Loading...
HomeMy WebLinkAbout(4) Soil Analytics.pdf � IdY I §t '' n1tC `�, Area of Embankment Sample 1 and Embankment Grab 1 3 S i �` " � �, Area of Embankment Sample } ` � '� °�� 2 and Embankment Grab 2 il 4, 1tI4 Y1 4- t ENVIROSCIENCE CONSULTANTS,INC. 2150 SMITHTOWN AVENUE,RONKONKOMA,NY 11779 g Soil Sampling m (631)580-3191 Figure 1 Strong's Yacht Center Sample Locations FAX 58 -3195 health p Mattituck,NY www.envirohealth.org Table 1 Soil Chemical Analytical Results Strongs Yacht Center September 18, 2020 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . A -Embankment 1 Embankment 2 tIm' bainkmentl , Embankment 2 Y SDEC NYSDEC . . ..... ......... Sample Location Grab'' Grab unrestricted Use Residential (VC)CS only) (VoCs only . Use SCO Barium NA NA 3.95 1.96 350 350 820 Chromium NA NA 1.31 1.34 30 36 NS Copper NA NA 1.40 1.50 50 270 1,720 Lead NA NA 0.50 0.48 63 400 450 Manganese NA NA 26.2 11.6 1,600 2,000 2,000 Nickel NA NA 0.56 0.82 30 140 130 Zinc NA NA 1.50 1.50 109 2,200 2,480 Notes: Only detected metals are summarized in this table. No VOC's were detected in any of the samples. NS = Not specified NA = Not Analyzed SCO = Soil Cleanup Objective Page 1 of 1 EN IROSCIENCE CONISULJANTS INC. ' PH0E/VIXk.�1" :-',.' Thursday, September 24, 2020 Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 Project ID: STRONGS YACHT CENTER SDG ID: GCG82052 Sample ID#s: CG82052 - CG82055 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. This report is incomplete unless all pages indicated in the pagination at the bottom of the page are included. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original. If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Sincerely yours, A UL Phyllis hiller Laboratory Director NJ Lab Registration #CT-003 NELAC -#NY11301 NY Lab Registration #11301 CT Lab Registration #PH-0618 PA Lab Registration #68-03530 MA Lab Registration #M-CT007 RI Lab Registration #63 ME Lab Registration #CT-007 UT Lab Registration #CT00007 NH Lab Registration #213693-A,B VT Lab Registration #VT11301 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06040 Telephone(860)645-1102 Fax(860)645-0823 Page 1 of 32 PHOU 77 t v rya F Environmental Laboratories, Inc. NY# 11301 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Sample Id Cross Reference September 24, 2020 SDG I.D.: GCG82052 Project ID: STRONGS YACHT CENTER Client Id Lab Id Matrix EMBANKMENT 1 CG82052 SOIL EMBANKMENT 2 CG82053 SOIL EMBANKMENT GRAB 1 CG82054 SOIL EMBANKMENT GRAB 2 CG82055 SOIL Page 2 of 32 PHOU VIX1,-i,3 elz;E01 Y Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 NY#11801 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Kathryn Loddengaard Enviroscience Consultants September 24, 2020 2150 Smithtown Ave Ronkonkoma, NY 11779 Sample Information Custody Information Date Time Matrix: SOIL Collected by: JF 09/18/20 10:25 Location Code: ENV-SCI Received by: B 09/21/20 15:14 Rush Request: 72 Hour Analyzed by: see "By" below P.O.#: Laboratory Data SDG ID: GCG82052 Phoenix ID: CG82052 Project ID: STRONGS YACHT CENTER Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By Reference Silver <0.34 0.34 mg/Kg 1 09/22/20 EK SW601OD Arsenic <0.67 0.67 mg/Kg 1 09/22/20 EK SW601OD Barium 3.95 0.34 mg/Kg 1 09/22/20 EK SW601OD Beryllium <0.27 0.27 mg/Kg 1 09/22/20 EK SW601OD Cadmium <0.34 0.34 mg/Kg 1 09/22/20 EK SW601OD Chromium 1.31 0.34 mg/Kg 1 09/22/20 EK SW601OD Copper 1.4 0.7 mg/kg 1 09/22/20 EK SW601OD Mercury <0.03 0.03 mg/Kg 2 09/22/20 RS SW7471B Manganese 26.2 0.34 mg/Kg 1 09/22/20 EK SW601OD Nickel 0.56 0.34 mg/Kg 1 09/22/20 EK SW601OD Lead 0.50 0.34 mg/Kg 1 09/22/20 EK SW601OD Selenium < 1.3 1.3 mg/Kg 1 09/22/20 EK SW601OD Trivalent Chromium 1.31 0.34 mg/kg 1 09/22/20 CALC 6010-7196 Zinc 1.5 0.7 mg/Kg 1 09/22/20 EK SW601OD Percent Solid 98 % 09/21/20 CJ SW846-%Solid Chromium,Hex.(SW3060 digestion) <0.40 0.40 mg/Kg 1 09/22/20 ARG SW7196A pH at 25C-Soil 4.64 1.00 pH Units 1 09/21/20 20:48 AP SW846 9045D Redox Potential -23.3 mV 1 09/21/20 AP SM2580B-09 Total Cyanide(SW9010C Distill.) <0.57 0.57 mg/Kg 1 09/23/20 EG SW9012B Mercury Digestion Completed 09/22/20 AW/VT SW7471B Soil Extraction for Herbicide Completed 09/21/20 J/D SW3550C Soil Extraction for PCB Completed 09/21/20 L/A/E SW3545A Soil Extraction for Pesticides Completed 09/21/20 L/A/E SW3545A Soil Extraction for SVOA Completed 09/21/20 R/E SW3546 Total Metals Digest Completed 09/21/20 B/AG SW3050B Chlorinated Herbicides 2,4,5-T ND 130 ug/Kg 10 09/22/20 JRB SW8151A Ver 1 Page 3 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82052 Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By 2,4,5-TP(Silvex) ND 130 ug/Kg 10 09/22/20 JRB SW8151A 2,4-D ND 250 ug/Kg 10 09/22/20 JRB SW8151A 2,4-DB ND 2500 ug/Kg 10 09/22/20 JRB SW8151A Dalapon ND 130 ug/Kg 10 09/22/20 JRB SW8151A Dicamba ND 130 ug/Kg 10 09/22/20 JRB SW8151A Dichloroprop ND 250 ug/Kg 10 09/22/20 JRB SW8151A Dinoseb ND 250 ug/Kg 10 09/22/20 JRB SW8151A QA/QC Surrogates % DCAA 54 % 10 09/22/20 JRB 30-150% % DCAA(Confirmation) 42 % 10 09/22/20 JRB 30-150% Polychlorinated Biphenyls PCB-1016 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1221 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1232 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1242 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1248 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1254 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1260 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1262 ND 330 ug/Kg 10 09/22/20 SC SW8082A PCB-1268 ND 330 ug/Kg 10 09/22/20 SC SW8082A QA/QC Surrogates % DCBP 133 % 10 09/22/20 SC 30-150% % DCBP(Confirmation) 122 % 10 09/22/20 SC 30-150% %TCMX 101 % 10 09/22/20 SC 30-150% %TCMX(Confirmation) 97 % 10 09/22/20 SC 30-150% Pesticides - Soil 4,4'-DDD ND 2.0 ug/Kg 2 09/22/20 CG SW8081B 4,4'-DDE ND 2.0 ug/Kg 2 09/22/20 CG SW8081B 4,4'-DDT ND 2.0 ug/Kg 2 09/22/20 CG SW8081B a-BHC ND 6.6 ug/Kg 2 09/22/20 CG SW8081B a-Chlordane ND 3.3 ug/Kg 2 09/22/20 CG SW8081B Aldrin ND 3.3 ug/Kg 2 09/22/20 CG SW8081B b-BHC ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Chlordane ND 33 ug/Kg 2 09/22/20 CG SW8081B d-BHC ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Dieldrin ND 3.3 ug/Kg 2 09/22/20 CG SW8081B Endosulfan I ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Endosulfan II ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Endosulfan