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HomeMy WebLinkAboutScavenger Waste Phase II Env Site AssessmentLI[ %%A L. K. McLean .4ssociates, PC. 437 South Country Road · Brookh[*ven · New Yolk * I 1'719 (631 ) 286-8668 · FAX (631 } 286°63 }4 ('ONSULTING ENGINEERS EUGENE F DALY, PE., PTO.ETM PRESIDENT aad CE O RAYMOND G DiB~ASE, PE · P TOE tM, EXECU FIVE VICE PRESIDENT JOSEPH F CLINE, P.E., VICE PRESIDENT ROY R. FULKERSON, PLS., VICE PRESIDENT ALBERT T DAWSON, PE, VICE PRESIDENT Town of Southold Law Depa~tment 53095 Route 25 P.O. Box 1179 Southold, New York 11971 April 16, 2007 Associates CHRISTOPHER F DWYER JAMES L. DeKONING, PE ROBERTA. STEELE, PE Attn: Patricia Fim~egan, Town Attorney Re.' Southold Town Scavenger Waste Facility - Phase II Environmental Site Assessment Closure Summary Report LKMA Project: 07009.000 Dear Ms. Finnegan: As requested by your office, L.K. McLean Associates administered a Phase II Enviromnental Site Assessment at the Town's former Scavenger Waste Treatment Facility. The soil and water analysis as defined in the Site Work Plan identified one of the eleven locations to yield elevated contaminants in the upper soil layer. The eleven test sampling locations (No. 1 l's location is shown on Page 11 of 11 in the Soil Boring Log) were positioned within the three (3) formerly leased parcels. Parcel One (1) had sampling locations No. 1 through No. 8 and No. 11, while Parcels Two (2) and Three (3) had sampling locations No. 9 and No. 10 respectively. Sampling location No. 10 yielded results in excess of the recommended cleanup objectives and will require a small scale soil removal (top 1 to 2 feet) at the area currently identified as the out-vessel drying beds. The drying bed is approximately 120'x 50'. Therefore if the Town were to remove the top two (2) feet of soil in that area (Parcel 3), approximately 445 cubic yards of material would need to be excavated and disposed of at a permitted facility. Using an average cost of $78 per ton, the estimated disposal costs associated with the cleanup would cost around $44,000 (assuming a conversion of 1.25 tons per cubic yard). Enclosed you will find two (2) copies of the summary report for your use. If you should have any questions regarding the content of this report or the recommendations made, please do not hesitate to contact this office directly, CFD:cfd Enc. (1) CC: Town Board Members LKMA File Copy w/enc. Very truly yours, Christopher F. Dwyer, Associate Founded itt 1950 Phase II Environmental Site Assessment Report April 2007 Submitted to: Town of Southold Prepared for: LK McLean Associates 437 South Country Road Brookhaven, NY 11719 PWGC Project No. LKM0701 Prepared by: PWGC Strategic Environmental & Engineering P.W. Grosser Consulting, Inc. 630 Johnson Avenue, Suite 7 Bohemia, NY 11716 Phone: (631) 589-6353 Fax: (631) 589-8705 Project Director: Frank Castellamo E-mail: Frankc @ pw.qrosser.com Pwoc TABLE OF CONTENTS Former Town of Southold Scavenger Waste Plant Moores Lane, Greenport, New York 1.0 INTRODUCTION .............................................................................................................................. 1 2.0 SITE DESCRIPTION AND BACKGROUND .................................................................................... 1 3.0 SUB-SURFACE INVESTIGATION ................................................................................................... 1 3.1 Collection of Soil Samples ............................................................................................................ 2 3.1.1 Soil Quality ................................................................................................................................... 3 3.2 Collection of Groundwater Samples ............................................................................................. 3 3.2.1 Groundwater Quality .................................................................................................................... 4 4.0 Conclusions and Recommendations ............................................................................................ 5 Table 1 Table 2 Table 3 Table 4 Table 5 Table 6 Figure 1 Appendix A Appendix B Tables Soil Analytical Results for Volatile Organic Compounds Soil Analytical Results for Semi-Volatile Organic Compounds Soil Analytical Results for Metals Groundwater Analytical Results for Volatile Organic Compounds Groundwater Analytical Results for Semi-Volatile Organic Compounds Groundwater Analytical Results for Metals List of Figures Site Plan with Boring Locations Appendices Soil Boring Logs Laboratory Analytical Reports P.W. Grosser Consulting, In~ · P.W. Grosser Consuiting Engineer & Hydrogeologist, PC 630 Johnson Avenue, Suite 7 · $chemia, NY I 1716 ° Branch Location - Seattle, WA PH 631.589.6353 · FX 631.589.8705 · www.pwgrosser.com Pwoc 1.0 INTRODUCTION P.W. Grosser Consulting, Inc. (PWGC) has prepared the following report on behalf of LK McLean Associates, PC (LKMA) to outline the results of the Phase II Environmental Site Assessment (ESA) performed at the former Town of Southold Scavenger Waste Plant. The work was conducted to identify and characterize potential contaminants within the surface/subsurface soils and groundwater prior to returning the site to the Village of Greenport. The investigative work was performed in accordance with the Phase II Investigation Work Plan, March 2007, prepared for the site. 2.0 SITE DESCRIPTION AND BACKGROUND The subject site is located on the west side of Moores Lane in the Village of Greenpod, NY. It is understood that the site has been utilized by the Town of Southold as their scavenger waste plant for the past twenty years under a lease agreement with the Village of Greenport. The lease term is now expiring and the Town has performed a Phase II ESA in an effort to characterize soil and groundwater quality at the site prior to returning the site to the Village. The overall objective of the Phase II ESA is to evaluate the condition of the property to determine if soil and/or groundwater have been impacted by the scavenger waste plant operations. 3.0 SUB-SURFACE INVESTIGATION The Phase II ESA involved the performance of a detailed sub-surface investigation consisting of the collection, field screening and laboratory analysis of soil and groundwater samples in an attempt to identify and characterize contaminants at the site. The investigation focused on those areas of the site with the greatest potential to have received an impact from the past site operations. The soil and groundwater sampling was accomplished through the performance of eleven soil borings using a GeoprobeTM. The boring locations were biased toward areas of the site believed to be vulnerable to impacts from past site operations such as adjacent to existing underground storage tanks, chemical and/or waste storage areas, topographic depressions, former drying beds, etc. The chosen location for each boring was coordinated as a joint effort between PWGC and LKMA on behalf of the Town of Southold, and Nelson, Pope and Voorhis, LLC on behalf of the Village of Greenport. The locations of the eleven borings are illustrated on Figure 1. P.W. Grosser Consulting, Inc ° P.W. Grosser Consulting Engineer & Hydrogeologist, PC 630 Johnson Avenue, Suite ? ° Bohemia, NY 11716 · Branch Location - Seattle, WA PH 631.589.6353 · FX 631.589.8?05 ' www.pwgrosser.com PW(SC 3. ~ Collection of $oil Sample$ On March 20, 2007 and March 21, 2007, soil borings were performed using a track mounted GeoprobeTM provided by Associated Environmental Services, Inc. of Hauppauge, New York. The GeoprobeTM uses direct push technology to drive core samplers to the desired depth for soil sample collection. This method can be performed quickly, so that in the event that refusal occurs, a new location can be accessed with minimal effort. As specified in the Work Plan, PWGC and their subcontractor followed GeoprobeTM operation and sampling procedures SOP No. 95-8500. At each of the eleven soil boring locations, soil samples were collected continuously from grade to the groundwater interface. Soil samples were characterized and screened in the field for the presence of volatile organic compounds using a photoionization detector (PID). Soils beneath the site were observed to consist of fine grained sands followed by a native clay layer. Groundwater was encountered at depths varying from three to fourteen feet below grade. This range was primarily due to the steep topographic elevation changes across the site. Soil borings logs for each of the soil borings are contained in Appendix A. No obvious visual evidence of contamination (i.e. staining), or elevated PID readings were recorded during the sampling program, therefore, in accordance with the Work Plan, the deepest soil sample above the groundwater table was retained and submitted for laboratory analysis from each boring, The eleven soil samples collected were submitted to American Analytical Laboratories, Inc. (AAL) of Farmingdale, New York, a New York State Department of Health (NYSDOH) ELAP certified laboratory (ELAP #11418). The soil samples were analyzed for the following parameters: · Volatile organic compounds by EPA Method 8260, · Semi-volatile organic compounds by EPA Method 8270, · Inorganic Compounds (Target Analyte List metals) Analytical results for the eleven soil samples are summarized in Tables 1 through 3. Complete analytical reports are contained in Appendix B. P.W. Grosser Consulting, Inc · P.W. Grosser Consulting Engineer & Hydrogeologisl, PC 630 Johnson Avenue~ Suite 7 · Bohemia, NY 11716 ° Branch Location - Seattle, WA PH 631.589.6353 ° FX 631.589.8705 ° www.pwgrosser.com PWGC : 3.1.1 Soil Quality In order to evaluate the soil quality at the site, soil analytical results were compared to the NYSDEC's Recommended Soil Cleanup Objectives (RSCOs) specified in the NYSDEC's Technical and Administrative Guidance Memorandum #4046 guidance document (TAGM). The TAGM was specifically designed to address soil clean-up goals at inactive hazardous waste sites, but is commonly utilized as a reference for soil quality to determine if additional investigation and/or remediation is warranted at non-inactive hazardous waste sites. As shown on Table 1, no volatile organic compounds were detected in the soil samples collected at concentrations exceeding the laboratory detection limits. As shown on Table 2, several semi-volatile organic compounds were reported slightly above their respective RSCOs in one of the eleven samples analyzed. Specifically, 4-Chloraniline, benzo(a)anthracene, benzo(b)flouranthene, benzo(a)pyrene, benzo(k)fiuoranthene, and chrysene were detected above the RSCOs in the sample collected from boring No. 10 located in one of the former drying beds. As shown on Table 3, several inorganic compounds were detected at elevated concentrations in one of the eleven samples analyzed. Cadmium, copper, mercury and zinc were detected above the NYSDEC RSCOs and Eastern USA Background levels in the sample collected from boring No. 10. In summary, several semi-volatile organic compounds and inorganic compounds were reported above their respective NYSDEC RSCOs in the soil sample collected from the drying bed at boring No. 10. These compounds could be associated with the past usage of the drying bed for scavenger waste and is likely indicative of soil quality conditions in the other drying beds at the site. Based upon the sampling performed, this is the only location at the site showing signs of impact. 3.2 Collection of Groundwater Samples Groundwater samples were also collected at each of the eleven soil boring locations. The purpose of the groundwater sampling was to characterize groundwater quality at specific locations at the site and to obtain a snapshot of site wide groundwater quality. Groundwater samples were collected approximately three feet below the water table at each location. A four-foot long screen point sampler was ddven to the desired depth using a GeoprebeTM, At the desired depth, a piece of disposable polyethylene tubing with a stainless P.W. Grosser ConsuJtlng, [nc * P.W. Grosser Consulting Engineer & HydrogeoJogist, PC 3 630 Johnson Avenue, Suite 7 ° Bohemia, NY 11716 · Branch Location - Seatlle, WA PH 631.589.6353 * FX 631.589.8705 * www.pwgrosser.corn PWOC steel check valve was inserted through the probe rods into the water bearing zone. The tubing was then hand oscillated to obtain the sample. Prior to sampling, one to two gallons of water was purged in an effort to reduce sample turbidity. Groundwater samples were collected in accordance with GeoprobeTM operation and sampling procedures SOP No. 95-1500 as specified in the Work Plan. When possible, dedicated, disposable sampling equipment was utilized during the sampling. Non-disposable sampling equipment was cleaned using distilled water and Alconox detergent with a distilled water rinse between sample locations. 3.2.1 Groundwater Quality The groundwater samples collected were submitted to American Analytical Laboratories, Inc. (AAL) of Farmingdale, New York, a New York State Department of Health (NYSDOH) ELAP certified laboratory (ELAP #11418). The groundwater samples were analyzed for the following parameters: · Volatile organic compounds by EPA Method 8260, · Semi-volatile organic compounds by EPA Method 8270, · Inorganic Compounds (TAL metals) Analytical results for the eleven groundwater samples are summarized in Tables 4 through 6. Complete analytical reports are contained in Appendix B. In order to evaluate the groundwater quality at the site, the analytical results were compared to the NYSDEC's groundwater quality standards (NYSDEC Class GA Groundwater Quality Standards, Technical and Operational Guidance Sedes (TOGS) 1.1.1, Ambient Water Quality Standards and Guidance Values and Groundwater Effluent Limitations, NYSDEC, June 1998). As presented in Table 4, no VOCs were detected above NYSDEC groundwater quality standards in each of the eleven samples. As shown in Table 5, no SVOCs were detected above NYSDEC quality standards in each of the eleven samples. As shown on Table 6, several metals were detected above NYSDEC standards in the eleven samples collected. These include: arsenic, badum, cadmium, chromium, copper, iron, lead, magnesium, manganese, nickel, silver, sodium, thallium and zinc. The presence of these metals is typically P.W. Grosset Consulting, Inc · P.W. Grosser Consulting Engineer & Hydrogeologist, PC 4 630 Johnson Avenue, Suite 7 ° Sohemia, NY 11716 ° Branch Location - Seattle~ WA PH 631.589.6353 · FX 631.589.8705 · www.pwgrosser.com PWGC representative of suspended sediment in the samples and not indicative of dissolved metal concentrations in the groundwater. Due to the presence of clay at or near the water table interface, the groundwater samples were observed to be turbid. The inorganic metal concentrations are therefore likely a result of the metals bound to the soil particles which dissolved into groundwater when they came in contact with the acidic preservative in the sampling glassware. This is a common occurrence and is commonly misinterpreted as a groundwater contamination issue when, in reality, the metal compounds detected in the groundwater are the result of interference from soil/sediment particles in the sample and not representative of dissolved metal concentrations. Therefore, the metal concentrations detected in the groundwater samples are not believed to be indicative of a contaminant release. 4.0 Conclusions and Recommendations The results of the Phase II ESA suggest the following: · The soils beneath the site are primarily made up of native sands in the uppermost region and a native clay layer, with groundwater occurring at depths ranging from three to fourteen feet below ground surface. · Soil quality samples collected from boring No. 10 contained semi-volatile organic compounds and inorganic compound (metal) concentrations that exceed the NYSDEC RSCOs. Soil samples from the other ten sampling locations were within NYSDEC RSCOs. · No semi-volatile organic compounds or volatile organic compounds were detected in groundwater samples in excess of NYSDEC groundwater standards at the site. Several inorganic compounds (metals) were detected above groundwater standards in the samples; however it is likely that this is the result of sediment in the samples and not representative of dissolved concentrations and/or a contaminant release. Based on the results of the Phase II testing, PWGC recommends the following: * The upper one to two feet of soil/sediment in the drying bed characterized by boring No. 10 should be excavated from the site and properly disposed of at an appropriated facility in accordance with NYSDEC regulations. · Remaining drying beds at the site of similar construction to the western most drying bed should be characterized to determine if similar remedial action is warranted. P.W. Grosset Comuiting, [nc · P.W. Grosser Consulting Engineer & Hydrogeologist, PC 630 Jol~so~ Avenue, Suite 7 * B~hernia, NY 11716 ' Brand~ Lo~afion - Seattle, WA PH 631.589.6353 · FX 631,589.8705 ° www.pwgrosser.com (1) NYSDEC Recommended Soil Cleanup CYojectives (RSCO), Technical and Administrative Guidance Memorandum (TAGM) #4046, 12/00 '* - New York State Background Concentration SB - Site Background TABLE 4 GROUNDWATER AN AL~f~JCAL RESULTS FOR VOLATILE OR(~.ANIC COMPOUNDS TABLE 5 GROUNDWATER ANALYTICAL RESULTS FOR SEMI-VOLATILE ORGANIC COMPOUNDS EPA METHOD 8270 Not~a: · *. NYSDEc Ambient Water Quali~y Stencil,s and Guidance ¥~lues 6/1998 ND - Non,erect ·. Guidance Value NS - NO Slandard Bolddtllghlighted Ind*ca~ed excsedance of ~le NYSDEC G rounci~te~ Star~ard (~) Applies to each isomer (1 r2 - ~.3 and 1.4) individu&lly TABLE6 GROUNDWATER ANALY'rlCAL RESULTS FOR METALS Forme~ Waste Scavanger Plant - Moores Lane - Greenpoint, New Y~k ~ Pollutm~ Metals ~ Uuminum as Al NS 461 170 265 608 279 759 143 227 245 957 640 ~,ntirnony as Sb 0.00.3 0.0250 0.0250 U 0.0250 U 0.0250 U 0.0255 0.0250 U 0.0250 U 0.0453 0.0250 L: 0.0250 0.0250 *' - NYSDEC Ambient Water Quality Standards and Guidance Values 6/1998 ND - Nor~deteet · - Guidance Value B - Indicates that the compound was detected in the method blank. J - indicates estimated concentration U - Analyte n~t detected NS - NO Standard PARCEL BASEMAP PROVIDED BY: L.K. McLEAN ASSOCIATES, P.C. CONSULTING ENGINEERS 437 S. COUNTRY ROAD BROOKHAVEN, NY PARCEL2~ NO. 9 NO.4 .~+No 2 LEGEND No.1 GROUNDWATER & SOIL SAMPLING LOCATION 60 0 60 I SCALE: 1"=60' 120 MOORES LANE GREENPORT, NY PWGC Strategic Epvironmental & E~,gineedng Solutions APPENDIX A SOIL BORING LOGS P.W. GROSSER CONSULTING, INC. IBorng# No. 1 MW# _ _Page 1 .of IPROJECT: Moo;es Lane- Oreenport, New York LOGGED BY: tDE P_R...~J. MNGR.~ !A__L DR LLING CONTRACTOR: Associated Environmental iDRILL METHOD: Geoprobe I. DRILLER: Timm and John i! Borehole diameter/drill bit type: i total depth - , Macrocore (2 diameter) elevation 'HAMMER Vel': iDROP: NA ~ No. 1 ST~-~ ~ 13:40 DATE: 3/20/07 Approximate borehole locations at site iCOMPLETION TIME: 14:10 DATE: 3/20/07 IBACKFILL TIME: 14:12 'DATE: 3/20/07 15' NA Sample [ Advance Depth I (ft) 0-5' 5' 5-10' 5' Recovered i Soil Description Notes Casing depth: _ (ft) I Unified Soil Classification System __ Screen depth: 0-2.5': 2' Moist, medium grained dark brown i silts. 0.5' Moist, dark brown clay. F 2.5~5': 0.5' Moist, dar brown clay. 2' Moist, ght brown c ay. IPID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. .5-7.5.0.5 Wet, brown clay. 0.5 Mo st, ~ ~medium grained reddish-brown sand. 1' I " I Grushed concrete. PID -> 5-7.5.0.0 ppm. 7.5-10." 0.0 ppm. f7.5-10': Dry, medium-fine reddish- grained brown sand. ~ 10-15' 5' 10-12.5: Wet, medium-fine grained reddish- brown sand with quartz stones. 112.5-5': 2' Wet, medium-fine grained reddish- brown sand with quartz stones. 0.5' Moist, brown clay: lGroundwater at 13'. interface located PID -> 10-12.5': 0.0 ppm. 12.5-15': 0.0 ppm. Soil sample collected fro 10-12.5',at 14:04. GW sample collected from 13-17 at 14:10. P.W GROSS ;;;~ ~ ~CT.-'~Moores La--~-e - Greenport, New ~ork_ -~ ~ ~.~ iDRILLING CONTRACTOR: Ass°ciated Envir°nmental II ~ / / / ~ , DRILL METHOD: Geoprobe ~ ~ ~ ~"-"""~ ....-~ ~ !DRILLER: Timm and John ~ ~ ~ ~ ~ ~ Iaorehoedameter/dr bt~p; ~ ~0 ~ ~/~ ~ Macrocore (2" d ameter) , e,evation----~ NA -- ~ No. 2 {START TIME: 1~ Approximate borehole locations at site COMPLETION TIME: 13:20 {DATE: 3/20/07 ...... ;BACKFILL TIME: 13:21 IDATE: 3/20/07 Sample Advance ' Recovered '- Soil Description Depth. (~ ~ (ft) Unified Soil Classification System Notes iCasing depth: __ ; Screen depth: 5~ 51 tl0-2.5' Moist, medium grained reddish-brown sand with quartz. 2.5-5': Moist, medium grained reddish-brown i sand w th quartz 5' 3.5' .... PID -> 0-2.5.0,0 ppm. 2.5-5.0.0 ppm. ~GW sample collected from 10-14' at 13:20. 15-7.5': Wet, medium-fine grained reddish- brown sand with quartz stone. 7.5-10': 1 Wet, gray c ay. 1 Wet, brown c ay. PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. i0.5' Moist, medium grained light brown sand ~ I with quartz. IGroundwater interface at 9'. Soil sample collected from 7.5-10' at 13:15. P.W. GROSSER CONSULTING, INC. '~, Approximate borehole locations at site Sample Advance Recovered IBoring# No. 3 iMW# ?'age 3 of 11 PROJECT: Moores Lane - Greenport, New York JOB # LKM 0701 LOGGED BY: !PRJ. MNGR.: ~ DRILLING CONTRACTOR: Associated Environmental DRILL METHOD: Geoprobe DRILLER: Timm and John Borehole diameter/drill bit type: Macrocore (2" diameter) total depth elevation HAMMER WT: DROP: NA 10' NA I-START TIME: 12:17 COMPLETION TIME: 12:55 IBACKFILL TIME: 12:56 DATE: 3/20/07 DATE: 3/20/07 DATE: 3/20/07 Soil Description Unified Soil Classification System Notes ,Casing depth: i Screen depth: 5' 5~ ;0-2.5': 2.5' Moist, dark brown silts. I ,iPID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. 2.5-5': 2.5' Moist, medium grained light brown ~,sand. 5-10' I 5' ~'0': 2' Moist, brown clay. 0.5' Wet, fine--~PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. . ~gra~ned brown sand. Groundwater interface at 8' i Soil sample collected from 5-7.5' at 12:49. GW sample collected from 8-12' at 12:55. Approximate borehole locations at site P.W. GROSSER CONSULTING, INC. No. 4~ Sample Advance Recovered Depth : (fi) (fi) IBoring# No. 4 MW# ~Pa~e 4 of ECT: Moores Lane - Greenport, New York ,LOGGED BY: ~DE iPRJ. MNGR.: ,AL ! r DRILLING CONTRACTOR: Associated Environmental IDRILL METHOD: Geoprobe DRILLER: Timm and John Borehole diameter/drill bit type: T total depth Macrocore (2" diameter) elevation 'HAMMER WT: DROP: NA iSTART TIME: 11:39 DATE: 3/20/07 r M - CO PLETION TIME: 12:10 - DATE: 3/20/07 ~~' -- DATE: 3/20/07 Soil Description Notes iCasing depth: Unified Soil Classification System ~ !Screen depth: 11 NA 0-5' 5' 5' ~0-2.5': 1' Moist, dark brown silts. 1.5' Moist, tmedium grained light brown sand with quartz. ,2.5-5': 2.5' Moist, medium grained light brown ,sand with quartz. PID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. 5-10' 5' 4' 10-15' .5-7.5': Moist, medium-fine grained reddish- brown sand. :7.5-10': 1.5' Moist, medium-fine grained reddish-brown sand. 0.5' Moist, medium-fine PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.1 ppm. grained gray sand. 0.5' Dry, medium grained , light brown sand with quartz. i 10-12.5': 0.5' Moist, gray clay. 2' Wet, medium grained light brown sand with quartz. PID -> 10-12.5': 0.0 ppm. 12.5-15': 0.0 ppm. 12.5-15': 2.5' Wet, medium grained light Ibrown sand with quartz. ,~ 'Soil sample collected from 10-12;5' at 12:02. I [ iGr°undwater interface at 12" I~GW sample c°llected fr°m 12'16 at 12:10' '! P.W. GROSSER CONSULTING, INC. Approximate borehole locations at site Samp~ Advance ~ Recovered Depth (ft) (ft) iBoring_~ No. 5_ ~MW# iPage 5 tPROJECT: Moores Lane - Greenport, New York i JOB # LKM 0701 ~_ of 11 LOGGED BY: ;DE ' iPRJ. MNGR.: ,AL DRILLING CONTRACTOR: Associated Environmental DRILL METHOD: Geoprobe DRILLER: Timm and John Borehole diameter/drill bit type~'''--~-- -- - total depth Mecrocore (2" diameter) elevation HAMMER WT: ~,DROP: NA !START TIME: 10:20 DATE: 3/20/07 ii ~ME: 11:00 ~BACKFILL TIME: 11:10 Soil Description '-~ -- - Unified Soil Classification System Notes DATE: 3/20/07 DATE: 3/20/07 Casing depth: Screen depth: 0-5' 5' 5' ;0-2.5': 2' Moist, medium grained dark brown silts. 0.5' Moist, mediumgrained light brown sand with quartz. ~- ---~PID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. 2.5-5': 1.5' Moist, medium grained light brown sand with quartz. 1' Moist, dark brown clay. 15-7.5': Moist, fine grained brown sand with i_quartz. 5-10' 5' 5' 7.5-10': 0.5' Moist, fine grained brown sand PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. t iwith quartz. 1' Moist, brown clay. 1' Dry, fine :grained light brown sand. 10-15' 5' 5' ~10-12.5': 0.5' Moist, brown clay. 2' Wet, ~ i medium grained light brown sand with quartz. -- ----; PID -> 10-12.5': 0.0 ppm. 12.5-15': 0.0 ppm. 112.5-15': 1.5' Wet, medium grained light brown sand with quartz. 1' Moist, brown clay. Soil sample collected from 10-12.5' at 10:53. Groundwater interface located at 12'. GW sample collected from 12-16' at 11:00. Boring# No. 6 i MW# ,P~ 6 _ i of 11 PROJECT: Moores Lane - Greenport, New York P.W. GROSSER CONSULTING, INC. Approximate borehole locations at site Sampl'~T Advance Recovered Depth (fi) (ft) JOB # LKM 0701 LOGGED BY: tDE ~PRJ. MNGR.: iAL __ i DRILLING CONTRACTOR: Associated Environmental ,DRILL METHOD: Geoprobe 'DRILLER: Timm and John ~ Boreho e d ameter/drill bit type: total depth 15' Macrocore (2" diameter) HAMMER WT: I START TIME: 14:20 i COMPLETION TIME: 14:50 BACKFILL TIME: 14:55 Soil Description - ~ Notes Unified Soil Classification System elevation NA DROP: NA DATE: 3/20/07 - IDATE: 3/20/07 DATE: 3/20/07 iCasing depth: Screen depth: 5-10' 10-15' 0-2.5': Moist, medium grained light brown sand with quartz pieces. i2.5-5': Moist, medium grained light bro,~,n Isand with quartz pieces. PID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. 5' 2' 5-10" Moist, medium-fine grained light brown l piD -> 5-10': 0.0 ppm. ~ sand. i10-12.5': Moist, medium-fine grained brown isand. reddish'brown!l PI D -> 10-12.5': 0.0 ppm. 12.5-15': 0.0 ppm. 1 2.5-1 5': Wet, ~ edi~ r-'~ed isand. _ .... Soil Sample collected from 10-12.5' at 14:421 iGroundwater interface located at 13'. [GW sample collected from 13-17' at 14:50. 5~ iBoring# No. 7 tMW# iPa~ge 7 of 11 P.W. GROSSER % Approximate borehole locations at site Sample 'l Advance Recovered Depth ~ (ft) ~ ~PROJECT: Moores Lane - Greenport, New York !JOB # LKM 0701 ILOGGED BY: DE PRJ. MNGR.: AL '~DRILLING CONTR~,C'~-OR: Associated Environmental 'DRILLER: John ..... !~~: to~ i 20' I Macrocore (2" diameter) i elevation NA HAMMER WT: DROP: NA I START TIME: 12:45 COMPLETION TIME: 13:57 IBACKFILL TIME: 13:58 Soil Description Notes Unified Soil Classification System DATE: 3/21/07 DATE: 3/21/07 ~DATE: 3/21/07 [ CasinQ depth: ~Screen depth: 0-5' 5' 5' 0-2.5': 1' Moist, medium grained dark brown Isilts. 1.5' Moist, medium-fine grained light ibrown sand with quartz. t2.5-5!: 2.5' Moist, medium-fine grained light brown sand with quartz. P D -> 0-2 5': 0.0 ppm. 2.5-5': 0.0 ppm. 5-10! 5-7.5': Moist, medium-fine grained reddish- brown sand. 10-15' 5' 4! 7.5-10!: Moist, medium-fine grained reddish- brown sand with concrete and red brick !debris. 10-12.5': Moist, medium-fine grained reddish- i brown sand with crushed quartz. 12.5-15: 2 Moist, medium-fine grained Ireddish-brown sand with crushed quartz. 0.5' !Wet, medium grained reddish-brown sand !with quartz. PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. PID -> 15-17.5': 0.0 ppm. 17.5-20': 0.0 ppm. Groundwater interface located at 14'. !Soil sample collected from 12.5-15! at 13:35~ IGW sample collected from 14-18' at 13:57. 15-20' 5' 5' 17.5-20': 0.5' Wet, medium-fine grained reddish-brown sand with quartz. 2! Moist, __ brown cl_.l.l.l.l.l.l.l.l~.. 15-17.5': Wet, medium-fine grained reddish- brown sand with quartz. PID -> 10-12.5:0.0 ppm. t2.5-15.0.0 ppm. P.W. GROSSER CONSULTING, INC.  Boring # No. 8 MW# iP._.~_ge 8 , P--~0~E-C~-~ ~l~"ores Lane- Greenport, New York Sample Advance ~ Recovered Depth (ft) (ft) 20' iof 11 iLOGGED BY: iDE - -'~PRJ. MNGR.: I DRILLING CONTRACTOFb Associated Environmental DRILL METHOD: Geoprobe_ -- -- -- ! DRILLER: Timm and John ~ ~O r~ (~ ' totaldepth Macrocore (2" diameter) ' elevation HAMMER WT: DROP: NA START TIME: 09:00 DATE: 3/20/07 COMPLETION TIME: 10:07 DATE: 3/20/07 ,BACKFILL TIME: 10:08 -- DATE: 3/20/07 Soil Description Notes Casing depth: Screen depth: NA Approximate borehole locations at site Unified Soil Classification System 0-2.5': Moist, medium grained silts with grass land roots. PID -> 0-2.5: 0.0 ppm. 2.5-5' 0.0 ppm. 0-5' 51 51 ~ Moist, medium-fine grained light brown i Isand with quartz rocks. i5-7.5': 0.5' Dry, medium-fine grained light ~brown sand with quartz rocks. 2' Moist, dark 5-10' 5' 5' .+ 10-15' 5~ 5' brown clay. ___ 7.5-10:1 Mo st, gray day. 0.5' Moist, brown ! PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. clay. 1' Dry, medium-fine grained reddish brown sand with quartz stones. 10-12.5': 1' Dry, medium-fine grained dark brown sand. 1.5 Mo st, medium grained reddish-brown sand with quartz rocks. 12.5-15': 1.5' Moist, medium grained reddish- brown sand with quartz rocks. 1' Moist, brown clay. PID -> 10-12.5': 0.0 ppm. 12.5-15.0.0 ppm. 15-20' 51 51 15-17.5': Moist, brown clay. -~PID -> 15-17.5': 0.0 ppm. 17.5-20': 0.0 ppm. 17.5-20': Moist, brown clay. Groundwater interlace located at 12'. Soil sample collected from 10-12.5' at 10:03. iGW sample collected from 13-15' at 10:07. ~ .Boring# No. 9___.;MW.__.~ ___~.~.~e __9 ~o_..~f 1--1 P.W. GROSSER tPROJECT: Moores Lane- Greenport, New York CONSULTING, INC. '~, ~ !~~ , -- ~i -~ ~ ~/~-'")~ iDRILLING CONTR'----------'"-----~CTOR----'~ ~sociated Environmental --~' r ' ~ ~ ~ ~ D"LLE": John ~ ~ / ~ n ~ ~ iota dept ~ 10 ~-- ~ ~ ~ Macrocore (2" diameter) ~ ~ .... ~l tAMMER ~: ',DROP: NA ~[ START TIME: 08:15 COMPLETION TIME: 10:16 , BACKFILL TIME: 10:20 Approximate borehole locations at site Sampl--e Advance '~ Recovered Soil Description Casing depth: Depth ~ (ft) (ft) Unified Soil Classification System Notes Screen depth: i DATE: 3/21/07 =DATE: 3/21/07 ' DATE: 3/21/07 0-2.5': 1' Moist, medium grained dark brown 0.5~ 5-10' 5~ silts. 1.5' Wet, medium-fine grained light brown sand with quartz stones. PID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. 2.5-5': Wet, medium-fine grained light brown Isand with quartz stones. 5~ ~5-7.5': 1' Wet, brown clay. 1.5' Moist, brown 7.5-10': 2.5' Moist brown clay. i Soil sample collected from 2.5-5' at 09:25. !Groundwater interface located at 4'. IGW sample collected from 4-8' at 10:16. Boring# No. 10 ~,MW# !P_.~_,ge 10___ !of 11 P.W. GROSSER iPROJECT:Moores Lane- Greenport, New York -'- CONSULTING, INC. i- f ,LOGGED BY: 'DRILLING CONTRACTOR: Associated Environmental f DRILL METHOD: Geoprobe-- DRILLER: John ........ ' ' i total depth ! 10' acrocore (2 diameter) i elevation NA HAMMER WT: DROP: NA ~ i'START TIME: 10:34 ~COMPLETION TIME: BACKFILL TIME: Sample~ Advance ' Recovered ' - Soil Description Depth (ft) (ft) U~nified Soil Classification System Notes i Casing depth: ' Screen depth: No. 10 Approximate borehole locations at site DATE: 3/20/07 DATE: 3/20/07 DATE: 3/20/07 0-5' 5' 2' 0-5': Moist, medium grained dark brown silts. PID -> 0-5': 0.8 ppm. 5-7.5': 0.5' Wet, fine grained brown and. 2' - ....... iMoist, brrown clay_:_ - - PID -> 5-7.5': 0.0 ppm. 7.5-10': 0.0 ppm. 7.5-10': 2.5' Moist, brown clay. Sol samp e collected from 2.5-5' at 10:55. ~ -----_ ~W sample collected from 1-3' at 12:17. P.W. GROSSER CONSULTING, INC. Approximate borehole locations at site Sample _Depth ! Boring# No. ll iMW# ~11 --',of 11 PROJECT: Moores Lane - GreenDort New York LOGGED BY: DE [PR J. MNGR.: ;AL ~C~OR: Asso_ciat._ed Environ__~menta___L DRILLER: John ....... ,Borehole diameter/dr b t type ......... Macrocore (2" diameter) elevation NA [START T ME 14 12 DATE: 3/21/07 COMPLETION TIME: 15:29 DATE: 3/21/07 BACKFILL TIME: 15:30 DATE: 3/21/07 Advance ' Recovered "---' --- Soil Description (ft) r (ft) Unified Soil Classification System Casin~] depth: Notes iScreen depth: 0-5' 5' 5-10' 10-15' 0-2.5': 1' Moist, medium grained dark brown Isilts. 1.5 Mo st, medium-fine grained reddish- ~brown sand. 5' F - -;PID -> 0-2.5': 0.0 ppm. 2.5-5': 0.0 ppm. i2,5-5': 2.5' Moist, medium-fine grained ~ ~ reddish-brown sand. ~5-7.5': 0.5' Moist, medium-fine grained brow¥ i~'.Moi~st_, light_ b_r_o_wn clay.. _ 17.5-10': Wet, medium grained reddish-brown PID -> 5-7.5.0.0 ppm. 7.5-10:0.0 ppm. 5~ tsand with quartz. ~ 10-12,5': 1' Wet, medium grained reddish- !brown sand with quartz. 1.5' Moist, brown 5' iclay-' 12.5-15': Moist, brown clay. !Groundwater interface located at 8'. ~PID -> 10-12.5': 0.0 ppm. 12.5-15': 0.0 ppm. I Soil sample collected from 5-7.5' at 15:15. iGW sample collected from 8-11' at 15:29. APPENDIX B ANALYTICAL DATA ., .MERICAN I,N&,LYTIC,t I L&BOR&TORIES NYSDOH NJDEP CTDOH PADEP 11418 NY050 PH-.0205 68-00573 Wednesday, March 28, 2007 Frank Castellano P.W. Grosser Consulting 630 Johnson Avenue Suite 7 Bohemia, NY 11716 TEL: (631) 589-6353 FAX (631) 589-8705 RE: Moores Lane Greenport, N.Y. Dear Frank Castellano: Order No.: 0703166 American Analytical Laboratories, LLC. received 14 sample(s) on 3/21/2007 for the analyses presented in the following report. Samples were analyzed in accordance with the test procedures documented on the chain of custody and detailed throughout the text of this report. The limits provided in the data package are analytical reporting limits and not Federal or Local mandated values to which the sample results should be compared. There were no problems with the analyses and all data for associated QC met laboratory specifications. If there are any exceptions a Case Narrative is provided in the report. If you have any questions regarding these tests results, please do not hesitate to call (631 ) 454-6100 or email me directly at lbeyer~american-analytical.com. Sincerely, Lori Beyer~~ Lab Director 56 TOLEDO STREET * FARMINGDALE, NEW YORK 11735 (631) 454-6100 * FAX: (631) 454-8027 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Project: Moores Lane Greenport, N.Y, Work Order Sample Summary Lab Order: 0703166 Lab Sumple ID Client Sample 0703166-01A No. 8 [10-12.5~] 0703166-02A No.5 [10-12.5'] 0703166-03A No. 4 [10-12.5'] 0703166-04A No. 3 [5-7.5'] 0703166-05A No. 2 [7.5-10'] 0703166-06A No. 1 [10-12.5'] 07031664)7A No. 6 [10-12.5'] 0703166-08A No. 8 [GW] 0703166-09A No. 5 [G W] 0703166-10A No. 4 [GW] 0703166-1 IA No. 3 [GW] 0703166-12A No. 2 [GW] 0703166-13A No. I [GW] 0703166-14A No. 6 [GW] Tag Number Date Collected Date Received 3/20/2007 10:03:00 AM 3/21/2007 3/20/2007 10:53:00 AM 3/2112007 3/20/2007 12:02:00 PM 3/21/2007 3/20/2007 12:49:00 PM 3/2112007 3/20/2007 1:15:00 PM 3/21/2007 3/20/2007 2:14:00 PM 3/21/2007 3/20/2007 2:40:00 PM 3/21/2007 3/20/2007 10:07:00 AM 3/21/2007 3/2012007 1 I:00:00 AM 3/21~007 3/20/2007 12:10:00 PM 3/21~007 3/20/2007 12:55:00 PM 3/21/*_007 3/20/2007 1:20:00 PM 3/21/2007 3/20/2007 2:10:00 PM 3/21/2007 3/20/2007 2:50:00 PM 3/21/2007 Page I of 1 NYSDOH 11418 ~ 56 TOLEDO STREET · FARMINGDALE, NEW YORK 11735 CTDOH PH-0205 ~LABORATOI~IES (631) 454-6100 · FAX (631) 454-8027 TAG # ! CCC NJDEP NY050 PADEP 68-573 CHAIN OF CUSTODY / REQUEST FOR ANALYSIS DOCUMENT CLIENT NAME/ADDRESS ~)L~, CONTACT: ~'V-~v'l~, ~G-i~,ll~*~"~O SAMPLER I$1GNATURE) S~PLE(S) ID" MATRIX TAINERS DATE/ SAMPLE fl- LOCATION TIME COOLER TEMPERATURE: ~PE G=G~B; C=COUPO~ITE, SS=SPLIT SPOON NORMAL~ STAT ~ RELINQUISHE~ BY (SIGNATURE) DAT~/p~ PRINTED NAME REC~E~GNATURE) D.E PRINTED NAME RELINQUlSHE~Y (SIGNATURE) DATE PRINTED ~ME REC NATURE) DATE PRINTED NAME TIME TIME WHITE-OFFICE / CANARY-LAB / PINK-SAMPLE CUSTODIAN / GOLDENROD-CLIEN' ==~=&MERIC&N NYSDOH 11418 E 56 TOLEDO STREET · FARMINGDALE, NEW YORK 11735 CTDOH PH-02O5 $ (631) 454-6100 · FAX (631) 454-8027 TAG # I COG NJDEP NY050 -- PADEP 68-573 CHAIN OF CUSTODY / REQUEST FOR ANALYSIS DOCUMENT SAMPLER (SIGN ~URE) ~7 ,~,~.. YES / NO ~¢'"~"'. "¢? I)~, ~s / NO SAMPLING ID ¢ MATRIX DATB SAMPLE ~ - LOCATION ~TILE VIAL TAINER8 TIME COOLE~ TEMPERATURE: ~T~I~ 8=SOIL; L=LIQUID; ~L=~LUDGE; A-AIR; W=WIPE; P=PAINT GHIP8; B=B~LK MATERIAL TURNAROUND REQUIRED: COMMENTS / INSTRUCTIONS ~PE G=G~B; C=COMPOSITE, SS=SPLIT SPOON NORMA~ STAT ~ BY RELINQUISHED BY (SIGNATURE) DAT~¢ PRINTED NAME RECEIVED BY ~B [SIGNATURE) DATE PRINTED NAME URE DATE . ~ DATE PRINTED NA~E~ RELINqUIShED BY (SI ) PRINTED NA~E RECEI~D ~Y ( ] NATUR ) TIME TIME WHITE-OFFICE / CANARY-LAB / PINK-SAMPLE CUSTODIAN / GOLDENROD-CLIENT American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 8 l10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 10:03:00 AM Lab]D: 0703166-01A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed MERCURY SW747'1B SW7471B Analyst: WN Mercury U 0.00954 mglKg-dry 1 3/23/2007 1:20;45 PM PERCENT MOISTURE D2216 Analyst: CM Percent Moisture 6.38 0 wt% 1 3/22/2007 TARGETANALYTE LIST METALS SW6010B SW3050A Analyst: JP Aluminum 5460 0.426 mg/Kg<Jry 1 3/23/2007 I:40:25 PM Antimony U 0.532 mg/Kg-d~ 1 3/23/2007 1;40:25 PM Arsenic 1.58 0.532 mglKg-dry 1 3/23/2007 1:40:25 PM Barium 18.9 0.426 mglKg~ry 1 3/23/2007 1:40:25 PM Beryllium U 0.426 mglKg<fPj I 3/23/2007 1:40:25 PM Cadmium 0.337 0.213 rog/Kg*dp/ 1 3/23/2007 1:40:25 PM Calcium 266 0.532 rog/Kg-dry 1 3/23/2007 1:40:25 PM Chromium 12.3 0.426 rog/Kg-dry I 312312007 1:40:25 PM Cobalt 2,38 0.426 mg/Kg~ry I 3/23/2007 1:40:25 PM Copper 4.99 0.426 mgtKg~l~j I 3/23/2007 1:40:25 PM Iron 4OB0 0.426 rog/Kg-dry 1 3/23/2007 1:40:25 PM Lead 12.9 0.319 mglKg<lty I 3/23/2007 1:40:25 PM Magnesium 810 0.426 mg/Kg~ry I 3~23~2007 1:40:25 PM Manganese 87.1 0.426 mglKg<by 1 3/23/2007 1:40:25 PM Nickel 4.64 0.426 mglKg<lty 1 3/23/2007 1:40:25 PM Potassium 634 2.13 mglKg-dry I 3/23/2007 1:40;25 PM Selenium U 0,532 rog/Kg-dry 1 3/23/2007 1:4025 PM Silver U 0.426 rog/Kg-dry I 3/23/2007 1:40:25 PM Sodium 133 1.28 mg/Kg-dry I 3/23/2007 1:40:25 PM Thallium U 0.426 mg/Kg~iry I 3/23/2007 1:40:25 PM Vanadium 11.7 0.426 rog/Kg-dry I 3/23/2007 1:40:25 PM Zinc 18.2 0.426 mglKg-dry 1 3/23/2007 1:40:25 PM SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3550A Analyst; PT 1,2,4-Trichlorobenzene U 130 pglKg-dry 1 3/23/2007 5:02:00 PM 1,2-Dichlorobenzene U 130 IJg/Kg-dry 1 3/23/2007 5:02:00 PM 1,3-Dichiorobenzene U 130 pg/Kg-dry 1 3/23/2007 5:02:00 PM 1,4-Dichlorobenzene U 130 pg/Kg-dry I 3/23/2007 5:02:00 PM 2,4,5-Trichiorophenol U 130 pg/Kg-dry I 3/2312007 5:02:00 PM 2,4,6-Trichlomphenol U 130 pg/Kg.