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Wet Chemistry Data Package 06/2005
Analytical Data Package For TOWN OF SOUTHOLD PI tT360 ROUTINE SIDG NQ: TSL002 l , Vater Samples Received: 6/10/05 WET CHEM TRY I ATA PACKAGE JUNE 2005 4 Al�*A I-AUS, INC401 Onvironment Testing Laboratories 575 Broad Hollow Road, Melville, N.Y. 11747 � ]l • • U2M LABS, INC. i"SLOOQ TABLE OF CONTENTS I. SAMPLE REPORTS II. Q.C. SUMMARY III. RAW DATA N O V) H U2M ILAI3S, INC. SAMPLE REPORTS • • U2M "USO INC. 575BfoadFUM hoed, MO& NY 11747 LABORATORY RESULTS (631)6943040. FAX (631)4M K% NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-001 Type: Groundwater Attn To Origin: Client ID. : MW -1D Collected :6/10/2005 9:00:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 4.3 1 mg/L E310.1 06/14/200511:37 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 4:30 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 3:10 PM Chloride 74.6 1 mg/L E325.2 06/13/2005 11:57 AM Chemical Oxygen Demand <10 1 mg/L E410.4 06/16/2005 11:52 AM Hardness (As CaCO3) 68.0 2 mg/L E130.2 06/14/2005 9:20 AM Nitrogen, Ammonia (As N) < 0.10 1 mg/L E350.1 06/22/200511:45 AM Nitrate as N 5.44 20 mg/L E353.2 06/11/2005 4:58 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 9:00 AM Sulfate 27.7 1 mg/L SW9038 06/20/2005 7:34 AM Total Dissolved Solids 208 1 mg/L E160.1 06/14/2005 2:44 PM Nitrogen, Kjeldahl, Total 0.29 1 mg/L E351.2 06/23/20051:26 PM Total Organic Carbon < 1.0 1 mg/L SW9060 06/13/2005 7:59 PM r� Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported: 6/27/2005 Page 1 of 12 Laboratory Manager U2M I AUS, INCe 57513toadHolow Road, Mt=lvie NY 11747 (631)691. M. FAX (631)4M.84,% NYSDOH ID# 10478 • Town of Southold Landfill Attn To : Origin: LABORATORY RESULTS Sample Information... Lab No. : 0506329-002 Type: Groundwater Client ID. : MW -1S Collected :6/10/2005 8:30:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(sl Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 3.9 1 mg/L E310.1 06/14/2005 11:38 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 4:35 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 3:15 PM Chloride 73.6 1 mg/L E325.2 06/13/2005 11:58 AM Chemical Oxygen Demand <10 1 mg/L E410.4 06/16/2005 11:53 AM Hardness (As CaCO3) 62.0 2 mg/L E130.2 06/14/2005 9:25 AM Nitrogen, Ammonia (As N) 0.12 1 mg/L E350.1 06/22/2005 11:45 AM Nitrate as N 5.35 10 mg/L E353.2 06/11/2005 4:58 PM Phenolics, Total Recoverable < 5.0 1 Ng/L E420.1 06/22/2005 9:15 AM Sulfate 23.8 2.5 mg/L SW9038 06/20/2005 7:36 AM Total Dissolved Solids 223 1 mg/L E160.1 06/14/2005 2:45 PM Nitrogen, Kjeldahl, Total 0.16 1 mg/L E351.2 06/23/2005 1:26 PM Total Organic Carbon < 1.0 1 mg/L SW9060 06/13/2005 8:28 PM • Qualifiers: E - Value above Quanlitalion range D - Results for Dilution D.F. = Dilution Factor Date Reported: 6/27/2005 Page 2 of 12 ? a4v"k. �h Laboratory Manager U2M "US, INC. 575BtaedHc1W hoed, Movie NY 11747 LABORATORY RESULTS (631)684.9040. FAX(631)4248436 NYSDOH1D#10478 Sample Information... Town of Southold Landfill Lab No. : 05506329-003 Type: Groundwater Origin: Attn To Client ID. : MW -3D Collected :6/10/200510:00:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 59.2 1 mg/L E310.1 06/13/2005 11:47 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 4:45 PM Bromide 0.9 1 mg/L E320.1 06/22/2005 3:30 PM Chloride 6.6 1 mg/L E325.2 06/13/200512:01 PM Chemical Oxygen Demand 29.3 1 mg/L E410.4 06/16/2005 11:56 AM Hardness (As CaCO3) 80.0 4 mg/L E130.2 06/14/2005 9:40 AM Nitrogen, Ammonia (As N) 0.11 1 mg/L E350.1 06/22/2005 11:47 AM Nitrate as N 1.06 5 mg/L E353.2 06/11/2005 5:00 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 10:00 AM Sulfate 14.9 1 mg/L SW9038 06/20/2005 7:38 AM Total Dissolved Solids 136 1 mg/L E160.1 06/14/2005 2:48 PM Nitrogen, Kjeldahl, Total 0.26 1 mg/L E351.2 06/23/2005 1:28 PM Total Organic Carbon 6.7 1 mg/L SW9060 06/13/2005 9:54 PM • • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 6/27/2005 Page 3 of 12 IH2M LAOS, INC. 5758roadHokw Rued, Mtivile NY 11747 LABORATORY RESULTS (631)694--3M.FAX- (631)4M436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. :0506329-004 Type: Groundwater Origin: AMn To Client ID. : MW -3S Collected :6110/2005 9:30:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 61.8 1 mg/L E310.1 06/13/200511:52 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 4:50 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 3:35 PM Chloride 6.6 1 mg/L E325.2 06/13/200512:02 PM Chemical Oxygen Demand 14.3 1 mg/L E410.4 06/16/2005 11:59 AM Hardness (As CaCO3) 88.0 4 mg/L E130.2 06/14/2005 9:45 AM Nitrogen, Ammonia (As N) 0.10 1 mg/L E350.1 06/22/2005 11:48 AM Nitrate as N 1.16 5 mg/L E353.2 06/11/2005 5:01 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/200510:15 AM Sulfate 15.2 1 mg/L SW9038 06/20/2005 7:40 AM Total Dissolved Solids 126 1 mg/L E160.1 06/14/2005 2:49 PM Nitrogen, Kjeldahl, Total 0.32 1 mg/L E351.2 06/23/2005 1:29 PM Total Organic Carbon 6.1 1 mg/L SW9060 06/13/2005 10:22 PM C, Qualifiers: E, Value above quantitation range •D . Results for Dilution D.F. = Dilution Factor Date Reported: 6/27/2005 Page 4 of 12 Q/ww � • . Laboratory Manager u2M 1. Uso INC. 575BradHdlm Rced, Md& NY 11747 LABORATORY RESULTS (631)694.3040. FAX (631)42084.% WSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-005 Type: Groundwater ' ttn To Origin: A Client ID.: MW -41) Collected :6/9/200512:00:00 PM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameters) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 41.9 1 mg/L E310.1 06/14/2005 11:41 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 4:55 PM Bromide 1.7 1 mg/L E320.1 06/22/2005 3:40 PM Chloride 24.6 1 mg/L E325.2 06/13/200512:03 PM Chemical Oxygen Demand 14.3 1 mg/L E410.4 06/16/2005 12:00 PM Hardness (As CaCO3) 60.0 2 mg/L E130.2 06/14/2005 9:50 AM Nitrogen, Ammonia (As N) 4.65 10 mg/L E350.1 06/22/2005 11:49 AM Nitrate as N 3.18 5 mg/L E353.2 06/11/2005 5:02 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 10:30 AM Sulfate 19.8 1 mg/L SW9038 06/20/2005 7:42 AM Total Dissolved Solids 135 1 mg/L E160.1 06/14/2005 2:50 PM Nitrogen, Kjeldahl, Total 4.17 10 mg/L E351.2 06/23/20051:30 PM Total Organic Carbon 3.7 1 mg/L SW9060 06/13/200510:50 PM r� Qualifiers: E - Value above quantitation range •D -Results for Dilution D.F. = Dilution Factor Date Reported: 6/27/2005 Page 5 of 12 ? aqt� A 1-d-&4� Laboratory Manager U24 "US, INC. 575BiaWH*w Road, M&& NY 11747 LABORATORY RESULTS (631)694, M -FAX (631)42M436 NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 05506329-006 Type : Groundwater i. Attn To : Origin: Collected :6/9/2005 1:30:00 PM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Client ID. : MW -5D Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 51.2 1 mg/L E310.1 06/13/2005 12:02 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:00 PM Bromide 0.7 1 mg/L E320.1 06/22/2005 3:45 PM Chloride 23.1 1 mg/L E325.2 06/13/2005 12:03 PM Chemical Oxygen Demand 11.8 1 mg/L E410.4 06/16/2005 12:01 PM Hardness (As CaCO3) 70.0 2 mg/L E130.2 06/14/2005 9:55 AM Nitrogen, Ammonia (As N) 4.63 10 mg/L E350.1 06/22/2005 11:49 AM Nitrate as N 3.08 5 mg/L E353.2 06/11/2005 5:02 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 10:45 AM Sulfate 20.3 1 mg/L SW9038 06/20/2005 7:44 AM Total Dissolved Solids 163 1 mg/L E160.1 06/14/2005 2:51 PM Nitrogen, Kjeldahl, Total 3.94 10 mg/L E351.2 06/23/2005 1:32 PM Total Organic Carbon 4.4 1 mg/L SW9060 06/13/2005 11:18 PM • Qualifiers: E - Value above quantitation range .D - Results for Dilution D.F. = Dilution Factor Date Reported : 6/27/2005 Page 6 of 12 Laboratory Manager 00 N O I— C/� U2M "US, INC. 57513roml lm R°ed' Mdvile W 11747 LABORATORY RESULTS (631)694.9040. FAX (631)42084% NYSDOH ID# 10478 Town of Southold Landfill Lab No. : 0506329-007 Sample Information... • Type : Groundwater Attn To : Origin: Collected :6/9/2005 12:30:00 PM Received :6110/20051:50:00 PM Collected By VG03 Copies To :Original CC Client ID.: MW -5S Parameters) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3), High 54.8 1 mg/L E310.1 06/13/2005 12:07 PM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:05 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 3:50 PM Chloride 23.3 1 mg/L E325.2 06/13/200512:04 PM Chemical Oxygen Demand 14.3 1 mg/L E410.4 06/16/2005 12:02 PM Hardness (As CaCO3) 60.0 2 mg/L E130.2 06/14/2005 10:10 AM Nitrogen, Ammonia (As N) 4.70 10 mg/L E350.1 06/22/200511:50 AM Nitrate as N 3.10 5 mg/L E353.2 06/11/2005 5:03 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 11:00 AM Sulfate 19.8 1 mg/L SW9038 06/20/2005 7:46 AM Total Dissolved Solids 148 1 mg/L E160.1 06/14/2005 2:52 PM Nitrogen, Kjeldahl, Total 3.74 10 mg/L E351.2 06/23/2005 1:32 PM Total Organic Carbon 4.5 1 mg/L SW9060 06/14/2005 12:45 AM • Qualifiers: E - Value above quantitation range fives^ • D - Results for Dilution D.F. = Dilution Factor Laboratory Manager Date Reported : 6/27/2005 Page 7 of 12 U2M "US, INC. 5758&oadH0111Aw Road, Mdv1e NY 11747 LABORATORY RESULTS (631)694,3040. FAX (631)42D8436 NYSDOH1D#10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-008 Type: Groundwater •. Attn To Origin: Collected :619/2005 2:30:00 PM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Client ID. : MW -6D Parameterfs) Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 41.0 2 mg/L E310.1 06/14/2005 11:42 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:10 PM Bromide 0.6 1 mg/L E320.1 06/22/2005 3:55 PM Chloride 24.2 1 mg/L E325.2 06/13/2005 12:05 PM Chemical Oxygen Demand 11.8 1 mg/L E410.4 06/16/200512:03 PM Hardness (As CaCO3) 58.0 2 mg/L E130.2 06/14/2005 10:15 AM Nitrogen, Ammonia (As N) 4.09 10 mg/L E350.1 06/22/2005 11:51 AM Nitrate as N 3.19 5 mg/L E353.2 06/11/2005 5:04 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 11:15 AM Sulfate 19.7 1 mg/L SW9038 06/20/2005 7:48 AM Total Dissolved Solids 153 1 mg/L E160.1 06/14/2005 2:53 PM Nitrogen, Kjeldahl, Total 4.68 10 mg/L E351.2 06/23/2005 1:33 PM Total Organic Carbon 3.5 1 mg/L SW9060 06/14/2005 1:13 AM • Qualifiers: E - Value above quantitation range A • D - Results for Dilution Q�K . D.F. = Dilution Factor Laboratory Manager Date Reported : 