sulfate ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Endrin ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Endrin aldehyde ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Endrin ketone ND 6.6 ug/Kg 2 09/22/20 CG SW8081B g-BHC ND 1.3 ug/Kg 2 09/22/20 CG SW8081B g-Chlordane ND 3.3 ug/Kg 2 09/22/20 CG SW8081B Heptachlor ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Heptachlor epoxide ND 6.6 ug/Kg 2 09/22/20 CG SW8081B Methoxychlor ND 33 ug/Kg 2 09/22/20 CG SW8081B Toxaphene ND 130 ug/Kg 2 09/22/20 CG SW8081B Ver 1 Page 4 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82052 Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By QA/QC Surrogates % DCBP 76 % 2 09/22/20 CG 30-150% • DCBP(Confirmation) 82 % 2 09/22/20 CG 30-150% •TCMX 73 % 2 09/22/20 CG 30-150% •TCMX(Confirmation) 78 % 2 09/22/20 CG 30-150% Volatiles 1,1,1,2-Tetrachloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1,1-Trichloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1,2,2-Tetrachloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1,2-Trichloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1-Dichloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1-Dichloroethene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,1-Dichloropropene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2,3-Trichlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2,3-Trichooropropane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2,4-Trichlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2,4-Tri methyl benzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2-Dibromo-3-chloropropane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2-Dibromoethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2-Dichlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2-Dichloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,2-Dichloropropane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,3,5-Tri methyl benzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,3-Dichlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,3-Dichloropropane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 1,4-Dichlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 2,2-Dichloropropane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 2-Chlorotoluene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 2-Hexanone ND 30 ug/Kg 1 09/21/20 JLI SW8260C 2-Isopropyltoluene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 4-Chlorotoluene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C 4-Methyl-2-pentanone ND 30 ug/Kg 1 09/21/20 JLI SW8260C Acetone ND 30 ug/Kg 1 09/21/20 JLI SW8260C Acrylonitrile ND 12 ug/Kg 1 09/21/20 JLI SW8260C Benzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Bromobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Bromochloromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Bromodichloromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Bromoform ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Bromomethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Carbon Disulfide ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Carbon tetrachloride ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Chlorobenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Chloroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Chloroform ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Chloromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C cis-1,2-Dichloroethene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C cis-1,3-Dichloropropene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Dibromochloromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Ver 1 Page 5 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82052 Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By Dibromomethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Dichlorodifluoromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Ethylbenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Hexachlorobutadiene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Isopropylbenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C m&p-Xylene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Methyl Ethyl Ketone ND 30 ug/Kg 1 09/21/20 JLI SW8260C Methyl t-butyl ether(MTBE) ND 12 ug/Kg 1 09/21/20 JLI SW8260C Methylene chloride ND 12 ug/Kg 1 09/21/20 JLI SW8260C Naphthalene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C n-Butylbenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C n-Propylbenzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C o-Xylene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C p-Isopropyltoluene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C sec-Butyl benzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Styrene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C tert-Butyl benzene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Tetrachloroethene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Tetrahydrofuran (THF) ND 12 ug/Kg 1 09/21/20 JLI SW8260C Toluene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Total Xylenes ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C trans-1,2-Dichloroethene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C trans-1,3-Dichloropropene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C trans-1,4-dichloro-2-butene ND 12 ug/Kg 1 09/21/20 JLI SW8260C Trichloroethene ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Trichlorofluoromethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Trichlorotrifluoroethane ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C Vinyl chloride ND 6.0 ug/Kg 1 09/21/20 JLI SW8260C QA/QC Surrogates % 1,2-dichlorobenzene-d4 99 % 1 09/21/20 JLI 70-130% %Bromofluorobenzene 102 % 1 09/21/20 JLI 70-130% % Dibromofluoromethane 96 % 1 09/21/20 JLI 70-130% %Toluene-d8 103 % 1 09/21/20 JLI 70-130% 1,4-dioxane 1,4-dioxane ND 90 ug/kg 1 09/21/20 JLI SW8260C Semivolatiles 1,2,4,5-Tetrachlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2,4-Trichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2-Diphenylhydrazine ND 340 ug/Kg 1 09/22/20 AW SW8270D 1,3-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,4-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4,5-Trichlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4,6-Trichloropheno) ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dichlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dimethylphenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dinitrophenol ND 340 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dinitrotoluene ND 240 ug/Kg 1 09/22/20 AW SW8270D Ver 1 Page 6 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82052 Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By 2,6-Dinitrotoluene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Chloronaphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Chlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Methyl naphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Methylphenol (o-cresol) ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Nitroaniline ND 340 ug/Kg 1 09/22/20 AW SW8270D 2-Nitrophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 3&4-Methylphenol(m&p-cresol) ND 340 ug/Kg 1 09/22/20 AW SW8270D 3,3'-Dichlorobenzidine ND 240 ug/Kg 1 09/22/20 AW SW8270D 3-Nitroaniline ND 340 ug/Kg 1 09/22/20 AW SW8270D 4,6-Dinitro-2-methyl phenol ND 340 ug/Kg 1 09/22/20 AW SW8270D 4-Bromophenyl phenyl ether ND 340 ug/Kg 1 09/22/20 AW SW8270D 4-Chloro-3-methyl phenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Chloroaniline ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Chlorophenyl phenyl ether ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Nitroaniline ND 540 ug/Kg 1 09/22/20 AW SW8270D 4-Nitrophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D Acenaphthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Acenaphthylene ND 240 ug/Kg 1 09/22/20 AW SW8270D Acetophenone ND 240 ug/Kg 1 09/22/20 AW SW8270D Aniline ND 340 ug/Kg 1 09/22/20 AW SW8270D Anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benz(a)anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzidine ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(a)pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(b)fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(ghi)perylene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(k)fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzoic acid ND 670 ug/Kg 1 09/22/20 AW SW8270D Benzy) butyl phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroethoxy)methane ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroethyl)ether ND 340 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroisopropyl)ether ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-ethylhexyl)phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Carbazole ND 340 ug/Kg 1 09/22/20 AW SW8270D Chrysene ND 240 ug/Kg 1 09/22/20 AW SW8270D Dibenz(a,h)anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Dibenzofuran ND 240 ug/Kg 1 09/22/20 AW SW8270D Diethyl phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Dimethylphthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Di-n-butylphthalate ND 340 ug/Kg 1 09/22/20 AW SW8270D Di-n-octylphthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Fluorene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorobutadiene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorocyclopentadiene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachloroethane ND 240 ug/Kg 1 09/22/20 AW SW8270D Indeno(1,2,3-cd)pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Ver 1 Page 7 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82052 Client ID: EMBANKMENT 1 RL/ Parameter Result PQL Units Dilution Date/Time By Isophorone ND 240 ug/Kg 1 09/22/20 AW SW8270D Naphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D Nitrobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodimethylamine ND 340 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodi-n-propylamine ND 240 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodiphenylamine ND 340 ug/Kg 1 09/22/20 AW SW8270D Pentachloronitrobenzene ND 340 ug/Kg 1 09/22/20 AW SW8270D Pentachlorophenol ND 340 ug/Kg 1 09/22/20 AW SW8270D Phenanthrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Phenol ND 240 ug/Kg 1 09/22/20 AW SW8270D Pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Pyridine ND 340 ug/Kg 1 09/22/20 AW SW8270D QA/QC Surrogates •2,4,6-Tribromophenol 95 % 1 09/22/20 AW 30-130% •2-Fluorobiphenyl 72 % 1 09/22/20 AW 30-130% •2-Fluorophenol 54 % 1 09/22/20 AW 30-130% % Nitrobenzene-d5 56 % 1 09/22/20 AW 30-130% % Phenol-d5 58 % 1 09/22/20 AW 30-130% %Terphenyl-d14 95 % 1 09/22/20 AW 30-130% Field Extraction Completed 09/18/20 SW5035A 1 =This parameter is not certified by the primary accrediting authority(NY NELAC)for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level(Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds(preceeded with a %)added by the lab to determine analysis efficiency. Surrogate results(%)listed in the report are not"detected"compounds. Comments: Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene.Azobenzene is used for the calibration of 1,2-Diphenylhydrazine. The regulatory hold time for pH is immediately.This pH was performed in the laboratory and may be considered outside of hold- time. Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If you are the client above and have any questions concerning this testing,please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. A UL Phyllis hiller, Laboratory Director September 24,2020 Reviewed and Released by: Rashmi Makol, Project Manager Ver 1 Page 8 of 32 PHOU VIX1,-i,3 elz;E01 Y Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 NY#11301 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Kathryn Loddengaard Enviroscience Consultants September 24, 2020 2150 Smithtown Ave Ronkonkoma, NY 11779 Sample Information Custody Information Date Time Matrix: SOIL Collected by: JF 09/18/20 10:30 Location Code: ENV-SCI Received by: B 09/21/20 15:14 Rush Request: 72 Hour Analyzed by: see "By" below P.O.#: Laboratory Data SDG ID: GCG82052 Phoenix ID: CG82053 Project ID: STRONGS YACHT CENTER Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By Reference Silver <0.34 0.34 mg/Kg 1 09/22/20 EK SW601OD Arsenic <0.69 0.69 mg/Kg 1 09/22/20 EK SW601OD Barium 1.96 0.34 mg/Kg 1 09/22/20 EK SW601OD Beryllium <0.27 0.27 mg/Kg 1 09/22/20 EK SW601OD Cadmium <0.34 0.34 mg/Kg 1 09/22/20 EK SW601OD Chromium 1.34 0.34 mg/Kg 1 09/22/20 EK SW601OD Copper 1.5 0.7 mg/kg 1 09/22/20 EK SW601OD Mercury <0.03 0.03 mg/Kg 2 09/22/20 RS SW7471B Manganese 11.6 0.34 mg/Kg 1 09/22/20 EK SW601OD Nickel 0.82 0.34 mg/Kg 1 09/22/20 EK SW601OD Lead 0.48 0.34 mg/Kg 1 09/22/20 EK SW601OD Selenium < 1.4 1.4 mg/Kg 1 09/22/20 EK SW601OD Trivalent Chromium 1.34 0.34 mg/kg 1 09/22/20 CALC 6010-7196 Zinc 1.5 0.7 mg/Kg 1 09/22/20 EK SW601OD Percent Solid 97 % 09/21/20 CJ SW846-%Solid Chromium,Hex.