-dry 1 3/23/2007 5:02:00 PM 2,4-Dichlemphenol U 130 pg/Kg-dry I 3/2312007 5:02;00 PM 2,4-Dimethylphenol U 130 pg/Kg~ry 1 3/23/2007 5:02:00 PM 2,4-Dinitrophenol U 130 pglKg-dry 1 3/23/2007 5:02:00 PM 2,4-DInitrotoluene U 130 pglKg-dry 1 3/23/2007 5:02:00 PM 2,~-Dinibotoluene U 130 pg/Kg-dry I 3/23/2007 5:02:00 PM B Analytc detected in the assodatcd Method Blank H Holding times far preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates the compotmd was analyzed for but not detecte E Value above quantitalloa range J Analyte detected below quantitation limits S Spike Recover' outside accepted recovery limits X Value exceeds Mr~ximum Cont'~inant Level Page I of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab 1D: P.W. Grosser Consulting 0703166 Moores Lane Greenport, N.Y. 0703166-01A Client Sample ID: No, 8 [10-t2.5'] Tag Number: Collection Date: 3/20/2007 10:03:00 AM Matrix: SelL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3550A 2-Chleronaphthalene U 130 I~glKg-d~y 2-Chlorophenol U 130 pg/Kg-dry 2-Methylnaphthalene U 13g p§lKg-dry 2-Methylphenol U 130 pglKg~ry 2-Nitroaniline U 130 tJg/Kg~ry 2-Nitrophenol U 130 pg/Kg-dry 3,3'-Dichlembe nzidine U 130 pg/Kg-dry 3+4-Methylphenol U 130 pg/Kg-dry 3-Nitroaniline U 130 pg/Kg-dry 4,6-Dinitro-2-mothylphen el U 130 pg/Kg-dry 4-Bromophenyl phenyl ether U 130 pg/Kg<iry 4-Chloro-3-methylphenol U '130 pg/Kg-dry 4-Chloroaniline U 130 pg/Kgq:iry 4-Chlorophanyl phenyl ether U 130 pg/Kg-dry 4-Nitroaniline U 130 pg/Kg-dry 4-Nitrophenel U 160 IJglKg-dry Acenaphthene U 130 pg/Kg-dry Acenaphthylene U 130 pglKg-d~y Aniline U 130 IJglKg<J~Y Anthracene U 130 ~glKg-dry Azobenzene U 130 pg/Kg-dry Benzidice U 130 pglKg-dry Benzo(a)anthracene U 130 pglKg-dPj Benzo(a)pyrene U 130 pglKg-dry Benzo(b)fluoranthene U 130 pig/Kg-dry Benzo(g,h.i)perylene U 130 gglKgq:by Benzo(k)fluoranthene U 13D pglKgq:lry Benzoic acid U 130 ~glKg-dry Benzyl alcohol U 130 IJglKg~ry Bi$(2-chlomethoxy)metha ne U 130 pglKg<lry Bis(2-chloroethyl)ether U 130 IJglKg-dry Bis(2-chlorolsopro pyl)ether U 130 pg/Kg-dry Bi$(2-et hylhexyl)phthalate U 130 pg/Kg~ry Butyl bctazyl phthalate U 130 pg/Kg*dly Carbazole U 130 IJg/Kg~ry ChPJsene U 130 iJg/Kg-dp] Dibenzo(a,h)aathrace ne U 130 pg/Kg-d~y Dibenzofumn U 130 pg/Kg-dry D[ethyl phthalate U 130 IJg/Kg~ry DF Date Analyzed Analyst: PT 3/23/2B07 5:02:00 PM 3/23/2007 5:02;00 PM 3/23/2007 5:02:00 PM 3/2312007 5:02:130 PM 3/2312007 5:02:00 PM 3/23/2007 5:02:00 PM 312312007 5:02:00 PM 312312007 5:02:00 PM 3/23/2007 5:02;00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PAl 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02;00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3~23~2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3123/2007 5:02:00 PM 312312007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3~23~2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/21t/2007 5:02:00 PM 3~3/2007 5:02:00 PM 3/23/2007 5:02:00 PM Value above quanLitation range Analyte dct¢cted below quantitatiea limits Spike Recovery outside accepted recovery limits Vala~ enc¢¢ds Maximum Contaminant Level Page 2 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W, Grosset Consuhing Client Sample ID: No. 8 [I0-I2.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 10:03:00 AM Lab ID: 0703166-01A Matrix: SOIL Analyses Result Limil Qual Units DF Date Analyzed SEMIVOLATILE SW-846 METHOD 8270 5W82700 SW3550A Dimethyr phthalate U 130 ~JglKg-d~y Di-n-butyl phthalate U 130 IJg/Kg-dP/ Di-n..octyl phthalate U 130 Fluoranthene U 130 pg/Kg~l~y Fluorene U 130 pg/Kg-d~y Hexachlorobenzene U 130 pg/Kg-d,'y Hexachlm-obutadie ne U 130 pg/Kg~y Hexachlomcyclopentadie ne U 160 pg/Kg~iy Hexachloroethane U 130 I~g/Kg-dry Indeno(1,2,3-c,d)pyrene U 130 IJg/Kg-dry Isophorone U 130 pg/Kg~ry Naphthalene U 130 pglKg-dry Nitrobenzene U 130 pglKg-dry N~litrosodimethylamine U 130 pg/Kg-dry N-Nitrosodi-n-propyramine U 130 pg/Kg-dry N-Nitrosodiphenylamine U 130 I~:j/Kg-dfy Pentachlorophenol U 160 pg/Kg.dry Phenanthrene U 130 pg/Kg~ry Phenol U 130 pglKg~ry Pyrene U 130 pglKg-dry Pyddine U 130 Hg/Kg-d[y Sum 2,4,6-Tribramephenol 62.2 22.124 %REC Surr: 2-Fluorobiphenyl 62.4 27-119 %REC Sum 2~luorophencl 90.5 21-123 %REC Suw. 4-Terphenyl-d 14 59.5 28-126 %REC Surf: Nitmbenzene-d5 64.9 21-118 %REC Sum Phenol-d6 86.5 18-129 %REC VOLATILE SW-846 METHOD 8260 SW82600 1,1,1,2-Tetrachloroethane U 5.2 [Jg/Kg-dry 1,1,1 -Tdchloroethane U 5.2 pg/Kg-dry 1,1.2,2-Tat rach;oroetha ne U 5.2 pgfKg-dry 1,1,2-Trichloro-1,2,2-trifluoroethane U 5.2 IJglKg~ry 1,1,2~Trichloroethane U 5.2 pg/Kg-dry 1,1.Dichloroethane U 5.2 pg/Kg.dry 1,1 -Dichloroethene U 5.2 ~g/Kg-dry 1,1 -Dichloropropene U 8.2 ~Jg/Kg-dry 1,2,3-Trichlombenzene U 5.2 pglKg-d~j 1,2,3-Trichlompropane U 5.2 pg/Kg-dry 1,2,4,5-Tetramet hylbenzene U 5.2 pg/Kg~ry Analyst: PT 3/2312007 5:02:00 PM 3/23/2007 5:02:00 PM 3123/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/2312007 5:02:00 PM 312312007 5:02:00 PM 312312007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2D07 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/2312007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 6:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:02:00 PM 3/23/2007 5:92:00 PM 3/23/2007 5:02:00 PM 3123/2007 5:02:00 PM Analyst: LD$ 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:56:00 PM 3121/2007 2:56:(30 PM 3/21/20n7 2:58:00 PM Qualificrs: B Ana[ytc detected in thc associated Method Blank Holding times for preparation o~ analysis exceeded ND Not Detected at the R~po~ing Limit U Indicates the compvund was ~maly;,.c d for but not dcteete E Value above quantitation range J Analyte detected below qum~titation limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 3 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenpo~,N.Y. 0703166-01A Client Sample ID: No. 8 [10~12.5'] Tag Number: Collection Date: 3~0/2007 10:03:00 AM Matrix: SOIL VOLATILE SW-846 METHOD 8260 1,2,4-Trichlo robenzene 1,2,4-Trimethy~be nzene 1,2-Dibmmo-3-chioropropane 1,2-Dibmmoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Drchloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1,3-dichlorepropane 1,4-Dichlombenzene 2,2-DIchloropropane 2-Chlomethyl vinyl ether 2-Chlorotoluene 2-Hexanone 2-Propanol 4-Chlorotoluene 4-[sopropyltoluene 4-Methyl-2-pentanone Acetone Acrolein Acrylonitffie Bromochloromethane Bromoform Carbon disuffide Carbon tetmchloride Chlorobenzene Chlorodifluoremethane Chleroethane Chloroform Ch~oromethane cis-.1,2-Dichloroethene cis-1,3-Dichlompropene Result Limit Qual Units SW82605 U 5.2 lag/Kg-dry U 5.2 pg/Kg-dry U 5.2 pglKg-dry U 5.2 pglKg-dry U 5.2 lag/Kg-dry U 5.2 ug/Kg-dry U 5.2 pg/Kg<lry U 5.2 pglKg-dry U 5.2 pglKg-dry U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry U 5.2 pg/Kg-d~y U 5.2 lag/Kg-dr/ U 5.2 pglKg~ry U 5.2 pglKg-dr~ U 52 t~glKg-thy U 5.2 IJglKg<lry U 5.2 pcJIKg-dry U 5.2 pg/Kg-dry U 5.2 pglKg-dry U 26 [ag/Kg~ry U 5.2 pglKg-dry U 5.2 pglKg-dry U 5.2 Hg/Kg-d~t U 5.2 ~JglK§-dry U 5.2 Hg/Kg-dry U 5.2 tag/Kg-dry U 5.2 ug/Kg-dry U 5.2 IJglKg-dry U 5.2 ~glKg-d~J U 5.2 lag/Kg-dry U 5.2 pg/Kg-clry U 5.2 pglKg-dry U 5.2 pglKg<lry U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry DF Date Analyzed Analyst: LD$ 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2807 2:58;00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 312112007 2:58:00 PM 3/21/2007 2:58:00 PM 312112007 2:58:00 PM 3/21/2007 2:55:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3121/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2;58:00 PM 312112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 312112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 312112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not De~cted at the Reporting Limit U Indicates tile compound w~s anal~rz~d for but not E Value above qunntitation range J Analytc dglected below quantimfion limiB S Spike Recovery outside accepted recovery limiL~ X Value exceeds Maximum Contaminant Level Page 4 of 70 American Analytical Laboratories, LLC. Date: 28-Maro07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 8 [10-12.Y] Lab Order: 0703166 Tag Number: Project: Mourns Lane Greenport, N.Y. Collection Date: 3/20/2007 10:03:00AM Lab ID: 0703166-0IA Matrtx: SOIL Result Limit Qual Units DF Date Analyzed Analyses VOLATILE SW-846 METHOD 8260 Dibromomethane Dichlorodlfluorometha ne Dlisopropyl ether Ethanol Ethyl acetate Ethylbenzene Freor~114 Hexachlorobutadiene Isopropyl acetate Isopropylbenzena m,p-Xylene Methyl tort-butyl ether Methylene chlo~de n-Amyl acetate Naphthalene n-Butyl acetate n-Butylbenzene n-Propyl acetate n-Propylbenzene o-Xylene p. Dlethylbenzene I>.Ethyltoluene sec-Bu[,jlbenzene Styrene t-Butyl alcohol tert-Butylbenzene Tetrachlotoethene Toluene trans-1,2-Dichloroethene trans-1,3-Dichloropropene Trichloroethene TdcMorofluoromethane Vinyl acetate Vinyl chlorMe Sum 4-Bromofluorobenznne Sum Dibrornofluoromethane Sum Toluene-d8 SW82600 U 5.2 pg/Kg-dry U 5.2 k~g/Kg~ry U 5.2 pg/Kg-dry U 26 pg/Kg~hy U 5.2 pg/Kg-d~y U 5.2 pg/Kg-dry U 5.2 pglKg-dry U 5.2 pg/Kg-dry U 5.2 IJg/Kg-dry U 5.2 IJg/Kg-dty U 10 IJg/Kg-dry U 5,2 pglKg-dly U 5.2 p§lKg-dry U 5.2 IJglKg-dry U 5,2 pg/Kg-dPy U 5.2 pglKg-d~y U 5.2 pg/Kg*dp/ U 5.2 IJg/Kg-dG' U 5,2 ~glKg-d~y U 5.2 pgtKgqJry U 5.2 IJglKg-dry U 5,2 IJg/Kg-dry U 5,2 IJg/Kgq:lry U 5.2 pg/Kgq:hy U 5.2 pg/Kg-dry U 5.2 pg/Kg-d~ U 5.2 pg/Kg-dry U 5.2 pg/Kg-dry U 5.2 IJg/Kg~ly U 5.2 pglKg-dry U 5.2 pg/Kg~ry U 5.2 pg/Kg-,d~y U 5.2 pg/Kg-dly U 5.2 IlglKgq~y 106 61-133 %REC 106 61-139 %REC 93,5 57-131 %REC Analyst: LDS 3/21/2007 2:58:013 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3121/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2t/2007 2:5fi:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/20fi7 2:58:00 PM 3/2112007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/21/2007 2:58:00 PM 3/2112007 2:55:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates the comljound was anal~zed for but nat detecto E Value above quaufitatinn range J Analyt¢ detected bcinw qumafitntion limils Page 5 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenpo~,N.Y. 0703166-02A Client Sample ID: No.5 [I0-12.5'] Tag Number: Collection Date: 3/20~007 10:53:00AM Matrix: SOIL Analyses Result Limit Qual Units MERCURY SW7471 I~ Mercury U 0,0107 PERCENT MOISTURE 02216 Percent Moisture 7.50 0 TARGET ANALYTE LIST METALS SW60'IOB Aluminum 1580 0.419 Antimony U 0.524 Arsenic U 0.524 Bariuro 7.42 0.419 Beryllium U 0.419 Cadroluro U 0.210 Calcium 133 0,524 Chromiuro 6.66 0.419 Cobalt U 0,419 Copper 1.76 0.419 Iron 1810 0.419 Lead 1,55 0.314 Magnesium 225 0.419 Manganese 29.0 0.419 Nickel 1.60 0.419 Potassium 231 2.10 Saleniuro U 0.524 Silver U 0.419 Sodium 78.0 1.26 Thalliuro U 0.410 Vanadium 3.84 0.419 Zinc 5.11 0.419 SEMIVOLATILE SW-846 METNOD 8270 SW82700 1,2,4-Tdchlo robenzene U 130 1,2.Dichlorobenzene U 130 1,3~DIchlombenze ne U 130 1,4-Dichlorobenzene U 130 2,4, 5-T~'ichlotop he n el U 130 2,4.6-Tfichlorophen el U 130 2,4-Dichlorophenol U 130 2,4-Dimethylphenol U 130 2,4-Dinitrophenel U 130 2,4-Dinitrotoluene U 130 2,6-Dinitrotoluene U 130 SW7471 B mg/Kg-dry wt% SW3050A rog/Kg-dry rog/Kg-dry mg/Kg-dPJ mglKg-dry rog/Kg-dry mglKgdry mg/Kg-d~7 rog/Kg-dry rog/Kg.-d~ rog/Kg-dry rog/Kg-dry mg/Kg-dry mg/Kg-dry mg/'Kg-d~J mg/Kg-d[y rog/Kg-dry rog/Kg..dt7 rog/Kg-dry rog/Kg-d~y rog/Kg-dry mg/Kg-d~ rog/Kg-dry SW355OA pgJKg-dry pglKg~P] pg/Kg-dry pglKg-dry pg/Kg~ pglKg-dry pg/Kg-dP/ pg/Kg-dry pg/Kg~lry ~lg/Kg.-d r~ pg/Kg-dry DF Date Analyzed Analyst: WN 3~23~2007 1:27:11 PM Analyst: CM 3/22/2007 Analyst: JP 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:t6:08 PM 3/23/2007 2:16:05 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:05 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:09 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:00 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:16:08 PM 3/23/2007 2:19:08 PM Analyst: PT 3/2312007 5:30:00 PM 3/2312007 5:30:00 PM 3/23/2007 5:30:00 PM 3/2312007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/2312007 5:30:.00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2067 5:30:00 PM Page 6 of TO American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Gmenpo~, N.Y. 0703166-02A Client SamplelD: No.5 [10-12.Y] Tag Number: Collection Date: 3/20/2007 10:53:00 AM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW$2700 SW3550A 2-Chloronaphthalene U 130 pg/Kg-dry 2-Chlorophenol U 130 IJg/Kg-dry 2-Methylnaphthalene U 130 IJg/Kg-dry 2-Methylphenol U 130 pg/Kg-dry 2-Nitrceniline U 130 lag/Kg-d~y 2-Nitrophenol U 130 pg/Kg-dry 3,3'-Dichlorobenzidine U 130 pg/Kg-d~J 3+4-Methylphenol U t 30 lag/Kg-dry 3-Nitroaniline U t30 ~g/Kg-d[Y 4,6-Dinitro-2-met hylphenol U 130 I~JIKg-dry 4-Bmmophenyl phenyl ether U 130 pg/Kg-dry 4-Ch[oro-3-rnethylphenoi U 130 pglKg-dry 4-Chlomaniline U 130 pg/Kg-dry 4-Chlorophenyl phenyl ether U 130 I~g/Kg-dry 4-Nitroaniline U 130 lag/Kg-dry 4-Nitrephenol U 160 pg/Kg-dry Acenaphthene U 130 pg/Kg-diY Acenaphthylene U 130 pg/Kg-d~/ Aniline U 130 pglKg.dry Anthracene U 130 pg/Kg-dry Azobenzene U 130 pg/Kg-dry Benzidine U 130 pglKg-dry Benzo(a)anthracene U 130 pg/Kg-dry Benzo(a)pyrene U 130 pg/Kg-dry Benzo(b)fluoranthene U 130 pg/Kg-dry Benzo(g,h,i)pePJlene U 130 pglKg<hy Beozo(k)fluoranthene U 130 pg/Kg-dry Benzoic acid U '130 lag/Kg-dry Benzyl alcohol U 130 pg/Kg-dry Bis(2-cMomethoxy}metha ne U 130 pgfKg-dry Bis{2-chlorcethyl)ether U 130 pg/Kg-dry Bis(2-chlemiaopropyl)ether U 130 pglKg-dry Bis(2-ethylhexyl}phthalate U 130 pglKg-dry Butyl benzyl phthalate U 130 pg/Kg-dry Carbazole U 130 pglKg-dry Chrysene U 130 pg/Kg-dry Dibenzo(a,h)anthracene U 130 gglKg-dry Dibenzofumn U 130 gg/Kg-dry Diethyl phths[atu U 130 pg/Kg-dry DF Date Analyzed Analyst: PT 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23f2007 5:30:00 PM 3123/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30;00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3~23~2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/2312007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/200'/' 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM Qualifiers: E Value above quaatitation range J Analyu: detected below quantitation limits S Spike Recovcn7 outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 7 of 70 American Analytical Laboratories, LLC. Date: 28-1VIar-07 CLIENT: P.W. Grosset Consulting Client SampleID: No.5 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Mooms Lane Greenporic, N.Y. Collection Date: 3/20/2007 10:53:00 AM Lab ID: 0703166-02A Matrix: SOIL Analyses Result Units DF Date Analyzed Limit Qual SEMIVOLATILE 8W-846 METHOD 8270 SW82700 SW3550A Dimethyl phthalate U 130 pg/Kg-dry Di-n-butyl phthalate U 130 pgtKg-dry Di-n-octyl phthalate U 130 pglKg-dry Fluoranthene U 130 ~g/Kg-dry Fluorene U 130 ~glKg-dry Hexachlorobenzene U 130 pglKg.d~t Hexachinmbutadiene U 130 ~JglKgq~ry Hexachlorocyclopent adJene U 180 pg/Kg-dry Hexachloroethane U 130 pg/Kg-dry Inde no( 1,2,3-c,d)pyrene U 130 IJglKg~ry Isophorone U t 30 rog/Kg-dry Naphthalene U 130 I~g/Kg-dry NRrobenzene U 130 pglKg-dry N.Nitrosodimethylamine U 130 pg/Kg.dry N-Nitrosodi-n-propylam[ne U 130 gglKg-dry N-Nitrosadiphenylamine U 130 rog/Kg-dry Pentachinrophenol U 160 pglKg~ry Phenanthrene U 130 roglKg~ry Phenol U 130 rog/Kg.dry Pyrene U 130 I~g/Kg-dry Pyddine U 130 pg/Kg-dry Surr: 2,4,6-Tdbmmophenol 68.0 22-124 %REC Surf: 2-Fluomb[phenyl 73.7 27-119 %REC Surf: 2-Fluo/ophenol 49.1 21-123 %REC Surf: 4-Terphanyl-d14 70.6 28-125 %REC Sum Nitrobenzene.d5 65.2 21-118 %REC Surf: Phenol-d6 63.0 1B-129 %REC VOLATILE SW-846 METHOD 8260 $W82600 1,1,1,2-Tetrachl0roethane U 5.0 pg/Kg-dry 1,1,1-Trichthroethane U 5.0 pglKg.dry 1,1,2,2-Tot rachinmethane U 5.0 ~Jg/Kg-dry 1,1,2-THchloro-1.2,2-trifluoroethane U 5.0 IJg/Kg.dry 1,1,2-Trichlornetha ne U 5,0 }~g/Kg-d~y 1,1-Dichlomethane U 5.0 pg/Kg-dry 1,1-D[chloroethene U 5.0 IJg/Kg-dry 1,1 -Dichloropmpene U 5.0 pg/Kg.dry 1,2.3-Tdchlorobenzene U 5,0 rog/Kg.dry 1,2,3-Tdchloropropane U 5.0 rog/Kg-dry 1,2,4,5-Tetramethylbenzene U 5.0 IJg/Kg-dry Analyst: PT 3123/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:50:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3123/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30:00 PM 3/23/2007 5:30;00 PM 3/23/2007 5:30:00 PM Analyst: LD$ 3/2112007 5:21:00 PM 3/21/2007 5:21:00 PM 3/2112007 5:21:00 PM 3/21/2007 5:21:00 PM 3121/2007 5:21:00 PM 3/2112007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3121/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM Qualifiers: E Annly~e detected in the ~$ociated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U indicates thc compound w~ analyzed for hut not detecto Page 8 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moores Lane Greenpo~, N.Y. 0703166-02A Client Sample ID: TagNumber: Collection Date: Matrix: No.5 [10-12.5'] 3/20/2007 10:53:00 AM SOIL Analyses Result VOLATILE 8W-846 METHOD 8260 1,2,4-Trichlorobenzene U 1,2,4-Tdmethylbenzene U 1,2-DIbromo-3.chlo ropropane U 1,2-D[bromoethane U 1,2-Dichtorobenzene U 1,2-Dichiomethane U 1,2-Dichloropropane U 1,3,5-Tr[methylbenzene U 1,3-Dichlorobenzene U 1.3-dichioroprepane U 1,4--Dichlorubenzene U 2,2-Diohloropropane U 2-Butanone U 2.Chlemethyl vinyl ether U 2-Chlorotoluene U 2-Hexanone U 2~Propanol U 4.Chlamtoluene U 4-1sopropyltoluene U 4-Methyl-2-pentanone U Acetone U Acroleln U Ac~71onitrile U Benzene U Bromobenzene U Bromochlommethane U Bmmodichloromethane U Bromoform U Bromomethane U Carbon disulfide U Carbon tetrachloride U Chlombenzene U Chlorodifluoromethane U Chlomethane U Chloroform U Chlommethane U cis-1,2-Dichloroethene U cis-1,3.Dichloropropene U Dibromochloromethane U Limit Qual Units DF Date Analyzed SW82600 Analyst: LDS 5.0 pg/Kg-dry 1 3121/2007 5:21:00 PM 5.0 pglKg-dp/ 1 312112007 5:21:00 PM 5.0 pglKg-dry I 3/21/2007 5:21:00 PM 5.0 pg/Kg-cky 1 3/2112007 5:21:00 PM 5.0 pg/Kg-dry 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-dry I 3/21/2007 5:21:00 PM 5.0 pg/Kg-dp/ 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-dry I 3/21/2007 5:21:00 PM 5.0 pg/Kg~ry 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-dty I 3/21/2007 5:21:00 PM 5.0 iJglKg-d~' I 312112007 5:21:00 PM 5.0 pg/Kg-dry I 3t21/2007 5:21:00 PM 5.0 pg/Kg<l~ 1 3/21/2007 5:21:00 PM 5.0 iJg/Kg~JrY 1 3/2112007 5:21:00 PM 5.0 IJg/Kg-dPJ I 3/21/2007 5:21:00 PM 5.0 pglKg-dry I 3/21/2007 5:21:00 PM 50 pglKg-d[y 1 3/2112007 5:21:00 PM 5.0 IJg.q(g-dPJ 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-dry I 3/21/2007 5:21:00 PM 5.0 pg/l(g~Jry 1 3/2112007 5:21:00 PM 5.0 pg/Kg-dP~ 1 3/21/2007 5:21:00 PM 25 pg/Kg-dr7 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-d~y I 3/21/2007 5:21:00 PM 5.0 IJ g/Kg-d~J I 3/21/2007 5:21:00 PM 5.0 pg/Kg-d~ I 3/21/2007 5:21:00 PM 5.0 pglKg-dry I 3/21/2007 5:21:00 PM 5.0 pglKg-dpj 1 3/21 ~2007 5:21:00 PM 5.0 pglKg-d~7 I 3/2112007 5:21:00 PM 5.0 iJg/Kg-dry t 3/21/2007 5:21:00 PM 5.0 pg/Kg-d~y 1 3121/2007 5:21:00 PM 5.0 pg/Kg-dP/ t 3/21/2007 5:21:00 PM 5~o }JglKg..dry I 3/21/2007 5:21:00 PM 5.0 pg/Kg-dry I 3/21/2007 5:21:00 PM 5.0 pglKg..dty 1 3/2112007 5:21:00 PM 5.0 pglKg-d~y 1 3/2112007 5:21:00 PM 5.0 pg/Kg-dry 1 3/2112007 5:21:00 PM 5.0 pg/Kg-dry 1 3/21/2007 5:21:00 PM 5.0 IJg/Kg-d~J 1 3/21/2007 5:21:00 PM 5.0 pg/Kg-dry I 3/21/2007 5:21:00 PM Qualifiers: B Analytc dct¢clcd in Ibc associatcd Method Blank H Holding times t'or p~paration or analysis exceeded ND Not Detected at thc Reporting Limit U Indicalc-s d~e compound w~ analyzed rot but not detcctc Page 9 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moores Lane Greenport, N.Y. 0703166-02A Client Sample ID: No.5 [10-12.5'] Tag Number: Collection Date: 3/20/2007 10:53:00 AM Matrix: SelL Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82600 Dibromomethane U 5.0 pg/Kg-dry Dichlorodifluoremeth eno U 5.0 pglKg-thy Di[sopropyl ether U 5.0 IJg/Kg-d ry Ethanol U 25 lag/Kg-dry EthyJ acetate U 5.0 pg/Kg-dry Ethylbenzene U 5.0 lag/Kg-dry Freon-114 U 5.0 pg/Kg-dry Hexachlorobutadlene U 5.0 lag/Kg-dry IsopropyJ acetate U 5.0 pg/Kg-dry Isopropylbenzene U 5.0 pg/Kg-dry m,p-Xylene U 10 pg/Kg-dry Methyl ter[-butyl ether U 5.0 lag/Kg-dry Methylene chloride U 5.0 lag/Kg-di3, n-Amyl acetate U 5.0 pg/Kg-dry Naphthalene U 5.D pg/gg-dry n-Butyl acetate U 5.0 lag/Kg-dry n-Buiylbenzene U 5.0 I~glKg-dry n-Propyl acetate U 5.0 pg/Kg-dry n~Propylbertzene U 5.0 pg/Kg-dry o-Xylene U 5.0 pg/Kg-dry p-Dlethylbenzene U 5.0 la§/Kg-dry p-Ethylthluene U 5.0 pg/Kg-dpj sec-Butylber~zene U 5.0 lag/Kg-dry Styrene U 5.0 gg/Kg-dry t-Butyl alcohol U 5.0 pg/Kg.dry tert-Butylbenzene U 5,0 t~g/Kg-dry Tetrachloroethene U 5.0 pg/Kg-dry Toluene U 5.0 pg/Kg-dry tran$-1,2-Dichloroethene U 5.0 lag/Kg-dry frans-1,3-DichJoropropene U 5.0 pg/Kg-dry Trfchloroethene U 5.0 lag/Kg-dry Ttichlorofluoromethane U 5.0 pg/Kg-dry Vinyl acetate U 5.0 pglKg-dry V~nyl chloride U 5.0 pglKg-dry Sum 4-Bromofluorobenzene 95.2 61-133 %REC Sum Dlbromofluoromethane 105 61-139 %REC Surf: Toluene-dB 94.9 57-131 %REC Units DF Date Analyzed Analyst: LDS 3/21/2007 5:21:00 PM 3/21/2007 5;21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/20{37 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/2112007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/20{37 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/20{37 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21;00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:0{3 PM 3/2112007 5:21:00 PM 3/21/2007 5:21:00 PM 3121/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2{307 5:21:00 PM 3/21/2007 5:21:00 PM 3/2t/2007 5:21:00 PM 3/21/2007 5:21;00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM 3/21/2007 5:21:00 PM Qualifle~: Value above quantitation range Analy~e d¢tecle~ below quantitation limits Spike Recovery outside accepted recovery limits Valu~ exceeds M oximum Conlaminant L~wl Page 10 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: P.W. Grosset Censulting Client Sample ID: No. 4 [10-12.5'] Lab Order: 0703166 Tag Number: Project: MooresLane Greenport, N.Y. Collection Data: 3/20/2007 12:02:00 PM Lab ID: 0703166-03A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed MERCURY 5W747~1S SW747'1B Analyst: WN Mercury U 0.0112 rag/Kg-dry 1 3/23/2007 1:29:20 PM PERCENT MOISTURE 02216 Analyst: CM Percent Moisture 15.5 0 wt% I 3/22/2007 TARGET ANALYTE LIST METALS SW60'IOB SW3050A Analyst: JP Aluminum 12000 4.73 mg/Kg.d~y 10 3/23/2007 3:03:59 PM Antimony U 9.592 rag/Kg-dry I 3/23/2007 2:18:09 PM Arsenic 2.51 0.592 mg/Kg~p/ I 3/23/2007 2:18:09 PM Barlura 40.7 0.473 mg/Kg~dry I 312312007 2:18:09 PM Beryllium U 0.473 rag/Kg.dry 1 3/2312007 2:18:09 PM Cadmium 0.286 0.237 rag/Kg-dry I 3/23/2007 2:18;09 PM Calcium 337 0.592 mg/Kg~y I 3/23/2007 2:18:09 PM Chroralura 15.0 0.473 rag/Kg-dry 1 3/23/2007 2:18:09 PM Cobalt U 0.473 rag/Kg-dry 1 3/23/2007 2:18:00 PM Copper 9.65 0.473 mg/Kg-d~J I 3/23/2007 2:18:09 PM Iran 8700 4.73 mg/Kg-dry 10 3/23/2007 3:03:59 PM Lead 12.7 0.355 rag/Kg-dry 1 3/23/2007 2:1S:09 PM Magnesium 2010 0.473 rag/Kg-dry 1 3/23/2007 2:19:09 PM Manganese 88.3 0.473 rag/Kg-ch7 I 3/23/2007 2;18;09 PM Nickel 8.03 0.473 mg/Kg-dry I 3/23/2007 2:18:09 PM Potassiura 1160 2.37 rag/Kg-dry 1 3/23/2007 2:18:00 PM Seleniura U 0.592 mglKg-dry 1 3/2312007 2:18:00 PM Silver U 0.473 mg/Kg-d~ 1 3t2312007 2:18:09 PM Sodium 207 1.42 rog/Kg-dry I 3/23/2007 2:18:09 PM Thalliura U 0.473 rog/Kg-dry 1 3/23/2007 2:15:09 PM Vanadiura 30.0 0.473 rag/Kg-dry I 3/23/2007 2:18:09 PM Zinc 27.7 0.473 rag/Kg-dry I 3/23/2007 2:15:09 PM SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3850A Analyst: PT 1,2,4-Tdchlorobenzene U 140 pg/Kg-d~/ 1 3/23/2007 5:58:00 PM 1,2-Dichlorobenzene U t40 pg~Kg~P/ 1 3/23/2007 5:58;00 PM 1,3-Dichlombenzene U 140 pg/Eg-dry 1 3/23/2007 5:58:00 PM 1,4--Dtchlarobenzene U 140 ug/Kg-dry 1 3123/2007 5:58:00 PM 2,4,5-Tdchlorophenol U 140 Hg/Kg-dry 1 3/23/2007 5:58:00 PM 2,4,6-THchlamphenol U 140 pglKg-dry I 3/23/2007 5:55:00 PM 2,4-Dichlorophenol U 140 pglKg-dry I 3/23/2007 5:58:00 PM 2,4--Diraethylphenol U 140 pg/Kg-dry 1 3/23/2007 5:58:00 PM 2,4-Dinitmphenol U 140 pg/Kg~lnj I 3/23/2007 5;58:00 PM 2,4-Dinitratoluene U 140 IJglKg-dry 1 3/23/2007 5:58:00 PM 2,6-DInitrotaluene U 140 pglKg-dry I 3/23/2007 5:58:00 PM Qualifiers: B Analytc detected in thc a~sociatcd Method Blank H Holding times For prcparntion or analysis cxccedcd ND Not Detected at thc Reporting Limit U Indicates the compound wa~ analyzed for but not detecto E Value abovc quandtalioa tm]ge J Analy~e dctectcd below quaatitation limils S Spike Recovery outsld¢ accepted recovery I/mlts X Value exceeds Maximum Contaminant Level Page 11 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P~W~ Grosset Consulting Client Sample ID: No. 4 Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N~Y. Collection Date: ~/20/2007 12:02:00 PM Lab ID: 0703166-03A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3550A 2-Chloronaphthalene U 140 pg/Kg-dry 2-Chlorophenol U 140 pg/Kg-dry 2-Methylnaphthalene U 140 pg/Kg-dry 2-Methyrphenol U 140 pg/Kg~7 2-NRroaniline U 140 pg/Kg-dry 2-NRrophenol U 140 pglKg.dty 3,3'-Dichlorobenzidine U 140 pgtKg-dry 3+4-Methylphenol U 140 pg/Kg-dry 3-Nitroaniline U 140 pg/Kg~l~j 4.6-Oinitm-2~net hylphenol U 140 pg/Kg-d~j 4-Bromophenyl phenyl ether U 140 pg/Kg-d~y 4-C hlom-3-methylpheno] U 140 pg/Kg~ry 4-Chlomanlline U 140 pg/Kg-dpj 4-Chlorophenyl phenyl ether U 140 pg/Kg-dry 4-Nitmaniline U 140 pg/Kg-dry 4-Nitmphenol U 180 pglKg-dry Acenaphthene U 140 pglKg-dry Acenaphthylene U 140 IJg/Kg-dry Aniline U 140 pg/Kg-dry Anthracene U 140 IJg/Kg-dry Azobenzene U 140 pg/Kg-dry Benzidlne U 140 gg/Kg-dry Benzo(a)anthracene U 140 pglKg~dry Benzo(a)pyreee U 140 pglKg-d~ Benzo(b)flaoranthenu U 140 pglKg-dry Benzo(g,h.0puP/lene U 140 pg/Kg-dry Benzo(k)fluoranthene U 140 pglKg-dry Benzoic acid U 140 pgtKg-dt~ Benzyl alcohol U 140 i.tg/Kg-dPJ Bis(2-cMoroethoxy)methane U 140 pglKg-dry Bis(2-chlomethyl)ether U 140 pg/Kg-dry Bis(2-chlomisupropy])uther U 140 pg/Kg..d~ Bis(2-ethylhexyl)phthalate U 140 pg/Kg~ry Butyl benzyl phthalate U 140 gg/Kg-d~y Carbazole U 140 pg/Kg<lry Chrysene U 140 pg/Kg-dry Dibenzo(a,h)anthmcene U 140 ~ag/Kg-d~7 Dthenzofuran U 140 pglKg-dPJ Diethyl phthalate U 140 pg/Kg-dry Analyst: PT 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:50:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:55:00 PM 3/23/2007 5:58:00 PM 3123/2007 5;58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:55:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:55:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2807 5:58:00 PM 3123/2007 5:58;00 PM 3/2312007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58.~0 PM 312312007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2807 5:58:00 PM 3/23/2007 5:58:00 PM B Anal)~e date=ted in the associated Method Blank H Holding times for preparation or analysis cxcccdsd ND Not Detected al the Reporting Limit U ]ndicnt~ the compound was an~13rzed for but not detecto E Value above quantitation ~ge J Anatyte dstectcd below quanlilalion limits S Spike Recove~ outside accepted recovevj limils X Value exceeds M ~ximum Contaminant Level Page 12 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 4 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 12:02:00 PM Lab 1D: 0703166-03A Matrix: SOIL Result Units DF Date Analyzed Analyses SEMIVOLATILE SW-846 METHOD 8270 Dimethy[ phthatate DLn-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopent adiene Hexachloreethane Indeno(1,2,3-c,d)pyrene [sophorone Naphthalene Nitrobenzene N-Nit rosodimet hylamine N-Nttrosodi-n~ropylarnine N-Nitrosodiphenylarnine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine Surr: 2,4,6-Tribromophenol Sur~ 2-Fluorobiphenyl Surf: 2-Fluorophenol Surf: 4-Terphenyl~14 Surf: Nittobenzene-d5 Sum Phenol-d6 VOLATILE SW-846 METHOD 8260 1,1,1,2-Tetrachloroethane 1,1,1-Trichleroethane 1,1,2,2-Tefaachloroeth ane 1,1,2-Trichlor~l ,2,2-tdfluoroethane 1,1,2-Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3--Trichlo robe r,z_en e 1,2,3-Trlchloropropane 1,2,4,5-Telramethylbenzene Analyst: PT 3/23/2007 5:58:00 PM 3/23/2007 5:55:00 PM 3/23/2007 5:58:00 PM 3/2312007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3123/2007 5:58:00 PM 3~23~2007 5:58:00 PM 3/23/20(37 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:56:00 PM 3/2312007 5:55:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:s8:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:56:00 PM 3/23/2007 5:58:00 PM 3/2312007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2007 5:58:00 PM 3/23/2067 5:55:00 PM 3/23/2007 5;55:00 PM Analyst: LDS U U U U U U U U U U U U U U U U U U U U U 63.5 62.9 86.3 67.9 60.4 85.4 SW3550A p§lKg-dry pglKg-cily pg/Kg-dry Hg/Kg-dry pg/Kg-dry pg/Kg<lry ;~g/Kg~ty pg/Kg-dry pg/Kg-dly I~g/Kg-dry IJg/Kg-dry pg/Kg-dry pglKg-dpJ pg/Kg-dry pg/Kg-d~ pg/Kg-dry pg/Kg-dP/ pg~Kg-dry pg/Kg~J pglKg-cky pg/Kg~' %REC %REC %REC %REC %REC %REC Limit Qual SW8270D 140 140 140 140 140 140 146 180 140 140 140 140 140 140 140 140 180 140 140 140 140 22-124 27-119 21-123 28-126 2%118 18-129 SW82608 5.6 5.6 5.6 5.6 5.6 5.6 5.6 5.6 5.6 5.6 5.8 U pg/Kg-dry I 3/21/2007 5:08:00 PM U pg/Kg-dry 1 3/21/2007 6:08:00 PM U pg/Kg,.clry 1 3/21/2007 6:05;00 PM U pg/Kg-dry 1 3/21/2007 6:08:00 PM U I~g/Kg~y I 3/21/2007 8:08:00 PM U pg/Kg-dq, 1 3/21/2007 5:08:00 PM U pg/Kg~ry 1 3/21/2(307 6:08:00 PM U pg/Kg-dry 1 3/21/2007 6:05:00 PM U pg/Kg*d~y 1 3/2112007 6:05:00 PM U pglKg..dfy 1 3/21/2007 6:06:00 PM U pg/Kg-dt7 I 3/21/2007 6:08:00 PM Value above quantitadon range Analytc tlctectcd below tluaatitation limits Spike Recovery outside accepled recovery limits Value exceeds MtJ.xlmura Contaminant Level Page 13 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 4 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Colleclion Date: 3/20/2007 12:02:00 PM Lab 16: 0703166-03A Matrix: SOIL Analyses Result Limit Qual Units DF VOLATILE SW-846 METHOD 8260 1,2,4-Trtchlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibrom o-3-chloropropa ne SW82606 U 5.6 I~g/Kg-dry U 5.6 IJglKg-dp/ U 5.6 pg/Kg-dry 1,2-Dibromcethane U 5.6 pg/Kg-dr./ 1,2-Dichlorobenzene U 5.6 lag/Kg-dry 1,2-Dichlomethane U 5.6 pg/Kg-dry 1,2~Dichlompropane U 5.6 pg/Kgq:lv/ 1,3,5-Trimethylbenzene U 5.6 pg/Kg-dee t ,~-Dichlorobenzen e U 5.6 pg/Kg-dee 1,3~lichloropropane U 5.6 pg/Kg-dry 1,4-Dichlombenzene U 5.6 pg/Kg-dry 2,2-Dichlompropane U 5.6 IJg/Kg-dry 2-Butanone U 5.6 pg/Kg-dPJ 2-Chlomethyl vinyl ether U 5.6 pgfKg-dee 2-Chlorotoluene U 5.6 pg/Kg~ee 2-Hexanone U 5.6 pg/Kg-dm7 2-Propano[ U 56 pglKg-dry 4-Chlomtoluene U 5.6 pg/Kg-dry 4.1sepmpyltoluene U 5.6 pg/Kg~ee 4-Methyl-2-pentanone U 5.6 i.tg/Kg-dry Acetone U 5,6 lag/Kg-d~/ Actolein U 28 pg/Kg<lry Ac~'ylonitdlu U 5.6 pglKg-dry Benzene U 5.6 pg/Kgq:lvj Bromobenzene U 5.6 lag/Kg-dee Bremochloromethane U 5.6 IJg/Kg-dry Bromodichloromethane U 5.6 pg/Kg-dry Bromoform U 5.6 pg/Kg-dee Bromomethane U 5.6 pglKg-dry Carbon disulfide U 5.6 pg/Kg-dry Carbon tetrachlorlde U 5.6 IJ01Kg-dee Chlorobenzene U 5.6 lag/Kg-dee Chlor~ditluorometh ane U 5.6 lag/Kg-dee Chioroethane U 5.6 pg/Kg-dry Chloroform U 5.6 Hg/Kg-dry Chloromethane U 5.6 I.tg/Kg-dee cis-1,2-Dichloroethene U 5.6 pglKg-do/ cis-1,3-Dichloropropene U 5.6 lag/Kg-dry Dibromuchlorome[hane U 5.6 pg/Kg-dry Date Analyzed Analyst: LDS 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3121/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6;08;00 PM 3/21/2007 6:06:00 PM 3/21/2007 6:06:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6;08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6;08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/2112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:06:00 PM 3121/2007 6:08;00 PM 3/21/2007 6:08:00 PM 3/2t/2007 6:08:00 PM 3/2112007 6;06:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 312112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM QuaJlfier$: E Valu= above quamitation range J Analyt¢ detecled below quantitation limils S Spike Reeovcr~ outside accepted recovery limits X Value exceeds M ~.ximum Cont~xninant L~vel Page 14 of 70 American Analytical Laboratories, LLC. Date: 2S-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 4 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 12:02:00 PM Lab 1D: 0703166-03A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE $W-846 METHOD 8260 SW82600 Dibromomethane U 5.6 IJg/Kg-dry Dtchlorcdifl uorometh ane U 9.6 pglKg-dry Diisopropyl ether U 5.6 pg/Kg-dry Ethanol U 28 pg/Kg-d~y Ethyl acetate U 5.6 pg/Kg.dp/ Ethylbenzene U 5.8 pg/Kg-d~y Freon~114 U 5.6 IJglKgq:l~ Hexach[ombutadiene U 5.6 pg/Kgq:l~y Isopropyl acetate U 5.6 pglKg-d~ Isopropylbenzene U 5.6 pg/Kg-dry m,p-Xyiene U 11 pglKg~fP/ Methyl ted-butyl ether U 5.6 pgtKg~ry Methy{ene chloride U 5.6 IJglKg-dry n.-Amyl acetate U 5.6 pglKg-dry Naphthalene U 5.6 pglKg-dPJ a-Butyl acetate U 5.6 pglKg-dry n-Butylbenzene U 5.6 pg/Kg-dry n-Propyl acetate U 5.6 pg/Kg-thy n-Propylbenzene U 5.6 pg~Kg-d~ o-Xylene U 5.6 pg/Kg-dry p-Diethylbenzene U 5.6 pglKg-dry p-Ethyltoluene U 5.8 IJglKg-dry sec-Butylbenzeae U 5.9 pglKg-dry Slyrene U 5.6 pg/Kg-dry t-Butyl alcohol U 5.6 pg/Kg-dry tert-Butylbenzene U 5.6 pg/Kg-dry Tetrachloroethene U 5.6 pg/Kg.dry Toluene U 5.6 pglKg-dry trans-1,2.Dichlorcethene U 5.6 pglKg-dp/ trans.1.3*Dichloropropene U 5.6 pg/Kg-dgt Tfichloroethene U 5.6 pg/Kg-dry Trichloroflu o romethane U 5.6 pglKg-dry Vinyl acetate U 5.6 pglKg-d~y Vinyl chloride U 5.6 pglKg.dry Surf: 4-Bromofluernhenzeae 99.7 6t-133 %REC Sure Dibromofluommethane 104 61 -I 39 %REC Sum Toluene-dB 98.9 57-131 %REC Analyst: LDS 3/21/2o07 8:08:0o PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/2112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08;00 PM 3/21/2007 6;06:00 PM 312112007 6:08:00 PM 3/2112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/2112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/2112007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 8:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3121/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/2112007 6:08:00 PM 3121/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3121/2007 6:08:00 PM 3/21/2007 6:08:00 PM 3/21/2007 6:08:00 PM Analyle detected in the associated Method Blank Holding times for preparation or analysis exceeded Not Detected at the Reporting Limit Indicates tile compound was annlyzcd for but not dctecte Page 15 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulling Client Sample ID: No. 3 [5-7.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 12:49:00 PM Lab ID: 0703166-04A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analy'zed MERCURY SW74718 SW7471 B Analyst: WN Mercury U 0.0115 mg/Kg~ ry I 3123/2007 1:31:29 PM PERCENT MOISTURE 02216 Analyst: CM Percent Moisture 15.0 0 wt% 1 3/22/2007 TARGET ANALYTE LIST METALS SW6010B SW3050A Analyst: JP Aluminum 15700 4.70 mg/'Kg~ry 10 312312007 3:06:17 PM Antimony U 0.588 rng/Kg-dry 1 3/23/2007 2:21:45 PM Arsenic 4.59 0.585 rog/Kg-dry I 3/23/2007 2:21:45 PM Barium 131 0.470 mglKg-d~ I 3~23~2007 2:21:45 PM Beryllium U 0.470 mglKg-dry 1 3/23/2007 2:21:46 PM Cadmium 0.414 0.235 rog/Kg-dry 1 3123/2007 2:21:45 PM Calcium 1280 0.586 rng/Kg-dry I 3/23/2007 2:21:45 PM Chromium 22.0 0.470 mglKg-dry I 3/2312007 2;21:45 PM Cobalt 1.99 0.470 mg/Kg-d~ I 3/2312007 2:21:45 PM Copper 22.0 0.470 mglKg-d~y 1 3/23/2607 2:21;45 PM iron 21900 4.70 rng/Kg-dry 10 3/23/2007 3:06:17 PM Lead 15.1 0.353 rog/Kg-dry I 3/23/2007 2:21:45 PM Magnesium 5040 0.470 mg/Kg-d~y I 3/23/2007 2:21:48 PM Manganese 369 0.470 rog/Kg-dry I 3/23/2007 2:21:45 PM Nickel 21.1 0.470 mg/Kg-dry I 3/23/2007 2:21:45 PM Potassium 4860 2.35 mglKg-dnJ 1 3/23/2007 2:21:45 PM Selenium U 0.588 mgfKg-d~y 1 3/23/2007 2:21:45 PM Silver U 0.470 rog/Kg.dry I 3/23/2007 2:21:45 PM Sodium 455 1.41 mglKg-dpj I 3/23/2007 2:21:45 PM Thallium U 0.470 mglKg-d~ I 3/23/2007 2:21:45 PM Vanadium 38.6 0.470 mg/Kg-dry I 3/2312607 2:21;45 PM Zinc 55.1 0.470 rog/Kg-dry I 3123/2007 2:21:45 PM SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3550A Analyst: PT 1,2,4-Trichiurobenzene U 140 pg/Kg-d~y I 312312007 6:25:00 PM 1,2-Dichlombenzene U 140 pglKg-d~y 1 3/2312007 6:28:00 PM 1,3-Dichlombenzene U 140 pglKg.-dry I 3/23/2007 6:26:00 PM 1,4-Dichlombenzene U 140 pg/Kg-dry 1 3/23/2007 6:26:00 PM 2,4,5-Trich]o rophencl U 140 pgfKg-dry 1 312312007 6:28:00 PM 2,4,6-Trichlarophenol U 140 pg/Kg.dry 1 3/23/2007 6:26:00 PM 2,4-Dichlorophenol U 140 pg/Kg-dry 1 3/23/2007 6:26:00 PM 2,4-Dirnathylphenol U 140 pg/Kg-d~y 1 3/23/2007 6:26:00 PM 2,4-Dinitrophenol U 140 pglKg-d~y I 3/23/2007 6:28;00 PM 2,4-Dintirotoluene U 140 pg/Kg-dry 1 3123/2007 6:26:00 PM 2,6-Dinitrotoiuene U 140 pgfKg-dry 1 312312007 8:26:00 PM Qualifiers: B Anal~te detected in the associated Method Blank H Holding times for preparation or annlysis exceeded ND Not Detected at the Reporting Limit U Indicates thc compound was naalyzod for but not dctccte $ Spike Recovc~ oul~ide acm@ted recovery limits Page 16 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 3 [5-7.5'] Lab Order: 0703166 Project: Moore$ Lane Greenport, N.Y, Lab ID: 0703166-04A Tag Number: Collection Date: 3/20/2007 12:49:00 PM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3$50A 2-Chroronaphlhalene U 14fi ug/Kg-d~ 1 2-Chtorophenol U 140 Ug/Kg~ry 1 2-Methylnaphthalene U 140 ~Jg/Kg-d~y 2-Methylphenol U 140 ug/Kg-dry 1 2-Nitroaniline U 140 pg/Kg-dry 1 2-Nitmphenol U 140 pg/Kg-dry 1 3,3'-Dichrombenzidine U 140 !Jg/Kg-dry 1 3*4-Meihyrphenol U 140 pg/Kg-d~ 1 4,6-Dinltro-2-methylphenol U 140 pg/Kg~d~t 1 4-Bremopbenyl phenyl ether U 140 ,ug/Kg-dry 1 4-Chloro-3-methylphenol U 1411 pglKg-d~7 1 4-Chlomaniline U t 40 ~Jg/Kg<lry 1 4-Chlorophenyl phenyl ethel U 140 pg/Kg~dry 1 4-Nitmaniline U 140 pglKg-dry 1 4-NilrophenDI U 170 pg/Kg-d~y 1 Acenaphthene U 140 pglKg-dry 1 Acenaphthylene U 140 pglKg-dry 1 Aniline U 140 IJg/Kg-dry 1 Anthracene U 140 pg/Kgqlry 1 Azobenzene U 140 pg/Kg-dry 1 Benzidine U 140 pglKg-dty 1 Benzo(a)anlhracene U 140 pglKg.