relinghed by: (Signature) ws Date Time R (Sign ived : e . Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time T9kMCt0e - ORIGINAL YELLOW COPY - CLIENT MK °., ^ • . - - - H2M LABS, INC. �l Sample Receipt Checklist Client Name PCTSL Date and Time Receive 4/1/2005 4:20:00 PM Work Order Numbe 0504024 Received by BGL Checklist completed b �' � Reviewed by --t(���--- ���fs Matrix Carrier name Hand Delivered Shipping container/cooler in good condition? Yes LJ No ❑ Not Applicable C Custody seals intact on shippping container/cooler? Yes EI No U Not Applicable Custody seals intact on sample bottles? Yes ❑ No 11 Not Applicable �J Chain of custody present? Yes CJ No Chain of custody signed when relinquished and received? Yes LJ No ❑ Chain of custody agrees with sample labels? Yes W No f Samples in proper container/bottle? Yes DV No ❑ Sample containers intact? Yes [J No ❑ Sufficient sample volume for indicated test? Yes l J No ❑ amples received within holding time? Yes LJ No ❑ i ainer/Temp Blank temperature in compliance? Yes Nox Water - VOA vials have zero headspace? No VOA vials submitted L-1 Yes V No Water - pH acceptable upon receipt? Yes �J No i_ - Adjusted? Checked b Any No and/or NA (not applicable) response must be detailed in the comments section b Client contacted Date contacted: Person contacted --- —' - - Contacted by: r Regarding Comments: Corrective Action NzA4 tAUS, eNc. INTERNAL CNAM OF CUSTODY CLIENT LIVERABLES: AROUND TWE: �5 SDG k CASE k. MATRIX: 6; ptI CFWICK Y m REMARKS:t R ( S RECEP ED BY: <a �Q U� SIGNATURE: A44*DATE: o0`V-7�►7E: TTT- CLIENT 1D H2M LAB M DATE COLLECTED BOTTLE TYPE 0 OF BOTTLES TESTS REQUESTED f Gs • � 5 •:k's `t.V, ' N N n n • VOLATILE P 02Os f it]2AA tA INCO IS Da �. INTERNAL CHAIN OF CUSTODY DATE TIME SAMPLE RELINQUISHED B7 SAMPLE RECEIVED BY PURPOSE OF BOTTLE CHARGE OF TYPE CUSTODY INIT slot s1 31 3low slaw slow slow slow slow S2Gw slow 3Iow slow 310H slow SIGM slow 910N slow SICN slow SIGN 21GO SIC" s1OW SIGH SIGN SIGN slow SIC" SIGH SICN slow SIO" J1Ow SIGN slow SIC" I. $ION Slow - i - slow slow - slow .21034 SIGN SIC" 23034 310w SIGN SIGN •"'i I SIGN VOLATILE r� 0 H lH2A► LAUS9 INC. INTERNAL CHAIN OF CUSTODY CLIENt` `L, DELIVERABLES:` j- TURN AROUND TIME: � 1 5 SDG #: _ CASE #: MATRIX: pH CHECyo- N REMARKS: r�)] RECEIVED BY: SIGNATURE: M METALS P 02tza IN 0911 - Ml b-,4 4 bqh. W Aff, 69 m ME METALS P 02tza � N2M ��1C -1 � lot' ' CLIENT: �- ' INTERNAL CHAIN OF CUSTODY DATE TIME SAMPLE RELINQUISHED BY SAMPLE RjtQ11VKD BY BOTTLE TYPE PURPOSE OF CHANGE OF CUSTODY INIT t slot s G t is eI SI ow j ear �I / �(/ OS eI It C) o e X16105 eI 13�d _ O1 (� S�ac� � ��11 1 sI _ 7IC)� allow 0.��i�i SI 4 c' D Gj3c0 SI 930 SIGN ? _lots SIGN SIGN SIGN SIGN SIGH SIGN Slow SIGN SION SIGN SIGN SIGN SIGN SIGN SIGN SIGN SIGN SIGN slow SIon SIGN SIGN SIGN SIGN SIGN SIGN SIGN SIGN 910N SIGN 1 A N METALS P 0260 t12A to US, INC. • INTERNAL CHAIN OF CUSTODY _ CLIENT: C 5L DELIVERABLES: JAURN AROUND TIME - 9t- SDG 1:T S QQ ( CASE It: MATRIX: pH cEEc Y I N I RECEIVED BY: S)GNA?URE: G Jv WET CHEMISTRY ,oa _w, P 024' WN Em" ""I., T., "..-j iEmmm SIT wi m Nlq M, WET CHEMISTRY ,oa _w, P 024' Nati LA"19 V,s � CLIENT & # • ul�r A1C. INTERNAL CHAIN OF CUSTODY Ull • WET CHEMISTRY �40 �• :.CRAMIC ,." -O. OF cu VIA mI►� _Y J/ wn Ull • WET CHEMISTRY �40 N2A UA,Es, &c. SDG: ��oo INTERNAL CHAIN OF CUSTODY • WET CHEMISTRY P 0249 PURPOSE OF CILAWN OF CUSTODY WM I, A/rf"'mil • WET CHEMISTRY P 0249 U"Uso INC. 575 Bl a Hollow Rd, Melville, NY 11747-5076 i50• EXTERNAL CHAIN OF CUSTODY* Tel. (516) 694-3040 Fax. (516) 420-8436 CLIENT: S0 (/7NOL)O &T`�)L_ 1H2M SDG NOT�_oo l PROJECT NAME/NUMBER Pq R T 3&0 8r9SEL l!(/ 6.o U s v _ SE .4kV >J M z ty NOTES: Project Contact. PSS / V Cr , yy 8 oio 1 J G( Phone Number: X so Lf TA ikj` bs TvY6 SAMPLERS: (signature)/Client DELIVERABLES: �S- -.Io —D °12 c Z r o U 1 ANALYSIS REQUESTED TURNAROUND TIME: De S ORGANIC INORG. DATE TIME MATRI FIELD I.D. Q ` 3 V Q i Z U LAB I.D. NO. REMARKS: N q i w W1M w —1-9-- -- a a 3 1 1/ 44 os /61 WW I /n w — / S' 33 6 :3 3 3 G .: _ -uc' %A /;15 ZM s —o 2-1 1 -uc_'i Relinquished by: (Signature) Date t7y0� 1 qT Received by: (Signature) Date y l 5 Time 1 -00 LABORATORY USE ONLY Discrepancies Between Sample Labels and COC Record? Y or N Explain: Samples were: 1. Shipped_ or_H,and Delivered�irbill# 2. Ambient o chilled 't(! L 3. Received i�condition (5r N 4. Properly preserved or N 5. Samples returned t ab Hrs from collection. COC Tape was: 1. Present on outer package:% y or N 2. Unbroken on outer package. Y or N 3. COC record present & complete upon sample receipt. Y or N Relinquished by: (Signature) Date R ived by: (Si ture) Date Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time Relinquished by: (Signature) Date Time Received by: (Signature) Date Time TW441C,6' - ORIGINAL YELLnw rnpv - rl tcKrr H2M LABS, INC. • Client Name PCTSL Work Order Numbe 0504067 ��1�� T L GG) Sample Receipt Checklist Date and Time Receive Received by FS 4/4/2005 Checklist completed b 1��� Reviewed by signature Date Initials✓ Date Matrix Carrier name Hand Delivered Shipping container/cooler in good condition? Yes W Custody seals intact on shippping container/cooler? Yes EvIl Custody seals intact on sample bottles? Yes ❑ Chain of custody present? Yes SOi Chain of custody signed when relinquished and received? Yes W] Chain of custody agrees with sample labels? Yes W Samples in proper container/bottle? Yes ❑� Sample containers intact? Yes 0 Sufficient sample volume for indicated test? Yes 0 received within holding time? Yes 0 6amples tainer/Temp Blank temperature in compliance? Yes Water - VOA vials have zero headspace? No VOA vials submitted Water - pH acceptable upon receipt? Yes No ❑ Not Applicable ❑ No ❑ Not Applicable ❑ No ❑ Not Applicable u No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ No ❑ Yes �J No ❑ Adjusted? Checked b No ❑ Any No and/or NA (not applicable) response must be detailed in the comments section b Client contacted Date contacted: `,r° T% Person contacted / Contacted by:/ n Regarding Comments: Ji I i Corrective Action N O t!1 H 9 If t1ZH tAUS, WqC- b4 -t- INTERNAL CHAIN OF CUSTODY CUENT_ � 1 t) �-- DELIVERABLES: TURN AROUND TDNE: 2,1 SDGS- -15L-( C) CASE #: MATRIX: - (A) pH CHECK Y or REMARKS: 0 Z 1 TLI - O RECErvW BY: SIGNATURE: DATE:TA�E:�� � " VOLATILE P 0,214 Wa 0 A VOLATILE P 0,214 f12A t A[S, INC. ENT: L ► s L&ODG #: - 1-51-y 0 1 - i INTERNAL CHAIN OF CUSTODY ATS TIRE SAMPLE RELINQUISHED BY PURPOSE OF SAMPLE BOTTLE CHANGE OF RECEIVED BY TYPE CUSTODY INIT �. f V O i slaw 31 fI slow nor slow slow slow slaw slow slow $IGN slow slow slow slow slow slow slow SIGN Slow SIGN 310H SIGN 3I0M SIGN 31010 SIGN slow 31cN -ilow SIGN slaw 310" 31010 SIGN !1010 SIGN 31010 3100 ., slow slow -- slur LION t+ sloe sic" 31024 SIGN 3I0N S1cN 1 i SIGN S1GN VOLATILE P 0215 a t j U2A ILAUS9 NC. INTERNAL CHAIN OF CUSTODY CLIEW:"Y— DELIVERABLES: U)'j) TURN AROUND TV -4E: 7-7 SDG N: - L— Ujul CASE it: MATRIX: c,Gk) pHN cflwl�) REMARKS: L) qe RECEWED BY. SIGNATURE: -DATE: T.W: 0 H2M LAD CLIENTID 0 DATE COLLECTEDI BOTTLE TYPE 0 OF BOTTLES1 TESTS REQUM,'��D L i #In Lu Cq- -44 L , X 10 METALS P 02.71 f IH2M UAUS, INC. Y i 3D0 w OC) V INTERNAL CHAIN O] • METALS P 0272 �� :� ;•CRAMS,. •:CUSTOD pur"sla�. 1, Shk P. z lal top ED • METALS P 0272 Nzk+ «►Us, NC. INTERNAL CHAIN OF CUSTODY *CLIENT: 5L --DELIVERABLES: B5 — 40 D TURN AROUND TDAE: Z _S SDG #: TS LLC) U CASE #: MATRIX: C (/V pH cf WCX(�- x REMARKS_ 6 Z t 10 T5, n�5 • is a� : Em iiG �r � .0 o CLIENT ID 0 +H2M LAB # DATE COLLECTED BOTTLE TYPE N OF BOTTLES TESTS REQUESTED i _oolC 3 --vC.-10bo _c,.) ' I ! 0D ' —Dolt I 4gwl —wL ' �a -tz1vI CIV — C _ vj � UbUVk 7 (ol q, �3+3,3 - CA 41U -e- 1 -e- • WET CHEMISTRY 0256 `n H WA UAUS, IVC. 0: "T5 -LOO I INTERNAL CHAIN OF CUSTODY Al • l M WET CHEMISTRY J* dv t of Si7 4ewe-C P 025'7 00 N 0 cn H •f "I :.CRAME Pup"sic OF OF CUSTGDY IN PAWNiing1 Al • l M WET CHEMISTRY J* dv t of Si7 4ewe-C P 025'7 00 N 0 cn H U2M► UAUs, CLIENT: (XT5coo1 SDG #:� mac: INTERNAL CHAIN OF CUSTODY DATE SAMPLE RELINQUISHED TIME T SAMPLE BY BOTTLE TYPE PURPOSE OF CHANGE OF INIT cCUSTODY cS sI o30 vc civ slow Y-t1-oS sION t Y = o0 SIGN Y-It-�s slow $;00 !ION slow slow y- �z•os slow 9 :ao slow K S slow slow µS 11W SIGN y 1,� Slow SIGN 'Iow SIGN S7W1 SIGN Slow SIGN slow SIGN slow SIGN slow 31014 !1016 slow Slow SIGN slow SIGN slow slow 910H SIGN 310w SIGN 1I on SIGN ZION SIGN SION SIGN t • WET CHEMISTRY P G2S8 N O N U2M "US, INC. • IV. ANALYTICAL DATA PACKAGE A. VOLATILES B. METALS C. WET CHEMISTRY • • • • H2M LABS, INC. 151 -col VOLATILE ORGANICS TABLE OF CONTENTS QC SUMMARY SAMPLE DATA PACKAGE STANDARDS DATA PACKAGE RAW QC DATA PACKAGE DOCUMENTATION H2M LABS, INC. I. QC SUMMARY FOR VOLATILE ORGANICS A. SYSTEM MONITORING COMPOUND RECOVERY FORM B. MS/MSD FORM C. MSB FORM D. METHOD BLANK FORM E. GC/MS TUNING FORM F. INTERNAL STANDARD AREA AND RT SUMMARY G. INSTRUMENT DETECTION LIMITS • N O H 2A WATER VOLATILE SYSTEM MONITORING COMPOUND RECOVERY Lab Name: H2M LABS, INC. Contract: Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 EPA SMCl SMC2 SMC3 I OTHER i TOT j SAMPLE NO. DCE # TOL # BFB # OUT l' 01 02 03 04 05 06 07 08 09 10 11 12 13 14 15 16 17 VBLK040405 97 98 87 I 0 F4040 - - I L --BO- 102 -- 100 —5 - - 101 I - j 0 MS13040405 95 100 98 0 EQUIPT. BLK 94 98 94 0 TB 4/1/05 95I! 99 95 0 ! 96 99_ i 97 �MW-3D IMW-3S -- 95 ` - _ 99 94 0 MW -5D 96 99 96 r 0 MW -5S 96 ' - 100 95 - t --- - _ 0 I ,MW -6D 96 1 99 95 I 0 1 MW -6S 94 99 93 j 0 jMW-8D 94 99 93 0 MW -8S 93 100 1 95 i 0 MW -1D 92 98 91 1 0 1MW-1S 93 99 94 ! 0 MW-1SMS 93 100 95 ( 0 TB 4-4-05 95 99 i 93 0 • 181MW-1SMSD 93 99 94 0 i QC Limit SMC1 DCE = 1,2-Dichloroethane-d4 (76-114) SMC2 TOL = Toluene -d8 (88-110) SMC3 BFB = 4-Bromofluorobenzene (86-115) # Column to be used to flag recovery values * Values outside of contract required QC limits page 1 of 1 FORM II VOA -1 I* OLM04.2 1r u • • 3A WATER VOLATILE MATRIX SPIRE/MATRIX SPIRE DUPLICATE RECOVERY Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix Spike - EPA Sample No.: MW -1S I I SPIKE SAMPLE MS i MS QC. I j ADDED CONCENTRATION CONCENTRATION j % LIMITS I— i-_ (N9/L) (N9/L) ! (Ng/L) i_ REC # REC.---- I ___COMPOUND 1 1 Dichloroethene REC # 50 i 0 47 ---- 93 _---_. 61-145 Benzene 50 0 49 1 99 76-127 Trichloroethene I 50 I 0 52 i 104 71-120 I Toluene 1 50 0 53 105 I 76-125 Chlorobenzene 50-I - 0 55 111 75130 I SPIKE --MSD MSD T-- ADDED CONCENTRATION % j % i QC LIMITS i COMPOUND (Ng/L) (Ng/L) REC # RPD # RPD REC. 1,1 Dichloroethene 5047 i 93 0 14 61-145 ;Benzene 50 - 49 98 - 1 11 76-127 Trichloroethene 50 52 j 104 0 14 71-120 Toluene 50 52 105 0 13 76-125 Chlorobenzene 50 j 56 112 1 ; 13 75-130 1 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits RPD: 0 out of 5 outside limits Spike Recovery: 0 out of 10 outside limits COMMENTS: FORM III VOA -1 OLM04.2 3A SYSTEM MONITORING SPIKE RECOVERY • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Sample ID MSB040405 Level:(low/med) LOW r� COMPOUND S IP KE T ADDED (P L) SAMPLE CONCENTRATION W/O SPIKE CONCENTRATION W/O SPIKE %, REC # QC. LIMITS REC. 1,1-Dichloroethene 50 0 50 100 61-145 Benzene 50 0 53 105 76-127 Trichloroethene 50 0 55 109 71-120 Toluene 50 0 55 109 76-125 Chlorobenzene 50 0 56 111 75-130 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits Spike Recovery: 0 out of 5 outside limits COMMENTS: FORM III SW8260B 3A SYSTEM MONITORING SPIKE RECOVERY Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Sample ID LFB040405 Level:(low/med) LOW r- COMPOUND SPIKET— SAMPLE T� ADDED CONCENTRATION (Ng/L) (yg/L) SPIKE I CONCENTRATION (Ng/L) SPIKE % REC # QC. LIMITS REC. Chloromethane 50 0 55 110 70-114 Vinyl chloride 50 0 55 111 66-117 Bromomethane 50 0 52 103 50-136 Chloroethane 50 0 52 104 71-116 Acetone 50 0 44 87 71-125 Acrylonitrile 50 0 56 112 74-122 lodomethane 50 0 52 105 70-122 Vinyl acetate 50 0 47 93 76-118 2-Butanone 50 0 47 94 74-121 Carbon disulfide 50 0 54 109 61-126 Trichlorofluoromethane 50 0 57 113 64-124 1,1-Dichloroethene 50 0 54 108 67-120 Methylene chloride 50 0 50 101 80-112 trans-1,2-Dichloroethene 50 0 52 104 74-115 1,1-Dichloroethane 50 0 53 105 77-114 as-1,2-Dichloroethene 50 0 50 101 78-116 Bromochloromethane 50 0 49 97 81-114 Chloroform 50 0 52 104 75-119 1,2-Dichloroethane 1,1,1 -Trichloroethane 50 50 0 0 51 57 101 113 76-120 66-126 Carbon tetrachloride Benzene 50 50 0 0 57 51 115 102 64-126 77-116 Trichloroethene 50 0 53 107 72-121 1,2-Dichloropropane 50 0 50 100 81-115 Dibromomethane 50 0 48 97 82-114 Bromodichloromethane 50 0 51 102 78-118 cis-1,3-Dichloropropene 50 0 50 100 79-116 Toluene 50 0 52 104 70-125 trans-1,3-Dichloropropene 50 0 49 98 77-120 1,1,2 -Trichloroethane 50 0 48 96 82-116 R Column to be useCf to ting recovery ana Ryu values Wltn an asterisx * Values outside of QC limits Spike Recovery: 0 out of 47 outside limits COMMENTS: FORM III SW8260B 3A SYSTEM MONITORING SPIKE RECOVERY • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Sample ID LFB040405 • • SDG No.: TSL001 Level:(low/med) LOW 1,2-Dibromoethane 50 0 48 95 81-117 4-Methyl-2-pentanone 50 0 43 87 79-121 Chlorobenzene 50 0 51 102 72-124 Tetrachioroethene 50 0 52 105 59-133 Dibromochloromethane 50 0 48 96 79-118 2-Hexanone 50 0 43 86 76-119 1,1,1,2 -Tetrachloroethane 50 0 50 101 76-119 Ethylbenzene 50 0 52 104 68-128 Xylene (total) 150 0 160 107 70-125 Styrene 50 0 50 100 72-124 Bromoform 50 0 46 93 75-121 trans-1,4-Dichloro-2-butene 50 0 46 93 47-135 1,1,2,2 -Tetrachloroethane 50 0 45 89 77-120 1,2,3-Trichloropropane 50 0 45 89 78-118 1,4 -Dichlorobenzene 50 0 50 100 67-128 1,2 -Dichlorobenzene 1,2-Dibromo-3-chloropropane 50 50 0 0 49 _ 44 99 89 71-123 74-123 # Column to be used to flag recovery and RPD values with an asterisk * Values outside of QC limits Spike Recovery: 0 out of 47 outside limits COMMENTS: FORM III SW8260B • • 4A EPA SAMPLE NO. VOLATILE METHOD BLANK SUMMARY VBLK040405 Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Lab File ID: A\A41196.D Lab Sample ID: VBLK040405 Date Analyzed: 04/04/05 Time Analyzed: 15:03 GC Column: R-502.2 ID: .53 (mm) Heated Purge: (YIN) N Instrument ID: HP5971 THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES, MS, AND MSD: EPA LAB i LAB TIME 01 W O' 04 0° OE 07 Of OE 1C 11 1� 12 14 1I 1E 17 COMMENTS: O/11VIrLC N%J. - JHIVIr Lr- IU rILr- IU -/11W1LTLCU LFBO40405 LFB040405 AW41197 D 15:39 16:06 MSB040405 MSB040405 AW41198 D EQUIPT. BLK 050402_4-009A AW41199.D 16:39 TB 4/1/05 _ 0504024-010A A\A41200.D 17:06 MW -3D 0504024-001A A\A41201.D 17:34 MW -3S 0504024-002A A\H41202.D A\A41203.D 18:01 18:34 MW -51) 0504024-003A MW -5S 0504024-004A AW41204.13 19:01 MW -61) 0504024-005A A\A41205.D 19:29 MW -6S 0504024-006A XA41206.13 19:56 MW -8D 0504024-007A AW41207.D 20:23 j MW -8s 0504024-008A A\A41208.D 20:51 r— — — MW-1D ----... --- 0504067-001A --------- -- A\A41209 D 21:54 MW -1s 0504067-002A A\A41210 D 22:21 MW -isms 0504067-002AMS A\A41211 D 22:48 TB 4-4-05 05040_67-003A A\A41212.D 23:16 L--MW-ISMSD 0504067-002AMSD A\A41213.D 23:44 page 1 of 1 FORM IV VOA OLM04.2 00 Ll1 SA • VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Lab File ID: A\A40923.D BFB Injection Date: 02/28/05 Instrument ID: HP5971 BFB Injection Time: 9:15 GC Column: R-502.2 ID: .53 (mm) -- - -r LAB I % RELATIVE We ION ABUNDANCE CRITERIA ABUNDANCE 50 15.0 - 40.0% of mass 95 16.2 75 30.0 - 60.0% of mass 95 47.3 95 Base peak, 100% relative abundance 100.0 { 96 5.0 - 9.0% of mass 95 6.9 173 Less than 2.0% of mass 174 0.0 (0.0)1 1 174-1 Greater than 50.0% of mass 95 ! 70.2 02' VSTD050 175 5.0 - 9.0% of mass 174 5.0 (7.1)1 176 ; 95.0 - 101.0% of mass 174 69.2 (98.6)1 I 177 5.0 - 9.0% of mass 176 4.8 (6.9)2 1 1 -Value is % mass 174 2 -Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: page 1 of 1 0 FORM V VOA OLM04.2 - EPA -- - -r LAB I - -- - - LAB DATE TIME • SAMPLE NO. I SAMPLE ID FILE ID ANALYZED ANALYZED 01 --VS-TD-0-10 VSTD010 A1A40925.D 02/28/05 10:38 j 02' VSTD050 VSTDO50 AW40927.D 02/28/05 11:41 03 VSTD100 VSTD100 A\A40928.D 02/28/05 13:05 04r VSTD200 VSTD200 A\A40929.D 02/28/05 1 1134 r- 051 - -. --- - - --a-- VSTD020 -- - - VSTD020 --- A\A40930.D 02/28/05 1443 page 1 of 1 0 FORM V VOA OLM04.2 5A • VOLATILE ORGANIC INSTRUMENT PERFORMANCE CHECK BROMOFLUOROBENZENE (BFB) • Lab Name: H2M LABS. INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Lab File ID: A\A41194.D BFB Injection Date: 04/04/05 Instrument ID: HP5971 BFB Injection Time: 14:16 GC Column: R-502.2 ID: _S (mm) We VSTD050 ION ABUNDANCE CRITERIA RELATIVE ABUNDANCE 50 15.0 - 40.0% of mass 95 17.0 75 30.0 - 60.096 of mass 95 47.1 95 Base peak, 100% relative abundance 100.0 96 5.0 - 9.0% of mass 95 6.9 173 Less than 2.0% of mass 174 0.0 (0.0)1 174 Greater than 50.0% of mass 95 71.8 175 5.0 - 9.0% of mass 174 5.3 (7.4)1 176 95.0 - 101.0% of mass 174 70.4 (98.1)1 177 5.0 - 9.0% of mass 176 4.4 (6.2)2 1 -Value is % mass 174 2 -Value is % mass 176 THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS, AND STANDARDS: 03 02 03 04 05 OE 07 0E 05 iC 11 12 13 14 15 16 17 16 15 EPA LAB LAB DATE TIME SAMPLE NO. SAMPLE ID FILE ID ANALYZED ANALYZED VSTD050 VSTD050 AW41195.D 04/04/05 14:31 VBLK040405 VBLK040405 AW41196.D 04/04/05 15:03 LFB040405 LFB040405 AW41197.D 04/04/05 15:39 MSB040405 MSB040405 AW41198.D 04/04/05 16:06 EOUIPT. BLK 0504024-009A A1A41199.D 04/04/05 16:39 TB 4/1/05 0504024-010A AW41200.D 04/04/05 17:06 MW -3D 0504024-001A AW41201.D 04/04/05 17:34 MW -3S 0504024-002A AV141202.D 04/04/05 18:01 MW -5D 0504024-003A AW41203.D 04/04/05 18:34 MWSS 0504024-004A AU441204.D 04/04/05 19:01 MW -6D 0504024-005A AW41205.D 04/04/05 19:29 MW -6S 0504024 -MA AV141206.D 04/04/05 19:56 MW -8D 0504024-007A AV441207.D 04/04/05 20:23 MW -8S 0504024-008A AW41208.D 04/04/05 20:51 MW -1D 0504067-001A AW41209.D 04/04/05 21:54 MWAS 0504067-002A A1A41210.D 04/04/05 22:21 MWASMS 0504067-002AMS AW41211.D 04/04/05 22:48 TB 4-05 0504067-003A AW41212.D 04/04/05 23:16 MWASMSD 0504067-002AMSD A\A41213.D 04/04/05 23:44 J{ page .1 of 1 FORM V VOA OLM04.2 • Lab Name: H2M LABS. INC. Lab Code: 10478 Lab File ID (Standard): Instrument ID: HP5971 8 INTERNAL STANDARD AREA AND RT SUMMARY XA41195.1) Date Analyzed: Time Analyzed: SDG No.: TSI -001 4/4/2005 14:31 GC Column: R-502.2 ID: .53 (mm) 329738 Heated Purge: (Y/N) N 15.04 021LFBO40405 312980 9.45 IS1 PFB j 10.45 IS2 DFB 15.04 IS3 CBZ 346009 IS4 DCB 356428 10.39 AREA # RT # AREA # RT # i AREA # RT # AREA # RT # 12 HOUR STD 1 332824 I 9.390 347437 334438 10.390 195269 15.030 169820 17.670 j 4UPPER LIMIT 665648 9.890 694874 10.39 10.890 390538 15.530 339640 18.170 LOWER LIMIT 166412 8.890 173719 #3S D 1 9.890 ! 97635 14.530 1 84910 17.170 I SAMPLE 09iMW-5S i 9.37 340095 10.38 180801 15.02 101MW-61) i NO. 343322 9.39 356004 10.40 187753 15.03 11 !MW -6S 01'VBLK040405 318511 9.40 329738 10.40 174042 15.04 021LFBO40405 312980 9.45 327677 j 10.45 1 186400 15.04 031MS13040405 346009 9.38 356428 10.39 i 191629 15.03 041EQUIPT. BLK i 346871 9.44 354500 i 10.42 187094 15.04 05 !TB 4/1/05 334438 9.33 346170 10.35 184441 15.02 061MW-313 332321 9.39 344711 10.39 181953 15.03 1 321797 9.34 333263 10.35 177396 15.01 #3S D 341487 9.42 349194 10.42 i 185396 i 15.03 09iMW-5S 331418 9.37 340095 10.38 180801 15.02 101MW-61) 343322 9.39 356004 10.40 187753 15.03 11 !MW -6S 336620 9.33 1 349791 10.34 184502 15.01 12'iMW-6D 371501 9.36 376788 10.36 j 197401 15.01 13 MW -8S 322970 9.36 i 335753 10.37 177905 15.02 14MW-113 374082 i 9.49 1 378916 10.47 196078 1 15.05 15jMW-1S 356391 9.36 366917 10.36 191620 15.01 16 MW-1SMS 335769 9.33 j 344703 j 10.34 183056 15.00 171TB 4-4-05 356281 9.36 1 362563 10.37 190636 15.01 18MW-1SMSD 360283 9.35 i 369679 , 10.35 193596 15.01 IS1 PFB = Pentafluorobenzene IS3 CBZ = Chlorobenzene-d5 IS2 DFB = 1,4-Difluorobenzene IS4 DCB = 1,4 -Dichlorobenzene -d4 AREA UPPER LIMIT = +100% of internal standard area AREA LOWER LIMIT = -50% of internal standard area RT UPPER LIMIT = +0.50 minutes of internal standard RT RT LOWER LIMIT = -0.50 minutes of internal standard RT # Column used to flag values outside QC limits with an asterisk. Values outside of QC limits. 