(SW3060 digestion) <0.38 0.38 mg/Kg 1 09/22/20 ARG SW7196A pH at 25C-Soil 4.73 1.00 pH Units 1 09/21/20 20:48 AP SW846 9045D Redox Potential 81.9 mV 1 09/21/20 AP SM2580B-09 Total Cyanide(SW9010C Distill.) <0.43 0.43 mg/Kg 1 09/23/20 EG SW9012B Mercury Digestion Completed 09/22/20 AW/VT SW7471B Soil Extraction for Herbicide Completed 09/21/20 J/D SW3550C Soil Extraction for PCB Completed 09/21/20 L/A/E SW3545A Soil Extraction for Pesticides Completed 09/21/20 L/A/E SW3545A Soil Extraction for SVOA Completed 09/21/20 R/E SW3546 Total Metals Digest Completed 09/21/20 B/AG SW3050B Chlorinated Herbicides 2,4,5-T ND 130 ug/Kg 10 09/22/20 JRB SW8151A Ver 1 Page 9 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82053 Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By 2,4,5-TP(Silvex) ND 130 ug/Kg 10 09/22/20 JRB SW8151A 2,4-D ND 260 ug/Kg 10 09/22/20 JRB SW8151A 2,4-DB ND 2600 ug/Kg 10 09/22/20 JRB SW8151A Dalapon ND 130 ug/Kg 10 09/22/20 JRB SW8151A Dicamba ND 130 ug/Kg 10 09/22/20 JRB SW8151A Dichloroprop ND 260 ug/Kg 10 09/22/20 JRB SW8151A Dinoseb ND 260 ug/Kg 10 09/22/20 JRB SW8151A QA/QC Surrogates % DCAA 53 % 10 09/22/20 JRB 30-150% % DCAA(Confirmation) 51 % 10 09/22/20 JRB 30-150% Polychlorinated Biphenyls PCB-1016 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1221 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1232 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1242 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1248 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1254 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1260 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1262 ND 340 ug/Kg 10 09/22/20 SC SW8082A PCB-1268 ND 340 ug/Kg 10 09/22/20 SC SW8082A QA/QC Surrogates % DCBP 93 % 10 09/22/20 SC 30-150% % DCBP(Confirmation) 98 % 10 09/22/20 SC 30-150% %TCMX 82 % 10 09/22/20 SC 30-150% %TCMX(Confirmation) 87 % 10 09/22/20 SC 30-150% Pesticides - Soil 4,4'-DDD ND 2.0 ug/Kg 2 09/22/20 CG SW8081B 4,4'-DDE ND 2.0 ug/Kg 2 09/22/20 CG SW8081B 4,4'-DDT ND 2.0 ug/Kg 2 09/22/20 CG SW8081B a-BHC ND 6.7 ug/Kg 2 09/22/20 CG SW8081B a-Chlordane ND 3.4 ug/Kg 2 09/22/20 CG SW8081B Aldrin ND 3.4 ug/Kg 2 09/22/20 CG SW8081B b-BHC ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Chlordane ND 34 ug/Kg 2 09/22/20 CG SW8081B d-BHC ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Dieldrin ND 3.4 ug/Kg 2 09/22/20 CG SW8081B Endosulfan I ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Endosulfan II ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Endosulfan sulfate ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Endrin ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Endrin aldehyde ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Endrin ketone ND 6.7 ug/Kg 2 09/22/20 CG SW8081B g-BHC ND 1.3 ug/Kg 2 09/22/20 CG SW8081B g-Chlordane ND 3.4 ug/Kg 2 09/22/20 CG SW8081B Heptachlor ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Heptachlor epoxide ND 6.7 ug/Kg 2 09/22/20 CG SW8081B Methoxychlor ND 34 ug/Kg 2 09/22/20 CG SW8081B Toxaphene ND 130 ug/Kg 2 09/22/20 CG SW8081B Ver 1 Page 10 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82053 Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By QA/QC Surrogates % DCBP 79 % 2 09/22/20 CG 30-150% • DCBP(Confirmation) 64 % 2 09/22/20 CG 30-150% •TCMX 77 % 2 09/22/20 CG 30-150% •TCMX(Confirmation) 73 % 2 09/22/20 CG 30-150% Volatiles 1,1,1,2-Tetrachloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1,1-Trichloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2,2-Tetrachloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2-Trichloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloropropene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichooropropane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Trichlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Tri methyl benzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromo-3-chloropropane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromoethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloropropane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,3,5-Tri methyl benzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichloropropane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 1,4-Dichlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 2,2-Dichloropropane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 2-Chlorotoluene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 2-Hexanone ND 28 ug/Kg 1 09/22/20 JLI SW8260C 2-Isopropyltoluene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 4-Chlorotoluene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C 4-Methyl-2-pentanone ND 28 ug/Kg 1 09/22/20 JLI SW8260C Acetone ND 28 ug/Kg 1 09/22/20 JLI SW8260C Acrylonitrile ND 11 ug/Kg 1 09/22/20 JLI SW8260C Benzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Bromobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Bromochloromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Bromodichloromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Bromoform ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Bromomethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Carbon Disulfide ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Carbon tetrachloride ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Chlorobenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Chloroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Chloroform ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Chloromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C cis-1,2-Dichloroethene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C cis-1,3-Dichloropropene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Dibromochloromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Ver 1 Page 11 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82053 Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By Dibromomethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Dichlorodifluoromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Ethylbenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Hexachlorobutadiene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Isopropylbenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C