-thy 1 Benzo(a)pyrene U 140 pg/Kg-dry 1 Benzo(b)fluoranlhene U 140 pg/Kg-d~ 1 · Benzo(g,h,i)per¥1ene U 140 pg/Kg-d~y Berum(k)fluoranthene U 140 pg/Kg-d~7 1 Benzoic acid U 140 Pg/K§-d~7 1 Benzyl alcohol U 140 pg/Kg-d~y 1 Bis(2'chl°r°eth°xT)methane U 140 pg/l<g~dp/ I BJs(2-chloroethyl)ether U 140 pg/Kgq~7 1 Bis(2-chloroisopropy[}ether U 140 pg/Kg-dPj 1 Bis(2-ethylhexyl)phthalat e U 140 pglKg-dr~ 1 Butyl benzy[ phthalate U 140 pg/Kg-dry Carbazole U 140 pg/Kg-d~y 1 Chrysene U 140 IJglKg--dry 1 Dibenzo(a,h)anthracene U 140 pgtKg-dry 1 Dibenzofuran U 140 pg/Kg-d~ 1 Diethyl phthalste U 140 pg/Kg-dry 1 Qualifiers: B /L, mlytc detected in thc associated Method Blank DF Date Analyzed Analyst: PT 312612007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/200? 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2607 6:26:00 PM 3/23/2007 6:26:fl0 PM 3/23/2007 6:26:00 PM 3/23/2067 6:26:00 PM 3/23/2007 6:26:0D PM 3/23/2007 6:26:00 FM 3123/2fl07 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2D67 5:26:00 PM 3/23/21167 6:26:00 PM 3/23/2007 6:26:~O PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/20fi7 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM E Value above quantitation range bi Holding times tar preparation or analysis exceeded ND Not Detected at the Reporting Limil U lndicalcs rite compound was analyzed for but not detecte J Analyte detected below quantitation limils S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 17 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CL1ENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Mooms Lane Greenpor; N.Y, 0703166-04A Client Sample ID: No. 3 [5-7.5'] Tag Number: Collection Date: 3/20/2007 12:49:00 PM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE 5W-846 METHOD 8270 SW82705 SW3558A Dimethyl phthalat~ U 140 pglKg~d~/ Di-n-butyl phthalat~ U 140 pg/Kg-dr¥ Di-n-octyl phthalate U 140 IJglKg-dry Fluoranthene U 140 ~g/Kg-dry Fluorene U 140 pg/Kg.dly Hexach[cmbenzene U 140 pg/Kg-d~y Hexachlornbutadiene U 140 Hg/Kg~r~ Hexachlorocyclopentadiene U 170 HglKg-dry Hexachloroethane U 140 pglKg-dry Indeno(1,2,3-c,d)pyrene U 140 pg/Kg-dry Isophorone U 140 pg/Kg-d~/ Naphthalene U 140 FglKg<~Y Nit~obenzene U 140 pg/Kg-d~/ N-Nitroscdimethylamine U 140 ~g/Kg-dry N-Nitrosodi-n-propylamine U 140 iJg/Kg-dry N-Nitrosodiphenylam[ne U t40 pglKg-clry pentachlcmphenol U 170 pg/Kg-dry Phenanthrene U 140 pg/Kg-d~/ Phenol U 140 pglKg-dry Pyreoe U 140 pgfKg-dry Pyddine U 140 pg/Kg-d~/ Surf: 2,4,6-Tribromophenol 29,9 22.124 %REC Surr: 2-Fluorobiphenyl 70.3 27-11 g %REC Sur~ 2-Fluorophenol 82.3 25-123 %REC Sum 4-Terphenyl-d 14 65.6 28-126 %REC Sum Nitrobenzeee-d5 61.7 21-11B %REC Sur~ Phenol-d6 82.7 1~-129 %REC VOLATILE SW-846 METHOD 8260 SW82608 1,1 ,t ,2-Tetrachloroethana U 5.8 ~g/Kg-dry 1,1,1 -Trichloroethane U 5.8 pglKg-d~/ 1,1,2,2-'~etrac~loroethane U 5,8 pg~g<l~/ 1,1,2-Trichloro-1,2,2-tdflu~methane U 5,8 pg/Kg-dty 1,1,2-Trichloroethane U 5.8 gg/Kg-dry 1,1-Dichloroethane U 5.8 pg/Kg-dry 1,1 -Dichloroethene U 5,5 pglKg-d~7 1,1 -Dichtompropene U 5.8 pg/Kg-dry 1,2,3-Trichlorobenzene U 5.8 pglKg-dl~ 1,2,3-Trichloropropane U 5.8 pg/Kg-dry 1,2,4,5-Tetramet hylbenzene U 5.8 HglKg-d~ DF Date Analyzed Analyst: PT 3/23/2007 6:26:00 PM 3123/2057 6:26:00 PM 3/23/2007 6:26:00 PM 3123/2007 6:26;00 PM 3/23/2007 6:28:00 PM 3~23~2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3~23~2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/2312007 6:26:00 PM 3123/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3123/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/~3/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM 3/23/2007 6:26:00 PM Analyst: LDS 3/21/2007 6:56:00 PM 3/21/2007 6:56:00 PM 3/21/2007 6:56:00 PM 3/2112007 5:66:00 PM 3/2112007 6:56:00 PM 3/2112007 6:56:00 PM 3/21/2007 6:56:00 PM 3/2112007 6:56:60 PM 3/21/2007 6:56:00 PM 3/21/2007 6:56:00 PM 3/21/2007 6:56:05 PM Qualifiers: B Analytc detected in thc ~ssocialcd Method Blank Holding times for prcparation or analysis cxc~ded ND Not Detected at thc R~porting Limit E Value above quantitslion range J Analyl¢ detected below qaantitation limits S Spike RccoveE/outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 18 ofT0 American Analytical Laboratories, LLC. ])ate: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 3 [5-7.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 12:49:00 PM Lab ID: 0703166-04A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW~846 METHOD 8260 SW82605 Analyst: LDS 1,2,4-Trichlorobenzene U 5.8 idg/Kg-d~y 1 3/21/2007 6:55:00 PM 1,2,4-THmethylbenzene U 5.8 po/Kal-dry 1 3/21/2007 6:56:00 PM 1,2-Dibromo-3-chloropropane U 5.5 pg/Kg-dry I 3/2t/2007 6:56:00 PM 1,2-Bibrornoethane U 5.5 pg/Kg-dp~ I 3/21/2007 6:56:00 PM 1,2-Dichiorobenzene U 5.8 trig/Kg-dry 1 3/21/2007 6:56:00 PM 1,2~Dichloroethane U 5.8 idg/Kg-dry 1 3/21/2007 6:56:00 PM 1,2-Dichloropropane U 5.8 pglKg-dry I 3/2112007 6:56:00 PM 1,3,5-Tfirnerbylbenzene U 5.8 idglKg-dry 1 3/21/2007 6:56:00 PM t ,3-Dichlorobenzene U 5.8 idg/Kg-dry 1 3/21/2007 6:56:00 PM 1,3-dichloropropane U 5.8 idg/Kg-dry I 3/2112007 6:56:00 PM 1,4.Dlchlorobenzene U 5.8 pg/Kg-dry I 3/21/2007 6:55:00 PM 2,2-Dichloropropane U 5.8 pglKg-dry 1 3/21/2007 6:56:00 PM 2-Butanone U 5.8 pg/Kg-dry 1 3/21/2007 6:56:00 PM 2-Chloroe/hyl vinyl ether U 5.8 idglKg-dry 1 312112007 6:56:00 PM 2-Chlorotoluene U 5.8 pg/Kg-clry 1 3/21/2007 6:56:00 PM 2-HexanDne U 5.5 pg/Kg-dry 1 3/21/2007 6:56:00 PM 2-Propanol U 58 pg/Kg-dry 1 3/21/2007 6:56:00 PM 4-Chlomloluene U 5.8 pg/Kg-dry I 3/2112007 6:56:00 PM 4qsopropylloluene U 5,8 idg/Kgq:lry I 312112007 6:56:00 PM 4-Methyl-2-pentanone U 5.6 pg/Kg-d~ 1 3121/2007 6:56:00 PM Acetone U 5.5 pg/Kg-dty I 3/21/2007 6:56:00 PM Acrolein U 29 pg/Kg-d~7 1 3121/2007 6:56:00 PM Acrylonitfile U 5.8 :ag/Kg-dry I 3/21/2007 6:56:00 PM Benzene U 5.8 ~g/Kg.dry I 3/21/2007 6:55:00 PM Bromobenzene U 5.5 ~g/Kg-dry 1 3121/2007 6:56:00 PM Brornochlorornethane U 5.8 IJg/Kg-dry 1 3/21/2007 6:56:00 PM Bromodichlorornethane u 5.6 id[I/Kg-dry I 312112007 6:56:00 PM Bromoform U 5.8 ~Jg/Kg-dry t 3/21/2007 6:56:00 PM Bromornethane U 5.5 idglKg-dry 1 3/21/2007 6:56:00 PM Carbon disulfide U 5.8 tJg/Kg~hy 1 3121/2007 6:56:00 PM Carbon tetrachloride U 5,8 idglKg-dry I 3/21/2007 6:56:00 PM Chlorobenzene U 5.8 idg/Kg-dry I 3/21/2007 6:56:00 PM Chloroditluoromethane U 5.8 pg/Kg-dry I 3/21/2007 6:56:00 PM Chloroethane U 5.8 ~gfKg-dry 1 3/21/2007 6:56:00 PM Chloroform U 5.8 ~Jg/Kg-dry I 3/21/2007 6:56:00 PM Chloromethane U 5.8 Idg/Kg<lry I 3/21/2007 6:56:00 PM c~s-l,2.Dichloroethene U 5.8 pg/Kg-dry I 3/21/2007 6:56:00 PM cis-l,3-Dichloropropene U 5.8 pg/Kg-dry 1 3/21/2007 6;56:00 PM Dtbrornochloromethane U 5.6 pg/Kg-dry 1 3/21/2007 6:56:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times £or p~paration or nnalysis exceeded ND Not Detecl*d at thc Reporting Limit U Indlcat~s lhe compound was analyzed [or but not detecte Value above quanlilution range Analyle detected below quaotitatlon limits Spike Recovery outside acccpt~:d recovery limits Value exceeds Maximum Contaminttnt Level Page 19 of 70 American Analytical Laboratories, LLC. Date: 28-bier-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Cons~ting 0703166 Moores Lane Greenpo~,N.Y. 0703166-04A Client Sample ID: Tag Number: Collection Date: Matrix: No. 3 3/20/2007 12:49:00 PM SOIL Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82606 Dthromomethane U 5.8 Dich[orodifluo romeih ane U 5.8 Dlisopropyl ether U 5 8 Ethanol U 29 Ethyl acetate U 5.8 Ethylbenzene U 5.8 Freon-114 U 5.6 Hexachlorobutadiene U 5.8 Isopmpyl acetate U 5.8 hepmpylbenzene U 5.8 m,p-Xylene U 12 Methyl tort-butyl ether U 5.8 Methylene chloride U 5.8 n-Amyl acetate U 5.6 Naphthalene U 5.8 n~utyl acetate U 5.8 n-Butylbenzene U 5.8 n-Propyl acetate U 5.8 n-Propylbenzene U 5.6 o-Xylene U 5.8 p-Dtathyibenzene U 5.8 p-Ethyltcluene U 5_8 sec-BubJlbenzene U 5.8 Styrene U 5.8 t-Butyl alcohol U 5.8 tert-Butylbenzene U 5.5 Tetrachloroethene U 5.8 Toluene U 5.8 trans-l,2-Dichlomethene U 5.8 lrans-1,3-Dichloropropene U 5.6 Trichlomethene U 5.6 Tdchiorofluoromethane U 5.8 Vinyl acetate U 5.8 Vinyl chloride U 5.8 Sur~ 4-8romofluombenzeeo 103 61-133 Surf: Dibromefluoromethane 114 61-139 Surf: Toloen~d8 97.4 57-131 Units DF Date Analyzed Analyst: LDS pg/Kg-dP/ 1 3/21/2067 6:56:00 PM pglKg-dry 1 3/21/2667 6:56:00 PM pglKg~ry I 3/21/2007 6:56:00 PM pglKg-dv/ 1 3/21/2007 6:56:00 PM pg/Kg-dry I 3/21/2007 6:56:06 PM pg/Kg-dvJ 1 3/21/2007 6:56:00 PM FglKg-dv/ 1 3/21/2007 6:56:00 PM pg/Kg<lry I 3/21/2007 6:56:00 PM :ag/Kg-dry I 3/2112007 6:56:00 PM pg/Kg.dry I 3/21/2007 6:56:00 PM pg/Kg-dl7 1 3/21/2007 6:56:00 PM pg/Kg-dry I 3/21/2007 6:56:~3 PM pg/Kg<lry 1 3/21/2007 8:56:00 PM pg/Kg-dry 1 3/21/2007 6:56:00 PM pg/Kg-dry I 3/2112007 6:55:00 PM pg/Kg~ry 1 3/21/2007 6:56:00 PM pg/Kg-dry I 3121/2007 6:56:00 PM pg/Kg-dry 1 3/21/2007 6:56:00 PM pg/Kg<try 1 312112007 6:56:00 PM pg/Kg~ I 3/21/2007 6:66:00 PM pg/Kg-dry I 3/21/2007 6:56:00 PM pg/Kg~ry I 3/2112007 6:56:00 PM pg/Kg-clry 1 3/21/2007 6:56:00 PM pg/Kg-dry 1 3/2112007 6:56:00 PM pg/Kg-dry 1 3/2112007 6:56:00 PM pglKg-d~y 1 312112007 6:56:00 PM pg/Kfl-clry 1 3/21/2007 6:56:00 PM pg/Kg-dr.j 1 3/21/2007 6:56:06 PM pg/Kg-dry 1 3/21/2007 6:56:00 PM pglKg-dry 1 3/21/2007 6:56:00 PM IJg/Kg-chy t 3/21/2007 6:56:00 PM pg/Kg-dry 1 3/21/2007 6:56:00 PM pg/Kg-dry 1 3/2112007 6:56:00 PM pglKg.-dPj ~ 3/21/2067 6:58:00 PM %REC 1 3/21/2n07 6:56:00 PM %REC I 3/21/2007 6:56:00 PM %REC 1 3/21/2607 6:56:00 PM Quatiliers: B Analyte dot,clod in the associated Method Blank H Holding times for preparation or anal~is exceeded ND Not Detecled at the Reporting Limit U Indicates thc compound wes analyzed for but not dctc~tc E Value above quantitation range J Analyte dete~ted bolow qua~titation timiLf S Spike Recove~ oulaide nc~ptcd r~ovc~ limits X Value cxccc~ M~/mum Cont~t Level Page 20 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Greenpon, N.Y. 0703166-05A Client Sample ID: No. 2 [7.5-10'] Tag Number: Collection Date: 3/20/2007 1:15:00 PM Matrix: SOIL Analyses Result Limit Qual Units MERCURY SW747'1B SW747'1B Mercury 0.0133 0.0102 mo/Kg-dry PERCENT MOISTURE 02216 Percent Moisture 14.9 0 wt% TARGET ANALYTE LIST METALS SW60'IOB SW3080A Aluminum 56800 4,85 rng/Kg-dry Antimony U 0.581 mglKg-dry Arsenic 1.20 0.581 rnglKg-dry Badum 44.8 0.465 rnglKg-dry Berylfiurn U 0.465 rnglKg-dry Cadmium U 0.232 rag/Kg-dry Calcium 272 0.581 rng/Kg~dry Chrorninrn 14.3 0.465 mg/Kg-dry Cobalt U 0.485 rog/Kg-dry Copper 6.52 0,485 rog/Kg-dry iron 4610 0.465 mg/Kg.dry Lead 6.B6 0.349 mg/Kgq:lpJ Magnesium 1810 0.465 rog/Kg-dry Manganese I24 0.465 mg/Kg-dry NicS. el 8.90 0.465 rog/Kg-dry Potassium 1180 2.32 rog/Kg-dry Selenium U 0.501 mg/Kg<lry Silver U 0.465 mg/Kg~ry Sodlurn 190 1.39 mg/Kg~ry Thallium U 0.465 rog/Kg-dry Vanadium 22.9 0.465 rog/Kg-dry Zinc 24.8 0.465 rog/Kg.dry SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3560A 1,2,4-Tdchlorobenzene U 140 pg/Kgq:lry 1,2-Dichlornbenzene U 140 ug/Kg-dry 1,3-Dichlorobenzene U 140 pglKg-dry 1,4-Dichlorobenzene U 140 Hg/Kg-dry 2,4,5-Tdchlorophenol U 140 Hg/Kg-dry 2,4,6-Tfichh3rophenel U 14g pg/Kg-d~J 2,4-Dich]ornphenol U 140 pglKg-dry 2,4-Dirnethylphenol U 140 pg/Kg-dry 2,4-Dinitrophenol U 140 pg/Kgq:i~y 2,4-D[nitrotoluene U 140 pg/Kg-d~y 2.6-Dinitrotoluene U 140 pglKg-dry DF 1 I 10 Date Analyzed Analyst: WN 3/23/2007 1:33:52 PM Analyst: CM 3/22/2007 Analyst: JP 3/23/2007 3:00:26 PM 3~23~2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2/24:33 PM 3/23/2007 2:24:33 PM 3123/2007 2:24:33 PM 3/23/2007 2:24:33 PM 3/23/2007 2:24:33 PM Analyst: PT 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2097 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3123/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM Qualifiers: B Analylc dcicclcd in tim ~sociatcd Method Blank Holding times for prcparatlon or analysis exceeded ND Not Detected at tbs: Reporting Limlt Value above quantitatinn range Analytc detected below quantitation limits Spike Recovery outside accepted recovery limits Value exceeds Maximum Contaminant Loyal Page 21 of 70 American Analytical Laboratories, LLC. m/e: 2&Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 2 [7.5-10'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 1:15:00 PM Lab ID: 0703166-05A Matrix: SOIL Result Limit Qnal Units DF Date Analyzed Analyses SEMIVOLATILE SW-846 METHOD 8270 SW8270D SWaSS0A 2-Chloronaphthalene U 140 ag/Kg-dry 2-Chiorephena} U 140 ag/Kg-dry 2-Methylnaphthalene U 140 ag/Kg-dry 2-Methylphenol U 140 pg/Kg-dry 2-Nitroa n/line U 140 pg/Kg-d,ry 2-Nltrophenol U 140 Fg/Kg-dry 3,3'-Dichlorobeaztdl~ e U 140 ~glKg-dry 3+4-Methylphenol U 140 p§/Kg<lry 3-Nitroanillne U 140 ag/Kg-dry 4,6-Dinitro-2..met hylphenol U 140 pg/Kg-d~y 4-Bromophenyl phenyl ether U 140 ag/Kg-dry 4-Chtorc-3--methylphenol U 140 pg/Kg-d~ 4-Chloroaniline U 140 ag/Kg-dry 4-Chlnrophenyl phenyl ether U 140 pg/Kg-dr./ 4-Nittoaniline U 140 ag/Kg-dry 4-Nitrophenol U 180 pg/Kgq:iry Acenaphthene U 140 aglKg-d~y Acenaphthylene U 140 ag/Kg-dry Aniline U 140 ~Jg/Kg<lry Anthracene U 140 pglKgq:l{y Azobenzene U 140 pgtKg-dry Benzidine U 140 ag/Kg-dry Benzo(a)anthracene U 140 ~Jg/Kgq:[r.J Benzo(a)pymne U 140 ag/Kg-dry Benze(b)fluoranthene U 140 ag/Kg-dry Benze(g,h,i)perglene U 140 ag/Kg-dry Benzo(k)fluoranthene U 140 ag/Kg-dry Benzoic acid U 140 ag/Kg-dry Benzyl alcohol U 140 pg/Kg41ry Bis(2.-chloroathoxy)meth ane U 1411 aglKgqf~, Bis (2-chloroethyl}ether U 140 ag/Kg</fy Bi${2-chloroisnpropyl)ether U 140 ag/Kg-dry Bis(2-ethylhexyl)p hthalate U 140 pg/Kg-dry Butyl benzyl phthalate U 140 ag/Kg-dry Carbazale U 140 ag/Kg-dry Ch~sene U 140 ag/Kg-dqt Dibenza(a,h}anthracene U 140 ag/Kg-dry Dibenzofuran U 140 ag/Kg-dry D/ethyl phthalate U 140 pglKg-dry Analyst: PT 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/2312007 6:54:00 PM 3123/2007 6:54:00 PM 3123/2D07 6:54:00 PM 3/23/2007 6:54;00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3t2312007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3123/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3123/2007 6:S4:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/200? 6:54:00 PM 3/23/2007 6:54:00 PM 3123/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6;54:00 PM 3/23/2007 6:S4:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM Qualifiers: E Value above quantiaxion range J Analy~e detoured below quantltatlon limils S Spike Recowt~ outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 22 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: LabID: P.W. Grosset Consulting 0703166 Moores Lane Greenport, N.Y. 0703166~05A Client Sample ID: No. 2 [7.5-10'] Tag Number: Collection Date: 3/2012007 I:15:00PM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82708 SW3550A Dimethyl phthalate U 140 pg/K,g.dry Di-n-butyl phthalale U 140 pg/Kg-dry Di-n-octyl phthalate U 140 pg/Kg-dr~ Fluoranthene U 140 pglKg-dP/ Fluomne U 140 pgt*Kg-dry Hexachlorobenzene U 140 gg/Kg-dr~ Hexachlorobutadiene U 140 pglKg-d~/ Hexachlorocyclopent adiene U 180 pg/Kg-dry Hexachloroethane U 140 pglKg-do/ thdeno(1,2,3-c,d)pyrene U 140 gg/Kg-dry Isophorone U 140 pg/Kg-d~ Naphthalene U 140 pglKgq:lry NRrobeezene U 140 pg/Kg.dry N-Nitrosodimeihylamine U 140 pg/Kg-d~ N-Niirosodi-n-pmpylamine U 140 pglKg-dry N-Nitrosodiphenylamine U 146 pg/Kg-d~t Pentachlorophenol U 190 pglKg-dry Phenanthrene U 140 pglKg~l~y Phenol U 140 IJglKg-d~J Pyrene U 140 Ng/Kg-dty Pyridine U 140 Ng/Kg-dry Sum 2,4,6-Tdbromophenol 66.1 22-124 %REC Sum 2-Flue mbiphenyl 69.7 27-119 %REC SUrE 2-Fluorophenol 89.0 21-123 %REC Sum 4-Terphenyl-dl 4 69.5 28-126 %REC Sum Nitrobenzene-d5 62.4 21-118 %REC SurE_ Phenol-d6 85~6 18-129 %REC VOLATILE SW-846 METHOD 8260 SW8260B 1,1,1,2-Tetrach!oroethane U 5.8 NglKg-d~/ 1,1,1-Trichloroethane U 5.8 pg/Kg-d~y 1,1,2,2-Tet rachloroethane U 5.8 t~g/Kg~ry 1,1,2-Trichloro-I ,2,2.tdfluoroethane U 5.8 pg/Kg-d~y 1,1,2-Tdchloroethane U 5.8 1,1-Dichloroethane U 5.8 pg/Kg-dq/ 1,1-Dichloroethene U 5.5 uglKg-dry 1 ,t-Dichloropropene U 5.8 pg/Kg-drY 1,2,3-Tdchlorobenzene U 5.8 ug/Kg-d~/ 1,2.3-Trichloropropane U 5.8 Ng/Kg..dt¥ t ,2,4,5-Tetramethy~i~enzene U 5.8 pglKg-dry DF Date Analyzed Analyst: PT 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:~4:06 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2907 6:,54:60 PM 3/23/2507 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/2312007 6:54:00 PM 3/23/2907 6:64:06 PM 3/23/2007 6:54:00 PM 3/23/2907 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2007 6:54:00 PM 3/23/2607 6:54:00 PM 3/23/2007 6:54:08 PM 3/23/2007 6:54:60 PM 3/23/2007 6:54:00 PM 3/23/2087 6:54:06 PM 3/23/2007 6:54:90 PM 3/23/2907 6:54:06 PM 3/23/2007 6:54:00 PM Anayst: LDS 3/21/2007 7:44:00 PM 3/21/2907 7:44:00 PM 3121/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/2112007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM Qualifiers: B Annlyte detected in the associmcd Method Blank 1-1oiding times for preparation or analysis exceeded ND Not ~t~cted at the Reposing Limit Value above quantitation range Ana]~'tc detected bclo~v quantiattien limits Spikc Rccovc~ outside acceplcd recovc~7 limits Value exceeds M~ximum Contmninaat Level Page 23 of 70 American Analytical Laboratories, LLC. Date: 2a-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 2 [7.5-I0'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 l :l 5:00 PM Lab ID: 0703166-05A Matrix: SOIL Result Limit Qual Units DF Analyses VOLATILE SW-846 METHOD 8260 1,2,4-Tdchlombanzene 1,2,4-Trimethylbenzene 1,2-D[bromo-3-chlompropan e 1.2-Dibmmoethane 1,2-Dtch[orobenzene 1,2-Dichloroethane 1,2-Dichloropmpar~e 1,3,5.Trimethylbenzene 1,3.Dichlorobenzece 1,3~ichloropropane 1,4-Dichlorobenzene 2,2-Dichloropropane 2-Butacene 2-Chloroethyl vinyl ether 2*Chlorotoluene 2.Hexanone 2-Propanol 4-Chlorotoluece 4-1sopropyltoluene 4-Methyl-2-pentanone Acetone A~rDrein Acrylonitrile Benzene Rromobencene Bromochloromethane Bromodichloromethane Bromofon'n Bromornethane Carbon disulfide Carbon tetrachlodde Chlombenzene Chloroditluoromethane Chloroethane Chloroform Chlommethane cia-1,2-Dichloroethene cia-1,3-Dichloropmpene Dibromochlommethace SW82600 U 5.8 pg/Kg-dry U 5./) pg/Kg-dry U 5.8 pg/Kg-dry U 5.8 pg/Kg-dry U 5.6 lag/Kg-dry U 5.8 pglKg~ry U 5.8 pglKg-dr/ U 5.8 pg/Kg-dPJ U 5.8 pglKg-dPJ U 5.8 pg/Kg-dry U 5.8 pg/Kg-dry U 5.8 pg/Kg~lry U 5.8 pg/Kg-dry U 5.8 gglKg-dry U 5,8 pg/Kg-dry U 5.8 pg/Kg-d~ U 58 pg/Kg-dry U 5.8 pg/Kg~ry U 5.8 pg/Kg-dry U 5.6 ~lglKg.-dry U 5.8 I~g/Kg-dry U 29 pglKg-dry U 5.8 pglKg-dry U 5.8 pg/Kg-dry U 5.8 pg/Kg-dry U 5.8 pg/Kg-dry U 5.8 pg/Kg-dry U 5.8 NgtKg-clry U 5.8 pg/Kg~ry U 5.8 pg/Kg~ry U 5.8 pg/Kg,.dry U 5.8 pgtKg-dry U 5,8 pg/Kg-dry U 5.8 pg/Kg-di7 U 5,8 pglKg-dP] U 5.8 pglKg-dry U 5.8 pglKg-dry U 5.8 Llg/Kg-dry U 5.8 pglKg-clry Date Analyzed Analyst: LDS 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/2t/2097 7:44:00 PM 3/21/2007 7:44:00 PM 3/2i/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/2112007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/2t/2007 7:44:00 PM 3/21/2007 7:44:80 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/2t/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3/21/2007 7:44:00 PM 3t21/2007 7:.44:00 PM Qualifiers: Page 24 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 2 [7.5-10'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 1:15:00 PM Lab ID: 0703166-05A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-845 METHOD 6260 Dibmmomethane Dichlomdifluu romethane Diisopropyl ether Ethanol Ethyl acetate Ethylbenzene Fmon-114 Hexachl~3rubu~adiene ]sopmpyl acetate Isopropylbeneene m,p-Xy[ene Methyl tart-butyl ether Methylene chloride n-Amyl acetata Naphthalene n-Butyl acetate n-Butylbunzena n-Pmpyl acetate n-Pmpylbenzene o-Xylene p-Dlethylbenzune p-Ethyltaluene aac-Butylbenzene SI'irene t-Butyl alcohol tert-Butyibeazene Tetrachloroethene Toluene trane-1,2-Dichloroethene trans-1,3-Dichlompropene Tdchloroethene Trichloroffuoromethane Vinyl acetate Vinyl chlodde Sun':. 4~Bromofluorobenzene Surr: Dibromofluoromethane Surf. To[uene-d8 SW82600 Analyst: LDS U 5.8 pg/Kg-d~ 1 3/21/2007 7:44:00 PM U 5.8 pglKg~n,, 1 312112007 7:44:00 PM U 5.8 pg/Kg-dry 1 3/21/2007 7:44:00 PM U 29 pg/Kg.*dry 1 3/21/2007 7:44:00 PM U 5.0 pg/Kg-dpj 1 3/21/2007 7:44:00 PM U 5.8 p§/Kg-dp/ 1 3/21/2007 7:44:00 PM U 5.8 pglKg-dry 1 3/21/2007 7:44:00 PM U 5.8 pg/Kg-dPJ I 3/21/2007 7:44:00 PM U 5.0 pg/Kg~y 1 3/2112007 7:44:00 PM U 5.8 pg/Kg.-d~y 1 3/21/2007 7:44:00 PM U 12 pg/Kg-dry 1 3/21/2007 7:44:00 PM U 5.8 pglKg-dry 1 3/21/2007 7:44:00 PM U 5.8 pglKg-d~y I 3/21/2007 7:44:00 PM U 5.8 pg/Kg-d~ 1 3121/2007 7:44:00 PM U 5.6 pglKg-dry 1 3/21/2007 7:44:00 PM U 5.8 pg/Kg-dry 1 3/21/2007 7:,44:~0 PM U 5.8 pgtKg-dry 1 3/21/2007 7:44:00 PM U 5.0 pg/Kg-d~y 1 3/21/2007 7:44:00 PM U 5.6 pg/Kg-d~y I 3/21/2007 7:44:00 PM U 5.8 pg/Kg~j 1 3/2112007 7:44:00 PM U 5.8 pg/Kg-d~ 1 3/21/2007 7;44:00 PM U 5.8 pg/Kg-dry I 3/21/2007 7:44:00 PM U 5.8 pg/Kg-d~y 1 3/21/2007 7:44:00 PM U 5.8 pglKg~hy 1 312112007 7:44:00 PM U 5.8 pg/Kg-d~y 1 3/21/2007 7:44:00 PM U 5.8 pg,'Kg-ary 1 3/21/2007 7:44:00 PM U 5.8 pg/Kg-dry 1 3/21/2007 7:44:00 PM U 5.8 Pg/Kg-thY 1 3121/2007 7:44:00 PM U 5.8 pg/Kg-dPj I 3/21/2007 7:44:00 PM U 5.8 pg/Kg-dry I 3/21/2007 7:44:00 PM U 5.8 gg/Kg-d[y 1 3/21/2007 7:44:O0 PM U 5.8 FglKg-thy 1 3/21/2007 7:44:00 PM U 5.8 pglKg-dry I 3/2112007 7:44:00 PM U 5.8 pg/Kg-d~y I 3/21/2007 7:44:00 PM 97.6 61-133 %REC 1 3/21/2007 7:44:00 PM 113 61-t39 %REC 1 3/21/2007 7:44:00 PM 96.5 57-131 %REC 1 312112007 7:44:00 PM Qualifiers: Analyte dctecled in the associatad Method Blank H Ho/ding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates the compound was analyzed for but not detecte E Value above quantitufion range ] Ana/yte detected below quantitation limits S Spike Reeove~ ouLside accepled recovery limits X Value exceeds Maximum Contaminant Level Page 25 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: P.W. Grosser Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: Lab ID: 0703166-06A Matrix: No. I [10-12.5'] 3/20/2007 2:14:00 PM SOIL Analyses Result Limit Qual Units M ERCU RY SW747~1B SW7471 B Mercu~ U 0.0106 rog/Kg-dry PERCENT MOISTURE 02216 Percent Moisture 8.11 0 wt% TARGET ANALYTE LIST METALS SW6010B SW3050A Aluminum 2200 0.428 tug,Kg-dry Antimony 0.674 0.536 mglKg-dry Arsenic 2.13 0.536 mglKg-dry Badum 8.33 0.428 mglKg-dry Beryllium U 0.428 mg/Kg.dry Cadmium 0.378 0.214 mg/Kg-dry Calcium 99.7 0.536 rng/Kg-dry Chromium 17.0 0.428 mg/Kg~ry Cobalt 1.01 0.428 rog/Kg-th7 Copper 4.73 0.428 mglKg-dry Iron 9330 4.28 mglKg~ry Lead 13.4 0.321 rog/Kg-dp/ Magnesium 338 0.428 rog/Kg-dry Manganese 69.7 0.428 mg/Kg-d~ Nickel 3.79 0,428 rog/Kg-dry Potassium 341 2.14 mglKg-d~J Selenium U 0.536 mg/Kg-dry Si~ver U 0.428 rog/Kg-dry Sodium 116 1 _28 mg/Kg-dry Thallium U 0.428 mglKg-d~ Vanadium 8.73 0.428 mglKg-dry Zinc 14.0 0.428 mglKg-dry SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3550A 1,2,4-Tdchlorobenzene U 130 pg/Kg-dry 1,2-Dichloro benzene U 130 pglKg-dry 1,3-Dichlombenzene U 130 pglKg-dry 1,4-Dichlombenzene U 130 pglKg~ 2,4,5-Tr~chlorophenol U 130 IJg/Kg-d~J 2,4,6-Tr~chlorsphenol U 130 pglKg-dry 2,4-Dichlomphenol U 130 pg/Kg-d~y 2,4-DImethylphenol U 130 ~glKg-dry 2,4-Dinitmphenel U 130 pg/Kg-d~y 2,4-Dinilmto]uene U 130 pg/Kg-dry 2,8-Dinitmteluene U 130 pg/Kg.dPJ DF Date Analyzed Analyst: WN 3/23/2007 1:30:45 PM Analyst: CM 3/22/2007 Analyst: JP I 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 312312007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:45 PM 1 3/23/2007 2:27:48 PM t0 3/23/2007 3:08:2t PM 1 312312007 2;27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM I 3/23/2007 2:27:48 PM I 3/23/2007 2:27:48 PM 1 3/23/2007 2:27:48 PM 1 3/23/2007 2:27;48 PM 1 3/23/2087 2:27:48 PM 1 3/23/2007 2:27;48 PM Analyst: PT 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 312312007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM 3/23/2007 7:22:00 PM Qualifiers: Analytc detected in the ~sociatcd Method Blank H Holding tlmcs for preparation or analysis exceeded ND Not Detected at ~¢ Reporting Limit U Indicates thc compound was anal~ed for bul not dctecte E Value above quamitation rangc J Analytc detected below quantitadon limits S Spike Recovery outside accepted recovery limits X Value exceeds M~xiraura Contaminant Level Page 26 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 1 [10-12.5'] Lab Order: 07§3166 Tag Number: Project: Moores Lane Grcenport, N.Y. Collection Date: 3/20/2007 2:14:00 PM Lab 1D: 0703166-06A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW-846 METHOD 8270 2-Chloronephthalene 2-Chlorophenol 2-Methylnaphthalene 2-Methylphenol 2-Nitroaniline 2-Nitrephenol 3,3'-Dlchlorobenzidine 3+4-Mothy[phenol 4,0-Dinilro-2-methylp henol 4-Bromophenyl phenyl ether 4-Chloro-3-methylphenol 4-Chlomaniline 4-Chloraphenyl phenyl ether 4-Nitroaniline 4-.Nitmphenol Acenaphthene Acenaphthylene Aniline Anthracene Azobenzene Benzidlne Benze(a)anthracene Benzo(a)pyrane I~enzo(b)~uoranthene Benzo(g,h,Opelylene Benzo(k)fluoranthene Benzoic acid Benzyl alcohol Bis(2-chloroet boxy)methane Bis(2-~hloraethyl)ether Bis(2-chloroisopropyl)ether Bis(2.ethylhexyl)phthalate Butyl benzyl phthalate Carbazole Chrysene Dibenzo(a,h)enth racene Dibenzofuran Diethyl phthalate SW8270D SW3550A Analyst: PT U 130 pg/Kg~lry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 Fg/Kg-dry I 3/23/2007 7:22:00 PM U 130 pg/Kg~ry 1 3~23~2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7;22:00 PM U 130 pg/Kg-dry I 3/23/2007 7:22:00 PM U 130 po/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22;00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 IJg/Kg~ry 1 3/23/2007 7:22:00 PM U 130 pglKg~dry I 3/23/2007 7:22:00 PM U 130 pglKg~ry I 3/23/2007 7:22:00 PM U 130 pg/Kg-dry I 3/23/2007 7:?.2:00 PM U 130 pglKg-dry 1 3/23/2007 7:22:00 PM U 160 pg/Kg~lry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3123/2007 7:22:00 PM U 130 iJg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg~ry 1 3/2312007 7:22:00 PM U 130 pglKg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg~ry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 312312007 7:22:00 PM U 130 ~Jg/Kg~ry 1 3/23/2007 7:22:00 PM U 130 [ag/Kg. dry 1 3/23/2007 7:22:00 PM U 130 pglKg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22;00 PM U 130 pg/Kg-d~y I 3/23/2007 7;22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22;00 PM U 130 Fg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg,'Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22;00 PM U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry I 3/23/2007 7:22:00 PM U 130 pglKg<lry I 3/23/2007 7:22:00 PM U 130 I~g/Kg-d~ 1 3/23/2007 7:22:00 PM U 130 pglKg-d~y 1 3/23/2007 7:22:00 PM U 130 pg/Kg-dry I 3/23/2007 7:22:00 PM B Analyte detected in tl~= associated Method Blank Holding times for preparation or analysis =xceeded ND Not Detected at the Reporting Limit U Indicales thc compound was analyzed l'or but not dctectc Value above quantitntion nmg¢ Analyte detected Below quantitation limits Spike Recovery outside accepted recovery limits Value ex~eds Mttximum Contaminant L~v¢l Page 27 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Groeser Consulting Client Sample ID: No. 1 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Grcenport, N.Y. Collection Date: 3/20/2007 2:14:00 PM Lab ID: 0703166-06A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW~846 METHOD 8270 SW8270D SW3580A Analyst: PT Dimethyl phthalate U 130 pg/Kg-d~y 1 3/23/2007 7:22:00 PM Di-n-bubjl phthalate U 130 pg/Kg-dry I 3/23/2007 7:22:00 PM Di-n-octyl phthalate U 130 pg/Kgq:lp] 1 3/23/2007 7:22:00 PM Fluoranthene U 130 Ilg/Kg-dry 1 3/23/2007 7:22:00 PM Fluorene U 130 pglKg<lry I 3/23/2007 7:22:00 PM Hexachlorobenzene U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM Hexachlombutadiene U 130 pgIKg-dry 1 3/23/2007 7:22:00 PM Hexachlorocyclope ntadlene U 160 pg/Kg-dry 1 3/23/2007 7:22:00 PM Hexachloroethane U 13i1 pg/Kg-dry I 3/23/2007 7:22:00 PM Indeno(1,2,3-c,d)pyrene U 130 pg/Kg-dry 1 3/23/2007 7:22:00 PM Isophomne ti 130 pg/Kg~lry 1 3/23/2007 7:22:00 PM Naphthalene U 130 pglKgql~, 1 3/23/2007 7:22:00 PM Ngrobenzene U 130 pglKg-d~y 1 3/23/2007 7:22:00 PM N-Nilrosodimethylamine U 130 pg/Kg-d~y 1 3/23/2007 7:22:00 PM N-Nitrosodi-n-propylamine U 130 pg/Kg-d~y I 3/23/2007 7:22:00 PM N-Nitrosodiphenylamine U 130 FglKg-dry I 3/23/2007 7;22:00 PM Pentachlorophenol U 160 pgA<g.dry I 3/23/2007 7:22:00 PM Phenanthrene U 130 I~g/Kg-d~y 1 3/23/2007 7:22:00 PM Phenol U 130 gglKg-dry 1 3/23/2007 7:22:00 PM Pyrene U 130 pg.'Kg-dry I 3/23/2007 7:22:00 PM Pyridine U 130 pgtKg-dry 1 3/23/2007 7:22:00 PM Sum 2,4,6-Tribromophenol 47.1 22-124 %REC 1 3/23/2007 7:22:00 PM Sun.: 2-Fluombiphenyl 75.4 27-119 %REC I 3/23/2007 7:22:00 PM Sum 2-Fluoropheanl 89.1 21-123 %REC 1 3/23/2007 7:22:00 PM Sun': 4--Terphenyl-dl 4 74.5 28-125 %REC 1 3/23/2007 7:22:00 PM Sure Nitmbenzene-d5 64.9 21-118 %REC 1 3~23~2007 7:22:00 PM Surr: Phenol-dB 92.2 18-129 %REC I 3/23/2007 7:22:00 PM VOLATILE SW,-846 METHOD 8260 SW8260B Analyst: LDS l,l,l,2-Tetrachloroethane U 5.8 [~g/Kg-dry 1 3/21/2007 8:31:00 PM 1,1, l-Trichloroethane U 5.8 pglKg-d~ 1 3/2112007 8:01:00 PM l,l,2,2-Tetrachloroethane U 5.8 pglKg-dry I 3/21/2007 8:31:00 PM 1,1,2-Ttichloro.1,2,2-trifluoroethane U 5.B ~JglKg-dp/ I 3/2112007 8:31:00 PM 1.1,2-Td¢hlomethane U 5.6 pglKg-dp/ I 3/21/2007 8:31:00 PM 1,1-Dichlomethane U 5.8 pg/Kg-dry I 3/21/2007 8:31:00 PM 1. I -Dichloroelhene U 5.8 pglKg.-dry I 3/21/2007 8:31:00 PM 1, t-Dichlompmpene U 5.8 pglKg-d~y 1 3/2112007 8:31:00 PM 1,2,3-Tfichlombenzene U 5.8 pglKg-d~y 1 3/21/2007 8:31:00 PM 1,2,3-Trichlompmpane U 5.8 iJg/Kg-d~t I 3/21/2007 8:31:00 PM 1.2,4,5-Tetramethylbenzene U 5.8 pglKg~dry I 3/21/2007 8:31:00 PM Qualifiers: B Analyle detected in thc associated Method Bla~tk H Holding times for preparation or anaI~is exce=ded ND Not Detected at the Reporting Limit U Indicntes the compound was analyzed for but not &creole Page 28 of 70 American Analytical Laboratories, LLC. Date: 28-Mtn'-OZ CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane GreenpoH, N.Y. 0703166-06A Client Sample ID: No. 1 [10-12.5'] Tag Number: Collection Date: 3/20/2007 2:14:00 PM Matrix: SOIL Analyses Result VOLATILE 8W-846 METHOD 8260 1,2,4-Trichlorobenze ne U 1,2,4-Trimet hy[benzene U 1,2-Dibmmo-3-¢hlompmpane U 1,2-Dibmmoethane U 1,2-Dichlombenzene U 1.2-Dichloroethane U 1,2-Dichloropropane U 1,3,5-Trimethylbenzene U 1,3-Dichlombenzeae U 1,3-dichlompmpane U 1,4-Dichlorobenzene U 2,2-Dichlompropane U 2-Butanone U 2-Chloroethyl vinyl ether U 2-Chlorotoluene U 2-Hexa~one U 2-Propane[ U 4-Chlomtoluene U 4-1sopmpy[tuluene U 4-Methyl-2-pentanone U Acetone U Acmlein U Acrylenitdle U Benzene U Brom~benzene U Bromochlommethane U Bromodichlommethane U Bromoform U Bromomethane U Carbon disulfide U Carbon tetrachloride U Chlorobeazene U Chlomdiflueromethane U Chlomethane U Chloroform U Chloromethane U cis-1,2-Dichteroethene U cis-1,3-Dichloropropene U Dibromochloromathane U Limit Qual Units SW82608 5.8 pglKg-d~j 5.8 pg/Kg-dPj 5.8 pg/Kg-dry 5.3 pg/Kg-dry 5.8 pg/Kg-dry 5~8 pg/Kg-dry 5.8 pg/Kg<fry 5.8 pg/Kg~ry 5.8 pg/Kg-dry 5.8 pg/Kg-dry 5.8 pg/Kg-dry 5.8 pg/Kg<lry 5.8 ~g/Kg-clry 5,8 pg/Kg-dp/ 5.8 pg/Kg-dry 5,8 58 pg/Kg-d~y 5.8 pg/Kg-dry 5.8 pglKg-dry 5.8 pglKg-dry 5.8 pgtl(g-dry 29 pg/Kg<lry 5.8 pg/Kg-d~t 5.8 pg/Kg-dry 5.8 pg/Kg-dry 5.8 pg/Kg.-dry 5.8 ~g/Kg-dry 5.8 pg/Kg-d~ 5.8 pglKg-dB~ 5.8 pg/Kg~lry 5.8 pg/Kg-d ~J 5.8 pg/Kg..dPJ 5.8 pg/Kg-dry 5.8 pglKg-dB~ 8.8 pg/Kg-dry 5.8 pg/Kg--dly 5.8 pg~Kg-dly 5.8 pglKg-dry 5.8 pglKg-dPJ DF Date Analyzed Analyst: LDS 3/2t/2(307 8;31;00 PM 3/21/2007 8:31;00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31 :DO PM 3/21/2007 8;31:00 PM 3/2112007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31;0(3 PM 3/21/2[307 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/2112007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:3t:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8;31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8;31:00 PM 3121/2007 8:31:00 PM 3/21/20(37 8:31:00 PM 3/21/2007 8:31:00 PM 3/21/2007 8:31:00 PM Qualifiers: B Analyte detected in the associated Me(3]od Blank H Holding timm for p~¢paration or analysis exceeded ND Not l~tectcd at ~ R~potting Limit Page 29 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 1 [10-12,5'] Lab Order: 0703166 Tag Number: Project: Mantas Lane Greenport, N.Y. Collection Date: 3/20/2007 2:14:00 PM Lab ID: 0703166-06A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-846 METHOD 8260 SWg2601~ Analyst: LDS Dibromomathane U 5.5 I~g/Kg<Jry 1 3/21/2007 8:31:00 PM D[chlorodifluommethane U 5.8 pglKg-dry 1 312112007 6:31:00 PM Diisopropyl ether U 5.8 faglKg-dry 1 3121 ~2007 8:31:00 PM Ethanol U 29 pg/Kg-dry 1 3/21/2007 8;31:00 PM Ethyl acetate U 8.8 ~glKg-dry 1 3/21/2007 8:31:00 PM Ethylbanzene U 5.8 fag/Kg-dry 1 3/2112007 8:31:00 PM Freon.114 U 5,8 1~9/Kg-dry 1 3/21/2007 8:31:00 PM Hexachlorobutadiene U 5.8 IJg/Kg-dry I 3/21/2007 8:31:06 PM tsopropyl acetate U 5.8 gglKg-dry I 3/2t/2907 8:31:00 PM Jsoprol~yJbenz_ene U 5.6 fa§lKg-dry 1 3/21/2007 8:31:00 PM m,p-Xylsne U 12 fag/Kg-dry 1 3121/2007 8:31:09 PM Methyl tort-butyl ether U 5.8 IJg/Kg-dry I 3/21/2007 8:3t :00 PM Methylene chloride U 5.8 pg/Kg-~p/ 1 3/2112007 8:31:90 PM n-Amyl acetate U 5.8 fag/Kg-dry I 3/21/2067 8:31:00 PM Naphthalene U 5.8 fag/Kg-dry 1 3/21/2007 8:31:09 PM n-Butyl acetate U 5.6 IJg/Kg-dP/ I 3/2112007 8:31:00 PM n. Butylbenzene U 5.8 gg/Kg-dry 1 3/21/2007 8:31:00 PM n-Propyi acetate U 5.8 faglK9-dry I 3/21/2097 8:31:00 PM n-Propylbenzene U 5.6 fag/Kg-dry 1 3121/2007 8:31:00 PM o-Xylene U 5.8 IJg/Kg-dry I 3/2112007 8:31:00 PM p-Diethylbenzene U 5.6 ~JglKg-dry 1 3/21/2007 8:31:00 PM p-Ethygoluene U 5.8 fag/Kg-dry t 3/21/2007 8:31:00 PM sec-Butylbenzene U 5.8 I~g/Kg-dry 1 3/2112007 8:31:00 PM Styrene U 5,5 gg/Kg-dry I 3/21/2007 8:31:00 PM t-Butyl alcohol U 5.8 I~glKg-dry 1 3/2t/2007 8:31:00 PM tert-Butylbenzene U 5.8 pglKg-dry I 312112007 8:31:00 PM Tetrachlamethene U 5.8 pgtKg-dry I 3/21/2007 8:31:06 PM Toluene U 5.8 pg/Kg-dry 1 3/21/2007 8:31:00 PM frans-1,2-Dichlaroethene U 5.8 pglKg-dry 1 ~21/2007 6:31:00 PM trans-l,3-Dlchfopopropnne U 5.8 fag/Ko-dry 1 3/21/2007 8:31:00 PM THchlomethene U 5.6 pg/Kg-dry 1 3/21/2007 8:31:0ff PM Trichlomguoromethane U 5.8 I~g/Kg-dry 1 3/21/2007 8:31:00 PM Vinyl acetate U 5.6 pglKg-dry 1 3/2112007 8:31:00 PM V~nyl chloride U 5.8 pg/Kg-dry I 3/21/2007 6:31:00 PM Sum 4-Bromafluorobenzene 98.6 61-133 %REC 1 3/21/2007 8:31:00 PM Surr: Dibromofluommethane 113 61-139 %REC 1 3/21/2007 8:31:D0 PM Sure Toluene-d8 97.5 57-131 %REC I 3121/2007 8:31:00 PM Qualifiers: B Analyle detected in the associated Method Blank H Holding tim~s for pmparatlon or analysis exceeded ND Not Detected at thc Rcpo~.ing Limit U indiactes the compound was annlyzed l'or but not det¢cte Value above quanlitctJon range Analytc detected below quantitadon limits Spike Rccovc~ outside accepted recovery limits Value exceeds Maximum Contaminant Level Page 30 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moores Lane Greenpo~,N.Y. 0703166-07A Client Sample 1D: No. 6 [10-12.5'] Tag Number: Collection Date: 3/20/2007 2:40:00 PM Matrix: SOIL Analyses Result Limit Qual MERCURY SW7471 B Mercu~J U 0.0105 PERCENT MOISTURE 02216 Percent Moisture 5.00 0 TARGET ANALYTE LIST METALS SW6010B Aluminum 1900 0.410 Antimony U 0.512 Arsenic 0.617 0.512 Barium 9.86 0.410 Beryllium U 0.410 Cadmium U 0.205 Calcium 137 0.512 Chromium 5.70 0.410 Cobalt U 0Al0 Copper 4.04 0.410 Imn 3080 0.410 Lead 2.94 0.307 Magnesium 405 0.410 Manganese 79.1 0.410 Nickel 2.64 0,410 Potassium 340 2.05 Selenium U 0.512 Silver U 0.4'10 Sodium 38.5 1.23 Thallium U 0.410 Vanadium 7.93 0.410 Zinc 8.67 0.410 SEMIVOLATILE SW-846 METHOD 8270 SW82700 1,2,4-Trichlo re benzene U 130 1,2.Dichlorobenzene U 130 1,3-DIchlorobenzene U 130 1,4-Dichlorobenzene U 130 2,4,5-Tdchlorophenol U 130 2,4,6-Trichlorephenol U 130 2,4-Dichlorophenot U 130 2,4-Dimethylphenol U 130 2,4-Din~ophenol U 130 2,4-Dinitrotolueee U 130 2,6-Dinitrololuene U 130 Units DF SW74715 rog/Kg-dry wt% 1 SW3050A mglKg-dry mg/Kg<Jry 1 mg/Kg<~ry 1 mg/Kg-dry 1 mglKg-dry 1 mg/Kg-dry rog/Kg-dry 1 mg/Kg-dry 1 mg/Kg-dry 1 rog/Kg-dry 1 rog/Kg-dry 1 rog/Kg-thy 1 mglKg-dry 1 rog/Kg-dry 1 mglKg-dry mglKg-dry 1 mg/Kg-dry 1 mg/Kg-clry 1 rog/Kg-dry 1 mglKg-dry 1 mglKg-d~/ 1 mg/Kg~ry 1 SW3550A pglKg--d~y gg/Kg-dry pg/Kg-d~ pglKg-dry pg/Kg-dry pglKg-dry pgtKg-dry pg/Kg-dry pg/Kg-dry pglKg-dry pg/Kg-dry Date Analyzed Analyst: WN 3/23/2007 1:38:54 PM Analyst: CM 3t22/2007 Analysl: JP 3/23/2007 2:29:49 PM 3~2312007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3123/2007 2:29;49 PM 3/23/2007 2:29:49 PM 3/23/2007 2:25:40 PM 3/23/2007 2:29:49 PM 3/23/2007 2:29:49 PM 3~23~2007 2:29:49 PM 3/23/2007 2:29:49 PM 3/'23/2007 2:29:49 PM 3/23/2007 2:29:49 PM Analyst: PT 3/23/2007 7:50:00 PM 3/23/2007 7:50:00 PM 3~23~2007 7:50:00 PM 3/23/2007 7:50:00 PM 3/23/2007 7:50:00 PM 312312007 7:50:00 PM 3/23/2007 7;5a:00 PM 3/2312007 7:50:00 PM 3/23/2007 7:50:00 PM 312312007 7:50:00 PM 3/23/2007 7:50:00 PM Qualifiers: S Analyte detected in thc ussocialcd Mcillod Blank H Holdin§ times for preparation or analysis cxc¢cdcd ND Not Detected at the R~orting Limit U Indicates thc compound was analyzcd for but not datccte Page 31 of 70 American Analytical Laboratories, LLC. Date: 2S-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 6 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 2:40:00 PM Lab ID: 0703166-07A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW82700 swafiSOA Anatyst: PT 2-Chloranaphthalene U 130 pglKg-dry 1 3/23/2007 7:50:00 PM 2-Chlorophenol U 130 pglKga:lry I 3/23/2007 7:50:00 PM 2-Methylnaphthalene U 130 pg/Kg~l~ 1 3/23/2007 7:50:00 PM 2-Methylphenol U 130 Izg/Kg~d~ I 3/23/2007 7:50:00 PM 2-Nitroaniline U 130 ~glKg-(J~ 1 3/23/2007 7:50:B0 PM 2-Nitrophenol U 130 pg/Kg<Jry 1 3/23/2007 7:50:00 PM 3,3'-Dichiorobenzidine U 130 pg/Kg-dry 1 3/23/2007 7:50:00 PM 3+4-Methyiphenol U 130 pglKg~lry' 1 3/23/2007 7:50:00 PM 3-Nitroaniline U 130 pg/Kgod~y I 3/23/2007 7:50:00 PM 4,6-Dinitro-2-methylphenol U 130 pg/Kg-d~ 1 3/23/2007 