140135 164715 163475 157193 158344 157229 148766 160200 154946 164207 159181 168357 155432 165597 169216 158058 159729 170225 &/06/0515:17 FORM VIII SW8260B 17.67 17.67 17.67 17.67 17.65 17.65 17.64 17.65 17.65 17.66 17.64 17.65 17.64 17.65 17.64 17.63 17.64 17.64 H2M LABS, INC. Date: 04 -Apr -05 • Test Code: 8260_W_360B/ METHOD DETECTION Test Number: SW8260B REPORTING LIMITS Test Name: PART 360 BASELINE VOLATILES WATER Matrix: Aqueous Units: gg/L Updated: 19 -Oct -01 Type Analyte MDL PQL loft A 1,1,1,2 -Tetrachloroethane 0.30 5 A 1,1,1 -Trichloroethane 0.24 5 A 1,1,2,2 -Tetrachloroethane 0.93 5 A 1,1,2 -Trichloroethane 0.63 5 A 1, 1 -Dichloroethane 0.34 5 A 1,1-Dichloroethene 0.64 5 A 1,2,3-Trichloropropane 1.1 5 A 1,2-Dibromo-3-chloropropane 1.6 5 A 1,2-Dibromoethane 0.68 5 A 1,2 -Dichlorobenzene 1.0 5 A 1,2-Dichloroethane 0.93 5 A 1,2-Dichloropropane 0.32 5 A 1,4 -Dichlorobenzene 0.67 5 A 2-Butanone 2.2 5 A 2-Hexanone 2.4 5 A 4-Methyl-2-pentanone 0.61 5 A Acetone 3.8 5 A Acrylonitrile 2.1 5 A Benzene 0.26 5 A Bromochloromethane 0.51 5 A Bromodichloromethane 0.37 5 A Bromoform 1.8 5 A Bromomethane 1.2 5 A Carbon disulfide 0.58 5 A Carbon tetrachloride 0.31 5 A Chlorobenzene 0.42 5 A Chloroethane 1.9 5 A Chloroform 0.34 5 A Chloromethane 0.87 5 A cis-1,2-Dichloroethene 0.29 5 A cis-1,3-Dichloropropene 0.29 5 A Dibromochloromethane 0.49 5 A Dibromomethane 0.64 5 A Ethylbenzene 0.41 5 A lodomethane 0.47 5 A Methylene chloride 0.58 5 A Styrene 0.35 5 A Tetrachloroethene 0.70 5 A Toluene 0.43 5 .A A trans-1,2-Dichloroethene trans- l,3-Dichloropropene 0.55 5 0.51 5 A trans-l,4-Dichloro-2-butene 1.2 5 loft H2M LABS, INC. Test Code: 8260 W 360B Test Number: SW8260B Test Name: PART 360 BASELINE VOLATILES WATER Matrix: Aqueous Units: gg/L Type Analyte Date: 04 -Apr -05 METHOD DETECTION / REPORTING LIMITS Updated: 19 -Oct -01 MDL PQL A Trichloroethene 0.48 5 A Trichlorofluoromethane 0.48 5 A Vinyl acetate 0.69 5 A Vinyl chloride 0.91 5 A Xylene (total) 0.35 5 I 1,4 -Dichlorobenzene -d4 - 5 I 1,4-Difluorobenzene - 5 I Chlorobenzene-d5 - 5 1 Pentafluorobenzene - 5 S 1,2-Dichloroethane-d4 3.6 5 S 4-Bromofluorobenzene 1.2 5 S Toluene -d8 1.4 5 X 1, 1 -Dichloropropene 0.49 5 X 1,2-Dichloroethene (total) 1.5 5 X m,p-Xylene 1.0 5 • X o -Xylene 0.42 5 • 2f2 H2M LABS, INC. 0 II. SAMPLE DATA PACKAGE FOR VOLATILE ORGANICS A. REPORTS B. RAW DATA • • 0 H2M LABS, INC. QUALIFIERS FOR REPORTING ORGANICS DATA Value - If the result is a value greater than or equal to the quantification limit, report the value. U - Indicates compound was analyzed for but not detected. The sample quantitation limit must be corrected for dilution and for percent moisture. For example, IOU for phenol in water if the sample final volume is the protocol -specified final volume. If a I to 10 dilution of extract is necessary, the reported limit is 100 U. For a soil sample, the value must also be adjusted for percent moisture. For example, if the sample had 24% moisture and a 1 to 10 dilution factor, the sample quantitation limit for phenol (330 U) would be corrected to: (300 U) 100% moisture x df where D = D 100 and df - dilution factor 100-24 For example, at 24% moisture, D = = 0.76 100 (300 U) x 10 - 4300 U rounded to the appropriate number of significant figures .76 For ser iivolatile soil samples, the extract must be concentrated to 0.5 mL, and the sensitivity of the analysis is not compromised by the cleanup procedures. Similarly, pesticide samples subjected to GPC are concentrated to 5.0 mL. Therefore, the CRQL values in Exhibit C will apply to all samples, regardless • of cleanup. However, if a sample extract cannot be concentrated to the protocol -specified volume (see Exhibit C), this fact must be accounted for in reporting the sample quantitation limit. J - Indicates an estimated value. This flag is used either when estimating a concentration for tentatively identified compounds where a 1:1 response is assumed or when the mass spectral data indicates the presence of a compound that meets the identification criteria but the result is less than the specified quantification limit but greater than zero. (e.g.: If limit of quantification is 10 ug/L and a concentration of 3 ug/L is calculated, report as 3J.) The sample quantitation limit must be adjusted for dilution as discussed for the U flag. N - Indicates presumptive evidence of a compound. This flag is only used for tentatively identified compounds, where the identification is based on a mass spectral library search. It is applied to all TIC results. For generic characterization of a TIC, such as chlorinated hydrocarbon, the N code is not used. P - This flag is used for a pesticide/Aroclor target analyte when there is greater than 25% difference for detected concentrations between the two GC columns (see Form X). The lower of the two values is reported of Form I with a "P". C - This flag applies to pesticide results when the identification has been confirmed by GC/MS.. If GC/MS confirmation was attempted but was unsuccessful, do not apply this flag, instead use a Laboratory defined flag, discussed below. B - This flag is used when the analyte is found in the associated blank as well as in the sample. It indicates possible probable blank contamination and warns the data user to take appropriate action. This flag must be used for a TIC as well as for a positively identified target compound. O 0 O E-� • H2M LABS, INC. E - This flag identified compounds whose concentrations exceed the calibration range of the GC/MS instrument for that specific analysis. If one or more compounds have a response greater than full scale, except as noted in Exhibit D, the sample or extract must be diluted and re -analyzed according to the specifications in Exhibit D. All such compounds with a response greater than full scale should have the concentration flagged with an "E" on the Form I for the original analysis. If the dilution of the extract causes any compounds identified in the first analysis to be below the calibration ranges in the second analysis, then the results of both analyses shall be reported on separate copies of Form I. The Form I for the diluted sample shall have the "DL" suffix appended to the sample number. NOTE: For total xylenes, where three isomers are quantified as two peaks, the calibration range of each peak should be considered separately, e.g. a diluted analysis is not required for total xylenes unless the concentration of the peak representing the single isomer exceed 200 ug/L or the peak representing the two coeluting isomers on that GC column exceed 400 ug/L. Similarly, if the two 1,2-Dichloroethene isomers coelute, a diluted analysis is not required unless the concentration exceed 400 ug/L. D - This flag identifies all compounds identified in an analysis at a secondary dilution factor. If a sample or extract is re -analyzed at a higher dilution factor, as in the "E" flag above, the "DL" suffix is appended to the sample number on the Form I for the diluted sample, and all concentration values reported on that Form I are flagged with the "D" flag. This flag alerts data users that any discrepancies between the concentrations reported may be due to dilution of the sample or extract. A - This flag indicates that a TIC is a suspected aldol -condensation product. X - Other specific flags may be required to properly define the results. If used, they must be fully • described and such description attached to the Sample Data Summary Package and the SDG narrative. Begin by using "X". If more than one flag is required use "Y" and "Z" as needed. If more than five qualifiers are required for a sample result, used the "X" flag to combine several flags as needed. For instance, the "X" flag might combine "A", "B", and "D" flags for some samples. The laboratory defined flags limited to the letters "X", "Y" and "Z". The combination of flags "BU' or "UB" is expressly prohibited. Blank contaminants are flagged "B" omy when they are detected in the sample. • • 1 �J lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: SPA SAMPLE NO. EQUIPT. BLR Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-009A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41199.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Bromomethane Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (AL) 74-88-4 Iodomethane CONCENTRATION UNITS: U CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 T U j --- ---- --�- 75-01-4 ----- -. -- Vinyl chloride - - - 5 - - - j U j 74-83-9 Bromomethane 5 U 75-00-3 j Chloroethane 5 U 67-64-1 Acetone - 5.. - U 107-13-1 Acrylonitrile 5 i U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 78-93-3 2-Butanone 5 U 75-15-0 - - - -_ - -- ---- 1 Carbon disulfide - 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 1 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane i 5 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U • 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4 -Methyl -2 -pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 • FORM I VOA - 2 OLM04.2 00 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET EQUIPT. BLK Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-009A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41199.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (/eg/L or µg/Kg) UG/L Q 591-78-6 1 2 Hexanone ` 5 U 630-20-6 11,1,1,2 -Tetrachloroethane 5 U 100-41-4 ; Ethylbenzene 5 j U 1330-20-7 Xylene (total) 5 5 j U 100-42-5 Styrene II - - - --- -- --i-- 75-25-2 --- -- -- _ - -- - - - Bromoform - 5 - U 1 • 110-57-6 trans-1,4-Dichloro-2-butene I 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 I U 96-18-4 1 2 3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 1 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 ! 1,2-Dibromo-3-chloropropane 5 U • FORM I VOA - 2 OLM04.2 00 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET EQUIPT. BLK TENTATIVELY IDENTIFIED COMPOUNDS Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.-. PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-009A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41199.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L - --- - -- CAS NUMBER J -- — — --- - COMPOUND NAME -- — — – _ RT I EST.CONC. Q • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41199.D Vial: 6 Acq On 4 Apr 2005 16:39 Operator: JV Sample : 0504024-009A Inst : H5971 Misc : TSLOOI,EQUIPT BLANK,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 4 17:05 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:13:18 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195 (Abundance TIC: A41199.1) 290000 2800001 i 2700001 260000 y — 250000 240000 230000 I 2200001 a 210000 200000 190000 i 180000 170000 160000- 1500001 140000 i 130000 i 120000 a 110000 100000 90000 80000 70000 60000 31 50000 40000 30000 1 20000 j �I •10000, l 0 Time—> 4.00 5.00 6.00 7.00 8.00 9.0 A41199.D 36EO228.M Wed Apr 06 14:18:13 2005 SYS1 Page 2 ED C • is LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41199.D Operator : JV Acquired 4 Apr 2005 16:39 using AcgMethod 36E0228 Instrument H5971 Sample Name: 0504024-009A Misc Info : TSLOOI,EQUIPT BLANK,H20,SAMP „ Vial Number: 6 Quant File :36E0228.RES (RTE Integrator) Abundance TIC: A41199.13 9.43 200000 150000 100000- 50000 0-- ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41199.13 200000 10.42 15.04 12.28 150000- 5000010000010.11 100000- 10.11 500001 0 ime-> 10.00 I I, T �T T� r r --r-- 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 undance TIC: A41199.1)1 lAb 47 1 67 200000- 000001500001000001 150000- 1000001 500001 j I i 0- Time-> 16.50 _17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 A41199.D 36E0228.M Wed Apr 06 14:38:01 2005 SYS1 N C) Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41199.D Vial: 6 Acq On 4 Apr 2005 16:39 Operator: JV Sample : 0504024-009A Inst : H5971 Misc : TSLOOI,EQUIPT BLANK,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 4 17:05 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:52:31 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.44 168 346871 50.00 UG/L 0.05 33) 1,4-Difluorobenzene 10.42 114 354500 50.00 UG/L 0.04 54) Chlorobenzene-d5 15.04 82 187094 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.67 152 157193 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.11 65 115079 46.79 UG/L 0.05 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.58% 52) Toluene -d8 12.29 98 339254 48.85 UG/L 0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 97.70% 53) 4-Bromofluorobenzene 16.46 95 215155 47.20 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 94.40% jearget Compounds Qvalue N N . O O -------------- - - - - ------------ M = qualifier out of range (m) = manual integration N A41199.D 36E0228.M Wed Apr 06 14:18:11 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 16:39 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41199.D Name: 0504024-009A &: TSLOOI,EQUIPT BLANK,H2O,SAMP „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41199.D 36E0228.M Wed Apr 06 14:38:01 2005 SYS1 • lA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: • • Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW SAS No.: ID: .53 (mm) (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -1D SDG No.: TSL001 A\A41209.D 04/04/05 04/04/05 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87 3 Chloromethane 5 U- 75-01-4 Vinyl chloride 5 U 74-83-9 I Bromomethane i 5 j U 75-00-3 i Chloroethane 5 U 67-64-1 Acetone S i U 107-13-1 j Acrylonitrile I 5 U 74-88-4 ; Iodomethane ! 5 U 108-05-4 Vinyl acetate 5 U 78-93-3 2 Butanone 5 U -. - - - — - - 75-15-0 ! Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U L 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride t 5 U _ 156-60-5 _ _ I trans-1,2-Dichloroethene 5 - U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 1 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 1 J FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET iLab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 • • Soil Extract Volume: Contract: EPA SAMPLE NO. MW -1D SAS No.: SDG No.: TSL001 Lab Sample ID: 0504067-001A Lab File ID: A\A41209.D Date Received: 04/04/05 Date Analyzed: 04/04/05 ID: .53 (mm) Dilution Factor: 1.00 (µL) Soil Aliquot Volume (µL) FORM I VOA - 2 OLM04.2 N O C/] CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 - 2 Hexanone_ 5 _U 630-20-6 ------ - 1,1,1,2 -Tetrachloroethane --- 5 U 100-41-4 Ethylbenzene 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 j U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 i 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 j U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 N O C/] 1F VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS AM Name: H2M LABS, INC. Contract: LJ Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) LOW % Moisture: not dec. Case No.: PCTSL WATER (g/mL) ML GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µl) EPA SAMPLE NO. MW -1D SAS No.: SDG No.: TSL001 Lab Sample ID: 0504067-OOIA Lab File ID: A\A41209.D Date Received: 04/04/05 Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume: 0 CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L i CAS NUMBER COMPOUND NAME RT j EST.CONC. Q • • FORM I VOA -TIC OLM04.2 (ML) IND N O Cid E'-� Quantitation Report Data File 0:\MS\HP5971\DATA\APR05\040405A\A41209.D Vial: 16 Acq On 4 Apr 2005 21:54 Operator: JV Sample 0504067-001A Inst : H5971 Misc TSLOOI,MW-1D,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 6 11:40 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 300000 280000 260001 24000( 22000( 20000( 18000( 16000( 14000( 12000( 10000( 8000( 6000( 4000( 2000( Time-> M - A41209.D 36E0228.M Wed Apr 06 14:23:09 2005 SYS1 Page 2 I� • • LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41209.D Operator : JV Acquired 4 Apr 2005 21:54 using AcgMethod 36EO228 Instrument : H5971 Sample Name: 0504067-001A Misc Info : TSL001,MW-1D,H20,SAMP „ Vial Number: 16 Quant File :36E0228.RES (RTE Integrator) Abundance TIC:A41209.D 500000 400000 300000 9.48 200000- 100000 ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 bundance TIC:A41209.D 5000001 � 1 400000 300000 200000 10.47 15.05 12.32 100000 10.15 13.93 0 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41209.D 500000 400000 � 300000 16.46 17.65 2000001 II 100000 1 I; i Time-> 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 A41209.D 36E0228.M Wed Apr 06 14:40:17 2005 SYS1 00 N 0 F-+ Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41209.D Vial: 16 Acq On 4 Apr 2005 21:54 Operator: JV Sample : 0504067-001A Inst : H5971 Misc : TSLOOI,MW-1D,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 6 11:40 2005 Quant Results File: 36EO228.RES Quant Method : C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.49 168 374082 50.00 UG/L 0.10 33) 1,4-Difluorobenzene 10.47 114 378916 50.00 UG/L 0.08 54) Chlorobenzene-d5 15.05 82 196078 50.00 UG/L 0.02 67) 1,4 -Dichlorobenzene -d4 17.65 152 165597 50.00 UG/L -0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.15 65 121281 46.14 UG/L 0.09 Spiked Amount 50.000 Range 76 - 114 Recovery = 92.28% 52) Toluene -d8 12.32 98 362327 48.81 UG/L 0.06 Spiked Amount 50.000 Range 88 - 110 Recovery = 97.62% 53) 4-Bromofluorobenzene 16.46 95 220765 45.31 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 90.62% 10arget Compounds Qvalue 58) Dibromochloromethane 13.94 129 5638 1.05 UG/L 88 N 0 O O ------------------------------------------------------------------------- V) (#) = qualifier out of range (m) = manual integration A41209.D 36EO228.M Wed Apr 06 14:23:07 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 21:54 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41209.D e: 0504067-001A : TSL001,MW-1D,H20,SAMP „ Method: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41209.D 36E0228.M Wed Apr 06 14:40:18 2005 SYS1 • O M O O C/1 F-" KJ • Redo 48 01 37 Rab 0 Sub 50 0 -- - - -- Scan 1016 (13.897 min): - - - -- - A41195.[ (-) 5 8 19 Dibromochloromethane Concen: 1.05 UG/L RT: 13.94 min Scan# 1020 Delta R.T. 0.04 min Lab File: A41209.D Acq: 4 Apr 2005 21:54 81 91 116 Iso 173 208 Tgt Ion:129 Resp: 5638 T ' ' 30 80 100 120 140 160 180 200 Ion Ratio Lower Upper Scan 1020 A41209.1) (13.937 min): 1g 129 100 127 66.5 55.5 95.5 f 131 16.0 4.4 44.4 A41209.D 36E0228.M Wed Apr 06 14:23:10 2005 Ion 126.80 (126.50 to 127.50): A41 1200 Ion 130.80 (130.50 to 131.50): A41 1000 13.94 800 600 400 200 0 , Ao_ -> 13.80 13.90 14.00 14. Page 3 M O O E -i IA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: • • Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW SAS No.: ID: .53 (mm) (µL) Lab Sample ID: EPA SAMPLE NO. MW -1S SDG No.: TSL001 Lab File ID: A\A41210.D Date Received: 04/04/05 Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (AL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg)UG/L Q 74-87-3 Chloromethane 5 U 75-01-41 Vinyl chloride _ 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane ! 5 5 U U 67-64-1 j Acetone 107-13-1 1 Acrylonitrile !� 5 U 74-88-4 Iodomethane 5 5 U i U 108-05-4 Vinyl acetate 78-93-3 ! 2-Butanone 5 U 75-15-0 1 Carbon disulfide 5 U 75-69-4 j Trichlorofluoromethane 5 5 U I U 75-35-4 1,1-Dichloroethene 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 j U 156-59-2j cis-1,2-Dichloroethene 5 j U 74-97-5 Bromochloromethane 1 5 U 67-66-3 j Chloroform 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 11,1,1 -Trichloroethane 5 U 1. 56-23-5 Carbon tetrachloride 5 U 71-43-2 4—Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 • • L.] 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW Contract: SAS No.: ID: .53 (mm) (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -1S SDG No.: TSL001 0504067-002A A\A41210.D 04/04/05 04/04/05 1.00 Soil Aliquot Volume (µL) FORM I VOA - 2 OLM04.2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78 6 12 Hexanone 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 j Ethylbenzene 5 �U 7 1330-20-7 Xylene (total) 5 1 5 j U U 100-42-5 Styrene 75-25-2 Bromoform 5 U 110-57-6 j trans-1,4-Dichloro-2-butene 5 5 U U 79-34-5 1,1,2,2 -Tetrachloroethane 96-18-4 1 1 2 3-Trichloropropane 5 ' U 106-46 7 T 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene -5 5 I U -- U 96-12-8 1,2-Dibromo-3-chloropropane FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -1S aName: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504067-002A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41210.D Level: (low/med) LOW Date Received: 04/04/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl1 Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. I Q • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41210.D Vial: 17 Acq On 4 Apr 2005 22:21 Operator: JV Sample : 0504067-002A Inst : H5971 Misc : TSL001,MW-1S,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 6 11:42 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 300000- 280000- 260000- 240000- 2200001 00000 -280000-260000- 240000-2200001 { 200000 180000 160000 140000 120000 i 1000001 I y Ij c 800001.1 60000 I I 40000 I 20000 j Time-=> 4.00 5.00 6.00 7.00 8.00 9.00 10.0C A41210.D 36E0228.M Wed Apr 06 14:23:22 2005 SYS1 Page 2 LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41210.D Operator : JV •Acquired 4 Apr 2005 22:21 using AcgMethod 36EO228 Instrument : H5971 Sample Name: 0504067-002A Misc Info : TSL001,MW-1S,H20,SAMP „ Vial Number: 17 Quant File :36E0228.RES (RTE Integrator) 400000 300000 200000 100000 0 ime—> 4.01 Abundance • 400000 I 300000 I 200000 100000 0 ime—> 10.00 Abundance I. 400000 300000 —� TIC: A41210.D 200000 100000 0 Wirne—> 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.44 17.64 IIII II _16.50 _ 17.00 _ 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 A41210.D 36E0228.M Wed Apr 06 14:40:27 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41210.D Vial: 17 Acq On 4 Apr 2005 22:21 Operator: JV Sample : 0504067-002A Inst : H5971 Misc : TSLOOI,MW-1S,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 6 11:42 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.36 168 356391 50.00 UG/L -0.03 33) 1,4-Difluorobenzene 10.36 114 366917 50.00 UG/L -0.03 54) Chlorobenzene-d5 15.01 82 191620 50.00 UG/L -0.02 67) 1,4 -Dichlorobenzene -d4 17.64 152 169216 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 Spiked Amount 50.000 52) Toluene -d8 Spiked Amount 50.000 53) 4-Bromofluorobenzene Spiked Amount 50.000 Orget Compounds 10.03 65 118665 46.62 UG/L -0.03 Range 76 - 114 Recovery = 93.24% 12.23 98 355175 49.41 UG/L -0.03 Range 88 - 110 Recovery = 98.82% 16.44 95 222297 47.12 UG/L -0.02 Range 86 - 115 Recovery = 94.24% Qvalue M • O ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A41210.D 36E0228.M Wed Apr 06 14:23:21 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 22:21 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41210.D N e: 0504067-002A : TSL001,MW-1S,H20,SAMP od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41210.D 36E0228.M Wed Apr 06 14:40:27 2005 SYS1 is • • • lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -3D SDG No.: TSL001 0504024-001A A\A41201.D 04/01/05 04/04/05 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 1 Vinyl chloride 5 U 74-83-9 Bromomethane I 5 U 75-00-3 Chloroethane 5 U 67-64-1 :_ Acetone 5 U 107-13-1 Acrylonitrile 5 U 74-88-4 j Iodomethane 5 U 108-05-4 ! Vinyl acetate 5 I U 78-93-3 2-Butanone 5 U 75-15-0 Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene S U 75-34-3 ! 1,1-Dichloroethane 1 j J 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 r— F it U- U - - 67 -G6-3 -- — - -- - --- Chloroform - - - 5 U -----107-06-2 1,2-Dichloroethane S U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 i U j 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 2 J 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 • 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (mm) (µL) Soil Extract Volume: Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -3D SDG No.: TSL001 0504024-OOIA A\A41201.D 04/01/05 04/04/05 1.00 Soil Aliquot Volume (µL) 40 FORM I VOA - 2 OLM04.2 C) L/2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 1 2-Hexanone 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 5 U i 1330-20-7 j Xylene (total) ! 3 100-42-5 ! Styrene 5 U 75-25-2 Bromoform 5 F U 110-57-6 trans-1,4-Dichloro-2-butene 1 5 i U •— 79-34-5 1,1,2,2 -Tetrachloroethane _ _ - - 5 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 - - 1,4 -Dichlorobenzene - - - 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 ! U 40 FORM I VOA - 2 OLM04.2 C) L/2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -3D TENTATIVELY IDENTIFIED COMPOUNDS Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-001A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41201.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L � I CAS NUMBER i COMPOUND NAME i RT EST.CONC. Q I • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41201.D Vial: 8 Acq On 4 Apr 2005 17:34 Operator: JV Sample : 0504024-001A Inst : H5971 Misc : TSLOOI,MW-3D,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:46 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 290000- 280000- 270000 90000280000270000 260000 1 w A41201.D 36E0228.M Wed Apr 06 14:21:06 2005 SYS1 Page 2 N O O C/] E-� LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41201.D Operator : JV •Acquired 4 Apr 2005 17:34 using AcgMethod 36E0228 Instrument : H5971 Sample Name: 0504024-001A Misc Info : TSLOOI,MW-3D,H20,SAMP „ Vial Number: 8 Quant File :36E0228.RES (RTE Integrator) Abundance TIC:A41201.D 1000000 800000 600000 400000 200000 9.39 -, - 7.10 7.50 8.12 8.91 0 Time- 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 bundance TIC: A41201.1) 1000000 800000 600000 400000- 200000 10.39 12.25 15.03 � 0.06 L &15.22 L-�-,, 10.98 't 15.80 0 , I - I . I . I 1 1 .. 