6/27/2005 Page 8 of 12 U24 "US, INC. 575BroedH0bN Road, W& NY 11747 LABORATORY RESULTS (631)684-.9040.FAX (631)42(}8M NYSDOH ID# 10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-009 Type: Groundwater Attn To : Origin: Client ID. : MW -6S Collected :6/9/2005 2:00:00 PM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameters) Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 25.2 1 mg/L E310.1 06/14/2005 11:43 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:15 PM Bromide 1.0 1 mg/L E320.1 06/22/2005 4:00 PM Chloride 24.9 1 mg/L E325.2 06/13/200512:05 PM Chemical Oxygen Demand 16.8 1 mg/L E410.4 06/16/200512:04 PM Hardness (As CaCO3) 62.0 2 mg/L E130.2 06/14/200510:20 AM Nitrogen, Ammonia (As N) 4.29 10 mg/L E350.1 06/22/2005 11:53 AM Nitrate as N 3.30 5 mg/L E353.2 06/11/2005 5:06 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/200511:30 AM Sulfate 45.2 2.5 mg/L SW9038 06/20/2005 7:50 AM Total Dissolved Solids 171 1 mg/L E160.1 06/14/2005 2:56 PM Nitrogen, Kjeldahl, Total 3.61 10 mg/L E351.2 06/23/2005 1:34 PM Total Organic Carbon 3.6 1 mg/L SW9060 06/14/2005 1:42 AM 11 Qualifiers: E - Value above quantitation range • D - Results for Dilution D.F. = Dilution Factor Date Reported : 6/27/2005 Page 9 of 12 Laboratory Manager F12M LABS, INC. 575BtoadFlobN laced, M*ft W 11747 LABORATORY RESULTS (631)6943040.FAX (631)QM36 WSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-010 Type: Groundwater • Attn To : Origin: Collected :6/9/2005 11:30:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Client ID. : MW -8D Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 44.1 2 mg/L E310.1 06/14/2005 11:44 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:20 PM Bromide 0.6 1 mg/L E320.1 06/22/2005 4:05 PM Chloride 23.7 1 mg/L E325.2 06/13/2005 12:06 PM Chemical Oxygen Demand 26.8 1 mg/L E410.4 06/16/2005 12:05 PM Hardness (As CaCO3) 60.0 2 mg/L E130.2 06/14/2005 10:25 AM Nitrogen, Ammonia (As N) 3.86 10 mg/L E350.1 06/22/2005 11:53 AM Nitrate as N 3.19 5 mg/L E353.2 06/11/2005 5:06 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 11:45 AM Sulfate 20.1 1 mg/L SW9038 06/20/2005 7:52 AM Total Dissolved Solids 161 1 mg/L E160.1 06/14/2005 2:57 PM Nitrogen, Kjeldahl, Total 3.12 10 mg/L E351.2 06/23/2005 1:34 PM Total Organic Carbon 3.9 1 mg/L SW9060 06/14/2005 2:11 AM • • Qualifiers: E - Value above Quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 6/27/2005 Page 10 of 12 Laboratory Manager 1H2M "US, INC. 575BradHdlav Road, ME#Vb NY 11747 LABORATORY RESULTS (631)6943040. FAX (631)4WK% NYSDOH ID# 10478 Town of Southold Landfill Lab No. : 0506329-011 Sample Information... • Type: Groundwater Attn To : Origin: Client ID. : MW -8S Collected :6/9/200510:50:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F. Units Method Number Analyzed Alkalinity, Total (As CaCO3) 38.8 1 mg/L E310.1 06/14/200511:45 AM Biochemical Oxygen Demand 3 1 mg/L E405.1 06/10/2005 5:25 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 4:10 PM Chloride 24.9 1 mg/L E325.2 06/13/200512:07 PM Chemical Oxygen Demand 14.3 1 mg/L E410.4 06/16/2005 12:06 PM Hardness (As CaCO3) 58.0 2 mg/L E130.2 06/14/200510:30 AM Nitrogen, Ammonia (As N) 3.60 10 mg/L E350.1 06/22/2005 11:54 AM Nitrate as N 3.21 5 mg/L E353.2 06/11/2005 5:07 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 12:00 PM Sulfate 18.4 1 mg/L SW9038 06/20/2005 7:54 AM Total Dissolved Solids 142 1 mg/L E160.1 06/14/2005 2:58 PM Nitrogen, Kjeldahl, Total 3.21 10 mg/L E351.2 06/23/2005 1:35 PM Total Organic Carbon 3.4 1 mg/L SW9060 06/14/2005 2:39 AM • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 6/27/2005 Page 11 of 12 Laboratory Manager U2M LADS, INC. 5758roadFt: ov Road, Movie NY 11747 LABORATORY RESULTS (631)694 W. FAX(631)4248436 NYSDOHID#10478 Sample Information... Town of Southold Landfill Lab No. : 0506329-012 Type : Groundwater • Attn To : Origin: Client ID.: EQPT BLANK Collected :6/10/200510:15:00 AM Received :6/10/20051:50:00 PM Collected By VG03 Copies To :Original CC Parameter(s) Results Qualifier D.F.. Units Method Number Analyzed Alkalinity, Total (As CaCO3) < 1.0 1 mg/L E310.1 06/14/2005 11:48 AM Biochemical Oxygen Demand < 2 1 mg/L E405.1 06/10/2005 5:30 PM Bromide < 0.5 1 mg/L E320.1 06/22/2005 4:15 PM Chloride < 2.0 1 mg/L E325.2 06/13/2005 12:07 PM Chemical Oxygen Demand <10 1 mg/L E410.4 06/16/2005 12:07 PM Hardness (As CaCO3) < 5.0 1 mg/L E130.2 06/14/2005 10:35 AM Nitrogen, Ammonia (As N) 0.12 1 mg/L E350.1 06/22/2005 11:55 AM Nitrate as N < 0.10 1 mg/L E353.2 06/11/2005 5:08 PM Phenolics, Total Recoverable < 5.0 1 pg/L E420.1 06/22/2005 12:15 PM Sulfate < 5.0 1 mg/L SW9038 06/20/2005 7:56 AM Total Dissolved Solids 10 1 mg/L E160.1 06/14/2005 2:59 PM Nitrogen, Kjeldahl, Total 0.16 1 mg/L E351.2 06/23/2005 1:36 PM Total Organic Carbon < 1.0 1 mg/L SW9060 06/14/2005 3:05 AM .7 • Qualifiers: E - Value above quantitation range D - Results for Dilution D.F. = Dilution Factor Date Reported : 6/27/2005 Page 12 of 12 Laboratory Manager U2M LABS, INC. 0 il. Q.C. SUMMARY • • 0 0 0 112M LABS, INC. Date: 24 -Jun -05 QC SUMMARY REPORT SDG: TSL002 Spike Sample Recovery RPDRef %RPD _-Sample ID: __Client Sample ID: Analyte Result Units Amount Result %REC Limits Value %RPD UCL IMBLKWW5 MBLK061405 LCS061405 LCS061405 0506329-002dms mw -isms 0506329-002ddup MW-1SDUP Alkalinity, Total (As CaCO3) < I mg/L Alkalinity, Total (As CaCO3) 21.2 mg/L 25 < 1 85 80 120 Alkalinity, Total (As CaCO3) 28.8 mg/L 25 3.9 115 75 125 Alkalinity, Total (As CaCO3) 4.0 mg/L 3.9 3.8 20 jlWBLK06i305 ILCS061305 -71MBLK66146 5 ILCS061305 ------ — 80 Bromide -T mg/L I MGVL 125 1 < 5 102 120 Alkalinity, Total (As CaCO3), High -5�5--l 21 L Bromide 0506329-002DMS MBLK061005 Bromide. 0506329-002Ddup mWL T ------- 7-- 84 75 125 MBLK061005 Biochemical Oxygen Demand < 2 LCS061005 LCS061005 Biochemical Oxygen Demand 203 mg/L 200 < 2 102 80 1120 0506329-002ddup JMW-1SDUP Biochemical Oxygen Demand < 2 � < 2 20 Alkalini Total As CaCO3 , Hi h TSL002 W16 MB -R50421 80 MB -1150421 MB -R50421 mg/L Bromide LCS-R50421 LCS-R50421 4.8 Bromide 0506329-002DMS 96 80 120 Bromide. 0506329-002Ddup -1SDUP 84 75 125 Bromide iMBLK061605 ;MBLK061605 !Chemical Oxygen Demand <10 mg/L iLCS061605 LCS061605 iChemical Oxygen Demand 1140 mg/L 1000 <10 114 80 120; t - 0506329-002cms !Mw -isms Chemical Oxygen Demand 1070 mg/L 1000 < 10 107 75 125 0-5-0-63-2-9---0-02 cd u p MW-ISDUP Chemical Oxygen Demand <10 ffV/L 10 0 _120 MB -061305 MB -061305 Chloride <2 mg/L LCS-061305 LCS-061305 mg/L 50.3 50 < 2 101 80 12+0 05D6329-002DMS mw -isms Chloride 97.6 mg/L 25 73.6 96 75 125 0506329-002DDUP MW-lSDUP Chloride 75.2 mg/L 2 < 0.5 mg/L 4.8 g/L 5 < 0.5 96 80 120 42 mg/L 5 < 0.5 84 75 125 < 0.5 mg/L iMBLK061605 ;MBLK061605 !Chemical Oxygen Demand <10 mg/L iLCS061605 LCS061605 iChemical Oxygen Demand 1140 mg/L 1000 <10 114 80 120; t - 0506329-002cms !Mw -isms Chemical Oxygen Demand 1070 mg/L 1000 < 10 107 75 125 0-5-0-63-2-9---0-02 cd u p MW-ISDUP Chemical Oxygen Demand <10 ffV/L 10 0 _120 MB -061305 MB -061305 Chloride <2 mg/L LCS-061305 LCS-061305 mg/L 50.3 50 < 2 101 80 12+0 05D6329-002DMS mw -isms Chloride 97.6 mg/L 25 73.6 96 75 125 0506329-002DDUP MW-lSDUP Chloride 75.2 mg/L 2 0 SDG: TSL002 Sample ID: Client Sample ID: Analvte Result M B K061405 K JMBLK061405 Hardness s CaCO3) <5 LCS061405 ILCS061405 ---FHardness (As CaCO3) 1040 0506329-002bms IHardness (As CaCO3) 1 268 0506329-002bdup jMW-1SDUP -Hardness (As (As CaCO3) 62.0 QC SUMMARY REPORT m b. --061 -10 5 �!M6-661-105 Nitrate as N mg/L. - --- --- lics--061105 1 -661 O�5 Nitrate 4mg/L 1.13 <0.1 93 8 , 0 120 TI - 5 al k2 �2 &6 - 0-0 2-6 M --S _JS S _N F65 MW -ISMS jNitrate _ajN 10.3 mg/ . L 5 5.35 .991-75 1125 - --4 ! -N- J P 0506329-002CDUP Im D Nitrate as 1 5.41 i mg/L 1 5.35 1 1.2 6 MB -062205 Nitrogen, Ammonia (As N) < 0. 1 mg/L MB -13915 -1 1 Nitrogen, Ammonia (As N) 1.15 LCS-13915 JLCS 062205 mg/L 1 < 0.1 1 115 80 120 0506329-002CMS smS. Nitrogen, Ammonia (As N) 5 57 I mg/L 5 0.12 1 109 75 1 0506329-002CDUP -FS6-U0 Nitrogen, Ammonia (As N) [_O mg/L 0.1 2 6.8 L20, j [mb-13925 imb 62305 !Nitrogen, Kjeldahl, Total <0.1- mg/L Ics-13925 Ics-062305 Nitrogen Kjeldahl, Total 4.11 mg -;L -4-.1- 1 6.1 i0o lio 1 mg/L 6666329-0026MS 75 120 4.1 .�Mw-isms Kjeldahl, Total 3.90 0.16 1 91 �110506329-002CDLJP MW-1SDUP �Nitrogen, Kjeldahl, Total 0.11 mg/L 0.16 40.9 20 MB -062205 Spike Sample Recovery RPDRef %RPD Units Amount Result %REC Limits Value %RPD UCL I m-g/L 7F 0506329-002Cdup MWASDUP Phenolics, Total Recoverable ug/L < 5 mg/L 1000 < 5 1 104 80 1201 mg/L ---I--- 200 62.0 103 75 125 mg/L62.0 - _- - I __fl 020 m b. --061 -10 5 �!M6-661-105 Nitrate as N mg/L. - --- --- lics--061105 1 -661 O�5 Nitrate 4mg/L 1.13 <0.1 93 8 , 0 120 TI - 5 al k2 �2 &6 - 0-0 2-6 M --S _JS S _N F65 MW -ISMS jNitrate _ajN 10.3 mg/ . L 5 5.35 .991-75 1125 - --4 ! -N- J P 0506329-002CDUP Im D Nitrate as 1 5.41 i mg/L 1 5.35 1 1.2 6 MB -062205 Nitrogen, Ammonia (As N) < 0. 1 mg/L MB -13915 -1 1 Nitrogen, Ammonia (As N) 1.15 LCS-13915 JLCS 062205 mg/L 1 < 0.1 1 115 80 120 0506329-002CMS smS. Nitrogen, Ammonia (As N) 5 57 I mg/L 5 0.12 1 109 75 1 0506329-002CDUP -FS6-U0 Nitrogen, Ammonia (As N) [_O mg/L 0.1 2 6.8 L20, j [mb-13925 imb 62305 !Nitrogen, Kjeldahl, Total <0.1- mg/L Ics-13925 Ics-062305 Nitrogen Kjeldahl, Total 4.11 mg -;L -4-.1- 1 6.1 i0o lio 1 mg/L 6666329-0026MS 75 120 4.1 .�Mw-isms Kjeldahl, Total 3.90 0.16 1 91 �110506329-002CDLJP MW-1SDUP �Nitrogen, Kjeldahl, Total 0.11 mg/L 0.16 40.9 20 MB -062205 ':Phenolics, Total Recoverable < b UgIL i I --IMB-062205 LCS-062205 LCS-062205 Phenolics, Total Recoverable 29.3 ug/L 30 < 5 98 80 120, 0506329-002CMS MW -1 SMS lPhenolics, Total Recoverable 19.6 ug/L 20 < 5 98 75 125:1 j 0506329-002Cdup MWASDUP Phenolics, Total Recoverable ug/L < 5 -fL < 5 j 20 mg/L MBLK-062005 MBLK-062005 Sulfate LCS-062005 LCS-062005 Sulfate 19.3 1 mg/L 20 < 5 96 1-80 J120 0506329-002DMS MW-1SMS Sulfate 73.5 mg/L 50 23.8 100 75 Sulfate 1 24.2 mg/L 3,8 J_ 2. L20 0506329-002DDUP MW-ISDUP N TSL002 W17 • SDG: TSL002 0 is QC SUMMARY REPORT MBLK-061305 MBLK-061305 Total Organic Carbon < 1 mg/L LCS-061305 LCS-061305 `Total Organic Carbon 1 26.6 mg/L 25 1 <1 106 80 120 ---- -- -- - - -- — y 0506329-002AMS MW -!SMS Total Organic Carbon ; 10 mg/L 10 1 < 1 100 � 75 125 ! _ -! i 0506329-002ADUP MW -1 SDUP ITotal Organic Carbon 1.2 mg/L l < 1 200 20 3 TSL002 W 18 Spike Sample Recovery RPDRef %RPD _Sample ID:- Client Sample ID_ Analyte Result Units Amount Result %REC Limits Value %RPD UCL 5 5 ;Total Dissolved Solids < 10 mg/L r - LICS06 4105 L1CS061405 ;Total Dissolved Solids 313 i mg/L 300 < 10 104 80 120 0506329-002dms -- MW -1 SMS !Total Dissolved Solids 549 I mg/L 300 223 109 ! 