7:50:00 PM 4-Bromophenyl pheny] ether U 130 pg/Kg-dry 1 3/23/2007 7:50:00 PM 4-Chlom-3-m ethylphe n ci U 130 pglKg-dry 1 3/23/2007 7:50:00 PM 4-Chloroaniline U 130 iJglKg-dry I 3/23/2007 7:50:00 PM 4-Chlorophenyl phenyl ether U 130 pg/Kg-dry 1 3/23/2007 7:50:00 PM 4-Nitroaniline U 130 pg/l(g-diy 1 3~23~2007 7:50:00 PM 4-Nitrophenol U 160 pg/Kg-d~y I 3/23/2007 7:50:00 PM Acenaphthene U 130 pg/Kg-d~y 1 3/23/2007 7:50:00 PM Acenaphthylene U 130 pglKg-dry 1 3/23/2007 7:50:00 PM Aniline U 130 pglKg~lry I 3/23/2007 7:50:00 PM Anthracene U 130 pglKg-dly 1 3/23/2007 7;50:00 PM Azobenzene U 130 pg/Kg-clp/ I 3/23/2007 7:50:00 PM Benzidine U 130 pglKg~y 1 3/23/2007 7:50:00 PM Benzo(a)anthracone U 130 pg/K§-d~y 1 3/23/2007 7:50:00 PM Benzo(a)pyrene U 130 IJglKg-clry I 3/23/2007 7:50:00 PM Benzo(b)fluoranthene U 130 pglKg<lry 1 3/23/2007 7:50:00 PM Benzo(g,h,i)peryreco U 130 pg/Kg-thy 1 3/23/2007 7:50:00 PM Benzo(t()fluoranthene U 130 pg/Kg~l~ 1 3/23/2007 7:50:00 PM Benzoic acid U 130 pglKg-dry 1 3/23/2007 7:50:00 PM Be~zyl alcohol U 130 pg/Kg-dry 1 3/23/2007 7:50:00 PM Bis(2-chlomethoxy)methana U 130 I~g/Kg-dry 1 3/2312007 7:50:00 PM Bis(2-chlomethyl)ether U 130 pg/Kg-dry I 3/23/2007 7:50:00 PM Bis(2-¢hlomlsopropyl)ether U 130 IJgtKg-dry I 3/23/2007 7:50:00 PM Bis(2-ethylhexyl)phthalate U 130 pg/Kg-dry 1 3/23/2007 7:50:00 PM Butyl benzyl phthalate U 130 pglKg-dry 1 3/23/2007 7:50:00 PM Carbazole U 130 UB/KB-d~y I 3/23/2007 7;50:00 PM Chrysene U 130 IJg/Kg-dry I 3/23/2007 7:50:00 PM Dibenzo(a,h)anthracene U 130 pglKg-dry I 3/23/2007 7:50:00 PM Dlbenzofuran U 130 p§/Kg-dry 1 3/23/2007 7:50:00 PM Diethyl phthalate U 130 ]Jg/Kg-d~y I 3/23/2007 7:50:00 PM Qualifiers: B Analytc detected in thc ossociatc~l Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Repot[Jug Limit Value above quantitatlon range Analyle detected below quantilation limits Spike Recovci3, outside accepted recovery limits Value exceeds Mmtimum Contaminant L~vel Page 32 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 6 [10-12.5'] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 2:40:00 PM Lab ID: 0703166-07A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE 8W-846 METHOD 8270 SW82705 SWa550A Analyst: PT Dimethyl phthalate U 130 pg/Kg-dry I 3/23/2507 7:50:00 PM Di-n-butyl phthalate U 130 pg/Kg-dry I 3/23/2507 7:50:00 PM Di-n-octyl phthalale U 130 I~glKg-dry 1 3/23/2007 7:50:00 PM Fluorartihene U 130 uglKg-dPJ 1 3/23/2007 7:50:09 PM Fluomne U 130 pg/Kg-dry I 3/23/2097 7:50:00 PM Hexachlorobenzene U 130 I~g/Kg-dry I 3/23/2507 7:50:00 PM Hexachlorobutadlene U 130 pg/Kg.dry 1 3/23/2007 7:50:00 PM Hexachlerocyclopentadlene U 160 pgtKg-dry 1 3/23/2507 7:50:00 PM Hexachloroethane U 130 pg/Kg-d~ 1 3/23/2007 7:50:00 PM Indeao(1,2,3..c,d)pyrene U 135 ug/Kg-dry I 3/23/2057 7:50:00 PM Isophomne U 130 pg/Kg-d~y 1 3/23/2007 7:50:00 PM Naphthalene U 130 IJg/Kg-d~y 1 3/23/2007 7:50:00 PM Nitrobenzene U 130 pg/Kgq:lry I 3/23/2007 7:50:00 PM N-Nitrosodimethylamine U 130 pglKg~t 1 3/23/2807 7:50:00 PM N-Nitmsodi-n-propylamine U 130 pgAKg-d~y 1 3/23/2007 7;50:00 PM N.Nitmsodiphenylamine U 130 pglKg-dry 1 3/23/2007 7:50:00 PM Pentachthrophenol U 160 pg/Kg-dry I 3/23/2007 7:50:00 PM Phenanthrene U 130 pglKgq:lry I 3/23/2007 7:59:00 PM Phenol U 130 IJg/Kg-dry I 3/23/2007 7:50:00 PM Pyrene U 130 pg/Kg-dnJ 1 3/23/2007 7:50:00 PM Pyridine U 130 pglKg~ry I 3/2312007 7:50:00 PM Sum 2,4,6-Tfibromophenol 53.8 22-124 %REC I 3/23/2097 7:50:00 PM Sum 2-Fluorobiphenyl 68.6 2%119 %REC 1 3/23/2007 7:50:60 PM Surf: 2.Fluorophenol 87.9 21-123 %REC I 3/23/2007 7:50:00 PM Sum 4-Terpheny~-d14 67.2 28-125 %REC 1 3/23/2007 7:50:00 PM Sum N[trobenzene-d5 63.4 21-118 %REC 1 3/23/2607 7:50:0[3 PM Sum Phenol-d6 85.3 18-129 %REC 1 3123/20fl7 7:58:00 PM VOLATILE SW-846 METHOD 8260 SW8260B Analyst; LDS 1,1,1,2-Tetrachlomethane U 6.3 pg/Kg~lry I 3/21/2907 9:19:00 PM 1,1,1-Trichloroethane U 6.3 pg/Kg-d~ 1 3/21/2007 9:19:99 PM 1,1,2,2-Tetrachloroet hane U 6.3 pglKg-dry 1 3/21/2007 9:19:00 PM 1,1,2-T[ichloro-1,2,2-tdfluomethane U 6.3 pglKg~lry I 3/21/2007 9:19:00 PM 1,1,2-Trichlomethane U 6.3 pg/Kg.dry 1 3/21/2007 9:19:00 PM 1,1-Dichlomethane U 6.3 IJglKg-dry 1 3/21/2007 9:19:00 PM 1.1-Dich[oreethene U 6.3 pg/Kg~J 1 3/21/2007 9:19:09 PM l,l-Dk:hloropropene U 6.3 pg/Kg~J I 3/21/2007 9:19:00 PM 1,2,3-Trichlorobenzene U 6.3 pglKg-dry 1 3/21/2007 9:t9:00 PM 1,2,3-Trichloropropane U 6.3 pglKg-dry I 3/21 ~2007 9:19:09 PM 1,2,4,5-Tetramethylbenzene U 6.3 pg/Kg-d~J 1 3/21/2007 9:19:00 PM Qaallfiers: B Analyt¢ detested in the associated Method Blank Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit D Indi*atcs thc r. ompound w~ analyzed for but not det¢cte Pa§e 33 of 70 American Analytical Laboratories, LLC. Date: 2a-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Greaser Consulting 0703166 Moores Lane Greenpon, N.Y. 0703166-07A Client Sample ID: No. 6 [10-I2.Y] Tag Number: Collection Date: 3/20/2007 2:40:00 PM Matrix: SOIL Analyses VOLATILE SW-$46 METHOD 8260 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-chloropropane 1,2-Dibmmoethane 1,2-Dichlorobenzene 1,2-Dichlomethane 1,2-Dichlompropane 1,3,5-Tdmethylbenzene 1,3-Dinhinrobenzene 1.3-~lchinropropane 1,4-Didalorobenzene 2~2-Diohloropmpane 2-Butanene 2-Chinroethyl vinyl ether 2-Chlomtoluene 2-Hexanone 2-Propanol 4-Chlorotoluene 4-tsopropyltoluene 4-Methyl-2-pentanone Acetone Acroleln Ac~lonitrile Benzene Bromebenzene Bremochlommethane Hromod[chleromethane Bromomethane Carbon disulfide Cadaon tetrachloride Chlorobenzene Chlorodifluoromethane Chloroethane Chloroform Chlommethane cis*1,2-Dichloroethena cis-1,3.Dichlompropene Dibromochloromethane Result Limit Qual Units SW8260B U 6,3 pg/Kg-dry U 6.3 U 6.3 uglKg-drY U 6.3 pglKg-dry U 6.3 ug/Kg-dry U 6.3 pg/Kg-dly U 6.3 gg/Kg-d~J U 6.3 pglKg-dqt U 6.3 i~g/Kg-dn/ U 6.3 pg/Kg-d[y U 6.3 pglKg-dP/ U 6.3 pglKg-d~ U 6.3 pglKg<~ly U 6.3 pg/Kg-dPJ U 6.3 pg/Kg-dry U 6.3 pglKg-dPJ U 63 pglKg~/ U 9.3 pg/Kg-dP/ U 6.3 pglKg-dry U 6.3 ~JglKg-dry U 6.3 pg/Kg-d~ U 31 ug/gg-d[y U 6.3 pg/Kg-do/ U 6,3 ug/Kg<try U 6.3 pg/Kg~by U 6.3 pg/Kg-d~J U 6.3 pg/Kg-dry U 6.3 pg/Kg<l~J U 6.3 pg/Kg-d~J U 6.3 IJglKg-dPJ U 6.3 ~g/Kg~ry U 6.3 pglKg-dry U 6.3 pglKg.dry U 6.3 pg/Kg-dry U 6.3 ~g/Kg~iry U 6.3 pglKg-dPJ U 6.3 pg/Kg-dry U 6.3 pglKg~ry U 6.3 pglKg-dry DF Date Analyzed Analyst: LDS 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/2112007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2097 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21t2007 9:19:00 PM 3/2112007 9:19:00 PM 3/2112007 9:19:00 PM 312112007 9;19:00 PM 3/2112007 9:19:90 PM 312112007 9:19:(30 PM 312112007 9;19:00 PM 3121f2007 9:19;00 PM 312112007 9:19:00 PM 3/21/2007 9:19:00 PM 3/2112007 9:t9:00 PM 312112007 9:19:00 PM 3/2112007 9:19:00 PM 3/21/2007 9:19:00 PM 3/2112007 9:19;00 PM 3/2112007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 312112007 9:19:00 PM 3/2112007 9;19:D0 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/2112007 9;19:00 PM 3121/2007 9:19:00 PM Qualifiers: Analyte detected in thc associated M¢fllotl Blank' H Holding times for preparation or analysis exceeded ND Not Detected at the ReporlJng Limit Vahc above quantitation range Aaalyie detected below quaatitatinn limits Spike Recoveqt outside accepted rccoveq* limits Value exceeds Maximum Contaminant Level Page 34 of'70 American Analytical Laboratories, LLC. Date: 28-3,10r-07 CLIENT: P.W. Grosset Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Moores Lane Greenpart, N.Y. Collection Date: Lab ID: 0703166-07A Matrix: No. 6 [10-12.5'] 3/20/2007 2:40:00 PM SOIL Analyses Result Limit Qual Units DF VOLATILE SW-846 METHOD 8260 SW8260B Dibromomethane U 6~3 pglKg-dry i Dichlerodifluorom ethane U 6.3 pg/Kg-dry 1 Diisopropyr ether U 6.3 pg/Kg-dry 1 Ethanol U 31 pg/K9-d~ 1 Ethyl acetate U 5.3 pg/Kg-d~y 1 Ethylbenzene U 5.3 pg/Kg-d~y 1 Freon-114 U 6.3 ~JglKg-dry 1 Hexachlorobutadiene U 9.3 FglKg-dry I Isopmpyl acetate U 5.3 pg/Kgq:lry Isopropylbenzene U 6.3 pg/Kg-dry m,p-Xylene U 13 tJg/Kg-dry 1 Methyl tert4~utyl ether U 6.3 pg/Kg-dty 1 Methylene chloride U 6.9 pg/Kgq~ry 1 n-^myl acetate U 6.3 IJg/Kg-dry 1 Naphthalene U 6.3 pg/l(g-dty 1 n-Butyl acetate U 6.3 pglKg-dry 1 n-Butylbenzene U 6.3 pg/Kg-dry 1 n-Propyl acetate U 6.3 pg/Kg-d~y 1 n-Propylbenzene U 6.3 pg/Kg-dp/ 1 o-Xylene U 6.3 pg/Kg-dry 1 I>-Diethylbenzene U 6.3 FgtKg-dry 1 p-Ethyltoluene U 6.3 pglKg-dty 1 sec-Butylbenzene U 6,3 JJglKgq:lry I Styrene U 6.3 pgtl<g-dry 1 t-Butyl alcohol U 8.3 gg/Kg-dty 1 tert-Elutylbenzene U 6.3 pglKg-dry 1 Tetrachloroethene U 6.3 pg/Kg~lry 1 Toluene U 6.3 Po/Kg-dry 1 trans-1,2-Diohlometheoe U 6.3 pg/Kg-dry 1 trans-1,3-D[chlompropene U 6.3 IJglKg-dry 1 Trichlomethene U 6.3 pg/Kg-dry 1 Tdehlomfluoromethane U 6.3 pg/Kg-dty 1 Vinyl acetate U 6.3 IiglKg-dP/ 1 Vinyl chloride U 6.3 pg/Kg-dry 1 Sum. 4-Bromofluorobenzene 96.1 61-133 %REC 1 Surr: Dibmmofluommethane 105 61-139 %REC 1 Sum. Toluene-d8 95.8 57-131 %REC 1 Date Analyzed Analyst: LDS 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3121/2097 9:19:00 PM 9/21/2007 9:19:00 PM 312112007 9:19:00 PM 3121/2007 g:19:00 PM 312112007 9:19:00 PM 3/21/2007 9:19:00 PM 3121/2007 9:19:00 PM 3/21/2007 g:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3121/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3121/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 312112007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3121/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9;19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM 3/21/2007 9:19:00 PM Qualifiers: Analytc dctcclcd in thc associated Method Blank Holding tim~s for preparation or analysis exceeded ND Not Detected at thc Reporting Limit U Indicatm thc compound was analyzed for but not dciccte Page 35 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moores Lane Greenpo~,N.Y. 0703166-08A Client Sample ID: Tag Number: Collection Date: Matrix: No. 8 [aw] 3/20/2007 10:07:00 AM LIQUID Analyses MERCURY Mercury TARGET ANALYTE LIST METALS Aluminum Antimony Arsenic Barium Beryllium Cadmium Calciuro Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel Potassiuro Selenium Silver Sodium Thallium Vanadium Zinc SEMIVOLATILE SW-846 METHOD 8270 1,2,4-Trlchlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlombenzene 2,4,5-Trishlorophenol 2,4,6-Ttichk3rophenol 2,4-Dichloropbenol 2,4-DImethylphenol 2,4-Dinitrophenot 2,4-D[nitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chloraphenol Result Limit Qual Units SW7470A U 0.000200 mglL $W60105 SW3010A 227 0.0200 mglL 0.0453 0.0250 mg/L 0.206 0.0250 rog/L 0.575 0.0200 mglL U 0.0200 mglL U 0,0100 rogtL 36.6 0.0250 mg/L 0.395 0.0200 mg/L U 0.0200 mg/L 0.489 0.0200 mglL 973 0.200 rog/L 0.187 0.0150 mg/L 23.4 0.0200 mglL 5,68 0.0200 mglL 0.276 0.0200 mg/L 31.0 0.100 mglL U 0.0250 mglL U 0,0200 mglL 15.7 0.0300 mg/L U 0.0150 roglL 0.699 0.0200 rog/L 0.577 0.0200 rog/L SW8270D SW3510 U 5.1 pg/L u 5.1 pg/L U 5,1 pg/L U 5,1 pg/L U 5.1 pglL U 5.1 pglL U 5.1 pglL U 10 pg/L U 5.1 pglL U 5.1 pg/L U 5.1 pg/L U 5.1 pg/L DF Date Analyzed Analyst: WN 3/23/2007 12:02:26 PM Analyst: JP 1 3/23/2607 9:42:26 AM I 3/23/2007 9:42:26 AM 1 3/23/2007 9:42;26 AM 1 3/23/2007 9:42:26 AM I 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 10 3/23/2007 10:15:17 AM 1 3123/2007 9:42:26 AM I 3~23/2007 9:42:26 AM I 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM I 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM 1 3/23/2007 9:42;26 AM I 3/23/2007 9:42:26 AM 1 3/23/2007 9:42:26 AM Analyst: RN 3/26/2007 6:16:00 PM 3/26/2007 6:10;00 PM 3/26/2907 6:10:00 PM 6/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6;10:00 PM 312612007 6:10:00 PM 3/25/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/2612007 6:10:00 PM 3/2512007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM Qualifiers: E Valuc above quantitaSon range J Analyte detcctad below qutmtitation limits S Spike RecovcD, oulsidc ncccpted mcovcr~ limits X Value exceeds Maximum Contaminant Level Page 36 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 8 [GW] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 10:07:00 AM Lab ID: 0703166-08A Matrix: LIQUID Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 Analyst: RN 2-Methylnaphthalene U 5.1 I~g/L I 3t26/25507 6:10:00 PM 2-Methylphena[ U 5.1 [Jg/L I 3/26/2007 6:10:00 PM 2-NItmaniline U 5.1 I~glL 1 3/23/2007 6:10:00 PM 2-Nitmphenol U 5.1 ~g/L 1 3/26/2007 6:10:00 PM 3,3'.Dichlombenzidine U 5.1 I~g/L 1 3/26/2007 6:10:00 PM 3+4-Methylphenar U 5.1 [~g/L 1 3125512007 6:10:00 PM 3-Nitroanlline U 5.1 pg/L I 3/26/2007 6:10:00 PM 4,6-Dinitro-2-methylphenol U 5.1 !ag/L 1 3/26/2007 6:10:00 PM 4-Bromophenyl phenyl ether U 5.1 L~g/L 1 3/26/2007 6:10:00 PM 4-Chlore-3-methylphencfl U 5.1 pgtL I 3/26/2007 6:10:00 PM 4-Chloreanlline U 5.1 :ag/L 1 3/26/2007 6:10:00 PM 4-Chlorophenyl phenyl ether U 5.1 pglL I 3/26/2007 6:10:00 PM 4-Nitmanilina U 5.1 pg/L 1 3/26/2007 6:10:00 PM 4-Nitrophenel U 5.1 pg/L 1 3/25/2007 6:10:00 PM Acenaphthene U 5.1 pg/L 1 3/26/2007 6:10:00 PM Acenaphthylene U 5.1 [Jg/L 1 3/26/2007 6:10:00 PM Aniline U 5.1 ug/L 1 3/26/2007 6:10:00 PM Anthracene U 5.1 pg/L 1 3/26/2007 6:10:00 PM Azobenzene U 5.1 pg/L 1 3/26/2007 6:10:00 PM Benzldine U 5.1 pg/L 1 3/26/2007 6:10:00 PM Benzo(a)anthmcene U 5.1 pglL 1 3/26/2007 6:10:00 PM Benzo(a)pyrene U 5.1 Ltg/L I 3/26/2007 6:10;00 PM Benzo(b)fluoranthene U 5.1 [~g/L 1 3/255/2067 6:10:00 PM Benzo(g,h,i)perylene U 5.1 lag/L t 3/26/2007 6:10:00 PM Benzo(k}tluoranthene U 5.1 pgtL I 3/26/2007 6:10:00 PM Benzoic acid U 5.1 gg/L I 3/26/2007 6:10:00 PM Benzyl alcohol U 5.1 pg/L 1 3/26/2007 6:10:00 PM Bis(2-chlomethoxy)methane U 5.1 Isg/L 1 3/26/2007 6:10:00 PM Bis(2-chroro~thyl)et~r U 5.1 gglL 1 6/26/2007 6:10:00 PM Bisf2-chlaroisopropyl)ether U 5.1 pglL I 3/26/2007 6:10:00 PM Bis(2-ethythexyl)phthatate U 5.1 L~g/L I 3/26/2007 6:10:00 PM Butyl benzyl phthalate U 5.1 gglL 1 3/255/2007 6:10:00 PM Carbazole U 5.1 L~glL I 3/26/2007 6:10:00 PM Ch~ysene U 5.1 Ltg/L 1 3/26/2007 6:10:00 PM Dibenzo(a,h) anthracene U 5.1 ~g/L 1 3/26/2007 6:10:00 PM Dibenzofuren U 5.1 pglL '1 3/26/2007 6:10:00 PM Diathyl phthatate U 5.1 pg/L 1 3/26/2007 6:10:00 PM Dimeth¥1 phthalate U 5.1 l~g/L 1 3/26/2007 6:10:00 PM Di-n-butyl phthalate U 5.1 1~g/L 1 312612007 6:1[}:00 PM Qualifiers: Value ahoy= quantitadon range Analyle detected below quantitation limits Spike Recovery outside accepted rc.c, ove~ limits Value exceeds M~.ximum Contaminant Level Page 37 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moores Lane G~enpo~,N.Y. 0703166-08A Client Sample ID: No. 8 [GW] Tag Number: Collection Date: 3/20/2007 10:07:00 AM Matrix: LIQUID Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 Di-n-octyl phthalate U 5.1 pg/L Fluoranthene U 5,1 pg/L Fluorene U 5.1 pg/L Hexachiorobenzene U 5.1 I~g/L Hexachlorobutadiene U 5.1 I~g/L Hexachlorocyciopentadiene U 5.1 pglL Hexachloroethane U 5.1 pg/L Indeno(1,2,3-c,d)pyrene U 5.1 pglL Isophorone U 5.1 pg/L Naphthalene U 5. ! pglL Nitrobenzene U 5.1 pg/L N-Nitmsodimethylamioe U 5.1 pglL N-Nitrosodi-n-propylamine U 5,1 pglL N-Nitrosodiphenylamine U 5.1 pglL Pentachlorophenol U 5.1 pgtL Phenanthrene U 5.1 pg/L Phenol U 5.1 pg/L Pyrene U 5.1 pg/L Pyridine U 5.1 pg/L Sum 2,4,6-Tdbmmophenol 65.8 22-124 %REC Sum 2-Fluorobiphenyl 66.4 1~-124 %REC Sun:. 2-Fiuorophenol 47,5 16-112 %REC Surr: 4-TerphenyFd14 75.0 17-121 %REC Sum NItrobenzene-d5 64.4 19-115 %REC Sum Pheno]~16 28.6 12-102 %REC VOLATILE SW-846 METHOD 8260 SW82600 1,1,1,2-Telrachloroet h an e U 1.0 pg/L 1,1,2,2-Tetrachloroet hane U 1.0 pg/L 1,1,2-THchloro-1,2,2-trifluoroelhane U 1.0 pglL 1,1,2-Trichloroethane U 1.0 pg/L 1,1-Dichloroethane U 1.0 pglL 1,1 ~Dichlomethene U 1.0 pglL 1,1-Dtchloroprapene U 1.0 pg/L 1,2,3-Trtchlorobe ozone U 1.0 gglL 1,2,3-Trichlompmpane U 1.0 pg/L 1,2,4,5--Tetramethylbenzene U 1.0 pg/L 1,2,4-Trichlorobenzene U 1.0 uglL 1,2,4-Trimethylbenzene U 1.0 pg/L DF Date Annlyzed Analyst: RN 3/2fi/2007 6:10:00 PM 3/26/2007 5:10:00 PM 3/26/2007 6:10:00 PM 3/26/2607 6:10:00 PM 3/26/2007 0;10:00 PM 3/2612007 6:10:00 PM 3/2612007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3126/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM :3/26/2007 8:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/2612007 6:10:00 PM 3/26/2007 6:10:00 PM 3t26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM 312612007 6:10:00 PM 3/26/2007 6:10:00 PM 3/26/2007 6:10:00 PM Anaiysl: LDS 3/2112007 2:34:00 PM 3/21/2007 2:34:00 PM 312112007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/2112007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2::34:00 PM 312112007 2:34:00 PM Qualifiers: B Analyte delectcd in thc ~sociated Method Blank H Holding tim~s for prcparation or nnal~is cxcccdcd ND Not Detected at ibc Rcporiing Limit U Indicales thc compound ,.ms ~al~d for but not dclcctc Page 38 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-OZ CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenpo~,N.Y. 0703166-08A Client Sample ID: Tag Number: Collection Date: Matrix: No. 8 [ow] 3/20/2007 10:07:00 AM LIQUID Analyses Result VOLATILE 8W-846 METHOD 8260 1,2-Dibmmo-3-chloropropane U 1,2-Dibromoethane U 1,2-Dichlorobenzene U 1,2-Dichloroethane U 1,2-Dichlompmpane U 1,3,5-Trimethylbenzene U 1,3-Dichlerobenzene U 1,3.dichlompropane U 1,4-Dichlorobenzane U 2,2-Dichlompropane U 2-Butanone U 2-Chioroethyl vinyl ether U 2-Chlorotoluene U 2-Hexanone U 2-Pmpanol U 4-Chlorotoluene U 4-1sopropyltoluene U 4-Methyl-2-pentanone U Acetone U Acroletn U Acrylonitrile U Benzene U Bromobenzene U Bromochlommethane U Bromodichloromethane U Bromot'orm U Bmmomethane U Carbon disulfide U Carbon tetrachlodde U Chlorobenzene U Chloredifluommethaae U Chloroethane U Chloroform U Chloromethane U cis-1,2-Dichlomethene U cis-1,3-Dichloropropene U Dibrornochloromet ha ne U Dibmmomethane U Dichlo mdlfluoromethane U Liroit Qual SW82600 1.0 1.0 1.0 3.0 1.0 2.0 1.0 1.0 2.0 2.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 Units DF Date Analyzed Analyst: LDS pglL 1 312112007 2:34:00 PM IJg/L I 312112007 2:34:00 PM l~g/L 1 3/21/2007 2:34:00 PM ptg/L 'i 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 312112007 2:34:00 PM pg/l. I 3121/2007 2:34:00 PM pg/L 1 3/2112007 2:34:00 PM pglL 1 3/21/2007 2:34:00 PM pg/L 1 3121/2007 2:34:00 PM uglL 1 3/21/2007 2:34:00 PM pBIL I 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM IJg/L 1 3/21/2007 2;34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM Hg/L 1 3/2112007 2:34:00 PM pglL 1 3/2112007 2:34:00 PM pglL I 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pglL 1 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM pg/L I 3f2112007 2:34:00 PM pg/L I 3121/2007 2:34:00 PM pglL 1 3/21/2007 2:34:00 PM pglL I 3/2112007 2:34:00 PM Hg/L 1 3/21/2007 2:34:00 PM pg/L 1 3121/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 3/21/2007 2:34:00 PM pg/L 1 3/21/2007 2:34:00 PM pg/L I 312112007 2:34:00 PM Qualifiers: B Analyte detected in thc msoclat~ Method Blank H Holding times for preparation or analysis exceeded E Value above quandtation range J Analytc detected below quantitadon limits S Spike Recovery oulzide accepted recovery limits X Value exceeds M~ximum Contaminant Level Page 39 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No~ 8 [GW] Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/20/2007 10:07:00 AM Lab ID: 0703166-0gA Matrix: L1QU1D Result Limit Qnal Units DF VOLATILE SW-846 METHOD 8260 SW8260B Dllsopmpyl ether U 1.0 pg/L Ethanol U 1.0 pglL Ethyl acetate U 1.0 pg/L Ethylbenzene U 1.0 pg/L Frean-114 U 1.0 pglL Hexachlorobutadiene U 1.0 pglL Isopropyl acetate U 1,0 pg/L Isopropylbenzene U 1.0 pg/L m,p-Xylene U 2.0 pglL Methyl ted-butyl ether U 1,0 pglL Methylene chloride U 1,0 pgtL n-Arnyl acetate U 1.0 pglL Naphthalene U 1.0 pglL n-Butyl acetate U 2,0 pg/L n-Butylbenzane U 1,0 pg/L n-Propyl acetate U 1.0 pg/L n-Propylbenzene U 1.0 pg/L o-Xylene U 1.0 pg/L p-Diethylbenzene U 1.0 pg/L p-Ethyltoluene U 1.0 pg/L sec-Butylbenzene U 1.0 pg/L Styrene U ~ .0 pg/L t-Butyl alcohol U 1.0 pg/L tert-Butylbenzene U 1.0 pg/L Tetrachloroethene U 1.0 pg/L Toluene U 1.0 pg/L trans-1,2-Dichlametheae U 1.0 pg/L Tdchloroethene U 1.0 pg/L Tdchlomflu~mmethace U 1.0 pg/L Vinyl acetate U 1.0 pg/L Vinyl chloride U 1.0 pglL Sum 4-Bromofluor=benzene 103 54-134 %REC Surr: Dibromofluoromelhane 104 52-132 %REC Surf: Toluene-d8 95,5 51-127 %REC Date Analyzed Analyst: LD$ 3/21/2007 2:34:00 PM 3/2112007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 312112007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2507 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 312112007 2:34:00 PM 3/21/2007 2:34:00 PM 312112007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2057 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/21/2007 2:34:00 PM 3/2112007 2:34:00 PM 512112007 2:34:00 PM 3/21/2507 2:34:00 PM Qualifiers: B Analytc detected in thc ossociated Method Blank H Holding times for preparation or analysis exceedcd ND 'Not l~tectcd at thc Rcporting Limlt U Indicates thc compound was analyzed for but not dclcctc Page 40 of 70 American Analytical Laboratories, LLC. note: 2S-Mar-O7 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulting 0703166 Moo~s Lane Greenpo~, N.Y. 0703166-09A Client Sample ID: Tag Number: Collection Dale: Matrix: No. 5 3/20/2007 t ] :00:00 AM LIQUID Analyses Result Limit Qual MERCURY SW7470A Mercury U 0.000200 TARGET ANALYTE LIST METALS SW6010B Aluminuro 279 Antimony 0.0255 0.0250 Arsenic 0.0937 0.0250 Barium 1.63 0.0200 Beryllium U 0.0200 Cadmium U 0.0100 Calcium 75~7 0.0250 Chromium 1.57 0.0200 Cobalt U 0.0200 Copper 0.739 0.0200 Iron 431 0.200 Lead 0,400 0.0180 Magnesium 51.8 0.0200 Manganese 7.36 0.0200 Nickel 0,422 0.0200 Potassium 72.5 0.100 Selenium U 0.0250 Silver U 0.0200 Sodium 36.9 0.0300 Thallium U 0.0150 Vanadium 0,420 0.0200 Zinc 1.51 0.0200 SEMIVOLATILE SW-846 METHOD 8270 SW8270D 1,2,4-Trichlombenzene U 5.3 1,2-Dichlerobenzene U 5.3 1,3-Dichlo robenzene U 5.3 1,4-Dichlorobenzene U 5.3 2,4,5-Trichlomphenol U 5.3 2,4,6-Trichlorophenol U 5.3 2,4-DIchlorophenol U 5.3 2,4-Dimethylphenol U 8.3 2,4-Dinitmphenol U 11 2,4-Dinilrololuene U 5.3 2,6-Dinitrotoluene U 5.3 2-Chloronaphthalene U 5.3 2-Chlomphenol U 5.3 Units DF mg/L 1 SW3010A mglL I mg/L 1 rng/L 1 mg/L 1 m9/L 1 mglL 1 mg/L 1 mglL 1 mg/L 1 mg/L 1 mglL 10 mg/L 1 mg/L 1 mg/L 1 mglL 1 mg/L 1 mg/L 1 mg/L 1 mglL 1 mglL 1 mg/L 1 SW3510 pg/L pg/L pg/L ~Jg/L pg/L pg/L ~g/L pg/L pg/L pglL pg/L pg/L IJg/L Date Analyzed Analyst: WN 3/23/2007 12:04:39 PM Analyst: JP 3/23/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3/2312007 9:44:40 AM 312312007 9:44:40 AM 3/23/2007 9:44:40 AM 3/26/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3123/2007 0:44:40 AM 3/23/2007 10:17:11 AM 312312007 9:44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 9:44:40 AM 312312007 9:44:40 AM 3/28/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 8:44:40 AM 6/23/2007 9;44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 9:44:40 AM 3/23/2007 8:44:40 AM Analyst: RN 3/26/2007 6:44:00 PM 312612007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3~26~2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 312812007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6;44:00 PM Qualifiers: B Analyte detected ia the associated Mctl:od Blank H Holding dmcs for preparation or analysis exceeded ND Not Detected at Ibc Reporting Limit E Value above quantitation range J Analyic detected below quantilation limils S Spike Recovery oulsidc acceplcd m~ovcl3, limils X Value exceeds Maximum Coalaminam Level Page 41 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 5 [GW] Lab Order: 0703166 Project: Moores Lane Greenport, N.Y. Lab ID: 0703166-09A Tag Number: Collection Date: 3/20/2007 1 I:00:00 AM Matrix: LIQU1D Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 2-Methylnaphthalene U 5.3 pg/L 2-Methylphenol U 5.3 ~gA- 2-Nitroaniline U 5.3 pglL 2-Nitrophenol U 5.3 pgA- 3,3'-Dichlcmbenzidine U 5.3 pg/L 3+4-Methyiphenol U 5.3 pglL 3-NRraaniline U 5.3 pg/L 4,~-Dinitro~2-met hylphenol U 5.3 .ugA- 4-Bromophenyl phenyl ether U 5.3 pg/L 4--Chloro-3-methylphenol U 5.3 4~Chloroaniline U 5.3 FglL 4-Chlorophenyl phenyl ether U 5.3 :ag/L 4-Nitmaailine U 5.3 ug/L 4-Nitraphenol U 5,3 pglL Acenaphthene U 5.3 gglL Acenaphthylene U 5.3 pg/L Aniline U 5,3 pg/L Anthracene U 5,3 pt}IL Azobenzeno U 5.3 pg/L Benzidina U 5.3 pg/L Benzo(a}anthmcene U 5.3 Benzo(a)pymne U 5.3 UgA- Benzo(b)fiu~'anlhene U 5.3 I~gA- Benzo(g,h.i)perylene U 5.3 pg/L Benzo(k)fluoranUlene U 5.3 I~g/L Benzoic acid 1.5 5.3 J pgA- Benzyl alcohol U 5.3 gg/L Bis(2-chloroethoxy)methane U 6.3 ~JglL B[s(2.chlomet hyl)ether U 5.3 gglL B[s(2-chloroisopropyl)ether U 5.3 pgA- Bls(2-ethylhexyl)phthalate 3.1 5.3 J iJgA_ Butyl benzyl phlhalate U 5.3 IJg/L Carflazole U 5.3 pglL Chrysene U 5.3 pglL Dibenzo(a,h)a nthracene U 5.3 pg/L Dibenzot~ran U 5.3 pglL Diethyl phthalate U 5.3 pgA- Dimethyl phthalate U 5.3 pg/L Di-n-bulyl phlhalate U 5.3 pgA. DP Date Analyzed Analyst: RN 3/26/2007 6:44:00 PM 3/26/2007 6:44:[}0 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/2612007 6:44:00 PM 3~26~2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/200? 6:44:00 PM 3126/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/20[}7 6;44:00 PM 6/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3126/2007 6:44:00 PM 3/26/[}007 6:44:~0 PM 3/26/2007 6:44;00 PM 3/26/2007 6:44;00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44~00 PM 3/2612007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/25/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3/26/2007 6:44:00 PM 3126/2007 6:44:00 PM 3126/2007 6:44:00 PM 3/26/2067 6:44:[}0 PM 3/26/2007 6:44:00 PM Qualifiers: Analyle detected Jn Ihe associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit E Value above quantitadon range J Analyte detected below quantilation limits Page 42 of 70 American Analytical Laboratories, LLC. ])ate: 28-Mar-07 CLIENT: P.W. ~3rosser Consulting Client Sample ID: No. 5 [GW] Lab Order: 0703 t 66 Project: Moores Lane Greenport, N.Y. Lab ID: 0703166-09A Tag Number: Collection Date: Matrix: 3/20/2007 1 ]:00:00 AM LIQUID Analyses Result SEMIVOLATILE SW-846 METHOD 8270 Dim..octyl phthalate U Fluoranthene U Fluorene U Hexachlorobenzene U Hexachlorobutadiene U HexachJorocyclope ntadiene U Hexachloroethane U Indeno(1,2,3-c,d)pymne U Isophorone U Naphthalane U Nitrobenzene U N-Nitrosodimethylamine U N-Nitrosodi-n-prapylam[ne U N-Nitrosodiphenylamine U Penlachlorophenol U Phenanthrene U Phenol U Pyrene U Pyridine U Sum 2,4,6-Tribromophenol 68.3 Surf: 2-Fluo,'obip henyl 75.5 Sum 2-Fluorophenel 51.0 Sum 4-Terpheny!<i14 80.7 Sum Nitrobenzene~5 65.8 Sum Phenol-d6 31.7 VOLATILE SW-846 METHOD 8260 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U 1 ,I ,2-Trichloro-1,2,24dfluoroethane U 1,1,2-Trichloroethane U 1 ,l-Dlchloroethane U 1,1 -Dichloroethene U 1,1-Dichleropropene U 1,2.3-Trlchlorobenzene U 1,2,3-Trichloropropane U 1,2,4,5-.Tetramethylbenzene U 1,2,4-Trlchlombenzene U 1,2,4-T~imethylbe nzene U Limit Qual Units DF Date Analyzed SW82700 SW3510 Analyst: RN 5.3 pglL 1 3/26/2007 6:44:{30 PM 5.3 pg/L I 3/26/2007 6:44:00 PM 5.3 pglL 1 3/26/2007 6:44:00 PM 5.3 pg/L 1 3126/2007 6:44:00 PM 5.3 pglL 1 3/26/2007 6:44:00 PM 5.3 pg/L 1 3/26/2007 6;44:00 PM 5.3 pg/L 1 3/26/2007 6:44:00 PM 5.3 pg/L I 3/26120{37 6:44:00 PM 5.3 pgJL 1 3/2612007 6:44:00 PM 5.3 pg/L I 3/26/2007 6:44:00 PM 5.3 pg/L 1 3/26/20{37 6:44:00 PM 5.3 ug/L 1 3/26/2007 6:44:{30 PM 5.3 pg/L I 3~26~2007 6:44:00 PM 5.3 I~g/L I 3/26/2007 6:44:00 PM 5.3 IJglL I 3/26/2007 6;44:00 PM 5.3 pglL I 3/26/2007 6:44:00 PM 5.3 pg/L 1 3/23/2007 6:44:00 PM 5.3 pg/L I 3/26/2007 6:44:00 PM 5.3 pg/L 1 3/26/2007 6:44:00 PM 22-124 %REC 1 3/26/2007 6:44:00 PM 18~124 %REC 1 3/26/2007 6:44:00 PM 16-112 %REC 1 3/26/2007 6:44:00 PM 17-121 %REC I 3/26/2007 6:44:00 PM 19-115 %REC I 3/26/2007 6:44:00 PM 12-102 %REC I 3/26/2007 6:44:00 PM SW8260B Analyst: LDS 1.0 pg/L I 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/I. I 3/21/2007 3:22:00 PM 1.0 pg/I. 1 3/21/2007 3:22:00 PM 1.0 pglL 1 3/2112007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3f2112007 3:22:00 PM 1.0 ug/L 1 3/21/2007 3:22:00 PM 1.0 pg/L I 3/21/2007 3:22:00 PM 1.0 pglL 1 3121/2007 3:22:00 PM 1.0 pg/L I 3/2112007 3:22:00 PM 1.0 uglL 1 3/21/2007 3:22:00 PM Q~alifiers: Page 43 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 MooresLane Greenport, N.y. 0703166-09A Client Sample ID: Tag Number: Collection Date: Matrix: t~o. 5 [ow] 3/20/2007 11:00:00 AM LIQUID Analyses Result VOLATILE SW-846 METHOD 8260 1,2-Dibrom~-3-chloropropane U 1,2-Dibromoethane U 1,2-D[chlorobenzene U 1,2-Dichloroethane U 1,2-Dichloropropane U 1,3,5-Trimethylbenzene U 1,3-Dichlombenzene U 1.3-dichloropmpane U 1,4-Dichlorobenzene U 2,2-Dichloropropane U 2-Butanone U 2-Chloroethyl vinyl ether U 2..Chlorotoluene U 2-Hexanone U 2-Propanol U 4-Chlorotoluene U 44sopropyltoluane U 4-Methyl-2~pentanone U Acetone U Acrolein U Acrylonitrile U Benzene U Bromobenzene U Bromochloromelhane U Bmmod[chloromethane U Bromofon-n U Bmmomethane U Carbon disulfide U Carbon tetrachlodde U Chlorobenzene U Chlorodifluoromethane U Chlomethane U Chlorofon~n U Chloromethane U cis-1,2-Dichloroethene U cis-1,3-Dichloropropene U Dibromochloromethane U Dibmmomethane U Dichlorodlfluomme[hane U Limit Qual Units DF Date Analyzed Swa260B Analyst: LDS 1.o pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3121/2007 3:22.:00 PM 1.0 ug/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3;22:00 PM 1.0 pglL t 3/21/2007 3:22:00 PM 1.0 gg/L I 3/21/2007 3:22:00 PM 1.0 IJg/L 1 312112007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 3.0 pglL I 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L I 3/21/2007 3:22:00 PM 2.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L I 3/21/2007 3:22:00 PM 1.0 p§IL I 3/21/2007 3:22:00 PM 2.0 gg/L 1 3/21/2007 3:22:00 PM 2.0 pg/I. I 312112007 3:22:00 PM 1.0 ~g/L I 3/21/2007 3:22:00 PM 1.0 Fg/L I 3/21/2007 3:22:00 PM 1.0 pglL 1 3/21/2007 3:22:00 PM 1.0 pglL 1 3/21/2007 3:22:00 PM 1.0 pg/L I 3/21/2007 3:22:00 PM 1.0 ~g/L 1 3/2112007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22;00 PM 1.0 ug/L 1 3/21/2007 3:22:00 PM 1.0 pg/L I 3/21/2007 3:22:00 PM 1.0 pg/L I 3/2112007 3:22.:(]0 PM 1.0 pg/L 1 3/21/21307 3:22:00 PM 1.0 pglL I 3/21/2007 3:22:D0 PM 1.0 pglL 1 3/21/2007 3:22:00 PM 1.0 pg/L 1 3/21/2007 3:22:00 PM 1.0 pglL 1 3/21/2007 3:22:00 PM 1.0 pglL 1 3/21/2007 3:22:00 PM 1.0 gg/L 1 3/21/2007 3:22:00 PM 1.0 IJg/L 1 3/21/2007 3:22:00 PM Qualifiers: Page 44 of TO American Analytical Laboratories, LLC. Date: 28-Mar-OZ CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Greenport, N.Y. 0703166-09A Client Sample ID: Tag Number: Collection Date: Matrix: No. 5 3/20/2007 11:00:00 AM LIQUID Analyses Result Limit Qual Units VOLATILE 8W-846 METHOD 8260 SW8260B Dilsopmpyl ether U 1.0 I~g& Ethanol U 1.0 uglL Ethyl acetate U 1.0 I~g/L Ethylbenzene U 1 .fi l~g/L Freon-114 U 1.0 pg/L Hexachlombutadiene U 1.0 I~g/L IsopropyJ acetate U 1.0 pg/L Isopropylbenzene U 1.0 pg/L m,p-Xylene U 2.0 pg/L Methyl tert-butyl ether U 1.0 pg/L Methylene chloride U 1.0 pg/L n-Amyl acetale U 1.0 pg/L Naphthalene U 1.0 pg/L n-Butyl acetate U 2.0 ug/L n-Buybenzene U 1.0 IJglL n-Propyl acetate U 1.0 pg/L n~Propylbenzene U 1.0 ug/L o-Xylene U 1.0 :Jg/L p-Diethylbenzene U 1.0 IJglL p-Ethyltoluene U 1.0 gg/L sec-gutylbenzene U 1.0 uglL Styrene U 1.0 pg/L t-Butyl alcohol U 1.0 pg/L te~t-Butylbenzece U 1.0 gg/L Tetrachlomethece U 1.0 pg/L Toluene U 1.0 Ng/L trans-1,2-Dichioroethece U 1.0 I~J/L trans-1,3-Dichloropropene U 1.0 gg/L Tdchloroethene U 1.0 pg/L TrichJorafluommethane U 1.0 pg/L Vinyl acetate U 1.0 pg/L Vinyl chlodde U 1.0 pg,'L Sum 4-Bromofluombenzene 101 54-134 %REC Sum Dibmmofluoromethane 97.7 52-132 %REC Sum Toluene-d8 99.2 5%127 %REC DF Date Analyzed Analyst: LDS 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/2112007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/2112007 3:22:00 PM 312112007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/2112007 3:22:00 PM 3/2112007 3:22:00 PM 3/21/2007 3:22:00 PM 3/2112007 3:22:00 PM 3/21/2fl07 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3121/2007 3:22:00 PM 3121/2fl07 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 312112007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22;~O PM 3/21/2007 3:22;00 PM 312112007 3:22:00 PM 3/21F2007 3:22:00 PM 312112007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3/21/2007 3:22:00 PM 3121/2007 3:22:00 PM Qualifiers: Value above quandtation range Pmalytc detected below quantilation limits Spike Recovery outside accepted recovery limits Value exr~eds Maximum Contaminant Level Page 45 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-OZ CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Montes Lane Greenport, N.Y. 0703166-10A Client Sample ID: Tag Number: Collection Date: Matrix: ~qo. 4 [GW] 3/20/2007 12:10:00 PM LIQUID Analyses Result Limit Qual Units MERCURY SW7470A Mercury U 0.000200 mg/L TARGET ANALYTE LIST METALS SW6010B SW30'IOA Aluminum 508 0.200 mg/L Antimony U 0.0250 mg/L Arsenic 0.0806 0.0250 mg/L Barium 1.50 0,0200 mg/L Beryllium U 0,0200 mglL Cadmium U 0.0100 mg/L Calcium 54,7 0.0250 mg/L Chromium 0.852 0.0200 mg/L Cobalt U 0.0200 mg/L Copper 0.826 0.02130 mglL Iron 350 0.200 mglL Lead 0,344 0.0150 mg/L Magnesium 71.2 0.0200 mg/L Manganese 5,23 0.0200 mg/L Nickel 0.419 0.0200 mg/L Potassium 96.2 O, 10g mglL Selenium U 0.0250 mg/t. Silver U 0.0200 mg/I. Sodium 26.9 0.0300 mg/L Thallium 0.0219 0,0150 mg/L Vanadium 0.668 0.0200 mglL Zinc 1.81 0.0200 rnglL SEMIVOLATILE SW-846 METHOD 8270 8W82700 SW35~10 1,2,4-Trichlorobenzene U 5,1 pg/L 1,2-Dich[ombenzene U 5.1 I~gtL 1,3-Dich[orobenzene U 5.1 pg/L 1,4-Dichlorohenzene U 5,1 pglL 2,4,5-Tdchlomphenol U 5.1 pg/L 2,4,6-Trichlarophenol U 5.1 p0/I. 2,4-Dichlomphenol U 5.1 pg/L 2,4-Dimethylphenol U 5.1 gg1L 2,4-Dlnltrophenol U 10 pg/L 2,4-Dinitrotoluene U 5.1 pg/L 2,G-Dinitratoluene U 5. I pg/L 2-Chlornnaphthalene U 5.1 ~g/L 2-Chlorophenol U 5.1 pg/L DF Date Analyzed Analyst: WN 3/23/2007 12:06:46 PM Analyst: JP 10 3/23/2007 10:35:20 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:49:45 AM t 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3/2312007 9:46:45 AM 1 3/2312007 9:46:46 AM I 3/23/2007 9:46;45 AM 1 3/23/2007 9:46:45 AM 10 3~23~2007 10:35:20 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3123/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM I 3/23/2007 g:46;45 AM 1 3/23/2007 9:46:45 AM I 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM 1 3/23/2007 9:46:45 AM Analyst: RN 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/2~2007 7:20:00 PM 3/26/2097 7:20:00 PM 3/26/2007 7:20:00 PM 3126/2007 7:20;00 PM 3/23/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/2612007 7:20:00 PM 3123/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM Qualifiers: B Analy~¢ detected in thc asso~ialed Mcthml Blank H Holding times for preparation or anal}sis exceeded Not Detected at the Repotting Limg U Indicates the compound was analyzed for but not detecte Page 46 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Greenpo~, N.Y. 0703166-10A Client Sample ID: No. 4 [GW] Tag Number: Collection Date: 3~0/2007 12:10:00 PM Matrix: LIQUID Analyses Result SEMIVOLAIILE SW-846 METHOD 8270 2-Methyinaphthelene U 2-Methylphenol U 2-Nltroaniline U 2-Nitrophenol U 3,3 '-Dichlorobenzidine U 3+4-Methylphenol U 3-Nitmanillne U 4,6-Dinitro-2-methylphenol U 4-Bmmophenyl phenyl ether U 4-Chloro-3-methylphenol U 4-Chloroaniline U 4-Chinrophenyl phenyl ether U 4-Nitroaniline U 4-Nitrophenol U Acenaphthene U Acenaphthylene U Aniline U Anthracene U Azobenzene U Ber~idine U Benzo(a)anthracene U Benzo(a)pyrene U Benzo(b)fluoranthene U Benza(g,h,i)perylene U Benzo(k)fluoranthene U Benzoic acid U Benzyl alcohol U Bis(2-chloroethoxy)met ha ne U Bis(2-chlomethyl)et her U Bis{2-chloroisopmpyl)ether U Bis(2-ethythexyl)phthalate U Butyl benzyl phthalate U Carbazole U Ch~ysene U Dibenzo(a,h)anthracen e U Dibenzofuran U Diethyl phthalate U Dimethyl phthalate U Di-n-butyl phthalate U Limit Qual SW8270D 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 5.1 pg/L 5.1 pglL 5.1 pg/L 5.1 Hg/L 5.1 pgA, 5.1 pg/L 5.1 pg/L 5.1 pglL 5.1 IzglL 5.1 pglL 5.1 pgA, 5.1 pg/L 5.1 llg& 5.1 pg/L 5.1 pg/L 5.1 pg/L 5.1 pg/L 5.1 pg/L 5.1 pgtL 5.1 pg/L 5.1 pglL Units DF Date Analyzed SW3510 pg/L pgfL pg/L ~Jg/L Pg& pg/L HglL pg/L pglL pg/L pgA. pg/L pg/L ~gA, pg/L pglL Analyst: RN 3/25/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3126/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3~26~2007 7:20:00 PM 6/26/2007 7:20:00 PM 3/26/2007 7:20:0D PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2D07 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:26:00 PM 3126/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3~26~2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3t26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/2612007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM Q.alifiers: Anal}ne detected in thc associated Method Blank H Holding dines for preparation or analysis exceeded ND Not Detected at thc Reporting Limit U Indicates tho compound was analy~d for but n~ detecto E Value above quantitefion range J Analyte detected below quantitation limits S Spike Recover, outside nccop[gd recovery limits X Value exceeds Maximum Contaminant Level Page 47 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Greaser Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Mooras Lane Greenpurt, N.Y. Collection Date: Lab ID: 0703166-10A Matrix: No. 4 [aw] 3/20/2007 12:10:00 PM LIQUID Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 8W82700 5W3510 Di-n-octyl phthalate U 5.1 pgtL Fluoranthene U 5.1 pg/L Fluorene U 5.1 pg/L Hexachtombenzene U 5.1 pg/L Hexachlorobutadiene U 5.1 ug/L Hexachlomcyclopentadiene U 6.1 pg/L Hexachloroethane U 5.1 pg/L Indeno(1,2,3-c,d}pyrene U 5.1 pg/L Isophorone U 5.1 pg/L Naphthalene U 5.1 IJg/L Nitrobenzene U 5.1 IJg/L N-Nitmsodimethylamine U 5.1 pg/L N-Nitmsodl-r>propyla mina U 5.1 pglL N-Nitrosodiphenyiamine U 5.1 pg/L Penlachlorophenol U 5.1 pglL Phenanthrene U 5.1 pglL Phenol U 5.1 pg/L Pymne U 5.1 pg/L Pyridine U 5.1 pg/L Surr: 2,4,fi.Tribromophenol 63.7 22-124 %REC Sure 2-Fluorobiphenyl 77.4 18-124 %REC Sum 2-Fluorophenol 53,1 16-112 %REC Sum 4-Terpheayl-d14 73.4 17-121 %REC Sum Nitrobenzene-d5 68.6 19-115 %REC Sum Phenol-d6 32,5 12-102 %REC VOLATILE $W-846 METHOD 8260 SW82600 1,1,1,2-Tetrachlomethane U 1.0 pg/L 1,1,2,2-Tet rachlametha ne U 1.0 pg/L 1,1,2-T~ch~ero-1.2,2-trifluoroethane U 1.0 pg/L 1,1,2-Trichloroethane U 1.0 pg/L 1,1-Dichlotoethane U 1.0 pg/L 1,1 -Dichloroethene U 1.0 pg/L 1,1 -Dichloropropene U 1.0 pg/L 1,2,3-Tfichlombenzene U 1.0 1,2,3-Trlchloropropane U 1.0 pg/L 1,2,4,5-Tetmmethylbenzene U 1.0 pg/L 1,2,4-.Trichlorobenzene U 1.0 pglL 1,2,4-Trimethylbenzene U 1.0 pfl/L DF Date Analyzed Analyst: RN 3~26~2007 7:20:00 PM 3/23/2007 7:20;00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:(10 PM 3/26/2007 7:20:00 PM 3/2612(107 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2907 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20;09 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 3~26~2007 7:20:00 PM 3/26/2007 7:20:00 PM 3/26/2007 7;20:00 PM 3/26/2007 7:20;00 PM 3/26/2007 7:20:00 PM 3/26/2007 7:20:00 PM 312612007 7:20:00 PM Analyst: LDS 3/21/20o7 4:o9:oo PM 3/21/2oo7 4:09:00 PM 3/21/2007 4:09:00 PM 3/2112007 4:09:00 PM 3/2112007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:0fi;00 PM 3/21/2007 4:09;00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM Qualifiers: Analy~e detected in the associated M,thru/Blank H Holding limes for preparation or anal)als exceeded ND Not Dctccled at Ihe Reporting Limit U Indicates the compound was analyzed for but not detecto E Value above quantitation range J Analy'~e detcctcd below quantitation limits S Spikc Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 48 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consult~g 0703166 Moores Lane Greenpo~,N.Y. 0703166-10A Client Sample ID: Tag Number: Collection Date: Matrix: No. 4 [GW] 3/20/2007 12:10:00 PM LIQUID Analyses Result VOLATILE SW-846 METHOD 8260 1,2-Dibromo-3-chloropropane U 1,2-Dibromoethane U 1,2-Dichlorobenzene U 1,2-D[chloroethane U 1,2-Dichlompropane U 1,3,5-Tdmethylbenzene U 1,3-Diclfiorobenzene U 1,3-dichloropmpane U 1,4-Dichlorobenzene U 2,2~Dichlompropane U 2-Butanone U 2-Chlomethyl viny] ether U 2-Chlorotoluene U 2-Hexanone U 2-Propar~l U 4-Chlorotoluene U 4-1sopropyltoluene U 4-Methyl-2-penianone U Acetone U Acrolein U Ac¥ouitrile U Benzene U Bromobenzene U Bromochlummethane U Bromodichloromethafle U Bromoform U Bromornethane U Carbon disulfide U Carbon tetmcfllorfde U Chlorobenzene U Chlorodifluommethane U Chloroethane U Chloroform U Chloromethene U cis-1,2-Dichloroethene U cis-1,3-Dichloropropene U Dibmmechloromethane U Dibromomethane U Dichlorodiflueromethane U Limit Qual Units SW82600 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 poll 1.0 pg/L 1.0 polL 1.0 p0/L 3.0 pg/L 1.0 pg/L 1.0 P0/L 2.0 polL 1,0 pg/L 1.0 polL 2.0 pg/L 2.0 polL 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 polL 1.0 pgA. 1.0 pg/L 1.0 polL 1.0 pg/L 1 .o pg/L 1.0 polL 1 ,o polL 1 ,O polL 1,0 polL 1.0 pg/L 1.0 pg/L 1.0 pg/L DF Date Analyzed Anatyst: LDS 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:90 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 312112007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/2112007 4:09:00 PM 1 312112007 4:09:00 PM I 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM 1 3/21/2907 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09;00 PM I 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/2112007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/2112007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/21/2007 4:09:00 PM 1 3/2112007 4:09:00 PM 1 3/21/2007 4:09:00 PM I 3/21/2007 4:09:00 PM 1 3/2112007 4:09:00 PM Qualifiers: E Value above quantitadon range J Analyte det¢clcd b~low quantitatlon limit~ Page 49 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenport, N.Y. 0703166-10A Client Sample 1D: No. 4 [GW] Tag Number: Collection Date: 3/20/2007 12:10:00 PM Matrix: LIQUID Analyses Result Limit Qual Units VOLATILE SW-846 METHOD 8260 SW8260B Diisopropyl ether U 1.0 pg/L Ethanol U 1.0 pg/L Ethyl acetate U 1.0 pg/L Ethylbenzene U 1,0 pglL Fmon-114 U 1,9 pglL Hexachlorobutediene U 1.0 pg/L Isopropyl acetate U t .0 pg/L Isopropylbenzene U 1.0 pg/L m,p-Xylene U 2.9 pg/L Methyl tort-butyl ether U t.0 pg/L Methylene chloride U 1.0 pglL n-Amyl acetata U 1.0 Hg/L Naphthalene U 1.0 pg/L n-Butyl acetate U 2.0 pg/L n-Butylbenzene U 1.0 pglL n-Propyl acetate U 1.0 pg/L n-Propylbenzene U 1.0 pglL o-Xylene U 1.0 pg/L p-Diethylbenzene U 1.0 pg/L p-Ethyltoluene U 1.0 pglL sec-I~utylbenzene U 1 .O pg/L Styrene U 1.0 pglL t-Butyl alcohol U 1.0 Fg/L iert-Butylbenzene U 1.0 pg/L Tetrachlamethene U 1.0 pg/L Toluene U 1.0 pg/L trans-1.2-Dichlomethene U 1.0 pg/L trana-1,3-Dichlompmpene U 1.0 pg/L Trichloroethene U 1.0 pg/L Trichlorofluoromet bane U 1.0 pgtL Vinyl acetate U 1.0 pg/L Vinyl chloride U 1.0 pg/L Sum. 4-Brnmofluorobenzene 103 54-134 %REC Sum. D[bromofluoromethane 105 52-132 %REC Sum Toluene-d8 95.5 51-127 %REC DF Date Analyzed Analyst: LDS 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3121/2007 4:09:00 PM 3/21/2007 4:09:0{3 PM 3121/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3121/2007 4:09;00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2907 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 312112007 4:09:00 PM 3/2112007 4:09:00 PM 3/21/2007 4:09:00 PM 3/2112007 4:09:00 PM 3/21/2007 4;09:00 PM 3/21/2007 4:09:00 PM 312112007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/2112007 4:09:00 PM 3/21/2007 4:09:00 PM 312112007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:09:00 PM 3/21/2007 4:00:00 PM 3/21/2007 4:09:00 PM 312112007 4:09:00 PM 3/21/2007 4:09:00 PM 3/2112007 4:09:00 PM 3~1/2007 4:09:00 PM 3/21/2007 4:09:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times fo~ preparation or analysis exceeded ND Not Detected at tite Reporting Limit Page 50 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: Lab ID: 0703166-1 IA Matrix: No. 3 [GW] 3/20/2007 12:55:00 PM LIQUID Analyses Result Limit Qual Units DF MERCURY SW7470A Mercury U 0.0002130 mglL 1 TARGET ANALYTE LIST METALS SW60'IOB SW3010A Aluminum 255 0.0200 mglL 1 Antimony U 0,0260 mglL 1 Arsenic 0.0718 0.0250 mg/L 1 Barium 1.20 0.0200 mg/L 1 Beryllium U 0.0200 mgtL 1 Cadmium U 0.0100 mglL 1 Calcium 36.4 0.0250 mg/L 1 Chromium 0.398 0.0200 mg/L 1 Cobalt U Copper 0.350 D.0200 mglL 1 Iron 180 0.0200 mg/L 1 Lead 0.280 0.0150 mglL 1 Magnesium 49.0 0.0200 mg/L 1 Manganese 6.50 0.0200 rnglL 1 Nickel 0,297 0,0200 rog fL 1 Potassium 75.3 0,100 mg/L 1 Selenium U 0.0250 mglL 1 Silver U 0.0200 mg/L 1 Sodium 21.3 0.0300 mg/L 1 Thallium U 0.0150 mglL 1 Vanadium 0.450 0.0200 mg/L 1 Zinc 0.974 0.0200 mg/L 1 SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 1,2,4-Trfchlorobenzene U 5.1 pg/L 1 1,2-Dichlorobenzene U 5.1 I~glL 1 1,4-Dichlorobenzene U 5.1 [tgiL 1 2,4, 5-Trichlorop henol U 5.1 Ilg/L 1 :~,4,6-Triohlorop henol U 5.1 IJglL 1 2,4-Dichlamphenol U 5.1 ~g/L 2,4-Dimethy}phenol U 5.1 pg/L 1 2,4-DInitrophenol U 10 gg/L 1 2,4-Dinitroteluene U 5.1 gg& 1 2,6-Diniirotoluene IJ 5.1 i~g.q_ 1 2-Chlomnaphthalene U 5.1 Iag/L 1 2-Chlorophenol U 5.1 IJg/L I Date Analyzed Analyst: WN 3/23/2007 12:08:53 PM Analyst: JP 3/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3t26/2007 9:49;03 AM 6/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49;03 AM 3/2312007 9:49:03 AM 3/2:~/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49:0:3 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49;03 AM 3/23/2007 9:49:03 AM 3/23/2007 g:49:03 AM 3/23/200? 9:49:03 AM 3123/2007 9:49:03 AM 3/23/2007 9:49:03 AM 6/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM 3/23/2007 9:49:03 AM Analyst: RN 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:55:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/2612007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for p~eparation or analysis exceeded ND Not Detected at the Reporting Limit U indicates thc compound was analyzed for but not detcete E Value above quantitation range J Analyt, detected below quantilation limits S Spike Rccewry outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 51 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Metres Lane Greenpoa, N.Y. 0703166-11A Client Sample ID: No. 3 [GW] Tag Number: Collection Date: 3/20/2007 12:55:00 PM Matrix: LIQUID Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82706 SW3510 2-Methylnaphthalene U 5~1 lag/L 2-Methylphenoi U 5.1 lag/L 2-Nitroaniline U 5.1 gglL 2-Nitrophenol U 5.1 laglL 3,3'-Dichlorobenzidine U 5.1 pg/L 3+4-Methylphenol U 5.1 lag/L 3-NitroanilJne U 5.1 pg/L 4,6-Dinitm-2-methylph enol U 5.1 pgfl_ 4-Bmmophenyr phenyl ether U 5.1 pglL 4-Chlora-3-methylphenol U 5.1 gg/L 4-Chloroanillne U 5.1 pg/L 4-ChJorophenyl phony[ ether U 5,t lag/L 4~Nitroaalllne U 5.1 pg/L 4-Nitrophenol U 5.1 lag/L Acenaphthene U 5.1 IJg/L Acenaphthylene U 5.1 pg/L Aniline U 5.1 pgtL Anthracene U 5.1 IJg/L Azobenzeoe U 5.1 pglL Benzidine U 5.1 pglL Benzo(a}anthracene U 5.1 !Jg/L Benzo(a)pymne U 5.1 pgP._ Benzo(b)flueranthene U 5.1 pg/L Benzo(g,h,i)perylene U 5.1 pg/L Benzo(k)fluoranthene U 5.1 pg/L Benzoic acid U 5.1 lag/L Benzyl alcohol U 5.1 laglL Bis(2-chloroethoxy)meth one U 5.1 pglL Bls (2-chloroet hyl)ether U 5.1 F§IL Bis(2-chtoroisopmpyl)ether U 5.1 lag/L Bis(2-ethylhexyl)pht halate U 5.1 pg/L Butyl benzyl phthaiate U 5.1 pglL Carbazole U 6.1 pg/L Chrysene U 5.1 gg/L Dibenzo(a,h)anthracene U 5.1 pg/L Dibenzofumn U 5.1 pg/L Diethyl phthaiate U 5.1 pg/L Dimethyl phthalate U 5.1 lag/L Di-n~utyl phthalale U 5. t lag,q- DF Date Analyzed Analyst: RN 312612007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2067 7:58:00 PM 3/26/2007 7;58:00 PM 3/26/2007 7:58:00 PM 6/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2067 7:58:06 PM 3/26/2007 7:58:08 PM 312612007 7:58:00 PM 3/2612007 7:58;00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:56:06 PM 312612007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2607 7:58:00 PM 3126/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:80 PM 3~26~2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2067 7:58:00 PM 3/26/2007 7:58:00 PM 312512007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 6/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM B Analytc detected in thc nssociatcd Mcthod Blank Holding times for preparation or analysis cxc. c~dcd ND Not Dctcctcd at ~c Rcpmtlog Limit U Indicates the compound was analyzed for but not dct¢cte Page 52 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consult~g 0703166 Moores Lane Greenpo~, N.Y. 0703166-I1A Client Sample ID: Tag Number: Collection Dale: Matrix: No. 3 [GW] 3/20/2007 12:55:00 PM LIQUID Analyses Result Limit Qual SEMIVOLATILE SW-846 METHOD 8270 SW82700 D[-n-octyl phthalate U 5.1 Fluoranthene U 5.1 Fluomne U 5.1 Hexachlorobenzene U 5.1 Hexachlorobutadiene U 5,1 Hexachlorocyclopentadiene U 5.1 Hexachloroethane U 5.1 Indeno(1,2,3-c,d)pyrene U 5.1 Isophomne U 5.1 Naphthalene U 5.1 Nitmbenzene U 5.1 N-Nitrosodimethylamine U 5.1 N-Nit rosodLn-propylamine U 5.1 N-Nitrosodiphen¥1amine U 5.1 Penlachlompheno[ U 5.1 Phenanthrene U 6.1 Phenol U 5.1 Pyrene U 5.1 Pyridine U 5.1 Sure 2,4,6-Tdbromophenol 70.7 22-124 Surf: 2-Fluombiphenyl 79.0 18-124 Sun; 2-Fluomphenol 56.4 16-112 Sure 4-Teq:)henyl-d14 75.1 17-121 Sum Nitrobenzene-d5 68.5 19-115 Sum Phenol-d6 34.7 12-102 VOLATtLE SW-846 METHOD 8260 SW82606 1.1,1,2-Tetrachloroethane U 1.0 1,1,1-Trichloroethane U 1.0 1,1,2,2-Tetrachloroethane U 1.0 1,1.2-Tdchloto-l,2,24dfluoroeth ane U 1.0 1,1,2-Trichloroethane U 1.0 1,1-D[chloroethane U 1.0 1,1 -Dichloroethene U 1.0 1,1 -Dichloroproperm U 1.0 1,2,3-Tdchlorobenzene U 1.0 1,2,3-Tdchloropropane U 1.0 1,2,4,5-Tet ramet hylbenzene U 1.0 1,2,4-Trichlorobenzene U 1.0 1,2,4-Trlmethylbenzene U 1.0 Qualifiers: B Analyte detected in the essoeiated Method Blank Uni~ DF Date Analyzed SW3510 pg/L 1 pg/L 1 pglL 1 pg/L 1 yglL 1 pg/L 1 pg/L 1 pglL 1 pglL 1 pglL 1 pg/L 1 p§/L 1 pglL 1 pg/L 1 pg/L I pg/L 1 IJg/L 1 pg/L 1 %REC 1 %REC 1 %REC 1 %REC 1 %REC 1 %REC 1 pg/L 1 pg/L 1 pg/L 1 p§tL 1 pglL 1 pglL 1 pgtL 1 1 pg/L 1 pg/L 1 pg/L 1 pglL 1 pg/L I Analyst: RN 3/26/2007 7:58:00 PM 3126/2007 7:58:00 PM 3/26/2007 7:58;00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:50:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:55:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:56:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/26/2007 7:58:00 PM 3/2612007 7:58:00 PM 3/26/2007 7:58:00 PM 3/20/2007 7:58:00 PM Analyst: LDS 3/21/2007 4:57;00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/2112007 4:57:00 PM 3/21/2007 4:57;00 PM 3/21/2007 4:57:00 PM 3/2112007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:87:00 PM E Value above quantitation range Analyta detected below quantitafion {imi~z Spike Recovery outside accepted recovery limits Va{ue exceeds Maximum Contaminant Level Page 53 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Cmtsulting 0703166 Mooros La~e Greenpoa, N.Y. 0703166-11A Client Sample ID: No. 3 [GW] Tag Number: CollectionDnle: 3/20/2007 12:55:00 PM Matrix: LIQUID Analyses Result VOLATILE SW-846 METHOD 8260 1,2-Dibrome-3-chlo rep mpan e U 1,2-Dibmmaethane U 1,2-Dichlnrnbenzene U 1,2-Dichloroethane U 1,2-Dichlompropane U 1,3,5-Trimethylbenzene U 1,3-Die. biota benzene U 1,3-diehlompropane U 1,4-Dichiorobenzene U 2,2-Dichloropmpane U 2-Butanone U 2-Chloroethyl vinyl ether U 2-Chlorotoluene U 2-Hexanone U 2-Propanol U 4-Chlomtoluene U 4-1sopr~oylloluene U 4-Methyl-2-pentanone U Acetone U Acrolein U Ac~lonitrile U Benzene U Bromobenzene U Bmmochlommethane U BromodichJoromethane U Brornoform U Bromomethene U Carbon disulfide U Carbon tetrachroflde U Chlorobenzene U ChlorodiSuommethane U Chlometbane U Chloroform U Chloromethane U cls~1,2-Dichloroethene U cis-1,3-Dichloropropene U Dibromochloromethane U Dibromomethane U Dichlomdifluommethane U Limit Qual Units SW82608 1 .O pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg& 1.0 HgfiL 1.0 pglL 1.0 pgtL 1.0 pglL 3.0 pg/L 1.0 pg/L 1.0 pg/L 2,0 pg/L 1.0 pg/L 1.0 ~Jg/L 2.0 pg/L 2.0 pg/L 1.0 pglL 1.0 pglL 1.0 pg/L 1.0 pglL 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pglL 1,0 pglL 1.0 pg/L 1.0 uQIL 1.0 pg/L 1.0 pg& DF Date Analyzed Analyst: LDS 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/2112007 4;57:05 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 312112007 4:57:00 PM 3/21/2007 4:57;00 PM 3/21/2007 4:57:00 PM 3121/2007 4:57:00 PM 3/21/2007 4:57:{)0 PM 3/21/2007 4:57:00 PM 3121/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3121/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2507 4:57:00 PM 3/21/2507 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3121/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57;00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detcct¢~ at the Reporting Limit E Value above quantitatian range J Analyte det¢cled bdow quantitadon limiL~ S Spike Recovery outside accepted recoveny limits X Value exceeds Maximum Contaminant Loyal Page 54 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenport, N.Y. 0703166-1 lA Client Sample ID: Tag Number: Collection Date: Matrix: No. 3 [Gw] 3/20/2007 12:55:00 PM Analyges Result VOLATILE SW-846 METHOD 8260 Diisopropyl ether U Ethanol U Ethyl acetate U Ethylbenzene U Freon-I 14 U Hexachlombutadiene U tsopropyl acetate U Jsopmpylbenzene U m.p-Xylene U Methyl te~t-bu[yl ether U Methylene chloride U n-Amyl acetate U Naphthalene U n.Butyl acetate U n-Butylbenzece U n-Propyl acetate U n-Propylbenzene U o-Xylene U p-Diethylbeozene U p-EthylteJuene U sec-Butylbenzene U Styrene U t-Butyl alcohol U tert-Butylbenzene U Tetrachloroethene U Toluene 2.4 irons-1,2-DichJorcethene U trans-1,3-Dichloropropene U Tdchloroethene U T~chlomfluommethane U Vinyl acetate U Vinyl chloride U Sum 4-Bfomofluorobenzene 98.9 Sum Dibromofluommethane 105 Surf: Toluene-d8 96.7 LL. nit Qual Units SW8260B 1.0 pglL 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 gg/L 1.0 pg/L 1,0 pglL 1,0 pglL 2.0 p§/L 1.0 JJB/L 1,0 pg/L 1.0 pg/L 1.0 pg/L 2.0 pg/L 1.0 pg/L 1.0 pglL 1.0 Fg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pgfL 1.0 1.0 pglL 1,0 pglL 1.0 pg/L 1.0 pg/L 1.0 pglL 1.0 pglL 1 .D pg/L 1.0 pg/L 54-134 %REC 52-132 %REC 51-127 %REC DF Dote Analyzed Analyst: LDS 3/21/2007 4:57;00 PM 3/2112007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:(30 PM 3/21/2007 4:57;00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3~1/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:D0 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4;57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM 3/21/2007 4:57:00 PM Qualifiers: B Analyte detected in tho associated Method Blank H Holding lime~ for preparation or analysis exceeded ND Not Dcleclcd al thc Rcportlng Limit U Indicates thc compound wus analyzed for but not dctgcle Value above quantitation range A~alytc detected below quimtitation limits Spike Recovery outside accepted recovcr~ limits Value exceeds Maximum Contaminant Level Page 55 of 70 American Analytical Laboratories, LLC. Date: 28-Mat:07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Greenpoff, N.Y. 0703166-I2A Client Sample m: Tag Number: Collection Date: Matrix: No. 2 [aW] 3/20/2007 1:20:00 PM LIQUID Analyses Result Limit Qual Units MERCURY SW7470A Memury U 0.000200 TARGET ANALYTE LIST METALS SW6010B Aluminum 170 0.0200 Antimony U 0.0250 Arsenic 0.0372 0.0250 Beduin 0.739 0.0200 Beryllium U 0.0200 Cadmium U 0.01 O0 Calcium 12.5 0.0250 Chromium 1.08 0.0200 Cobalt U 0.0200 Copper 0.276 0.0200 iron 137 0.0200 Lead 0.136 0.0150 Magnesium 27.6 0.0200 Manganese 4.08 0.0200 Nickel 0.602 0.0200 Potassium 22.9 0,100 Selenium U 0.0250 Silver U 0.0200 Sodium 10.0 0.0300 Thallium U 0.0150 Vanadium 0.374 0.0200 Zinc 0,665 0.0200 SEMIVOLATILE SW-846 METHOD 8270 SW82700 1,2,4-Trichlombenzene U 5.2 1,2-Dichlombenzene U 5.2 1,3-Dichlorobenzene U 5.2 1,4-Dichlorobenzene U 5.2 2,4,5-Trichlorophenol U 5.2 2,4,6-Tfichlorophenol U 5.2 2,4q3ichloropheoal U 5.2 2,4-Dimethylphenol U 5.2 2,4~Dlnilrophenol U 10 2.4-Dinitrotoluene U 5.2 2,6-Dinitrotoluene U 5.2 2-Chlomnaphthalene U 5.2 2-Chlomphenol U 5.2 DF Date Analyzed Analyst: WN mglL 1 3/23/2007 12:11:01 PM SW3010A Analyst: JP mg/L 1 3/23/2007 0:51:20 AM mg/L I 312312007 9:51:20 AM mg/L 1 3t23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L I 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L 1 3123/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L t 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L 1 3~23~2007 9:51:20 AM mglL I 3/23/2007 9:51:20 AM mglL I 3/23/2007 9:51:20 AM mglL I 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L 1 3/23/2007 9:51:20 AM mg/L I 3/23/2007 9:51:20 AM mglL 1 3~23~2007 9:51:20 AM mglL I 3/23/2007 9:51:20 AM mg/L I 3/23/2007 9:51:20 AM SW3SI0 Analyst: RN pgtL I 3/27/2007 9:12:00 AM pg/L 1 3/27/2007 9:12:00 AM pg/L 1 3/27/2007 9:12;00 AM pg/L I 3/27/2007 9:12:00 AM pg/L 1 3/27/2007 9:12:~0 AM pg/L 1 3/27/2007 9:12:00 AM pg/L I 3/27/2007 9:12:00 AM pg/L 1 3/27/2007 9:12:00 .AM iJg/L I 3/27/2007 9:12:00 AM pgA. 1 3/27/2007 9:12:09 AM pg/L 1 3/27/2007 9:12:00 AM pglL 1 3/2712007 9:12:00 AM p§/L I 3/27/2007 9:12:00 AM Qualifiers: B Analyte detected in Utc associaled Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicales the compound was analyzed for but not detecte E Value above quantitation range J Analyte detected below quanfilation limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 56 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greanpon, N.Y. 0703166-12A Client Sample ID: No. 2 [GW] Tag Number: Collection Date: 3/20/2007 1:20:00 PM Matrix: LIQUID Analyses Result SEMIVOLATILE SW-846 METHOD 8270 2-Methylnephthalene U 2-Methy[phenol U 2-Nitroa niline U 2-Nitrophenol U 3,3'-Dichlorobenzidine U 3+4-Methylphenol U 3~Nitroaniline U 4,6-Dinilm-2-methy~phenol U 4-Bromophenyi phenyl ether U 4-Chloro-3-met hyiphenol U 4-Chloroaniline U 4-Chlomphenyl phenyl ether U 4-Nitroaniline U 4-Nitrophenol U Acenaphthene U Acenaphthylene U Aniline U Anthracene U Azobenzen~ U Benzidine U Benzo(a)anthracane U Benzo(a)pyrene U Benan(b)§uoranthene U Benzo(g,h,i)pe~lene U Benzo(k)fluoranthene U Benzoic acid U Benzyl alcohol U Bis(2-chleroethoxy)meihane U Bis(2-chleroethyl)ether U BIs(2-ch~omisopmpyl)ethe~' U BIs(2-et hylhexyl)phthalate U Butyl benzyl phthalate U Carbazole U Ch~/sene U Dibenan(a,h)anthracene U Diflenzofumo U Diethyl phthalate U Dimethyl phthalate U DJ-n-butyl phthalate U Limit Qual Units 8W82700 8W3510 5.2 HelL 5.2 pgA. 5.2 pglL 5.2 t~g/L 5.2 pg/L 5.2 pglL 5.2 pglL 5.2 pg/L 5.2 pg/L 5.2 pgA. 5.2 pg/L 5.2 pg/L 5.2 pglL 5.2 pglL 5.2 NelL 5.2 ~Jg/L 5.2 pg/L 5.2 IJg/L 5.2 pg/L 5.2 pBIL 5.2 pgA. 5.2 pg/L 5,2 pglL 5.2 NelL 5.2 ~glL 5.2 pg/L 5.2 pg/L 5.2 pg/L 5.2 Pfl/L 5.2 pg/L 5.2 pg/L 5.2 pgA. 5,2 pgA. 5,2 ~g/L 5.2 pglL 5,2 pglL 5.2 pg/L 5,2 pg/L 5,2 pglL DF Date Analyzed Analyst: RN 312712007 9:12:00 AM 3~27~2007 9:12:00 AM 312712007 9:t2:00 AM 3/2712007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3127/2007 9:12:00 AM 3/2712007 9:12:00 AM 3/27/2007 9:12:00 AM 3/2712007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/2712007 9:12:00 AM 3/2712007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/2712007 9:12:00 AM 3/27/2007 B:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3427/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3127/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM Qualifiers: B Aaalyte delected in the associated Method Blank H Holding times for preparation or anal}sis exceeded Value above quanfitatinn range Analytg detected below quantitalion limits Spike Rccove~ outside accepted recovery limits V~lue exceeds Maximum Contaminant Level Page 57 of 70 American Analytical Laboratories, LLC. Date: 2&Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: Lab ID: 0703166-I2A Matrix: No. 2 [GW] 3/20/2007 1:20:00 PM LIQU1D Analyses Result Limit Qual Units DF SEMIVOLATILE SW-846 METHOD 8270 SW82706 SW3S10 Dt-n-octyl phlhalate U 5,2 pg/L 1 Fluoranthene U 5.2 pg/L 1 Fluorene U 5.2 I~g/L 1 Hexachlorobenzene U 5.2 pg/L 1 Hexachlombutadiene U 5.2 pg/L Hexachlemcyc[opentadiene U 5.2 pglL 1 Hexachloroethane U 5.2 pg/L 1 thdeno(1,2,3-c,d)pyrene U 5.2 pglL 1 Isophorone U 5.2 pg/L 1 Naphthalene U 5.2 1~91L 1 Nitrobanzene U 5.2 IJglL 1 N-Nitrosadimethylamine U 5.2 pg/L 1 N-Nitrosodi-n-propylamine U 5.2 pg~_ N-Nitmsodiphenylamine U 5.2 ~g/L 1 Pentachlorophenol U 5.2 pglL I Phenanthrene U 5,2 pglL 1 Phenol U 5.2 pglL 1 Pyrene U 5.2 pg/L t Pyridine U 5.2 [Jg/L 1 Sum 2,4,6-Tfibmmophenol 59.5 22-124 %REC 1 Sum 2-Fluorobipheayl 73.4 18-124 %REC 1 Surf: 2-Fluorophenol 49.5 16-112 %REC 1 Sun':. 4--Terphenyl-d 14 85.7 17-121 %REC 1 Sun: Nitmbenzene<15 65.3 19-115 %REC 1 Sun: Phenol-d6 31.1 12-102 %REC 1 VOLATILE SW-846 METHOD 8260 SW82600 1,1,1,2-Tetrachloroethane U 1.0 pg& 1 1,1,2-Tfichloro-1,2,2-trifluoroethane U 1.0 I~g/L 1 1,1,2-Tdchloroethane U 1.0 pg/L 1 1,1-Dichloroethane U 1.0 pg& 1 1,1-Dichloroethene U 1.0 pg/I. 1 l,l-Dlchloropropane U 1.0 pglL 1 1,2,3-Trf chlerobanzene U 1.9 pglL 1 1,2,3-Tdchloropropana U 1.0 pg/L 1 1,2,4,5-Tetramethylbenzene U 1.6 IJg/L 1 1,2,4-Trlchlorobenzene U 1.6 pg/L 1 1,2,4-Trlmethylbenzene U 1.0 pglL 1 Date Analyzed Analyst: RN 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2607 9:12:00 AM 312712007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9;12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2097 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2607 9:12:00 AM 3/27/2607 g: 12:00 AM 3~27~2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:00 AM 3/27/2007 9:12:90 AM Analyst: LDS 3/21/2007 5:44:00 PM 3/21/2007 5:44;00 PM 3/21121107 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM Qualifiers: B Annlyle detected in the a~sociated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit Page 58 of 70 American Analytical Laboratories, LLC. Onto: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moo~s Lane Greenpon, N.Y. 0703166-12A Client Sample ID: No. 2 [GW] Tag Number: Collection Date: 3/20/2007 h20:00PM Malrix: LIQUID Analyses Result VOLATILE 8W-846 METHOD 8260 1,2-Dib romo-3-chloropropane U 1,2-Dibromoethane U 1,2-Dichlorobenzene U 1,2-DIchtoroethane U 1,2-Dich~oropropane U 1,3,5-Tfimethylbenzene U 1,3-DIchlorobenzene U 1,3-d[chloropropane U 1,4-Dichlorobenzene U 2,2-Dichloroprepane U 2-Butanone U 2-Chloroethyl vinyl ether U 2-Chlomtoluane U 2-Hexanone U 2-Propaanl U 4-Chlomtoluene U 4-1sopmpy~toluane U 4~ethyl-2-pentanone U Acetone U Acmlein U Ac~/Ion~ile U Benzene U Bromobanzene U Bromochloromethane U Bmmodichloromethane U Bromoform U Bromomethane U Carbon disulfide U Carbon tetrachloride U Cl~lerobenzene U Chlorodi~uoromethane U Chloroethane U Chloroform U Chloromethane U cis-1,2-Dichloroethene U cis-1,3-Dichloropropene U Dibromoohloromethane U Dibmmomethane U Dichlorodifluo romethan e U Limit Qual Units SW8260B 1.0 pg/L 1,0 pg/L 1.0 pglL 1.0 pg/L 1.0 pg/L 1.0 pg/L 1 .o pg/L 1.0 pg/L 1.0 pg/L 3.0 pg/L 1.0 pglL 1.0 pglL 2.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 NglL 2.0 pg/L 2.0 pg/l_ 1.0 pg/L 1.0 pg/L 1.0 pg.rt. 1.0 pglL 1.0 pglL 1.0 yglL 1 _0 pg/L 1.0 pg/L 1.0 p§IL 1.0 pglL 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 Ng/L DF Date Analyzed Analyst: LDS 3/2112007 5:44:00 PM 3/21/2007 5:44;00 PM 3/2112007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 3121/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44;00 PM 3/21/2007 5:44;00 PM 3/21120fi7 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 312112007 5:44:00 PM 312112007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 3/2112007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 3/21/2.007 5:44:00 PM 3/21/2o07 5:44:ofi PM 312112007 5:44;00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3~1/2007 5:44:00 PM 312112007 5:44:00 PM 3/21/2007 5:44:00 PM B Analyle detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Rcponing Limil E Value above quanfitetion range J Analylc detected below quantilalion limits S Spike Recovery outside accepted recovery limits X Value exceeds M&ximum Conteminunt Level Page 59 of TO American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. GrosserConsulling 0703166 Moores Lane Greenpon, N.Y. 0703166-12A Client Sample ID: Tag Number: Collection Date: Matrix: No. 2 [aW] 3/20/2007 1:20:00 PM LIQUID Analyses Result Limit Qual Units VOLATILE SW-846 METHOD 8260 SW8260B D~sepmpyJ ether U 1.0 pglL Ethanol U 1.0 I~g/L Ethyl aeelata U 1,0 ug/L Ethylbenzene U 1.0 Freon-114 U 1.0 ~glL Hexachlorobuladiene U 1.0 IJg/L Isopropyl acetate U 1.0 pg/L Isopropylbenzene U 1.0 IJg/L m,p-Xylene U 2.0 IJg/L Methyl tert-butyl ether U 1.0 pg/L Methylene chloride U 1,0 pg/L n-Amyl acetate U 1.0 pg/L Naphthalene LI 1.0 pgtL n-Butyl acetate U 2,0 pg/L n-Butylbeezene U 1,0 I~g,'L n-Propyl acetate U 1.0 IJglL n-Propylbenzene U 1.0 pg/L o-Xylene U 1.0 pglL p-Diethylbenzene U 1.0 pglL p-Ethyltaluene U 1.0 pg/L sec-Butylbenzene U 1,0 pg/L Styrene U 1.0 pg/L t-Butyl alcohol U 1.0 pg/L tert-Buty~benzene U 1.0 JJglL Tetrachiomethene U 1.0 IJg/L Toluene 10 1.0 pg/L trans-1,2-Dichloroethene U 1,0 IJg/L trans-1,3-Dichloropropene U 1.0 pg/L Trichloroethene U 1,0 pg/L TriGhlorofluommethane U 1.0 pg/L Vinyl acetate U 1.0 IJglL Vinyl chlodde U 1.0 HglL Sum. 4-Bmmofluorobenzene 98.8 54-134 %REC Sum. Dibremofluoromethane 105 52-132 %REC Sum Toluene-d8 97.3 51-127 %REC DF Date Analyzed Analyst: LDS 3/21/2007 5:44:00 PM 3/21/2007 5:44:0{3 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 312112007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2(307 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/2112007 5:44:00 PM 3121/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:{30 PM 3/21/2007 5:44:00 PM 3/21/2007 5:44:00 PM Qualifiers: B Analyle detected in thc associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates thc compound was analyzed for but not detecto Page 60 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenport, N,Y. 0703166-13A Client Sample ID: Tag Number: Collection Date: Matrix: No. 1 [GWl 3/20/2007 2:10:00 PM LIQUID Analyses Result MERCURY Mercury 0.00114 TARGET ANALYTE LIST METALS Aluminum 491 Antimony U Amenic 0.413 Barium 1.03 Beryllium U Cadmium U Calcium 22.9 Chromium 1.39 Cobalt U Copper 0,978 Imn 319 Imn 1280 Lead 0,286 Magnesium 39.2 Manganese 10.5 Nickel 0.729 Potassium 52.4 Selenium U Silver U Sodium 16,9 Thallium U Vanadium 1.02 Zinc 0.867 SEMIVOLATILE 8W-846 METHOD 8270 1,2,4-Trichlorobar, zen e U 1,2-Dichlombenzena U 1,3-Dichlombenzene U 1,4-Dichlombenzene U 2,4,5-Tdchlorophenol U 2,4,6-Trichlorophenol U 2,4-Dichlorophenol U 2,4-Dimethylphenol U 2,4-Dinitmphenol U 2,4-Dinitrotoluene U 2,6-DiniLroteluene U 2-Chloronaphlhalene U Limit Qual Units DF Date Analyzed SW7470A Analyst: WN 0.000200 mgA- I 3/27/2007 12:05:55 PM SW6010B SW3010A Analyst: JP 0.200 mglL 10 3/23/2007 11:16:52 AM 0.0250 mg/L I 3/23/2007 9:54:25 AM 0.0250 mg/L 1 3/23/2007 9:54:25 AM 0.0200 mg/L 1 3/23/2007 9:54:25 AM 0.0200 mg/L 1 3/23/2007 9:54:25 AM 0.0100 mg/L I 3/23/2007 9:54:25 AM 0.9250 mg/L 1 3/23/2007 9:54:25 AM 0.0200 mglL 1 3/23/2007 9:54:25 AM 0.0200 mg/L I 3/23/2007 9:54:25 AM 0.0200 ragA- 1 3/23/2007 9:54:25 AM 0.0200 mg/L t 3/23/2007 9:54:25 AM 0.200 mg/L 10 3/23/2907 11:16:52 ^M 0.0150 mg/L 1 3123/2007 9:54:25 AM 0.0200 mglL 1 3/23/2007 9:54:25 AM 0.0200 mg/L 1 3/23/2007 9:54:25 AM 0,0200 mg/L 1 3/2312007 9:54:25 AM 0.100 mg/L I 3/23/2007 9:54:25 AM 0.0250 mg/L 1 3/23/2007 9:54:25 AM 0.0200 mg/L I 3/23/2007 9:54:25 AM 0.0300 mg/L I 3/23/2007 9:54:25 AM 0.0150 mg/L I 3/23/2007 9:54:25 AM 0.0290 mg/L 1 3/23/2007 9:54:25 AM 0.0200 mg/L 1 3/23/2007 9:54:25 AM SW82700 SW3510 Analyst: RN 5.4 jJg/L I 3/27/2007 0:41:00 AM 5.4 pg/L I 3/27/2007 9:41:00 AM 5.4 pg/L I 3/27/2007 9;41:00 AM 5.4 pg/L 1 3/2712007 9:41:00 AM 5.4 pgA_ I 3/27/2007 9:41:00 AM 5.4 pg/L 1 3/2712007 9:41:00 AM 5.4 pg/L I 3/27/2007 9:41:00 AM 5.4 pg/L I 3/27/2007 9:41:00 AM 11 pg/L 1 3/27/2007 9:41:00 AM 5,4 pg/L 1 3/27/2007 9:41:00 AM 5.4 p~/L 1 3/27/2007 9:41:00 AM 5.4 pg/L 1 3/27/2007 9:41:00 AM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected ut the Reporting Limit U Indicates the compound was analyzcd for bul not detcctc E Value above quandtation range J Analytc detected below quantitation limi~ S Spiko Recovery outside accepted recovery limits X Value exceeds Maximum CDntaminant Level Page 61 ofT0 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consult~g 0703166 Moores Lane Greenpo~, N.Y. 0703166-13A Client Sample ID: No. 1 [GW] Tag Number: Collection Date: 3/20/2007 2:10:00 PM Matrix: LIQUID Analyses Result SEMIVOLATILE SW-846 METHOD 8270 2-Chlorophenol U 2-Methy[nsphthalene U 2-MethyJphenol U 2-Nitmaniline U 2-Nitrophenol U 3,3'-Dichlorobenzidine U 3+4-Methylphenol U 3-NRreaniline U 4,6-Dinit ro-2.methylphenol U 4-Bromaphenyl phenyl ether U 4-Chlom-3-methylphenol U 4-Chloroani[ine U 4-Chlorophenyl phenyl ether U 4'-Nitroanlline U 4-Nitrophenol U Acenaphthene U Acenaphthylene U Aniline U Anthracene U Azobenzene U Benzidine U Benzo(a)anthracene U Benzo(a)pyrene U Benzo(b)flueranthane U Benzo(g,h,I)peyene U Benzo(k)fluoranthene U Benzoic acid U Benzyl alcohol U Bis(2-chlorcethoxy)methane U BIs(2~chloroethy0ether U Bl$(2.-~hloroisopropyl)et her U Bis(2-elhylhexyl)phthalate U Butyl benzyl phthalate U Carbazole U Chrysene U D[benzo(a,h)ant hracene U Dlbenzofuran U Diethyl phthalate U Dimethyl phthatate U Limit Qual Units SW82709 SW3510 5.4 pg/L 5.4 pglL 5.4 pg/l. 5.4 IJg/L 5.4 pg/L 5.4 pg/L 5.4 pgA. 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pglL 5.4 pg/L 5.4 IJglL 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5,4 pglL 5,4 pglL 5.4 pg/L 9.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 IJg/L 5,4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 pg/L 5.4 ug/L 5.4 pg/L DF Date Analyzed Analyst: RN 3/27/2007 9:41:00 AM 3/27/2907 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 312712007 9:41:00 AM 3/27/2007 0:41:00 AM 3/2712007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2097 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/2712007 9:41:00 AM 3/27/2907 9:41:00 AM 3/2712007 9:41:00 AM 3/2712007 9:41:00 AM 3/27/2007 9:41:00 AM 3~27~2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/2712007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 312712007 9:41:00 AM 3/2712007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3t27/2007 9:41:00 AM Qualifiers: B Anal)ne detected in the assoalmcd Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at thc Reporling L~mit U {ndicales the compound was analyzed for but not dclectc E Value above quamitation range J Analyle d~ected belmv quamilation I/mits S Spike Recovery outside acccpt,~:i rccovc~, limits X Value excccds Maximum ContmnJa~tnl Levcl Page 62 ofT0 American Analytical Laboratories, LLC. Date: 28-blar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane Greenport, N.Y. 07031664 3A Client Sample ID: Tag Number: Collection Date: Matrix: No. I [GW] 3/20/2007 2:10:00 PM LIQUID Analyses Result Limit Qual SEMIVOLATILE SW-846 METHOD 8270 SW8270D Di-n~ulyl phthalata U 5.4 Di-n-octyl phtharate U 5.4 Fluoranthene U 5.4 Finorene U 5.4 Hexachlorobenzene U 5.4 Hexachlorobutadiene U 5.4 Hexachlo rocycropentadiene U 5.4 Hexachloroethane U 5.4 Indeno(1.2,3-c,d)pymne U 5.4 Isophorone [J 5.4 Naphthalene U 5.4 Nitrobenzene U 5.4 N-Nitrosodime[hylamine U 5.4 N-Nthosadi..n-propylamine U 5.4 N-Nitroeodiphenylamioe U 5.4 Pentachlomphenol U 5.4 Phenanthreoe U 5.4 Phenol U 5.4 Pymne U 5.4 Pyridine U 5.4 Sure 2,4,6-Tflbmmophenol 1570 22-124 S Surr: 2-Fluombiphenyl 73.6 19-124 S un':. 2-Fluorophenol 50.6 16-112 Surr: 4-TerphenyFd14 89.0 17-121 Sure Nttmbenzene~5 63.1 19-115 Sum Pheno{-d5 32.2 12-102 VOLATILE SW-846 METHOD 8260 SW8260B 1,1,1-Tdchiuroethane U 1.0 1,1,2,2-Tetrachloroethane U 1.0 1,1,2-Trichlom-I .2,24rifluoroetbane U 1.0 1,1,2-Trich]oroethane U 1.0 1,1 -Dichinraeth ane U 1.0 1 ,t -Dichloroethene U 1.0 1,1 -Dichlompropene U t .0 1,2,3-Trichlorobe nzene U 1.0 1,2,3-Trfchloropropane U 1.0 1,2,4,5-Tetramethylbenzene U 1.0 1,2,4-Tflch[ombenzene U 1 .D Units SW3510 pg/L 1 l~g/L pg/L 1 pglL 1 pglL 1 pglL 1 pglL 1 pg/L 1 pg/L 1 IJg/L 1 pglL 1 pglL 1 pg/L 1 pg/L 1 pg/L 1 pg/L pg/L 1 pg/L 1 pgtL 1 pg/L 1 %REC 1 %REC 1 %REC 1 %REC 1 %REC I %REC I 1 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pglL I pglL 1 pg/L 1 pglL 1 ~g/L 1 pg/L 1 DF Date Analyzed Analyst: RN 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 312712007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41 :OD AM 3/27/2007 9:41:00 AM 3/27/2007 9;41:00 AM 3/2712007 9:41:00 AM 3/2712007 9:41:00 AM 3~27~2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:00 AM 3/27/2007 9:41:OD AM 3/2712007 9:41:00 AM 3/27/2007 9:41:00 AM 3/2712007 9:41:00 AM 3/2712007 9:41:00 AM 3/2712007 9:41:00 AM 3/2712007 9:41:00 AM 3127/2007 9:41:00 AM 3127/2007 9;41:00 AM 3/27/2007 9;41:00 AM 3127/2007 9:41:OD AM Analyst: LDS 3/21/2007 5:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3121/2007 6:32:00 PM 3/21/2007 6:32;OD PM 3/2112007 5:32:OD PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:0n PM 3/21/2007 6:32:00 PM 3/2112007 6:32:00 PM Qualifiers: Analyte detected in lhe associated Method Blank Holding times for preparation or analysis exceeded Nol Detected at the Reponing Limit Indicates the compound was analyzed for but not dctecte Value al)ava quantitafion range Ana/yte detected below quamltafion limits Spike Recovel~ outside accepted recovep/limits Value exceeds M0ximum Contaminant Level Page 63 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consult~g 0703166 Moores Lane Greenpo~,N.y. 0703166-13A Client Sample ID: Tag Number: Collection Date: Matrix: No. 1 [GW] 3/20/2007 2:! 