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41201.13 1000000- 000000800000600000 800000- 600000 f i 4000001 I 1 16.45 17.65 2000001 17.13 0 (lime-> 16.50 17.00 17.50 _18.00 1850 19.00 19:50 20.00 20.50 21.00 21.50 A41201.D 36E0228.M Wed Apr 06 14:38:43 2005 SYS1 M O Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41201.D Vial: 8 Acq On 4 Apr 2005 17:34 Operator: JV Sample : 0504024-001A Inst : H5971 Misc : TSLOOI,MW-3D,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:46 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.39 168 332321 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.39 114 344711 50.00 UG/L 0.00 54) Chlorobenzene-d5 15.03 82 181953 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.65 152 157229 50.00 UG/L -0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.06 65 114361 47.82 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.64% 52) Toluene -d8 12.25 98 335530 49.68 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.36% 53) 4-Bromofluorobenzene 16.45 95 213962 48.27 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 96.54% rget Compounds Qvalue 23) 1,1-Dichloroethane 8.70 63 5897 1.47 UG/L 90 46) Toluene 12.38 92 9826 2.24 UG/L 99 64) Xylene (total) 15.22 106 9005m 3.20 UG/L d' • O ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A41201.D 36E0228.M Wed Apr 06 14:21:05 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 17:34 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41201.D me: 0504024-001A c: TSLOOI,MW-3D,H20,SAMP „ hod: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41201.D 36E0228.M Wed Apr 06 14:38:43 2005 SYS1 C r1 L J • Re f0 0 n/z-> kbundance Rab 0 n/z-> 30 35 40 kbundance Sub 50 0 n/z-> 30 35 40 %bundance Re fo 41 0 n/z--> kbundan Rao 0 n/z-> Scan 488 (8.692 min): A41195.D (-) #23 1,1-Dichloroethane Concen: 1.47 UG/L RT: 8.70 min Scan# 489 Delta R.T. 0.01 min Lab File: A41201.D Acq: 4 Apr 2005 17:34 Tgt Ion: 63 Resp: 5897 Ion Ratio Lower Upper Scan 489 (8.704 min): A41201.D 63 100 65 28.4 11.9 51.9 83 4.5 0.0 32.0 bundancelon 63.00 (62.70 to 63.70): A41201.D Ion 65.00 (64.70 to 65.70): A41201.D Ion 83.00 (82.70 to 83.70): A41201.D 1500 50 55 60 65 70 75 80 85 90 95 100 105 110 8.70 Scan 489 (8.704 min): A41201.D (-) 1000 500 83 T^ rr 0 - 50 55 60 65 70 75 80 85 90 95 100 105 110 ime--> 8.60 8.65 8.70 8.75 8.80 8.85 can 862 S (12.379 min): A41195.D (-) #46 1 Toluene Concen: 2.24 UG/L RT: 12.38 min Scan# 862 69 Delta R.T. 0.00 min Lab File: A41201.D Acq: 4 Apr 2005 17:34 114 Tgt Ion: 92 Resp: 9826 100 110 120 Ion Ratio Lower Upper 201.D 92 100 91 166.9 148.5 188.5 II86 6 51 57 63 1 74 30 40 50 60 70 80 90 ce Scan 862 (12.381 min): A41 3500 lion 91.00 (90.70 to 91.70): A41201.D 3000 J 2500 scan can tstiz (iz.3si min): A41Zu1.0 (-► �1 2000 /12.3 98 Sub { 1500, ' 5011000 { j 39 500 44 51 65 70 - T- - - O 0 0 �w m/z--> , 30 4050 60 70 80 90 100 110 120 fim A41201.D 36E0228.M Wed Apr 06 14:21:08 2005 SYS1 E-� Page 3 Rek • I 0 z-> bundanG Rao 0 51 39 I 1209 (15.800 min): A41195.D (-) 63 60 in 1150 (15.220 min): A41201.D Sub 106 50 39 51 77 82 117 11 44 65 0 �T rr 7-1 1 -TT- -> 30 40 50 60 70 80 90 100 110 120 • 0 A41201.D 36E0228.M #64 Xylene (total) Concen: 3.20 UG/L m RT: 15.22 min Scan# 1150 Delta R.T. -0.58 min Lab File: A41201.D Acq: 4 Apr 2005 17:34 Tgt Ion:106 Resp: 9005 Ion Ratio Lower Upper 106 100 91 230.9 205.3 245.3 105 39.8 36.2 76.2 bundancelon 106.00 (105.70 to 106.70): A41201 4000 Ion 91.00 (90.70 to 91.70): A41201.D Ion 105.00 (104.70 to 105.70): A41201 Wed Apr 06 14:21:09 2005 3000 2000- 1 . 2 0001.2 1000- 0 --> 15.00 1 SYS1 Page 4 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SKEET MW-3S • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-002A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41202.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 Bromomethane { 5 U 75-00-3 Chloroethane 5 U 67-64-1 Acetone 5 U 107-13-1 1 Acrylonitrile ! 5 U • 74-88-4 I Iodomethane 5 U 108-05-4Vinyl acetate - 5 U — — -- -- — 78-93 3 2 Butanone 5 U- 75-15-0 Carbon disulfide 5 U 75-69-4 j Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U C 156-60-5 1 trans -1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 ! cis-1,2-Dichloroethene 5 U 74-97-5 j Bromochloromethane 5 U 67-66-3 Chloroform 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1-Trichloroethane 5 U 56-23-5 ! Carbon tetrachloride 5 U 71-43-2 { Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 7 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2-Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 • Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 • • 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: SAS No.: GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -3S SDG No.: TSL001 0504024-002A A\A41202.D 04/01/05 04/04/05 1.00 Soil Aliquot Volume (µL) FORM I VOA - 2 OLM04.2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg)UG/L Q 591-78-6 2-Hexanone 5 U 1, 1-,1 CU630-20-6 5 100-41-4 1 Ethylbenzene - - -- - 5 U 1330-20-7 i Xylene (total) 10 100-42-5 i Styrene —Bromoform ! -ii 5 U 75-25-2 5 U l 110-57-6 trans-1,4-Dichloro-2-butene i 1,1,2,2 -Tetrachloroethane j 5 5 U U 79-34-5 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 ! 1,4 -Dichlorobenzene 5 U - 95-50-1 — 1,2 -Dichlorobenzene 1,2-Dibromo-3-chloropropane - - -- 5 5 U - U 96-12-8 FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -3S WName: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-002A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41202.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. 1 4 • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File 0:\MS\HP5971\DATA\APR05\040405A\A41202.D Vial: 9 Acq On 4 Apr 2005 18:01 Operator: JV Sample 0504024-002A Inst : H5971 Misc TSLOOI,MW-3S,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:48 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 270000 260000 250000 240000 230000 220000 210000 200000 190000 180000 170000 160000 150000 140000- 130000 120000 110000 100000- 90000- 80000- 70000 60000 50000 40000 30000 i li I I I it I � 20000 j l j l 10000 ? �; I I � 01 1 LLITime-> 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 A41202.D 36EO228.M Wed Apr 06 14:21:30 2005 SYS1 Page 2 • Am Time-> LSC Report - Integrated Chromatogram File 0:\MS\HP5971\DATA\APR05\040405A\A41202.D Operator JV Acquired 4 Apr 2005 18:01 using AcgMethod 36E0228 Instrument H5971 Sample Name: 0504024-002A Misc Info : TSLOOI,MW-3S,H20,SAMP „ Vial Number: 9 Quant File :36E0228.RES (RTE Integrator) 1650 17.00 N O 1 O 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 1 F .� A41202.D 36E0228.M Wed Apr 06 14:38:52 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41202.D Vial: 9 Acq On 4 Apr 2005 18:01 Operator: JV Sample : 0504024-002A Inst : H5971 Misc : TSLOOI,MW-3S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 5 9:48 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.34 168 321797 50.00 UG/L -0.05 33) 1,4-Difluorobenzene 10.35 114 333263 50.00 UG/L -0.04 54) Chlorobenzene-d5 15.01 82 177396 50.00 UG/L -0.02 67) 1,4 -Dichlorobenzene -d4 17.64 152 148766 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 Spiked Amount 50.000 52) Toluene -d8 Spiked Amount 50.000 53) 4-Bromofluorobenzene Spiked Amount 50.000 rget Compounds 6) Toluene 64) Xylene (total) 10.02 65 110186 47.66 UG/L Range 76 - 114 Recovery = 95.32% 12.22 98 324224 49.66 UG/L Range 88 - 110 Recovery = 99.32% 16.44 95 201186 46.95 UG/L Range 86 - 115 Recovery = 93.90% 12.35 92 15.20 106 28875 26133m 6.82 UG/L 9.52 UG/L -0.04 -0.04 -0.02 Qvalue 97 M a 0 ------------------------------------------------------------------------- v� (#) = qualifier out of range (m) = manual integration E-4 A41202.D 36E0228.M Wed Apr 06 14:21:29 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 18:01 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41202.D Name: 0504024-002A 0 c: TSLOOI,MW-3S,H20,SAMP „ hod: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41202.D 36E0228.M Wed Apr 06 14:38:52 2005 SYS1 • • undance Scan 862 (12.379 min): A41195.D (-) 0 bundana Rao 0 z-> bundana Sub 50 #46 Toluene Concen: 6.82 UG/L RT: 12.35 min Scan# 859 Delta R.T. -0.03 min Lab File: A41202.D Acq: 4 Apr 2005 18:01 T Tgt Ion: 92 Resp: 28875 Ion Ratio Lower Upper 92 100 91 164.9 148.5 188.5 1 39 45 I " 11, 6I 70����� 40 50 60 70 80 90 100 110 1 Re4 0 bundance Scan 1148 (15.199 min): A41202.D 1 Ra i 1 I los 40 5165 77 1 82 , 117 01 z-> 3040. 5.0 60 70 80 90 100 110 120 _ _ bundance Scan 1148 (15.199 min): A41202.D (-) 1 1 Sub 1 501 106 � I 39 51 77 65 82 117 II ►n/z--> _ 30 40 50 60 70 80 90 100 110 120 10000 8000 6000 4000 2000 0 to 12.20 12.30 12.40 12.50 #64 Xylene (total) Concen: 9.52 UG/L m RT: 15.20 min Scan# 1148 Delta R.T. -0.60 min Lab File: A41202.D Acq: 4 Apr 2005 18:01 Tgt Ion:106 Resp: 26133 Ion Ratio Lower Upper 106 100 91 229.8 205.3 245.3 105 45.7 36.2 76.2 10000 8000 6000 4000 2000 0 91.00 (90.70 to 91.70): A41202.D 105.00 (104.70 to 105.70): A4120, 1 I A41202.D 36E0228.M Wed Apr 06 14:21:32 2005 SYS1 r..� � I � O 5.50 16.00____) C!1 Page 3 • • lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Soil Extract Volume: CAS NO. COMPOUND Contract: EPA SAMPLE NO. MW -5D SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-003A Lab File ID: A\A41203.D Date Received: 04/01/05 Date Analyzed: 04/04/05 (mm) Dilution Factor: 1.00 (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 5 U -01 -4 chloride 5 5 - - - 5 U U —7.5 -Vinyl 74-83-9 Bromomethane 75-00-3 Chloroethane 79-01-6 5 1 5 U 67-64-1 Acetone j U 107-13-1 Acrylonitrile U 5 U 74-88-4 Iodomethane 5 ; U j 108-05-4 Vinyl acetate 5 U 1 78-93-3 2-Butanone 5 I U 75-15 0 ! Carbon disulfide 5 % U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U 1 156-60-5 ! trans-1,2-Dichloroethene 5 U j 75-34-3 1,1-Dichloroethane 2 J 156-59-2 cis-1,2-Dichloroethene 2 - - - j 5 J —�, U 74-97-5 Bromochloromethane _ 67-66-3 Chloroform 5 U 107-06-2 ; 1,2-Dichloroethane 5 C. - U TT 71-CZ1Z-G T 1 1-Tri-1,1-rr,o 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 108-90-7 Chlorobenzene 3 J 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 6 U 74-95-3 Dibromomethane 5 j U 75-27-4 Bromodichloromethane 5 U _ 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 3 J 127-18-4 Tetrachloroethene 5 U 124-48-1 • Dibromochloromethane 5 - U FORM I VOA - 1 OLM04.2 • 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: LOW Contract: SAS No.: ID: .53 (mm) (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -5D SDG No.: TSL001 A\A41203.D 04/01/05 04/04/05 1.00 Soil Aliquot Volume (µL) FORM I VOA - 2 OLM04.2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2-Hexanone 5 U 630-20-6 j 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 5 U 1330-20-7 Xylene (total) 5 5 U i U 100-42-5 Styrene 75-25-2 Bromoform I 5 ; U 110-57-6 1trans-1,4-Dichloro-2-butene 5 5 U r U 79-34-5 1,1,2,2 -Tetrachloroethane 96-18-4 ! 1 2,3-Trichloropropane 1 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 5 U I U 96-12-8 1,2-Dibromo-3-chloropropane FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -5D Name: H2M LABS, INC. Contract: Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TS1,001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41203.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (Al) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME I RT EST.CONC. Q • • FORM I VOA -TIC OLM04.2 00 C/1 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41203.D Vial: 10 Acq On 4 Apr 2005 18:34 Operator: JV Sample : 0504024-003A Inst : H5971 Misc : TSLOOI,MW-5D,H20,SAMP „ Multiplr: 1.00 .MS Integration Params: RTEINT.P Quant Time: Apr 5 9:51 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 290000 280000 270000 260000 250000 240000 230000 220000 210000 200000 190000 10180000 170000 160000 150000 140000 130000- 120000 110000 100000 9800000000, ] 70000 60000 50000 40000 i 30000 20000 10000 Time->_ 4 A4120_ .D 36EO228.M Wed Apr 06 14:21:42 2005 SYS1 Page 2 m - m m � m _ m a � _ O1 C C z d m e 0 j � � L U j � y o 0 � I �I i !I I i I o LI t i d W n e F I � I 'I I�i'I it I I 00 5.00 6.00 7.00 8.00 9.00 10 .00 1 00_ 12 00 13.0 14.00 15 —,--� .00 16.00 17.00 18.00 19.00 20.00 21 .D 36EO228.M Wed Apr 06 14:21:42 2005 SYS1 Page 2 • • LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41203.D Operator : JV Acquired 4 Apr 2005 18:34 using AcgMethod 36E0228 Instrument : H5971 Sample Name: 0504024-003A Misc Info : TSL001,MW-5D,H2O,SAMP „ Vial Number: 10 Quant File :36E0228.RES (RTE Integrator) bundance TIC:A41203.D 1500000 1000000 500000 9.42 0 7.14 8.18 9.2;� ^6.50 ime-> 4.00 4.50 5.00 5.50 6.00 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41203.13 1500000 1000000 I 500000- 10.42 12.27 15.03 10.09 0 11.00 ime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41203.13 1500000 i 10000001 111 i i 5000001 I i 16.45 17.65 n 0 Time -16.50 17.00 17.50 �- 18.00 18.50 19.00 19.50 20.00 _ 20.50 _ 21.00 21.50 A41203.D 36E0228.M Wed Apr 06 14:39:04 2005 SYS1 O O Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41203.D Vial: 10 Acq On 4 Apr 2005 18:34 Operator: JV Sample : 0504024-003A Inst : H5971 Misc : TSLOOI,MW-5D,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:51 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:50:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.42 168 341487 50.00 UG/L 0.03 33) 1,4-Difluorobenzene 10.42 114 349194 50.00 UG/L 0.03 54) Chlorobenzene-d5 15.03 82 185396 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.65 152 160200 50.00 UG/L -0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.09 65 116679 48.16 UG/L 0.03 Spiked Amount 50.000 Range 76 - 114 Recovery = 96.32% 52) Toluene -d8 12.27 98 338196 49.44 UG/L 0.01 Spiked Amount 50.000 Range 88 - 110 Recovery = 98.88% 53) 4-Bromofluorobenzene 16.45 95 214619 47.80 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 95.60% Compounds Qvalue 18rget 3) 1,1-Dichloroethane 8.74 63 6630 1.60 UG/L 93 27) cis-1,2-Dichloroethene 9.29 96 5340 2.24 UG/L # 86 40) 1,2-Dichloropropane 11.00 63 17008 6.08 UG/L 94 55) Chlorobenzene 15.09 112 14689 2.68 UG/L 96 II � it • O O ---------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration E4 A41203.D 36E0228.M Wed Apr 06 14:21:41 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 18:34 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41203.D Name: 0504024-003A S: TSLOOI,MW-5D,H2O,SAMP „ od: C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41203.D 36E0228.M Wed Apr 06 14:39:04 2005 SYS1 • 0 • nce Re¢p 0 Rao 40 83 #23 1,1-Dichloroethane Concen: 1.60 UG/L RT: 8.74 min Scan# 493 Delta R.T. 0.05 min Lab File: A41203.D Acq: 4 Apr 2005 18:34 Tgt Ion: 63 Resp: 6630 Ion Ratio Lower Upper 63 100 65 28.9 11.9 51.9 83 7.6 0.0 32.0 bun �reIon 63.00 (62.70 to 63.70): A41203.D Ion 65.00 (64.70 to 65.70): A41203.D Ion 83.00 (82.70 to 83.70): A41203.1) 0 -k T--T--T---T-"+- 1500 8.74 n/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 kbundance Scan 493 (8.743 min): A41203.13(-) 63 1000 Sub 50 500 0 40 1r 83 -TTI �� -r -TI 0 _L r n/z--> 30 35 40 45 rT TT 50 55 60 65 70 75 80 85 90 95 100 105 110Time-> TI 8.60 8.65 8.70 8.75 8.80 8.85 8.90 4bundance #27 Scan 545 (9.254 min): A41195.13 (-) 1 96 cis-1,2-Dichloroethene Concen: 2.24 UG/L RT: 9.29 min Scan# 549 Refo Delta R.T. 0.04 min Lab File: A41203.D 35 Acq: 4 Apr 2005 18:34 0 r,rtT 47 52 67 72 Tgt Ion: 96 Resp: 5340 n/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Ion Ratio Lower Upper 4bundance Scan 549 (9.295 min): A41203.13 sl1 96 100 96 61 131.0 134.2 174.2# 98 60.4 44.6 84.6 Rai ao bundancelon 96.00 (95.70 to 96.70): A41203.13 lIon 61.00 (60.70 to 61.70): A41203.D 4000 lion 98.00 (97.70 to 98.70): A41203.13 0 /z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 bundance Scan 549 (9.295 min): A41203.13(-) 3000 6�I1 96 2000 Sub ! �� 50, M 1000 l 44 _ O 0 0�r-TTrT O kn/z-> 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ime-> 9.20 9.25 9.30 9.35 9.40 9.45 A41203.D 36E0228.M Wed Apr 06 14:21:44 2005 E"4 SYSl Page 3 - -- -- -- Scan 720 (10.979 min): A4119 -5.D (-) 4 0 1,2-Dichloropropane Concen: 6.08 UG/L RT: 11.00 min Scan# 722 Refo 76 Delta R.T. 0.02 min • Lab File: A41203.D a1 � Acq: 4 Apr 2005 18:34 as 112 0 3� � 63 - -�+--T - Tgt Ion: 63 Resp: 17008 /z-> 30 40 50 60 70 80 90 100 110 120 • ndance Scan 722 (11.000 min): A41203.13 Ion Rat to Lower Upper Delta R.T. -0.01 min 63 100 Lab File: 112 1.4 0.0 24.9 51 41 59.3 44.0 84.0 Ra� 2005 18:34 41 38 70 601.Tgt 3 90 99 J.J1,9 1291360 76 Abundancelon Resp: 14689 63.00 (62.70 to 63.70): A41203.13 I R Lower Upper ndance Scan 1137 (15.091 min): A41203.D Ion 112.00 (111.70 to 112.70): A41203 1 7 11122 10000 41.00 (40.70 to 41.70): A41203.D 77 83.8 59.3 99.3 49Ion 114 31.4 12.4 52.4 Ra 4000 0 bundancelon 112.00 (111.70 to 112.70): A41203 54 40 I 11.00 -> 30 40 50 60 70 80 90 100 110 120 6 4 - ndance Scan 722 (11.000 min): A41203.13 (-) 41 3000 76 Sub 2000 50 1000- 00049 4 9 1L 00 1 -> 30 40 50 60 70 80 90 100 110 120 ime-> 10.90 11.00 11.10 #55 ndance Scan 1138 (15.100 min): A41195.D (-) 12 Chlorobenzene Concen: 2.68 UG/L 77 RT: 15.09 min Scan# 1137 ResfO Delta R.T. -0.01 min Lab File: A41203.D 51 Acq: 4 Apr 2005 18:34 38 70 601.Tgt 3 90 99 J.J1,9 1291360 Ion:112 Resp: 14689 -> 30 40 50 60 70 80 90 100 110 120 130 140 I R Lower Upper ndance Scan 1137 (15.091 min): A41203.D 1 7 11122 10000 77 83.8 59.3 99.3 82 114 31.4 12.4 52.4 Ra bundancelon 112.00 (111.70 to 112.70): A41203 54 40 I 4000 Ion 77.00 (76.70 to 77.70): A41203.D Ion 114.00 (113.70 to 114.70): A41203 6 4 - 15.09 3000 Scan 1137 (15.091 min): A41203.13 (-) 1 7 2000 Sub 82 501 1000- 54 I j 38 78 616 jn/z-> 30 40 50 - 60 70 80 90 100 110 120 130 140 ime--> 15.00 15.10 15.20 A41203.D 36E0228.M Wed Apr 06 14:21:45 2005 SYS1 Cn Page 4 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -5S • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-004A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41204.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (gg/L or µg/Kg) UG/L Q 74-87-3 87- I C Chloromethane 5 U I -- --- - 75-01-4 ----- - -- Vinyl chloride - - I - - 5 U 74-83-9 Bromomethane 5 U 75-00-3j Chloroethane j 5 U 67-64-1 Acetone 5 U 107-13-1 1 Acrylonitrile 5 U 74-88-4 ; Iodomethane 5 U • 108-05-4 Vinyl acetate 5 U 78-93-3 2-Butanone 5 U - 75-15-0 I — -- -- — - Carbon disulfide - - _ - - - 5 i U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 i Bromochloromethane 5 U j 67-66-3 Chloroform 5 U 107-06-2 ! 1,2-Dichloroethane I 5 U 71-55-6 - 1,1,1 -Trichloroethane 5 U -- 56-23-5 - - - Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane i 5 U FORM I VOA - 1 OLM04.2 r-+ O CM% H IB VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Contract: ID: .53 (mm (/tL) EPA SAMPLE NO. MW -5S SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-004A Lab File ID: A\A41204.D Date Received: 04/01/05 Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (Ag/L or µg/Kg) UG/L Q 591-78-6 1 2-Hexanone 5 U } I 630-20-6 1,1,1,2-Tetrachloroethane5 U 100-41-4 Ethylbenzene 5 I U 1330-20-7 Xylene (total) 5 i U 100-42-5 Styrene 5 ! U 75-25-2 - j Bromoform I 5 U 110-57-6 trans 1,4-Dichloro-2-butene j 5 U • 79-34-5 1,1,2,2 -Tetrachloroethane _ 5 U 96-18-4 1,2 3-Trichloropropane 5 U 106-46-7 ! 1,4 -Dichlorobenzene 5 U - - - 95-50-1 r — — — - --- -- - - 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U • FORM I VOA - 2 OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -5S TENTATIVELY IDENTIFIED COMPOUNDS 40 Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TS1,001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-004A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41204.D Level: (low/med) LOW Date Received: 04/01/05 W Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (Al) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT f EST.CONC. Q • FORM I VOA -TIC OLM04.2 r— C) Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41204.D Vial: 11 Acg On 4 Apr 2005 19:01 Operator: JV Sample : 0504024-004A Inst : H5971 Misc : TSLOOI,MW-5S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 5 9:52 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 280000 270000 260000 250000- 240000- 230000- 220000 50000240000230000220000 210000- 200000 190000 180000 70000 160000 1 150000 140000- 130000- 120000- 110000- 100000, 40000130000120000110000100000 90000 I 800001 I I 70000 60000 50000 j 40000+ 300001 200001 •10000- 0 - Time-> 4.0 A41204 h D 36EO228.M Wed Apr 06 14:21:55 2005 SYS1 Page 2 00 V1 5 I I 0 I, I D 5_00 6.00 7.00 8.00 9.00 10.00 D 36EO228.M Wed Apr 06 14:21:55 2005 SYS1 Page 2 00 V1 • LSC Report - Integrated Chromatogram File 0:\MS\HP5971\DATA\APR05\040405A\A41204.D Operator JV Acquired 4 Apr 2005 19:01 using AcgMethod 36E0228 Instrument H5971 Sample Name: 0504024-004A Misc Info : TSLOOI,MW-5S,H20,SAMP „ Vial Number: 11 Quant File :36E0228.RES (RTE Integrator) Abundance TIC: A41204.1) -� 1200000- 1000M 800000- 600000 400000 200000 9.36 &1 0 . I I I ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC:A41204.D 12000001 1000000 800000 600000 400000 200000 10.37 12.24 15.02 0.04 0 ime--> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC:A41204.D 1200000 i I I 1000000 800000 600000 400000 i 16.45 17.65 2000001. A ^ 1 01- 'Time-> 16.50 17.00 17.50 _18.00 _ 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 A41204.D 36E0228.M Wed Apr 06 14:39:14 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41204.D Vial: 11 Acq On 4 Apr 2005 19:01 Operator: JV Sample : 0504024-004A Inst : H5971 Misc : TSLOOI,MW-5S,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 5 9:52 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\3GE0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards ------------------------------------------------------------------------- R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.37 168 331418 50.00 UG/L -0.02 33) 1,4-Difluorobenzene 10.38 114 340095 50.00 UG/L 0.00 54) Chlorobenzene-d5 15.02 82 180801 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.65 152 154946 50.00 UG/L -0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.04 65 112958 47.88 UG/L -0.02 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.76% 52) Toluene -d8 12.24 98 332002 49.83 UG/L -0.02 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.66% 53) 4-Bromofluorobenzene 16.45 95 208116 47.59 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 95.18% arget Compounds Qvalue O • O ----------------------- '-� (#) = qualifier out of range (m) = manual integration 1--4 A41204.D 36E0228.M Wed Apr 06 14:21:54 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 19:01 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41204.D Name: 0504024-004A A: TSLOOI,MW-5S,H20,SAMP „ Rod: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41204.D 36E0228.M Wed Apr 06 14:39:14 2005 SYS1 • • lA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW ID: .53 (µL) EPA SAMPLE NO. MW -6D SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-005A Lab File ID: A\A41205.D Date Received: 04/01/05 Date Analyzed: 04/04/05 mm) Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane j 5 U 75-01-4 t Vinyl chloride 5 � UU 74-83-9 Bromomethane 5 I U j 75-00-3 Chloroethane j 5 U 67-64-1 j Acetone 10 --i - - - -U 107-13-1 Acrylonitrile 5- 74-88-4 Iodomethane 5 U 108-05-4 • Vinyl acetate 5 U - 78-93-3 2-Butanone S U 75-15-0 Carbon disulfide 5 1 U 75-69-4 ' Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U --1 75-09-2 Methylene chloride 5 U 156-60-5 _ - _.._--- --._- trans-1,2-Dichloroethene 5 75-34-3 1 1,1-Dichloroethane -- 5 �-U —, U 156-59-2 cis-1,2-Dichloroethene j 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform I 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 ! 1,1,1 -Trichloroethane 5 U { 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 1 J 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 14 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane S U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -6D 0 Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-005A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41205.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (AL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2 Hexanone 5 U 630-20-6 1,111,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 3 J _ 1330-20-7 I Xylene (total) v 20 100-42-5 j Styrene 5 U 75-25-2 i Bromoform i 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U • 79-34-5 1,1,2,2 -Tetrachloroethane 5 - U 96-18-4 1,2,3-Trichloropropane ; 5 U { 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane i 5 U FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -6D 0 Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-005A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41205.