75 125 0506329-002ddup _- MW -1 SDUP !Total Dissolved Solids 209_ i mg/L _ f — - 6.5 20 223 __ MBLK-061305 MBLK-061305 Total Organic Carbon < 1 mg/L LCS-061305 LCS-061305 `Total Organic Carbon 1 26.6 mg/L 25 1 <1 106 80 120 ---- -- -- - - -- — y 0506329-002AMS MW -!SMS Total Organic Carbon ; 10 mg/L 10 1 < 1 100 � 75 125 ! _ -! i 0506329-002ADUP MW -1 SDUP ITotal Organic Carbon 1.2 mg/L l < 1 200 20 3 TSL002 W 18 U2M "US, INC. • III. RAW DATA • • Analysis Ident Amount TALK High 2 ICV TV=125MG/L 100 6/13/2005 9.91 2.56 128.00 4.44 102.40% 11:17:33 AM TALK High 2 ICB 100 6/13/2005 5.04 0.04 2.00 4.28y�, 11:29:38 AM TALK High 2 0506239-003a 1 6113/2005 5.98 0.94 4700.00 4.44 11:31;50 AM TALK High 2 0506286-003a 1 6/13/2005 5.84 0.57 2875.00 4.42 11:37:24. AM TALK High 2 0506276-003e 50 6/13/2005 6.20 1.00 100.00 4.46 WW -7462-060805- 11:42:06 AM COLLECTION TRENCH TALK High 2 0506276404e 100 6/13/2005 5.96 0.67 33.50 4.48 WW -7462 060805- 11;47:40 AM SY3S71&fWEFFL PENT TALK High 2 0506329-003d 100 6/13/2005 5.99 1.19 59.25 4.44 MW -3D 11:52:25 AM TALK High 2 0506329=004d 100 6/13/2005 5.73 1.24 61.75 4.47 MW -3S 11:57:48"AM TALK High 2 0506329-005d 100 6/13/2005 5.60 0.89 44.25 4.44 MW -4D 12:02:29 PM ja W TALK High 2 0506329-006d 100 6/13/2005 5.92 1.02 51.25 4.45 MW -5D 12:06;4'!; PM TALK High 2 0506329-007d 100 6/13/2005 5.93 1.10 54.75 4.40 MW -5S 12:11:29 PM TALK High 2 0506329=008d 100 6/13/2005 5.68 0.95 47.25 4.45 Qin e 0tv MW -61) 12:1652 PM "a TALK High 2 CCV TV= 125MG/L 100 6/13/2005 10.06 2.55 127.25 4.43 101.80% 12:21:1$ PM TALK High 2 CCB 100 6/13/2005 5.19 0.04 2:00 4.40 12132:15:PM et S- .06= TALK High 2 0506329-009d 100 6/13/2005 5.45 0.59 29.50 4.47 W av MW -6S 12:34:20 PM vJ TALK High 2 0506329-010d 100 6/13/2005 5.70 0.94 47.00 4.46 MW -813 12:38:10 PM TALK High 2 0506329-011d 100 6/13/2005 5.73 0.91 45.50 4.47 MW -8S 11,42:40, PIVI TALK Hight Ifb tv=125mg/f 1`00 6/1 .: Q05 10.12 2.58 12875 437 1.03°Io 12 4�E?M� TALK High 2 Ifbd 100 6/1312,00.5 10.08 2.56 127.75` 4.44 r pd=0:780% 12 58:16 PM TALK High' 2 ccv tv=25mgA 100 611.0.05 10:09 2.55 12fi26'' 4.43 101:80% 1 �M TALK High 2 ccb 100 6/1 015 5.28 0.04 200 4.39 1.19:18 PM c� ozrn z001si �� D• IN�y Pa f1 D6Ao09 4ovf*607 w T • ex 6/oma Analysis Ident Amount TALK low ICV TV=25MG/L 100 6/14/2005 9.91 2.26 0.14 4.19 21.25 85% 11:34:22 AM TALK low ICB 100 6/14/2005 5.60 0.17 0.16 4.16 <1.0 11:46:48 AM. TALK low 0506276-004e 100 6/14/2005 6.05 3.19 0.30 4.15 28.90 WW -7462-060805- 11:51:14 AM SYSTEM EFFLUENT TALK low 050B329 -001d 100 6/14/2005 5.75 0.61 0.18 4.16 4.30 =1 R 11 57:5- AM TALK low 0506329-002d 100 6114/2005 5.39 0.57 0.18 4.16 3.90 MW -IS 12 0415 PM - TALK low 0506329-002dms 100 6MC2005 6.18 3.07 0.19 4.18 28:80 99.60% 00s ", 26mg/l 12k,4; 1? A TALK low 050632"02ddup 100 6/14/2005 5.36 0.58 0.18 4.15 4.05 u e MW -1S 12:17:04 PM: r'% � TALK low 05063,2"05d 50 6/1`4/2005 5.74 2.31 0.22 4.16 41.90 "D 12.22;1`4; PM - TALK low 0506329-008d 50 6/14/2005 5.72 2.24 0.19 4.18 41.00 11tMi-6Q 12.9.8-01, PM TALK IoW 0506329r -009d 100 61/4/2005 5.57 2.73 0:21 4.19 25.25 12 334 PM TALK low 0503629-010d 50 6/14/2005 5.76 2.38 0.18 4.16 44.10 MW -8D 12:39:20 PMr TALK low 0508329-0 1d 50 6'M412005 5.73 2.14 0.20 4.16 38°.80 low S 12`r4SM"'I" 1�M' TALK low CCV TV=25MG/L 100 6/14/2005 9.48 2.58 0.13 4.14 24.50 98% 12:50:41 PM TALK low CCB 100 6/14/2005 5.21 0.09 0.09 4.17 <1.0 1:01:02 PM TALK low 0506329-012d 100 6/14/2005 5.42 0.13 0.09 4.20 <1.0 EQPT-BLANK 1:04:37 PM TALK low 0506232-001 a 100 6/14/2005 6.61 5.03 0.19 4.17 48.40 1:0$:44 PM TALK low 0506232-002a 100 6/14/2005 6.29 2.17 0.18 4.16 19.90 1:17:40 PM TALK low 0506232=003a 100 6/942;005 6.36 1.51 0.15 4.19 1160 TALK low 0506265=001 a 100 6/14/2005 5.42 0.62 0.18 4:14 4.40 1:33:01 PM TALK low 0506275-001 a 50 6/14/2005 6.15 1.02 0.14 4.18 17.60 1:3 ;29 PM TALK low 0505294-001 a 100 6/14/2005 7.04 6.49 0.27 4.11 62.25 1;45:31 PM • Page W 'I.aW9., 0 ZZA Z00'IS.L Analysis Ident Amount .. TALK low 0506298-001 a 100 6/14/20055.84 1.23 0.16 4.18 10.70 1:55:54 PM TALK low 0506298-002a 100 6/14/2005 5.56 0.89 0.17 4.18 7.20 2:02:22 PM TALK low 0506313-001a 100 6/14/2005 5.80 1.08 0.19 4.15 8.95 2:07:48 PM TALK low ccv tv-25mg/I 100 6/14/2005 9.44 2.61 0.15 4.17 24.65 98.60% 2:14:09 PM TALK low ccb 100 6/14/2005 5.33 0.10 0.14 4.17 <1.0 2:25:33 PM TALK low 0506313-002a 100 6/14/2005 5.38 0.41 0.17 4.16 2.45 2:29:32 PM TALK low 0506316-001 a 100 6/14/2005 5.61 0.59 0.18 4:17 4.15 2:34:50 PM TALK low 0506331-001 a 100 6/14/2005 5.55 0.73 0.20 4.19 5.35 2:40:28 PM TALK low 0506345-001 a 100 6/14/2005 6.53 2.22 0.21 4.14 20.10 2:45:35 PM TALK low 0506345-002a 100 6/14/2005 7.06 6.94 0.25 4.17 66.95 2:52:54 PM TALK low 0506345-003a 100 6/14/2005 6.66 3.61 0.19 4.17 34.20 3:02:12 PM TALK low 0506374-001 a 100 6/14/2005 5.38 0.71 0.25 4.14 4.65 3:10:29 PM TALK low 0506374-002a 100 6/14/2005 5.67 0.69 0.20 4.15 4.95 3:15:17 PM TALK low 0506374-003a 100 6/14/2005 6.82 1.05 0.19 4.16 8.65 3:21:03 PM TALK low ccv tv--25mg/l 100 6/14/2005 9.53 2.63 0.17 4.17 24.65 98.60% 3:29:18 PM TALK low ccb 100 6/14/2005 5.44 0.13 0.15 4.16 <1.0 3:41:25 PM 0 Page 0 0 i H2M LABS, INC. BROMIDE • G H Br (mg/L) = 13,320 x A x B_ D x E C F B & E = Normality of Titrant = 0.0075 N DATE: 4m , - ANALYST: A = AsAm E - ABS D = DsAmmE - DBj wtc ABS = 3816 mL DBS = 4,� mL ) S L (�Z LAB # ICV 5. m CLIENT ID MLS USED C & F MLS OF 0.0075N Na2S203 TITRATED FOR DIFFERENCE G - H RESULT MG/L IODIDE + BR IODIDE A�,� Ds,�g ICB c)Sofo ZJ, 2. -,,oz. ,nw -) 3A, 3. 4. �Q� _�L Z• �. JJa..� c� 0.7 � - c'31 W- 3 Z- `l O Z -7 0. 6. - Vv\ 0 - .3 J Z 3, 0000 J -COS �nw- y L.3 0-0�alZ"7� tet; mw - s Z 7 • caa�� i Z ~ .'l io. CCV 5.0 m cca To Z.3 0 oho -5v) -W11 rv1W- S•1 Z.$ .�.�����SJ ).fl 2. 3. 0 �J_;S 3.0 too co•5 4. ,pi2� G�� 1 I.t�n� � .0 J. JJoat�.: �7 <�•� 6. 7. Y t. 9. to. .0 m $.0 Z5 0,0 a 2-3 .o') c0 -S P 0029 ,y. • BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run report Post -run Report Name of Run CL061305 Name of Analysis :cl.ANL Date of Report 6/13/05 System No. :1 Date of Run 6/13/05 Type of System :TRAACS Operator CP Start/Stop time :11:16 - 12:15 Comment Calibr. Fit Quadratic MSL, TSL, DCA Corr. Coeff. MSZ oC 4 , L 90Z 1.0000 Base 69 Channel Type Real Data Channel 2 2 Method Method 2 Dilution Unit mg/1 mq/l Calibr. Fit Quadratic Corr. Coeff. 1.0000 Base 69 Gain 18 Sensitivity 0.5510 Sample Limit 1 Sample Limit 2 � �pyn Pk Cup Sample Id Value Va�[ie�� v\'� �� 0 0 B Baseline -0.016 0 1 1 P Primer 99.434 1 2 1 D Drift 98.431 1 3 1 H1 High 98.308 1 4 0 L1 Low 0.413 1 5 0 Ll Low 0.413 1 6 1 C Cal. 100.085 1 7 2 C Cal. 74.746 1 8 3 C Cal. 50.223 1 9 4 C Cal. 20.075 1 10 5 C Cal. 9.770 1 11 0 C Cal. 0.117 1 12 9 QC3 CRA 2.0 1.707 1 13 10 QC1 LCS 50 50.339 101 /• 1 14 0 QC10MBLK -0.098 <.Z.0 1 15 11 S 0506199-001A 47.653 � ,,'n 1 16 12 S 0506199-002A 132.329 1��/1``�-- 11, 1 17 13 S 0506254-001A 22.392 W 1 ��- 18 14 S 0506256-001A 20.813 1 1 19 15 S 0506256-002A 14.859 1 20 16 S 0506256-003A 11.007 1 21 17 S 0506265-OOIA 6.099 1 BRAN+LUEBBE AACE 5.47 Post -run Report •22 18 S 0506275-OOIA 22.706 1 23 19 S 0506282-OOIA 18.320 1 24 20 S 0506294-001A 33.410 1 25 2 QC1 ccv75 74.756 1007- 1 26 0 QC1 ccb 0.024 < 27 21 S 0506298-001A 5.340 1 28 22 S 0506298-002A 13.472 1 29 23 S 0506307-001A 8.840 1 30 24 S 0506307-002A 32.437 1 31 25 S 0506307-003A 20.944 1 32 26 S 0506307-004A 53.472 1 33 27 S 0506307-005A 57.465 1 34 28 S 0506313-001A 7.360 1 35 29 S 0506313-002A 2.600 1 36 30 S 0506316-001A 7.084 1 37 2 QC1 ccv75 74.951 I0O %, 1 38 0 QC1 ccb -0.101 < Z, 1 39 31 S 0506316-001AMS%r 33.938 to7 j, 1 40 32 S 0506316-001ADUP 6.942 VD 2 % 1 41 33 S 0506331-OOIA 132.597 KXAZtAN^ 1 Over c` mer 42 34 S 0506332-001A 13.781 V 1 c4'rgol?�� 43 35 S 0506333-001A 12.127 1 u 44 36 S 0506279-OO1C 36.961 1 .20lag EC- OW - 7Z- O6o8os 45 37 S 0506329-OO1D K W - IV 74.600 1 •46 38 S 0506329-002D n w - IS 73.640 1 47 39 S 0506329-002DMS1J12 97.604 `��p/, 1 48 40 S 0506329-002DDUP 75.166 Q,QD Z -/.l 49 2 QC1 ccv75 74.981 100% 1 50 0 QC1 ccb 0.349 < Z A 1 51 41 S 0506329-003D rtW.35 6.585 1 52 42 S 0506329-004D OJW-33> 6.576 1 53 43 S 0506329-005D KW - 4D 24.555 1 54 44 S 0506329-006D KW ' 6-l% 23.069 1 55 45 S 0506329-007D flW - Ss 23.312 1 56 46 S 0506329-OOBD KW- rp�10 24.232 1 57 47 S 0506329-009D nW - CS 24.908 1 58 48 S 0506329-010D KW . 81 b 23.652 1 59 49 S 0506329-011D n W - ?$ 24.896 1 60 50 S 0506329-012D EQ 1r% UO)k' -0.183 1 61 2 QC1 ccv75 75.032 1Od /. 1 62 0 QC1 ccb 0.100 L 2 •0 1 63 51 S 0506276-003E 1634.597 100 tjW " 74 CZ - 0GO$OS' GaLLECTION T izEKCj1i Sysl�i�~fFL�%� 64 52 S 0506276-004E 1647.398 100 W 65 2 QC1 ccv75 73.765 4 0 % 1 66 0 QC1 ccb -0.031 <Z-0 1 67 1 D Drift 98.431 1 68 0 B FinalBase -0.016 1 N •BRAN+LUEBBE RACE 5.47 QC Limits Channel QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel Baseline Drift Carry over 8: • ** <END OF REPORT> ** • 2 2 Yes Yes Yes 1.9 Post -run Report BRAN+LUEBBE AACE 5.47 0 Name of run :CL061305.RUN Comment min Channel 2 Method Method 2 Unit mg/l Base 69 Gain 18 Corr. 1.0000 H2M LABS INC. Post -run chart Post -run chart Name of analysis :cl.ANL 2 ------------------ I ------------------ L ------------------------------------ 9 --- ----------------------- ---- ----- - - - - - -- i 8 - ---------- - - -- -' , , - --------------------------------------------- ----- - - - - - ' 10 - - - -------------4---------- - - -- - -- 12 ' ' ' SOB --- ------------- :1P , i2D 14 ------------------------- 3H ' �41, , :5L :6C Page 1 of 4 -0.016 99.434 98.431 98.308 M 0.413 N 0.413 O 100.085 C/1 BRM+LUEBBE AhCE 5.47 Name of run :CL061305.RUN Comment Post -run chart Name of analysis :cl.ANL I , I '7C 74.746 1 I I I � , 1 I 1 18C 50.223 1 I 1 � , 1 I 19C 20.075 18 -------------- 1 --------------- ----------------- ------------------i 1 I 1 '10C 9.770 1 I I 1 �11C 0.117 , i 1 I 1 1 1 I 1 I I 1 ' - -� 12QC3 1.707 20 - - - -------------------------------- '------------ - - - - ------ - - - - -- I 1 i13QC150.339 I 1 I 1 1 114QC1-FD . 