0:00 PM LIQUID Analyses Result VOLATILE SW-848 METHOD 8260 1,2,4-Trimet hylbenzene U 1,2-Dibromo.3-chloropfopane U 1,2-Dibromt~ethane U 1,2-Dichlorobenzene U 1,2-Dichlorcethane U 1,2-Dichlompropane U 1,3,5-THmethylbenzene U 1,3-Dichlorobenzene U 1,3-dichloropropane U t ,4-Dichlorobenzene U 2,2-Dichlnropropane U 2-Butanone U 2-Chloroeihyl vinyl ether U 2-Chlotololuene U 2-Hexanone U 2-Propanol U 4-Chloroteluene U 4-1sopropyltoluene U 4-Methyl-2-pentanone U Acetone U Acmlein U Acrylonitrile U Benzene U Brornohenzene U Bramochloromethane U Bromodichinromethane U Brornoforrn U Bromomethane U Carbon disulfide U Carbon teirachlodde U Chlofobenzene U Ch]orodifluoromethane U Chloroethane U Chinro~on~ U Chlommethane U als-1,2-Dichloroethene U cis-1,3-Dichlarapropene U Dibromochlorornethane U Dibromorneihane U Limit Qual Unils SW8260B 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pglL 1.0 pg/L 1.0 gg/L 1.0 pg/L 3.0 pg/L 1.0 pg/L 1.0 pglL 2.0 pg/L 1.0 pg/L 1.0 pg/L 2.0 I~glL 2.0 pg/i. 1.0 yg/L 1.0 pg/L 1.0 pg/L 1.0 pglL 1.0 pD/L 1.0 pg/L 1.0 pglL 1.0 pg/L 1.0 pg/L 1.0 pglL 1.0 pg/L 1.0 pgfL 1.0 pg/L 1.0 pg/L 1.0 ]Jg/L 1.0 pg/L 1.0 pglL DF Date Analyzed Analyst: LD$ 3/21/2007 6:32:00 PM 3121/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/2112007 6:32:00 PM 3/21/2007 6;32:00 PM 3/21/2007 6:32:00 PM 312112007 6:32:00 PM 3/21/2007 6;32:00 PM 312112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6;32:00 PM 3/21/2007 6:32:0fi PM 3121/2007 6:32:00 PM 3/2112007 6:32:00 PM 3/21/2007 6:32:00 PM 3,121/2007 6:32:00 PM 312112007 6:32:00 PM 3/2112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 312112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM Qualifiers: B Analyte dclcctcd in thc associaled Method Blank H Holding times For preparation or anal~is exceeded ND Not Detected at the Reporting Limit U Indicates ~hc compound was analyzed tbr but not detecto Value above quantitatinn range AnaIyl¢ detected below quantitation )italia Spike Recovery outside accepted reeovaty limits Value exceeds Maximum Contaminant Level Page 64 of 70 American Analytical Laboratories, LLC. Date: 2&Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Lane G~enport, N.Y. 0703166-13A Client Sample ID: No. I [GW] Tag Number: Collection Date: 3/20/2007 2:10:00 PM Matrix: LIQUID Analyses Result Limit Qnal Units VOLATILE SW-84fi METHOD 8260 SW8260B DIchlorodifluommethane U 1.0 IJg/L Dlisopropyl ether U 1.0 pg/L Ethanol U 1.0 pg/L Ethyl acelate U 1~0 [JglL Ethylbenzene U 1.0 pg/L Frenn-114 U 1.0 IJglL Hexachlarobutadlene U 1.0 pglL Isopropyl acetate U 1.0 IJglL Isopropyibenzene U 1.0 IJg/L m ,p-Xylene U 2.0 [Jg/L Methyr te~t-butyl ether U 1.0 ug/L Methylene chloride U 1.0 [.Jg/L n-Amyl acetate U 1.0 ug/L Naphthalene U 1.0 gg/L n-Butyl acetate U 2.0 pglL n-Butylbenzene U 1.0 IJg/L n-Pmpyl acetate U 1.0 pglL n-Pmpylbenzene U 1.0 pglL o-Xylene U 1,0 pglL p-Diethylbenzene U 1.0 IJglL p-Ethyltoluene U 1,0 pg/L sec-Butylbenzene U 1.0 lJg/I- Styrene U 1.0 pg/L t-Butyl alcohol U 1.0 IJg/L tert-Butylbenzene U 1.0 pg/L Tetrachloroethene U 1.0 Hg/L Toluene U 1.0 IJg/L trans-1,2-Dichloroethene U 1.0 IJglL tmns-1,3--Dichloropmpe ne U 1.0 I JelL Tdchloroethene U 1.0 HglL Tdchlorofluoromethene U 1.0 IJg/L Vinyl acetate U 1.0 IJG/L Vinyl chlodde U 1.6 IJG/L Burr: 4-Bromofluorobenzene 98.9 54-134 %REC Sum Dibromofluoromethane '108 52-132 "AREC Sum Toluene<lB 96.0 51-127 %REC DF Date Analyzed Analyst: LDS 312112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 312112007 6:32:00 PM 3/21/2007 6;32:00 PM 3121/2007 6:32:00 PM 312112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32;00 PM 3/2112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/2112007 6:32:06 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6;32:00 PM 3/21/2007 6:32:00 PM 312112007 6:32:00 PM 3/2112007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3121/2007 6:32:00 PM 3/21/2fl07 6:32:00 PM 3/21/2oo7 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6;32:00 PM 3/21/2007 6:32:00 PM 3121/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3/21/2007 6:32:00 PM 3t21/2007 6:32:00 PM Qualifiers: B Anatyte detected in the ossoeiated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected al the Reporting Limit U Indicates the compound was analyzed for but not delecte E Value above quantitedon range J Analyt e detected be[ow qulmfitation limits S Spike Recovery oalside accepted recover3' limits X Value exceeds Maximum Conteminant Level Page 65 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moo~s Lane G~enport, N.Y. 0703166-14A Client Sample ID: Tag Number: Collection Date: Matrix: No. 6 [OW] 3/20/2007 2:50:00 PM LIQUID Analyses MERCURY Mercury TARGET ANALYTE LIST METALS Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc SEMIVOLATILE SW-846 METHOD 8270 1,2,4-Trichlorobenzene 1,2.Dichlombenzene 1,3-Dichlorobenzene t ,4-DIchlorobenzene 2,4,5-Trichlerophenol 2,4,6-Trichlorophenol 2,4-Dichlomphenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotaluene 2,6-DJnitmtoluene 2-Chlornnaphthalene 2-Chlorophenol Result Limit Qual Units SW7470A 0.000270 0.000200 mg/L SW6010B SW3010A 759 0,200 mglL U 0.0250 mg/L 0.380 0.0250 mg/L 1.92 0.0200 mg/L U 0.0200 mg/L 0.0114 0.0100 mg/L 50.9 0.0250 mg/L 1.66 0.0200 mg/L U 0.0200 mg/L 1.58 0.0200 mglL 1500 0.200 mg/L 0,478 0.0150 ragA- 68.5 0.0200 rog/l_ 18.3 0,0200 ragA- 0.763 0.0200 mg/L 81.6 0.100 mgA- U 0.0250 mg/L U 0.0200 mglL 23.6 0.0300 mg/L U 0,0150 mg/L 1.49 0,0200 mglL 1.79 0,0200 mg/L SW82700 SW35'I0 U 5.2 pg/L U 5.2 pgA- U 5.2 pgfL U 5.2 pgA_ U 5.2 pgA_ U 5.2 pglL U 5.2 pg/L U 5.2 pglL U 10 pgA- U 5,2 pg/L U 5.2 pg/L U 5.2 pg/L U 5.2 pgA_ DF Date Analyzed Analyst: WN 3/27/2007 12:08:03 PM Analyst: JP 10 3/23/2007 11:21:05 AM I 3/23/2007 9:56:54 AM 1 3/23/2007 9:58:54 AM I 3/23/2007 9:56:54 AM I 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM I 3/23/2007 9:56:54 AM I 3/23/2007 9;56:54 AM 1 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM 10 3/23/2007 11:21:05 AM 1 3/2312007 9:56:54 AM 1 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM I 3/23/2007 9:56:54 AM I 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM I 3/23/2007 9:56:54 AM 1 3/23/2007 9:56:54 AM I 3/23/2007 9:66:54 AM 1 3/23/2007 9:56:54 AM Analyst: RN 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/2712007 10:10:00 AM 312712007 10:10:00 AM 3/27/2007 lfi:10:00 AM 3/27/20137 10:10:00 AM 3/27/2007 10:10:00 AM Qualifiers: Analyte detecled in the associated Method Blank Holding tim~ for prcparation or anal~yais cncccdcd ND Not Dcl¢cled at the Reporting Limit U lndicales the compound xva~ analyzed for but not detecte Page 66 of 70 American Analytical Laboratories, LLC. l~ate: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: Lab Order: 0703166 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: Lab ID: 0703166-14A Matrix: No. 6 3/20/2007 2:50:00 PM LIQUID Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE 8W-846 METHOD 8270 SW82700 8W3510 Analyst: RN 2-Methylnaphtharene U 5.2 ~§/L I 3127/2007 10:10:00 AM 2-Methyyhenol U 5.2 ~g/L 1 3/27/2007 10:10:00 AM 2-Nitroaniline U 5.2 ,ug/L 1 3/27/2007 10:10:00 AM 2-Nitrophenol U 5,2 I~g/L 1 3/27/2007 10:10:00 AM 3,3'-Dich[orobenzidine U 5.2 IJg/L 1 3/27/2007 10:10:00 AM 3+4-Methylpbenol U 5,2 pg/l_ 1 3127/2007 10:10:00 AM 3-Nitroanirine U 5.2 pg/L 1 3/27/2007 10:10:00 AM 4,6-Dinitm-2-met hylphenol U 5.2 IJ g/L 1 3~27~2007 10:10:00 AM 4-Bromephenyl phenyl ether U 5.2 I~g/L 1 312712007 10:10:00 AM 4-Chlom-3-methylphenol U 5.2 pg/L I 3/2712007 10:10:00 AM 4-Chthraaniline U 5.2 pg/L 1 312712007 10:10:00 AM 4-Chlorophenyl phenyl ether U 5,2 ,uB/L 1 3/27/2007 10:10:00 AM 4*Nitraaniline U 5.2 I~glL I 3/27/2007 10:10:00 AM 4~Nitrophenol U 5.2 pg/L I 3/27/2007 10:10:00 AM Acenaphthene U 5,2 p§/L I 3/27/2007 10:10:00 AM Acenaphthylene U 5.2 i~glL I 3/27/2007 10:10:00 AM Aniline U 5.2 pglL I 3/27/2007 10:10:00 AM Anthracene U 5.2 pglL I 3/27/2007 10:10:00 AM Azohenzene U 5.2 I~g/L 1 3/27/2007 10:10:00 AM Benzidine U 5.2 ~Jgfl_ 1 3/27/2007 10:10:00 AM Benze(a)anthracer~e U 5.2 pgA_ 1 3/27/2007 10:10:00 AM Benzo(a)pyrene U 5.2 pgA_ 1 3/27/2007 10:10:00 AM Benzo(b)fluoranthene U 5.2 pDIL 1 3/2712007 10:10:00 AM Benze(g,h,l)perylene U 5.2 pgA_ 1 3127/2007 10:10:00 AM Banzo(k)fluoranthene U 5.2 IJg/L 1 3/27/2007 10:10:00 AM Benzoic acid U 5.2 pg/L 1 3/27/2007 10:10;00 AM Benzyl alcohol U 5.2 pg/L I 3/27/2007 10:10:00 AM Bis(2-chloroethoxy)methane U 5.2 pglL 1 3127/2007 10:10:00 AM Bis(2-chlomethyl)ether U 5.2 pg/L I 3/27/2007 10:10:00 AM Bis(2-chloroisopropyl)elher U 5.2 pg/L 1 3/27/2007 10:10:00 AM Bis(2-ethylhexyl}phthalate U 5.2 pglL I 3/27/2007 10:10:00 AM Butyl benzyl phthalate U 5,2 pg/1.. 1 3/2712007 10;10:00 AM Carbazole U 5.2 pg/L 1 3/27/2007 10:10;00 AM Chrysene U 5.2 pgA- 1 3/27/2007 10:10:00 AM Dibenzo(a.hIanthracene U 5.2 pg/L 1 3/27/2007 10:10;00 AM Dlbenzofuran U 5.2 pg/L t 3/27/2007 10:10:00 AM Diethy[ phthalate U 5.2 pg/L I 3/27/2007 10:10:00 AM Dirnethyl phthalate U 5.2 F§/L 1 3/2712007 10:10:00 AM Di-n-butyl phlhalate U 5.2 ~g/L I 312712007 10:10:00 AM Qualifiers: Analyte detected in the ~ssoclated Method Blank Holding times for preparation or analysis exceeded ND Not Detected at thc Reporting Limit E Value above quandtation range J Analyte detecled below quantitation liraits S Spike Rcco'~ery outside accepted recovery limits X Value exceeds Maximum Contaminanl Level Page 67 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703166 Moores Laae Greenport, N.Y. 0703166-]4A Client Sample ID: No. 6 [GW] Tag Number: Collection Date: 3/20/2007 2:50:00 PM Matrix: LIQUID Analyses Result SEMIVOLATILE SW-846 METHOD 8270 Di-n..octyl phthalate U Fluoranthena U Fluorene U Hexachlorobenzene U Hexachlorobuladiene U Hexachlorocyclopentadiene U Hexachloroethane U Indeno(1,2,3-c,d}pytene U Isophorone U Naphthalene U Nitrobanzene U N-Nitmsodlmuthylamine U N-Nitrosodi-n-pmpylamine U N-Nitmsocliphenylamine U Pentachlurophenol U Phenanthrene U Phenol U Pyrene U Pyddine U Sum 2,4,6-Trlbromophenol 72.0 Sum 2-Fluorobiphenyl 75.0 Sum 2-Fluomphenol 53.6 Surf: 4-TerphenyFd14 84,0 Sum Nitrobenzerle~15 64.2 Surr: Phenol-d6 32.9 VOLATILE SW-846 METHOD 8260 1,1 ,l,2-Tet rachloroet hane U 1,1,1-Tdchlomethane U 1,1,2,2-Tetrachloroethane U 1,1,2-Trichloroethane U 1,1 -Oichloroethanu U 1,1 -Dtchlomethene U 1,1-Dichlompmpene U 1,2,3-Trichlorobenzene U 1,2,3-Trichletopropane U 1,2,4,5-Tat ramet hylbenzene U 1,2,4-Tdchlorobenzene U 1,2,4-Trim ethylbenzene U Limit Qual Units SW82700 8W3510 5.2 pglL 5.2 Poll 5.2 pg/L 5.2 pg/L 5.2 pg/L 5,2 pg/L 5,2 pg/L 5.2 p0/L 5.2 p01L 5.2 pg/L 5.2 polL 5,2 p0/L 5.2 gg/L 5,2 poll 5.2 polL 5.2 p0/L 5.2 pglL 5.2 pg/L 5.2 pg/L 22-124 %REC 18-124 %REC 16-112 %REC 17-121 %REC 19-115 %REC 12-102 %REC SW82600 1.0 polL 1.0 polL 1.0 gg/L 1.0 polL 1.0 IJg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 pg/L 1.0 poll DF 1 1 1 1 1 Date Analyzed Analyst: RN 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/2712007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 I0:10:00 AM 3/27/2007 10:10:00 AM 3/2712007 10:10:00 AM 3/27/2007 10:10:00 AM 3/2712007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2067 10:10:00 AM 3/2712007 10:10:g0 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 I0:10:0g AM 3/2712007 lg:10:00 AM 3/27/2007 10:10:00 AM 3/27/2097 10:10:00 AM 3/2712007 10:10:00 AM 3/27/2007 10:10:00 AM 3/2712007 10:10:00 AM 3/27/2007 10:10:00 AM 3/27/2007 10:10:00 AM Analyst: LDS 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 312112007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/2112007 7:20:00 PM 312112007 7:20:00 PM 3/21/2007 7:20:00 PM Qanlif'mrs: B Anatyle detected in the associated Method Blank H Holding times for preparation or analysis exceeded Not De~ected at thc ReporQng Limit U lnthcatcs thc compound w~s analyzed for but not detecte E Value above quamitation ~ngc J A~alytc detected below quamilation limits S Spike Rccove~ outside I~CC~pt ed recovery limits X Value :ncc:ds Maximum Contaminant L~v¢l Page 68 of 70 American Analytical Laboratories, LLC. Oatc: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703166 Moores Lane Greenpon, N.Y. 0703166-14A Client Sample ID: Tag Number: ColLection Date: Matrix: No. 6 [OW] 3/20/2007 2:50:00 PM LIQUID Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82600 1,2-Dibromo-3-chloropropane U 1.0 1,2-Dibromoethane U 1.0 1,2-Dichlorobenzene U 1.0 1,2-Dichlorcethane U 1.0 1,2-Dichlempropane U 1.0 1,3,§-Tdrnethylbenzena U t.0 1,3-Dichlorobenzene U 1.0 1,3~ichloropropane U 1.0 1,4-Dichlorobenzene U 1.0 2,2-Dlchloropropane U 1.0 2-Butanone U 3.0 2-Chloroethyl vinyl ether U 1.0 2-Chlor~oluene U t .0 2-Hexanone U 2.0 2-Propanol U 1.0 4-Chlerotoluene U 1.0 4-1sopmpyllo{uene U 1.0 4-Methyl-2-pentanone U 2.0 Acetone U 2.0 ^crolein U 1.0 Acrylonitrile U 1.0 Benzene U 1.0 Bromobenzene U 1.0 BromochJerornethane U 1.0 Bmrnodichloromethane U 1.0 Bromoform U 1.0 Bromomethace U 1.0 Carbon disulfide U 1.0 Carbon tetrachloHde U 1.0 Chlorobenzene U 1.0 Chlorodifiuorornethane U 1.0 Chloroethane U 1.0 Chlorofem~ U 1.0 Chloromethane U 1.0 c[s-1,2-Dichloroethene U 1.0 cis-1,3-Dtchloropropene U 1.0 Dibromochloromethane U 1.0 Dibrornomethane U 1,0 Dichlerodifluoromethane U 1.0 Units DF Date Analyzed Anatyst: LDS pg/L I 3/21/2007 7:20:00 PM I~g/L 1 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L 1 3/2112007 7:20:00 PM pg/L 1 3/21/'2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM ~Jg/L I 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:{30 PM pg/L 1 3/21/2007 7:20:00 PM ~g/L I 3/2112007 7:20:00 PM I~g/L 1 3/2t/2007 7:20:00 PM pglL I 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L I 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L I 3/21/2007 7:20:00 PM I~g/L 1 3/21/2007 7:20:00 PM pglL 1 3/21/2007 7:20:00 PM pg/L I 3/21/2007 7:20:00 PM ~g/L 1 3/2112007 7:20:00 PM ~glL 1 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L I 3/21/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pglL 1 3/21/2007 7:20:00 PM ~Jg/L 1 312112007 7:20:00 PM ug/L 1 3/2t/2007 7:20:00 PM ~glL 1 3/21/2007 7:20:00 PM pg/L I 3/21/2007 7:20:00 PM pg/L 1 3/21/2{307 7:20:00 PM pgfL I 3/21/2007 7:20:00 PM ~Jg/L 1 3/21/2007 7:20:~X3 PM pg/L 1 3/2112007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM pg/L I 3121/2007 7:20:00 PM pg/L 1 3/21/2007 7:20:00 PM B Analyte detected in Ibc 0asoclated Mc[had Blank H Holding times for preparation or analysis exceeded ND Not Detected at Se Reporting Limit U Indicates file compound was nn ~lyz=d for but not detecte E Value above quantilation range J Analytc detected below quantita~ion limit~ S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Conlaminanl Level Page 69 of 70 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Orosser Consulting 0703166 Moores Lane Greenport, N.Y, 0703166-14A Client Sample ID: Tag Number: Collection Date: Matrix: No. 6 [aWl 3/20/2007 2:50:00 PM LIQUID Analyses Result Limit Qual Units VOLATILE SW-846 METHOD 8260 SW82608 Diisopropyl ether U 1.0 pg/L Ethanol U 1.0 pg/L Ethyl acetate U 1.0 pg/L Ethylbenzene U 1.0 ug/L Freoa- 114 U 1.0 [uglL Hexachlorobutadiene U 1.0 IJglL Isopropyl acetate U 1,0 pg/L Isopropylbenzene U 1.0 pg/L m,p-Xylene U 2.0 ug/L Methyl ted-butyl ether U 1.0 IJglL Methylene chloride U 1.0 pglL n-Amyl acetate U 1.0 pg/L Naphthalene U 1.0 pg/L n-Butyl acetate U 2.0 ug/L n-Butylbenzene U 1.0 IJg/L n-Propyl acetate U 1,0 pglL n-Propylbenzene U 1.0 lJg/L o-Xylene U 1.0 pg/L p-Diethylbenzene U 1.0 pg/L p-Ethyltoluene U 1.9 pg/L sec-Butylbenzene U 1.0 Styrene U 1.0 pg/L t-Butyl alcohol U 1.0 ~g/L tert-Butylbenzene U 1.0 pg/L Tetrachloroethene U 1.0 pg/L Toluene 3.3 1.0 pg/L tmns-1.2-Dichloroethene U 1.0 uglL trans-1,3-Dichloropropene U 1.0 pg/L Tfichloroethene U 1.0 pg/L Triehlorafluoromethane U 1.0 pg/L Vinyl acetate U 1.0 pg/L Vinyl chloride U 1.0 jJg/L Sun. 4-Bromofluorobenzene 101 544 34 %REC Sun. Dibmmo0uoromethane 106 52-132 %REC Surr: Toluene-d8 95.7 51-127 %REC DF Date Analyzed Analyst: LDS 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/2112007 7;20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20;00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20;00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/2112007 7:20;00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3t21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM 3/21/2007 7:20:00 PM Qualifiers: B Analytc detected in the associated Method Blank H Holding times for preparation or analysis cxcc~dcd ND Not Dclecled at the Reporting Limit U Indicates thc compound was analyzed for but not detecte E Value above quantitation range J Analyle detecled below quantitstion l/mits S Spike Recover7 outside accepted recuve~ limits X Value exceeds Maximum Contaminant Level Page 70 of 70 .&MERIC&N &,N&LYTIC&,L L&BOR&TORIES NYSDOH NJDEP CTDOH PADEP 11418 NY050 PH-0205 684~0573 Wednesday, March 28, 2007 Frank Castellano P.W. Grosser Consulting 630 Johnson Avenue Suite 7 Bohemia, NY 11716 TEL: (631) 589-6353 FAX (631) 589-8705 RE: Moores Lane Greenport, N.Y. Dear Frank Castellano: Order No.: 0703179 American Analytical Laboratories, LLC. received 8 sample(s) on 3/22/2007 for the analyses presented in the following report. Samples were analyzed in accordance with the test procedures documented on the chain of castody and detailed throughout the text of this report. The limits provided in the data package are analytical reporting limits and not Federal or Local mandated values to which the sample results should be compared. There were no problems with the analyses and all data for associated QC met laboratory specifications. If there are any exceptions a Case Narrative is provided in the report. If you have any questions regarding these tests results, please do not hesitate to call (631 ) 454-6100 or email me directly at lbeyer~american-analytical.com. Sincerely, Lori Beyer Lab Directo~r 56 TOLEDO STREET * FARMINGDALE, NEW YORK 11735 (631)454-6100 ,* FAX: (631)454-8027 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Project: Lab Order: Lab Sample ID 0703179-0 IA 0703 t 79-02A 0703179-03A 0703179-04A 0703179-05A 0703179-06A 0703 t 79-07A 0703179-08A Moores Lane Greenport, N.Y. 0703179 Client Sample ID No. 9 [2.5-5'l No. 9 [GW] No. 10 [2.5-5] No. 10 [OW] No. 7 [12.5-15'] No. 7 [ow] No. l 1 [5-7.5'] No. 1~ [GW] Tag Number Work Order Sample Summary Date Collected Date Received 3/21/2007 9:25:00 AM 3/22/2007 3/21/2007 10:16:00 AM 3/22/_9007 3/21/2007 10:55:00 AM 3/22/2007 3/21/2007 12:17:00 PM 3/22/2007 3/21/2007 1:35:00 PM 3/22/2007 3/21/2007 1:57:00 PM 3/22/2007 3/21/2_007 3:15:00 PM 3/22/2007 3/21/2007 3:29:00 PM 3/22/2007 Page 1 of 1 NYSDOH 11418 56 TOLEDO STREET · FARMINGDALE, NEW YORK 11735 CTDOH PH-02O5 (631) 454-6100 · FAX (631) 454-8027 TAG # ! COG NJDEP NY050 PADEP 68-573 CHAIN OF CUSTODY / REQUEST FOR ANALYSIS DOCUMENT CLIENT NAMEIADDRESS~, C. CONTACT: Fr~l~ c~l~.ll(~ ~3~ ~O~tn~ ~. ~ SEALED YES / NO NOL PRESERVED ID ~ MA~IX TAINERS DA~ SAMPLE ~. LOCATION TIME I COOLER TEMPE~TUR~: ~PE G=G~B; C=COMPOSITE, SS=SPLIT 8POO~ NORMAL~ STAT RELINQUISHED BY (SIGNATURE) DATE',/', PRINTED ~ME RECEi~D BY ~B (SIGNATURE) T;%~ PRINTED NAME RELINQUISHED BY (SIGNATURE) DATE PRINTED NAME RECEIVED~B (SIGNATURE) gATE PRINTED NAME TIME TIM~ WHITE-OFFICE / CANARY-LAB / PINK-SAMPLE CUSTODIAN / GOLDENROD-CLIENT AMERICAN ANALYTICAL LABORATORIES, LInC 56 TOLEDO STREET FARMINGDALE, NEW YORK 11735 ... TELEPHONE: (631) 454-6100 FAX: (631) 454.8027 DATA REPORTING QUALIFIERS For repealing results, the following "Results Qualitiers" are used: Value U B E D P N H If the result is greater than or equal to the detection limit, report the value Indicates the compound was analyzed for but was not detected. Report the minimum detection limit for the sample with the U, i.e. "IOU". This is not necessarily the instrument detection limit attainable for this particular sample based on any concentration or dilution that may have been required. Indicates an estimated value. The flag is used: (1) When estimating a concentration for a tentatively identified compound (library seamh hits, where a 1:1 response is assumed.) (2} When the mass spectral data indicated the identification, however the result was less than the specified detection limit greater than zero. If the detection limit was 10ug/L and a concentration of 3uglL was calculated roped as 3J. This flag is used when similar situations arise on any organic parameter i.e. Pesticide, PCBs and others. Indicates the analyte was found in the blank as well as the sample re port "1 OB". Indicates the analytes concentration exceeds the calibrated range of the instrument for that specific analysis. This flag identities all compounds identified in an analysis at a secondary dilution factor. This flag is used for Pesticide / PCB target analyte when there is >25% difference for detected concentrations between the two GC Columns. The higher of the two values is reported on Form I and flagged with a "P". This flag indicates presumptive evidence of a compound. This is only used for tentatively identified compounds (TICs}, where the identification is based on a mass spectral library search. It applies to all TIC results. For generic characterization of a TIC, such as chlorinated hydrocarbon, the flag is no{ used. Indicates sample was received and/or analyzed outside of The method allowable holding time American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-01A Client Sample ID: Tag Number: Collection Date: Matrix: No. 9 [2.5-5'] 3/21/2007 9:25:00 AM SOIL Analyses Result Limit Qual MERCURY SW7471B Mercury U 0.0109 PERCENT MOISTURE D2216 Percent Moisture 12.8 0 TARGET ANALYTE LIST METALS SW60'IOB Aluminum 1130 0.443 Antimony U 0.553 Arsenic 1.15 0.653 Barium 8.58 0.440 Beryllium O 0.443 Cadmium U 0.221 Calcium 126 0.553 Chromium 4.10 0,443 Cobalt U 0.443 Copper 5.36 0.443 Iron 2470 0.443 Lead 9.49 0.332 Magnesium 283 0.443 Manganese 45.4 0.443 Nickel 2,25 0,443 Potassium 229 2.2'1 Selenium U 0.553 Silver U 0.443 Sodium 72.2 1.33 Thallium U 0,443 Vanadium 5.20 0.443 Zinc 9.79 0,443 SEMIVOLATILE SW-848 METHOD 8270 SW8270D 1,2,4-T~fiohlorobenzene U 130 1,2-Dichlorobenzene U 130 1,3-Dichlorobenzene U 130 1,4-D[chlorobenzene U 130 2,4,5-Trichlorophenol U 130 2,4,6-Trichlorophenol U 130 2,4-Dichlorophenol U 130 2,4-Dimethylphenol U 130 2,4-Dinitrophenol U 130 2,443initrotuluene U 130 2,6-D[nitrotoluene U 130 Units DF Date Analyzed SW7471B Analyst: WN nng/Kg-dry 1 3/27/2007 12:33:28 PM Analyst: CM wt% I 3/22/2D07 SW3050A Analysl: JP mg/Kgq:lry 1 3~27~2007 12:14:00 PM rog/Kg-dry 1 3/27/2007 12:14:00 PM mg/Kgq:lry 1 3/27/2007 12:14:00 PM mg/Kg-dry 1 3~27~2007 12:14;00 PM rng/Kg~ry I 3/2712007 12:14:00 PM ms/Kg-dry 1 3/27/2007 12:14:00 PM mg/Kgqlry 1 3/2712007 12:14:00 PM rng/Kgq:lry 1 3/27/2007 12:14:00 PM mg,*Kg-d~ 1 3~27~2007 12:14:00 PM mg/Kg-dsy I 3/27/2007 12:14:00 PM mg/Kg~lry I 3127/2007 12:14:00 PM ms/Kg-dry 1 3/27/2007 12:14:00 PM ms/Kg-dry I 3/2712007 12:14:00 PM mglKg-dry I 3/2712007 12:14:00 PM ms/Kg-dry I 3/27/2007 12:14:00 PM mg/Kgq:lry 1 3/2712007 12:14:00 PM ms/Kg.dry I 3/2712007 12:14:00 PM rog/Kg-dry 1 3/2712007 12:14:00 PM mg~g~try 1 3/2712007 12:14;00 PM mglKg<lry 1 3/27/2007 12:14:00 PM rog/Kg-dry 1 3127/2007 12:14:00 PM rnglKg-dry I 3/27/2007 12:14:00 PM SW3550A Analyst: RN pglKg-dry I 3/26/2007 3:1g:00 PM ps/Kg-dry 1 3/26/2007 3:19:00 PM tJg/Kgqt~y I 3/25/2007 3:19:00 PM pglKg-dry 1 3/26/2007 3;19:00 PM pglKg-dry 1 3/26/2007 3:19:00 PM IJg/Kgq:lry 1 3/26/2007 3:1g:00 PM IJg/Kg-dry 1 3/26/2007 3:19:00 PM pgtKg-dry I 3/26/2007 3:19:00 PM IJglKg-dsy 1 3/26/2007 3:19:00 PM pglKg-dry 1 3/26/2007 3:19:00 PM PS/Kg-city 1 0/26/2007 3:I9:00 PM Qualifiers: B Analyte delected in the associated Method Blank Holding times for preparation or analysis exceeded ND Hot Dcteeted at thc Rcporiing Limit U lndicnt~ thc compound was analyzed for but not detecto E Value above quantitalion range J Analyla detected beloxv quaatitation limils S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminanl Level Page 1 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consult~g 0703179 Moores Lane Greenpo~,N.Y. 0703t79-01A Client Sample ID: No. 9 [2.5-5'] Tag Number: Collection Date: 3/21/2007 9:25:00 AM Matrix: SOIL Analyses Result Limit Qual SEMIVOLATILE SW-84fi METHOD 8270 SW82700 2-Chloronaphthalene U 130 2-Chlorophenol U 130 2-Melhylnaphthalene U 130 2-Methylphenel U 130 2-Nilroaniline U 130 2-Nilrophenal U 130 3,3 '-Dichlnrobenzidine U 130 3+4-Methylphenol U 130 3-Nit roaniline U 130 4,6-Dinitro-2-met hylphenol U 130 4-Brernaphenyl phenyl ether U 130 4-Chlore-3-rnethylphenel U 130 4-Chloroaniline U 130 4-Chlorophenyl phenyl etiler U 130 4-Nitroaalline U 130 4-Nitrophenol U 160 Acenaphthene U 130 Acenaphthylene U 130 Aniline U 130 Anthracene U 130 Azobenzene U 130 Benzicline U 130 Benzo(a)anthracene U 130 nenzo(a)pyrene U 130 Benzo(b)ileoranthene IJ 130 Benzo(g,h,i)perylene U 130 Benzo(k)fluoranthene U 130 Benzoic acid U 130 Benzyl alcohol U 130 Bis(2-chloroethoxy)malhane U 130 Bis(2-chleroethyl)ethe r U 130 Bis(2'chlaroisepropy0et her U 130 Bis(2-ethylh exyl)phthelate U 130 Butyl benzyl phthalate U 130 Carbazole U 130 Chrysene U 130 Dlbenzo(a,ll)anthracene U 130 Dibenzofuran U 130 Diethyl phthalate U 130 Units DF Date Analyzed SW3550A Analyst: RN [Jg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/2612007 3:19:00 PM pg/Kg.Jry 1 312612007 3:19:00 PM [Jg/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg.dry I 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry 1 3126/2007 3:19:00 PM lag/Kg-dry I 3126/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3;19:00 PM pg/Kg-clry I 3/26/2007 3:19:00 PM pg/Kg<lry 1 3/26/2007 3:19:00 PM IJg/Kg-dry I 3/26/2007 3:19:00 PM IJg/Kg-dry 1 3/26/2007 3:19:00 PM IJg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM pglKg-dry I 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3;19:00 PM pg/Kg-d~y I 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg-dry I 3126/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg--dry I 3/26/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM IJg/Kg-clry 1 3/26/200? 3:19:00 PM IJg/Kg-dry 1 3/26/2007 3:19:00 PM I.tg/Kg~ry 1 3/26/2007 3:19:00 PM pg/Kg-clry 1 3/26/2007 3:19:00 PM pglKg<lry I 3/26/2007 3:19:00 PM ug/Kg.:lry I 3/26/2007 3:19:00 PM pg/Kg<lry I 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/2612007 3:19;00 PM [Jo/Kg-dry 1 3/26/2007 3:19:00 PM [ag/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg-dry I 3/26/2007 3:19:00 PM pg/Kg-dry 1 3/26/2007 3:19:00 PM Qualifiers: E Value above quantitafion range J Analyte detected below quantitation limits S Spike Recover7 outside accepted re, c. oveff limiu X Value exceeds Maximum Contaminant Level Page 2 o[40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Montes Lane Greenport, N.Y. 0703179431A Client Sample ID: Tag Number: Collection Date: Matrix: No. 9 [2.5-5'] 3/21/2007 9:25;00 AM SOIL SEMIVOLATILE SW-846 METHOD 8270 Dimethyl phthalate Dim~butyl phthalate Di-n-octyl phthalate Hexachlombutadiene Hexachlorocyclepent adiene Indeno(1,2,3-c.d}pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodimethylamine N-Nitrosodi-n-pmpylamine N-Ngrosodiphenylamine Pentachlomphenol Phenanthmna Phenol Pyddine Surf:. 2,4,6-Tribromophenol Surf: 2-Fluorobiphenyl Sure 2-Fluoropheno[ Sun':. 4-Terphenyl-d14 Sum Nitrobenzene-d5 Sun-: Phenol-d6 VOLATILE SW-846 METHOD 8260 1,1,1,2-Tetrachlomethane 1,1,2.2-Tetrachloroethane t ,1,2-Tdchloro-1,2,2-trifluoroathaee 1,1,2-Tdchloroelhane 1.1-Dichloroethane 1,1-DIchloroethene 1,1-Dichlnmpropene 1,2,3-Trichlo robenzene 1.2,3-Trichlompropane 1,2,4.5-Tel ramethyibenzene Result Limit Qual Units DF Date Analyzed SW82700 SW3550A U 100 pg/Kg-dry 1 U 130 pglKg-dry 1 U 130 pg/Kg-dry 1 U 130 pg/Kg-dry 1 U 130 pg/Kg-dry 1 U 130 pg/Kg-dry I U 130 IJg/Kg-dry 1 U 160 pg/Kg-dry 1 U 130 pglKg-dry 1 U 130 pg/Kg-dry 1 U 130 pg/Kg-d~J 1 U 130 pg/Kg-d~y 1 U 130 pg/Kg-dry 1 U 130 pg/Kg-dry 1 U 130 IJg/Kg-dry 1 U 130 pg/Kg-dry 1 U 160 pg/Kg~ry 1 U 130 ~g/Kg-dPJ U 130 p~/Kg.dry U 130 pglKg-dry 1 U 130 pg/Kg-d[y 1 59.5 22-124 %REC 1 58.4 27-119 %REC 1 31.2 21-123 %REC 1 62.8 28-126 %REC 1 51.2 21-118 %P. EC 1 42.6 18-129 %REC 1 SW8260B U 5.9 IJglKg-dry 1 U 5.9 pglKg-dry 1 U 5.9 pg/Kg-diy 1 U 5.9 pg/Kg-d~y 1 U 5.9 gg/Kg-dly 1 U 5.9 pg/Kg-dry 1 U 5.9 Fg/Kg-dp/ 1 U 5.9 IJg/Kg..d~y 1 U 5.9 pg/Kg-d~y 1 U 5.9 IJgtKg~ry 1 U 5.9 pg/Kg-d~y 1 Analyst: RN 3/29/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/29/2007 3:19:00 PM 3/29/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/29/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/2612007 3:19:00 PM 3/26/2007 3:19:00 PM 312612007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/2612007 3:19:00 PM 3/26/2007 3:19:00 PM 3~2612007 3:19:00 PM 3126/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3/26/2007 3:19:00 PM 3~26/2007 3:19:00 PM Analyst: MB 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22J2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3122/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM Qualifiers: B Analyle detected in the ossociated Method Blank H Holding times for preparation or analysis exceeded E Value above quantitatJon range J Analyte detected below quamilaion limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contmninam Level Page 3 of 40 American Analytical Laboratories, LLC. Date: 28-Mar~07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpo~,N.Y. 0703179-01A Client Sample ID: No. 9 [2.5-5] Tag Number: Collection Date: 3/21/2007 9:25:00 AM Matrix: SOIL Analyses Result VOLATILE SW-846 METHOD 8260 1,2,4-Trichlorobenzene U 1,2,4-Trimethyibenzene U 1,2-Dibromo-3-chloropropane U 1,2-Dlbrornoethaae U 1,2-Dichlorobenzene U 1,2-Dichloroethane U 1,2-Dichloropropane U 1,3,5-Trimethylbanze ne U 1,3-Dichlorobenzene U 1,3-dich[oropropane U 1,4-Dichlorobenzene U 2,2-Dichloropropane U 2-Butanone U 2-Chloroethyl vinyr ether U 2-Chloroto[uene U 2-Hexanone U 2-Propanol U 4-Chlorotoluene U 4-1sepropyltoluene U 4-Methyl-2-pentanone U Acetone U Acrolein U Ac~ylonitdle U Benzene U Bromobenzene U Brornechlorornethane U Bromodichlorornethane U Bromoform U Brornomethane U Carbon disulfide U Carbon tetrachioride U Chlorobenzene U Chlorodifluoromethane U Chloroethane U Chloroform U Chloromethane U cis-1,2-Dichioroethene U c~a-1,3-Dichloropropene U Dibromochleromethane U Limit Qual SW82606 5.9 5.9 5.9 5.9 5.9 5.9 5.9 5.9 5.9 5.9 5,9 5.9 5.9 59 5,6 6.9 5.9 30 5.9 5.9 5.9 5.9 5.9 5.9 5.9 5.6 5.9 5.9 5.6 5,9 5.9 5.6 5.9 Units ug/Kg-dry pg/Kg-d~j gg/Kg-dry pg/Kg.dry gg/Kg-d~J pg/Kg-dry pg/Kg-dry pg/Kg-dry pg/Kg-dw Fg/Kg-dPj pg/Kg-d~j pg/Kg~w pg/Kg-d~ pg,'Kg-d~ pg/Kg-dPJ pg/Kg-dry pg/Kg-dry pg/Kg.dry pg/Kg-d~ pg/Kg-dry pg/Kg-dr,j pglKg-dry pgfKg-d,~ gg/Kg-d~ pg/Kg-dry gg/Kg-dPj pg/Kg~ly pg/Kg-d~y pg/Kg-dry pg/Kg-dry p§lKg-dry pg/Kg-d~y pg/Kg~ry 9g,'Kg.dry pg/Kg-dry pg/Kg-d~y pg/Kg-dry pg/Kg-thy DF Date Analyzed Analyst: MB 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/20(37 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2607 6:02:00 PM 3/22/2007 6:02;(30 PM 3/22/2007 6:02:00 PM 3/22/2(307 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:0D PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/200'/6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02;00 PM 3/22/2007 6:02:{30 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/20(37 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/23/2007 6;02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:(32:00 PM 3/22/2007 6:02:00 PM 3/22/20{}7 6:62:00 PM 3122/2007 6:02:00 PM 3/22/2007 6:62:00 PM Qualifiers: B Anal)lc detected in thc ~ssociated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Rcportlng Limit U Indicates the compound w~s analyzed for bul not dctecte E Value above quantitalion range J Analyt= detected below quamitation limils 5 Spike Rccovc~ outside accepted rcmvcry limits X Value cxcccds Maximum Conlaminant Level Page 4 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane G~enport, N.Y. 0703179-01A Client Sample ID: No. 9 [2.5-5'] Tag Number: Colleelion Date: 3/21/2007 9:25:00 AM Matrix: SOIL Analyses Result Limit Qual Units VOLATILE SW-846 METHOD 8260 SW82600 Dibremomethane U 5.9 pg/Kg-dpj Dichlorodifluoromethane U 5.9 Hg/Kg~i~ Diisopmpyl ether U 5.9 pglKg~ry Ethanol U 30 pg/Kg-dry Ethyl acetate U 5.9 pg/Kg-d~ Ethylbeazene U 5.9 pg/Kg~ry Freon-114 U 5.9 pg/Kg-d~ Hexachlorobutadiena U 5.9 pg/Kg-d~j Isopropyl acetate U 5.9 pg/Kg.-diy Isopropylbenzene U 5.9 pgfKg-dry m,p-Xylene U 12 pg/Kg~ Methyl teA-butyl ether U 5.9 pg/Kg.dry Methylene chloride U 5.9 pg/Kg-dry n-Amyl acetate U 5,9 pglKg-dry Naphthalene U 5,9 IJg/Kg-.dry n-Butyl acetate U 5.9 pglKg-d~j n-Butylbenzene U 5.9 pg/Kg-dry n-Propyl acetate U 5.9 pg/Kg~ry n-Propylbenzene U 5,9 pg/Kg-dry o-Xylene U 5.9 i~g/Kg-dry p-Diethylbenzene U 5.9 pg/Kg~ry p-Ethyltoluene U 5.0 pg/Kg-dry sec-Butylbenzene U 5.9 pglKg-dry Styrene U 5.9 gglKg-d~y t-Butyl alcohol U 5.9 IJglKg-dry tart-Butylbenzeae U 5.9 pglKg-d~y Tatrachloroethene U 5.9 pg/Kg-dry Toluene U 5.9 pg/Kg-d~ frans-1,2-Dlchloroethene U 5.9 pglKg~ry trans-1,3-DIchloropropene U 5.9 IJg/Kg..dry Trichroroethene U 5,9 I~g/K§-dry Trichlorofluoremethane U 5.9 pg/Kg-dry Vinyl acetate U 5.9 pg/Ko.dry Vinyl chloride U 5,9 pg/Kg<lry Surr: 4-Bramofluorabenzene 94,7 61-133 %REC Sun': Dibromofluoromethane 108 61-139 %REC Sum Toluene-d8 94.1 57-131 %REC DF Date Analyzed Analyst: MB 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3122/2007 6:02;00 PM 3/22/2007 6:02;00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02;00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2067 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02;00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6;02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 EM 3/22/2007 6:02:00 PM 3/22/2007 6:02:06 PM 3/22/2007 6:02:00 PM 312212007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM 3/22/2007 6:02:00 PM Qualifiers: B Analyle detected in the associated Method Blank Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates the compound was analyzed for but not deteete E Valuo above quantitation range J Analyte detected below quantitation limits S Sp~e Recovcq, outsid= acccpted rccovcq, limits X Value exceeds M~ximum Conteminant Level Page 5 of 40 American Analytical Laboratories, LLC. Date: 28-Ma,'-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpart, N.Y. 0703179-02A Client Sample ID: Tag Number: Collection Date: Matrix: No. 9 3/21/2007 10:16:00 AM LIQUID MERCURY MercuP~ TARGET ANALYTE LIST METALS Antimony Arsenic Barium Beryllium Cadmium Calcium Cobalt Copper iron Lead Nickel Selenium Sodium Thallium Vanadium Zinc SEMIVOLATILE SW-846 METHOD 8270 1,2,4-Tfiuhlombenzene 1,2-Dichlombenzone 1,3-DIchlombenzene 1,4-Dichlombenzene 2,4,5-Tfichlorophe hal 2,4,6-Trfchlorophenol 2,4-Dichlorophenol 2,4-Dirnethylphenol 2,4-Din[tmphenol 2, 4-Dlnitrotaluene 2,6-Dinit;otoluene 2-Chloronaphthalena 2-Chlomphennl Result Limit Qual Units SW7470A U 0.000200 mg/L SW6010B SW3010A 245 0,0200 mg/L U 0.0250 mg/L 0.149 0.0250 mg/L 1.99 0.0200 mg/L U 0.0200 mglL 0.0233 0.0100 mg/L 40.6 0.0250 mglL 1.10 0.0200 mg/L U 0.0200 mg/L 0.g96 0.0200 mg/L 416 0.200 mgR. 1.12 0.0150 mg/L 69.7 0.0200 mg/L 8.20 0.0200 mgR. 0.895 0.0200 mg/L 66,7 0.100 mgR. U 0.0250 mg/L U 0.0200 mglL 31.6 0.0300 mg/L 0.0518 0.0150 mg/L 0.663 0.0200 mg/L 1.66 0,0200 mglL SW82700 SW3510 U 5.7 pg/L U 5.7 pg/L U 5.7 pg/L U 5.7 pglL U 5.7 pgR. U 5.7 J~g/L U 5.7 pg/L U 5.7 pg/L U 11 pg/L U 5.7 ug/L U 5.7 pglL U 5.7 pg/L U 5.7 uglL DF Date Analyzed Analyst: WN 3/23/2007 12:13:00 PM Analyst: JP 1 3/27/2007 2:04;52 PM 1 3/27/2007 2:04:52 PM I 3/27/2007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3/2712007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3127/2007 2:04:52 PM I 3/27/2007 2:04:52 PM 10 3/27/2007 2:16:52 PM 1 3/2712007 2:04:52 PM 1 3/27/2007 2:04:52 PM I 3/27/2007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3/27/2007 2:04;52 PM 1 3/27/2007 2:04:52 PM I 3/2712007 2:04:52 PM 1 3/27/2007 2:04:52 PM 1 3/27/2007 2:04:52 PM I 3/27/2007 2:04:52 PM I 3/27/2007 2:04:52 PM Analyst: RN 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42;00 PM 1 3126/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/28/2007 1:42:00 PM I 3/20/2007 1:42:00 PM I 3/26/2007 1;42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:~0 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM Qualifiers: B Annlyte detected in the associated Method Blank H Holding dmcs for prcpnrndon or analysis ~ceedcd ND Not Detected at the Reporting Limit U Indicates the compound was analyzed £or but not d~cctc Value above quantJtafion range A~aly~e detected below quantitation IimiL~ Spike Recovery outside accepted recovery limils Value exceeds M~ximum Contaminant L~vel Page 6 of 40 American Analytical Laboratories, LLC. Date: 2S-Mar-07 CLIENT: P.W. Grosser Consulting Client Sarople ID: No. 9 [GW] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-02A Tag Nurober: Collection Dale: 3/21/2007 10:16:00AM Matrix: LIQUID Analyses Result Limit Qual Units SEMIVOLATILE 8W-846 METHOD 8270 SW82700 SW35'10 2-Methyinaphthalene U 5,7 ug/L 2-Methylphenot U 5.7 IJg/L 2-Nitroaniline U 5~7 gg/L 2-Nitrophenol U 5.7 I~g/L 3,3'-Dichthrobenzidine U 5.7 !J§IL 3+4-Methylphenol U 5.7 I~glL 3-Nilmaniline U 5.7 pg/L 4,6-Dinitro-2-melhylp henol U 5.7 ~g/L 4-Bromophenyl phenyl ether U 5.7 I~glL 4-Chloro-3-methyll~henol U 5.7 IJg/L 4-Chlomaolline U 5.7 gg/L 4-Chlorophenyl phenyl ether U 5.7 gg/L 4-Nit roaniline IJ 5.7 ~g/L 4-Nitrophenol U 5.7 Acenaphthene U 5.7 gg/L Acenaphthylene U 5.7 ~Jg/L Aniline U 5.7 iJgfL Anthracene U 5.7 pg/L Azobenzene U 5.7 pg/L Benzidine U 5.7 gglL Benzo(a)anthracene U 5.7 Benzo(a)pyrene U 5.7 Benao(b)fluoronthene U 5.7 IJglL Benzo(g,h,i}per¥1ene U 5.7 pglL Benzo(k)fluaranthene U 5,7 IJgtL Benzoic acid U 5.7 pg/L Benzyl alcohol U 5.7 IJg/L Bia(2-chinroethoxylmethane U 5.7 IJg/L Bis(2-chlamethy0ether U 5.7 pglL Bis(2-chloroIsopmpyl}ether U §.7 g§/L Bia(2-ethylhexyl}phthalate U 5.7 pglL Butyl benzyl phthalate U 5.7 pg/L Carbazole U 5.7 pg/L Chrysene U 5.7 pgJL D~benzo(a,h)anlhracene U 5.7 pg/L Dibenzofuran U 5.7 Hg/L Dielhyl phthalate U 5.7 g§/L DImethyl phthalate U 5.7 pglL Dim-butyl phthalate U 5.7 pg/L DF Date Analyzed Analyst: RN 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 312612007 1:42:00 PM 1 3/26/2007 1:42:00 laM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 312612007 1:42:00 PM 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM I 3/23/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:60 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/23/2067 t:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 t:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:0D PM 1 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM I 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3/26/2007 1:42:00 PM 1 3~26~2007 1:42:00 PM 1 3/26/2007 1:42:00 PM Qualifiers: Analyte detected in the ~socinted Merited Blank H Holding times for preparation or analysis exceeded ND Not Detected at tho Reporting Limit U Indicates the compound was analyzed for but not delecte E Value above quantitaimn range J Anal)lc dctccled b¢lmv quantimtir~n limits S Spike Recovery oulsld¢ accepted recovery limits X Value exceeds Maximum Contaim~ant l.