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME I RT EST.CONC. l Q l • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41205.D Vial: 12 Acq On 4 Apr 2005 19:29 Operator: JV Sample : 0504024-005A Inst : H5971 Misc : TSLOOI,MW-6D,H20,SAMP „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Apr 5 9:55 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuinq Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D Abundance 300000-00 0 28 0 - 260000" 240000 220000- 200000- 160000 140000 120000 100000 80000 60000 400001 r 20000 ; g a Time—> 4.00 5.00 6.00 7.00 0 Ca cd b u 0 H fi, m I! c I mI 9.00 10.00 11.00 12.0 I �I 0 13.00 14.00 15. N �� II 17.00 18.00 19.00 20.00 21 A41205.D 36EO228.M Wed Apr 06 14:22:17 2005 SYSl Page 2 File Operator Wcquired instrument Sample Name: Misc Info . Vial Number: Quant File : LSC Report - Integrated Chromatogram 0:\MS\HP5971\DATA\APR05\040405A\A41205.D JV 4 Apr 2005 19:29 using AcgMethod 36E0228 H5971 0504024-005A TSLOOI,MW-6D,H20,SAMP „ 12 36E0228.RES (RTE Integrator) Abundance TIC: A41205.1) 250000 9.39 200000 150000- 50001000050000 100000- 50000- 0 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 bundance TIC:A41205.D 25000 2000 15.03 10.39 12.26 150000 100000 I� 0.07 I 15.22 50000 15.79 0-- rTime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41205.13 250000 1 45 1765 200000 150000 III SII !� 100000i I i illi 500001 II I a_� 16.68 17.14 17.0 l T17.98 ~ Mime-> _ 16.50 - 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50- A41205.D 36E0228.M Wed Apr 06 14:39:23 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41205.D Vial: 12 Acq On 4 Apr 2005 19:29 Operator: JV Sample : 0504024-005A Inst : H5971 Misc : TSLOOI,MW-6D,H20,SAMP „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Apr 5 9:55 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.39 168 343322 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.40 114 356004 50.00 UG/L 0.01 54) Chlorobenzene-d5 15.03 82 187753 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.66 152 164207 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.07 65 118168 47.85 UG/L 0.01 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.70% 52) Toluene -d8 12.26 98 346506 49.68 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.36% 53) 4-Bromofluorobenzene 16.45 95 217334 47.48 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 94.96% get Compounds Qvalue ) Acetone 7.32 43 4195 10.38 UG/L 91 37) Benzene 10.20 78 8474 1.26 UG/L 88 46) Toluene 12.38 92 62498 13.82 UG/L 95 61) Ethylbenzene 15.11 106 7113 3.30 UG/L 96 64) Xylene (total) 15.22 106 59505m 20.47 UG/L ,kV`r C� • O ------------------------------------------------------------------------- ,--1 W = qualifier out of range (m) = manual integration A41205.D 36E0228.M Wed Apr 06 14:22:16 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 19:29 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41205.D Name: 0504024-005A S: TSLOOI,MW-6D,H2O,SAMP „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41205.D 36E0228.M Wed Apr 06 14:39:24 2005 SYS1 C �J 00 O O E-� 0 t'� .T. i—> 26 28 30 32 undance Sub 50 0 -nlz—> Abundance • Re& i 0 z—> _ Abundance Rao 40 0 nim /z--> 30 _ 35 40 58 Scan 641 (10.201 min): A41: 65 51 I � i0 55 60 65 70 75 80 1000 Ion 57.95 (57.65 to 58.65): A41205.13 7.32 800 600 400 200 0-- b---- unda— nce -- -- - (7-— Scan 348 (7.312 - - -min—): A41195.D------(-) #7 43 Acetone oncen: 1.26 UG/L T: Concen: 10.38 UG/L Scan# 641 elta R.T. 0.00 min RT: 7.32 min Scan# 349 File: RefO cq: 4 Apr Delta R.T. 0.01 min gt Ion: 78 Resp: 8474 58 Lab File: A41205.D Lower Upper 78 a0 Acq: 4 Apr 2005 19:29 30.1 4.4 44.4 36 0 Tgt Ion: 43 Resp: 4195 z—> 26 2830 32 34 36 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 Lori Ratio Lower Upper Abundance Scan 349(7.323 min): A41205.1) j 4,0 43 100 58 22.4 7.3 47.3 Ra - - - 0 t'� .T. i—> 26 28 30 32 undance Sub 50 0 -nlz—> Abundance • Re& i 0 z—> _ Abundance Rao 40 0 nim /z--> 30 _ 35 40 58 Scan 641 (10.201 min): A41: 65 51 I � i0 55 60 65 70 75 80 1000 Ion 57.95 (57.65 to 58.65): A41205.13 7.32 800 600 400 200 0-- 2000 r10I22 )0 105 110 1500 j 1000 Sub 50 65 51 I 500 i 39 � I � 102 0 44 /z-> 0 35 40 45 50 55 60 65 0 75 80 85 90 95 100 105 110 ime—? 10.10 1 A41205.D 36E0228.M Wed Apr 06 14:22:18 2005 SYS1 Page 3 7.20 7.20 7.30 7.40 7.50 I 37 enzene oncen: 1.26 UG/L T: 10.20 min Scan# 641 elta R.T. 0.00 min ab File: A41205.D cq: 4 Apr 2005 19:29 gt Ion: 78 Resp: 8474 on Ratio Lower Upper 78 100 77 30.1 4.4 44.4 2000 r10I22 )0 105 110 1500 j 1000 Sub 50 65 51 I 500 i 39 � I � 102 0 44 /z-> 0 35 40 45 50 55 60 65 0 75 80 85 90 95 100 105 110 ime—? 10.10 1 A41205.D 36E0228.M Wed Apr 06 14:22:18 2005 SYS1 Page 3 0� Scan 862 (12.379 min): A41195.D (-) RefO 69 41 I 6 51 57 63 I 74 86 114 p96 n �,+r 40 50 60 70 80 90 100 110 kbundance Scan 862 (12.380 min): A41205.13 RaA 0 Sub 50 0 Re f0 0 RaA 0 #46 Toluene Concen: 13.82 UG/L RT: 12.38 min Scan# 862 Delta R.T. 0.00 min Lab File: A41205.D Acq: 4 Apr 2005 19:29 Tgt Ion: 92 Resp: 62498 Ion Ratio Lower Upper 92 100 91 161.5 148.5 188.5 20000 15000 10000 5000 12.20 12.30 12.40 12.50 12.60 Scan 1140 (15.120 min): A41195.D (-) I #61 �1 Ethylbenzene Concen: 3.30 UG/L RT: 15.11 min Scan# 1139 Delta R.T. -0.01 min 106 131 Lab File: A41205.D Acq: 4 Apr 2005 19:29 35 a 59 65 79P 121 137 Tgt Ion:106 Resp: 7113 40 50 60 70 80 90 100 110 120 130 140 Scan 1139 (15.110 min): A41205.D Ion Ratio Lower Upper 106 100 91 365.5 355.7 395.7 105 15.0 0.0 35.3 bu25000 Ion 106.00 (105.70 to 106.70): A41205 Ion 91.00 (90.70 to 91.70): A41205.D ',Ion 105.00 (104.70 to 105.70): A41205 1 9�1 1�7 i Sub 82 50 J 52 106 39 65 76. j •hl/z-> _ 30 40 50 60 70 80 90 100 110 120 130 140 20000- 15000- 10000 00001500010000 5000 I 4 0 ime--> 1 5 00 I A41205.D 36E0228.M Wed Apr 06 14:22:19 2005 SYS1 Page 4 Abundance Scan 1209 (15.800 min): A41195.13(-) I 911 0i RaA 0 Sub 50 • 51 77 39 63 86 40 50 60 70 80 9( 106 98 , 100 110 1 106 39 51 63 77 117 30 40 50 60 70 80 90 100 110 120 Scan 1150 (15.219 min): A41205.13 (-) 30 40 50 60 70 80 90 100 110 120 0 A41205.D 36E0228.M #64 Xylene (total) Concen: 20.47 UG/L m RT: 15.22 min Scan# 1150 Delta R.T. -0.58 min Lab File: A41205.D Acq: 4 Apr 2005 19:29 Tgt Ion:106 Resp: 59505 Ion Ratio Lower Upper 106 100 91 223.3 205.3 245.3 105 41.5 36.2 76.2 )undancelon 106.00 (105.70 to 106.70): A41205 Ion 91.00 (90.70 to 91.70): A41205.1) 25000 Ion 105.00 (104.70 to 105.70): A41205 20000- 15000- 10000 00001500010000 1 2 5000 me--> 15.00 15.50 16.00 Wed Apr 06 14:22:20 2005 SYSi Page 5 00 O E-� • lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Contract: EPA SAMPLE NO. MW -6S SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-006A Lab File ID: A\A41206.D Date Received: 04/01/05 Date Analyzed: 04/04/05 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) 75-09-21 Methylene chloride ! 5 U — 156-60-5 1 trans-1,2-Dichloroethene 5 U 75-34-3 1 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene CONCENTRATION UNITS: U CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 Vinyl chloride 5 i U { 74-83-9 Bromomethane 5 U 75-00-3 ; Chloroethane 5 U 67-64-1 Acetone ! 11 J 107-13-1 j Acrylonitrile 5 U 74-88-4 j Iodomethane 5 U 108-05-4 Vinyl acetate 5 ; U -- - - - 78-93-3 j - — - 2 Butanone - - 5- U 75-15-0 1 -- Carbon disulfide I - - 5 --- U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-21 Methylene chloride ! 5 U — 156-60-5 1 trans-1,2-Dichloroethene 5 U 75-34-3 1 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform l 5 U 107-06-2 1,2-Dichloroethane j 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 j Carbon tetrachloride 5 U 71-43-2 Benzene 1 J 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 14 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 N 00 O N 1B VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: EPA SAMPLE NO. MW -6S SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-006A Lab File ID: A\A41206.D GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: (µL) Date Received: 04/01/05 Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q - -630-206 r1,lela2-Tetrachloroethane - - 5 U 100-41-44Ethylbenzene j 4 J ! 1330-20-7 i Xylene (total) 21 100-42-5 Styrene --- - - - 5 ;- U i L 75-25-2 Bromoform 5 U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 79-34-5 • 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1 2,3-Trichloropropane 5 U 106-46-7 11,4 -Dichlorobenzene 5 } U 95-50-1 j 1,2 -Dichlorobenzene 5 U j 96-12-8 1,2-Dibromo-3-chloropropane ! 5 U • FORM I VOA - 2 OLM04.2 M 00 O F-� 1F VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS Name: H2M LABS, INC. Contract: W Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: EPA SAMPLE NO. MW -6S Case No.: PCTSL SAS No.: SDG No.: TS1,001 WATER Lab Sample ID: 0504024-006A (g/mL) ML Lab File ID: A\A41206.D Date Received: 04/01/05 Date Analyzed: 04/04/05 ID. .53 (mm) Dilution Factor: 1.00 Number TICS found: 0 j CAS NUMBER • (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L COMPOUND NAME RT EST.CONC. Q I FORM I VOA -TIC OLM04.2 00 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41206.D Vial: 13 Acq On 4 Apr 2005 19:56 Operator: JV Sample : 0504024-006A Inst : H5971 Misc : TSLOOI,MW-6S,H20,SAMP „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 5 9:56 2005 Quant Results File: 36EO228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 290000 280000 270000 260000 250000 240000- 230000 220000 210000- 200000, 10000200000 190000 7-170000 160000 150000 140000 130000 120000- 110000. 100000 90000 80000 70000 60000 �{ 50000 40000 30000 20000 •10000 Time—> 4 A4120E d I 1 00 5.00 6.00 7.00 ;.D 36EO228.M Wed Apr 06 14:22:31 2005 SYS1 Page 2 File Operator Acquired Instrument Sample Name Misc Info Vial Number Quant File LSC Report - Integrated Chromatogram 0:\MS\HP5971\DATA\APR05\040405A\A41206.D . JV 4 Apr 2005 19:56 using AcgMethod 36E0228 H5971 0504024-006A TSLOOI,MW-6S,H20,SAMP „ 13 :36E0228.RES (RTE Integrator) Abundance TIC:A41206.D 200000 9.33 150000- 100000 50000 0 ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC:A41206.D 200000 10.34 15.01 12.21 150000 100000 .01 15.21 50000 15/78 ime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41206.13 16144 1764 200000 j II I� 150000 1000001 I I� 500001 I i it 16.67 17.13 17.98 `76.9 Tine- •-> 16.50 --_ 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 A41206.D 36E0228.M Wed Apr 06 14:44:17 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41206.D Vial: 13 Acq On 4 Apr 2005 19:56 Operator: JV Sample : 0504024-006A Inst : H5971 Misc : TSLOOI,MW-6S,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:56 2005 Quant Results File: 36EO228.RES Quant Method : C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.33 168 336620 50.00 UG/L -0.06 33) 1,4-Difluorobenzene 10.34 114 349791 50.00 UG/L -0.05 54) Chlorobenzene-d5 15.01 82 184502 50.00 UG/L -0.02 67) 1,4 -Dichlorobenzene -d4 17.64 152 159181 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.01 65 113760 46.88 UG/L -0.05 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.76% 52) Toluene -d8 12.21 98 339557 49.55 UG/L -0.05 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.10% 53) 4-Bromofluorobenzene 16.44 95 210184 46.73 UG/L -0.02 Spiked Amount 50.000 Range 86 - 115 Recovery = 93.46% �rget Compounds Qvalue 7) Acetone 7.27 43 4181 10.55 UG/L 96 37) Benzene 10.15 78 8730 1.32 UG/L 93 46) Toluene 12.34 92 63772 14.35 UG/L 100 61) Ethylbenzene 15.10 106 7544 3.56 UG/L 94 64) Xylene (total) 15.21 106 59925m 20.98 UG/L ��j C� C A 00 0 O ------------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration C/� A41206.D 36EO228.M Wed Apr 06 14:22:29 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 19:56 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41206.D Name: 0504024-006A S: TSLOOI,MW-6S,H2O,SAMP od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41206.D 36EO228.M Wed Apr 06 14:44:18 2005 SYS1 • • 00 00 O H Refo Ra 58 40 0 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 40 43 K I i j 58 0 Tn rT T.1P7 m T^ T Tf r l 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 4bundance Scan 344 (7.274 min): A41206.D (-) Sub 50 #7 Acetone Concen: 10.55 UG/L RT: 7.27 min Scan# 344 Delta R.T. -0.04 min Lab File: A41206.D Acq: 4 Apr 2005 19:56 Tgt Ion: 43 Resp: 4181 Ion Ratio Lower Upper 43 100 58 29.2 7.3 47.3 Ion 57.95 (57.65 to 58.65): A41206.D 800 7-27 600 4 400 200 1 01i i v i i 0 ;,1-T-T-Trrr-TrTr7T F-7 T - T-- , ---- F -T - T ,n/z--> 26 28 30 32 3436 38 40 42 44 46 48 50 52 54 56 58 60 62 64 66 �ime- 7.10 7.20 7.30 7.40 Wbundance • Re& 39 0 rr i T. , /z-> 30 35 40 45 Rab 0 65 65 70 75 6 0.152 min): A41 7 1 #37 Benzene Concen: 1.32 UG/L RT: 10.15 min Scan# 636 Delta R.T. -0.05 min Lab File: A41206.D Acq: 4 Apr 2005 19:56 Tgt Ion: 78 Resp: 8730 110 Ion Ratio Lower Upper 78 100 77 27.8 4.4 44.4 11on 77.0 (76.70 to 77.70): A41206.D 2000 102 10.15 100 105 110 1500 Sub.' 50 a 65 51 319 44 j 102 rn/z-> 30 35 40 45 50 55 60 65 70 75 80 5 90 95 101 5 10 im A41206.D 36E0228.M Wed Apr 06 14:22:32 2005 1000 500 10.00 10.10 1 SYS1 O .30 O Page 3 Scan 862 (12.379 min): A41195-. D (-) #4 6 Toluene Concen: 14.35 UG/L RT: 12.34 min Scan# 858 Delta R.T. -0.04 min Lab File: A41206.1) Acq: 4 Apr 2005 19:56 Tgt Ion: 92 Resp: 63772 Scan 858 (12.341 min): A41206.13 - Ion Ratio Lower Upper 9�1 92 100 91 169.2 148.5 188.5 0 Rab 0 Sub 50 0 /z-> bundance Scan i Refo i 35 0 r 43 Z-> 30 40 391. 44 51 65 1. 70 77 98 Rab 59 65 79 T'r 60 70 8( Scan 1138 (15 106 131 � I A121 37 100 110 120 130 1d ( 40 54 j li 65 01 761 /z-> 30 40 50_ 60 70 80 90 100 110 120 130 140 bundance Scan 1138 (15.101 min): A41206.1) (-) i 91 117 1 Sub 501 82 I I 106 54 I 39 65 7F •-- 0 - m/z 30 40 50 60 70r� -> = _ 80 90 _ 100 _110 120 130 140 A41206.D 36E0228.M Wed Apr 06 14:22:33 20 20000- 0000150002. 15000- 10000 2. 5000 0 me-> 12.10 12.20 12.30 12.40 12.50 12.60 #61 Ethylbenzene Concen: 3.56 UG/L RT: 15.10 min Scan# 1138 Delta R.T. -0.02 min Lab File: A41206.D Acq: 4 Apr 2005 19:56 Tgt Ion:106 Resp: 7544 Ion Ratio Lower Upper 106 100 91 360.6 355.7 395.7 105 15.3 0.0 35.3 Ion 91.00 (90.70 to 91.70): A41206.13 Ion 105.00 (104.70 to 105.70): A41201 20000 15000 10000 O 5000 15.10!_ oj Time--> 15.00 15.05 15.10 15.15 05 SYS1 Page 4 • - �bundance Scan 1209 (15.800 min)—: A411 - 95.D (-) #64 Xylene (total) Concen: 20.98 UG/L m RT: 15.21 min Scan# 1149 Refp� 106 Delta R.T. -0.59 min Lab File: A41206.D 51 77 Acq: 4 Apr 2005 19:56 39 o T ss J� 86 J, 98 1�1Tgt Ion:106 Resp: 59925 n/z-> 30 40 50 60 70 80 90 100 110 120 Ion Ratio Lower Upper lbundance Scan 1149 (15.209 min): A41206.D 91 106 100 91 225.5 205.3 245.3 105 42.8 36.2 76.2 Ra4, 106 bundanceIon 106.00 (105.70 to 106.70): A41206 Ion 91.00 (90.70 to 91.70): A41206.13 { 9 51 65 77 25000 Ion 105.00 (104.70 to 105.70): A41206 117 n/z-> 30 40 50 60 70 80 90 100 110 120 T 20000 \bundance Scan 1149 (15.209 min): A41206.1) (-) 1 15000 Sub 106 10000 1 1 50 5000 65 77 0T3}'- �r f ii. 117 - n/z- 30 40 50 60 70 80 90 100 110 120[Time-> 15.00 15.50 16.00 • A41206.D 36E 0228.M Wed Apr 06 14:22:34 2005 SYSl Page 5 O C/1 H lA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW Contract: EPA SAMPLE NO. MW -8D SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-007A ID: .53 (mm) (µL) Lab File ID: A\A41207.D Date Received: 04/01/05 Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (gL) N CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 -A- Chloromethane - - I - -, 75-01-4 -- - - Vinyl chloride 5 U 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 I U a 67-64-1 Acetone _ 5 - U -- - 107-13-1 -------.. .__. - -- - -- - Acrylonitrile - - - 5 --- - - T U 74-88-4 j Iodomethane 5 U • I 108-05-4 i Vinyl acetate 5 i U ! 78-93-3 ! 2-Butanone 5 U 75-15-0 i Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U { 75-35-4 1,1-Dichloroethene i 5 1 U 75-09-2 Methylene chloride 5 U 156-60-5 r trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 i U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 j U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 - -;-- trans -1 3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 N 1B VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: EPA SAMPLE NO. MW -8D Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-007A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41207.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (ML) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2 Hexanone 5 U j 630-20 6 1,1,1,2 -Tetrachloroethane 5 U j 100-41-4 Ethylbenzene 5 I U 1330-20-7 Xylene (total) 5- 100-42-5 j 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 110-57-6 trans-1,4-Dichloro-2-butene ! 5 U 79-34-5 • 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1 2,3-Trichloropropane 5 U 106-46-7 — - -- - - 1,4 -Dichlorobenzene - S U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U • FORM I VOA - 2 OLM04.2 M O E-� IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -8D 0 Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-007A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41207.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICs found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT i EST.CONC. 1 Q • • FORM I VOA -TIC OLM04.2 CN r-� Cid E-� Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\O40405A\A41207.D Vial: 14 Acq On 4 Apr 2005 20:23 Operator: JV Sample : 0504024-007A Inst : H5971 Misc : TSLOOI,MW-8D,H2O,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:57 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuinq Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 300000 280000 260000 240000 220000 200000' I 180000 160000 140000 120000 100000 80000 600001 40000' 20000 I i 0 ime-_ 4.00 5.00 6.00 7.00 8.00 T x 0 63 0 N ii j i ,I �i i i II ! �_ i 10.00 11.00021 0 13.00 14.00 15.00 16.00 17.00 1 A41207.D 36EO228.M Wed Apr 06 14:22:43 2005 SYS1 Iall O O 00 21.00 Page 2 File Operator *Acquired Instrument Sample Name Misc Info Vial Number Quant File LSC Report - Integrated Chromatogram : 0:\MS\HP5971\DATA\APR05\040405A\A41207.D JV 4 Apr 2005 20:23 using AcgMethod 36E0228 H5971 : 0504024-007A : TSLOOI,MW-8D,H20,SAMP „ : 14 :36E0228.RES (RTE Integrator) Abundance TIC:A41207.D 1200000 1000000 800000 600000 400000 9.36 200000 0 ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC:A41207.D 1200000 1000000 800000 600000 400000 200000 10.36 12.23 15.01 .04 0 10.95 I t . I I I I I . I t I . I . t I . I . t . I . .� I ' Tim 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00L 15.50 Abundance TIC: A41207.13 1200000 1000000 800000 1 6000007 ' 4000001. I 16.44 17.65 200000- 00000- r' 0 T ime-> 16 50 17.00 T T T T T •'T TAT 17.50 18T.00 18i.50m 19.00 19.50 20.00 20.50 21.00 21.50 _22.00 A41207.1) 36E0228.M Wed Apr 06 14:39:54 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41207.D Vial: 14 Acq On 4 Apr 2005 20:23 Operator: JV Sample : 0504024-007A Inst : H5971 Misc : TSLOOI,MW-8D,H20,SAMP „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 5 9:57 2005 Quant Results File: 36EO228.RES Quant Method C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:52:31 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.36 168 371501 50.00 UG/L -0.04 33) 1,4-Difluorobenzene 10.36 114 376788 50.00 UG/L -0.03 54) Chlorobenzene-d5 15.01 82 197401 50.00 UG/L -0.02 67) 1,4 -Dichlorobenzene -d4 17.65 152 168357 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.03 65 123073 47.08 UG/L -0.04 Spiked Amount 50.000 Range 76 - 114 Recovery = 94.16% 52) Toluene -d8 12.23 98 364004 49.31 UG/L -0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 98.62% 53) 4-Bromofluorobenzene 16.44 95 224763 46.39 UG/L -0.02 Spiked Amount 50.000 Range 86 - 115 Recovery = 92.78% �rget Compounds Qvalue r- • O ------------------------------------------------------------------------- C/) (##) = qualifier out of range (m) = manual integration A41207.D 36EO228.M Wed Apr 06 14:22:42 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 20:23 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41207.D Name: 0504024-007A • TSLOOI,MW-8D,H2O,SAMP „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41207.D 36EO228.M Wed Apr 06 14:39:54 2005 SYS1 • 00 O F-� lA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. • Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Contract: Case No.: PCTSL SAS No.: WATER (g/mL) ML LOW ID: .53 (mm) (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW -8S SDG No.: TSL001 0504024-008A A\A41208.D 04/01/05 04/04/05 1.00 Soil Aliquot Volume (µL) 124-48-1 Dibromochloromethane 5 107-06-2 ! CONCENTRATION UNITS: U CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane 5 U 75-01-4 i Vinyl chloride 5 U j 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 67-64-1 { Acetone 5 r U 107-13-1 Acrylonitrile 5 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate 5 U 78-93-3 2-Butanone 5 U 75-15-0 1 Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 5 U 75-09-2 I Methylene chloride �5 U j 156-60-5 trans -1 2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U I 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 124-48-1 Dibromochloromethane 5 107-06-2 ! 1,2-Dichloroethane U 71-55-6 1,1,1 -Trichloroethane 5 56-23-5 Carbon tetrachloride U 71-43-2 Benzene 5 79-01-6 Trichloroethene U 78-87-5 1,2-Dichloropropane 5 74-95-3 Dibromomethane U 75-27-4 Bromodichloromethane 5 10061-01-5 cis-1,3-Dichloropropene U 108-88-3 Toluene 5 10061-02-6 trans-1,3-Dichloropropene U -- 79-00-5 1,1,2 -Trichloroethane 106-93-4 1,2-Dibromoethane 108-10-1 4-Methyl-2-pentanone 108-90-7 Chlorobenzene 127-18-4 Tetrachloroethene • 124-48-1 Dibromochloromethane 5 U 5- U 5 U 5 U 5 U 5 U 5 U 5- U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U 5 U -- FORM I VOA - 1 OLM04.2 CN C) C/] • IB VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 WML) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 (µL) Soil Extract Volume: Contract: EPA SAMPLE NO. MW -8S SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-008A Lab File ID: A\A4120B.D Date Received: 04/01/05 Date Analyzed: 04/04/05 mm) Dilution Factor: 1.00 Soil Aliquot Volume (µL) • FORM I VOA - 2 OLM04.2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg)UG/L Q _ -- -- - -- - 591 78-6 - -- - — - - -- 2 Hexanone - _ - 5 - U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5-25-2- fBromoform - -- 5_ - U 110-57-6 trans-1,4-Dichloro-2-butene 5 U 79-34-5 . } 1,1,2,2 -Tetrachloroethane 5 1 U 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 96-12-8 1,2 -Dichlorobenzene 1,2-Dibromo-3-chloropropane 5 —y U 5 U • FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS MW -8S 0Name: H2M LABS, INC. Contract: La Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TS1,001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-008A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41208.