098 1 1 1 I , , 1 I � ' 1 1155 47.653 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -1 I 5132.329* 1 ' 1 1 ,175 22.392 1 1 1 '18S 20.813 24 - - - - - - ------- - - - - j - - - - - - - - - - - - - - - -----------------j------------------1 I 1 1 I ' 119S 14.859 1 1 1 �20S 11.007 I I 1 1 �21S 6.099 26 --------- _______J ------------------ L ----------------- 1 _ _ _ _ - _ - _ - _ _ - - - - - _ -I , 1 1 1 1 I 122S 22.706 I I I I 1 1 �23S 18.320 I 1 1 i 1 124S 33.410 28 - - - - - ----------- - -i - - - --- --------- r -- - - - ------ - - - - --------------- - - - - -I , 1 1 �25QC174.756 , I 1 �260C1 0.024 I I 1 1 30 - - - - - - -- ' i27S 5.340 1 1 1 1 '28S 13.472 I I I 1 1 I I 1 i29S 8.840 I 1 1 1 1 1 1 32 ' ' ' '30S 32.437 _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ J _ - _ _ _ _ _ - _ _ _ _ _ _ - L - _ - - - _ _ _ _ _ - - _ _ _ _ _ J _ - _ _ 1 1 1 i 131S 20.944 1 I 1 I 1 32S 53.472 1 I I 1 i I I 1 1 I I 1335 57.465 1 I 1 �34S 7.360 I I 1 Page 2 of 4 BRAN+LVEBBE AACE 5.47 Name of run :CL061305.RUN Comment Post -sun chart Name of analysis :c1 -ANL i 135S 2.600 -----------------,36S 7.089 370C174. 951 :38001--0.101 :39S 33.938 38 -----------------J--------- ------ L ----------------- ------------------ ,905 6.992 i 5132.597* ,52S 6.576 153S 24.555 98 - - - - - - - - - - - - - - - -- ' �54S 23.069 �55S 23.312 1156S 24.232 50 '57S 24.908 - - - - - - - - - - - - - - - - J - - - - - - - - - - - - - - - - L - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 158S 23.652 :59S 24.896 �60S -0.183 52 - - -------- - - - - ---------------------------------------4------------------� :61QC175.032 �62QC1 0.100 Page 3 of 4 i i42S 13.781 40 - - - - - - - - - - - - - - -- ------------------------------------- ------------- - - - - - � :43S 12.127 ' '44S 36.961 i 79.600 42 - - - - - - - - - - - - - - - -- ;- i45S 46S 73.640 i i47S 97.604 X485 75.166 ---------------- J------------------ , L----------- ______1 , 1 '4900174.981 ' �500C1 0.349 i 151S 6.585 46 - - - - - - -- - - - - - - - - -i - - - - - - - - - - - - - - - - - - r- - - - - - - - - - - - - - - --------------- - - - - - I ,52S 6.576 153S 24.555 98 - - - - - - - - - - - - - - - -- ' �54S 23.069 �55S 23.312 1156S 24.232 50 '57S 24.908 - - - - - - - - - - - - - - - - J - - - - - - - - - - - - - - - - L - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - 158S 23.652 :59S 24.896 �60S -0.183 52 - - -------- - - - - ---------------------------------------4------------------� :61QC175.032 �62QC1 0.100 Page 3 of 4 BRAN+LVEBBE AACE 5.47 Name of run :CL061305.RUN Comment Post -run chart Name of analysis :cl.ANL Ir ----------------- -----------------,------------------r---------- --------, :64SI647.398 ' �65QC173.765 �660C1--0.031 56----- ------------ ------------------ '------------------ ------------------� 167D 98.431 ' ',68B -0.016 i -----------------------------------� 69------------------ 4------------------�------------------a------------------� i - ' 68 -----------------I------------------F-- i ---------- ---------------------- i 70 -------- --------'----------- - - - - --------------- - - - - -' -------------------- Page 4 of 4 • Cj BRAN+LOEBBE AACE 5.17 H2M LABS INC. Calibration Curve Calibration Curve Name of run :CL061305.RUN Name of analysis :cl.ANL Comment Channel :2 Method :Method 2 Curve fit :quadratic a= -9.1562E+000 b=9.5695E-009 c=1.7793E-008 Corr. coeff. :1.0000 Peak [%] 100 80 60 90 20 0 0.00 10.00 20.00 30.00 40.00 50.00 60.00 70.00 80.00 90.00 100.00 110.00 Conc. [ mg/l ] Page 1 of 1 tf2A ILAIDS., INC. Mat st Date: Start time: t. COD I M Calibration 1/6/2005 cone abs 0 0 10 0,01 25 0,016 50 0,025 125 0,055 250 0,105 375 0,153 500 0.202 625 0.257 750 0,305 875 0.353 1000 0.404 Intercept (b) -10.742 slope (m) 2501 r 0.9999 COD Calibration 1/05/2005 1100 1000 Y = 500.7x - 10.742 900 800 700 CD 600• cone 500 --Linear (cone) 0 c 400 v 300 200 100 0 -100 42 Absorbance L�Ak Z001SZ 0 Page * 0 • t12M ILAUS, INC. G<iluu,•l Ghloni(� GaF1���l19�'i Ci 106 HARDNESS = B x N x 100,000 A HARDNESS 9�vv DATE: ANALYST: ,DGAoaa j5 i oo,-2 TI -t?. I NM)r. CLIENT ID LAB# MLS USED MLS. MG/L NOTES ' A TITRATED B ICV(1000 mg/1) /0 /l%• ti O ICB 00 e6 -.o Ps lq.;2 y.;2 It, y 2G a5 C-0 Ivo 1. If) -an SU 3. $' /. .s -o I J . ?6 V 3 6. v V V moi(/ J• _ 7 3 Js as . as a. a 8Q 9. 3.J d to 6 3. S70 CCV(1000 mg/1) id t lOt/��. CCB I lJV O v . < . 10 �0 0 ?.9 6fr 4.I. IM 0/0 3-0 s. YS Oji 6. . d /0 3..o f1 v - 10. F V:- CCV(1000 mg/1) 10 10• /OVO CCB loo 0.3 S P 0039 z 9 3�.'- ooS 2.M LAU%. � ■I o �c S� 0 Z NAME: DATE: 3 -C& - 6� 1 t -#ot AMMONIA DISTILLATION . LAB NO. CLIENT ID SAMPLE VOLUME FINAL VOLUME DATE SPIKE SAMPLE WEIGHT ©gS I z9s-.00i Oh S GRAMS mq 16 MLS MLS ,G ANALYZED 1 �e i. S4 Tj I 3z9- oo3d m w - 3 0 3.0 5,10 S. 0 p G, 025 S: 0 S.0 9 3�.'- ooS ►� - krA 3 -C& - 6� 1 t -#ot M I 3 - vile Mx - �S 3t -vr 9" P f I� Its-vol ©gS I z9s-.00i Oh S mq 16 h F h2) ,G 3.0 5,10 S. 0 p G, 025 S: 0 S.0 • BRAN+LUEBBE AACE 5.47 H2M LABS INC. Post -run Report Post -run report Name of Run NH3062205 Name of Analysis :NH3.ANL Date of Report 6/22/05 System No. :1 Date of Run 6/22/05 Type of System :TRAACS Operator CP Start/Stop time :11:24 - 12:03 Comment :#13915 PCTSL i s L ooZ Channel Type Real Data Channel 2 2 Method NH3 Dilution Unit mg/L mg/L Calibr. Fit Linear Corr. Coeff. 0.9988 Base 75 Gain 37 Sensitivity 0.2562 Sample Limit 1 Sample Limit 2 • Value Va e Pk Cup Sample P Id 0 0 B Baseline 0.010 0 1 1 P Primer 2.981 1 2 1 D Drift 3.013 1 3 1 H1 High 3.060 1 4 0 L1 Low 0.081 1 5 0 L1 Low 0.081 1 6 1 C Cal. 3.033 1 7 2 C Cal. 0.898 1 8 3 C Cal. 0.457 1 9 4 C Cal. 0.225 1 10 5 C Cal. 0.124 1 11 0 C Cal. 0.053 1 12 5 QC1 CRA 0.1 0.087 1 13 9 QC4 LCS-13915 1.153 1 14 10 QC10MB-13915 0.073 < 0,1 1 15 11 S 0506329-OO1C 0.094 1 H W — it) 16 12 S 0506329-002C 0.121 1 17 13 S 0506329-002CMS)%f= 5.0 5.572 101 >. 10 18 14 S 0506329-002CDUP 0.113 J> % %. 1 V 19 15 S 0506329-003C 0.109 1 20 16 S 0506329-004C 0.102 1 _ 3S 21 17 S 0506329-005C 4.647 10 — 1 D Post -run Report •BRAN+LUEBBE AACE 5.47 22 18 S 0506329-006C 23 19 S 0506329-007C 24 20 S 0506329-008C 25 2 QC4 CCV 1.0 26 0 QC10CCB 27 21 S 0506329-009C 28 22 S 0506329-010C 29 23 S 0506329-011C 30 24 S 0506329-012C 31 25 S 0506295-001A 32 26 S 0506295-002A 33 27 S LFB-13915 ► V 5 . !) 34 28 S LFBD-13915 35 2 QC4 CCV 1.0 36 0 QC10CCB 37 1 D Drift 38 0 B FinalBase QC Limits CORRECTIONS Channel 4.633 Channel 10 nup - 5b 4.695 QC 1 Cond. 1 45-5 4.092 Limit 1 • — 6 Cond. 2 83,>% 1 Limit 2 0.081 QC 2 Cond. 1 4.292 Limit 1 10 h W Cond. 2 10 Limit 2 3.605 QC 3 Cond. 1 r SS 0.122 Limit 1 1 F Q r) N K 1.409 Cond. 2 1 Limit 2 QC 4 Cond. 1 5.559 111'/. Limit 1 5.533 Cond. 2 0.828 Limit 2 1 QC 5 Unused < O. QC 6 Unused 3.013 QC 7 Unused QC 8 Unused 1 QC 9 Unused QC10 Unused CORRECTIONS Channel 4.633 10 nup - 5b 4.695 10 45-5 4.092 10 — 6 0.827 83,>% 1 0.081 Z-00 1 4.292 10 h W 3.860 10 — $� 3.605 10 r SS 0.122 1 F Q r) N K 1.409 1 15.576 20 5.559 111'/. 10 5.533 e?D 10 0.828 6 3>'. 1 0.083 < O. 1 3.013 1 0.010 1 2 Below 0.080 Above 0.120 Below 0.400 Above 0.600 Below 2.000 Above 3.000 Below 0.800 Above 1.200 2 Post -run Report • BRAN+LUEBBE RACE 5.47 ** <END OF REPORT> ** Baseline Yes Drift Yes Carry over Yes $: 4.6 • 11 Post -run Report N N O E--� BRAN+LUEBBE RACE 5.47 0 Name of run :NH3062205.RUN Comment :#13915 min Channel : 2 Method NH3 r r r r Unit mg/L Base 75 Gain 37 Corr. 0.9988 H2M LABS INC. Post -run chart Post -run chart Name of analysis :NH3.ANL Page 1 of 3 r r r r r r r r i r i r r r i r r r i r r r i r r r i r 2 ------------------ J ------------------ L ----------------- I ------------------ r r i r i r r r r r r r i r r r 9 -- r r r r r r r r -------- - - - - -------------------- ---------------- ---------------- - - - - -' r r r r r r i r r r i r r r r r r r i r r r r r r r r r r r i r r r r r i i r i r i r i r i r 8 - - - r r r r r i r r r r r r - -- - - ------------------ ' -------- -- ------------- - - - - -- - - r r r i r r r r r r r r r r r r r r r i r r r i r r r r r 10 - - - - - - - - - ---4------------------------------------ ------------- - - - - - r r r r r r r i r r r i r r r i r OB i r 0.010 r1P 2.981 12 - - - - - - - - - - - - - - - - - 1 r r 2D r r r 3.013 r r :3H r r 3.060 r i r r r 0.081 19 r91, - - - - -- r r r r 5L r 0.081 r :6C i r 3.033 r r i r ' '7C 0.898 Page 1 of 3 BRAN♦LUEBBE AACE 5.47 Name of run :NH3062205.RUN Comment :#13915 Post -run chart Name of analysis :NH3.ANL 1 1 1 1 �8C 0.457 19C 0.225 I I I 1 1 I I 1 18 - - - - - - - - - - 10C 0.124 �11C 0.053 ' 112QC1 0.087 1 I 1 I 1 , 1 20 - - - - - - - - - - - - - - - -- '------------- L - - - - - - - - - - - - - - - --------------------i13QC4 1.153 I I 1 I 114QC10D.073 1 I i 1 1 1 1 1 :15S 0.094 1 i I I 1 1 , 1 22 - - -------- - - ---- 1 I '16S 0.121 ------------------r-----------------7------------------1 :17S 5.572 18S 0.113 1 I I 1 24i X195 0.109 -------------------------------------------------------------------- I I I I I 1 1 I 120S 0.102 1 I I 1 1215 4.647 I I I 1 26 1 1 ' _ - - _ 22S 4.633 I 1 I 1 1235 4.695 1 I I I i 124S 4.092 1 1 1 1 1 1 28' 125QC4 0.827 ------- - - - - -------------- -- - - -- ---------- - - - - --- - - - - -- �26QC10D.081 1 1 1 1 I I 1 1 127S 4.292 30 -______!