~vel Page 7 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consult~g 0703179 Moores Lane Greenpon, N.Y. 0703179-02A Client Sample ID: No. 9 [GW] Tag Number: Collection Date: 3/21/2007 10:16:00AM Matrix: LIQUID Analyses Result Limit Qual Units DF SEMIVOLATILE SW-846 METHOD 8270 ,~W82700 SW3510 Di-n-octyl phthalate U 5.7 I~g/L Fluoranthene U 5.7 t~gfL FIuorene U 5.7 IJg/L Hexachlorobenzene U 5.7 IJg/L Hexachlorobutadiene U 5.7 pglL Hexachlorocyclopentadtene U 5.7 pglL Hexachloroethane U 5.7 ,u§IL Indeno(1,2,3-c,d)pyrene U 5.7 pg/L Isophorone U 5.7 pg/L Naphthalene U 5.7 pg/L Nitrobenzene U 5.7 IJg/L N-Nitrosodimethylamine U 5.7 ~g/L N-N~tmsodl-n-pmpyiamine U 5.7 ~g/L N~litrosodiphenylamine U 5.7 pg/L Pentachlorophenol U 5.7 pg/L Phenanthrene U 5.7 pg/L Phenol U 5.7 I~g/L Pyrene U 5.7 pg/L · Pyricline U 5.7 .ug/L Sun': 2,4,6-Tdbmmophenol 67,6 22-124 %REC Sun': 2~Fluorobiphenyl 78.7 18-124 %REC Surr: 2~=[uorophenol 54.6 16-112 %REC Surr: 4-Tarphenyl-d 14 79.5 17-121 %REC Sum Nitrobenzene-d5 56.3 19-115 %REC Surf; Phenol-d6 34.6 12-102 %REC VOLATILE SW-846 METHOD 8260 SW82600 1,1,1,2-Tetmchloroethane U 1.0 ~Jg/L 1 1,1,2,2-Tetrachlomethane U 1.0 pg/L 1 1,1,2-Trtchloro-1,2,2-tdfluoroethane U 1.0 pg/L 1 1,1,2-Trichloroethane U 1.0 pg/L 1 1,1 -Dichloreethane U 1.0 pg/L 1 1,1 -Dichloroethene U 1.0 pg,'L 1,1 -Dichloropropene U 1.0 pg/L 1 1,2,3-Trichlorobenzene U 1.0 IJglL 1,2,3-Trichloropropane U 1.0 pglL 1 1,2,4,5-Tetramethylbenzene U 1.0 IJglL 1 1,2,4-THchlorobenzene U 1.0 pgtL 1 1,2,4--Trimethy[benzene U 1.0 i.lg/L 1 Date Analyzed Analyst: RN 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/2612007 1:42:00 PM 3126/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3~26~2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/2612007 1:42:00 PM 3/25/2007 1:42:00 PM 3/26/2007 1:42:00 PM 3/26/2007 1:42:00 PM Analyst: MB 3/22/2007 1:16;00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 312212007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM Qualifiers: Page 8 of 40 American Analytical Laboratories, LLC. Date: 28~Mar-O7 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 9 [GW] Lab Order: 0703179 Tag Number: Project: Montes Lane Greanport, N.Y. Collection Date: 3/21/2007 10:16:00 AM Lab ID: 0703179-02A Matrix: LIQUID Analyses Result Limit Qual Units DF VOLATILE SW-846 METHOD 8260 SW8260B 1,2-D)bromo.3-chloropropane U 1 .D pg/L 1,2-Dibromoethane U 1 .D pglL 1,2-Dich[orobenzene U 1.0 pg/L 1,2-Dichloroethane U 1.0 IJglL 1,2-Dichloropropane U 1.0 pg/L 1,3,5--Trim et hylbenzene U 1.0 pg/L 1,3-Dichlombenzene U 1.0 pg/L 1,3-dichlompmpane U 1.0 pg/L 1,4-Dichlorobenzene U 1.0 pglL 2,2-Dichlompropane U 1.0 pg/L 2-Butanone U 3.0 pg/L 2-Chlomethyl vinyl ether U 1.0 pg/L 2-Chlorotoluane U 1.0 pglL 2-Hexanone U 2.0 pg/L 2-P[opanol U 1.0 pglL 4-Chlorololuane U 1.0 pg/L 4-1sopropyltoluene U 1.0 pg/L 4-Methyl-2-penlanone U 2.0 pg/L Acetone U 2,0 pg/L Acm[ein U 1,0 pg/L Acrylonitdle U 1.0 pglL Benzene U 1 .fi p§/L Bmmobenzene U 1.0 pglL Bromechlommethane U 1.0 pg/L Bromodichlsromethane U 1.0 pglL Bmmot'or'm U 1.0 pglL Bromomethane U 1.0 pglL Carbon disulfide U 1.0 pg/L Carbon tetrachloride U 1.0 pg/L Chlombenzene U 1.0 pg/L Chlorodlfluoromethane U 1.0 pg/L Chlor~ethane U 1.D pg/L Chloroform U 1.0 pglL ChJoromethane U 1.0 pglL cis-1,2-DicMoroethene U 1.6 pglL cis-1,3-Dichlompmpene U 1 ~0 pglL Dibromochloromethane U 1.0 pglL Dibromomethane U 1.0 pg/L Dichlomdifluorom ethane U 1.0 pglL Date Analyzed Analyst: MB 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3~22/2007 1:16;00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:18:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:{30 PM 3/22J2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16;00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1;16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1;16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3122/2007 1:16:00 PM 3/22/2007 1:16:00 PM Qaaliflers: B Ana~ytc detected in thc associated Mcthod Blank 1-] Holding times for prcparation or anai~is cxcc~ded ND Not Dctcctcd at thc RepoSing Limlt U Indicates thc compound wa5 analyzed for but not detecto Page 9 of 40 American Analytical Laboratories, LLC. Date: 2S-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 9 [GW] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y, La b ID: 0703179-02A Tag Number: Collection Date: 3/21/2007 10:16:00 AM Matrix: LIQUID Analyses Result Limit Qual Units VOLATILE 8W-846 METHOD 8260 SW8260B Diisopropyl ether U 1.0 pg/L Ethanol U 1,0 ug/L Ethyl acetate U 1,0 pg/L Ethylbenzene U 1.0 pg/L Hexachlorobutadiene U 1.0 ~g/L [sopropyl ac. stale U 1.0 pg/L [sopropylbenzene U 1.0 pg/L m.p-Xytane U 2.0 pg/L Methyl ted-butyl ether U 1.0 IJglL Methylene chtadde U 1.0 pg/L n-Amy[ acetate U 1.0 pglL Naphthalene U 1.0 pg/L n-Butyl acetate U 2.0 n-Butylbenzena U 1.0 pg/L n-Propyl acetate U 1.0 pg/L n-Propylbenzene U 1.0 pglL ~-Xylene U 1,0 pg/L p-Diethylbenzene U 1.0 pg/L p-Ethyltoluene U 1.0 pg/L sec-Butylbenzene U 1.0 pg/L Styrene U 1.0 pg/L t-Butyl alcohol U 1.0 pg.n_ tert-Butylbenzene U 1.0 pg/L Telrach[oroethene U 1.0 pg/L Toluene U 1.0 pg/L trans.1,2-Dichlomethene U 1.0 pg/L trans-1,3-Dichloropropene U 1.0 pg/L Trichlomethene U 1.0 pg/L Trichlorofl uoromet ha ne U 1.0 pg/L Vinyl acetate U 1.0 I~g/L Vinyl chloride U 1.0 pg/L Sum 4-Brornofluorobenzene 101 54-134 %REC Sun: Dibrornofluoromelhane 105 52-132 %REC Sum Toluene-d8 96.6 5%127 %REC DF Date Analyzed Analyst: MB 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 l:t 6:00 PM 312212007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:06 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3122/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2067 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:$6:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2007 1:16:00 PM 3/22/2607 1:16:00 PM 6/22/2007 1:16:00 PM Qualifiers: B Analyte deteclcd in the a~so¢ialad Method Blank H Holding times for preparation or analysis exc~!eded ND Not Detected at die Reporting Limit U Indicates the compound was analyzed for but not detecte E Value nbove quantltation range J Analyte detected below quantilation limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 10 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-O7 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenpon, N.Y. 0703179-03A Client Sample ID: No. I0 [2.5-5'] Tag Number: Collection Dale: 3/21/2007 10:55:00 AM Matrix: SO1L Analyses Result Limit Qual Units MERCURY SW7471 B SW7471 B Mercu~J 1.07 0.0599 mg/Kg<lp/ 5 PERCENT MOISTURE 02216 Percent Moisture 24,8 0 wt% 1 TARGET ANALYTE LIST METALS swg01 OB SW3050A Aluminum 2530 0.517 rog/Kg-dp/ Antimony U 0.647 rog/Kg-dry Arsenic 3.48 0.647 mglKgq:lry Barium 141 0.517 rog/Kg-dp/ Beryllium U 0.517 rog/Kg-dry Cadmium 1.14 0.259 rog/Kg-dp/ Calcium 10200 0.647 mglKg-dry Chromium 17.2 0.517 mglKg-dp/ Cobalt U 0.517 rog/Kg-dp/ Copper 473 0.517 mg/Kg~ry Iron 5140 0.517 mg/Kg-dry Lead 101 0.388 rog/Kg-dp/ Magnesium 763 0,517 mg/Kgq:ip/ Manganese 111 0,517 mg/Kgq:lry Nickel 14.4 0.517 Potassium 307 2.59 mg/Kgq:lp/ Selenium U 0.647 mglKg-dp/ Silver 3.79 0.517 mg/Kg-dr~ Sodium 246 1.55 rog/Kg-dry Thalllum U 0,517 rog/Kg-dry Vanadium 6.36 0.517 mg/Kgqlry Zinc 276 0.517 mg/Kg~p/ SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3550A 1,2,4-Trichlorobenzene U 150 pglKg-dp/ 1 1,2-Dichlorel3enzene U 150 Fg/Kg-d~y 1 1,3-Dichlombenzane U 150 pg/Kg.-dp/ 1 1,4-Dichlerebenzene 410 150 pg/Kg-dp/ 1 2,4,5-Trichlorophenol U 150 lag/Kg-dp/ 1 2,4,6-Trichlorophen el U 150 lag/Kg-dp/ 1 2,4-Dichlorephenol U 150 lag/Kg-dp/ 1 2,4-Dimethylphenol U 150 lag/Kg-dp/ 1 2,4-Dinitmphenol U 150 lag/Kg-dp/ 1 2,4-Dinitrotolueno U 150 2,6-Dinitrotoluene U 150 ~g/Kg-dp/ 1 DF Date Analyzed Analyst: WN 3/27/2007 2:20:18 PM Analyst: CM 3/22/2007 Analyst: JP 3/27/2907 12:16:05 PM 3~27~2007 12:16:05 PM 3/27/2007 12:15:08 PM 3/27/2007 12:16:98 PM 3/27/2007 12:16:08 PM 3/27/2007 12:15:08 PM 3/27/2007 12:15:08 PM 3/27/2097 12:16:08 PM 3/27/2007 12:16:06 PM 3/27/2007 12:16:05 PM 3/27/2007 12:16:08 PM 3t27/2007 12:16:08 PM 3/27/2007 12:16:08 PM 3/27/2007 12:16:08 PM 3/27/2007 12:16:08 PM 3/27/2007 12:16:0B PM 3/27/2007 12:16:08 PM 3/27/2007 12:15:08 PM 3/27/2007 12:t5:08 PM 3/27/2007 12:16:08 PM 3/27/2007 12:16:08 PM 3/27/2007 12:16:08 PM Analyst: RN 312612007 3:50:00 PM 312612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/28/2007 3:50:00 PM 3128/2a07 3:50:00 PM 3/20/2007 3:50;00 PM 3/25/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50:00 PM 3/26/2007 3:50:00 PM B Analym detected in thc msociated Method Blank Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicates file compound woz analyzed for but not detecto Analyte detected below quantitation limits Spike Recovery outside accepted recovery limits Value exceeds Maximum Contaminant Level Page 11 of 40 American Analytical Laboratories, LLC. Date: 28~Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 10 [2.5-5'] La b Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab/D: 0703179-03A Tag Number: Collection Date: 3/21/2007 10:55:00 AM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3550A 2~Chloronaphthalene U 150 ~Jg/Kg-dry 2-ChlorophenoJ U 150 .ug/Kg-d~j 2-Methylnaphthalene U 150 FglKg-dry 2-Methylphenol U 150 pg/Kg-dry 2-Nitroaniline U 150 pg/Kg-th7 2-Nitmphenoi U 150 pg/Kg.d~y 3,3'-Dlchlombenzidine U 150 p6/K§~ry 3+4-Methyiphenol U 150 p6/Kg4~y 3-Nitroaniline U t50 pglKg4~y 4.6-Dinitm-2-methylphenol U 150 pg/Kg-thy 4-Bmmophenyl phenyl ether U t 50 pg/Kg-thy 4-Chlom-3-methylphenol U 150 pglKg-dry 4-Chlomaniline 520 150 pg/Kg-dry 4-Chlomphenyl phenyl ether U 150 pg/Kg-dry 4-Nltroaniliae U 150 iJglKg-dry 4-Nittopheno] U lgO pg/Kg-dp2 Acenaphthene U 150 pg/Kg-dry Acenephthylene U 150 pg/Kg-dry Aniline U 150 pg/Kg~lr? Anthracene U 150 pg/Kg~ Azobenzene U 150 pg/Kg~by BenzJdine U 150 p6/Kg-dry Benzo(a}anthracene 730 t 50 Benzo(a)pymne 750 150 pglKg-dry Benzo(b)fluoranthene 780 150 pg/Kg-d~y Benzo(g,h,i)perylene 540 t50 pglKg~lry Benzo(k)fluoranthene 550 150 pg/Kg~ Benzoic acid U 150 [Jg~g-thy Benzyl alcohol U 150 NglKg-dry gis(2-chloroet hoxy)metha ne U 150 pg/Kg~lry Bis(2-chloroethy0et her U 150 pg/Kg~y Bis(2-chlomisopropyl)et her U 150 pglKg-d~y Bi$(2-et hylhexyl}phthalate 900 150 pglKg-dry Butyl benzyl phthalate U 150 pg/Kg-d~y Carb~zole U 150 pg/Kg.dry Chrysene 930 150 pg/Kg~ry Dibenzo (a,h)anthracene U 150 pg/Kg-d~j Dibenzofuran U 150 pglKg.dry Diethyl phthalate U 150 pglKg~ry DF Date Analyzed Analyst: RN 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 312612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/2612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50:00 PM 3~26~2007 3:50:00 PM 312612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM Qualifiers: B Analyle detected in the associated Method Blank H Holding times for pmparation or analysis exceeded ND Not Detcn:ted at the Re@oaing Limit U Indicates the compound wa~ analyzed for but not delecte E Value above quantilafion range J Analytc detected below quantitation limits S Spike Re¢ove~ outside accepled tecove~ limits X Value exceeds Maximum Contaminant Level Page 12 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consult~g 0703179 Moores Lane Greenpo~, N.Y. 0703179-03A Client Sample ID: No. 10 [2.5-5'] Tag Number: Collection Date: 3/21/2007 10:55:00 AM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE 8W-846 METHOD 8270 SW82700 SW3550A Dirnethyl phthalate U 150 pg/Kg-dry DJ-n-butyl phthalate U 150 pg/Kg-dry Di-n-octyl phtharate U 150 pg/Kg-d~y Fluoranthene 880 150 IJg/Kg-dry Fluorene U 160 IlglKg-dry Hexachlorobenzene U 150 ugfKg-dry Hexachlorobutadiene U 150 [~g/Kg-dry Hexachlomcyclopentadiene U 190 pg/Kg-dfy Hexachloroethane U 150 pglKg-dry Indeno( 1,2,3-c,d)pyrene 440 150 pg/Kgq:lry Isophorone U 150 pg/Kg-dry Naphthalene U 150 pglKg-dry Nitrobenzene U 160 pg/Kgq:lry N-Nitrosodimethylamine U 150 Fg/Kg-d~j N-Nit rosodi-n-propylamine U t 50 gg/Kg-dp/ N-Nitrosodiphenylarnlne U 150 ~g/Kg-dry Pentachlarophenol U 190 pg/Kg-dry Phenanthrene 230 150 pg/Kg~ry Phenol U 150 pg/Kg-d~t Pyrene 11 O0 150 pg/Kg~lry pyddine U 150 ~Jg/Kg-dry Sum 2,4,6-Tribromophenol 64.8 22-124 %REC Sum 2-Fluorobiphenyl 63.7 27-11 g %REC Sum 2-Fluorophenol 33.5 21-123 %REC Sum 4-Terphenyl~14 64.3 26-126 %REC Sum Nitmbenzene-d5 51.2 21-118 %REC Surf: Phenol-d6 46.2 18-129 %REC VOLATILE SW-846 METHOD 8260 SW8260B 1,1,1,2-Tetrachloroethane U 6.8 gg/Kg-dry 1,1,1-Trichloroethane U 6.8 pg/Kg-dry 1,1,2,2-Tel rachloroetha ne U 6.8 pg/Kg-d~J 1,1,2-Trtchloro-I ,2,2-tHfluoroethane U 6.8 IJglKg-d~J 1,1,2~Trichloroethane U 6.B IJg/Kg-d~' 1 ,l-Dichloroethane U 6.8 pg/Kg-dpJ 1.1.Dichloroethene U 6.8 pg/Kg-dry 1,1-Dichloropropene U 6.8 pg/Kg-dry 1,2,3-Trichlorobenzena U 6.8 NglKg-dry 1,2,3-T[ichloropropane U 6.5 pglKg-dt-/ 1,2,4,5-Tetrarnet hylbenzene U 6.8 pg/Kg-dry DF Date Analyzed Analyst: RN 3/26/2067 3:50:00 PM 312612007 3:50:00 PM 312612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50;00 PM 3/26/2007 3:50:00 PM 3/25/2007 3:50.00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:5(1:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50'00 PM 3/26/2007 3:50:00 PM 312612007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50:00 PM 3/26/2007 3:50;00 PM 3/26/2007 3:50.00 PM 3~26~2007 3:50:00 PM Analyst: MB 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50.00 PM 3/22/2007 6:50:00 PM 3/22/2007 5:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM Qualifiers: B Analy~e detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at thc Reporting Limit Indicates th= compound was analyzed for but not dctccte E Value above quantitalion range J Analyle detected below quantitation limits S Spike Recovc~ outside accepted recove~ limits X Value exceeds Maximum Contaminant Level Page 13 of 40 American Analytical Laboratories, LLC. Date: 28-3~Iar-07 CLIENT: P.W. Grosser Consulting Client SamplelD: No. 10 [2.5-5'] Lab Order: 0703179 Tag Number: Project: Moores Lane Greeaport, N~Y. Collection Date: 3/21/2007 10:55:00 AM Lab ID: 0703179-03A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-846 METHOD 8260 SW82605 Analyst: MB 1,2,4-Tdchlorobnnzene U 6.5 pg/K§-dry 1 3/22/2007 6:50:00 PM 1,2,4*Tdmethylbenzene U 6.8 pglKg-dry 1 3122/2007 6:50:00 PM 1,2-Dibromo-3-chloropropane U 0.5 pglKg-dry I 3/22/2007 6:50:00 PM 1,2-Dibromoethane U 6,5 pg/Kg-d~y I 3/22/2007 6:50:00 PM 1,2-Dichlombenzene U 6.5 pg/Kg-dry 1 3/22/2007 6:50;00 PM 1,2-Dichloroethane U 6.8 pg/Kg-dry I 3/22/2007 6:50;00 PM 1,2-Dlchlorapfopane U 6.5 pg/Kg-dry 1 3/22/2007 6:50:00 PM 1,3,5-Trimethyibenzene U 5,8 pg/Kg-dry 1 3/22/2007 6:50:00 PM 1,3-Dichlorobenzene U 6.6 pglKg~ry I 3/22/2007 6:50;00 PM 1,3-dichloropmpane U 6.6 pg/Kg~ry I 3/22/2007 6:50:00 PM 1,4-Dlchlorabenzene U 6.8 pg/Kg~ry I 3/22/2007 6:50:00 PM 2,2-Dichloropropane U 6.8 ~g/Kg-dry 1 3/22/2007 6:50;00 PM 2-Butanane U 6.8 pg/Kg-d~/ 1 3/22/2007 6:50:00 PM 2-Chloreethyl vinyl ether U 6.8 pD/Kg<lry '[ 3/22/2007 6:50:00 PM 2-Chlarotoluene U 6.8 pg/Kg-dry 1 3/22/2007 6:50:00 PM 2-Hexanooe U 6.6 ug/Kg-dry I 3/22/2007 6:50:00 PM 2-Propanol U 66 pg/Kg-dry I 3/22/2007 6:50:00 PM 4-Chlorotoluene U 6.8 pg/Kg-d~j 1 3/22/2007 6:50:00 PM 4-1sopropyltoluene U 6.8 iJg/Kg~lry 1 3/22/2007 6:50:00 PM 4-Methyl-2-pentanone U 6.8 pg/Kg-dry I 3/22/2007 6:50:00 PM Acetone U 6.8 pg/Kg<h7 I 3122/2007 6:50:00 PM Acreleln U 34 pg/~g<lry I 3/22/2007 6:50:00 PM A¢~ylonitrile U 6.8 gg/Kg-dry I 3122/2007 6:50:00 PM Benzene U 6.8 pg/Kg-clry 1 3t22/2007 6:50:00 PM Bromebenzene U 6.6 !~g/Kg~ry 1 3/22/2007 6:50:00 PM Bromachleromethane U 6.8 pg/Kg-dry I 3/22/2007 6:50:00 PM Bromodichloromethane U 6.8 pg/l<g-d~ 1 3/22/2007 6:50:00 PM Bromoform U 6.8 pg/Kg~ry I 3/22/2007 6:50;00 PM Bromomathane U 5.5 pg/~g~lry I 3122/2007 6:50:00 PM Carbon disulfide U 5,8 pg/Kg-dry I 3/22/2007 6:50:00 PM Carbon tetmchloride U 8.8 pg/Kg-dry I 3/22/2D07 5:50:00 PM Chlombenzene U 6.8 pg/Kg-dry 1 3/22/2007 6:50:00 PM Chlomdifluoromethane U 6.8 pg/Kg~ry I 3/22/2007 6:50:00 PM Chioroethane U 6.8 pg/Kg-dry 1 3/22/2007 6:50:00 PM Chloroform U 6.8 gg/Kg-dry 1 312212007 6:50:00 PM Chlommethane U 8.8 pg/Kg-dry I 3/22/2007 6:50:00 PM cis-l,2-Dichloroethene U 6.8 Fg/Kg-dry 1 3/22/2007 6:50:00 PM cis-l,3-Dichloropropeae U 8.5 ~Jg/Kg-dry 1 3/22/2007 6:50:00 PM Dibromochloromethaae U 6.8 fig/Kg-dry 1 3/22/2007 6:50:00 PM Qualifiers: B Anal}ts dctected in the associalcd Method Blank H Holding times t'ur preparation or a~alysis exceeded ND Not Detected at tho Reporting Limit U ladicates Ihe compound was analyzed for but not detects Value above quamitation range Anal}lc detected below quanthation limits Spike RecoveR, outside accepted recovery limits Page 14 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpo~,N.Y. 0703179-03A Client Sample ID: No. I0 [2.5-5'] Tag Number: Collection Date: 3/21/2007 10:55:00 AM Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-846 METHOD 8260 SW82606 Dibromamethane U 6,8 ~Jg/Kg.dry Dichlomdifluorometha ne U 6~8 pg/Kg-dty Diisopropyl ether U 6.8 IJg/Kg-dry Ethanol U 34 pglKg-d~y Ethyl acetate U 6.8 P9/Kg-dry Ethylhenzene U 6.8 pg/Kg-dry Fmon-1 t4 U 6.8 pg/Kgq:iry Hexachlorobutadiene U 6.8 pg/Kg-dry lsopropyl acetate U 6,8 IJg/Kg<lry Isopropylbenzene U 6.8 ~glKg-dry m,p-Xylene U 14 Methyl ter[-bu¥ ether U 6.8 pg/Kg-dry Methylene chloride U 6.8 pg/Kg-d~ n-Amyl acetale U 6.8 pg/Kg-dry Naphthalene U 6.6 IJglKgq:hy ri.Butyl acetate U 6.8 pglKgq:i~ n-Butylber~zene U 6.8 pg/Kgq:il'y n-Propyl acetate U 6.8 pglKg-dry n-Propylbenzene U 6.8 pg/Kg-dry o-Xylene U 8.8 I~g/Kgq:l~ p-Diethylbenzene U 6.8 pg/Kg-th¥ p-Ethyltoluene U 6.8 pglKg-dry sec-Butylbenzene U 6.6 pg/Kg~y Styrene U 6.8 IJg/Kg-d~y t. Butyl alcohol U 6.8 pg/Kg-dry tert-Butylbenzeae U 6.8 pglKg~ry Tetrachlomethene U 6.5 ~g/Kg<lly Tolueoe U 6.6 Hg/Kg-dry trans-1,2-Dichloroethene U 6,6 IJglKg-dry trans-1,3-Dichloropropene U 6.8 IJg/Kg-dry Tfichloroethene U 6.8 pg/Kg-d~ Trichlorofl oo romethane U 6.8 IJglKg-dB' Vinyl acetate U 6.8 pg/Kg-dp7 Vinyl chloride U 6.8 pg/Kg4~y Surf: 4-Bromofluorobenzene 85.7 61-133 %REC Sum Dibmmofluoromethane 107 61-139 %REC Sum Toluene-d8 94.2 57-131 %REC Analyst: MB 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2067 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:60:00 PM 3/22/2607 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2067 6:50:00 PM 3FZ2/2007 5:50:09 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 5:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 5:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 5:50:00 PM 3/22/2007 6:50:00 PM 3/'22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2067 6:50:00 PM 3/22/2007 6:50:00 PM 3/2272007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM 3/22/2007 6:50:00 PM Qualifiers: Analyle detected in the associated Method Blank Holding timcs for preparation or analysis exceeded ND Not Detected at thc Rcponing Limit U Indicates thc compound was analyzed for but not detectc E Value gbove quanfitation range J Analyte detected below quantitetlon limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 15 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 10 [GW] Lab Order: 0703179 Project: Moores Lone Greenport, N.Y. Lab 1D: 0703179-04A Tag Number: Collection Date: Matrix: 3/2_1/2007 12:17:00 PM LIQUID Analyses MERCURY Mercury TARGET ANALYTE LIST METALS Aluminum Antiroony Arsenic Bariuro Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel Potassiuro Selenium Silver Sodium ?ha[lium Vanadium Zinc SEMIVOLATILE SW-846 METHOD 8270 1,2,4-Triehlorobenzene 1,2-Dichlorobenzene 1,3*-Diahlorobenzene 1,4-Dichlorobenzene 2,4,5-Tfichlorophenol 2,4,6-Tdchlorophenol 2,4-Dichlorophenol 2,4-Dimathylphenol 2,4-Dinitrophenol 2,4-Dinitrotolueoe 2,6-Dinitrotoluene 2-Chloronaphthalene 2-ChlorophenoJ Result Limit Qual Units DF SW7470A 0.00738 0.000200 mg/L t SW60'IOB SW3010A 957 0.200 rnglL 10 U 0.0250 mg/L 1 0.237 0.0250 rog/L 1 6,98 0.0200 rog/L 1 U 0.0200 mg/L 0.0208 0.0100 rog/l_ 1 83.7 0,0250 rog/L 1 1.53 0.0200 mg/L 1 U 0.0200 mglL 1 3.27 0.0200 rog/L 1 737 0.200 mglL 10 1.27 0.0150 mg/L 1 175 0.0200 rog/L 1 11,4 0.0200 mglL 1 1.18 0.0200 rng/L 1 145 0.100 mgiL 1 U 0.0250 mg/L 1 0.0702 0~0200 mg/L 1 39.4 0,0300 mg/L 1 U 0.0150 mg/L 1 1.84 0.0200 mg/L 1 4.83 0.0200 mg/L 1 SW8270D SW3510 U 5.6 pg/L 1 U 5.6 pg/L 1 U 5.6 pg/L 1 U 5.6 pglL 1 U 5.6 I~glL 1 U 5.6 pglL 1 U 5.6 tJg/[. 1 U 5.6 pg/L 1 U 11 gg/L 1 U 5.6 pg/L 1 U 5.6 IJg/L 1 U 5.6 pglL 1 U 5.6 pgtL 1 Date Analyzed Analyst: WN 6/27/2007 12:10:11 PM Analyst: JP 3/27/2007 2:19:24 PM 3/27/2007 2:07:01 PM 312712007 2:07:01 PM 3127/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/2712007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:19:24 PM 3/27/2007 2:07:01 PM 3/2712007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/27/2007 2:07:01 PM 3/2712007 2:07:01 PM 3127/2007 2;07:01 PM Analyst: RN 3/26/2007 2:12:00 PM 3126/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/23/2007 2:12:00 PM 3/20/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM QualiJicrs: B Analyte detected in 0to associated Method Blank H Holding times for preparation or analysis cxcccdcd ND Not Detected at thc Reporting Limit U Indicates thc compound was analyzed for but not detecto E Value nbove qmmtitadon range J Analyte detected below quantitatioa limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 16 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CL1ENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpor[N.Y. 0703179-04A Client Sample ID: No. 10 [GW] Tag Number: Collection Date: 3/21/2007 12:17:00 PM Matrix: LIQUID Analyses Result Limit Qual Units SEMIVOI_ATILE SW-846 METHOD 8270 SW82700 SW3510 2-Methylnaphthalene U 5.6 pg/L 2-Methylphenol U 5.6 pg/L 2-Nitmaniline U 5.6 pg/L 2-Nitrophenol U 5.6 Hg/L 3,3 '-Dichlorobe nzidine U 5.6 pg/L 3+4-Melhylphenol U 5.6 pg/L 3-Nitroaniline U 5.6 pg/L 4,6-Dinltro-2-met hylph en ol U 5.6 IJg/L 4-Bromophenyl phenyl ether U 5.6 pglL 4-C hloro-3-methylphenol U 5.6 pglL 4-Chloroaniline U 5.6 pg/L 4-Chlomphenyl phenyl ether U 5.6 ~Jg/L 4-Nitroaniline U 5.6 4-Nitrophenol U 5.6 pg/L Acenaphthene U 5.6 Acenaphthy[ene U 5.6 lJglL Aniline U 5.6 pg/L Anthracene U 6.6 I~glL Azohenzene U 5.6 ug/L BenzldJne U 5.6 ug/L [lenzo(a)anthracene U 5.8 pg/L Benzo(a)pyrene U 5.6 pgtL Benzo(b)fluoranthene U 5.6 uglL aenzo(g,h,i)pe~jlene U 5.6 IJglL Benzo(k)fluomnthene U 5.0 pglL Benzoic acid U 5.6 HglL Benzyl alcohol U 5.6 pg/L Bis(2-chloroethoxy) methane U 5.6 pg/L Bis(2-chloroethyl)ether U 5.6 ~Jg/L Bis(2-chloroisopropyl)ether U 5.6 uglL Bis(2-ethylhexyl)pht halate U 5.6 I~glL Butyl benzyl phthelate U 5.6 Carbazole U 5.6 pg/L Chrysene U 5.6 ug/L Dibenzo(a,h)a nlhracene U 5.6 Ilg/L Dibenzoruran U 5.6 FglL Diethyl phthalate U 5.6 lugtl_ Dimethyl phthalate U 5.6 FglL Dim-butyl phthalate U 5.6 pg/L DF Date Analyzed Analyst: RN 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2607 2:12:00 PM 3~26~2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/2612007 2:12:00 PM 3/2612007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/25/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/2612007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:60 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/2612007 2:12:00 PM 3/26/2007 2:12:00 PM 3/2012007 2:12:00 PM 3/2612007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3~26~2007 2:12:00 PM 3~26~2007 2;12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/20/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM Qualifiers: B Analyte detected in thc associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indlaatcs the compound was analyzed for lint not detente ValLe above quantitation range Analyte detected below quantitation limits Spike Recov¢D' outside ncccpted recover' limits Value exceeds Maximum Contaminant Level Page 17 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: La b ID: P.W. Grosser Consulting 0703179 Moores Lane Greenport, N.Y. 0703179-04A Client Sample ID: Tag Number: Collection Date: Matrix: No. 10 [GW] 3/21/2007 12:17:00 PM LIQUID Analyses Result Limit Qual SEMIVOLATILE SW-846 METHOD 8270 SW8270D DLn-octyl phlhalate U 5.5 Fluoranthene U 5.5 Fluomne U 5.6 Hexachlorobanzene U 5.6 Hexachlorobuladiena U 5.6 Hexachlorocyclope nt adiene U 5.6 Hexachloroethane U 5.6 Indeno(1,2,3-c,d)pyrene U 5.6 Isophorone U 5.6 Naphthalene U 5.6 Nitrobenzene U 5.6 N-Nitrosodirnet hylarnine U 5.6 N-Nitresodi-n-propylamine U 5.6 N-Nitmsodiphenylamine U 5.6 Pentachlorophenol U 5.6 Phenanthrene U 5.6 Phenol U 5.6 Pyrene U 5.6 Pyddine U 5.6 Sum, 2,4,6-Ttibmmophenol 60.8 22.124 Sum 2-Fluomb[phenyl 63.1 18-124 Surr; 2-Fluorophenol 49.9 15-112 Sum. 4-Teqohenyl-d14 60.0 17-121 Sum. Nitrobenzene-d5 59.7 19-115 Sum Phenol-d6 31.8 12-102 VOLATILE SW-846 METHOD 8260 SW8260B 1,1,1,2-Tetrachloroethane U 1.0 1,1,2,2-Tetrachlomethane U 1.0 1,1,2-Trichloro-I ,2,2-trifluoroethane U 1.0 1,1,2-Tdchlomethane U 1.0 1,1 -Dichloroethane U 1,0 1,1-Dichlomethene U 1.0 1,1-Dichloropmpene U 1.0 t ,2,3-Tdchlorobenzene U 1.0 1,2,3-Trichloroprapane U 1.0 1,2,4,5-Tetramethylbenzene U 'i.0 1,2,4-Ttichlorobenzsne U 1.0 1,2,4-Trimethylbenzene U 1.0 Uni~ SW3510 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg,'L 1 pg/L 1 pg/L 1 pglL 1 pg/L 1 pg/L 1 pg/L I pg/L 1 pglL 1 pglL 1 1 pg/L DF Date Analyzed Analyst: RN 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:013 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM 3/26/2007 2:12:00 PM Analysl: MB 3/22/2007 2;04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04;00 PM 3/22/2007 2:04:00 PM 3/22/2007 2;04:00 PM 3/22/2007 2;04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3~22~2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM Qualifiers: B Analyte detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at the Reporting Limit U lodlcatm the compound was analyzed for hut not detecte Valuc above quantilation range Analyte detected below quantitation limits Spike Recovery outside acccpted rccovco, limiLs Value exceeds Maximum Contaminant L~vcl Page 18 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. 10 [GW] Lab Order: 0703179 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/21/2007 12:17:00 PM Lab ID: 0703179-04A Matrix: LIQUID Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-846 METHOD 8260 SW8260B 1,2-Dihmme-3..chlompmpane U 1.0 pg/L 1,2-Dibromeethane U 1 .fl pg/L 1,2-Dichlombenzene U 1.0 pg/L 1,2-Dichloroethane U 1.0 pg/L 1,2-Dichloropropane U 1.0 ~Jg/L 1,3,5-Trimet by[benzene U 1.0 pg& 1,3-Dichlorobenzene U t .0 pg/L 1,3-dichleropmpane U 1.0 pg/L 1,4-Diehlorobenzene U 1.0 pg/L 2,2-Dichloropropane U 1.0 pg/L 2-Butermne U 3.0 pg/L 2-Chloroethyl vinyl ether U 1.0 pgtl_ 2-Chlorotoluene U 1.0 pg/L 2-Hexanone U 2.0 pg/L 2-Pmpanol U 1.0 pglL 4-Chlorotoluene U 1.0 IJglL 4qsopmpylloluene U 1.0 pglL 4-Methyl-2-pentanene U 2.0 pg/L Acetone U 2.0 pglL Acrolein U 1.0 pg/L Acrylonitrile U 1 .O pglL Benzene U 1.0 IJglL Bromobenzene U 1.0 pglL Bromoehloromethane U 1.0 pg/L Bmmedichleromethene U 1.0 pg/L Bromoform U 1.0 pglL Bromomethane U 1.0 ~glL Cerbon disulfide U 1.0 IJg/L Carbon tetrachlodde U 1.0 pg/L Chlombenzene U 1.0 I~g/L Chlorodifluommethane U 1.0 pg/L Chloreethane U 1.0 pg/L Chloroform U 1.0 pg/L Chloromethane U 1.0 pg/L cis-1,2-Dichloroethene U 1.0 pg/L cis-1,3-Dichloropropene U 1.0 I~glL Dibromochloromethane U 1.0 pg/L DibromDmethane U 1.0 I~glL Dichlorodiflu oromethane U 1.0 I~g/L Analyst: MB 3/22/2007 2:04:00 PM 3/2212007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:01] PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM '3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2;04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/21107 2:04:00 PM 3/22/2007 2:04:00 PM 3/2212007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04;00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04;00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2;04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM Qualifiers: B Analytc detected in thc associated Mc~od Blank Holding times for preparation or analysis exceeded ND Not Datcctcd at thc Reporting Limit U Indicates thc compound was analyzed for but not delecte E Value above quantitntion range J Analyle detected belmv quantitation limits S Spike Rccove~ ou~idc accepted recover, limit~ X Value exceeds M~ximum Contanlitlarll Level Page 19 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 10 [GW] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-04A Tag Number: Collection Date: Matrix: 3~ 1/2007 12:17:00 PM LIQUID Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82688 Diisopropyl ether U 1.0 Ethanol U 1.0 Ethyl acetate U 1.0 Ethylbenzene U 1.0 Fmon-114 U 1.0 Hexachlorebutadiene U 1,0 Isopmpyl acetate U 1.0 Iscpropylbenzene U 1.0 m,p-Xylene U 2.0 Methyl tart-butyl ether U 1.0 Methylene chloride U 1,0 n-Amyl acetate U 1.0 Naphthalene U 1.0 n-Butyl acetate U 2.0 n-Butylbenzene U 1.0 n-propyl acetate U 1.0 n-Pmpylbenzene U 1.0 o-Xylene U 1.0 p-Diethylbanzene U 1.0 p-Ethyltoluene U 1 .o sec-Butylbenzene U 1.0 Styrene U 1.0 t-Butyl alcohol U 1.0 tert-Butylbenzene U 1.0 Tetrachleroethene U 1.0 Toluene U 1,0 lrans-1,2-Dichlorcethene U 1.0 trans-1,3-Dichlompropene U 1.0 Trich[oroethane U 1.0 Trichlorofluoromethane U 1.0 Vinyl acetate U 1.0 Vinyl chloride U 1.0 Sum 4-Bromollucrobenzene 94.9 54-134 Sum Dibrnmofluoromethane 100 52-132 Surf. Toluene-d8 98.1 51-127 Units DF Date Analyzed pg/L pg/L ug/L pg/L pg/L pg/L pg/L pglL ~Jg/L pglL pg/L pg/L 1 pg/L 1 pglL 1 pgtL 1 pg/L 1 pg/L 1 pglL 1 pglL 1 pg/L 1 pg/L pg/L 1 pg/L 1 pglL 1 pglL I Analyst: MB 3/22/2007 2:04:00 PM 3/22/2007 2;04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22~007 2:04:00 PM 3/22/2087 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2097 2:04:00 PM 3/22.,2007 2:04:00 PM 3/23/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3f22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:D0 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:80 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/200? 2:04;00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM 3/22/2007 2:04:00 PM Qualifiers: B A~aly~e dctcclcd in the associated Method Blank H Holding times for preparation or analysis cxcccdcd ND Not Dc~cclcd at thc Reposing Limil U tadicnles the compound w0s m~alyzcd for but not. dclccte Page 20 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Greaser Consulting Client Sample ID: La b Order: 0703179 Tag Number: Project: Madras Lane Greeaport, N.Y. Collection Date: Lab ID: 0703179-05A Matrix: No. 7 [12.5-15'] 3/21/2007 1:35:0~] PM Sell Analyses Result Limit Qual Units MERCURY SW7471 B SW74710 Memury U 0.00893 rag/Kg-dry PERCENT MOISTURE O2216 Percent Moisture 2.57 0 wt% TARGET ANALYTE LIST METALS SW6010B SW3050A Aluminum 1760 0.401 rog/Kg-dry Antimony U 0.501 rog/Kg.dry Arsenic Z21 0.501 mc/Kg-dry Barium 15.0 0.404 rag/Kg-dry Beryllium U 0.401 rog/Kg-dry Cadmium U 0.200 mc/Kg.dry Calcium 262 0.501 rog/Kg-dry Chromium 9.11 0.40t rag/Kg-dry Caball U 0.401 mc/Kg-dry Copper 5.55 0.401 mc/Kg.dry Iron 3610 0.401 mg/Kg-d~y Lead 11.0 0.301 mg/Kg-dry Magnesium 589 0.401 mc/Kg-dry Manganese 92.0 0,401 mc/Kg-dry Nickel 3.14 0.401 mglKg-dry Potassium 456 2.00 mc/Kg-dry Selenium U 0.501 rog/Kg-dry Silver U 0.401 mc/Kg-dry Sodium 62.1 1.20 mc/Kg-dr7 Thallium U 0.401 mc/Kg-dry Vanadium 7.04 0.401 mg/Kg-dry Zinc 8.50 0.401 rog/Kg-dry SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW35S0A 1,2,4-Tfichiarobenzen e U 120 pg/Kg-dry 1,2-Dichlombenzene U 120 pg/Kg<lry 1,3-Dichlorobenzene U 120 pglKg-dry 1,4-Dichlorobenzene U 120 IJglKg-d~y 2,4,5-Trichlorophenel U 120 I~glKg.qtry 2,4,6-Tdchlorophenol U 120 NglKg-dry 2,4-Dichlarophenol U 120 pg/Kg-clry 2,4-DlmethyDhenel U 120 pc/Kg-dry 2,4-Dinitmphenol U 120 pc/Kg.dry 2,4-Dinitmtoluene U 120 pc/Kg-dry 2,6-Dinitrololuene U 120 ~Jg/Kg-dry DF Date Analyzed Analyst: WN 312712007 12:38:45 PM Analyst: CM 3/22/2007 Analyst: Jp 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 312712007 12:20:14 PM 3/27/2007 12:20:14 PM 3/2712007 12:20:14 PM 3/27/2007 12:20:14 PM 3127/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3~27~2007 12:20:14 PM 3/2712007 12:20:14 PM 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3/27/2067 12:20:14 PM 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3~27~2007 12:20:14 PM 3/27/2007 12:20;14 PM 3/27/2007 12:20:14 PM 3/27/2007 12:20:14 PM 3/2712007 12:20:14 PM Analyst: RN 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:16:00 PM 3/26/2007 4:15:00 PM 3/23/2007 4:15:00 PM 3/2612007 4:t5:00 PM 3/26/2007 4:15:00 PM 3126/2007 4:15:00 PM 3/26/2007 4:15:00 PM Qualifiers: 0 Analy~e detected in the associaled Method Blank H Holding times for preparation or analysis exceeded ND Not Dctecled at the Reporting Limit U Indicates the compound w~ analyzed for but not detect* E Value above qannfitation r0nge J Analyte dctectcd balow quamitation limits S Spike Rccovc~ outside accepted recovery limits X Value exceeds M~ximum Contaminant Level Page 21 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. 7 [12.5-15'] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-05A Tag Number: Collection Date: 3/21/2007 l:35:00PM Matrix: SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3$$0A 2-CMoronaphthalene U 120 pg/Kg-dry 1 2-Chlorophenol U 120 gg/Kg-dry 1 2-Methylnaphthalene U 120 pglKg-dpj 1 2-Methylphenol U 120 IJglKg-dry 1 2-NItroanillne U 120 pg/Kg.dry 1 2-N~tmphenol U 120 pg/Kg-dry 1 3,3'-Dichlorobenzldine U 120 pg/Kg-dry 1 3+4-Methylphenol U 120 pglKg~ry 1 3-Nitroanittne U 120 p§/Kg-dr~ 1 4,6-Dinitro-2-m ethylphenol U 120 pg/Kg-dry 1 4-Bromophenyl phenyl ether U 120 pg/Kg~i~j 1 4-Chloro-3-methylphen al U 120 pg/Kg~l~j I 4-Chloroanilthe U 120 p§lKg-dry 1 4-Chlorophenyl phenyl ether U 120 pg/Kg-dry 1 4-Nitmaniline U 120 pg/Kg-dry 1 4-Nitrophenol U 140 Fg/Kg-d[y 1 Acenaphthene U 120 I~glKg-d~y I Acenaphthylene U 120 IJglKg-d[y I Aniline U 120 pg/Kg~ry 1 Anthracene U 120 iJg/Kg-dry 1 Azobenzene U 120 pg/Kg.dry 1 Benzidine U 120 pglKg-dpJ 1 Benzo(a)anthracene U 120 pg/Kg-dpj 1 Benzo(a)pyrene U 120 lJg/Kg.dry 1 Banzo(b)fluoranthene U 120 ~Jg/Kg-dry 1 Benzo(g,hj)perylene U 120 pg/Kg-dry 1 Benzo(k)fluoranthene U 120 pg/Kg.dry Benzoic acid U 120 ~Jg/Kg-d ~J 1 Benzyl alcohol U 120 pglKg-dry 1 Bis(2-chlomethoxy)meihane U 120 IJg/Kg~l~ 1 Bis(2-chloroethyl)ether U 120 Fg/Kg-dG, 1 Bis(2-chloroisopropyl)ether U 120 ug/Kg~lpJ 1 Bis(2-eihylhexyl)phthalat e U 120 pg/Kg-dry 1 Butyl benzyl phthalate U 120 IJg/Kg-dry Carbazole U 120 pg/Kg-dry 1 Ch~'sene U 120 pg/Kg~iry 1 Dibenzo(a,h)anthtacene U 120 pg/Kg.dry 1 Dibenzofuran U 120 I~g/Kg-d~j 1 Diethyl phthalate U 120 Fg/Kg-dr~ 1 DF Date Analyzed Analysl: RN 3126/2007 4:15:00 PM 3/25/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/2612007 4:15:00 PM 312612007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/2612007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/2612007 4:15:00 PM 3/26/2007 4:15:o0 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/25/2007 4:15:00 PM 3/26/2007 4:15:o0 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 312612007 4:15:o0 PM 3/26/2007 4:15:00 PM 3/26/2007 4:t5;00 PM 3126/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM 3/26/2007 4:15:00 PM Qualifiers*. Analyic dctcctcd in thc associated Method Blank H Holding time's for preparation or analysis ~:ccedcd ND Not l~tectcd at thc Reporting Limit U Indicates the compound was analyzed for but not detecto Page 22 0£40 American Analytical Laboratories, LLC. Date: 2S-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenport, N.Y. 0703179-05A Client Sample ID: Tag Number: Collection Date: Matrix: No. 7 [1-~.5-15'1 3/21/2007 1:35:00 PM SOIL Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 Dimethyl phthalate U 120 Di-n Jautyl phthalate U 120 Di-n-oclyl phthalate U 120 Fluoranthene U 120 Fluorene U 120 Hexachlorobenzene U 120 Hexachlorobutadiene U 120 Hexachlorocyc[opent adiene U 140 Hexachloroethane U 120 Indeno(1,2,3-c,d}pyrene U 120 ]sophorone U 120 Naphthalene U 120 Nitrobenzene U 120 N-Nitrosodimethylamine U 120 N-Nitrosodi-n4)mpyls mine U 120 N-Nit rosodiphenylamlne U 120 Pentachlorophenol U 140 Phenanthrene U 120 Phenol U 120 Pyrene U 120 Pyrldtee U 120 Sun': 2,4,6-Tribromophenol 52.7 22-124 S urr: 2-Fluombiphenyl 71.6 27-119 Surr: 2-Fluorophenol 34.7 21-123 Sum, 4-Terphenyl-d14 71.8 28-126 -Surr. Nitmbenzene-d5 60.9 21-118 Sun':. Phenol-d6 49.5 18-129 VOLATILE SW-846 METHOD 8260 SW6260B 1,1,1,2-Tetrachloroethane U 4.5 1,1, I -Tfichloroethane U 4.0 1,1,2,2-Tetrachlorostha ne U 4.9 1,1,2-Tdchlom-l,2,2-tdfluoroethane U 4.9 1,1,2-Tdchloroethane U 4.9 1,1 -Dichlomethane U 4.9 1,1-Dichlnroethene U 4.9 1,1-Dichloropropone U 4.9 1,2,3-Trichlombenzene U 4.9 1,2,3-Ttichloropropane U 4.9 1,2,4,5-Tot ramethylbenzene U 4.9 DF Date Analyzed SW3550A Analyst: RN IJg/Kg-dry 1 3/26/2007 4:t 5:00 PM IJg/Kg-dry 1 3/26/2007 4:15:00 PM ~g/Kg-dty I 312612007 4:15:00 PM I~g/Kg-dry I 3/26/2007 4:15:00 PM pg/Kg-dty 1 3/26/2007 4:15:00 PM ~g/Kg-d~y 1 3/26/2007 4:15:00 PM ~g/Kg-dry 1 3/26/2007 4:15:00 PM pg/Kg-dry I 3/26/2007 4:15:00 PM pg/Kg.-dry I 3/26/2007 4:15:00 PM pg/Kg.Jry 1 3/26/2007 4:15:00 PM IJg/Kg~Jry I 3/25/2507 4:15:00 PM pg/Kg-dty 1 3/26/2007 4:15:00 PM pglKg-dry 1 3/2612007 4:15:00 PM IJg/Kg-dry I 3/26/2007 4:15:00 PM pg/Kg-dry I 3/26/2007 4:15;00 PM pglKg-d~j I 3/26/2007 4:15:00 PM pglKg-dry 1 3/26/2007 4:15:00 PM pg/Kg-dry I 3/26/2007 4:15:00 PM pg/Kg~ry I 3/26/2007 4:15:00 PM IJg/Kg-dry I 3/26/2007 4;t5:00 PM pg/Kg-dry 1 3/26/2007 4:15:00 PM %REC 1 3/26/2007 4:15:00 PM %REC 1 3/26/2007 4:15:00 PM %REC I 3/26/2507 4:15:00 PM %REC I 3/26/2007 4:15:00 PM %REC 1 3/26/2007 4:15:00 PM %REC 1 3/26/2007 4:15:00 PM Analyst: MB pg/Kg-d~y 1 3/22/2007 7:37:00 PM pg/Kg-dry I 3/22/2007 7:37:00 PM pg/Kg-di'y 1 3/22/2007 7:37:00 PM pg/Kg--dry I 3/22/2007 7:37:00 PM pglKg-dry I 3/22/2007 7:37:00 PM pg/Kg-dry I 3/22/2007 7;37:00 PM Hg/Kg-dry 1 3/22/2007 7:37:00 PM IJg/Kg.