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q • 0 FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41208.D Vial: 15 Acq On 4 Apr 2005 20:51 Operator: JV Sample : 0504024-008A Inst : H5971 Misc : TSLOOI,MW-8S,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 5 9:57 2005 Quant Results File: 36E0228.RES Method : O:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 280000 270000 260000 250000 240000 230000 220000 210000 200000 190000 180000 170000 160000 d O cn m E� c m 0 U A41208.D 36E0228.M Wed Apr 06 14:22:57 2005 SYS1 Page 2 LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41208.D Operator : JV AftAcquired 4 Apr 2005 20:51 using AcgMethod 36E0228 Instrument H5971 Sample Name: 0504024-008A Misc Info : TSLOOI,MW-8S,H20,SAMP „ Vial Number: 15 Quant File :36E0228.RES (RTE Integrator) Abundance TIC: A4A41208.131400000 1200000 1000000 800000 600000 400000 200000 9.36 L.) 0 , , - ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41208.13 1400000 1200000 1000000 800000 600000 ` 400000 200000 10.37 12.23 15.01 0.04 10.97 0 . I . I . I I . . I . I . I I I . ime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00L 14.50 15.00 15.50 Abundance TIC: A41208.13 1400000 I 1200000 1000000 I 800000 600000 iI M O 400000 16.44 17.64 200000 0 I O ime--> 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 I O A41208.1) 36E0228.M Wed Apr 06 14:40:03 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41208.D Vial: 15 Acq On 4 Apr 2005 20:51 Operator: JV Sample : 0504024-008A Inst : H5971 Misc : TSLOOI,MW-8S,H20,SAMP „ Multiplr: 1.00 is MS Integration Params: RTEINT.P Quant Time: Apr 5 9:57 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.36 168 322970 50.00 UG/L -0.03 33) 1,4-Difluorobenzene 10.37 114 335753 50.00 UG/L -0.02 54) Chlorobenzene-d5 15.02 82 177905 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.64 152 155432 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.03 65 108760 46.69 UG/L -0.03 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.38% 52) Toluene -d8 12.23 98 329308 50.06 UG/L -0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.12% 53) 4-Bromofluorobenzene 16.44 95 206068 47.73 UG/L -0.02 Spiked Amount 50.000 Range 86 - 115 Recovery = 95.4616 IVrget Compounds Qvalue O 0 o ------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration [..� A41208.D 36E0228.M Wed Apr 06 14:22:56 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 20:51 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41208.D Name: 0504024-008A S: TSLOOI,MW-8S,H2O,SAMP „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41208.D 36E0228.M Wed Apr 06 14:40:04 2005 SYS1 • • • • lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Soil Extract Volume: CAS NO. Contract: EPA SAMPLE NO. TB 4/1/05 SAS No.: SDG No.: TSL001 Lab Sample ID: 0504024-OIOA Lab File ID: A\A41200.D Date Received: 04/01/05 Date Analyzed: 04/04/05 (mm) Dilution Factor: 1.00 (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L Q 74-87-3 j Chloromethane 5 5 U 75-01-4 Vinyl chloride 5 ` - - 5_- - U 74-83-9 Bromomethane U 75-00-3 Chloroethane 5 --- 5 - - U r U 67-64-1 ! Acetone 107-13-1 Acrylonitrile 5 71-43-2 U 74-88-4 Iodomethane 5 U 108-05-4 Vinyl acetate ; 5 r U - 78-.93-3 Butanone-- 5 i U ,2 - { _ 5 C 75-15-0 - Carbon disulfide 5 U 75-69-4 _ - - - - Trichlorofluoromethane - - j 5 --, U 75-35-4 1,1-Dichloroethene 5 U 1 75-09-2 Methylene chloride 5 U U 156-60-5 i trans-1,2-Dichloroethene 5 U i U 75-34-3 1,1-Dichloroethane 5 U I U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 ! Bromochloromethane 5 U 67-66-3 ! Chloroform 5 1 U FORM I VOA - 1 OLM04.2 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane 5 ~ U 1 56-23-5 - - - - Carbon tetrachloride - 5 + U j - 71-43-2 { Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane _ 5 U 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: • EPA SAMPLE NO. TB 4/1/05 Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-010A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41200.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Xylene (total) Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) 110-57-6 trans-1,4-Dichloro-2-butene CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg)UG/L Q 591-78-6 t 2 Hexanone 5 U 630-20-6 j 1,1,1,2 -Tetrachloroethane 5 U j 100-41-4 Ethylbenzene 5 U 1330-20-7 Xylene (total) - - 5 5 U U 100-42-5 ! Styrene 75-25-2 Bromoform 5 I U 110-57-6 trans-1,4-Dichloro-2-butene 5 5 U I U 79-34-5 1,1,2,2 -Tetrachloroethane 96-18-4 1 2,3-Trichloropropane 5 - U 106-46-7 1,4 -Dichlorobenzene 5 j U 95-50-1 1,2 -Dichlorobenzene 5 T 5 U U 96-12-8 ! 1,2-Dibromo-3-chloropropane FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TB 4/1/05 TENTATIVELY IDENTIFIED COMPOUNDS Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504024-010A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41200.D Level: (low/med) LOW Date Received: 04/01/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (Al) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME RT EST.CONC. Q J • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41200.D Vial: 7 Acq On 4 Apr 2005 17:06 Operator: JV Sample : 0504024-010A Inst : H5971 Misc : TSLOOI,TRIP BLANK,H20,SAMP „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 4 17:29 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:13:18 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D { 290000 280000 i 270000 j 260000 vi - Y 250000 m 240000 - 230000- 220000 - - 210000 a 200000 190000 " U i 180000 0 170000 160000 150000 140000 1 130000 { 120000 1 1100001 ` u 100000 i 90000 N 80000 70000 ! 60000 50000 1 I { 400001 II 30000 II 20000 1•, j ; 10000 L�j I{ --___.�'LL- 0�_ J r 1 - Mime-> 4.00 5.00 6.00_ 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 1 1 A41200.D 36E0228.M Wed Apr 06 14:18:44 2005 SYS1 Page 2 • • LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41200.D Operator : JV Acquired 4 Apr 2005 17:06 using AcgMethod 36E0228 Instrument : H5971 Sample Name: 0504024-010A Misc Info : TSLOOI,TRIP BLANK,H20,SAMP „ Vial Number: 7 Quant File :36E0228.RES (RTE Integrator) (Abundance I TIC:A41200-D 200000 9.33 150000 100000 50000- 0 - - - T T r�r- ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41200.13 200000 10.35 15.01 12.22 150000- 100000 .01 50000- 0- ime-> 10.00 r r��= 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41200.D 1 45 1 65 200000 1 1 li � 1500001 II 1000001 ` I 50000 1 i I ` I pr:-�- _ --- - �---- -- ---- --- - -_ - --- _�_ 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00 4 Time--> 16.50 17.00 17,50 A41200.D 36E0228.M Wed Apr 06 14:38:33 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41200.D Vial: 7 Acq On 4 Apr 2005 17:06 Operator: JV Sample : 0504024-010A Inst : H5971 Misc : TSLOOI,TRIP BLANK,H20,SAMP „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 4 17:29 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.33 168 334438 50.00 UG/L -0.06 33) 1,4-Difluorobenzene 10.35 114 346170 50.00 UG/L -0.04 54) Chlorobenzene-d5 15.02 82 184441 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.65 152 158344 50.00 UG/L -0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.02 65 113684 47.34 UG/L -0.04 Spiked Amount 50.000 Range 76 - 114 Recovery = 94.68% 52) Toluene -d8 12.22 98 336276 49.58 UG/L -0.04 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.16% 53) 4-Bromofluorobenzene 16.45 95 211738 47.57 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 95.14% 0rget Compounds Qvalue • O ------------------------------------------------------------------------- W = qualifier out of range (m) = manual integration V) E-� A41200.D 36E0228.M Wed Apr 06 14:18:42 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 17:06 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41200.D Name: 0504024-010A TSLOOI,TRIP BLANK,H20,SAMP „ Mod: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41200.D 36E0228.M Wed Apr 06 14:38:33 2005 SYS1 • • N O Cn H • • IA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: WATER LOW (g/mL) ML ID: .53 (mm) (µL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. TB 4-4-05 SDG No.: TSL001 0504067-003A A\A41212.D 04/04/05 04/04/05 1.00 Soil Aliquot Volume (µL) 156-59-2 cis-1,2-Dichloroethene CONCENTRATION UNITS: U CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 Chloromethane f 5 U - __ - -- 75-01-4 ? - - - - - ---- - -- Vinyl chloride - -- --i -- - -- - 5 U 74-83-9 Bromomethane Carbon tetrachloride 5 I U 75-00-3 Chloroethane 5 U 5 5 UU ! U 67-64-1 Acetone 107-13-1 Acrylonitrile 1,2-Dichloropropane ! 5 U I 74-88-4 Iodomethane U 5 U 108-05-4 Vinyl acetate 10061-01-5 - - - - 5 --� { U 78-93-3 2-Butanone Toluene 5 U 75-15-0 Carbon disulfide 5 5 U 75-69-4 Trichlorofluoromethane { 5 U 75-35-4 i 1,1-Dichloroethene 5 U 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 j 1,1-Dichloroethane j 5 I U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 107-06-2 1,2-Dichloroethane j 5 U 71-55-6 1,1,1 -Trichloroethane 5 U j 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 Bromodichloromethane T 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U FORM I VOA - 1 OLM04.2 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U • 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 IB VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: EPA SAMPLE NO. TB 4-4-05 Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504067-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41212.D Level: (low/med) LOW Date Received: 04/04/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2 Hexanone 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5— U— 100-41-4 Ethylbenzene 5 I U 1330-20-7 Xylene (total) 5 U 100-42-5 ! Styrene 5 U 75-25-2 i Bromoform 5 U 110-57-6 trans -1 4 Dichloro 2 -butene 5 U 79-34-5 1,1,2,2 -Tetrachloroethane 5 U i 96-18-4 1,2,3-Trichloropropane 5 U 106-46-7 1,4 -Dichlorobenzene 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U i L FORM I VOA - 2 OLM04.2 1F EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS TB 4-4-05 Name: H2M LABS, 0,b INC. Contract: Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TS1,001 Matrix: (soil/water) WATER Lab Sample ID: 0504067-003A Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41212.D Level: (low/med) LOW Date Received: 04/04/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L CAS NUMBER COMPOUND NAME j RT EST.CONC. Q • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41212.D Vial: 19 Acq On 4 Apr 2005 23:16 Operator: JV Sample : 0504067-003A Inst : H5971 Misc : TSLOOI,TB 4/4/05,H20,SAMP „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 6 11:43 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D ndance TIC: A411212.13 290000- 280000- 270000- A41212.D 36E0228.M Wed Apr 06 14:23:47 2005 SYS1 Page 2 LSC Report - Integrated Chromatogram File : 0:\MS\HP5971\DATA\APR05\040405A\A41212.D Operator : JV cquired 4 Apr 2005 23:16 using AcgMethod 36EO228 Instrument : H5971 Sample Name: 0504067-003A Misc Info : TSLOOI,TB 4/4/05,H2O,SAMP Vial Number: 19 Quant File :36EO228.RES (RTE Integrator) bundance - TIC: A41212.13 200000 150000 100000 50000 ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41212.D 200000 15.01 10.37 12.23 150000 100000 03 50000 0 ime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A41212.D 1 FU 44 17.64 200000- 150000- 100000 00000150000 100000 500001 r --i 00 ' ---- -�--- - - - -- o Clime-> 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 - 20.50 21.00 21.50 22.00 A41212.D 36EO228.M Wed Apr 06 14:40:38 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41212.D Vial: 19 Acq On 4 Apr 2005 23:16 Operator: JV Sample : 0504067-003A Inst : H5971 Misc : TSLOOI,TB 4/4/05,H20,SAMP „ Multiplr: 1.00 *MS, Integration Params: RTEINT.P Quant Time: Apr 6 11:43 2005 Quant Results File: 36EO228.RES Quant Method : C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.36 168 356281 50.00 UG/L -0.03 33) 1,4-Difluorobenzene 10.37 114 362563 50.00 UG/L -0.02 54) Chlorobenzene-d5 15.01 82 190636 50.00 UG/L -0.02 67) 1,4 -Dichlorobenzene -d4 17.64 152 159729 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 Spiked Amount 50.000 52) Toluene -d8 Spiked Amount 50.000 53) 4-Bromofluorobenzene Spiked Amount 50.000 *rget Compounds 10.03 65 119449 47.49 UG/L -0.03 Range 76 - 114 Recovery = 94.98% 12.23 98 351835 49.53 UG/L -0.03 Range 88 - 110 Recovery = 99.06% 16.44 95 217398 46.63 UG/L -0.02 Range 86 - 115 Recovery = 93.26% Qvalue 00 i _______________________________________________________________________ (#) = qualifier out of range (m) = manual integration A41212.D 36EO228.M Wed Apr 06 14:23:45 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 23:16 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41212.D N e: 0504067-003A : TSLOOI,TB 4/4/05,H20,SAMP „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41212.D 36E0228.M Wed Apr 06 14:40:38 2005 SYS1 H2M LABS, INC. 0 III. STANDARD DATA PACKAGE FOR VOLATILE ORGANICS A. INITIAL CALIBRATION FORM B. STANDARD GC/MS CHROMATOGRAMS C. DATA SYSTEM REPORT D. CONTINUING CALIBRATION FORM E. STANDARD GC/MS CHROMATOGRAMS F. DATA SYSTEM REPORT • • • • • 6A VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSLO01 Instrument ID: HP5971 Calibration Date(s): 02/28/05 02/28/05 Heated Purge: (Y/N) N Calibration Times: 10:38 14:43 GC Column: R-502.2 ID: .53 (mm) LAB FILE ID: VSTD050 A40927.D COMPOUND Chloromethane Vinyl chloride VSTDOIO A40925.D VSTD100 A40928.D l VSTDO11STD02-ISTDO5 0.282 0.209 0.343 0.256 VSTD020 A40930.1) VSTD200 A40929.D j I i 1 STD10CYSTD200 RRF r 0.223 0.215 0.223 I 0.230 0.267 0.264 0.273 0.281 i RSD I 12.7 �. 12.5 Bromomethane 0.405 0.298 0.329 , 0.319 0.326 1 0.335 12.2 'Chloroethane Acetone 0.231 0.092 0.178 0.080 0.193 0.076 0.191 0.081 0.202 0.080 0.199 1 : 0.082 i 10.1 - -I 7.6 crylonitrile 0.488 0.367 0.412 0.398 0.408 0.415 'j 10.8 lodomethane 0.864 0.656 0.715 1 0.673 0.698 j 0.721 11.6 Vinyl acetate 0.270 0.198 0.201 0.243 0.241 0.230 13.2 '2-Butanone 0.180 0.140 0.132 j 0.129 0.127 0.141 15.7 !Carbon disulfide 1.077 0.796 i 0.848 0.788 0.804 0.863 14.2 {Trichlorofluoromethane 0.862 0.638 0.741 0.696 0.742 0.736 i 11.2 1,1-Dichloroethene 0.396 0.296 ! 0.314 { 0.309 0.317 I 0.326 ' 12.3 Methylene chloride 0.461 0.330 0.363 0.349 0.369 0.375 i 13.6 itrans-1,2-Dichloroethene 0.459 0.345 0.370 0.361 0.377 0.382 11.6 1,1-Dichloroethane 0.830 0.635 0.694 1 0.673 0.699 0.706 i 10.4 ;cis-1,2-Dichloroethene 0.494 0.365 0.403 0.392 0.416 j 0.414 1 11.7 Bromochloromethane 0.320 0.242 0.266 0.267 0.284 0.276 1 10.5 ;Chloroform 1.033 0.778 0.879 1 0.838 0.871 j 0.880 10.8 1:1,2-Dichloroethane 0.581 0.425 0.518 0.491 0.520 ! 0.507 11.2 ;1,1,1 -Trichloroethane 0.884 0.653 0.756 0.716 0.743 0.750 11.3 Carbon tetrachloride (Benzene " 0.889 1.331 0.649 1.015 I 0.740 ! l 1.058 1 0.704 1.036 0.716 1.072 I 0.740 ! 1.102 12.1 11.8 Trichloroethene 0.609 0.458 0.498 ! 0.491 0.506 ! 0.513 11.1 1,2-Dichloropropane Obromomethane 0.536 0.545 0.407 0.416 0.439 ! 0.463 0.435 0.466 0.444 0.485 ! 0.452 0.475 10.8 9.8 Bromodichloromethane 1.135 0.856 0.976 0.939 0.977 I 0.977 10.4 cis-l3-Dichloropropene .Toluene 0.878 0.928 0.686 0.712 0.757 1 0.747 ! 0.744 0.738 0.782 0.758 ! 0.770 0.777 ; 9 11.1 'trans-1,3-Dichloropropene 0.806 0.604 I 0.685 0.661 0.689 0.689 10.7 1,1,2 -Trichloroethane 1,2-Dibromoethane 0.473 0.768 0.357 0.576 0.386 0.650 0.389 0.673 0.400 0.697 0.401 0.673 10.8 10.4 !4-Methyl-2-pentanone 0.660 0.500 0.511 0.518 0.530 0.544 12.1 Chlorobenzene Tetrachloroethene 2.146 1.126 1.624 0.892 1.650 0.833 1.580 0.976 1.514 0.957 ! 1.703 0.957 14.8 11.5 1,1-Dichloropropene 0.689 0.527 0.558 0.534 0.544 ! 0.571 11.8 umromocniorometnane 1.806 1 1.370 1.450 1.422 1 1.338 1.477 12.8 ' FORM VI VOA - 1 OLM04.2 N O E-4 6B VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Lab Code: 10478 Case No Instrument ID: HP5971 Heated Purge: (YIN) N GC Column: R-502.2 Contract: PCTSL SAS No.: SDG No.: TSL001 Calibration Date(s): 02/28/05 02/28/05 Calibration Times: 10:38 14:43 ID: .53 (mm) LAB FILE ID: VSTDO10 A40925.1) VSTD020 A40930.D ` VSTD050 A40927.D VSTD100 A40928.D VSTD200 A40929.1) { COMPOUND STDO1 STD02 - T ---- 1- - --- (J WSTD05�STD10WSTD20Q RRF " RSD 2-Hexanone 1,1,1,2 -Tetrachloroethane 0.557 1.274 0.425 0.960 0.398 1.013 0.409 0.962 0.357 0.931 0.429 1.028 17.7 13.7 j Ethylbenzene 0.974 0.700 0.727 0.652 0.631 0.737 ! 18.7 �Y-Iene (total) 'Styrene 1.140 1.911 0.858 1.476 0.867 1.479 0.817 1.423 0.783 1.360 0.893 I 1.530 15.9 14.3 Bromoform 1.319 1.008 1.035 1.043 0.983 1.077 12.7 trans-1,4-Dichloro-2-butene 0.293 0.225 0.250 0.243 0.242 j 0.251 10.2 1,1,22 -Tetrachloroethane 1.644 1.220 1.283 1.277 1.296 1 1.344 12.6 11,2,3-T6chloropropane 0.256 0.206 j 0.213 0.228 0.216 0.224 8.8 1 4 -Dichlorobenzene 2 327 1 776 1 1 827 1 834 1 857 1 924 11.8 • FORM VI VOA - 2 OLM04.2 ;1,2 -Dichlorobenzene 2.124 1.699 1.619 1.669 1.691 1 1.760 11.7 • j1,2-Dibromo-3-chloropropane 0.369 0.294 0.297 i 0.306 0.303 i i 0.314 9.9 I.m,p-Xylene 1.227 0.933 0.924 0.895 0.844 j 0.965 15.6 I ' !o -Xylene 1.140 0.858 0.867 0.817 1 0.783 0.893 15.9 " * Compounds with required minimum RRF and maximum %RSD values. All other compounds must meet a minimum RRF of 0.010. • FORM VI VOA - 2 OLM04.2 LAB FILE ID: VSTDO10 A40925.D VSTD020 A40930.D 6B • VSTD100 A40928.D VOLATILE ORGANICS INITIAL CALIBRATION DATA Lab Name: H2M LABS, INC. Contract: jSTD050JSTD10WSTD20gl RRF Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 0.345 Instrument ID: HP5971 Calibration Date(s): 02/28/05 02/28/05 1.447 Heated Purge: (Y/N) N Calibration Times: 10:38 14:43 27.5 GC Column: R-502.2 ID: .53 (mm) LAB FILE ID: VSTDO10 A40925.D VSTD020 A40930.D VSTD050 A40927.D VSTD100 A40928.D VSTD200 A40929.1) ` COMPOUND �STDO1�jSTD02 jSTD050JSTD10WSTD20gl RRF I RSD 1,2-Dichloroethane d4 0.531 0.345 0.386 0.3 0.437 0.416 i 84 17.2 Toluene -d8 1.447 0.908 1 0.976 0.740 0.865 0.987 27.5 4-Bromofluorobenzene 0.954 0.611 1 0.681 0.587 0.685 0.704 1 20.8 * Compounds with required minimum RRF and maximum %RSD values. All other compounds must meet a minimum RRF of 0.010. • FORM VI VOA - 3 OLM04.2 Q Q E"� Quantitation Report Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40925.D Vial: 3 Acq On : 28 Feb 2005 10:38 Operator: JV Sample : VSTDO10 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 28 12:17 2005 Quant Results File: 36EO228.RES Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:59:34 2005 Response via : Continuinq Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Abundance TIC:A40925.D 270000 260000 250000 F 240000 m m 230000 n 220000 210000 200000 190000 180000 m 170000 o m 60000 150000 140000 130000 120000 d C6 110000 d m E F � d 100000 m t 90000 tT a xC , o 80000 41 F o 70000v 60000 d 2ID O~ E ~ L C n a C O L o°° o m o I? a U q ~ c c C O L U L d UO O N IO N U�LL o O U OH G o 50000 t , 7 o E L 40000 O F- C L N_ S v a $ V C� O O O O O N N y � C 0 o � 30000 2 d o d E _° c� 1 L O 20000iE U>� I 10000 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 22.00 23.00 A40925.D 36E0228.M Wed Apr 06 16:29:51 2005 H5971 Page 3 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40925.D Vial: 3 Acq On : 28 Feb 2005 10:38 Operator: JV Sample : VSTDO10 Inst : H5971 OMisc : ,,,ICAL „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Feb 28 12:17 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Feb 28 12:15:34 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\FEBO5\022805A\A40927.D DataAcq Meth FK 0215 Internal Standards ------------------------------------------------------------------------- R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 272988 50.00 UG/L 0.15 33) 1,4-Difluorobenzene 10.31 114 280526 50.00 UG/L 0.13 54) Chlorobenzene-d5 14.82 82 153503 50.00 UG/L 0.06 67) 1,4 -Dichlorobenzene -d4 17.54 152 126910 50.00 UG/L 0.02 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 9.99 65 29772 13.75 UG/L 0.14 Spiked Amount 50.000 Range 76 - 114 Recovery = 27.500# 52) Toluene -d8 12.08 98 81200 14.83 UG/L 0.09 Spiked Amount 50.000 Range 88 - 110 Recovery = 29.66°# 53) 4-Bromofluorobenzene 16.34 95 53537 14.00 UG/L 0.03 Spiked Amount 50.000 Range 86 - 115 Recovery = 28.00%# rget Compounds Qvalue ) Dichlorodifluoromethane 4.20 85 28712 12.26 UG/L 99 3) Chloromethane 4.67 50 15395 12.67 UG/L 94 4) Vinyl chloride 4.98 62 18703 12.85 UG/L 100 5) Bromomethane 6.09 94 22119 12.32 UG/L 97 6) Chloroethane 6.26 64 12630 12.00 UG/L 100 7) Acetone 7.33 43 5032 12.20 UG/L # 52 8) Acetonitrile 7.63 41 6975 75.15 UG/L 83 9) Allyl Chloride 7.87 41 32883 12.46 UG/L 93 10) Acrolein 7.26 56 11601 70.75 UG/L 99 11) Acrylonitrile 8.75 53 26651 11.85 UG/L 99 12) Iodomethane 7.82 142 47199 12.09 UG/L 94 13) Vinyl acetate 8.64 43 14717 13.42 UG/L 91 14) Chloroprene 8.75 53 26651 11.85 UG/L 93 15) 2-Butanone 9.02 43 9831 13.67 UG/L 81 16) Carbon disulfide 8.03 76 58814 12.70 UG/L 100 17) Trichlorofluoromethane 6.72 101 47069 11.63 UG/L 96 18) 1,1-Dichloroethene 7.48 96 21639 12.64 UG/L 97 19) methyl tert-butyl ether 8.13 73 53440 11.85 UG/L 96 21) Methylene chloride 7.98 84 25181 12.69 UG/L 93 22) trans-1,2-Dichloroethene 8.28 96 25051 12.39 UG/L # 84 23) 1,1-Dichloroethane 8.67 63 45329 11.96 UG/L 96 24) Propionitrile 9.08 54 1217 9.39 UG/L 88 25) Isobutyl alcohol 9.28 43 5642 81.14 UG/L # 27 26) Methacrylonitrile 9.25 67 7285 14.09 UG/L 90 27) cis-1,2-Dichloroethene 9.22 96 26965 12.24 UG/L 84 Bromochloromethane 9.52 128 17481 12.06 UG/L 98 �) ---) 2,2-Dichloropropane----------9_18---77 -------- ---------------------------- 38082 12.51 UG/L -98 (#) = qualifier out of range (m) = manual integration A40925.D 36E0228.M Wed Apr 06 16:29:47 2005 H5971 Page 1 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40925.D Vial: 3 Acq On : 28 Feb 2005 10:38 Operator: JV Sample : VSTDO10 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Feb 28 12:17 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth : FK 0215 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.35 83 56426 11.76 UG/L 98 31) 1,2-Dichloroethane 10.07 62 31731 11.21 UG/L 99 32) 1,1,1 -Trichloroethane 9.74 97 48253 11.69 UG/L 99 35) 1,1-Dichloropropene 9.85 75 38668 12.34 UG/L 90 36) Carbon tetrachloride 9.99 117 49860 12.00 UG/L 100 37) Benzene 10.12 78 74694 12.59 UG/L 98 38) Methyl Methacrylate 10.78 69 18891 12.68 UG/L # 73 39) Trichloroethene 10.69 95 34191 12.23 UG/L 97 40) 1,2-Dichloropropane 10.87 63 30064 12.20 UG/L # 96 41) Dibromomethane 11.22 93 30602 11.78 UG/L 90 42) 2-Chloroethyl vinyl ether 11.33 63 14699 11.45 UG/L # 60 44) Bromodichloromethane 11.14 83 63699 11.63 UG/L 98 45) cis-1,3-Dichloropropene 11.71 75 49286 11.61 UG/L 96 Toluene 12.20 92 52081 12.42 UG/L 93 406) 7) Ethyl Methacrylate 12.19 69 39631 12.34 UG/L # 81 8) trans-1,3-Dichloropropene 12.36 75 45215 11.77 UG/L 94 49) 1,1,2 -Trichloroethane 12.64 83 26543 12.27 UG/L 93 50) 1,2-Dibromoethane 14.06 107 43113 11.81 UG/L 96 51) 4-Methyl-2-pentanone 11.36 43 37045 12.93 UG/L 83 55) Chlorobenzene 14.89 112 65879 13.00 UG/L 90 56) 1,3-Dichloropropane 13.05 76 48013 13.12 UG/L 95 57) Tetrachloroethene 13.26 164 34561 13.52 UG/L # 90 58) Dibromochloromethane 13.65 129 55450 12.45 UG/L 100 59) 2-Hexanone 12.52 43 17108 14.01 UG/L 89 60) 1,1,1,2 -Tetrachloroethane 14.93 131 39106 12.57 UG/L # 29 61) Ethylbenzene 14.92 106 29889 13.40 UG/L 93 62) m,p-Xylene 15.04 106 75362 26.56 UG/L # 82 63) o -Xylene 15.65 106 34992 13.14 UG/L # 81 64) Xylene (total) 15.65 106 34992 13.14 UG/L # 81 65) Styrene 15.69 104 58676 12.92 UG/L 93 66) Bromoform 16.13 173 40484 12.74 UG/L 100 68) trans-1,4-Dichloro-2-buten 16.42 53 7447 11.73 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.23 83 41716 12.81 UG/L 100 70) Pentachloroethane 17.10 167 29953 12.92 UG/L # 33 71) 1,2,3-Trichloropropane 16.40 112 6505 12.03 UG/L # 18 72) 1,3 -Dichlorobenzene 17.47 146 51433 12.03 UG/L 95 73) 1,4 -Dichlorobenzene 17.57 146 59074 12.74 UG/L 92 74) 1,2 -Dichlorobenzene 17.98 146 53906 13.12 UG/L 93 75) 1,2-Dibromo-3-chloropropan 18.79 75 9355 12.42 UG/L 96 0----------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A40925.D 36E0228.M Wed Apr 06 16:29:48 2005 H5971 Page 2 Quantitation Report Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40930.D Vial: 7 Acq On : 28 Feb 2005 14:43 Operator: N Sample : VSTD020 Inst : H5971 Misc : ,,,CCV„ Multiplr: 1.00 *S Integration Params: RTEINT.P Quant Time: Feb 28 15:07 2005 Quant Results File: 36EO228.RES Method : C:\HPCHEM\1\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:59:34 2005 Response via : Continuinq Cal File: C:\HPCHEM\1\DATA\FEBOS\022805A\A40927.D Abundance TIC:A40930.D 320000 300000 d 280000 a C d N N L