_______ ' 1 ,28S 3.860 -------- , -----------,------------------------------------ I 29S 3.605 1 I 1 1 130S 0.122 1 , I 32 - - - - - - - - - - - - -----'--- --- - - - - -L- - - - - - - - - - - - - - - - -------------------,315 1.409 1 1 132S 15.576 1 I I 1 ' 133S 5.559 1 ' ' 34S 5.533 - - - - - - - - - - -4 - - - - - - - - - - - - - - - - - - - - - - 35QC4 0.828 i 1 1 I Page 2 of 3 BRAN-LVEBBE RACE 5.47 Name of run :NH3062205.RUN Comment :#13915 Post -run chart Name of analysis :NH3.ANL 1 I I 136QC100.083 I I 1 1 i 1 1 I ----------------I 37D 3.013 36 ----------------- --------------- I I 1 I 1 I 1 I 1 I 1 I I 1 1 1 I I I 1 I I I I I I I I I 38 --- -------------J ------------------ L ------ ----' 1 I 1 I I I I I 1 1 1 1 1 1 1 1 1 I 1 1 1 I 1 I 38B 0.010 I I I I I I 1 I I I 1 1 1 1 I I 1 I i 1 I I 1 1 I 42 - - - - - 1 I I ----------- - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - i 1 I I I 1 I I I 1 I 1 1 1 1 1 I I 1 I 1 1 1 I 1 1 I I 1 1 ----------------- J ------------------ L ----------------- J ------------------ 46 ____-____46 -----------------i------------------ ----------------- ------------------I I I I I 1 1 I 1 1 I i I 1 1 I I 1 1 I 1 1 I I I 1 1 1 I I I I 1 I I 1 I 96 -------I ------- I I -------I ---------- I I 1 I 1 1 1 1 I I I 1 I I I 1 I 1 I I 1 I I I 1 I I I 1 1 1 1 I 1 1 1 50 -----------------J ----------------- L -----------------J------------------ 52 ---------------- 52 -------------------------------------- ----------------- ------------------I 1 1 1 I i I I 1 1 1 I I I I I 1 I I I I I I I I 1 i I 1 I I I 1 I I 1 1 Page 3 of 3 BRAN+LUEBBE RACE 5.47 • Name of run :NH3062205.RUN Comment :#13915 j H2M LABS INC. Calibration Curve Calibration Curve Name of analysis :NH3-ANL Channel :2 Method :NH3 Curve fit :linear a= -1.9039E-001 b=6.2187E-005 Corr. coeff. :0.9988 Peak [$] 100 80 60 90 O 20 0 0 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 Conc. [ mg/L ] Page 1 of 1 BRAN+LUEBBE RACE 5.47 H2M LABS INC. Post -run report Name of Run no3061105R1 Name of Analysis :NO3.ANL Date of Report . 6/12/05 System No. :1 Date of Run 6/11/05 Type of System :TRAACS Operator PW Start/Stop time :16:34 - 17:28 Comment PCTSL TSf_c�c7Z Channel Type Real Data Channel 1 2 Method NO3 Dilution Unit mg/l mg/l Calibr. Fit Linear Corr. Coeff. 0.9999 Base 85 Gain 12 Sensitivity 0.8622 Sample Limit 1 Sample Limit 2 • Pk Cup Sample Id Value V �%�o Q� 0 0 B Baseline 0.007 0 1 1 P Primer 2.052 1 2 1 D Drift 2.038 1 3 6 H1 High/no2 2.028 1 4 0 Ll Low 0.020 1 5 0 Ll Low 0.020 1 6 1 C Cal. 2.012 1 7 2 C Cal. 0.981 1 8 3 C Cal. 0.491 1 9 4 C Cal. 0.198 1 10 5 C Cal. 0.103 1 11 0 C Cal. 0.009 1 12 5 QC1 cra0.1 0.097 1 13 10 QC1 lcs1.13 1.047 %t, 1 14 0 QC1 mblk 0.003 40.1 1 15 11 S 0506329-OO1C (WMA—I(> 5.439 20 16 12 S 0506329-002C W wJ - IS 5.349 10 17 13 S 0506329-002CMS 1-R.=5.,3 10.347 ,40b 10 18 14 S 0506329-002CDUP 5.412 atci=/_ 10 19 15 S 0506329-003C ^0-3�) 1.065 5 20 16 S 0506329-004C ^0— SS 1.162 5 21 17 S 0506329-005C Mj 3.178 5 • Post -run Report QC Limits Channel BRAN+LUEBBE AACE 5.47 QC 1 Unused QC 2 Unused QC 3 Unused 22 18 S 0506329-006C AW - 5D 3.076 QC 7 5 23 19 S 0506329-007C rA%J- SS 3.104 5 24 20 S 0506329-008C fAVJ - (UP 3.194 5 25 2 QC1 ccvl.0 0.998 pa,/% 1 26 0 QCI ccb 0.009 (0.1 1 27 21 S 0506329-009C IAVJ' (0 s 3.298 5 28 22 S 0506329-010C .-AIJ- $ti 3.187 5 29 23 S 0506329-011C *ArJ- 8 $ 3.206 5 30 24 S 0506329 -012C& - PS btA^ - 0.006 1 31 25 S 0506282-001A 2.470 ftC-N 1 e t;.vr c 32 26 S 0506294-001A 6.504 10 oJe J 33 27 S 0506298-001A 2.101 10 34 28 S 0506298-002A 9.011 10 35 29 S 0506307-001A 0.061 M"r*- 5 JJ&d' Cod. 36 30 S 0506307-002A 7.668 5 37 2 QC1 ccv1.0 0.974 4r X. 1 38 0 QC1 ccb 0.012 L0.1 1 39 31 s 0506307-003A 1.681 5 40 32 S 0506307-004A 2.243 5 41 33 S 0506307-004AMS -T�(1 �^..5 4.755 100% 5 42 34 S 0506307-004ADUP 2.263 5 43 35 S 0506307-005A 1.744 5 44 36 S 0506313-001A 3.284 10 45 37 S 0506313-002A 0.683 Cerul` 10 uj f LG►•C . 38 S 0506316-001A 3.684 5 •46 47 39 s 0506331-OOIA 8.070 10 48 40 S 0506332-001A 4.980 5 49 2 QC1 ccvl.0 0.976 Lit % 1 50 0 QC1 ccb 0.008 [O • 1 1 51 41 S 0506333-001A 6.428 5 52 42 S 0506334-001A 5.060 10 53 43 S LFB-061105 '�=�5 0.496 g1% 1 54 44 .:s LFBD-061105 0.497 �VO 1 55 2 QC1 ccvl.0 0.981 1 56 0 QC1 ccb 0.006 1 57 1 D Drift 2.038 1 58 0 B FinalBase 0.007 1 QC Limits Channel 1 QC 1 Unused QC 2 Unused QC 3 Unused QC 4 Unused QC 5 Unused QC 6 Unused QC 7 Unused Post -run Report 00 N O F-+ CORRECTIONS Channel Baseline Drift Carry over ** <END OF REPORT> ** • • 1 Yes Yes Yes 2.4 Post -run Report BRAN+LUEBBE RACE 5.47 QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel Baseline Drift Carry over ** <END OF REPORT> ** • • 1 Yes Yes Yes 2.4 Post -run Report BRAN+LUEBBE RACE 5.47 Name of run :no306llO5Rl.RUN 40 Comment • • H2M LABS INC. Calibration Curve Calibration Curve Name of analysis :NO3.ANL Channel :1 Method :NO3 Curve fit :linear a= -1.1186E-001 b=3.9201E-005 Corr. coeff. :0.9999 Peak [%] 100 80 60 40 20 0 0.00 0.20 0.40 0.60 0.80 1.00 1.20 1.40 1.60 1.80 2.00 2.20 Conc. [ mg/l ) Page 1 of 1 O N O B"04LUEBBE AACE 5.17 H2M LABS INC. Post -run chart Il , of run :no306llO5Rl.RUN Comment min Channel 1 Method NO3 Unit mg/l Base 85 Gain 12 Corr. : 0.9999 Post -run chert Name of analysis :NO3.ANL 2 ---------------- J ------------------ L ----------------- j------------------� 4 ---------------- -+--- --------- - - - - --------------------------------- -- - - - � ---------- - - - - --- - = - - -- ----------------- 6 -------------- -- j - - - - - - - - - - - - - - - - ------------------- j - - - - - - - - - - - - - -- - - - � 10 ----------------4----------------------------------- I - - - - - - - - - - - - - - - -- - � 12 ---------------------------------- 1-----------------� 14 ---------- - - - - -------------- - - - - ------------- - - - - ------------ --- - - - - - � SOB 'IP i2D Page 1 of 4 r4 0.007 2.052 N 2.038 F"4 BRAN+LUEBBE AACE 5.47 Name of run :no3061105Rl.RUN Comment Poet -run chart Name of analysis :NO3.ANL 30 - - - - - - - - I- -- - - - - - - - - - - - - - I - - -- - - - - - - - - - - - - - - - - - - - - -I :24S 3.194 1 , I , 1 , 25OC1 0.998 , , I 26OC1 0.009 32 - - - - - - - - - - - -------------- - - - - -------------------'------------- - - - - - ' '27S 3.298 � I 1 128S 3.187 , I I I I I 1 X295 3.206 It1 - - - - - - - - - - - - - - - - - - - - ti - - - - - - - - - - - - - - - - - - r ------------------ 1 I , I 1305 0.006 I 1 I Page 2 of 4 , 13H 2.028 1 ' I , , I :4L 0.020 I 1 15L 0.020 I I 1 1 18 ---------------------------------- 1 I I I � ,6C 2.012 1 1 I I 1 17C 0.981 I , , I I 1 I 18C 0.491 20 -----------------------------------L-------------------4------------------' 1 19C 0.198 I 1 1 1 I 10 0.103 I I 1 1 11C 0.009 1 , , 1 -- --- ----- - - - - -- ---------- - - - - ------- - - - - -- 1 r 1 ' 112QC1 0.097 I 1 1 1 , 1 I 113QC1 1.047 1 1 1 I , 1 114QC1 0.003 29 ------- -------- ------------------ ----------------- 2------------------� 1155 5.439 1 I I I 1 - ' 116S 5.349 , 1 1 17S 10.347 26 ----------------- ---------- --------`------------------ J------------------' 1 ' ' '18S 5.412 I I I 1195 1.065 �20S 1.162 I 1 i 1 1 1215 3.178 I , X225 3.076 1 , 1 I , I I I I 1235 3.104 I , , 30 - - - - - - - - I- -- - - - - - - - - - - - - - I - - -- - - - - - - - - - - - - - - - - - - - - -I :24S 3.194 1 , I , 1 , 25OC1 0.998 , , I 26OC1 0.009 32 - - - - - - - - - - - -------------- - - - - -------------------'------------- - - - - - ' '27S 3.298 � I 1 128S 3.187 , I I I I I 1 X295 3.206 It1 - - - - - - - - - - - - - - - - - - - - ti - - - - - - - - - - - - - - - - - - r ------------------ 1 I , I 1305 0.006 I 1 I Page 2 of 4 BRAN+LUEBBE AACE 5.47 Name of run :no3061105R1.RUN Comment Post -run chart Name of analysis :NO3.ANL Page 3 of 4 ' '32S 6.504 36 --------- -------;----------------------------------- ;------------------� 33S 2.101 ' �34S 9.011 ,35S 0.061 38 ----------------- ------ --L------------------------------------' :36S 7.668 i i �37QC1 0.974 138QC1 0.012 i '39S 1.681 ,40S 2.243 '41S 4.755 - i ,42S 2.263 '43S 1.744 144S 3.284 _____----------- J------------------ L ----------------- J ------------------ 1 :45S 0.683 1 1 ' 146S 3.684 1 1 47S 8.070 i 148S 4.980 �490C1 0.976 ' 'SOQC1 0.008 98 ----------------- - - - - - -� ----------------------- i i 51 6.428 :52S 5.060 �53S 0.496 50 ------------ --- J ------------------ ' ------------------ J------------------' ' �54S 0.497 ' 1550C1 0.981 560C1 0.006 52 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - -- ------------------- - - - - -' '57D 2.038 Page 3 of 4 BRAN+LVEBBE AKE 5.17 Name of run :no306llO5Rl.RUN Comment Post -run chart Name of analysis :NO3.ANL ------- ----- - - - - -- - -- wr -------------�------------------ ---------- r--------- I 56 - - - - - - - - - - - - - - - -------------------- L - - - - - - - - - - - - - - - --------------- - - - - - � i I I I I I I I 1 I I I I I I I I 1 1 58 - - - - - - - - - - - - - - - --------------------1------------------------------- - - - - -I i I i I I I I 1 I I 1 I 1 1 I I 1 I 1 1 I I 1 1 I 1 I I I I , I I 1 1 I 1 1 1 I I I I 1 1 I 1 62 -- - - - - - - - - - - -- -- - -- --- ----------- - - - - - ' I 1 ' 1 I I i 1 I 1 1 I 1 1 1 I 1 I 1 I I 1 I 69 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ----------- -- - - - - --------------- - - - - - I r I I I I I I 1 I 1 1 1 I 1 I 1 I I I 1 1 1 I 1 1 1 i I I 1 r r r r I I r 1 I I I I I 1 1 I 68 ----------- - - - - -------------- - - - - ------------- - - - - --------------- - - - - - ' 1 r I r I I I 1 1 I I I I I 1 1 70 - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - - ------------------- ---- - - - - -- - - - - - ' I 1 I I 1 I I I 1 1 I I 1 I I 1 I I I 1 1 1 I 1 1 1 1 1 1 I Page 4 of 4 U2M TAUS, 1 N Ce Phenols Method 420.1 Distillation Date: b--;2-0 Time:- -k. U_ Pc r 5� 00Z Analyst:d/ Date: -4-22 'O ../f/ 0 Ph* P 000 Moroi Wn ■ -929 .-_- � �� ■■c�ra��■■��� � - � � �■mac®i���� 0 Ph* P 000 Calibration 1.2405 conc 0 abs 0.000 5 0.01 10 0.022 20 0.048 30 0.072 40 0.099 50 0.122 Intercept (b) 0.6708 slope (m) 402.96 r 0.9997 Phenol Calibration 1/24/05 60- 50- -Y;--,402.96x + 0.6708 40 3 ♦ conc 30 – —Linear (conc) 0 v 20- 10- 0 10 - 0 4 /00or 0.000 0.050 0.100 0.150 Absorbance gg,AA ZOOJSJ 0 Page 0 • 1 J 1 I 1 1 1 1 SULFATE Pe T51 002- DATE: ANALYST: N• ; 7.1 w MY rVAI/I CLIENT ID LAB# MLS USED ABS. MUL (GRAPID MG/L NOTES ICV (20:0 mg/I,) ,t.f o. ,2 8 /� 3 96• •�' ICB •I.f o • o0 0 .t S: o 1r11C - oSv S -oat S_ 6.36 V kit -IS - 00110 to #./o .ix ISL_ x - oa to 10.391- 19• Y a JG S ApJf. Y• ug- 903,E jr o.mr,/ . CCv(20.0 mg/L) j S 0.2yr (9.3 96 •-�'. CCB �r- wAk- •sosu - 00 o.19fl �S 2 me, -r 3 - •o 0-116, t9•P - Shp- vv 1 X0.2 G 2_ 10 • �- 6A is,Y Ccv(Zo.o.) J.3 o. z Yp , 3 96 , ,� • cm d 3l- o • o00 .c,t: o v.- eSob - Von to o. 13( yr3 Mf- VIOD s O.t6o M•r ay -Ss I 5u -,Ifo hr 13sr_ /f Q rT 51,9-visto x r. 0 OS $Is - oo( a. oo Q • s'. 