<hy I 3/22/2007 7:37:00 PM ~JglKg~pJ I 3/22/2007 7:37:00 PM pg/Kg,.dP/ I 3122/2007 7:37:00 PM pg/Kg..d~, 1 3/22/2007 7:37:00 PM Qualifiers: B Analyte det~cled in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at thc Reponin§ Limit U Indicates thc compound was ~nalyzed for but not detecte Page 23 of 40 American Analytical Laboratories, LLC. Date: 28-Ma,'-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenpo~,N.Y. 0703179-05A Client SampleID: No. 7 [12.5-15'] Tag Number: ColleetionDate: 3/21/2007 l:35:00PM Matrix: SOIL Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82600 1,2,4-Tdchlombenzene U 4,0 1,2,4-Trimethylbenzene U 4.9 1,2-Dibmmo-3.chloropmpane U 4.9 1,2-Dibromoethane U 4.9 1,2-Dichlombenzene U 4.9 1,2-Dichlomsthane U 4.9 1,2-DIchloropropane U 4.9 1,3,5-Trknethylbunzene U 4.9 1,3-Dichlorobenzene U 4.9 1,3-dichloropmpane U 4.9 1,4-Dichlombenzene U 4.9 2,2..Dichloropropane U 4.9 2-Butanone U 4.9 2-Chloroethyl vinyl ether U 4.9 2-Chloroioluene U 4.9 2-Hexanone L! 4.9 2-Propanol U 49 44~hlorotoluene U 4.9 4-1sopropyltoluene U 4.9 4-Methyl-2-pentanone U 4.0 Acetone U 4.9 Acrolein U 24 Acrylonitrile U 4.9 Benzene U Bromobenzene U 4.9 Bmmochloromethane U 4.9 Bromodlchloromethane U 4.9 Bromoform U 4.9 Bromomethane U 4.9 Carbon disulfide U 4.9 Carbon tetrachlor~de U 4.0 Chlorobenzene U 4.9 Chlorodifluoromethane U 4.0 Chloroethane U 4.9 Chloroform U 4.9 Chloromethane U 4.9 cts-1,2-Dicfllomethene U 4.9 cis-1,3q3[chloropropene U 4.9 Dibromochloromethane U 4.9 Units DF Date Analyzed pg/Kg-dry pg/Kg-dry pglKg-dry IJg/Kg~P7 pg/Kg-dl7 pg/Kg-dpj pg/Kg-dry pg/Kg-dry pg/Kg-dry ~Jg/Kg,.d~ IJg/Kg..dr¥ pg~Kg-dr,J pg~(g-dry pg/Kg-dry ~g~Kg-dry pg/Kg-d~ pg~Kg-d~ pg/Kg..d~ ~g~Kg-dw pg/Kg..d~J pg~Kg-d~ pg/Kg-dPJ pg/Kg-d~ pglKg-dry ~gfKg-d~J tJglKg..dry pglKg..d~j pg/Kg-ciPj pg/Kg~ry pglKg-d~J pg/Kg..dry pg/Kg~ry pg/Kg-dry pg/Kg..dry pglKg~ry ~g/Kg-dry pg/Kg.dry Analyst: MB 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/2PJ2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3122/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7;37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7;37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM Analylc detected in thc ~ociatcd IVlelhod Blank H Holding times/'or preparation or anal)sis exceeded ND Not Detected at the Reporting Limit U Indicates the compound was analyzed for but not detects Value above quantitation range Analyle detected below quantitation limits Spike Recov¢[y outside accepted recovery limits Value exceeds Maximum Contaminant Lgvcl Page 24 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Grcenport, N.Y. 0703179-05^ Client Sample ID: No. 7 [12.5-15'] TagNumber: Collection Date: 3/21/2007 I:35:00PM Matrix: SOIL Analyses Result Limit Qual Units VOLATILE SW-846 METHOD 8260 SW8260B Dibromomethene U 4.9 tJglKg-dry Dichlorodifluoromethane U 4.9 ug/Kg-dry Diisopropyl ether U 4.9 ug/Kg-dry Ethanol U 24 pg/Kg-dry Ethyl acetate U 4.9 pg/Kg-dry Ethylbenzene U 4.9 pg/Kg~ry Freon-114 U 4.9 pg/Kg-dry Hexachlorobutadiene U 4.9 pg/Kg<iry Isopropyl acetate U 4.9 pg/Kg-dry Isopropylbenzene U 4.9 IJg/Kg-dry m,p-Xylene U 9.7 pg/Kg*d~ Methyl tart-butyl ether U 4.9 ~§/Kg-dry Methylene chloride U 4.9 pg/Kg-dry n-Amyl acetate U 4.9 pg/Kg-dry Naphthalene U 4.9 pg/Kg-dry n-Butyl acetate U 4.9 pg/Kg-dry n-Butylbenzene U 4.9 pg/Kg<lry n-Propyl acetate U 4.9 n-Propylbenzene U 4.9 pg/Kg.dry o-Xylene U 4.9 pglKg-dry p-Diethylbenzene U 4.9 gglKg-dPJ p-Ethyltolueee U 4.9 Ng/Kg-dry sec-Butyltlenzene U 4.9 Ng/Kg-dry Styrene U 4.9 pg/Kg-dry t-Butyl alcohol U 4.9 pgJKg-dry tert-Butylbenzene U 4.9 pglKg-thy Tetrachlatcethene U 4.9 pg/Kg-dry Toluene U 4.9 p§/Kg-cl~j trans-1,2-Dichloroethene U 4.9 Ilg/Kg-d~ trees-1,3-Dichloropropene U 4.9 Ng/Kg-dry Trlohlomethene U 4,9 pg/Kg-dry Trichlorofluommethane U 4.9 Vinyl acetate U 4.9 gg/Kg-dqt Vinyl chledde U 4.9 pg/Kgqlry Sun. 4,-Bromofluombenzene 101 61-133 %REC Sum Dibromofluoromethane 107 61-139 %REC Sun. Toluene-d8 95.4 57-131 %REC DF Date Analyzed Analyst: MB 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2067 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37;00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37;00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM 3/22/2007 7:37:00 PM B Analytc detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not I)~tccted at the Rcponing Limit U Indicates the compound was analyzed for but not detecte E Value above qaantit arian range J Analyte detected below qanafitction limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminan[ Level Page 25 of 40 American Analytical Laboratories, LLC. Date: 28-Ma,'-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenpo~,N.Y. 0703179-06A Client Sample ID: Tag Number: Collection Date: Matrix: No. 7 [GW] 3/21/2007 1:57:00 PM LIQUID Analyses Result Limit Qual Units MERCURY SW7470A Mercury U 0.000200 mg/L TARGET ANALYTE LIST METALS SW6010B SW3010A Aluminum 143 0.0200 mg/L Antimony U 0.0250 mg/L Arsenic 0.109 0.0250 mg/L Barium 1.06 0. D260 mg/L Beryllium U 0.0200 mg/L Cadmium U 0.0100 mg/L Calcium 57.9 0.0250 mg/L Chromium 0.985 0.0200 mg/L Cobalt 0.0259 0.0200 mg/L Copper 0.635 0.0200 rog,q_ Iron 289 0.200 mg/L Lead 0.171 0.0150 mg/L Magnesium 37.2 0.0200 mglL Manganese 18.7 0.0200 mglL Nickel 0.373 0.0200 mglL Potassium 45.7 0.100 mglL Selenium U 0.0250 mg/L Silver U 0.0200 mglL Sodium 34.1 0.0300 mg/L Thallium U 0.0150 mgfL Vanadium 0.279 0.0200 mg/L Zinc 0.028 0.0200 mg/L SEMIVOLATILE SW-846 METHOD 8270 SW§2700 SW3510 1,2,4-Trichlorobenzene U 5.0 lag/L 1,2-Dichl~robenzene U 5.0 pg/L 1,3-Dichlorobenzene U 5.0 pg/L 1,4-Dichlombenzene U 5.0 pg/L 2,4,5-Tdchlorophenol U 5.0 pglL 2,4,6-Trichloroph eno[ U 5.0 pglL 2,4-Dichlorophenol U 5.0 pglL 2,4-Dimethylphenol U 5.0 pg/L 2,4-Dinitmphenol U 10 ,ug/L 2,4-Dinibotoluene U 5.0 pg/L 2,6-Dinltmtaluene U 5.0 i~g/L 2-Chloronaphthalene U 5.0 pg/L 2-Chlomphenol U 5.0 pg/L DF Date Analyzed Analyst: WN 3~23~2007 12:15:16 PM Analyst: JP 1 3/27/2007 2:09:36 PM I 3/27/2007 2:09:36 PM 1 312712007 2:09:36 PM I 3/27/2007 2:09:36 PM I 3/27/2007 2:09:39 PM I 3/27/2007 2:09:36 PM I 3/2712007 2:09:36 PM I 3~27~2007 2:09:36 PM 1 3/27/2007 2:09:36 PM 1 3/27/2007 2:09:36 PM I0 3/27/2007 2:21:31 PM 1 3/27/2007 2:09:36 PM 1 3/27/2007 2:09:36 PM 1 3/27/2007 2:09:36 PM 1 3/27/2007 2:09:36 PM I 3/27/2007 2:06:36 PM 1 3/27/2607 2:09:36 PM I 3/2712007 2:09:36 PM 1 3/27/2007 2:09:36 PM 1 3/27/2007 2:09:36 PM I 3/27/2007 2:09:36 PM I 3/27/2007 2:09:36 PM Analyst: RN 1 3/26/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM 1 3/25/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM I 3/26/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM I 3/26/2007 2:42:00 PM I 3/26/2007 2:42:00 PM I 3/26/2007 2:42:00 PM 1 3/26/2007 2:42:00 PM 1 3/2612067 2:42:00 PM Qualifiers: E Value above quantitattan range J Ana]yte detected below quamitation limits S Spike Recover, outside accepted recovery limils X Value exceeds Maximum Contaminant Level Page 26 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. G~sserConsulting 0703179 Moores Lane Greenport, N.Y. 0703179-06A Client SamplelD: No. 7 [GW] Tag Number: Collection Date: 3/21/2007 I:57:00PM Matrix: LIQUID Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLATILE SW-840 METHOD 8270 SW82708 2-Methylnaphthalene U 5.0 2-Methylphenol U 5.0 2-Nitroaniline U 5.0 2-Nitrophenol U 5.0 3,3 '-Dichrom be nzid[ne U 5.0 3+4~'lethylphe hal U 5.0 3-Nitroaniline U 5.0 4,6-DInitro-2-rnet hylph enel U 5.0 4-Bremephenyl phenyl ether U 5.0 4-Chlaro-3-methylphenol U 5.0 4-Chloroaniline U 5.0 4-Chlomphenyl phanyl ether U 4-Nitmaniline U 4-Nitmphenol U 88.0 Acenephthene U 5.0 Acenaphthylene U 5.0 Aniline U 5.0 pg/L Anthracene U 5.0 pg/L Azobenzene U 5.0 pg/L Benzidine U 5.0 Ng/L Benzo(a)anthmcene U 5.0 pglL Benzo(a)pyrene U 5.0 pglL Benze(b)fluoranthene U 5.0 pglL Benze(g,h,i)parjlene U 5.0 pglL Benzo{k}fluoranthene U 5.0 pg/L Benzoic acid U 5.0 pg/L Benzyt alcohol U 5.0 Ng/L Bis (2-chloroeth oxy)methane U 5.0 pg/L Bis{2-chlomet hyt)ether U 5.0 pglL Bis(2-chloroiscpropyl}ether U 5.0 pglL Bis(2-e[hylhexyl}phth elate U 5.0 og/L Butyl benzyl phthalate U 5.0 pglL Carbazole U 5.0 Ng/L Chrysene U 5.0 pgJL Dibenzo(a,h)ant brace ne U 5.0 pg/L Dibenzofuren U 5.0 pg/L Dlelhyl phthalate U 5.0 pg/L Dimethyl phthalate U .5.0 gg/L Di-n-butyl phthalale U 5.0 pg1L SW3510 gg/L pg/L pg/L pglL pg/L pg/L pg/l_ Ng/L pg/L pg/L pg/L pg/L pg/L pglL pg/L pg/L Analyst: RN 3t26/2007 2:42:00 PM 3/26/2007 2:42:00 PM .3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/20887 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/;[007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/2612007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:09 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3128812007 2:42:00 PM 3/26/2007 2:42:00 PM 6/26/2007 2:42:o0 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/28807 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3126/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:D0 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM Qualifiers: B Analyte detected in thc asscciut~d Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at thc Repotting Limit U Indicates the compound was analyzed f~- but not detecto E Value above quantimdon range J Analyte d~l¢¢led below quanliladon limits S Spike Recovery outside ~ceptcd recovery limits X Value exceeds Maximum Contaminant Level Page 27 of 40 American Analytical Laboratories, LLC. Date: 28-Mc.'-07 CLIENT: P.W. Grosser Consulting Client Sample ID: Lab Order: 0703179 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: Lab ID: 0703179-06A Matrix: lqo. 7 [Gw] 3/21/2007 1:57:00 PM LIQUID Analyses Result Limit Qual Units DF SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 Di-n-octyl phthalate U 5.0 ~g/L 1 Fluoranthene U 5.0 pg/L 1 Fluorene U 5.0 IJg/L t Hexachthrobenzene U 5.0 FglL 1 Hexachlombutadiene U 5.0 pg/L 1 Hexachlorocyclopentadia ne U 5.0 pg/L 1 Hexachlomelhane U 5,0 pg/L 1 Indeno(1,2,3-c,d)pyrene U 5.0 ~g/L 1 laophorone U 5.0 pg/L 1 Naphthalene U 5.0 pg/L 1 Nitmbenzene U $.0 pg/L 1 N-Nltrosadimethylamine U 5.0 Ng/L 1 N-Nitrosodi-n-propyla mine U 5.0 pg/L 1 N-NRrosodiphenylamine U 5.0 pg/L 1 Pentachlomphenol U 5.0 uglL Phenanthrene U 5.0 I~g/L 1 Phenol U 5.0 iJg/L Pyrene U 5.0 iJglL 1 Pyridine U 5.0 IJg/L 1 Surf. 2,4,6-Tdbromophenol 71.8 22-124 %REC 1 Sum 2-Fluorabiphenyl 79.2 18q24 %REC 1 Sun-: 2*Fluerophenol 53.1 16-112 %REC 1 Sure 4-Terphenyl-d14 87.5 17-121 %REC 1 Sure Nitrobenzene-d5 69.4 19-115 %REC 1 Sum Phenol-d6 33.1 12-102 %REC 1 VOLATILE SW-846 METHOD 8260 SW8260B 1,1,1,2-Tetrachloroetha ne U 1.0 I~g/L 1 1,1,2,2-Tetrachla roet hane U 1.0 tJg/L 1 1,1,2-Trichloro-1,2,2-tritluoroelhane U 1.0 IJg/L 1 1,1,2-Trichloroethane U 1.0 ~g/L 1 1,1-DIchloroethane U 1.0 pgt[ 1 1,1-Dichlomethene U 1.0 pg& 1 1,1-Dichloropropene U 1.0 Ng/L 1 1,2,3-Tdchlombenzene U 1.13 pg/L 1 1,2,3-Trichlo ropropane U 1.0 Ng/L 1 1,2,4,5-Tetramethylbenzene U 1.0 pg/L 1 1,2,4-Tdchlotobenzerte U 1.0 ~glL 1 1,2,4-Tdmethylbenzene U 1.0 pg/L 1 Date Analyzed Analyst: RN 3/25/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/2612007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:a0 PM 3126/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2607 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3126/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM 312612007 2:42:00 PM 3/26/2007 2:42:00 PM 3/2612007 2:42:00 PM 3/26/2007 2:42:00 PM 3/26/2007 2:42:00 PM Analyst: MB 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51;00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51;00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM B Analytc detcctcd in thc associated Method Blank H Holding times for preparation or analysis cxcccdcd ND Not Detected at thc Reporting Limit Indicates thc compound w~s maalyzcd far but not detecle E Value above quantitntion range J Pmalyte detected balmy quantilalioa limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 28 of 40 American Analytical Laboratories, LLC. Date: 28-Ma,'-07 CLIENT: P.W. Grosser Consulting Client Sample lB: No. 7 [GW] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-06A Tag Number: Collection Date: Matrix: 3/21/2007 1:57:00 PM LIQUID Analyses Result VOLATILE SW-B46 METHOD 8260 1,2-Dibromo-3-chlorop ropane U 1.2-Dibromoethane U 1.2-Dichlorobenzene U 1,2-Dichlorcethane U 1,2-Diohloropropace U 1,3,5-Tdmethylbenzene U 1.3-Dichlorobenzene U 1.3-dichloropropane U 1,4-Dichlorobenzene U 2,2-Diahloropropane U 2-Butanone U 2-Chloroethyi vinyl ether U 2-Chlorotoluene U 2-Hexanoce U 2-Pmpanol U 4-Chlemtoluene U 4-1sopropyltoluece U 4-Methyl-2-pentanone U Acetone U Acrolein U ^ctTIouit rile U Benzene U Bromobenzene U Bmmochloromethane U Bromodichloromelhane U Bromoform U Bromomethane U Carbon disulfide U Carbon tetrachlorfde U Chlorobenzene U Chlorodifluoromethane U Chlomethane U Chloroform U Chlommethane U cis-1,2-Dichloroethene U els-1,3-Dichloropropene U Dibromochloromethane U Dibromomethane U Dichlo rodlfluoro methane U Limit Qual SW8260B 3.0 2.0 1.0 2.0 Units DF Date Analyzed Analyst: MB pgfi_ 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pglL 1 3/22/2007 2:51:00 PM pglL 1 3/22/2007 2:51:00 PM pg/L I 3/22/2007 2:51:00 PM pg/L I 3/22/2007 2:51:00 PM pg/L I 3/22/2007 2:51:00 PM pglL I 3/22/2007 2:51:00 PM pg/L I 3/22/2007 2:51:00 PM IJg/L 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM ug/L 1 3122/2007 2:51:00 PM gglL I 3/22/2007 2:51:00 PM iJglL 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM gg/L I 3/22/2007 2:51:00 PM pg/L '/ 3/22/2007 2:51:00 PM IJg/L I 3/22/2007 2:51:00 PM IJg/L I 3/22/2007 2:51:00 FM I~g/L I 3/22/2007 2:51:00 PM iJglL 1 3/22/2007 2:51:00 PM pglL 1 3/22/2007 2:51:00 PM pglL I 3/2212007 2:51:00 PM pglL 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pg/L I 3/22/2007 2:51:00 PM pg/L I 3122/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM IJ§lL I 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pglL 1 3/22/2507 2:51:00 PM pg/L 1 3122/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pglL 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM pg/L 1 3/22/2007 2:51:00 PM gglL 1 3/22/2007 2:51:00 PM Value above quantltation rang~ ~"|~[g delcctcd below quantltation limits Spike Recoveq~ ou~id= ac~pled recover, llmiLs Value exceeds Maximum Conlamlnant Level Page 29 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenpo~N.Y. 0703179-06A Client Sample ID: No. 7 [GW] Tag Number: Collection Date: 3/21/2007 1:57:00 PM Matrix: LIQUID Analyses Result VOLATILE SW-848 METHOD 8260 Diisopropyl ether U Ethanol U Ethyl acetate U Ethylbenzene U Freon-114 U Hexachlorobutediene U Isopropyl acetate U Isopmpylbenzene U m,p-Xyleae U Methyl tart-butyl ether U MeJhylene chloride U n-Amyl acetate U Naphthalene U u-Butyl a~elate U n-Butylhenzane U n-Propyl acetate U n-Propylbenzene U o-Xylene U p-Diethylbenzene U p-Ethyltoluene U sec-Butylbenzene U Styrene U t-Butyl alcohol U teR~utylbenzene U Tetrachloroathene U Toluene U trans-1,2-Dichloraethene U trans-1,3-Dichlompropene U Tdchloroethene U Tdchlemfluaromethane U Vinyl acetate U Vinyl chlodde U Surr: ~Bromofluorobenzene 92.8 Sum Dibramofluoromathane 99.0 Sum Toluene-el8 93.3 Limit Qual Units DF SW82608 1.0 pg/L 1.0 pglL 1.0 pg/L 1.0 pgP._ 1.0 pglL 1.0 pgFL 2.0 gglL 1.0 ~Jg/L 1.0 IJg/L 1.0 pg/L 1.0 pg/L 2.0 pg/L 1.0 pglL 1.0 PD/L 1.0 Itg/L 1.0 pglL 1.0 tJg/L 1.0 IJglL 1.0 gglL 1.0 pglL 1.0 pglL 1.0 IJg/L 1.0 pg/L 1.0 pg/L 54-134 %REC 52-132 %REC 5%127 %REC Date Analyzed Analyst: MB 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2507 2:51:00 PM 3/22/2507 2:51 :BO PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/2212007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 312212007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 5/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:011 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22,'2007 2:51:00 PM 3/22/2007 2:51:00 PM 3/22/2007 2:51:00 PM Qualifiers: B Analy~c dctccted in thc ~sociatcd Method Blank H Halding times for prepmation or analysis exceeded ND Not Detected at thc Reportin§ Limit U Indicates thc compound was analyzed for bul not dmecte Page 30 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpon, N.Y. 0703179-07A Client Sample ID: Tag Number: Collection Date: Matrix: No. 11 [5-7.5'] 3/21/2007 3:15:00 PM SOiL Analyses Result MERCURY Mercury 0.0t95 PERCENT MOISTURE Percent Moisture 16,9 TARGET ANALYTE LIST METALS Aluminum 11200 Antimony U Arsenic 1.69 Barium 22.7 Beryllium U Cadmium U Calcium 260 Chmmium 13.3 Cobalt U Copper 7.86 Iron 9060 Lead 10.5 Magnesium 1800 Manganese 106 Nickel 9.70 Potassium 769 Selenium U Silver U Sodium 160 Thallium U Vanadium 22.2 Zfnc 20.5 SEMIVOLATILE SW-848 METHOD 8270 1,2,4-Trichlorebenzene U 1,2-Dichlorobenzene U 1,3-Dlchlambenzene U 1,4-Dichlorobenzene U 2,4,8-Trichlorophenol U 2,4,6-Tdchloropheool U 2,4-Dlchlorophenol U 2,4-Dimethylphenal U 2,4-Dinitrephenol U 2,4-Dinitrotoluene U 2,6-Dinitrotoluene U Limit Qual Units DF 8W74718 8W74718 0.0115 mg/Kg<lry 1 02216 0 wt% 1 SW601 OB SW3050A 4.80 rog/Kg-dry 10 0.600 mg/Kg.dry 1 0.600 mg/Kg~ry 1 0.480 mg/Kg-dry 1 0.480 mg/Kg-clry 1 0.240 rog/Kg-dry 1 0.600 rog/Kg-dr7 1 0.480 rog/Kg-dry 1 0,480 rog/Kg-dry 0.490 mg/Kg-dry 1 4.60 rog/Kg-dry 10 0.360 rog/Kg-dry 1 0.480 mg/Kg-dry 1 0,480 rog/Kg-dry 1 0.480 mg/Kg~ry 1 2.40 mg,'Kg-dry 1 0.680 mg/Kg*dry 1 0.480 mgtKg-dry 1 1 ~44 rog/Kg-dry 1 0.480 mg/Kg-dry 1 0.480 rog/Kg.dry 1 0.480 mg/Kg-<lry 1 SW8270D SW3550A 140 pg/Kg-dry 1 140 ~Jg/Kg<Jr~ 1 140 IJglKg-d~/ 1 140 pg/Kg-dry 1 140 pg/Kg-dry 1 Date Analyzed Analyst: WN 3/27/2007 t2:41:01 PM Analyst: CM 3/22/2007 Analyst: Jp 3/28/2007 11:48:47 AM 3/27/2007 12:22:19 PM 3/27/2087 12:22:t9 PM 3/27/2007 12:22:19 PM 3/27/2807 12:22:t9 PM 3/27/2007 12:22:19 PM 3/2712007 12:22:19 PM 3/27/2007 12:22:19 PM 3/27/2097 12:22:19 PM 3/27/2007 12;22:19 PM 3/29/2007 1 t:48:47 AM 3/2712007 12:22:19 PM 3/27/2007 12:22:19 PM 3/2712007 12:22:19 PM 6/27/2007 12:22:19 PM 3127/2007 12:22:19 PM 3127/2007 12:22:19 PM 3/27/2007 12:22:19 PM 3/27/2007 12:22:19 PM 3/27/2007 12:22:19 PM 3/27/2007 12:22:19 PM 3/2712g07 12:22:19 PM Analyst: RN 3/20/2007 4:40:00 PM 3/26/2007 4:40.'00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 140 pg/Kg-dry 140 pg/Kg-dry 140 pg/Kg-dry 140 pglKg-dry 140 pglKg-dry 140 pglKg-dry I 3/26/2007 4:40:00 PM 3/28/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM Qualifiers: B Analy~c detected in the o~socialed Method Blaak H Haldi~g limes for preparation or analysis exceeded ND Not Detected at thc Rcpo~ng Limit U Indicates the compound was analyzed for but not detecto Page 31 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. I 1 [5-7.5'] Lab Order: 0703179 Tag Number: Project: Moores Lane Greenport, N.Y. Collection Date: 3/21/2007 3:15:00 PM Lab ID: 0703179-07A Matrix: SOIL Analyses Result Limit Qual Units DF Date Analyzed SEMIVOLAT[LE SW-846 METHOD 8270 SW82700 SW3550A Analyst: RN 2-ChlomnapMhalene U 140 pg/Kg-dfy 1 3/26/2007 4:40:00 PM 2-Chlorophanol U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM 2-Methylnaphthalene U 140 pg/Kg<lry I 3/26/2007 4:40:00 PM 2-Methylphenol U 140 ~g/Kg<J~j I 3/26/2007 4:40:00 PM 2-Nitroaniline U 140 ~JglKg-dry t 3/26/2007 4:40:00 PM 2-Nitmphenol LI 140 pg/Kg-d~/ 1 3/26/2007 4:40:00 PM 3,3'-Dichlorobenzidine U 140 ~g/Kg-dry 1 3/26/2007 4:40:00 PM 3+4-Methylphenc~l H 140 pit/Kg-dry I 3/26/2007 4:40:00 PM 3-Nitma n[line U 140 pg/Kg.dry I 3/26/2007 4:40:00 PM 4,6-Dinitro.2.methylphenol U 146 lag/Kg-d~y 1 3/26/2007 4:40:00 PM 4-Bmmophenyl phenyl ether U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM 4-Chloro-3-methylphenol U 140 ~g/Kg-dry 1 3/26/2007 4:40:00 PM 4-Chloroan~ine U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM 4-Chlomphenyl phenyl ether U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM 4-Nitroaniline U 140 pglKg~ry I 3/26/2007 4:40:00 PM 4-Nitrophenol U 1 §0 pglKg..d~y I 3/26/2007 4:40:00 PM Acenaphthefle U 140 ~glKg-dty 1 3/26/2007 4:40:00 PM Acenaphthylene U 140 gg/Kg-dry 1 3/26/2007 4:40:00 PM Aniline U 140 ~g/Kg-clry I 3/26/2007 4:40:00 PM Anthracene U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM Azobenzene U 140 pg/Kg-d~/ I 3/26/2007 4:40:00 PM Benzidine U 140 pg/Kg-dry 1 3/26/2007 4;40:00 PM BeP. zo(a)anthracene U 140 pg/Kg-dry I 3/26/2007 4:40:00 PM Benzo(a)pyrene U 140 pglKg-d~y 1 3/26/2007 4:40:00 PM rtenzo(b)flueranthene U 140 pglKg-do/ I 3/26/2007 4:40:00 PM Benzo(g,h,i)petylene U 140 pglKg-dry I 3/26/2007 4:40:00 PM Benzo(k}fluoranthene U 140 pg/Kg<l~] 1 3/26/2007 4:40:00 PM Benzoic ac~d U 140 i~g/Kg-dry 1 3/2612007 4;40:00 PM Benzyl atcohol U 140 pg/Kg-dry I 3/26/2007 4:40:00 PM Bis(2-chlorcethoxy)methane U 140 pg/Kg-dry I 312612007 4:411:00 PM Bis(2-chlomethyl)ether U 140 pg/Kg<hl I 312612007 4:40:00 PM Bis(2.chlo misopropyl)ether U 140 I~glKg-dry I 3/26/2007 4:40:00 PM Bis(2-ethylhexyl)phthalate U 140 gglKg-d ~/ I 3/26/2007 4:40:~O PM Butyl benzyl phthalate U 140 gg/Kg~ry 1 3/26/2007 4:40:00 PM Carbazole U 140 IJg/Kg-thy 1 3/26/2007 4:40:00 PM Chrysene U 140 pg/Kg-dry 1 3/26/2007 4:40:00 PM Dibenzo(a,h)anthracene U 140 lig/Kg-dly 1 3/26/2007 4:40:00 PM Dibenzofuran U 140 pg/Kg.d~t I 3/26/2007 4:40:00 PM Diethyl phthalate U 140 pglKg-di'j 1 3/26/2007 4:40:00 PM Qualifiers: Analyte detected in thc associated Method Bhmk Holding times for preparation or analysis exceeded ND Not Detected ttt thc Rcporting Limit E Value above quant halloa range J Analyte detected below quantitntion limits S Spike P, ecoveq, outside accepted recovery limits X Value exceeds Maximum Contaminant Level Page 32 of 40 American Analytical Laboratories, LLC. ])ate: 28-Mar~07 CLIENT: P.W. Grosset Consulting Client Sample ID: No. I 1 [5-7.5'] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-07A Tag Number: Collection Date: 3/21/2007 3:15:00 PM Matrix: SOIL A~mlyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW8270D SW3550A Dimethyl phthalate U 140 Ng/Kg-dry 1 Di-n-buty[ phthalate U 140 t~g/Kg-dpj 1 Di-n-octyl phthalata U 140 I~g/Kg~lry 1 Flueranthene U 140 pglKg-dp/ 1 Fluorene U 140 PB/Kg~' 1 Hexachlorobenzene U 140 pg/K6~ 1 Hexach~ombutadiene U 140 pg/Kg-dry 1 Hexechlorocyclope ntadiene U 180 IJg1Kg-dry 1 Hexachloroethane U 140 p§/Kg-dry 1 Indeno(1,2,3~,d)pytene U 140 pg/Kg~ry 1 Isophomne U 140 Fg/Kg-dry 1 Naphthalene U 140 pglKg-dry 1 Nitrebenzene U 140 I~glKg-dry 1 N-Nitrosodimethylamine U 140 pg/Kg-d~ 1 N-Niffosodi-n~oropylamine U 140 pglKg-d~y 1 N-Nitrosodipheny~amine U 140 pg/Kg-dry 1 Pentachlomphenol U 150 pg/Kgq:lry 1 Phenanthrene U 140 pg/Kg~lry 1 Phenol U 140 pg/Kg-dry 1 Pyrene U 140 pg/Kg-dry 1 Pyridine U 140 pg/Kg~ry 1 SurF, 2,4,6-Trlbromophenel 49,0 22-124 %REC 1 Surf: 2-Fluorobiphenyl 50,4 27-119 %REC 1 Surf, 2-Fluomphenol 28,6 21-123 %REC 1 Surr: 4-Terphenyl-d14 52,7 28-126 %REC Surf: Nitmbenzene~15 44.1 21-118 %REC 1 Sum Phenol-d6 37.7 18-129 %REC 1 VOLATILE SW-846 METHOD 8260 SW8260B 1.1,1,2-Tettachlomethane U 5.9 pg/Kg-dry 1,1,1-Trichlomethane U 5.9 pg/Kg-d~ 1 1,1,2,2-Telrachloroelhane U 5.9 pg/Kg-dry 1 1,1,2-Trichlaro-1,2,2-trifluomethane U 6.0 pg/Kg-d~J 1 1,1,2-T~iohbreethane U 5.9 pg/Kg-dry 1 ,l-Dichloroethane U 5.9 pg/Kg-dry 1 1,1-Dlchloroethene U 5.9 pg/Kg-dry 1 1,1-Dichloropropene U 5.9 pg/Kg-d~j 1 1,2.3-Trichlorobenzene U 5.9 I~g/Kg-dry 1 1,2,3-Tdchloropropane U 5.9 pg/Kg-dry 1 1,2,4,5-Tetramethylbenzene U 5.0 pg/Kg-d~ DF Date Analyzed Analyst: RN 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 312612007 4:46:00 PM 3/26/2007 4:40:00 PM 312612007 4:40:00 PM 3/26/2087 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 312612007 4:40:00 PM 3/26/2007 4:40:0(3 PM 3125/2007 4;40:00 PM 312512007 4:40:00 PM 3/28/2007 4;40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM 3/26/2007 4:40:00 PM Analyst: MB 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2067 8:25:(30 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3~22~2007 8:25;00 PM 3/22/2007 5:25:00 PM Analytc dctcctcd in the ~ssociatcd Method Blank }I Holdin§ limes for preparation or analysis exceeded ND Not Detected at thg Reporting Limit U Indicates the campound was analyzed t'or but not delecte Page 33 of 40 American Analytical Laboratories, LLC. Date: 28-Mar.-07 CLIENT: P.W. Grosser Consulting Client Sample ID: No. l ] [5-7.5'] Lab Order: 0703179 Project: Moores Lane Greenport, N.Y. Lab ID: 0703179-07A Tag Number: Collection Date: 3/21/2007 3:15:00 PM Matrix: SO1L Analyses VOLATILE SW-846 METHOD 8260 1,2,4-Trichrorobenzene 1,2,4-Trimet hylbenzene 1,2-Dibrome-3-chlompropan e 1,2-Dibrornoethane 1,2-Dichlorobenzene 1,2~Dichlomethane 1,2-Dichloropropane 1,3,5-Trimethylbenzene 1,3-Dichlorobenzene 1 ,~dichleropropane 1,4-Dichlo¢obenzene 2,2-Dichlowpropane 2-Butanone 2-Chloroethyl vinyl ether 2-Chlorotoluene 2-Hexanone 2-Propanol 4-Chlorotoluene 4-1sopropyltoluene 4-Methyg2-pentanone Acetone Acrolein Acrylonltrile Brornobenzene Bromochloromethane Bromodichloromethane Bromoform Bromemethane Ca,ben disulfide Carbon tetrachlodde Chlorobenzene Ch]orodifluoromethane Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1.3-Dichlorapwpene Dibromochloromethane Result Limit Qual Units SW8260B U 5.9 pg/Kg-dry U 5.9 pg/Kg~ry U 5.9 pglKg~lr~ U 5.9 pg/Kg-d~ U 5.9 ug/Kg-dry U 5.9 pg/Kg~ry U 5.g pg/Kg-dry U 5.9 IJg/Kg-dry U 5.~ pg/Kg-dry U 5.9 pg/Kg~lry U 5.9 pg/Kg~l[y U 5.9 pg/Kg-d~y U 5.g gg/Kg-dry U 5.9 pg/Kg-dry U 5.g pg/Kg-dly U 5.9 pg/Kg-dry U 58 pg/Kg-d~ U 5.9 pg/Kg-dry U 5.9 I~g/Kg-d~y U 5.9 pg/Kg.cb7 U 5.9 pg/Kg-dry U 29 pg/Kg-dry U 5.9 pg/Kg-dry U 5.9 pglKg..dry U 5.9 IJglKg-d[y U 5.9 pg/Kg-dry U 5.g pg/Kg-dr~ U 5.g pg/Kg-d~y U 5.9 pg/Kg~lry U 5.9 pg/Kg-dry U 5.9 pg~Kg~y U 5.9 pg/Kg*d~y U 5.9 pg/Kg.-d~y U 5.9 NglKg-d~y U 5.9 pglKg-d~y U 5.g pglKgod~y U 5.g pg/Kg-dry U 5.g pg/Kg-dry U 5.9 uglKg-dly DF Date Analyzed Analyst: MB 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/2212007 8:25:00 PM I 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM I 3/22/2007 8:25:00 PM I 3/22/2007 8:25:0(] PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 5:25:8n PM 1 3122/2007 8:25:00 PM 1 3/22/2007 5:25:00 PM 1 3122/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/22/2007 8:25;00 PM 1 3/22/2007 8:25:00 PM 1 3/22/2007 8:25:00 PM I 3/2212007 8:25:00 PM 1 3/22/2007 8:25:00 PM 1 3122/2007 8:25:00 PM I 3/22/2007 8;25;00 PM 1 3122/2007 8:25:00 PM Qualifiers: B Analytc deteclt-d in the associated Me0wd Blank H Holding times for preparation or analysis cxeccdcd ND Not Dctacled at the Reporting Limit Value above quantitation range Analyle detected below quantitation lirnits Spike Recovery outside accepted recovery limits Value exceeds Mmximum Contaminant Level Page 34 of 40 American Analytical Laboratories, LLC. Date: 28-Mw'-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Montes Lane Greenpor~N.Y. 0703179-07A Client Sample ID: No. l I [5~7.5'] Tag Number: Collection Dale: 3/21/2007 3:15:00 PM Matrix: SOIL Analyses Result VOLATILE SW-846 METHOD 8260 Dibrnmomethane U Dichlorodiflu oromet bane U Diisopmpyl ether U Ethanol U Ethyl acetate U Ethylbenzene U Freon-114 U Hexachlombutadiene U Isopropyl acetate U Isopmpylbenzene U m,p-Xylene U Methyl tart. butyl ether U Methylene chlodde U n-Amyl acetate U Naphthalene U n-Butyl acelate U n-Butylbenzene U r~Propyl acetate U n-Propyl~enzene U o-Xylene U p-Diethy~benzene U p-Ethyltaluene U sec-Butylbenzene U Styrene U t-Butyl alcohol U tett. Butylbenzene U Tetrachloroethene U Toluene U trans-1.2-Dichlomethene U frans-1,3-Dich[oropropene U Trichlomethene U Tfichlorofluommethane U Vinyl acetate U Vinyl chloride U Sure 4-Bremoflu~robenzene 93.0 Surf. Dibr~mofluommethane 102 Surf.. Toluene-d5 98.0 Limit Qual Units SW8260B 5.9 pg/Kg-dry 5.9 pglKg-d~ 5.9 pg/Kg.dpj 29 pg/Kg-dpJ 5.9 pg/Kg*dry 5.9 pgtKg-dry 5.9 IJglKg-dry 5.9 pg/Kg-dry 5.0 pg/Kg-d~ 5.g pg/Kg-dry 12 gglKg..dry 5.g pg/Kg-dry 5.9 pglKg-d~j 5.9 pg/Kg-d[y 5.9 pg/Kg-dry 5.9 pglKg~ry 5.9 pg/Kg~iry 5.9 pg/Kg-thy 5.9 pg/Kg-thy 5.9 pg/Kg-dpj 5.9 pg/Kg~lPj 5.9 pg/Kg-d~J 5.9 ~Jg/Kg~y 5.9 pg/Kg~ry 5.9 IJglKg-dry 5.9 pglKg-d~y 5.9 pg/Kg-d~ 5.9 pglKg.d~j 5.9 pg/Kg-dry 5.9 I~g/Kg-dry 5.9 pg/Kg-drj 5.9 pg/Kg-dry 5.9 pglKg~ry 5.9 pglKg..dry 61-133 %REC 61-139 %REC 57-131 %REC DF Date Analyzed Analyst: MB 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3122/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 5:25:00 PM 3/22/2097 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2097 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2097 5:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2097 5:25:00 PM 3/22/2007 5:25:00 PM 3/22/2007 8:25:(30 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22J2007 8:25:00 PM 3/22/2007 8:25:00 PM 3122/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3122/2007 8:25:00 PM 3122/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:09 PM 3/22/2007 8:25:00 PM 3/22/2007 8:25:00 PM 3/2~2007 8:25:00 PM 3/22/2007 6:25:00 PM Qualifiers: B Anal}lc detected in the ossociated Method Blank H Holdiag times for preparation or analysis exceeded E Value above quantitation range J A~talyte detected below quantitation limits S Spike Recovery outside accepted rccovc~ ]imil5 X Value cxcceds Maximum Contaminant Level Page 35 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpon, N.Y. 0703179-08A Client Sample ID: No. 11 [GArI Tag Number: Collection Date: 3/21/2007 3:29:00PM Matrix: LIQUID Analyses MERCURY Mercury TARGET ANALYTE LIST METALS Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel PolassJum Selenium Silver Sodium Thallium Vanadium Zinc SEMIVOLATILE SW-846 METHOD 8270 1,2,4-Trichlorobenzene 1,2-DIchlombenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinilrophenol 2,4-Dinitrotoluene 2,§-Dinitrotoluene 2--Chlomnaphthalene 24;hlomphenol Result Limit Qual Units SW7470A U 0000200 mg/L SW6010B SW3010A 640 0.200 mg/L U 0.0250 mg/L 0,123 0.0250 mg/L 1.82 0.0200 mg/L U 0.0200 mg/L U 0.0100 mg/L 53.0 0.0250 mglL 1.20 0.0200 mg/L U 0.0200 mgtL 0.768 0.0200 mg/L 557 0.200 mglL 0.273 0.0150 mg/L 83.6 0.0200 mg/L 5.98 0.0200 mg/L 0.668, 0.0200 mg/L 92.3 0. I00 mg/L U 0.0250 mglL U 0.0200 mglL 25.1 0.0300 mg/L U 0.0150 mglL 1.29 0.0200 mg/L 0.950 0.0200 mg/L SW8270D SW3510 U 5.O pg/L U 5.0 pglL U 5.0 pglL U 5.0 pg/L U 5.0 pg/L U 5.0 pg/L U 5.0 pg/L U 5.0 Hg/L U 10 pg/L U 5.0 pglL U 5.0 ~g/L U 5.0 pg/L U 5.0 pglL DF Date Analyzed Analyst: WN 3/23/2007 12:17:24 PM Analyst: JP 10 3/27/2007 2:24;23 PM 1 3/2712007 2:11:53 PM I 3/27/2007 2et 1:53 PM 1 3/27/2007 2:11:53 PM 1 3/27/2007 2:11:53 PM 1 3/27/2007 2:11:53 PM 1 3/9712007 2:11:53 PM 1 3/27/2007 2:11:53 P M 1 3/27/2007 2:t 1:53 PM I 3/2712007 2:11:53 PM 10 3/27/2007 2:24:23 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2;11:53 PM 3/2712007 2:11:53 PM 3/27/2007 2:11:53 PM 3/27/2007 2:11:53 PM Analyst: RN 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 312612007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:130 PM 3/26/2007 3:41:00 PM Qualifiers: B Analyle detected in the associated Method Blank H Holding times for preparation ~ analysis exceeded ND Not Detecled at the Reporting Limit U Indicates the compound was analyzed for but not detecte E Value above quuntilation range J An~ly~c detected bclow quantitation limits S Spike Recovery outside accepted recovery limits X Value exceeds Mo.xbnum Contaminant Level Page 36 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greanpo~, N.Y. 0703179-08A Client Sample ID: No. 11 [GW] Tag Number: Collection Date: 3/21/2007 3:29:00PM Matrix: LIQUID Analyses Result Limit Qual Units SEMIVOLATILE SW-846 METHOD 8270 SW82700 SW3510 2-Methylnaphthalane U 5.0 pglL 2-Msthylphenol U 5.0 IJglL 2-Nitroa niline U 5.0 pg/L 2-Nitrophenol U 5.0 I~g/L 3,3'-Dichlombenzidine U 5.0 pg/L 3'~4-Methylphenol U 5.0 pg/L 3-Nilmaniline U 5.0 pg/L 4,6-Diaitro-2-methylpheno[ U 5.0 pg/L 4-Bromophenyi phenyl ether U 5.0 pglL 4-Chloro-~met hylphenol U 5.0 pglL 4-Chleroaniline U 5.0 pg/L 4-Chlomphenyl phenyl ether U 5.0 ~Jg/L 4-Nitmaniline U 5.0 pglL 4-Nitmpheanl U 5.0 pg/L Aceaaphthene U 5.0 gg/L Acenaphthylene U 5.0 ~g/L Aniline U 5.0 pglL Anthracene U 5.0 pg/L Azobenzene U 5.0 pglL Benzidine U 5.0 pglL Benzo(a)anthracene U 5.0 IJg/L Benzo(a)pyrene U 5.0 ~Jg/L Benzo(blfluoranthene U 5.0 gg/L Benzo(g,h,~pelylene U 5.0 IJg/L Benzo(k)flanranthene U 5.0 pg/L Benzoic acid U 5.0 pg/L Benzyl alcohol U 5.0 pglL Bis(2-chlemethaxy)methane U 5.0 pg/L Bis(2-chloroethyl)ethe r U 5.0 pg/L Bis(2-chlomisopropyl)ethe r U 5.0 pglL Bis(2-ethylhexyl)phthalate U 5.0 pg/L Butyl benzyl phthalate U 5.0 pg/L Carbazole U 5,0 pg/L Chrysene U 5.0 pg/L Dibenzo(a,h)anthracene U 5.0 pg/L Dibenzofu~an U 5.0 pg/L Diethyl phthalate U 5.0 pg/L Dimethyl phthalate U 5,0 pglL DJ-n-butyl phlhalate U 5.0 pg/L DF Date Analyzed Analyst: RN 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/23/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/25/2007 3:41:00 PM 3/2612007 3:41:00 PM 3126/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/25/2007 3:41:00 PM 3/26/2007 3:41;00 PM 312612007 3:41:09 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41;00 PM 3/2612007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/2612007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM Qualifiers: B Analyte detected in thc associated Method Blank H Holding times for pmparagon or analysis ~xceeded ND Nol Detected at thc Rcpor[ing Limit U Indicates thc compound was analyzed for but not detecto Value above quantitaiion range Analy~e detected b=low qu[mtitatien limi~ Spike R~¢overy ou~id¢ accepted r~covcry limiL~ Value exceeds M[ximum Contaminanl Level Page 37 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Greenpon, N.Y. 0703179-08A Client Sample ID: Tag Number: Collection Date: Matrix: No. 11 [GW] 3121/2007 3:29:00 PM LIQUID Analyses SEMIVOLATILE 8W-846 METHOD 8270 DLn-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlombutadiene Hexachlorocyc[opentadiene Hexachtoroethane Indeno(1,2,3-c,d)pyrene Isophomne Naphlhalene Nitrobenzene N-Nltmsodimethylamine N-Nitrosodi-n-pmpylamine N-NibosodiphenyMmine Pentachloropher~ol Phenanthrene Phenol Pyrens Pyridine Surr: 2,4,6--Tribromop hanoi Sum 2-Fluorobiphenyl Sum 2*Fluomphenol Surr: 4-Terphenyl~I4 Sun: Nitmbenzene~i5 Sure Phenobd6 VOLATILE SW-846 METHOD 8260 1,1,1,2-Tetrachlaroethane 1,1,2,2-Tetrachloroethane 1,1,2-Trichloro-1,2,2-trifluoroethane 1,1,2-Tfichlomethane 1,1 -Dichlomethane 1,1-Dichlsroethene 1,1-Dichlompmpene 1,2,3-Tfichlombenzane 1,2,3-Trichlomoropane 1.2,4.5-Teb'amethylbenzene 1,2,4-Tfichinrobenzene 1,2,4-Trimethylbenzene Result Limit Qual Units SW82700 SW3510 U 5.0 p0/L U 5.0 pg/L 1 U 5.0 PolL 1 U 5.0 pg/L 1 U 5.O pg/L 1 U 5.0 pg~L 1 U 5.0 pgA- 1 U 5.0 polL 1 U 5.0 pgA- 1 U 5.0 pgA- 1 U 5~0 pg/L 1 U 5.0 pglL 1 U 5.0 pgA- 1 U 5.0 pg/L 1 U 5.0 pgA- 1 U 5.0 pg/L 1 U 5.0 polL 1 U 5.0 polL 1 U 5.0 pg/L 1 74.2 22-124 %REC 1 77.7 18-124 %REC 1 57.5 16-112 %REC 1 88.9 17-121 %REC 1 71.0 19-115 %REC 1 36.4 12-102 %REC 1 SW$260B U 1.0 polL 1 U 1.0 polL 1 U 1.0 pgA_ 1 U 1.0 pg/L 1 U 1.0 pg/L 1 U 1.0 polL 1 U 1.9 pgA- 1 U 1.0 p01L 1 U 1.0 IJg/L 1 U 1.0 polL 1 U 1.0 polL 1 DF Date Analyzed Analyst: RN 312612007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:4t:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:09 PM 3/26/2007 3:41:00 PM 3/26/2007 3;41:00 PM 3/26/2007 3:41:00 PM 3/2612007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3/26/2007 3:41 :DO PM 3/26/2007 3:41 :DO PM 3/26/2007 3:41:00 PM 3/26/2007 3:41:00 PM 3126/2007 3:41:00 PM Analyst: MB 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3122/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3122/2007 3:39:00 PM B Analy~e detected in the associated Method Blank H Holding times for preparation or analysis exceeded ND Not Detected at thc Rcportin§ Limit U Indicates the compound was analyz, cd £or but not detcctc E Valuc above quanfitafion range J Analyte dctcctcd below quantitation limits S Spike Recovery outside accepted recovery limi~ X Value exceeds M&ximum Contaminant Level Page 38 of 40 American Analytical Laboratories, LLC. Date: 28-Mar~07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosser Consulting 0703179 Moores Lane Gmenpon, N.Y. 0703179-08A Client Sample ID: No. 11 [GW] Tag Number: Collection Date: 3/21/20073:29:00PM Matrix: LIQUID Analyses Result Limit Qual VOLATILE SW-846 METHOD 8260 SW82609 t ,2-Dibromo-3-chloropropane U 1.0 1,2-Dibromoethane U 1.0 1,2-Dichlorobenzene U 1.0 1,2-Dichloroelhane U 1.0 1,2-Dichloropropane U 1.0 1.3.5-Trimethylbenzen e U 1.0 1,3-Dichlorobenzene U 1.0 1,3-dicMotopropane U 1.0 1,4-Dichlorobenzene U 1.0 2,2-Dichloropropane U 1.0 2-Butanone U 3.0 2-Chloroethyl vinyl ether U 1.0 2-Chlorotoluene U 1.0 2-Hexanone U 2.0 2-Propanol U 1.0 4-Chlorotoluene U 1.0 4-1sopropyfioluene U 1.0 4-Methyl-2-pentanone U 2.O Acetone U 2.0 Acrolein U 1.0 Ac~lonitfile U 1.0 Benzene tJ 1.0 Bromobenzene U 1.0 Bromochloromethane U 1.0 Bromodichloromethane U 1.0 Bromofonn U 1.0 Bmmomethane U 1.0 Carbon disulfide U 1.D Carbon tetrachloride U 1.0 Chlorobenzene U 1.0 Chlorodifluoromethane U 1.0 Chloroethane U 1.0 Chloroform U 1.0 Chloromethane U 1.0 cis-1,2-Dichlemethene U 1.0 cis-1,3-Dichloropropene U 1.0 Dibmmochlommethane U 1.9 Dibromomethane U 1.0 Dichlorodifluommethane u 1.0 Units DF Date Analyzed pg/L pg/L pg/L pg/L pg/L pg/L gg/L pglL pg/L pg/L pg/L ug/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pglL pglL pg/L pg/L pg/L pg/L pg/L pg/L ~J/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L pg/L Analyst: MB 3/22/2007 3:39:09 PM 3/2212007 3:39:00 PM 3/;?2/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3;39:09 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/:'097 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3;39:90 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/~2/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39;00 PM 3/22/2007 3;39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39;00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM Qualifiers: B Analytc dmccted in thc associated Method Blank H Holding dines for preparation or analysis exceeded ND Not Detected at the Reporting Limit U Indicams thc compound was analyzed for but not detecto E Value above quandtafioa mage J Analyle detect~ below quandtatlon limits S Spike Recovery outside acccple~l recovery limit~ X Value exceeds Maximum Contaminant Level Page 39 of 40 American Analytical Laboratories, LLC. Date: 28-Mar-07 CLIENT: Lab Order: Project: Lab ID: P.W. Grosset Consulting 0703179 Moores Lane Greenpo~,N.Y. 0703179-08A Client Sample ID: No. 11 [GW] Tag Number: Collection Date: 3/21/2007 3:29:00 PM Matrix: L1QUID Analyses Result Limit Qual Units DF Date Analyzed VOLATILE SW-846 METHOD 8260 SW82609 Diisopropyl ether U 1.0 !Jg/L Ethanol U 1.0 IJg/L Ethyl acetate U 1.0 iJg/L Ethylbenzene U 1.0 pg/L Freon-114 U 1.0 p§IL Hexachlorobutadiene U 1.0 pglL Isepropyl acetate U 1.0 Fg/L Isopropylbenzene U 1.0 gg/L m,p-XyJene U 2.0 P9tL Methyl tart-butyl ether U 1.0 IJ9/L Methylene chloride U 1.0 og/L n-Amyl acetate U 1.0 Hg/L Naphthalene U 1.0 pglL n-Butyl acetate U 2.0 ~Jg/L n-Butylbenzene U 1.0 pB/L n-Pmpyl acetate U 1.0 IJg/L n-Propylbenzene U 1.0 pglL o-Xylene U 1,0 pg/L p-Diethylbenzene U 1.0 pg/L p-Ethyltoluene U 1.0 pg/L sec-Butylbenzene U 1.0 pglL Styrene U t .0 pglL t-Butyl alcohol U 1.0 pg/L tert-Butylbenzene U 1.0 pg/L Tetrachloraethene U 1.0 pg/L Toluene U t .0 IJglL trans*1.2-Dichlomethene U 1.0 pg/L trans-1,3-Dichloropropene U t ,0 pg/L Trichloroethene U 1.0 IJ~/L Trichloroflua romethane U 1.0 pg/L Vinyl acetate U 1.0 ~glL Vinyl chloride U 1.0 pg/L Surr: 4-Bromofluombenzene 101 54-134 %REC Sum Dibmmofluoromethane 107 52-132 %REC Sum Toluene-d8 99.2 51-127 %REC Analyst: MB 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3122/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/27J2007 3:39:00 PM 3/22/2097 3:39:00 PM 3/22/2007 3:39:0D PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39;00 PM 3/22/2007 3:39:0fl PM 3/22./2007 3:39:013 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:D0 PM 3/22/2097 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM 3/22/2007 3:39:00 PM Qualifiers: Analyte detected in thc associatcd Mcflmd Blank Holding times for pnxparation or analysis cxccedcd ND Not Detected at the Rcporling Limit U Indicates thc compound was analyzed for but not dctccte E Value above quantltetion range J Analyle detected below quantitation limits S Spike Recovery outside accepted recovery limits X Value exceeds Maximum Contminant Level Page 40 of 40