W II O 260000 H t0 240000 220000 200000 v N N 180000 O O o R N d � a E � a 160000 a o � L 140000 ai co d c ai a O 120000 U) a m r b v U 100000 t? ai Cepp O C C ry O- m C L N HL wy� O 00 •� a 21 O E �O `O O O N N O O o o o c n 80000 F- C6� t a o ai c t b' cr0� EHE '- m o E c o 60000 r o D o o E cn o m �" E `o v r E '^ O a H O E o O G O d N O 40000 O o r ° om > `o f E ow U 20000 JL - 77-� I 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 22.00 23.00 A40930.D 36EO228.M Wed Apr 06 16:30:12 2005 H5971 Page 3 N Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40930.D Vial: 7 Acq On : 28 Feb 2005 14:43 Operator: JV Sample : VSTD020 Inst : H5971 isc : ,,,CCV,, Multiplr: 1.00 �SIntegration Params: RTEINT.P M Quant Time: Feb 28 15:07 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Feb 28 12:15:34 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.32 168 292809 50.00 UG/L 0.13 33) 1,4-Difluorobenzene 10.29 114 297318 50.00 UG/L 0.12 54) Chlorobenzene-d5 14.83 82 164433 50.00 UG/L 0.07 67) 1,4 -Dichlorobenzene -d4 17.55 152 139271 50.00 UG/L 0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 9.97 65 41073 17.89 UG/L 0.13 Spiked Amount 50.000 Range 76 - 114 Recovery = 35.78°# 52) Toluene -d8 12.08 98 108012 18.62 UG/L 0.10 Spiked Amount 50.000 Range 88 - 110 Recovery = 37.24%# 53) 4-Bromofluorobenzene 16.35 95 72622 17.92 UG/L 0.04 Spiked Amount 50.000 Range 86 - 115 Recovery = 35.840# Compounds Qvalue it"get ) Dichlorodifluoromethane 4.17 85 46024 18.31 UG/L 99 3) Chloromethane 4.65 50 24492 18.79 UG/L 99 4) Vinyl chloride 4.95 62 30033 19.23 UG/L 99 S) Bromomethane 6.06 94 34886 18.11 UG/L 97 6) Chloroethane 6.22 64 20794 18.43 UG/L 99 7) Acetone 7.28 43 9345 21.11 UG/L 90 8) Acetonitrile 7.59 41 11282 113.33 UG/L 92 9) Allyl Chloride 7.84 41 53505 18.89 UG/L 95 10) Acrolein 7.22 56 17527 99.65 UG/L 99 11) Acrylonitrile 8.73 53 43006 17.83 UG/L 100 12) Iodomethane 7.80 142 76788 18.33 UG/L 93 13) Vinyl acetate 8.60 43 23179 19.70 UG/L 97 14) Chloroprene 8.73 53 43006 17.83 UG/L 91 15) 2-Butanone 8.99 43 16342 21.18 UG/L 88 16) Carbon disulfide 8.00 76 93242 18.78 UG/L 98 17) Trichlorofluoromethane 6.69 101 74768 17.22 UG/L 95 18) 1,1-Dichloroethene 7.44 96 34626 18.86 UG/L 98 19) methyl tert-butyl ether 8.11 73 86120 17.80 UG/L 96 21) Methylene chloride 7.95 84 38613 18.15 UG/L 95 22) trans-1,2-Dichloroethene 8.25 96 40424 18.65 UG/L # 84 23) 1,1-Dichloroethane 8.64 63 74431 18.31 UG/L 98 24) Propionitrile 9.06 54 2241 16.12 UG/L 77 25) Isobutyl alcohol 9.25 43 9092 121.91 UG/L # 42 26) Methacrylonitrile 9.24 67 11243 20.27 UG/L 92 27) cis-1,2-Dichloroethene 9.19 96 42797 18.11 UG/L 93 Bromochloromethane 9.49 128 28374 18.25 UG/L 98 �) ------------------------------------------------------------------------- 2,2-Dichloropropane 9.16 77 53656 16.44 UG/L 98 (#) = qualifier out of range (m) = manual integration A40930.D 36E0228.M Wed Apr 06 16:30:07 2005 H5971 Page 1 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40930.D Vial: 7 Acq On : 28 Feb 2005 14:43 Operator: JV Sample : VSTD020 Inst : H5971 Misc : ,,,CCV„ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Feb 28 15:07 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Feb 28 12:15:34 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth 36E0228 ------------------------------------------------------------------------- Compound R.T. QIon Response Conc Unit Qvalue 30) Chloroform 9.33 83 91082 17.70 UG/L 99 31) 1,2-Dichloroethane 10.06 62 49774 16.40 UG/L 99 32) 1,1,1 -Trichloroethane 9.72 97 76466 17.27 UG/L 100 35) 1,1-Dichloropropene 9.84 75 62631 18.86 UG/L 88 36) Carbon tetrachloride 9.96 117 77170 17.53 UG/L 97 37) Benzene 10.10 78 120738 19.20 UG/L 100 38) Methyl Methacrylate 10.78 69 30007 19.01 UG/L # 71 39) Trichloroethene 10.68 95 54489 18.38 UG/L 98 40) 1,2-Dichloropropane 10.85 63 48445 18.55 UG/L # 99 41) Dibromomethane 11.22 93 49519 17.99 UG/L 90 42) 2-Chloroethyl vinyl ether 11.32 63 24618 18.10 UG/L 88 44) Bromodichloromethane 11.13 83 101813 17.53 UG/L 99 45) cis-1,3-Dichloropropene 11.71 75 81586 18.13 UG/L 95 46) Toluene 12.20 92 84634 19.05 UG/L 98 07) Ethyl Methacrylate 12.19 69 65294 19.19 UG/L # 83 8) trans-1,3-Dichloropropene 12.36 75 71809 17.63 UG/L 95 49) 1,1,2 -Trichloroethane 12.65 83 42500 18.54 UG/L 94 50) 1,2-Dibromoethane 14.06 107 68512 17.71 UG/L 99 51) 4-Methyl-2-pentanone 11.34 43 59496 19.60 UG/L 84 55) Chlorobenzene 14.90 112 106816 19.68 UG/L 90 56) 1,3-Dichloropropane 13.04 76 76240 19.45 UG/L 93 57) Tetrachloroethene 13.27 164 58642 21.41 UG/L # 90 58) Dibromochloromethane 13.65 129 90118 18.89 UG/L 100 59) 2-Hexanone 12.52 43 27933 21.35 UG/L 92 60) 1,1,1,2 -Tetrachloroethane 14.93 131 63155 18.95 UG/L # 29 61) Ethylbenzene 14.93 106 46012 19.26 UG/L # 77 62) m,p-Xylene 15.05 106 122743 40.38 UG/L 88 63) o -Xylene 15.66 106 56449 19.79 UG/L # 79 64) Xylene (total) 15.66 106 56449 19.79 UG/L # 79 65) Styrene 15.70 104 97069 19.95 UG/L 94 66) Bromoform 16.14 173 66282 19.47 UG/L 97 68) trans-1,4-Dichloro-2-buten 16.44 53 12557 18.03 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.23 83 67969 19.02 UG/L 99 70) Pentachloroethane 17.10 167 45275 17.80 UG/L # 36 71) 1,2,3-Trichloropropane 16.39 112 11495 19.37 UG/L # 41 72) 1,3 -Dichlorobenzene 17.49 146 89951 19.18 UG/L 94 73) 1,4 -Dichlorobenzene 17.58 146 98959 19.44 UG/L 96 74) 1,2 -Dichlorobenzene 17.98 146 94647 20.99 UG/L 92 75) 1,2-Dibromo-3-chloropropan 18.79 75 16385 19.83 UG/L 97 (#) = qualifier out of range (m) = manual integration A40930.D 36E0228.M Wed Apr 06 16:30:08 2005 H5971 Page 2 Quantitation Report Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Vial: 5 Acq On : 28 Feb 2005 11:41 Operator: JV Sample : VSTDO50 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Feb 28 12:16 2005 Quant Results File: 36E0228.RES Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:59:34 2005 Resoonse via : Continuina Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Abundance TIC:A40927.D 480000 460000 440000 420000 m 400000 380000 g F U o 360000 e F a 340000 - L v � o o 320000 N R e � 300000 N ti U) a 0 80000ai N C O 260000 a 0 � 240000 220000 v v ~ v U c ~ 200000 o N E m ¢ o ai F4 m 180000o c o 00 o m v m 0 6b M QL.j Up d /-O O L N O 160000 y < 9 E 0 0 �~ 0 o o d U �m'`o 60 ! 3 H ai Vk'V Ih _0 v a F O O F- N 140000 U A E' � o a Qj t OU a N 7 O 0i = O 120000fi v o 0 o r E U o M 100000 =o t 020 0 0 0 2 F d o o ' 80000 o r m a ~ u v m� 0m 60000 S d o 0t ~ _U O U m0 _ry 40000 i5:5 0 C 20000 0 ILJ� ime--> 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 22.00 23.00 A40927.D 36E0228.M Wed Apr 06 16:30:30 2005 H5971 Page 3 Quantitation Report (Not Reviewed) Data File C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Vial: 5 Acq On 28 Feb 2005 11:41 Operator: JV Sample VSTD050 Inst : H5971 Misc ,,,ICAL „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Feb 28 12:16 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.20 168 239497 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.17 114 249853 50.00 UG/L 0.00 54) Chlorobenzene-d5 14.77 82 149565 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.53 152 122488 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 9.85 65 96453 50.00 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 100.000 52) Toluene -d8 11.99 98 243801 50.00 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.00° 53) 4-Bromofluorobenzene 16.31 95 170263 50.00 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.000 Compounds Qvalue 46rget 2) Dichlorodifluoromethane 4.11 85 102771 50.00 UG/L 96 3) Chloromethane 4.54 50 53310 50.00 UG/L 98 4) Vinyl chloride 4.82 62 63867 50.00 UG/L 99 5) Bromomethane 5.84 94 78776 50.00 UG/L 95 6) Chloroethane 6.04 64 46151 50.00 UG/L 100 7) Acetone 7.12 43 18100 50.00 UG/L 89 8) Acetonitrile 7.44 41 20357 250.00 UG/L 93 9) Allyl Chloride 7.67 41 115812 50.00 UG/L 93 10) Acrolein 7.06 56 35966 250.00 UG/L 98 11) Acrylonitrile 8.59 53 98653 50.00 UG/L 99 12) Iodomethane 7.64 142 171285 50.00 UG/L 97 13) Vinyl acetate 8.46 43 48108 50.00 UG/L 100 14) Chloroprene 8.59 53 98653 50.00 UG/L 96 15) 2-Butanone 8.84 43 31550 50.00 UG/L 94 16) Carbon disulfide 7.86 76 203102 50.00 UG/L 99 17) Trichlorofluoromethane 6.54 101 177529 50.00 UG/L 96 18) 1,1-Dichloroethene 7.30 96 75092 50.00 UG/L 99 19) methyl tert-butyl ether 7.95 73 197822 50.00 UG/L 93 21) Methylene chloride 7.80 84 87025 50.00 UG/L 94 22) trans-1,2-Dichloroethene 8.09 96 88663 50.00 UG/L # 86 23) 1,1-Dichloroethane 8.50 63 166202 50.00 UG/L 98 24) Propionitrile 8.91 54 5685 50.00 UG/L 93 25) Isobutyl alcohol 9.11 43 15250 250.00 UG/L # 45 26) Methacrylonitrile 9.09 67 22681 50.00 UG/L 88 27) cis-1,2-Dichloroethene 9.05 96 96635 50.00 UG/L 90 8) Bromochloromethane 9.37 128 63596 50.00 UG/L 98 -2,2-Dichloropropane----------9 02---77 ----------------------- 133507 50.00 UG/L------97 (#) = qualifier out of range (m) = manual integration A40927.D 36E0228.M Wed Apr 06 16:30:26 2005 H5971 Page 1 Quantitation Report (Not Reviewed) Data File C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Vial: 5 Acq On 28 Feb 2005 11:41 Operator: JV Sample VSTD050 Inst : H5971 Misc ,,,ICAL „ Multiplr: 1.00 SIntegration Params: RTEINT.P Quant Time: Feb 28 12:16 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth : 36E0228 (#) = qualifier out of range (m) = manual integration A40927.D 36E0228.M Wed Apr 06 16:30:27 2005 H5971 Page 2 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.20 83 210495 50.00 UG/L 99 31) 1,2-Dichloroethane 9.94 62 124158 50.00 UG/L 99 32) 1,1,1 -Trichloroethane 9.58 97 181083 50.00 UG/L 99 35) 1,1-Dichloropropene 9.71 75 139504 50.00 UG/L 89 36) Carbon tetrachloride 9.84 117 184970 50.00 UG/L 100 37) Benzene 9.99 78 264241 50.00 UG/L 98 38) Methyl Methacrylate 10.68 69 66336 50.00 UG/L # 71 39) Trichloroethene 10.57 95 124538 50.00 UG/L 96 40) 1,2-Dichloropropane 10.75 63 109724 50.00 UG/L # 98 41) Dibromomethane 11.11 93 115683 50.00 UG/L 91 42) 2-Chloroethyl vinyl ether 11.22 63 57164 50.00 UG/L 90 44) Bromodichloromethane 11.02 83 243981 50.00 UG/L 98 45) cis-1,3-Dichloropropene 11.61 75 189090 50.00 UG/L 95 6) Toluene 12.11 92 186683 50.00 UG/L 93 ) 08 Ethyl Methacrylate 12.12 69 142982 50.00 UG/L # 83 ) trans-1,3-Dichloropropene 12.26 75 171113 50.00 UG/L 94 49) 1,1,2 -Trichloroethane 12.55 83 96322 50.00 UG/L 94 50) 1,2-Dibromoethane 13.99 107 162505 50.00 UG/L 97 51) 4-Methyl-2-pentanone 11.25 43 127553 50.00 UG/L 84 55) Chlorobenzene 14.84 112 246790 50.00 UG/L 89 56) 1,3-Dichloropropane 12.95 76 178287 50.00 UG/L 96 57) Tetrachloroethene 13.18 164 124568 50.00 UG/L # 90 58) Dibromochloromethane 13.56 129 216920 50.00 UG/L 99 59) 2-Hexanone 12.42 43 59500 50.00 UG/L 93 60) 1,1,1,2 -Tetrachloroethane 14.88 131 151537 50.00 UG/L # 59 61) Ethylbenzene 14.88 106 108674 50.00 UG/L 91 62) m,p-Xylene 15.00 106 276474 100.00 UG/L # 82 63) o -Xylene 15.62 106 129737 50.00 UG/L # 82 64) Xylene (total) 15.62 106 129737 50.00 UG/L # 82 65) Styrene 15.66 104 221269 50.00 UG/L 93 66) Bromoform 16.11 173 154805 50.00 UG/L 99 68) trans-1,4-Dichloro-2-buten 16.41 53 30628 50.00 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.21 83 157118 50.00 UG/L 100 70) Pentachloroethane 17.07 167 111840 50.00 UG/L # 33 71) 1,2,3-Trichloropropane 16.36 112 26093 50.00 UG/L # 34 72) 1,3 -Dichlorobenzene 17.46 146 206277 50.00 UG/L 94 73) 1,4 -Dichlorobenzene 17.56 146 223828 50.00 UG/L 92 74) 1,2 -Dichlorobenzene 17.95 146 198281 50.00 UG/L 96 75) 1,2-Dibromo-3-chloropropan 18.76 75 36339 50.00 UG/L 95 (#) = qualifier out of range (m) = manual integration A40927.D 36E0228.M Wed Apr 06 16:30:27 2005 H5971 Page 2 Quantitation Report Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40928.D Vial: 5 Acq On : 28 Feb 2005 13:05 Operator: N Sample : VSTD100 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 *SIntegration Params: RTEINT.P Quant Time: Feb 28 13:29 2005 Quant Results File: 36E0228.RES Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:59:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Abundance TIC: A40928.D 1000000 950000 U a 900000 850000 800000 d E N 750000 2 o 700000 o 650000 a 0000 Z N N _ 550000 m d d � U Q N 500000 t v 0 450000 o 400000 N mra t o Oa 2n a nr o a E o 350000 _ o _O O :U � o r O d o f A o T- _oO u� n o v N 300000 E CL 0 C C L O 250000 t o o o M E0 0 c' 0 n` o E E 200000 wJe M _ E a E o ° A o U 150000 E OL U Oq H H 100000 O E- 0 o 030 0 F d C_ o U > U Q v 50000 0 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 22.00 23.00 A40928.D 36E0228.M Wed Apr 06 16:30:43 2005 H5971 Page 3 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40928.D Vial: 5 Acq On : 28 Feb 2005 13:05 Operator: JV Sample : VSTD100 Inst : H5971 : ,,,ICAL„ Multiplr: 1.00 ,Misc MS Integration Params: RTEINT.P Quant Time: Feb 28 13:29 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Feb 28 12:15:34 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) ------------------------------------------------------------------------- 1) Pentafluorobenzene 9.20 168 266802 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.18 114 276355 50.00 UG/L 0.00 54) Chlorobenzene-d5 14.77 82 170454 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.52 152 135519 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 9.86 65 211976 99.35 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 198.70%# 52) Toluene -d8 11.99 98 408872 75.81 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 151.629-A# S3) 4-Bromofluorobenzene 16.32 95 324632 86.19 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 172.38°# Compounds Qvalue 46rget 2) Dichlorodifluoromethane 4.12 85 217838 95.14 UG/L 96 3) Chloromethane 4.55 SO 114888 96.73 UG/L 99 4) Vinyl chloride 4.84 62 140934 99.04 UG/L 98 5) Bromomethane 5.85 94 170058 96.89 UG/L 96 6) Chloroethane 6.05 64 101702 98.91 UG/L 99 7) Acetone 7.13 43 43207 107.14 UG/L 92 8) Acetonitrile 7.44 41 48423 533.81 UG/L 94 9) Allyl Chloride 7.68 41 233945 90.67 UG/L 92 10) Acrolein 7.07 56 87401 545.35 UG/L 97 11) Acrylonitrile 8.59 53 212387 96.63 UG/L 99 12) Iodomethane 7.65 142 359120 94.10 UG/L 94 13) Vinyl acetate 8.47 43 129469 120.79 UG/L 97 14) Chloroprene 8.59 53 212387 96.63 UG/L 93 15) 2-Butanone 8.86 43 68665 97.68 UG/L 98 16) Carbon disulfide 7.86 76 420431 92.91 UG/L 99 17) Trichlorofluoromethane 6.53 101 371264 93.86 UG/L 97 18) 1,1-Dichloroethene 7.30 96 164758 98.48 UG/L 99 19) methyl tert-butyl ether 7.95 73 404902 91.87 UG/L 93 21) Methylene chloride 7.81 84 186483 96.18 UG/L 94 22) trans-1,2-Dichloroethene 8.10 96 192585 97.49 UG/L # 86 23) 1,1-Dichloroethane 8.50 63 359344 97.04 UG/L 97 24) Propionitrile 8.92 54 12787 100.95 UG/L 97 Z. 25) Isobutyl alcohol 9.12 43 33601 494.46 UG/L # 56 M 26) Methacrylonitrile 9.10 67 51534 101.98 UG/L 89 '4 27) cis-1,2-Dichloroethene 9.06 96 209311 97.22 UG/L 91 Bromochloromethane 9.36 128 142396 100.50 UG/L 98 274865 92.41 UG/L------99 O ---)-2,2_Dichloropropane----------903---77 -------------------- r� (#) = qualifier out of range (m) = manual integration DO A40928.D 36E0228.M Wed Apr 06 16:30:38 2005 H5971 Page 1 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40928.D Vial: 5 Acq On : 28 Feb 2005 13:05 Operator: JV Sample : VSTD100 Inst : H5971 ,Misc : ,,,ICAL „ Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 28 13:29 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth : 36EO228 (#) = qualifier out of range (m) = manual integration A40928.D 36E0228.M Wed Apr 06 16:30:40 2005 H5971 Page 2 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.19 83 446960 95.30 UG/L 99 31) 1,2-Dichloroethane 9.94 62 261801 94.64 UG/L 99 32) 1,1,1 -Trichloroethane 9.59 97 382237 94.74 UG/L 97 35) 1,1-Dichloropropene 9.72 75 295211 95.66 UG/L 90 36) Carbon tetrachloride 9.85 117 389096 95.09 UG/L 100 37) Benzene 9.99 78 572756 97.98 UG/L 97 38) Methyl Methacrylate 10.68 69 144211 98.27 UG/L # 73 39) Trichloroethene 10.58 95 271434 98.53 UG/L 97 40) 1,2-Dichloropropane 10.75 63 240235 98.97 UG/L # 99 41) Dibromomethane 11.12 93 257566 100.65 UG/L 90 42) 2-Chloroethyl vinyl ether 11.24 63 135078 106.82 UG/L 93 44) Bromodichloromethane 11.03 83 519048 96.17 UG/L 99 45) cis-1,3-Dichloropropene 11.62 75 411294 98.33 UG/L 96 Toluene 12.11 92 407741 98.73 UG/L 96 W6) 7) Ethyl Methacrylate 12.11 69 313090 98.99 UG/L # 85 48) trans-1,3-Dichloropropene 12.26 75 365535 96.57 UG/L 96 49) 1,1,2 -Trichloroethane 12.56 83 215000 100.90 UG/L 95 50) 1,2-Dibromoethane 13.99 107 372143 103.52 UG/L 97 51) 4-Methyl-2-pentanone 11.26 43 286218 101.44 UG/L 85 55) Chlorobenzene 14.84 112 538721 95.77 UG/L 87 56) 1,3-Dichloropropane 12.96 76 400059 98.45 UG/L 99 57) Tetrachloroethene 13.19 164 332661 117.16 UG/L # 90 58) Dibromochloromethane 13.57 129 484921 98.08 UG/L 99 59) 2-Hexanone 12.43 43 139500 102.86 UG/L 94 60) 1,1,1,2 -Tetrachloroethane 14.88 131 328009 94.96 UG/L # 61 61) Ethylbenzene 14.88 106 222312 89.75 UG/L # 82 62) m,p-Xylene 15.00 106 610029 193.61 UG/L 90 63) o -Xylene 15.63 106 278580 94.21 UG/L # 83 64) Xylene (total) 15.63 106 278580 94.21 UG/L # 83 65) Styrene 15.66 104 484968 96.16 UG/L 93 66) Bromoform 16.12 173 355406 100.72 UG/L 99 68) trans-1,4-Dichloro-2-buten 16.41 53 65796 97.08 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.21 83 346138 99.56 UG/L 99 70) Pentachloroethane 17.07 167 159026 64.26 UG/L # 36 71) 1,2,3-Trichloropropane 16.37 112 61717 106.89 UG/L # 54 72) 1,3 -Dichlorobenzene 17.46 146 438340 96.03 UG/L 94 73) 1,4 -Dichlorobenzene 17.56 146 497054 100.36 UG/L 93 74) 1,2 -Dichlorobenzene 17.96 146 452237 103.07 UG/L 94 75) 1,2-Dibromo-3-chloropropan 18.77 7S 82963 103.18 UG/L 84 (#) = qualifier out of range (m) = manual integration A40928.D 36E0228.M Wed Apr 06 16:30:40 2005 H5971 Page 2 Quantitation Report Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40929.D Vial: 6 Acq On : 28 Feb 2005 13:34 Operator: JV Sample : VSTD200 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Feb 28 13:58 2005 Quant Results File: 36E0228.RES Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Tue Apr 05 09:59:34 2005 Res►)onse via : Continuina Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D Abundance TIC:A40929.D 1900000 U 1800000 a c W K 1700000 0 1600000 1500000 1400000 d 1300000 U)$�dQNN Dv OO 11000 00000000000 UNd O 10 O 900000 U�L_O�NZUNO 800000 �aC aoo t o£ E 700000 SO am L 0 o _o 00 -O CE FU(naOOO 600000 o 1= o c`- � oL NO 500000 oEO & 06400000 oE0300000��o ~ ao to oo o d � v 200000 O mo U> 100000 4 0 4.00 5.00 6.00 7.00 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 2200. 23.00 A40929.D 36E0228.M Wed Apr 06 16:31:01 2005 H5971 Page 3 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40929.D Vial: 6 Acq On : 28 Feb 2005 13:34 Operator: JV Sample : VSTD200 Inst : H5971 OMisc : ,,,ICAL „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Feb 28 13:58 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.14 168 245206 50.00 UG/L -0.06 33) 1,4-Difluorobenzene 10.13 114 257800 50.00 UG/L -0.04 54) Chlorobenzene-d5 14.76 82 174716 50.00 UG/L -0.01 67) 1,4 -Dichlorobenzene -d4 17.54 152 130108 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 9.80 65 450553 226.36 UG/L -0.05 Spiked Amount 50.000 Range 76 - 114 Recovery = 452.72%# 52) Toluene -d8 11.96 98 892248 177.35 UG/L -0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 354.70%# 53) 4-Bromofluorobenzene 16.32 95 706704 201.14 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 402.28%# *get Compounds Qvalue ) Dichlorodifluoromethane 4.11 85 414141 196.80 UG/L 95 3) Chloromethane 4.51 50 219145 200.75 UG/L 99 4) Vinyl chloride 4.80 62 267913 204.86 UG/L 98 5) Bromomethane 5.77 94 320216 198.51 UG/L 95 6) Chloroethane 5.94 64 197978 209.50 UG/L 99 7) Acetone 7.06 43 78797 212.60 UG/L 92 8) Acetonitrile 7.36 41 86034 1031.97 UG/L 95 9) Allyl Chloride 7.61 41 446867 188.44 UG/L 92 10) Acrolein 6.99 56 162240 1101.48 UG/L 96 11) Acrylonitrile 8.52 53 400555 198.29 UG/L 98 12) Iodomethane 7.58 142 684125 195.05 UG/L 95 13) Vinyl acetate 8.39 43 236429 240.01 UG/L 95 14) Chloroprene 8.52 53 400555 198.29 UG/L 92 15) 2-Butanone 8.78 43 124551 192.79 UG/L 99 16) Carbon disulfide 7.80 76 788972 189.71 UG/L 98 17) Trichlorofluoromethane 6.48 101 727382 200.09 UG/L 96 18) 1,1-Dichloroethene 7.23 96 310918 202.20 UG/L 98 19) methyl tert-butyl ether 7.88 73 776234 191.63 UG/L 93 21) Methylene chloride 7.74 84 362046 203.17 UG/L 94 22) trans-1,2-Dichloroethene 8.03 96 369969 203.78 UG/L # 86 23) 1,1-Dichloroethane 8.44 63 685685 201.48 UG/L 97 24) Propionitrile 8.85 54 25092 215.55 UG/L 99 25) Isobutyl alcohol 9.05 43 53526 857.05 UG/L # 73 26) Methacrylonitrile 9.04 67 95436 205.49 UG/L 91 27) cis-1,2-Dichloroethene 9.00 96 407997 206.19 UG/L 88 Bromochloromethane 9.30 128 278787 214.08 UG/L 96 �) ) ------------------------------------------------------------------ 2,2-Dichloropropane 8.96 77 511981 187.28 UG/L------98 (#) = qualifier out of range (m) = manual integration A40929.D 36E0228.M Wed Apr 06 16:30:57 2005 H5971 Page 1 Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\FEB05\022805A\A40929.D Vial: 6 Acq On : 28 Feb 2005 13:34 Operator: JV Sample : VSTD200 Inst : H5971 Misc : ,,,ICAL „ Multiplr: 1.00 *SIntegration Params: RTEINT.P Quant Time: Feb 28 13:58 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Feb 28 12:15:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\FEB05\022805A\A40927.D DataAcq Meth : 36EO228 O -0 ---------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A40929.D 36E0228.M Wed Apr 06 16:30:58 2005 H5971 Page 2 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.14 83 854644 198.28 UG/L 98 31) 1,2-Dichloroethane 9.89 62 509626 200.45 UG/L 100 32) 1,1,1 -Trichloroethane 9.53 97 729020 196.61 UG/L 97 35) 1,1-Dichloropropene 9.66 75 561360 195.00 UG/L 91 36) Carbon tetrachloride 9.79 117 738325 193.43 UG/L 99 37) Benzene 9.94 78 1105457 202.73 UG/L 96 38) Methyl Methacrylate 10.64 69 278357 203.34 UG/L # 73 39) Trichloroethene 10.53 95 521327 202.85 UG/L 98 40) 1,2-Dichloropropane 10.70 63 457743 202.16 UG/L # 100 41) Dibromomethane 11.08 93 499694 209.32 UG/L 89 42) 2-Chloroethyl vinyl ether 11.20 63 259307 219.82 UG/L 92 44) Bromodichloromethane 10.99 83 1007298 200.07 UG/L 98 45) cis-1,3-Dichloropropene 11.58 75 806880 206.78 UG/L 96 Toluene 12.07 92 781473 202.85 UG/L 93 08) Ethyl Methacrylate 12.08 69 605019 205.05 UG/L # 87 trans-1,3-Dichloropropene 12.23 75 710461 201.20 UG/L 96 49) 1,1,2 -Trichloroethane 12.53 83 412210 207.38 UG/L 96 50) 1,2-Dibromoethane 13.97 107 718734 214.33 UG/L 98 51) 4-Methyl-2-pentanone 11.22 43 546385 207.58 UG/L 85 55) Chlorobenzene 14.83 112 1058412 183.57 UG/L 86 56) 1,3-Dichloropropane 12.93 76 772735 185.51 UG/L 99 57) Tetrachloroethene 13.16 164 668600 229.74 UG/L # 90 58) Dibromochloromethane 13.54 129 934749 184.44 UG/L 99 59) 2-Hexanone 12.40 43 249375 179.39 UG/L 97 60) 1,1,1,2 -Tetrachloroethane 14.87 131 650370 183.70 UG/L # 66 61) Ethylbenzene 14.87 106 440788 173.61 UG/L # 83 62) m,p-Xylene 14.99 106 1179701 365.27 UG/L 90 63) o -Xylene 15.62 106 547195 180.53 UG/L # 85 64) Xylene (total) 15.62 106 547195 180.53 UG/L # 85 65) Styrene 15.66 104 950288 183.82 UG/L 94 66) Bromoform 16.12 173 687108 189.98 UG/L 99 68) trans-1,4-Dichloro-2-buten 16.41 53 125786 193.32 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.21 83 674566 202.10 UG/L 98 70) Pentachloroethane 17.08 167 284792 119.86 UG/L # 37 71) 1,2,3-Trichloropropane 16.37 112 112329 202.64 UG/L # 37 72) 1,3 -Dichlorobenzene 17.47 146 863055 196.95 UG/L 94 73) 1,4 -Dichlorobenzene 17.57 146 966514 203.26 UG/L 92 00 M 74) 1,2 -Dichlorobenzene 17.96 146 879902 208.89 UG/L 94 75) 1,2-Dibromo-3-chloropropan 18.78 75 157466 203.97 UG/L 83 ~✓ O -0 ---------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration A40929.D 36E0228.M Wed Apr 06 16:30:58 2005 H5971 Page 2 • • • SDG No.: TSL001 7A 14:31 02/28/05 VOLATILE CONTINUING CALIBRATION CHECK Lab Name: H2M LABS, INC. Contract: RRF %D Lab Code: 10478 Case No.: PCTSL SAS No.: 0.184 I -s Instrument ID: HP5971 Calibration Date: 04/04/05 Lab File ID: A\A41195.D Init. Calib. Date(s) EPA Sample No.