0 CCv(20.0 mg1L) s� o. i Y p / y. 3 9 6• f_ CCB V ootk If p• 19 Wl 33.t- v - 0. o.) S; 3 1-'e P. orz o 571- py-r � 6.o0P 0 3?1 •ooh - 0.007- v Ccs rVAI/I Calibration 05/06/05 conc abs 0 0.000 5 0.04 10 0.112 15 0.167 20 0.236 25 0.326 30 0.412 35 0.49 40 0.542 Intercept (b) 2.0043 slope (m) 69.66 torr. Coeff. 0.9966 89A Z00'ISZ SO4 05/06/05 y = 69.661 x + 2.0043 40 30 E 20 ♦ ♦ conc —Linear (cone) 0 v ♦ 10- 0 0.000 0.100 0.200 0.300 0.400 0.500 0.600 Absorbance Pag* 2 0 mWjvj6-j Wj u u u W SOLIDS (ipded VVt.(a) - Taro wt_ (a)WO00IM000 / SS/ TS Sollda(mgA)m mL Sample ANALYST: TEMP. CC/9Q C-, r�6wv m O ©'� �f s L- c-)� • • A DRIED SOLIDm IN OM40 ma w ® + • ��� + af• %. "IF29 mew mus, �%lmm i 1 >� r mmmmmm J a •o m ®mm• ,W.• ,MCINIM0101110110110 KIM + ' • �. 1.MEKIM ME mimm- On" '"'ame, M=dp mmmmJAPEm mmmmmm • • A if�..i �...► &n.� l...: L•J u u ir�...� 4"'j MW 09� Z00'IS,I,, OLIDS lfQfied Mal - Taro M. 1011x10001MOOO D / SS/ TS Solid{s(�mg//I)■ mL Sample ANALYST:•-1'�� 1 ' ► TEMP. DATE! te) 11-41 U< START---------WUMIDmr. 0 • 0 TARE RESULT W1,;j14 - M -ox's NJ=- �-q E ��. r��� • �� a' �'+ •, �r pie ®® I1wo''Mum IM16"-sb woSAM wiltomz, MEMINNIMINIM 11MIM106smiomm �Lwv : mo `o _, r MMMMMM-- 0 • 0 ..�.r ....r �r ara>•r �a1 Now `A Lel L—A SOLIDS 19Ak ZOO'ISi--j [(Dried MA) - Taro Wt. (a))'x100oN1000 J�o / SS/ TS Solids(mgA)= mL Sample TEMP. DRIED TARE I LAB # i CLIENT ID I CRUC I sAMLI E I WT (GI WEIGHT WEIGHT IG1 WEIGHTD(G1 I RESULT DRIED JIGNITED VOL. VOLATILE NL WT (G) WT (G) WT (G) RES. (Mt; &) 0 0 & 10-AN-1,Iffim—=;�—�.u�'+vti����a ma* "6,. as w*e "6wMo 110 "o M*S. Moo. MMMMMIEmil liarroammm-0 Mo MIMM mmmF,m. F. - "'Lme lmiaM-z I mummmmm 0 0 & NAM sbolt IH28t LAUS, INC.* P'sb °° Z sp1- r 1 DATE: 6-11 - V TOTAL �/TRN DIGESTIONS 7'p 4 4 P 0045 I F12M LABS, IN, A ag. �9 30 X, 32 33 3y 140 Ilm C M 00 2, bNb1979 TOTAL WI6'S/TKN DIGESTIONS NAME. AllrimM DATE • 6 -11 -p urtkl LAB NO. CLIENT ID SAMPLE WEIGHT GRAMS SAMPLE VOLUME MLS FINAL VOLUME MLS DATE ANALYZED SPIKE -orr - S 'vj o o f toth OL4 I r woo PA -§k I ( -mtk S.t" k 6 0-1 -ce th JO 3- o0 vil- 00 R5PI 3�s-ar 1�ox �•S b F bA �s� `�• P 004t; j SL OOZ 13N]-Sg/B Concentration listed after Optical Blank Correction. TKNData Preparation dilution factor not applied to results. AMA SamplelD SampTy Conc Units DF Conc x DF AnalDate AnalTime TestCod ME I Primer PRIM 2.999 mg/1 1 2.999 6/23/05 01:06:47 PM tkn_W 2 Drift DRIF 3.014 mg/l 1 3.014 6/23/05 01:07:27 PM tkn_W 3 High HIGH 3.032 mgA 1 3.032 6/23/05 01:08:07 PM tkn_W 4 Low LOW 0.034 mg/1 1 0.034 6/23/05 01:08:47 PM tkn_W 5 Low LOW 0.034 mg/l 1 -0.0341623/05 01:09:27 PM tkn W 6 Cal. CALB 3.015 mg/l 1 3.OI5 6/23/05 01:10:08 PM tkn_W 7 Cal. CAM 0.964 mgA 1 0.964 6/23/05 01:10:47 PM tkn_W 8 Cal. CALB 0.475 mgA 1 0.475 6/23/05 01:11:28 PM tkn_W 9 Cal. CAM 0.198 mg/l 1 0.198 6/23/05 01:12:07 PM tkn_W 10 Cal. CALB 0.102 mgA I 0.102 6/23/05 01:12:47 PM tkn_W I I Cal. CAM 0.026 mgA I 0.026 6/23/05 01:13:30 PM tkn_W 12 optical bink QUAL 0.777 mg/l 1 0.777 6/23/05 01: 14:08 PM tkn_W 13 Ics-13925 1cs �%_ 11.) 0.4113 mg/l 10 4.113 6/23/05 190 /- 01:14:48 PM tkn_W 14 mb-13925 mblk 0.003 mg/l 1 0.003 6/23/05 C0.1 01:15:28 PM tkn_W • 15 mdl l SAMP 0.225 mgA 1 0.225 6/23/05 01:16:09 PM tkn_W 16 mdl2 SAMP 0.22 mgA I 0.22 6/23/05 Ol :16:48 PM tkn_W 17 mdl3 SAMP 0.271 mg/l 1 0.271 6/23/05 01:17:28 PM tkn_W 18 mdl4 SAMP 0.234 mg/I I 0.234 6/23/05 Ol :18:09 PM tkn_W 19 mdl5 SAMP 0.281 mgA I 0.281 6/23/05 Ol :18:48 PM tkn_W 20 md16 SAMP 0.265 mg/l 1 0.265 6/23/05 01:19:28 PM tkn_W 21 mdl7 SAMP 0.396 mg/l 1 0.396 6/23/05 01:20:08 PM tkn_W 22 std 0.1025 SAMP 0.154 mgA I O.I54 6/23/05 1 S'ei 01:20:48 PM tkn_W 23 known#525 SAMP 1.1188 mg/l 10 11.188 6/23/05 01:21:28 PM tkn_W 24 known#525dup DUP 1.1181 mg/l 10 , 11.181 6/23/05 LID OX 01:22:08 PM tkn_W 25 ccvL0 CCv 0.969 mg/l 1 0.969 6/23/05 '97%. 01:22:49PM tkn_W 26 ccb CCB 0.031 mg/l 10 0 13 6/23/05 < D-1 01:23:27 PM tkn_W 27 0506183-009a SAMP 2.3386 mgA 10 23.386 623/05 01:24:09 PM tkn_W 28 0506183-009aMS ms 1 1!_ ,' 2.7968 mg/l 101 27.968 6/23/05 12 % . 01:24:48 PM tkn_W 29 0506183-009aDUP dup 2.4975 mg/l 10 24.975 6/23/05Q 17 % % 01:25:28 PM tkn_W 30 0506329-001 C 1K W - 1 SAMP 0.288 mg/l I i �- 0.288 623/05 01:26:08 PM tkn_W 0/2005 2:01:37 PM Page I of 3 Peak SamplelD SampTy Cone Units DF Cone x DF AnalDate AnalTime TestCod is 31 0506329-002C n W - 15 SAMP 0.162 mg/l 1 I 0.162 6/23/05 01:26:48 PM tkn_W 32 0506329-002CMS ms j V= ,' 0.3901 mg/1 10 3.901 6/23/05 % 01:27:29 PM tkn_W 33 0506329-002CDUP dup 0.107 mg/l 1 0.107 6/23/05 V D 0.4/,01:28:08 PM tkn_W 34 0506329-003C M W - 3) SAMP 0.259 mg/l 1 0.259 6/23/05 01:28:48 PM tkn_W 35 0506329-004C P 1 W - 35 SAMP 0.318 mg/1 I 0.318 6/23/05 01:29:28 PM tkn_W 36 0506329-005C M W J SAMP 0.4171 mg/l 10 4.171 6/23/05 01:30:08 PM tkn_W 37 ccv 1.0 ccv 0.961 mg/I 1 O.9611 6/23/05 �� 01:30:49 PM tkn_W 38 ccb ccb 0.026 mg/l 1 0.026) 6/23/05 ZO 11 01:31:27 PM tkn_W 39 0506329-006C V�1 - !� SAMP 0.3939 mg/l 101 3.939 6/23/05 01:32:09 PM tkn_W 40 0506329-007C f1 W ' 575 SAMP 0.374 mg/l 10 3.74 6/23/05 01:32:48 PM tkn_W 41 0506329-008C MW - 01 SAMP 0.468 mg/I 10 4.68 6/23/05 01:33:28 PM tkn_W 42 0506329-009C M W - 6 S SAMP 0.3609 mg/l 10 3.609 6/23/05 01:34:08 PM tkn_W 43 0506329-OI OC M W - g:I� SAMP 0.3124 mg/I 10 3.124 6/23/05 01:34:48 PM tkn_W - S 44 0506329-011C /-1W- SAMP 0.321 mg/I 10 3.2 6/23/05 F 01:35:29 PM tkn_W 45 0506329-012C E Q?I +3LA N K SAMP 0.16 mg/l 1 0.16 6/23/05 01:36:08 PM tkn_W 46 0506370-001 B .P t 326 - 00 1 SAMP 0.209 mg/1 1 0.209 6/23/05 01:36:48 PM tkn_W • 47 0506370-001BMSms 1 V= .' 0.3814 mg/l 10 1 3.814 6/23/05 ��/, 01:37:27 PM tkn_W 48 0506370-OOIBDUP dup 0.21 mg/1 10.21 6/23/05 v/ 01:38:08 PM tkn-W 49 ccvLO ccv 0.957 mg/1 1 ' 0.957 6/23/05 6 / 01:38:49 PM tkn_W 50 ccb ccb 0.026 mg/1 1 (( 6/23/05 /D.( 01:39:27 PM tkn_W 51 0506486-001 B 090.7 0-0% SAMP 0.262 mg/l I 1 0262 6/23/05 01:40:08 PM tkn_W 52 0506270-002A SAMP 0.2234 mg/l 10 2.234i 6/23/05 01:40:46 PM tkn_W 53 0506602-001B- 013 ` 001 SAMP 0.528 mg/l 1 1 0.5281 6/23/05 01:41:28 PM tkn_W 54 0506482-OOIA SAMP 1.039 mg/l 1 1.039 6!23/05 01:42:09 PM tkn_W 55 0506482-002A SAMP 0.2858 mg/l 10 2.858 6/23/05 01:42:47 PM tkn_W 56 0506375-OOIA SAMP 0.30248 mg/1 50 15.124 6/23/05 01:43:27 PM tkn_W 57 LFB-13925 Ifb I V-rn. 0.3948 mg/I 10 3.948 6/23/05 01:44:08 PM tkn_W 58 LFBD-13925 Ifbd 0.3658 mg/I 10 3.658 6/23/05 Q Qq 8/. 01:44:48 PM tkn-W 59 ccvl.0 ccv 0.954 mg/1 1 r- 0.9541 6/23/05 J S �, 01:45:28 PM tkn_W 60 ccb ccb 0.023 mg/l 1 ! 0.0231, 6/23/05 4(0.1 01:46:07 PM tkn_W 61 Drift DItIF 3.014 mg/1 I i_ 3.014 6/23/05 01:46:48 PM tkn_W N /2005 2:01:37 PM _ Page 2 of 3 O E-� Peak SampleID SampTy Conc Units DF Conc z DF AnalDate AnalTime TestCod 062 End • END 0.02 mg/1 1 0.02 6/23/05 01:48:19 PM tkn_W 005 2:01:37 PM Page 3 of 3 BRAN+LUEBBE AACE 5.47 0 Name of Run TKN062305 Date of Report 6/23/05 Date of Run 6/23/05 Operator CP Comment MDL,TSL,BNLS,MDR prof H2M LABS INC. Post -run report Name of Analysis :tkn.ANL System No. :1 Type of System :TRAACS Start/Stop time :12:55 - 13:48 Channel Type Real Data Channel 2 2 Method tkn Dilution Unit mg/l Calibr. Fit Linear Corr. Coeff. 0.9998 Base 78 Gain 22 Sensitivity 0.3889 Sample Limit 1 Sample Limit 2 • Pk Cup Sample Id Value Value 0 0 B Baseline 0.020 0 1 1 P Primer 2.999 1 2 1 D Drift 3.014 1 3 1 H1 High 3.032 1 4 0 L1 Low 0.034 1 5 0 Ll Low 0.034 1 6 1 C Cal. 3.015 1 7 2 C Cal. 0.964 1 8 3 C Cal. 0.475 1 9 4 C Cal. 0.198 1 10 5 C Cal. 0.102 1 11 0 C Cal. 0.026 1 12 8 QC1 optical bink 0.777 1 13 9 QC1 lcs 4.1 4.890 10 14 10 QC1 mblk 0.780 1 15 11 S mdll 1.002 1 16 12 S mdl2 0.997 1 17 13 S md13 1.048 1 18 14 S mdl4 1.011 1 19 15 S md15 1.058 1 20 16 S mdl6 1.042 1 • 21 17 S md17 1.173 1 Post -run Report QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused Post -run Report 00 N BRAN+LUEBBE AACE 5.47 22 18 S std 0.1025 0.931 1 23 19 S known#525 11.965 10 24 20 S known#525dup 11.958 10 25 2 QC1 ccvl.0 0.969 1 26 0 QC1 ccb 0.031 1 27 21 S 0506183-009a 24.163 10 28 22 S 0506183-009aMS 28.745 10 29 23 S 0506183-009aDUP 25.752 10 30 24 S 0506329-001C 1.065 1 31 25 S 0506329-002C 0.939 1 32 26 S 0506329-002CMS 4.678 10 33 27 S 0506329-002CDUP 0.884 1 34 28 S 0506329-003C 1.036 1 35 29 S 0506329-004C 1.095 1 36 30 S 0506329-OOSC 4.948 10 37 2 QC1 ccvl.0 0.961 1 38 0 QC1 ccb 0.026 1 39 31 S 0506329-006C 4.716 10 40 32 S 0506329-007C 4.517 10 41 33 S 0506329-OOBC 5.457 10 42 34 S 0506329-009C 4.386 10 43 35 S 0506329-010C 3.901 10 44 36 S 0506329-011C 3.987 10 45 37 S 0506329-012C 0.937 1 •46 38 S 0506370-OOIB 0.986 1 47 39 S 0506370-OOIBMS 4.591 10 48 40 S 0506370-OOIBDUP 0.987 1 49 2 QC1 ccvl.0 0.957 1 50 0 QC1 ccb 0.026 1 51 41 S 0506486-001B 1.039 1 52 42 S 0506270-002A 3.011 10 53 43 S 0506602-001B 1.305 1 54 44 S 0506482-001A 1.816 1 55 45 5 0506482-002A 3.635 10 56 46 S 0506375-OOIA 15.901 50 57 47 S LFB-13925 4.725 10 58 48 S LFBD-13925 4.435 10 59 2 QC1 ccv1.0 0.954 1 60 0 QC1 ccb 0.023 1 61 1 D Drift 3.014 1 62 0 B FinalBase 0.020 1 QC Limits Channel 2 QC 1 Unused QC 2 Unused QC 3 Unused Post -run Report 00 N CORRECTIONS Channel BRAN+LUEBBE AACE 5.97 Baseline QC 4 Unused Yes QC 5 Unused %: QC 6 Unused QC 7 Unused QC 8 Unused QC 9 Unused QC10 Unused CORRECTIONS Channel 2 Baseline Yes Drift Yes Carry over Yes %: 1.3 .. <END OF REPORT> — • • Post -run Report N O H BRAN+LUEBBE RACE 5.47 • Name of run :TKN062305.RUN Comment min Channel 2 r Method tkn Unit mg/l � ' Base 78 r Gain 22 -- Corr. 0.9998 H2M LABS INC. Post -run chart Post -run chart Name of analysis :tkn.ANL Page 1 of 4 0.020 2.999 3.014 3.032 0.034 0.034 r3 N 3.015 C) 0.964 r r ' r r r r ' r � ' r i r r � � � 2 -- r r ir ---------------J-------------------'-------------- � ----j---------------- � -- r r r i r r r r 4 ------------------I ------------------ r ----------------- i r ------------------ i ' r ----------------- r r i r i r i ' r r 8------------------ r r -'------------------ '------------------ r r i r i r -'-----------------' r r r i i r r i i r r r r i r i r r r r r r r i r r 10 ------------------ ----------------------------------- ------------------' OB r r ' r ' lip i r r r r2D , r i � r 3H r x41, 14-- ---------------'- -----------------'-----------------I------------------' - i r 51, r , r 16C r r � r :7C Page 1 of 4 0.020 2.999 3.014 3.032 0.034 0.034 r3 N 3.015 C) 0.964 BRAN-LUEBBE AACE 5.47 