(VSTD0504#): VSTD050 Init. Calib. Times: Heated Purge: (YIN) N 0.100 i 22.7 GC Column: R-502.2 ID: .53 (mm) 0.266 1 SDG No.: TSL001 Time: 14:31 02/28/05 02/28/05 10:38 14:43 - - I- MIN j MAX I COMPOUND RRF RRF50 RRF %D %D Chloromethane 0.230 0.184 I -s j -20.2 - Vinyl chloride 0.281 0.217 0.100 i 22.7 25.0 Bromomethane 0.335 0.266 1 0.100 i -20.7 25.0 Chloroethane 0.199 0.159 i -20.0 Acetone 0.082 0.059 I -27.8 Acrylonitrile 0.415 0.337 -18.7 1 lodomethane i 0.721 0.603 j I -16.4 i Vinyl acetate 0.230 0.193 - j 16.2 2-Butanone 0.141 0.109 i 22.9 j ;Carbon disulfide 0.863 0.697 19.2 Trichlorofluoromethane il,l-Dichloroethene 0.736 0.517 -29.7 I 0.326 0.252 0.100 i -22.8 25.0 Methylene chloride 0.375 0.335 ' 1 -10.6 trans-1,2-Dichloroethene j 0.382 0.314 j -17.9 � 1 1 Dichloroethane 0.706 0.605 I 0.200 -14.4 25.0 cis 1,2-Dichloroethene 0.414 0.349 -15.7 Bromochloromethane 0.276 0.245 11.2 ;Chloroform 0.880 0.721 1 0.200 -18.1 25.0 11,2-Dichloroethane 0.507 0.428 0.100 -15.6 25.0 r aneI 0.750 0.568 0.100 -24.3 25.0 ---------- _ Carbont tetrachloride - 0.740 -- 0.542 - - 0.100 26.7 25.0 Benzene 1.102 0.944 ; 0.500 -14.4 25.0 Trichloroethene 0.513 0.411 0.300 1 -19.8 25.0 1,2-Dichloropropane 1 0.452 0.400 -11.5 Dibromomethane i 0.475 0.414 -12.9 Bromodichloromethane 0.977 0.816 0.200 ! -16.5 25.0 ;cis-1,3-Dichloropropene 0.770 0.677 0.200 -12.0 25.0 Toluene 0.777 0.635 0.400 -18.2 25.0 itrans-l,3-Dichloropropene 0.689 0.607 0.100 11.9 25.0 ;1,1,2 -Trichloroethane 0.401 0.352 0.100 -12.2 25.0 1,2-Dibromoethane 0.673 0.595 -11.6 4-Methyl-2-pentanone 0.544 0.328 -39.7 Chlorobenzene 1.703 1.477 0.500 -13.3 25.0 Tetrachloroethene 0.957 0.729 0.200 -23.8 25.0 Dibromochloromethane 1.477 1.367 0.100 -7.5 25.0 All other compounds must meet a minimum RRF of 0.010. FORM VII VOA - 1 OLM04.2 • L GC Column: R-502.2 ID: .53 (mm) 7B VOLATILE CONTINUING CALIBRATION CHECK I MIN i - Lab Name: H2M LABS, INC. Contract: RRF IRRF50 RRF %D Lab Code: 10478 Case No.: PCTSL SAS No.: 0.429 SDG No.: TSL001 9.4 Instrument ID: HP5971 Calibration Date: 04/04/05 Time: 14:31 Lab File ID: A\A41195.D Init. Calib. Date(s): 02/28/05 02/28/05 � 0.737 EPA Sample No.(VSTD050##): VSTD050 Init. Calib. Times: 10:38 14:43 - --- Heated Purge: (Y/N) N 0.774 — -- 0.3001 13.3 25.0 • L GC Column: R-502.2 ID: .53 (mm) I MIN i - MAX COMPOUND RRF IRRF50 RRF %D %D i2-1-lexanone 0.429 0.389 9.4 1,1,1,2 -Tetrachloroethane 1.028 0.890 f -13.4 !Ethylbenzene � 0.737 0.574 0100 22.1 25.0 jXylene (total) — — — - -- - — - --- 0.893 — 0.774 — -- 0.3001 13.3 25.0 (Styrene I 1.530 1.354 0.300 11.5 1 25.0 lBromoform 1.077 0.990 0.100 -8.1 I 25.0 trans-1,4-Dichloro-2-butene 0.251 0.214 -14.6 1,1,2,2 -Tetrachloroethane fi 1.344 1.217 I 0.300 9.4 25.0 1,2,3-Tnchloropropane 0.224 0.200 i. -10.7 11,4 -Dichlorobenzene 1.924 1.695 -11.9 I 1,2 -Dichlorobenzene 1,760 1.500 14.8 1,2-D6romo-3-chloropropane 0.314 0.275 i i -12.3 All other compounds must meet a minimum RRF of 0.010. FORM VII VOA - 2 OLM04.2 • All other compounds must meet a minimum RRF of 0.010. • FORM VII VOA - 3 OLM04.2 C/1 7B VOLATILE CONTINUING CALIBRATION CHECK Lab Name: H2M LABS, INC. Contract: • Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Instrument ID: HP5971 Calibration Date: 04/04/05 Time: 14:31 Lab File ID: A\A41195.D Init. Calib. Date(s): 02/28/05 02/28/05 EPA Sample No.(VSTD050##): VSTDO50 Init. Calib. Times: 10:38 14:43 Heated Purge: (YIN) N GC Column: R-502.2 ID: .53 (mm) — MIN MAX 1 COMPOUND RRF--i-RRF50j RRF %D %D 1,2-Dichloroethane-d4 0.416 0.347 j -16.7 - -- !Toluene-d8 --- — 0.987 0.980 -0.7 j 4-Bromofluorobenzene 1 0.704 t 0.643 L 0.200 -8.6 j 25.0 • All other compounds must meet a minimum RRF of 0.010. • FORM VII VOA - 3 OLM04.2 C/1 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41195.D Vial: 2 Acq On 4 Apr 2005 14:31 Operator: JV Sample : VSTD050 Inst : H5971 Misc : ,,,CCV „ Multiplr: 1.00 is MS Integration Params: RTEINT.P Quant Time: Apr 4 16:29 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:13:18 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 650000- 50000- 600000- 600000 550000- 550000 500000 500000 450000 100000' 7 A m 1 I,I e 5 50000 i 5 A41195.D 36E0228.M Wed Apr 06 14:13:44 2005 e a N I N III INS N �v1 I O 7.00 18.00 19.00 20.00 21.00 SYS1 Page 3 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41195.D Vial: 2 Acq On 4 Apr 2005 14:31 Operator: JV Sample : VSTD050 Inst : H5971 Misc : ,,,CCV „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 4 16:29 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 31 11:04:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36E0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.39 168 332824 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.39 114 347437 50.00 UG/L 0.00 54) Chlorobenzene-d5 15.03 82 195269 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.67 152 169820 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.06 65 120515 50.00 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 100.00% 52) Toluene -d8 12.26 98 340338 50.00 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.00% 53) 4-Bromofluorobenzene 16.46 95 223382 50.00 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 100.00% Compounds Qvalue 0rget 2) Dichlorodifluoromethane 4.35 85 92350 50.00 UG/L 99 3) Chloromethane 4.79 50 61279 50.00 UG/L 98 4) Vinyl chloride 5.10 62 72326 50.00 UG/L 98 5) Bromomethane 6.15 94 88655 50.00 UG/L 95 6) Chloroethane 6.31 64 52759 50.00 UG/L 99 7) Acetone 7.31 43 19597 50.00 UG/L 90 8) Acetonitrile 7.62 41 27332 250.00 UG/L 96 9) Allyl Chloride 7.86 41 146644 50.00 UG/L 97 10) Acrolein 7.25 56 47012 250.00 UG/L 97 11) Acrylonitrile 8.78 53 112053 50.00 UG/L 99 12) Iodomethane 7.84 142 200856 50.00 UG/L 92 13) Vinyl acetate 8.64 43 64092 50.00 UG/L 99 14) Chloroprene 8.78 53 112053 50.00 UG/L 92 15) 2-Butanone 9.05 43 36343 50.00 UG/L 98 16) Carbon disulfide 8.05 76 231897 50.00 UG/L 99 17) Trichlorofluoromethane 6.74 101 172035 50.00 UG/L 96 18) 1,1-Dichloroethene 7.49 96 84024 50.00 UG/L 99 21) Methylene chloride 7.99 84 111628 50.00 UG/L 98 22) trans-1,2-Dichloroethene 8.29 96 104434 50.00 UG/L # 85 23) 1,1-Dichloroethane 8.69 63 201402 50.00 UG/L 98 24) Propionitrile 9.11 54 7450 50.00 UG/L 97 25) Isobutyl alcohol 9.31 43 16381 250.00 UG/L # 57 26) Methacrylonitrile 9.29 67 31166 50.00 UG/L 93 27) cis-1,2-Dichloroethene 9.25 96 116236 50.00 UG/L 91 ) Bromochloromethane 9.57 128 81458 50.00 UG/L 99 ) ------------------------------------------------------------------------- 2,2-Dichloropropane 9.21 77 139403 50.00 UG/L 98 (#) = qualifier out of range (m) = manual integration A41195.D 36E0228.M Wed Apr 06 14:13:40 2005 SYS1 Page 1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41195.D Vial: 2 Acq On 4 Apr 2005 14:31 Operator: JV Sample : VSTD050 Inst : H5971 Misc : ,,,CCV „ Multiplr: 1.00 .MS Integration Params: RTEINT.P Quant Time: Apr 4 16:29 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Thu Mar 31 11:04:34 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.39 83 240082 50.00 UG/L 99 31) 1,2-Dichloroethane 10.15 62 142564 50.00 UG/L 100 32) 1,1,1 -Trichloroethane 9.79 97 189170 50.00 UG/L 98 35) 1,1-Dichloropropene 9.92 75 159153 50.00 UG/L 91 36) Carbon tetrachloride 10.05 117 188342 50.00 UG/L 98 37) Benzene 10.20 78 328111 50.00 UG/L 98 38) Methyl Methacrylate 10.90 69 87282 50.00 UG/L # 78 39) Trichloroethene 10.80 95 142722 50.00 UG/L 99 40) 1,2-Dichloropropane 10.98 63 139145 50.00 UG/L # 99 41) Dibromomethane 11.36 93 143922 50.00 UG/L 91 44) Bromodichloromethane 11.27 83 283412 50.00 UG/L 99 45) cis-1,3-Dichloropropene 11.87 75 235252 50.00 UG/L 95 46) Toluene 12.38 92 220697 50.00 UG/L 92 Ethyl Methacrylate 12.38 69 182741 50.00 UG/L # 84 W7) 48) trans-1,3-Dichloropropene 12.54 75 210854 50.00 UG/L 95 49) 1,1,2 -Trichloroethane 12.85 83 122413 50.00 UG/L 93 50) 1,2-Dibromoethane 14.32 107 206717 50.00 UG/L 97 51) 4-Methyl-2-pentanone 11.50 43 113907 50.00 UG/L 94 55) Chlorobenzene 15.10 112 288509 50.00 UG/L 88 56) 1,3-Dichloropropane 13.26 76 227395 50.00 UG/L 97 57) Tetrachloroethene 13.50 164 142379 50.00 UG/L # 89 58) Dibromochloromethane 13.90 129 266923 50.00 UG/L 99 59) 2-Hexanone 12.70 43 75958 50.00 UG/L 93 60) 1,1,1,2 -Tetrachloroethane 15.12 131 173794 50.00 UG/L # 58 61) Ethylbenzene 15.12 106 112076 50.00 UG/L # 79 62) m,p-Xylene 15.23 106 327889 100.00 UG/L 90 63) o -Xylene 15.80 106 151151 50.00 UG/L # 86 64) Xylene (total) 15.80 106 151151 50.00 UG/L # 86 65) Styrene 15.83 104 264359 50.00 UG/L 94 66) Bromoform 16.26 173 193332 50.00 UG/L 100 68) trans-1,4-Dichloro-2-buten 16.55 53 36332 50.00 UG/L # 1 69) 1,1,2,2 -Tetrachloroethane 16.35 83 206612 50.00 UG/L 99 70) Pentachloroethane 17.21 167 134203 50.00 UG/L # 31 71) 1,2,3-Trichloropropane 16.51 112 34018 50.00 UG/L # 39 72) 1,3 -Dichlorobenzene 17.60 146 242524 50.00 UG/L 93 -zt 73) 1,4 -Dichlorobenzene 17.70 146 287864 50.00 UG/L 92 74) 1,2 -Dichlorobenzene 18.10 146 254653 50.00 UG/L 95 j 75) 1,2-Dibromo-3-chloropropan 18.92 75 46753 50.00 UG/L 88 O • ------------------------------------------------------------------------- V1 (#) = qualifier out of range (m) = manual integration A41195.D 36E0228.M Wed Apr 06 14:13:41 2005 SYS1 Page 2 H2M LABS, INC. 0 IV. RAW QC DATA PACKAGE FOR VOLATILE ORGANICS A. TUNING B. BLANK C. MATRIX SPIKE BLANK D. SPIKE AND SPIKE DUPLICATE E. COPY OF CALCULATIONS • • CLPBFB Data File : 0:\MS\HP5971\DATA\FEB05\022805A\A40923.D Vial: 1 Acq On . 28 Feb 2005 9:15 Operator: JV Sample : 50 NG BFB Inst : H5971 Misc . ,,,TUNE „ Multiplr: 1.00 • MS Integration Params: RTEINT.P Method 0:\MS\5973\METHODS\CLPW0301.M (RTE Integrator) Title VOA Standards for 5 point calibration 4Abundance TIC: A40923.1) 100000 i 80000] 11 'I 600001 I A40923.D CLPW030l.M Wed Apr 06 16:26:26 2005 20000{ i I I 15000; j 174 I II 10000! 75 1 50001 50 � 69 i37 45 ��j 56 61 �� ilii 81 87 .1h 141 0 --r-, - 4 1, . +��u J -t y-4 6vz--> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 AutoFind: Scans 284, 285, 286; Background Corrected with Scan 277 I Target I Rel. to I Lower I Upper I Rel. I Raw I Result I Mass I Mass I Limits I Limit% I Abn% I Abn I Pass/Fail I ---------------------------------------------------------------------- 50 1 95 1 15 1 40 1 16.2 1 3452 1 PASS I 1 75 1 95 1 30 1 60 1 47.3 1 10056 1 PASS I 1 95 I 95 i 100 1 100 1 100.0 1 21248 1 PASS I 96 I 95 I 5 1 9 1 6.9 I 1475 1 PASS 1 1 173 I 174 1 0.00 I 2 1 0.0 1 0 1 PASS I 1 174 1 95 1 50 1 100 1 70.2 1 14916 1 PASS. I 175 1 174 1 5 1 9 1 7.1 1 1055 1 PASS I •1 1 176 1 174 1 95 I 101 1 98.6 1 14706 1 PASS I 1 ---------------------------------------------------------------------- 177 1 176 1 5 1 9 1 6.9 1 1011 1 PASS I A40923.D CLPW030l.M Wed Apr 06 16:26:26 2005 Fe.'. Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41194.D Vial: 1 Acq On 4 Apr 2005 14:16 Operator: JV Sample : 50 NG BFB Inst : H5971 •Misc : ,,,TUNE „ Multiplr: 1.00 MS Integration Params: RTEINT.P Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS bundance 100000 I i 80000 60000 40000 20000 I 0 ime-> 7.20 7.40 7.60 Abundance 20000 • 15000 10000 i i. ` 5000 i I I II 0 hvz—> 30 40 1 50 60 70 80 90 100 110 120 130 140 150 160 170 180 AutoFind: Scans 210, 211, 212; Background Corrected with Scan 202 TargetRel. to Lower I Upper I Rel. I Raw ( Result Mass I Mass I Limit% Limit% Abn% Abn Pass/Fail f ---------------------------------------------------------------------- 50 95 15 40 17.0 3670 PASS 75 95 30 60 47.1 10169 PASS 95 95 100 100 100.0 21576 PASS 96 95 5 9 6.9 1499 PASS C� 173 174 0.00 2 0.0 0 PASS 174 95 50 100 71.8 15494 PASS 175 174 5 9 7.4 1151 PASS 176 174 95 101 98.1 15192 PASS 177 176 5 9 6.2 942 PASS ---------------------------------------------------------------------- C!� E -i A41194.D 36E0228.M Wed Apr 06 14:13:27 2005 SYS1 lA VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Contract: • Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW EPA SAMPLE NO. VBLK040405 SAS No.: SDG No.: TSL001 Lab Sample ID: VBLK040405 ID: .53 (mm) (µL) Lab File ID: A\A41196.D Date Received: Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (µL) 00 C) C/j CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 74-87-3 i Chloromethane 5 U 75-01-4 Vinyl chloride 5 U 74-83-9 I Bromomethane 5 U 75-00-3 Chloroethane 5 67-64-1 Acetone5 I -U --� U I - - - 107-13-1 i - - — --- - - -- - -- - Acrylonitrile - -- - - -- 5 — U 74-88-4 ~ Iodomethane 5 U 108-05-4 Vinyl acetate 5 j U 78-93-3 2 Butanone ! 5 U 75-15-0 Carbon disulfide 5 U 75-69-4 j Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene - -� 5 U 75-09-2 Methylene chloride 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 1746-599_5 cis-1,2-Dichloroethene 5 5 r U U --� Bromochloromethane 67-66-3 Chloroform 5 U 107-06-2 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U 71-43-2 Benzene 5 — U 79-01-6 Trichloroethene 5 U 78-87-5 1,2-Dichloropropane i 5 i U 74-95-3 Dibromomethane 5 ! U 75-27-4 Bromodichloromethane 5 - U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 5 U 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 5 U 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 00 C) C/j • • • 1B VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Contract: (mm Soil Extract Volume: (µL) EPA SAMPLE NO. VBLK040405 SAS No.: SDG No.: TSL001 Lab Sample ID: VBLK040405 Lab File ID: A\A41196.D Date Received: Date Analyzed: 04/04/05 Dilution Factor: 1.00 Soil Aliquot Volume (µL) FORM I VOA - 2 OLM04.2 CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q - - 591-78-6 r 2 Hexanone - - 5 - U — -630-20-6 r 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 5 U 1330-20-7 Xylene (total) 5 U j 100-42-5 1 Styrene } 5 U 75-25-2 i Bromoform 5 1 U 110-57-6 trans-1,4-Dichloro-2-butene j 5— U--1� 79-34-5 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 1 1 2 3-Trichloropropane ! 5 U j 106-46-7 1 1,4 -Dichlorobenzene 1 5 U 95-50-1 1,2 -Dichlorobenzene 5 U 96-12-8 i 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 IF EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS VBLK040405 Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: VBLK040405 Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41196.D Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µl) Soil Aliquot Volume: 0 (µL) CONCENTRATION UNITS: Number TICS found: 0 (µg/L or µg/Kg) UG/L I CAS NUMBER COMPOUND NAME RT EST.CONC Q • • FORM I VOA -TIC OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41196.D Vial: 3 Acq On 4 Apr 2005 15:03 Operator: JV Sample : VBLK040405 Inst : H5971 Misc : ,,,MBLK „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 4 16:47 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:13:18 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D ndanra TIR•AA11QR h I 260000 250000 I 240000 2300001 I 220000 210000 200000 190000 180000 170000 60000 150000 ; 140000 130000- 120000 110000 j 1000010-1 90000] 80000 ! 70000 60000 5000011 40000�� 300001' 20000 0 10000; oiT-- Time—> 4.00 5.00 6.00 7.00 A41196.D 36E0228.M R fa f� m o I 8.00 9.00 10.00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 18.00 19.00 20.00 21.00 CJ) E-� Wed Apr 06 14:13:56 2005 SYS1 Page 2 LSC Report - Integrated Chromatogram File 0:\MS\HP5971\DATA\APR05\040405A\A41196.D Operator JV cquired 4 Apr 2005 15:03 using AcgMethod 36EO228 Winstrument H5971 Sample Name: VBLK040405 Misc Info : ,,,MBLK „ Vial Number: 3 Quant File :36E0228.RES (RTE Integrator) C. r bundce an TIC: A41196.1)1 2000001 9.40 150000- 5000010000050000 100000- 50000 0---- - ime-> 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 Abundance TIC: A41196.13 200000 10.40 15.04 12.27 150000 100000 0.07 50000 i .. - --- - - - - - -L ---- �., 0 - - =-- ime-> 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 Abundance TIC: A411196.13 1 47 1767 200000 150000 i 1000001 50000 I Ii ,I I 0 II T -'~--T - -- --- --- - Time, > _ 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 A41196.D 36E0228.M Wed Apr 06 14:32:40 2005 SYS1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41196.D Vial: 3 Acq On 4 Apr 2005 15:03 Operator: JV Sample : VBLK040405 Inst : H5971 Misc : ,,,MBLK „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Apr 4 16:47 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:36:20 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.40 168 318511 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.40 114 329738 50.00 UG/L 0.02 54) Chlorobenzene-d5 15.04 82 174042 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.67 152 140135 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.08 65 110644 48.37 UG/L 0.02 Spiked Amount 50.000 Range 76 - 114 Recovery = 96.74% 52) Toluene -d8 12.27 98 317033 49.08 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 98.16% 53) 4-Bromofluorobenzene 16.47 95 185432 43.73 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 87.46% 10rget Compounds Qvalue 1) Methylene chloride 8.01 84 2567 1.20 UG/L 87 M • O O rA (#) = qualifier out of range (m) = manual integration P-, A41196.D 36E0228.M Wed Apr 06 14:13:55 2005 SYS1 Page 1 Tentatively Identified Compound (LSC) summary Operator ID: JV Date Acquired: 4 Apr 2005 15:03 Data File: 0:\MS\HP5971\DATA\APR05\040405A\A41196.D N e: VBLK04Q405 ,MBLK „ od: C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title: WATER PART360E ORGANICS PLUS Library Searched: C:\DATABASE\NIST98.L TIC Top Hit name RT EstConc Units Area IntStd ISRT ISArea ISConc ---------------------------------------------------------------------------- A41196.D 36E0228.M Wed Apr 06 14:32:40 2005 SYS1 • • • • >bundanceScan 417 (7.992 min): A41195.D (-) { 4� 84 Refp 0 _ 36 42 70 88 r n/z–> 0 35 40 45 50 55 60 65 70 75 80 85 kbundance Scan 418 (8.008 min): A41196.13 i 49 44 Rani 84 95 0 ,4T— z–> 30 35 40 _45 50 55 60 65 70 75 80 85 90 95 Abundance Scan 418 (8.008 min): A41196.D49 (-) 84 Sub 50 �I 0r, 44 /z–> 30 35 40 4545 50 5555 60 65 70 75 80 85 90 95 #21 Methylene chloride Concen: 1.20 UG/L RT: 8.01 min Scan# 418 Delta R.T. 0.02 min Lab File: A41196.D Acq: 4 Apr 2005 15:03 Tgt Ion: 84 Resp: 2567 Ion Ratio Lower Upper 84 100 86 50.4 47.2 87.2 49 117.7 107.2 147.2 1000 Ion 86.00 (85.70 to 86.70): A41196.13 Ion 49.00 (48.70 to 49.70): A41196.13 800 600 8. 1 400 f 200 0 -> 7.90 7.95 8.00 8.05 8.10 A41196.D 36E0228.M Wed Apr 06 14:13:58 2005 SYS1 Page 3 lA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET MW -ISMS • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504067-002AMS Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41211.D Level: (low/med) LOW Date Received: 04/04/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q j 74-87-3 Chloromethane 5 - U ._ - - -75---01-4--;- 75-01-4 ' Vinyl chloride j 5 U j 74-83-9 Bromomethane 5 U 75-00-3 Chloroethane 5 U 67-64-1 Acetone L 5 U 107-13-1 Acrylonitrile j 5 j U 74-88-4 i Iodomethane 5 U 108-05-4 • Vinyl acetate j 5U - - - - - - - -- -- -... -- - 78-93-3 2-Butanone 5 t U 75-15-0 Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene j 47 75-09-2 Methylene chloride 5 U 156-60-5 trans-1,2-Dichloroethene 5 U 75-34-3 1,1-Dichloroethane 5 U 156-59-2 cis-1,2-Dichloroethene 5 U 74-97-5 Bromochloromethane 5 U 67-66-3 Chloroform 5 U 107-06-2 j 1,2-Dichloroethane 5 U 71-55-6 1,1,1 -Trichloroethane 5 U 56-23-5 Carbon tetrachloride 5 U i 71-43-2 Benzene 49 79-01-6 Trichloroethene 52 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U 75-27-4 i Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 53 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 55 127-18-4 Tetrachloroethene 5 U 124-48-1 • Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. Contract: SAS No.: GC Column: R-502.2 ID: .53 (mm) Soil Extract Volume: ()AL) Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW-1SMS SDG No.: TSL001 0504067-002AMS A\A41211.D 04/04/05 04/04/05 1.00 Soil Aliquot Volume (µL) 110-57-6 j trans-1,4-Dichloro-2-butene CONCENTRATION UNITS: U j CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2-Hexanone 5 U 630-20-6 1,1,1,2 -Tetrachloroethane 5 U 100-41-4 Ethylbenzene 5 r U 1330-20-7 Xylene (total) 5 U 100-42-5 Styrene 5 U 75-25-2 Bromoform 5 U 110-57-6 j trans-1,4-Dichloro-2-butene 5 U j 79-34-5 • 1,1,2,2 Tetrachloroethane 5 U 96-18-4 1,2,3-Trichloropropane S U 106-46-7 1,4 -Dichlorobenzene 5 U r--- - - 95-50-1 -- -- -- ----- --- _ 1,2 -Dichlorobenzene 5 - ------i U I 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41211.D Vial: 18 Acq On 4 Apr 2005 22:48 Operator: JV Sample : 0504067-002AMS Inst : H5971 Misc : TSLOOI,MW-1SMS,H20,MS „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 6 11:42 2005 Quant Results File: 36E0228.RES Method 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 290000 280000 270000 260000 250000 240000 230000 220000 210000 200000 190000 0i180000 170000 160000 150000 140000 130000 120000 110000 100000 90000 80000 70000 60000 50000 40000 3000,01 200001 • 100004 0� ,Tim e—> 41 A41211 m m N C e 0 0 a I' U f Q If I� I I i i I I� )0 5.00 6.00 7.00 8.00 9.00 1 0 .00 11.00 12.00 13.00 14.00 15.00 16.00 17.00 11 .D 36E0228.M Wed Apr 06 14:23:35 2005 SYS1 19.00 20.00 21.00 Page 00 O 0 L, 2 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41211.D Vial: 18 Acq On 4 Apr 2005 22:48 Operator: JV Sample : 0504067-002AMS Inst : H5971 Misc : TSL001,MW-1SMS,H20,MS „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 6 11:42 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:52:31 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.33 168 335769 50.00 UG/L -0.06 33) 1,4-Difluorobenzene 10.34 114 344703 50.00 UG/L -0.05 54) Chlorobenzene-d5 15.00 82 183056 50.00 UG/L -0.03 67) 1,4 -Dichlorobenzene -d4 17.63 152 158058 50.00 UG/L -0.04 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.01 65 111189 46.50 UG/L -0.05 Spiked Amount 50.000 Range 76 - 114 Recovery = 93.00% 52) Toluene -d8 12.21 98 336027 49.76 UG/L -0.05 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.52% 53) 4-Bromofluorobenzene 16.43 95 210189 47.42 UG/L -0.03 Spiked Amount 50.000 Range 86 - 115 Recovery = 94.84% rget Compounds Qvalue 8) 1,1-Dichloroethene 7.42 96 79212 46.72 UG/L 99 37) Benzene 10.15 78 321741 49.42 UG/L 99 39) Trichloroethene 10.75 95 147671 52.14 UG/L 99 46) Toluene 12.34 92 230245 52.58 UG/L 99 55) Chlorobenzene 15.06 112 300099 55.48 UG/L 90 a\ • O ------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration A41211.D 36E0228.M Wed Apr 06 14:23:34 2005 SYS1 Page 1 lA VOLATILE ORGANICS ANALYSIS DATA SHEET 10 Lab Name: H2M LABS, INC. • is Lab Code: 10478 Matrix: (soil/water) Sample wt/vol: 5 Level: (low/med) % Moisture: not dec. GC Column: R-502.2 Soil Extract Volume: Case No.: PCTSL WATER (g/mL) ML LOW Contract: SAS No.: ID: .53 (mm) (µL) CAS NO. COMPOUND 74-87-3 Chloromethane 75-01-4 Vinyl chloride 74-83-9 Bromomethane Lab Sample ID: Lab File ID: Date Received: Date Analyzed: Dilution Factor: EPA SAMPLE NO. MW-1SMSD SDG No.: TSL001 0504067-002AMSD A\A41213.D 04/04/05 04/04/05 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or µg/Kg)UG/L Q ----- --+ - - -5 — - - -U- 5 U - 5 U 75-00-3 Chloroethane 5 U 67-64-1 Acetone 5 U 107-13-1 Acrylonitrile 5 U 74-88-4 Iodomethane - 5 U 108-05-4 Vinyl acetate 5 U j 78-93-3 2-Butanone 5 U 75-15-0 ll Carbon disulfide 5 U - —- - -.-1 75-69-4 ---- - --- Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 47 U 75-09-2 Methylene chloride 156-60-5 1 trans-1,2-Dichloroethene 75-34-3 1,1-Dichloroethane 156-59-2 cis-1,2-Dichloroethene 74-97-5 Bromochloromethane 67-66-3 Chloroform — 5 5 5 5 - 5 5 U U U U U U 71-55-6 1,1,1 -Trichloroethane i 5 U 56-23-5 1 Carbon tetrachloride 5 U 71-43-2 Benzene 49 79-01-6 Trichloroethene 52 78-87-5 1,2-Dichloropropane 5 U 74-95-3 Dibromomethane 5 U j 75-27-4 Bromodichloromethane 5 U 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 52 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 56 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 1B VOLATILE ORGANICS ANALYSIS DATA SHEET • Lab Name: H2M LABS, INC. • • Contract: EPA SAMPLE NO. MW-1SMSD Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: 0504067-002AMSD Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41213.D Level: (low/med) LOW Date Received: 04/04/05 % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 2-Hexanone 5 U 630-20-6 1,1,1,2 Tetrachloroethane 5 I U 100-41-4 j Ethylbenzenei 5 U 1330-20-7 Xylene (total) 5 U 100-42-5 I 75-25-2 Styrene Bromoform j 5 5 U U I 110-57-6 trans-1,4-Dichloro-2-butene j 5 U 79-34-5 , 1,1,2,2 -Tetrachloroethane 5 U 96-18-4 - - - - - - j 1,2,3-Trichloropropane - - 5 U 106-4677 1,4 -Dichlorobenzene I 5 U -- - - 95-50-1 - ------ - -- 1,2 -Dichlorobenzene -- 5 U 96-12-8 ! 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41213.D Vial: 20 Acq On 4 Apr 2005 23:44 Operator: JV Sample : 0504067-002AMSD Inst : H5971 Misc : TSL0OI,MW-1SMSD,H20,MSD „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Apr 6 11:44 2005 Quant Results File: 36EO228.RES Method 0:\MS\HP5971\METHODS\36EO228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D ii 5.00 7.00 8.00 9.00 10. A41213.D 36EO228.M Wed Apr 06 14:23:58 2005 SYS1 Page 2 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41213.D Vial: 20 Acq On 4 Apr 2005 23:44 Operator: JV Sample : 0504067-002AMSD Inst : H5971 Misc : TSLOOI,MW-1SMSD,H20,MSD „ Multiplr: 1.00 S Integration Params: RTEINT.P Quant Time: Apr 6 11:44 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:52:31 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 3GE0228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.35 168 360283 50.00 UG/L -0.04 33) 1,4-Difluorobenzene 10.35 114 369679 50.00 UG/L -0.03 54) Chlorobenzene-d5 15.01 82 193596 50.00 UG/L -0.03 67) 1,4 -Dichlorobenzene -d4 17.64 152 170225 50.00 UG/L -0.03 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.03 65 119209 46.48 UG/L -0.03 Spiked Amount 50.000 Range 76 - 114 Recovery = 92.96% 52) Toluene -d8 12.23 98 358898 49.55 UG/L -0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.10% 53) 4-Bromofluorobenzene 16.44 95 224450 47.22 UG/L -0.03 Spiked Amount 50.000 Range 86 - 115 Recovery = 94.44% Wget Compounds Qvalue 8) 1,1-Dichloroethene 7.44 96 84609 46.51 UG/L 98 37) Benzene 10.17 78 343246 49.16 UG/L 98 39) Trichloroethene 10.77 95 157468 51.85 UG/L 100 46) Toluene 12.34 92 245451 52.26 UG/L 98 55) Chlorobenzene 15.06 112 321139 56.14 UG/L 90 M �O O O ----------------------------------------------------------------------- (#) = qualifier out of range (m) = manual integration [� A41213.D 36E0228.M Wed Apr 06 14:23:57 2005 SYS1 Page 1 �I J • lA VOLATILE ORGANICS ANALYSIS DATA SHEET Lab Name: H2M LABS, INC. Lab Code: 10478 Case No.: PCTSL Matrix: (soil/water) WATER Sample wt/vol: 5 (g/mL) ML Level: (low/med) LOW % Moisture: not dec. GC Column: R-502.2 ID: .53 Soil Extract Volume: (µL) CAS NO. COMPOUND Contract: EPA SAMPLE NO. MSB040405 SAS No.: SDG No.: TSL001 Lab Sample ID: MSB040405 Lab File ID: A\A41198.D Date Received: Date Analyzed: 04/04/05 mm) Dilution Factor: 1.00 Soil Aliquot Volume (µL) CONCENTRATION UNITS: (µg/L or Ag/Kg) UG/L Q -- - - - - - ' 74-87-3 Chloromethane 5 I U U 75-01-4 Vinyl chloride 5 5 74-83-9 i Bromomethane U 75-00-3 Chloroethane 5 5 j U U 67-64-1 Acetone ...107 -13 -1 ----- -- -- _ -- ----- --- -- - Acrylonitrile ! - -- - _ _ ._ 5 ---- U 74-88-4 Iodomethane 5 5 U 108-05-4 Vinyl �- U -- - - --- - 78-93-3 -- -acetate-, - - -- --- 2-Butanone - -- - -; 5 - - U 75-15-0 Carbon disulfide 5 U 75-69-4 Trichlorofluoromethane 5 U 75-35-4 1,1-Dichloroethene 50 75-09-2 Methylene chloride 4 BJ 156-60-5 f trans-1,2-Dichloroethene T j 5 U - - - - - -- 5 II — 75-34-3 1,1-Dichloroethane 156-59-2 1 cis-1,2-Dichloroethene 5 -5 i U 74-97-5 Bromochloromethane - U 67-66-3 i Chloroform 5 U 107-06-2 1,2-Dichloroethane j 5 U—� /1 -bb -6 1,1,1-Trlchioroethane 5 U 56-23-5 Carbon tetrachloride 5 1 U 71-43-2 1 Benzene 53 79-01-6 I Trichloroethene 55 78-87-5 1,2-Dichloropropane 5 U 74-95-3 ! Dibromomethane 5 U 75-27-4 Bromodichloromethane ; 5 * U J 10061-01-5 cis-1,3-Dichloropropene 5 U 108-88-3 Toluene 55 10061-02-6 trans-1,3-Dichloropropene 5 U 79-00-5 1,1,2 -Trichloroethane 5 U 106-93-4 1,2-Dibromoethane 5 U 108-10-1 4-Methyl-2-pentanone 5 U 108-90-7 Chlorobenzene 56 127-18-4 Tetrachloroethene 5 U 124-48-1 Dibromochloromethane 5 U FORM I VOA - 1 OLM04.2 110 CA CAS NO. COMPOUND 591-78-6 2-Hexanone 630-20-6 1,1,1,2 -Tetrachloroethane 100-41-4 ! Ethylbenzene E CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L -5- - 5 - 5 1330-20-7 ' Xylene (total) I 5 100-42-5 Styrene 5 75-25-2 Bromoform 5 110-57-6 trans-1,4-Dichloro-2-butene U U U U 79-34-5 j 1,1,2,2 -Tetrachloroethane 1B 5 EPA SAMPLE NO. 96-18-4 { VOLATILE ORGANICS ANALYSIS DATA SHEET U 106-46-7 ! 1,4 -Dichlorobenzene { 5 MSB040405 • Lab Name: H2M LABS, INC. Contract: U 96-12-8 Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: MSB040405 Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41198.D Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (pL) CAS NO. COMPOUND 591-78-6 2-Hexanone 630-20-6 1,1,1,2 -Tetrachloroethane 100-41-4 ! Ethylbenzene E CONCENTRATION UNITS: (µg/L or µg/Kg) UG/L -5- - 5 - 5 1330-20-7 ' Xylene (total) I 5 100-42-5 Styrene 5 75-25-2 Bromoform 5 110-57-6 trans-1,4-Dichloro-2-butene U U U U 79-34-5 j 1,1,2,2 -Tetrachloroethane 5 U I 96-18-4 { 1 2 3-Trichloropropane 5 U 106-46-7 ! 1,4 -Dichlorobenzene { 5 ! U 95-50-1 1,2 -Dichlorobenzene 7 5 U 96-12-8 1,2-Dibromo-3-chloropropane 5 U FORM I VOA - 2 OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41198.D Vial: 5 Acq On 4 Apr 2005 16:06 Operator: JV Sample : MSB040405 Inst : H5971 Misc : ,,,LCS „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 4 16:53 2005 Quant Results File: 36E0228.RES Method : 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:19:41 2005 Response via : Continuinq Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D 300000 280000- 260001 80000260001 240001 220001 200001 ,18000( 16000( 14000( 12000( 10000( 8000( 6000( 4000( 2000( ( rime - A41198.D 36E0228.M Wed Apr 06 14:19:51 2005 SYS1 Page 2 C/) Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41198.D Vial: 5 Acq On 4 Apr 2005 16:06 Operator: JV Sample : MSB040405 Inst : H5971 Misc : ,,,LCS „ Multiplr: 1.00 Is MS Integration Params: RTEINT.P Quant Time: Apr 4 16:53 2005 Quant Results File: 36E0228.RES Quant Method : C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Mon Apr 04 16:36:20 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth : 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.38 168 346009 50.00 UG/L 0.00 33) 1,4-Difluorobenzene 10.39 114 356428 50.00 UG/L 0.00 54) Chlorobenzene-d5 15.03 82 191629 50.00 UG/L 0.00 67) 1,4 -Dichlorobenzene -d4 17.67 152 163475 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.05 65 117544 47.54 UG/L 0.00 Spiked Amount 50.000 Range 76 - 114 Recovery = 95.08% 52) Toluene -d8 12.25 98 348351 49.89 UG/L 0.00 Spiked Amount 50.000 Range 88 - 110 Recovery = 99.78% 53) 4-Bromofluorobenzene 16.46 95 224828 49.05 UG/L 0.00 Spiked Amount 50.000 Range 86 - 115 Recovery = 98.10% 0rget Compounds Qvalue 8) 1,1-Dichloroethene 7.48 96 87772 50.24 UG/L 98 21) Methylene chloride 7.98 84 9187 3.96 UG/L 92 37) Benzene 10.20 78 354229 52.62 UG/L 99 39) Trichloroethene 10.79 95 159648 54.52 UG/L 99 46) Toluene 12.37 92 247870 54.74 UG/L 97 55) Chlorobenzene 15.09 112 314460 55.53 UG/L 90 f� i ------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration E.., A41198.D 36E0228.M Wed Apr 06 14:19:49 2005 SYS1 Page 1 • • Re& 0 e Scan 366 (7.490 min): A41195.13 (-) 96 Ra 40 47 82 0 f Sub 50 j g7 47 0}�f 25 30 35 40 45 96 82 70 75 80 85 90 95 ndance Scan 417 (7.992 min): A41195.13I Ain (-) sa RefO�' it 36 42 -> 30 35 40 45 50 55 ndance Scan 416 (7.983 min): A41198.13 49 84 Rao 40 I 44 1 � � I i -> 30 35 40 4-5-- 50 55 60 65 70 75 80 85 ---------------------- ndance Scan 416 (7.983 min): A41198.13 (-) 49 Md I Sub! 501 I • m/z-> 4I1 i 0- -- T 30 35 40 45 - 50 55 60 65 70 75 80 85 #18 1,1-Dichloroethene Concen: 50.24 UG/L RT: 7.48 min Scan# 365 Delta R.T. -0.01 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion: 96 Resp: 87772 Ion Ratio Lower Upper 96 100 61 169.0 145.8 185.8 63 56.4 35.0 75.0 ndancelon 96.00 (95.70 to 96.70): A41198.13 Ion 61.00 (60.70 to 61.70): A41198.13 35000 Ion 63.00 (62.70 to 63.70): A41198.D 30000 25000 20000 7.4 15000 10000 5000 0 a-> 7.30 7.40 7.50 7.60 7.70 #21 Methylene chloride Concen: 3.96 UG/L RT: 7.98 min Scan# 416 Delta R.T. -0.01 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion: 84 Resp: 9187 Ion Ratio Lower Upper 84 100 86 60.1 47.2 87.2 49 118.3 107.2 147.2 dancelon 84.00 (83.70 to 84.70): A41198.13 lion 86.00 (85.70 to 86.70): A41198.13 3000 ,Ion 49.00 (48.70 to 49.70): A41198.13 1 2500 90 95 2000 1500 1000 500 88 95 A41198.D 36E0228.M Wed Apr 06 14:19:52 2005 00 0- 7.857.90 + 8597 07.958.008.058.108.15 I O E-� SYSi Page 3 Re�O • 0 /z-> undana Rao 0 z-> bundana Sub 50 0 /z--> 30 35 40 45 50 55 60. 65 70- 75 80 85 90 95 100 1 Abundance Scan 702 (10.802 min): A41195.D (-) • � � 9� 1�2 Scan 641 (10.201 min): A41195.D (-) rt' -7 55 60 65 70 #37 Benzene Concen: 52.62 UG/L RT: 10.20 min Scan# 641 Delta R.T. 0.00 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion: 78 Resp: 354229 Ion Ratio Lower Upper 78 100 77 23.7 4.4 44.4 llon 77.00 (76.70 to 77.70): A41198.D8000010.20 85 90 95 100 105 60000 ON-) Re& 30 RaA1jj so 82 fill IIf 0 90 100 110 120-130 140__ .793 min): A41198.13 96 130 0 37 47 66� 82 III 114 f 36 r /z-> 30 40 50 60 70 80 90 100 110 120 130 140 �undance Scan 701 (10.793 min): A41198.1) (-) a Sub 504 60 ii 47 037 1 66 82 i r • /z-> 30 40 50 60 70 80 90 100 110 120 130 140 40000 20000 0 1 #39 Trichloroethene Concen: 54.52 UG/L RT: 10.79 min Scan# 701 Delta R.T. -0.01 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion: 95 Resp: 159648 Ion Ratio Lower Upper 95 100 130 99.3 78.3 118.3 132 98.1 77.0 117.0 A41198.D 36E0228.M Wed Apr 06 14:19:53 2005 IIon 130.00 (129.70 to 130.70): A411 ilon 132.00 (131.70 to 132.70): A411 40000 10.79 30000 20000 10000 0 �- O 10.60 10.80 11.00 11.20 r --f >A SYS1 Page 4 e Scan 862 (12.37 min): A41195.D (-) 0 z-> bundana Ra 0 z-> bundana Sub 50 0 39 r 40 45 51 50 T 60 6I5 70 74 80 85 I ,,)1.....�,�T 90 98 100 110 120 Tgt Ion:112 Resp: 314460 Ion Ratio Lower Upper 112 100 77 67.4 59.3 99.3 114 32.2 12.4 52.4 Abundance Scan 1138 (15. •77 Rek i 51 i 38 60 0 /z-> 30 40 50 60 70 81 77 RaA 112 1 #46 Toluene Concen: 54.74 UG/L RT: 12.37 min Scan# 861 Delta R.T. -0.01 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion: 92 Resp: 247870 Ion Ratio Lower Upper 92 100 91 164.5 148.5 188.5 1 51 38 44 I , 62 j ,3 91 99 19 01'+� �-+-�-T-rj�+Tl -� -+�- -- r -r+'+'* t T' rT'T z--> 30 40 50 60 70 80 90 100 110 120 130_140 6undance Scan 1137 (15.091 min): A41198.D (-) i 1 2 { 77 Sub 50 j 38 1. 44 5I1 61 3 91 99 19 �n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 i A41198.D 36E0228.M Wed Apr 06 14:19:54 200 80000 60000 40000 20000 0 1 #55 Chlorobenzene Concen: 55.53 UG/L RT: 15.09 min Scan# 1137 Delta R.T. -0.01 min Lab File: A41198.D Acq: 4 Apr 2005 16:06 Tgt Ion:112 Resp: 314460 Ion Ratio Lower Upper 112 100 77 67.4 59.3 99.3 114 32.2 12.4 52.4 )undanceIon 112.00 (111.70 to 112.70): A41198 Ion 77.00 (76.70 to 77.70): A41198.D Ion 114.00 (113.70 to 114.70): A41198 80000 15.09 60000 40000 o 200001 '--� o: 14.80 15.00 15.20 15.40 O 5 SYS1 Page 5 IA EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET LFB040405 is Lab Name: H2M LABS, INC. Contract: Vinyl chloride y j 55 Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Chloroethane Matrix: (soil/water) WATER Lab Sample ID: LFB040405 107-13-1 ! Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41197.D ! 52 Level: (low/med) LOW Date Received: 78-93-3 2-Butanone % Moisture: not dec. - - _ 75-15-0 Date Analyzed: 04/04/05 75-69-4 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 % 54 j Soil Extract Volume: (AL) Soil Aliquot Volume (µL) • CONCENTRATION UNITS: CAS NO. COMPOUND (pg/L or pg/Kg) UG/L Q 74-87-3 Chloromethane 55 --- 75-01-4 Vinyl chloride y j 55 74-83-9 Bromomethane j 52 75-00-3 Chloroethane 52 67-64-1 Acetone 44 107-13-1 ! Acrylonitrile 56 74-88-4 Iodomethane ! 52 108-05-4 Vinyl acetate 47� 78-93-3 2-Butanone 47 - - _ 75-15-0 —- --- - -- Carbon disulfide --- - --I - ---1 54 75-69-4 Trichlorofluoromethane 57 i 75-35-4 1,1-Dichloroethene % 54 j 75-09-2 Methylene chloride 50 B 156-60-5 trans-1,2-Dichloroethene 52 75-34-3 1 1,1-Dichloroethane 53 156-59-2 cis-1,2-Dichloroethene 50 74-97-5 Bromochloromethane 49 67-66-3 Chloroform 52 107-06-2 1,2-Dichloroethane 51 71-55-6 1,1,1 -Trichloroethane 57 56-23-5 Carbon tetrachloride 57 71-43-2 '. Benzene - - _- 51 - - - 79-01-6 Trichloroethene 53 78-87-5 T 1,2-Dichloropropane 50 74-95-3 ` Dibromomethane 48 75-27-4 Bromodichloromethane 51 10061-01-5 cis-1,3-Dichloropropene 50 108-88-3 Toluene 52 10061-02-6 trans-1,3-Dichloropropene 49 79-00-5 11112 -Trichloroethane 48 106-93-4 1,2-Dibromoethane 48 108-10-1 4-Methyl-2-pentanone 43 108-90-7 Chlorobenzene 51 127-18-4 Tetrachloroethene 52 124-48-1 • Dibromochloromethane 48 FORM I VOA - 1 OLM04.2 1B EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET LFB040405 • Lab Name: H2M LABS, INC. Contract: Lab Code: 10478 Case No.: PCTSL SAS No.: SDG No.: TSL001 Matrix: (soil/water) WATER Lab Sample ID: LFB040405 Sample wt/vol: 5 (g/mL) ML Lab File ID: A\A41197.D Level: (low/med) LOW Date Received: % Moisture: not dec. Date Analyzed: 04/04/05 GC Column: R-502.2 ID: .53 (mm) Dilution Factor: 1.00 Soil Extract Volume: (µL) Soil Aliquot Volume (µL) CONCENTRATION UNITS: CAS NO. COMPOUND (µg/L or µg/Kg) UG/L Q 591-78-6 none 630-20-6 1,1,1,2 -Tetrachloroethane -2-Tetrachloroethane - — 50 - --- _, 100-41-4 Ethylbenzene 52 1330-20-7 Xylene (total) 160 100-42-5 Styrene 50 75-25-2 Bromoform 46 110-57-6 trans-1,4-Dichloro-2-butene 46 • 79-34-5 1,1,2,2 -Tetrachloroethane 45 96-18-4 ! 1,2,3-Trichloropropane 45 - - - - 106 46-7 1,4 -Dichlorobenzene 50 95-50-1 112 -Dichlorobenzene 49 96-12-8 ! 1,2-Dibromo-3-chloropropane 44 P� FORM I VOA - 2 OLM04.2 Quantitation Report Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41197.D Vial: 4 Acq On 4 Apr 2005 15:39 Operator: JV Sample : LFB040405 Inst : H5971 Misc : ,,,LFB „ Multiplr: 1.00 *MS Integration Params: RTEINT.P Quant Time: Apr 4 16:48 2005 Quant Results File: 36E0228.RES Method 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update : Wed Apr 06 14:13:18 2005 Response via : Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D ndance TIC: A41197.13 —� 650000 600000 550000 500000 450000 350000 300000 250000 200000 150000 �i l 0 01,--r f ime—> 4.00 A41197.D c E 100000. ~ r c O �U C r 5000011� o S �i l 0 01,--r f ime—> 4.00 A41197.D 4 00 15.00 16.00 17.00 1 36E0228.M Wed Apr 06 14:17:39 2005 SYS1 Page 3 E F O C c O �U C r W G b U W O c m4 r' o a !$ 4 00 15.00 16.00 17.00 1 36E0228.M Wed Apr 06 14:17:39 2005 SYS1 Page 3 E F O C c O �U C r W G �GIII I I 0 _7.00 8.00 9.00 10.00 11 4 00 15.00 16.00 17.00 1 36E0228.M Wed Apr 06 14:17:39 2005 SYS1 Page 3 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41197.D Vial: 4 Acq On 4 Apr 2005 15:39 Operator: JV Sample : LFB040405 Inst : H5971 Misc : ,,,LFB „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 4 16:48 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:36:20 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 36EO228 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) Pentafluorobenzene 9.45 168 312980 50.00 UG/L 0.06 33) 1,4-Difluorobenzene 10.45 114 327677 50.00 UG/L 0.06 54) Chlorobenzene-d5 15.04 82 186400 50.00 UG/L 0.01 67) 1,4 -Dichlorobenzene -d4 17.67 152 164715 50.00 UG/L 0.00 System Monitoring Compounds 34) 1,2-Dichloroethane-d4 10.12 65 116124 51.08 UG/L 0.06 Spiked Amount 50.000 Range 76 - 114 Recovery = 102.16% 52) Toluene -d8 12.29 98 321580 50.09 UG/L 0.03 Spiked Amount 50.000 Range 88 - 110 Recovery = 100.18% 53) 4-Bromofluorobenzene 16.47 95 212771 50.50 UG/L 0.01 Spiked Amount 50.000 Range 86 - 115 Recovery = 101.00% �rget Compounds Qvalue 2) Dichlorodifluoromethane 4.37 85 100785 58.03 UG/L 100 3) Chloromethane 4.85 50 63437 55.04 UG/L 97 4) Vinyl chloride 5.16 62 75348 55.39 UG/L 100 5) Bromomethane 6.24 94 86009 51.58 UG/L 98 6) Chloroethane 6.39 64 51741 52.14 UG/L 100 7) Acetone 7.39 43 16051 43.55 UG/L 96 8) Acetonitrile 7.70 41 20602 200.39 UG/L 99 9) Allyl Chloride 7.94 41 139280 50.50 UG/L 97 10) Acrolein 7.32 56 39258 222.00 UG/L 100 11) Acrylonitrile 8.85 53 117648 55.83 UG/L 99 12) Iodomethane 7.91 142 197450 52.27 UG/L 98 13) Vinyl acetate 8.72 43 56184 46.61 UG/L 98 14) Chloroprene 8.85 53 117648 55.83 UG/L 97 15) 2-Butanone 9.11 43 32004 46.82 UG/L 97 16) Carbon disulfide 8.13 76 236736 54.28 UG/L 100 17) Trichlorofluoromethane 6.83 101 182897 56.53 UG/L 99 18) 1,1-Dichloroethene 7.56 96 85037 53.81 UG/L 98 21) Methylene chloride 8.07 84 105548 50.27 UG/L 98 22) trans-1,2-Dichloroethene 8.37 96 102471 52.17 UG/L 96 23) 1,1-Dichloroethane 8.76 63 199621 52.70 UG/L 100 24) Propionitrile 9.19 54 6220 44.39 UG/L 99 25) Isobutyl alcohol 9.38 43 16124 261.68 UG/L 84 26) Methacrylonitrile 9.36 67 26286 44.84 UG/L 91 27) cis-1,2-Dichloroethene 9.32 96 110303 50.46 UG/L 96 Bromochloromethane 9.63 128 74499 48.63 UG/L 99 *8) 928 77 152655 58.22 UG/L------98 --9)-2,2_ (##) ---------Dichloropropane = qualifier out of range (m) = manual integration A41197.D 36E0228.M Wed Apr 06 14:17:35 2005 SYS1 Page 1 Quantitation Report (QT Reviewed) Data File : 0:\MS\HP5971\DATA\APR05\040405A\A41197.D Vial: 4 Acq On 4 Apr 2005 15:39 Operator: JV Sample : LFB040405 Inst : H5971 Misc : ,,,LFB „ Multiplr: 1.00 •MS Integration Params: RTEINT.P Quant Time: Apr 4 16:48 2005 Quant Results File: 36E0228.RES Quant Method C:\HPCHEM\1\METHODS\36E0228.M (RTE Integrator) Title WATER PART360E ORGANICS PLUS Last Update Mon Apr 04 16:36:20 2005 Response via Continuing Cal File: C:\HPCHEM\1\DATA\APR05\040405A\A41195.D DataAcq Meth 36EO228 Compound R.T. QIon Response Conc Unit Qvalue ------------------------------------------------------------------------- 30) Chloroform 9.46 83 235384 52.13 UG/L 99 31) 1,2-Dichloroethane 10.21 62 136034 50.73 UG/L 99 32) 1,1,1 -Trichloroethane 9.85 97 201667 56.68 UG/L 99 35) 1,1-Dichloropropene 9.98 75 162897 54.26 UG/L 99 36) Carbon tetrachloride 10.11 117 204136 57.46 UG/L 99 37) Benzene 10.26 78 315724 51.01 UG/L 99 38) Methyl Methacrylate 10.94 69 73270 44.50 UG/L 94 39) Trichloroethene 10.85 95 143717 53.38 UG/L 99 40) 1,2-Dichloropropane 11.03 63 130843 49.85 UG/L # 99 41) Dibromomethane 11.40 93 131463 48.43 UG/L 99 44) Bromodichloromethane 11.30 83 273466 51.15 UG/L 100 45) cis-1,3-Dichloropropene 11.91 75 222357 50.11 UG/L 100 46) Toluene 12.42 92 216638 52.04 UG/L 98 Ethyl Methacrylate 12.41 69 158984 46.12 UG/L 99 07) 48) trans-1,3-Dichloropropene 12.58 75 193873 48.75 UG/L 99 49) 1,1,2 -Trichloroethane 12.87 83 110836 48.00 UG/L 99 50) 1,2-Dibromoethane 14.35 107 186136 47.74 UG/L 100 51) 4-Methyl-2-pentanone 11.54 43 93345 43.45 UG/L 99 55) Chlorobenzene 15.11 112 280507 50.93 UG/L 100 56) 1,3-Dichloropropane 13.29 76 205411 47.32 UG/L 99 57) Tetrachloroethene 13.52 164 142664 52.48 UG/L 99 58) Dibromochloromethane 13.92 129 245806 48.24 UG/L 99 59) 2-Hexanone 12.73 43 61993 42.75 UG/L 99 60) 1,1,1,2 -Tetrachloroethane 15.13 131 167282 50.42 UG/L 96 61) Ethylbenzene 15.13 106 111154 51.95 UG/L 100 62) m,p-Xylene 15.24 106 325156 103.88 UG/L 99 63) o -Xylene 15.81 106 150029 51.99 UG/L 99 64) Xylene (total) 15.24 106 465222m 161.22 UG/L qvv� 65) Styrene 15.84 104 253559 50.24 UG/L 100 66) Bromoform 16.27 173 171252 46.40 UG/L 100 68) trans-1,4-Dichloro-2-buten 16.55 53 32711 46.41 UG/L # 97 69) 1,1,2,2 -Tetrachloroethane 16.36 83 178857 44.62 UG/L 100 70) Pentachloroethane 17.21 167 127426 48.95 UG/L ## 97 71) 1,2,3-Trichloropropane 16.52 112 29409 44.57 UG/L ## 89 72) 1,3 -Dichlorobenzene 17.60 146 233129 49.55 UG/L 99 W) 73) 1,4 -Dichlorobenzene 17.70 146 278001 49.78 UG/L 99r- 74) 1,2 -Dichlorobenzene 18.10 146 243546 49.30 UG/L 98 75) 1,2-Dibromo-3-chloropropan 18.92 75 40359 44.50 UG/L 98 . _ O O ------------------------------------------------------------------------- (##) = qualifier out of range (m) = manual integration Cn [� A41197.1) 36E0228.M Wed Apr 06 14:17:36 2005 SYS1 Page 2 Quantitation Report Data File 0:\MS\HP5971\DATA\APR05\040405A\A41197.D Vial: 4 Acq On 4 Apr 2005 15:39 Operator: JV Sample LFB040405 Inst : H5971 Misc ,,,LFB „ Multiplr: 1.00 •13flaffifatT4metiAprPaCatb6:4RTEMUT.P Quant Results File: temp.res Method 0:\MS\HP5971\METHODS\36E0228.M (RTE Integrator) Title : WATER PART360E ORGANICS PLUS Last Update Wed Apr 06 14:13:18 2005 Response via Single Level Calibration bundance Ion 106.00 (105.70 to 106.70): A41197.13 j 200000 150000 100000 50000 14.20 14.40 14.60 14.80 15.00 15.20 15.40 15.60 15.80 16.00 16.20 16.40 16.60 16. abundance Scan 1152 (15.238 min): A41197.13 1 100000 106 50000 77 39 44 51 55 61 65 73 82 87 95 10 112x117121 131135 ,,-rrT,.-'1T--rf-fi,-r, .--,--i- L -r -,T -----7-r -+-fir{,--,-rr+-rrr;,-tri-rrrT,7,�--,T-rri ,T, i -,fir rt Fr,-rr,-r-,-F- I ,T,-,-rT-r-,-rr n/z-> 30. 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 125 130 135 140 _ lbundance Scan 1209 (15.800 min): A41195.13 (-) 5000 39 51 78 43 1 1 55� � 63 74 z-> 30 35 40 45 50 55 60 65 70 75 1 (64) Xylene (total) (1) 15.24min 161.22UG/L m response 465222 Ion Exp% Act% 106.00 100 100 91.00 225.30 223.81 105.00 56.20 47.22 0.00 0.00 0.00 r �J 106 98 10 t 95 100 105 110 115 120 125 130 135 140 A41197.D 36E0228.M Wed Apr 06 14:18:32 2005 SYS1 H2M LABS, INC. • WHERE: • COMPUTATIONS FOR VOLATILE ORGANICS PERFORMED BY RTE DATA SYSTEM OF HP Ax Is CONC =-------- ----- Ais x RRF W CONC = Concentration in sample (ug/L or ug/KG) Ax = Area of characteristic ion of compound Ais = Area of characteristic ion of internal standard RRF = Relative response factor as area per (ng) of compound, divided by area per ng of respective internal standard Is = Amount of internal standard injected (ng) W = Volume of sample in (ml) or dry weight (g) Generally the amount of each internal standard injected is 250 ng. • H2M LABS, INC. V. DOCUMENTATION FOR VOLATILE ORGANICS A. LOG BOOK PAGES B. REPORTING ANALYST SIGNATURE PAGE • • 00 r - r O H mops, . �mm r i IM 1�- MMEaIMM, �o mm .WIr' :.0 l Wor m :M M r a" i� . T.�A IN MME■,ITSS', ' ; l KE Y M 1✓ 77 r / ► III `�_. �� J :.�l���f�i����® -=.. mm,-►�. ©M -M,■.■. -.■MM■_■ MMEMORI =mom Mom", IMMOMMOOMMEME ., , Elm mmm�m • H2M LABS, INC. SDG # TSL001 SCAN: VOA This data package was reported by the undersigned. This reporting includes data calculations, manual edits, if necessary, and compilation of raw data. The information presented is true and correct to the best of my knowledge. Signature: • 4/6/2005 C7 N 00 O O E—