Post -run chert Name of run :TKN062305.RUN Name of analysis :tkn.ANL Comment Page 2 of 4 BRAN+LUEBBE AACE 5.47 Name of run :TKN062305.RUN Comment Post -run chert Name of analysis :tkn.ANL 365 4.948 1 ' ' 137QC1 0.961 1 36 -- - ----- ' --------;------------------ - - - - - - - - - - , - - - - - - - - - - - - ,- - - - - - - - - - I ;38QC1 0.026 , , 1 �39S 4.716 I I ' 1905 9.517 38 --------------- J - - - - - - - - - - - - - - - - - - L - - - - - - -----------'------------- - - - - - ' 1 1 ' :415 5.457 , , I I 1 142S 4.386 1 1 I 1 1 I I I I I 1 ' ' :43S 3.901 I 1 I ' '44S 3.987 ' 455 0.937 I � '46S 0.986 I 42 - - - - - - - - - - - - - -, - - - - - - - - - - - - - - - - - - r - - - - - - - - - - - - - - - - - ; - - - - - - - - - - - - - - - - - -, ;47S 4.591 I I I 1 1 1 '48S 0.987 , I 1 I I • , I 199QC1 0.957 _ _ _ - - - _ _ _ - _ _ _ J _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ L - _ _ _ - _ _ _ - _ _ _ _ _ _ _ _ J - _ _ - _ _ _ _ _ _ _ _ _ - _ - _ _1 1 I ' :500C1 0.026 , 1 I 1 151S 1.039 I I 1 ' X525 3.011 I 1 46 ---- -----------+------------------1----------------- ------------------ y I I I 1 1 153S 1.305 1 I I 1 1595 1.816 , , I I I I 1 155S 3.635 I 1 I 1 I 1565 15.901 1 I I I '57S 4.725 I I 1 I I 1 I 1 I 1 1585 4.435 50 - - - -- --- - - - - -'-----------------'------------------ J - - - - - - - - - - - - - - - - - - ' ' ;59QC1 0.954 1 160QC1 0.023 1 I ,61D 3.014 52 - - - - -- - ------- - - - -- ------------------------------ 1 I I 1 ;62B 0.020 I I I 1 Page 3 of 4 Post -run chert BRAN+LUEBBE AACE 5.47 Name of run :TKN062305.RUN Name of analysis :tkn.ANL ('nmmonY Page 4 of 4 BRAN+LUEBBE AACE 5.47 • Name of run Comment • H2M LABS INC. Calibration Curve TKN062305.RUN Calibration Curve Name of analysis :tkn.ANL Page 1 of 1 Sample Results Report Print Date/Time: 605'/06/74 8:46:14 Sample ID Result Std. Dev. RSD Mode ALT --------------------- I 0.3047 0.0139 4.58 UTILITY C IO:."Zy 26.5585 0.8535 3.21 TOC CBO 4,,6 0.7201 0.1594 22.14 TOC RI ............................. 11S.DY- 1.1549... 0.1640.. 14.20 ... TOC .. BLK�11� cLO 0.2001 0.0533 26.64 TOC 506276-003B C011ca-VIX"Wv% 2.0962 0.3595 17.15 TOC 506276-004B.44'5*n.V.Y ............4/00.6383... 0.1649.. 25.84 ... TOC .. 506329-001A MW-1p� 0.8899 0.1271 14.29 TOC 506329-002A Mu '15 0.7812 0.1928 24.68 TOC 506329-002AMS. .......... cn-VC 9.9798... 2.3285.. 23.33 ... TOC .. 506329-002ADU RPO% ZcO'` 1.1517 0.0732 6.35 TOC 506329-003A MW -fO 6.7013 0.7452 11.12 TOC 506329-004A.Mw:31 ................. 6.1437... 0.4267.. 6.94 ... TOC .. 506329-005A MW -y0 3.7472 0.3508 9.36 TOC 506329-006A hW'50 4.3503 0.8188 18.82 TOC CV -.Y! zSPPW .................. 27.3498... 0.7328.. 2.68 ... TOC .. CB c/.0 0.6606 0.1314 19.88 TOC 506329-007A AW -SS 4.4622 0.4262 9.55 TOC 506329-008A.M1ip................. 3.4742... 0.4578.. 13.18...TOC .. 506329-009A NW- S 3.6323 0.1530 4.21 TOC 506329-010A MW"10 3.8792 0.6984 18.00 TOC 506329-011A.fAW-S5 3.3508... 0.3649.. 10.89...TOC .. ................. 506329-012A EAP gM� cl-0 0.3963 0.0805 20.31 TOC FB '1'v,-Pf r p� fit.= 9(.Sx 9.6518 0.4242 4.40 TOC FBD'T:' Off1`.............eP� :..t:13'�.. 9.8599... 0.1020.. 1.03 ... TOC . . Cv '1V%'LSP pr" lO7,yx 26.8536 0.1701 0.63 TOC CB 0.4786 0.0499 10.43 TOC • Dcw(-a TSL 001 0 N O F-, Sample Results Report Print Date/Time: 2005/06/14 8:46:14 Method ID Sample Type :leaning Procedure Sample s 10 STE WATER Sample 'OIWSTE WATER Sample 'OC WASTE WATER ...Sample .. 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample .. 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample .. 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample ._ 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample .. 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample .. 'OC WASTE WATER Sample 'OC WASTE WATER Sample 'OC WASTE WATER ...Sample .. OC WASTE WATER Sample OC WASTE WATER Sample OC WASTE WATER ...Sample .. OC WASTE WATER Sample OC WASTE WATER Sample r L J Vial Timestamp Message p 2005/06/13 16:28 Low Sample Detect 1 2005/06/13 17:01 2 2005/06/13 17:31 Low Sample Detect 3..2005/06/13 18:00 ..Low Sample Detect 4 2005/06/13 18:30 Low Sample Detect 5 2005/06/13 18:59 Low Sample Detect 6..2005/06/13 19:29 ..Low Sample Detect 7 2005/06/13 19:59 Low Sample Detect 8 2005/06/13 20:28 Low Sample Detect 9..2005/06/13 20:57 .. Sample Detect 10 2005/06/13 21:26 Low Sample Detect 11 2005/06/13 21:54 12..2005/06/13 22:22 .. 13 2005/06/13 22:50 14 2005/06/13 23:18 15..2005/06/13 23:44 .. 16 2005/06/14 00:17 Low Sample Detect 17 2005/06/14 00:45 18..2005/06/14 01:13 ..Low Sample Detect 19 2005/06/14 01:42 Low Sample Detect 20 2005/06/14 02:11 Low Sample Detect 21..2005/06/14 02:39 ..Low Sample Detect 22 2005/06/14 03:05 Low Sample Detect 23 2005/06/14 03:37 24..2005/06/14 04:05 .. 25 2005/06/14 04:34 26 2005/06/14 05:04 Low Sample Detect N O F-, ample ID: CRI ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 Aerator ID: JASON SAMUEL e0 ppm C ug C Raw Data Mode: TOC Filename: 06131608 Timestamp: 2005/06/13 18:00 Sample Type: Sample Beginning Ending Integration Detailed Analysis Report Print Date/Time: 2005/06/14 8:46:16 ;ample ID: DI Mode: UTILITY fethod: Cleaning Procedure Filename: 06131608 aurve: TOC WW CURVE 42805 Timestamp: 2005/06/13 16:28 )poor ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2946 0.1473 36927 9.898 10.095 129 2 0.2955 0.1477 37017 9.908 10.107 129 3 0.3041 0.1520 37879 9.912 10.109 130 4 0.3246 0.1623 39937 9.933 10.132 130 ----------------------------------------------------------------------------- x< Statistics>>> Mean: 0.3047 Std Dev: 0.0139 RSD: 4.58 ;ample ID: LCS Mode: TOC fethod: TOC WASTE WATER Filename: 06131608 'al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 17:01 operator ID: JASON SAMUEL Sample Type: Sample .ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 27.4095 1.3705 282040 10.133 11.129 116 2 25.5727 1.2786 263636 10.210 11.200 114 3 27.1161 1.3558 279100 10.219 11.207 116 4 26.1358 1.3068 269278 10.196 11.191 116 ---------------------------------------------------------------------------- < tistics>>> - Mean: 26.5585 Std - Dev: 0.8535 - -------------------------- RSD: 3.21 ample ID: ICB Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 17:31 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.9114 0.0456 16543 10.172 10.219 120 2 0.5695 0.0285 13117 10.178 10.203 120 3 0.6098 0.0305 13521 10.169 10.191 120 4 0.7896 0.0395 15323 10.170 10.207 120 ---------------------------------------------------------------------------- ast Message: Low Sample Detected <<Statistics>>> Mean: 0.7201 Std Dev: 0.1594 RSD: 22.14 ample ID: CRI ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 Aerator ID: JASON SAMUEL e0 ppm C ug C Raw Data Mode: TOC Filename: 06131608 Timestamp: 2005/06/13 18:00 Sample Type: Sample Beginning Ending Integration ample ID: 0506276-004B ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 perator ID: JASON SAMUEL Mode: TOC Filename: 06131608 Timestamp: 2005/06/13 19:29 Sample Type: Sample ep # ppm C ug C Baseline Baseline Time 1 1.3505 0.0675 20943 10.207 10.244 120 2 1.0529 0.0526 17961 10.202 10.202 120 3 1.2256 0.0613 19691 10.169 10.182 120 4 0.9904 0.0495 17334 10.155 10.181 120 --------------------------------------------------- ajessage: Low Sample Detected ------------------------------------- as essage: Low Sample Detected <<Statistics>>> Mean: 1.1549 Std Dev: 0.1640 RSD: 14.20 ample ID: MBLK Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 18:30 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.2694 0.0135 10111 10.062 10.065 120 2 0.1870 0.0093 9284 10.060 10.069 120 3 0.2034 0.0102 9449 10.051 10.068 120 4 0.1406 0.0070 8820 10.054 10.062 120 -------------------------------------------------------------------------- ast Message: Low Sample Detected <<Statistics>>> Mean: 0.2001 Std Dev: 0.0533 RSD: 26.64 ample ID: 0506276-003B Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 18:59 p * r ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 2.5862 0.1293 33324 10.031 10.052 120 2 1.7246 0.0862 24691 10.025 10.058 120 3 2.0014 0.1001 27464 10.007 10.054 120 4 2.0726 0.1036 28178 9.993 10.044 120 ---------------------------------------------------------------------------- ast Message: Low Sample Detected <<Statistics>>> Mean: 2.0962 Std Dev: 0.3595 RSD: 17.15 ample ID: 0506276-004B ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 perator ID: JASON SAMUEL Mode: TOC Filename: 06131608 Timestamp: 2005/06/13 19:29 Sample Type: Sample ep # ppm C ug C Raw Data Beginning 120 10.044 120 10.003 Baseline 1 0.8644 0.0432 16072 10.015 2 0.6365 0.0318 13788 10.008 3 0.4747 0.0237 12168 10.004 4 0.5775 0.0289 13198 9.990 --------------------------------------------------- ajessage: Low Sample Detected Ending Integration Baseline Time 10.041 120 10.044 120 10.003 120 10.003 ----------------------- 120 00 N O E-� <<Statistics>>> Mean: 0.6383 Std Dev: 0.1649 RSD: 25.84 ample ID: 0506329-001A Mode: TOC e TOC WASTE WATER Filename: 06131608 a urve: TOC WW CURVE 42805 Timestamp: 2005/06/13 19:59 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 1.0536 0.0527 17967 9.980 9.992 120 2 0.9274 0.0464 16703 9.966 9.988 120 3 0.7901 0.0395 15328 9.957 9.994 120 4 0.7883 ---------------------------------------------------------------------------- 0.0394 15310 9.947 9.978 120 ast Message: Low Sample Detected <<Statistics>>> Mean: 0.8899 Std Dev: 0.1271 RSD: 14.29 ample ID: 0506329-002A Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 20:28 Aerator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.5791 0.0290 13214 9.999 10.002 120 2 0.9108 0.0455 16537 9.936 9.944 120 3 0.9775 0.0489 17205 9.912 9.936 120 0.6574 - --------------------- 0.0329 ----13999---------9_889-------9_892-------120----- ast Message: Low Sample Detected <<Statistics>>> Mean: 0.7812 Std Dev: 0.1928 RSD: 24.68 ample ID: 0506329-002AMS Mode: TOC athod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 20:57 aerator ID: JASON SAMUEL Sample Type: Sample ap # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 12.8214 0.6411 135875 9.908 10.904 107 2 10.9469 0.5473 117093 9.915 10.914 108 3 8.1074 0.4054 88643 9.880 10.870 106 4 8.0434 ---------------------------------------------------------------------------- 0.4022 88002 9.877 10.874 106 ,<Statistics>>> Mean: 9.9798 Std Dev: 2.3285 RSD: 23.33 ample ID: 0506329-002ADUP Mode: TOC �thod: TOC WASTE WATER Filename: 06131608 jlourve: TOC WW CURVE 42805 Timestamp: 2005/06/13 21:26 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration 4.1183 0.2059 4 3.4208 Baseline Baseline Time 1 1.2577 0.0629 20012 9.911 9.934 120 1.1027 0.0551 18460 9.905 9.923 120 1.1430 0.0572 18864 9.896 9.935 120 4 •---------------------------------------------------------------------------- 1.1033 0.0552 18465 9.899 9.939 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 1.1517 Std Dev: 0.0732 RSD: 6.35 ;ample ID: 0506329-003A Mode: TOC lethod: TOC WASTE WATER Filename: 06131608 :al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 21:54 )perator ID: JASON SAMUEL Sample Type: Sample ;ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 7.2763 0.3638 80316 9.988 10.981 104 2 7.2404 0.3620 79956 10.016 11.008 104 3 5.6838 0.2842 64360 10.004 11.004 104 4 6.6047 0.3302 73587 10.035 11.035 104 ---------------------------------------------------------------------------- <<Statistics>>> Mean: 6.7013 Std Dev: 0.7452 RSD: 11.12 ample ID: 0506329-004A Mode: TOC TOC WASTE WATER Filename: 06131608 Ae a urve: TOC WW CURVE 42805 Timestamp: 2005/06/13 22:22 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 6.2041 0.3102 69573 10.118 11.116 103 2 6.2059 0.3103 69591 10.126 11.120 104 3 6.5977 0.3299 73517 10.140 11.135 105 4 ---------------------------------------------------------------------------- 5.5671 0.2784 63191 10.137 11.127 104 <<Statistics>>> Mean: 6.1437 Std Dev: 0.4267 RSD: 6.94 ample ID: 0506329-005A ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 perator ID: JASON SAMUEL ep # ppm C ug C Raw Data 1 3.9736 0.1987 2 3.4759 0.1738 3 4.1183 0.2059 4 3.4208 0.1710 47225 42238 48674 41686 Mode: TOC Filename: 06131608 Timestamp: 2005/06/13 22:50 Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 10.235 11.224 101 10.232 11.232 100 10.213 11.212 101 10.225 ----------------------------------------- 11.214 101 00 N O F-+ :« Statistics>>> Mean: 3.7472 Std Dev: 0.3508 RSD: 9.36 ;ample ID: 0506329-006A Mode: TOC 4e&: TOC WASTE WATER Filename: 06131608 a urve: TOC WW CURVE 42805 Timestamp: 2005/06/13 23:18 )perator ID: JASON SAMUEL Sample Type: Sample tep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 5.3379 0.2669 60894 10.280 11.273 102 2 4.5945 0.2297 53445 10.289 11.282 102 3 4.0645 0.2032 48135 10.309 11.307 101 4 3.4044 •---------------------------------------------------------------------------- 0.1702 41522 10.328 11.320 100 X< Statistics>>> Mean: 4.3503 Std Dev: 0.8188 RSD: 18.82 ;ample ID: CCV Mode: TOC lethod: TOC WASTE WATER Filename: 06131608 .al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/13 23:44 )perator ID: JASON SAMUEL Sample Type: Sample .ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 27.0774 1.3539 278712 10.495 11.488 114 2 26.7077 1.3354 275008 10.595 11.592 114 3 28.4014 1.4201 291978 10.666 11.660 114 4 27.2129 1.3606 280069 10.679 11.668 113 -------------------------------------------------------------------- <0 tistics>>> Mean: 27.3498 Std Dev: 0.7328 RSD: 2.68 ample ID: CCB Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 00:17 perator ID: JASON SAMUEL Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.6163 0.0308 13587 10.812 10.843 120 2 0.6268 0.0313 13692 10.871 10.916 120 3 0.5487 0.0274 12909 10.906 10.953 120 4 0.8507 ---------------------------------------------------------------------------- 0.0425 15935 10.920 10.978 120 ast Message: Low Sample Detected <<Statistics>>> Mean: 0.6606 Std Dev: 0.1314 RSD: 19.88 ample ID: 0506329-007A Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 00:45 aerator ID: JASON SAMUEL Sample Type: Sample r �J tep #ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 4.8398 0.2420 55904 11.067 12.065 100 2 4.1348 0.2067 48839 11.085 12.075 101 3 4.0538 0.2027 48029 11.087 12.077 101 0.2410 55709--------11_119------12_114-------102 ----- -�---4_8204- :« Statistics>>> ------ Mean: ----- 4.4622 Std Dev: 0.4262 RSD: 9.55 ;ample ID: 0506329-008A Mode: TOC lethod: TOC WASTE WATER Filename: 06131608 :al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 01:13 )perator ID: JASON SAMUEL Sample Type: Sample ;ep #ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 4.1181 0.2059 48672 11.202 11.285 120 2 3.1367 0.1568 38839 11.224 12.215 99 3 3.4845 0.1742 42324 11.238 12.232 99 4 ----------------------------------------------------------------------------- 3.1577 0.1579 39050 11.260 12.256 98 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 3.4742 Std Dev: 0.4578 RSD: 13.18 ;ample ID: 0506329-009A Mode: TOC lethod: TOC WASTE WATER Filename: 06131608 :al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 01:42 )poor ID: JASON SAMUEL Sample Type: Sample - :ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 3.7558 0.1878 45042 11.357 11.398 120 2 3.4262 0.1713 41740 11.327 11.399 120 3 3.7410 0.1871 44894 11.347 11.414 120 4 ----------------------------------------------------------------------------- 3.6061 0.1803 43543 11.348 11.416 120 ,ast Message: Low Sample Detected :«Statistics>>> Mean: 3.6323 Std Dev: 0.1530 RSD: 4.21 ample ID: 0506329-OIOA Mode: TOC lethod: TOC WASTE WATER Filename: 06131608 :al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/1 02:11 )perator ID• JASON SAMUEL Sample Type: Sample .ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 4.9158 0.2458 56665 11.394 12.388 102 2 3.6478 0.1824 43961 11.416 12.412 100 3 3.5507 0.1775 42988 11.426 12.419 100 4 3.4024 0.1701 41502 11.431 11.484 120 ----------------------------------------------------------------------- .ast Message: Low Sample Detected :« Statistics>>> Mean: 3.8792 Std Dev: 0.6984 RSD: 18.00 >a ID: 0506329-011A Mode: TOC Raw Data 9e . TOC WASTE WATER Filename: 06131608 'al.Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 02:39 )perator ID: JASON SAMUEL Sample Type: Sample 10.0333 tep # ppm C ug C Raw Data Beginning Ending Integration 2 9.3500 Baseline Baseline Time 1 3.5549 0.1777 43030 11.489 12.480 99 2 3.7480 0.1874 44964 11.496 11.567 120 3 3.1482 0.1574 38955 11.500 12.491 98 4 2.9522 ----------------------------------------------------------------------------- 0.1476 36991 11.511 12.506 99 ,ast Message: Low Sample Detected ample ID: LFBD X< Statistics>>> Mean: 3.3508 Std Dev: 0.3649 RSD: 10.89 TOC ample ID: 0506329-012A Mode: TOC rve: TOC fethod: TOC WASTE WATER Filename: 06131608 .al. Curve: TOC WW CURVE 42805 Timestamp: 2005/06/14 03:05 )perator ID: JASON SAMUEL Sample Type: Sample ;ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 0.4879 0.0244 12300 11.492 11.494 120 2 0.2989 0.0149 10406 11.500 11.516 120 0.3713 0.0186 11131 11.483 11.480 120 0.4269 ---------------------------------------------------------------------------- 0.0213 11689 11.442 11.443 120 -ast Message: Low Sample Detected <<Statistics>>> Mean: 0.3963 Std Dev: 0.0805 RSD: 20.31 ample ID: LFB ethod: TOC WASTE WATER al. Curve: TOC WW CURVE 42805 perator ID: JASON SAMUEL Mode: TOC Filename: 06131608 Timestamp: 2005/06/14 03:37 Sample Type: Sample ep # ppm C ug C Raw Data Beginning Ending Integration Baseline Baseline Time 1 10.0333 0.5017 107940 10.960 11.947 108 2 9.3500 0.4675 101094 10.878 11.877 107 3 9.2246 0.4612 99837 10.822 11.817 107 4 ---------------------------------------------------------------------------- 9.9993 0.5000 107599 10.755 11.747 106 <<Statistics>>> Mean: 9.6518 Std Dev: 0.4242 RSD: 4.40 ample ID: LFBD Mode: TOC ethod: TOC WASTE WATER Filename: 06131608 al rve: TOC WW CURVE 42805 Timestamp: 2005/06/14 04:05 M 00 N O H )perator ID: JASON SAMUEL tep # ppm C ug C Raw Data 1 9.9618 0.4981 107223 107 9.8659 0.4933 106262 10.503 9.7194 0.4860 104794 4 9.8925 0.4946 106529 :«Statistics>>> Mean: 9.8599 ;ample ID: CCV fethod: TOC WASTE WATER :al. Curve: TOC WW CURVE 42805 )perator ID: JASON SAMUEL Sample Type: Sample Beginning Ending Integration Baseline Baseline Time 10.552 11.552 107 10.519 11.514 107 10.503 11.497 107 10.487 11.486 107 ----------------------------------------- Std Dev: 0.1020 RSD: 1.03 115 Mode: TOC Filename: 06131608 Timestamp: 2005/06/14 04:34 Sample Type: Sample ;ep # ppm C ug C Raw Data Beginning Ending Integration 0.4087 0.0204 11506 3 0.4771 Baseline Baseline Time 1 26.9406 1.3470 277341 10.405 11.399 115 2 26.9823 1.3491 277759 10.475 11.474 113 3 26.6054 1.3303 273983 10.458 11.458 114 4 ----------------------------------------------------------------------------- 26.8861 1.3443 276796 10.457 11.455 113 X<Statistics>>> Mean: 26.8536 Std Dev: 0.1701 RSD: 0.63 ;ample ID: CCB fethod: TOC WASTE WATER 'a�urve: TOC WW CURVE 42805 �p or ID: JASON SAMUEL .ep # ppm C ug C Raw Data 1 0.5098 0.0255 12519 2 0.4087 0.0204 11506 3 0.4771 0.0239 12192 4 ----------------------------------- 0.5187 0.0259 12608 ,ast Message: Low Sample Detected <<Statistics>>> Mean: 0.4786 C7 Mode: Filename: Timestamp: Sample Type: Beginning Baseline 10.416 10.436 10.442 10.448 ------------ TOC 06131608 2005/06/14 05:04 Sample Ending Integration Baseline Time 10.434 120 10.442 120 10.475 120 10.474 ----------------------- 120 Std Dev: 0.0499 RSD: 10.43 It 00 N O F-+ Calibration Report Print Date/Time: 2005/06/14 8:46:35 :al. Curve ID: TOC WW CURVE 42805 .reated: 2005/04/29 08:26 .ali ration Factor (m): 2.004e+05 rcept (b): 4931 -s red: 0.99970 Standard ID Y X Expected Measured Message Raw Data ug C ug C ►I 11765 0.000 0.034 Low Sample De 1.5PPM 13772 0.025 0.044 Low Sample De .OPPM 17398 0.050 0.062 Low Sample De �.OPPM 50434 0.250 0.227 O.OPPM 98824 0.500 0.469 S.OPPM 250200 1.250 1.224 ,O.OPPM 506419 2.500 2.503 5.OPPM 758873 3.750 3.762 • �J Date & Time 2005/04/28 16:09 2005/04/28 16:27 2005/04/28 16:45 2005/04/28 17:02 2005/04/28 17:20 2005/04/28 17:38 2005/04/28 17:56 2005/04/28 18:14 00 N O V) F-4 0 • r� U2M UAUS, INC. SDG NO.: C-66 L SCAN: VV J4 , This data package was reported by the undersigned. This reporting includes data calculations, manual edits if necessary and compilation of raw data. The information presented is true and correct to the best of my knowledge. ,, Sign Rev 110 00 N O Cn E -i