m&p-Xylene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Methyl Ethyl Ketone ND 28 ug/Kg 1 09/22/20 JLI SW8260C Methyl t-butyl ether(MTBE) ND 11 ug/Kg 1 09/22/20 JLI SW8260C Methylene chloride ND 11 ug/Kg 1 09/22/20 JLI SW8260C Naphthalene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C n-Butylbenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C n-Propylbenzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C o-Xylene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C p-Isopropyltoluene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C sec-Butyl benzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Styrene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C tert-Butyl benzene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Tetrachloroethene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Tetrahydrofuran (THF) ND 11 ug/Kg 1 09/22/20 JLI SW8260C Toluene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Total Xylenes ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C trans-1,2-Dichloroethene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C trans-1,3-Dichloropropene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C trans-1,4-dichloro-2-butene ND 11 ug/Kg 1 09/22/20 JLI SW8260C Trichloroethene ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Trichlorofluoromethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Trichlorotrifluoroethane ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C Vinyl chloride ND 5.7 ug/Kg 1 09/22/20 JLI SW8260C QA/QC Surrogates % 1,2-dichlorobenzene-d4 98 % 1 09/22/20 JLI 70-130% %Bromofluorobenzene 102 % 1 09/22/20 JLI 70-130% % Dibromofluoromethane 93 % 1 09/22/20 JLI 70-130% %Toluene-d8 103 % 1 09/22/20 JLI 70-130% 1,4-dioxane 1,4-dioxane ND 85 ug/kg 1 09/22/20 JLI SW8260C Semivolatiles 1,2,4,5-Tetrachlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2,4-Trichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,2-Diphenylhydrazine ND 340 ug/Kg 1 09/22/20 AW SW8270D 1,3-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 1,4-Dichlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4,5-Trichlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4,6-Trichloropheno) ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dichlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dimethylphenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dinitrophenol ND 340 ug/Kg 1 09/22/20 AW SW8270D 2,4-Dinitrotoluene ND 240 ug/Kg 1 09/22/20 AW SW8270D Ver 1 Page 12 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82053 Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By 2,6-Dinitrotoluene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Chloronaphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Chlorophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Methyl naphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Methylphenol (o-cresol) ND 240 ug/Kg 1 09/22/20 AW SW8270D 2-Nitroaniline ND 340 ug/Kg 1 09/22/20 AW SW8270D 2-Nitrophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 3&4-Methylphenol(m&p-cresol) ND 340 ug/Kg 1 09/22/20 AW SW8270D 3,3'-Dichlorobenzidine ND 240 ug/Kg 1 09/22/20 AW SW8270D 3-Nitroaniline ND 340 ug/Kg 1 09/22/20 AW SW8270D 4,6-Dinitro-2-methyl phenol ND 340 ug/Kg 1 09/22/20 AW SW8270D 4-Bromophenyl phenyl ether ND 340 ug/Kg 1 09/22/20 AW SW8270D 4-Chloro-3-methyl phenol ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Chloroaniline ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Chlorophenyl phenyl ether ND 240 ug/Kg 1 09/22/20 AW SW8270D 4-Nitroaniline ND 540 ug/Kg 1 09/22/20 AW SW8270D 4-Nitrophenol ND 240 ug/Kg 1 09/22/20 AW SW8270D Acenaphthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Acenaphthylene ND 240 ug/Kg 1 09/22/20 AW SW8270D Acetophenone ND 240 ug/Kg 1 09/22/20 AW SW8270D Aniline ND 340 ug/Kg 1 09/22/20 AW SW8270D Anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benz(a)anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzidine ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(a)pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(b)fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(ghi)perylene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzo(k)fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Benzoic acid ND 670 ug/Kg 1 09/22/20 AW SW8270D Benzy) butyl phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroethoxy)methane ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroethyl)ether ND 340 ug/Kg 1 09/22/20 AW SW8270D Bis(2-chloroisopropyl)ether ND 240 ug/Kg 1 09/22/20 AW SW8270D Bis(2-ethylhexyl)phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Carbazole ND 340 ug/Kg 1 09/22/20 AW SW8270D Chrysene ND 240 ug/Kg 1 09/22/20 AW SW8270D Dibenz(a,h)anthracene ND 240 ug/Kg 1 09/22/20 AW SW8270D Dibenzofuran ND 240 ug/Kg 1 09/22/20 AW SW8270D Diethyl phthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Dimethylphthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Di-n-butylphthalate ND 340 ug/Kg 1 09/22/20 AW SW8270D Di-n-octylphthalate ND 240 ug/Kg 1 09/22/20 AW SW8270D Fluoranthene ND 240 ug/Kg 1 09/22/20 AW SW8270D Fluorene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorobutadiene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachlorocyclopentadiene ND 240 ug/Kg 1 09/22/20 AW SW8270D Hexachloroethane ND 240 ug/Kg 1 09/22/20 AW SW8270D Indeno(1,2,3-cd)pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Ver 1 Page 13 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82053 Client ID: EMBANKMENT 2 RL/ Parameter Result PQL Units Dilution Date/Time By Isophorone ND 240 ug/Kg 1 09/22/20 AW SW8270D Naphthalene ND 240 ug/Kg 1 09/22/20 AW SW8270D Nitrobenzene ND 240 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodimethylamine ND 340 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodi-n-propylamine ND 240 ug/Kg 1 09/22/20 AW SW8270D N-Nitrosodiphenylamine ND 340 ug/Kg 1 09/22/20 AW SW8270D Pentachloronitrobenzene ND 340 ug/Kg 1 09/22/20 AW SW8270D Pentachlorophenol ND 340 ug/Kg 1 09/22/20 AW SW8270D Phenanthrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Phenol ND 240 ug/Kg 1 09/22/20 AW SW8270D Pyrene ND 240 ug/Kg 1 09/22/20 AW SW8270D Pyridine ND 340 ug/Kg 1 09/22/20 AW SW8270D QA/QC Surrogates •2,4,6-Tribromophenol 90 % 1 09/22/20 AW 30-130% •2-Fluorobiphenyl 68 % 1 09/22/20 AW 30-130% •2-Fluorophenol 52 % 1 09/22/20 AW 30-130% % Nitrobenzene-d5 55 % 1 09/22/20 AW 30-130% % Phenol-d5 56 % 1 09/22/20 AW 30-130% %Terphenyl-d14 90 % 1 09/22/20 AW 30-130% Field Extraction Completed 09/18/20 SW5035A 1 =This parameter is not certified by the primary accrediting authority(NY NELAC)for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level(Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds(preceeded with a %)added by the lab to determine analysis efficiency. Surrogate results(%)listed in the report are not"detected"compounds. Comments: Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene.Azobenzene is used for the calibration of 1,2-Diphenylhydrazine. The regulatory hold time for pH is immediately.This pH was performed in the laboratory and may be considered outside of hold- time. Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If you are the client above and have any questions concerning this testing,please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. A UL Phyllis hiller, Laboratory Director September 24,2020 Reviewed and Released by: Rashmi Makol, Project Manager Ver 1 Page 14 of 32 PHOU VIX1,-i,3 elz;E01 Y Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 NY#11301 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Kathryn Loddengaard Enviroscience Consultants September 24, 2020 2150 Smithtown Ave Ronkonkoma, NY 11779 Sample Information Custody Information Date Time Matrix: SOIL Collected by: JF 09/18/20 10:35 Location Code: ENV-SCI Received by: B 09/21/20 15:14 Rush Request: 72 Hour Analyzed by: see "By" below P.O.#: Laboratory Data SDG ID: GCG82052 Phoenix ID: CG82054 Project ID: STRONGS YACHT CENTER Client ID: EMBANKMENT GRAB 1 RL/ Parameter Result PQL Units Dilution Date/Time By Reference Volatiles 1,1,1,2-Tetrachloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1,1-Trichloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2,2-Tetrachloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2-Trichloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloropropene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichloropropane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Trichlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Tri methyl benzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromo-3-chloropropane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromoethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloropropane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,3,5-Tri methyl benzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichloropropane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1,4-Dichlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 2,2-Dichloropropane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 2-Chlorotoluene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 2-Hexanone ND 27 ug/Kg 1 09/22/20 JLI SW8260C 2-Isopropyltoluene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 1 4-Chlorotoluene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C 4-Methyl-2-pentanone ND 27 ug/Kg 1 09/22/20 JLI SW8260C Ver 1 Page 15 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82054 Client ID: EMBANKMENT GRAB 1 RL/ Parameter Result PQL Units Dilution Date/Time By Acetone ND 27 ug/Kg 1 09/22/20 JLI SW8260C Acrylonitrile ND 11 ug/Kg 1 09/22/20 JLI SW8260C Benzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Bromobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Bromochloromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Bromodichloromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Bromoform ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Bromomethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Carbon Disulfide ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Carbon tetrachloride ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Chlorobenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Chloroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Chloroform ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Chloromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C cis-1,2-Dichloroethene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C cis-1,3-Dichloropropene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Dibromochloromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Dibromomethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Dichlorodifluoromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Ethylbenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Hexachlorobutadiene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Isopropylbenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C m&p-Xylene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Methyl Ethyl Ketone ND 27 ug/Kg 1 09/22/20 JLI SW8260C Methyl t-butyl ether(MTBE) ND 11 ug/Kg 1 09/22/20 JLI SW8260C Methylene chloride ND 11 ug/Kg 1 09/22/20 JLI SW8260C Naphthalene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C n-Butylbenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C n-Propylbenzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C o-Xylene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C p-Isopropyltoluene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C sec-Butyl benzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Styrene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C tent-Butyl benzene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Tetrachloroethene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Tetrahydrofuran (THF) ND 11 ug/Kg 1 09/22/20 JLI SW8260C Toluene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Total Xylenes ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C trans-1,2-Dichloroethene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C trans-1,3-Dichloropropene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C trans-1,4-dichloro-2-butene ND 11 ug/Kg 1 09/22/20 JLI SW8260C Trichooroethene ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Trichlorofluoromethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Trichlorotrifluoroethane ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C Vinyl chloride ND 5.4 ug/Kg 1 09/22/20 JLI SW8260C QA/QC Surrogates % 1,2-dichlorobenzene-d4 99 % 1 09/22/20 JLI 70-130% %Bromofluorobenzene 102 % 1 09/22/20 JLI 70-130% % Dibromofluoromethane 94 % 1 09/22/20 JLI 70-130% Ver 1 Page 16 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82054 Client ID: EMBANKMENT GRAB 1 RL/ Parameter Result PQL Units Dilution Date/Time By %Toluene-d8 104 % 1 09/22/20 JLI 70-130% 1,4-dioxane 1,4-dioxane ND 81 ug/kg 1 09/22/20 JLI SW8260C Field Extraction Completed 09/18/20 SW5035A 1 =This parameter is not certified by the primary accrediting authority(NY NELAC)for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level(Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds(preceeded with a %)added by the lab to determine analysis efficiency. Surrogate results(%)listed in the report are not"detected"compounds. Comments: Results are reported on an "as received" basis, and are not corrected for dry weight. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If you are the client above and have any questions concerning this testing,please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Phyllis hiller, Laboratory Director September 24,2020 Reviewed and Released by: Rashmi Makol, Project Manager Ver 1 Page 17 of 32 PHOU VIX1,-i,3 elz;E01 Y Environmental Laboratories, Inc. 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 NY#11801 Tel.(860)645-1102 Fax(860)645-0823 Analysis Report FOR: Attn: Kathryn Loddengaard Enviroscience Consultants September 24, 2020 2150 Smithtown Ave Ronkonkoma, NY 11779 Sample Information Custody Information Date Time Matrix: SOIL Collected by: JF 09/18/20 10:40 Location Code: ENV-SCI Received by: B 09/21/20 15:14 Rush Request: 72 Hour Analyzed by: see "By" below P.O.#: Laboratory Data SDG ID: GCG82052 Phoenix ID: CG82055 Project ID: STRONGS YACHT CENTER Client ID: EMBANKMENT GRAB 2 RL/ Parameter Result PQL Units Dilution Date/Time By Reference Volatiles 1,1,1,2-Tetrachloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1,1-Trichloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2,2-Tetrachloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1,2-Trichloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloroethene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,1-Dichloropropene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2,3-Trichloropropane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Trichlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2,4-Tri methyl benzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromo-3-chloropropane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dibromoethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,2-Dichloropropane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,3,5-Tri methyl benzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,3-Dichloropropane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1,4-Dichlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 2,2-Dichloropropane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 2-Chlorotoluene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 2-Hexanone ND 26 ug/Kg 1 09/22/20 JLI SW8260C 2-Isopropyltoluene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 1 4-Chlorotoluene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C 4-Methyl-2-pentanone ND 26 ug/Kg 1 09/22/20 JLI SW8260C Ver 1 Page 18 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82055 Client ID: EMBANKMENT GRAB 2 RL/ Parameter Result PQL Units Dilution Date/Time By Acetone ND 26 ug/Kg 1 09/22/20 JLI SW8260C Acrylonitrile ND 10 ug/Kg 1 09/22/20 JLI SW8260C Benzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Bromobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Bromochloromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Bromodichloromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Bromoform ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Bromomethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Carbon Disulfide ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Carbon tetrachloride ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Chlorobenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Chloroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Chloroform ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Chloromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C cis-1,2-Dichloroethene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C cis-1,3-Dichloropropene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Dibromochloromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Dibromomethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Dichlorodifluoromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Ethylbenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Hexachlorobutadiene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Isopropylbenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C m&p-Xylene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Methyl Ethyl Ketone ND 26 ug/Kg 1 09/22/20 JLI SW8260C Methyl t-butyl ether(MTBE) ND 10 ug/Kg 1 09/22/20 JLI SW8260C Methylene chloride ND 10 ug/Kg 1 09/22/20 JLI SW8260C Naphthalene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C n-Butylbenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C n-Propylbenzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C o-Xylene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C p-Isopropyltoluene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C sec-Butyl benzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Styrene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C tent-Butyl benzene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Tetrachloroethene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Tetrahydrofuran (THF) ND 10 ug/Kg 1 09/22/20 JLI SW8260C Toluene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Total Xylenes ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C trans-1,2-Dichloroethene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C trans-1,3-Dichloropropene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C trans-1,4-dichloro-2-butene ND 10 ug/Kg 1 09/22/20 JLI SW8260C Trichooroethene ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Trichlorofluoromethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Trichlorotrifluoroethane ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C Vinyl chloride ND 5.1 ug/Kg 1 09/22/20 JLI SW8260C QA/QC Surrogates % 1,2-dichlorobenzene-d4 98 % 1 09/22/20 JLI 70-130% %Bromofluorobenzene 102 % 1 09/22/20 JLI 70-130% % Dibromofluoromethane 95 % 1 09/22/20 JLI 70-130% Ver 1 Page 19 of 32 Project ID: STRONGS YACHT CENTER Phoenix I.D.: CG82055 Client ID: EMBANKMENT GRAB 2 RL/ Parameter Result PQL Units Dilution Date/Time By %Toluene-d8 103 % 1 09/22/20 JLI 70-130% 1,4-dioxane 1,4-dioxane ND 77 ug/kg 1 09/22/20 JLI SW8260C Field Extraction Completed 09/18/20 SW5035A 1 =This parameter is not certified by the primary accrediting authority(NY NELAC)for this matrix. NY NELAC does not offer certification for all parameters at this time. RL/PQL=Reporting/Practical Quantitation Level(Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds(preceeded with a %)added by the lab to determine analysis efficiency. Surrogate results(%)listed in the report are not"detected"compounds. Comments: Results are reported on an "as received" basis, and are not corrected for dry weight. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. If you are the client above and have any questions concerning this testing,please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Phyllis hiller, Laboratory Director September 24,2020 Reviewed and Released by: Rashmi Makol, Project Manager Ver 1 Page 20 of 32 PHOENIX x Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester,CT 06045 NY# 11301 � QA/QC Report Tel. (860)645-1102 Fax(860)645-0823 September 24, 2020 QA/QC Data SDG I.D.: GCG82052 Blk Sample Dup Dup LCS LCSD LCS MS MSD MS Rec RPD Parameter Blank RL Result Result RPD % % RPD % % RPD Limits Limits QA/QC Batch 546359(mg/kg),QC Sample No: CG82052 40X(CG82052,CG82053) Chromium Hexavalent - Soil Chromium,Hexavalent BRL 0.40 <0.40 <0.40 NC 102 85-115 30 Chromium, Hexavalent(Ins) 110 99.6 85-115 30 Chromium,Hexavalent(Sol) 93.4 107 85-115 30 QA/QC Batch 546354(mg/kg),QC Sample No: CG81780 2X(CG82052,CG82053) Mercury-Soil BRL 0.03 0.04 0.04 NC 112 111 0.9 87.9 91.0 3.5 70-130 30 Comment: Additional Mercury criteria:LCS acceptance range for waters is 80-120%and for soils is 70-130%. MS acceptance range is 75-125%. QA/QC Batch 546265(mg/kg),QC Sample No: CG81773(CG82052,CG82053) ICP Metals - Soil Arsenic BRL 0.67 1.59 1.76 NC 93.9 88.6 5.8 95.6 75-125 35 Barium BRL 0.33 49.7 53.7 7.70 99.2 93.0 6.5 112 75-125 35 Beryllium BRL 0.27 0.47 0.48 NC 104 96.5 7.5 97.4 75-125 35 Cadmium BRL 0.33 0.58 0.63 NC 99.6 93.3 6.5 95.1 75-125 35 Chromium BRL 0.33 10.9 11.4 4.50 96.5 90.3 6.6 96.8 75-125 35 Copper BRL 0.67 24.4 27.5 11.9 94.6 85.5 10.1 95.6 75-125 35 Lead BRL 0.33 25.7 30.8 18.1 90.9 85.9 5.7 96.0 75-125 35 Manganese BRL 0.33 237 249 4.90 97.1 90.3 7.3 95.2 75-125 35 Nickel BRL 0.33 9.02 9.78 8.10 104 97.4 6.6 96.9 75-125 35 Selenium BRL 1.3 <1.3 <1.5 NC 95.3 88.1 7.9 96.5 75-125 35 Silver BRL 0.33 <0.32 <0.38 NC 83.1 78.1 6.2 95.0 75-125 35 Zinc BRL 0.67 38.3 43.2 12.0 95.2 90.4 5.2 97.6 75-125 35 Comment: Additional Criteria:LCS acceptance range is 80-120%MS acceptance range 75-125%. Page 21 of 32 PHOENIX x Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester,CT 06045 NY# 11301 � QA/QC Report Tel. (860)645-1102 Fax(860)645-0823 September 24, 2020 QA/QC Data SDG I.D.: GCG82052 Blk Sample Dup Dup LCS LCSD LCS MS MSD MS Rec RPD Parameter Blank RL Result Result RPD % % RPD % % RPD Limits Limits QA/QC Batch 546439(mg/Kg),QC Sample No: CG82052 38.5X(CG82052, CG82053) Total Cyanide(SW9010C Distill.) BRL 0.38 <0.57 <0.57 NC 97.0 112 80-120 30 Comment: Additional:LCS acceptance range is 80-120%for soils MS acceptance range 75-125%for soils QA/QC Batch 546326(PH), QC Sample No: CG81590(CG82052,CG82053) pH at 25C-Soil 8.23 8.20 0.40 100 85-115 20 Page 22 of 32 PHOENIX x Environmental Laboratories, Inc. 587 East Middle Turnpike, P.O.Box 370, Manchester,CT 06045 NY# 11301 � QA/QC Report Tel. (860)645-1102 Fax(860)645-0823 September 24, 2020 QA/QC Data SDG I.D.: GCG82052 Blk LCS LCSD LCS MS MSD MS Rec RPD Parameter Blank RL % % RPD % % RPD Limits Limits QA/QC Batch 546246(ug/Kg),QC Sample No: CG82052 1 OX(CG82052,CG82053) Chlorinated Herbicides - Soil 2,4,5-T ND 130 76 80 5.1 67 81 18.9 40-140 30 2,4,5-TP(Silvex) ND 130 74 75 1.3 65 79 19.4 40-140 30 2,4-D ND 250 73 77 5.3 68 86 23.4 40-140 30 2,4-DB ND 2500 67 65 3.0 59 80 30.2 40-140 30 Dalapon ND 130 69 69 0.0 52 54 3.8 40-140 30 Dicamba ND 130 88 88 0.0 78 81 3.8 40-140 30 Dichloroprop ND 130 73 75 2.7 60 82 31.0 40-140 30 Dinoseb ND 130 100 81 21.0 88 91 3.4 40-140 30 •DCAA(Surrogate Rec) 52 % 52 56 7.4 47 59 22.6 30-150 30 •DCAA(Surrogate Rec)(Confirm 52 % 49 53 7.8 44 55 22.2 30-150 30 Comment: Additional criteria:LCS acceptance range is 40-140%MS acceptance range 30-150%. QA/QC Batch 546220(ug/Kg),QC Sample No: CG82046 2X(CG82052,CG82053) Polychlorinated Biphenyls - Soil PCB-1016 ND 33 73 75 2.7 66 73 10.1 40-140 30 PCB-1221 ND 33 40-140 30 PCB-1232 ND 33 40-140 30 PCB-1242 ND 33 40-140 30 PCB-1248 ND 33 40-140 30 PCB-1254 ND 33 40-140 30 PCB-1260 ND 33 72 90 22.2 78 86 9.8 40-140 30 PCB-1262 ND 33 40-140 30 PCB-1268 ND 33 40-140 30 %DCBP(Surrogate Rec) 80 % 74 86 15.0 76 85 11.2 30-150 30 %DCBP(Surrogate Rec)(Confirm 78 % 74 86 15.0 81 87 7.1 30-150 30 %TCMX(Surrogate Rec) 77 % 76 80 5.1 68 78 13.7 30-150 30 %TCMX(Surrogate Rec)(Confirm 76 % 74 81 9.0 74 81 9.0 30-150 30 QA/QC Batch 546232(ug/Kg),QC Sample No: CG82046 2X(CG82052,CG82053) Pesticides - Soil 4,4'-DDD ND 1.7 89 82 8.2 84 85 1.2 40-140 30 4,4'-DDE ND 1.7 117 91 25.0 95 89 6.5 40-140 30 4,4'-DDT ND 1.7 77 73 5.3 74 75 1.3 40-140 30 a-BHC ND 1.0 74 66 11.4 70 74 5.6 40-140 30 a-Chlordane ND 3.3 71 66 7.3 68 69 1.5 40-140 30 Aldrin ND 1.0 72 66 8.7 71 71 0.0 40-140 30 b-BHC ND 1.0 109 100 8.6 104 122 15.9 40-140 30 Chlordane ND 33 77 72 6.7 73 75 2.7 40-140 30 d-BHC ND 3.3 85 78 8.6 80 82 2.5 40-140 30 Dieldrin ND 1.0 71 65 8.8 67 69 2.9 40-140 30 Endosulfan I ND 3.3 55 60 8.7 61 68 10.9 40-140 30 Page 23 of 32 QA/QC Data SDGiD.: GCG82052 Y6 � am LCS LCSo LCS MS MSD MS Rec nPD Parameter Blank nL m % nPD % % RPD Limits umnu enuovvKanx wo 3.3 7/ 73 5.3 /3 75 2J *o 1*o uo enuovuxanauhate wo 3.3 90 88 22 80 97 7.5 40 1*o zm enunn wo 3.3 72 07 72 08 09 1�5 w» 1*o xo enunoamohyoe wo 3.3 90 86 4.5 88 90 8.7 w» 1*o xo Endnnxomno wo 33 100 87 19.7 82 87 5.8 w» 1*o xo g'oHC wo 1.0 75 08 8.3 73 81 10.4 w» 1*o xo g~Cxlo"duno wo 33 77 72 0.7 73 75 2.7 w» 1*o xo Heptachlor wo 33 08 03 9.1 07 08 2.8 w» 1*o xo Heptachlor epoxide wo 33 74 08 8.5 09 71 2.8 w» 1*o xo mmhoxvcx|o, wo 33 88 82 8.2 104 108 3.8 w» 1*o xo Toxupmene wo 130 mx mx NC wx mx NC 40-1*0 uo •oCoP 75 % 78 74 0.5 72 73 1.4 uo 1su uo •oCeP(Cormnnauinn) 82 % 82 78 3.7 70 78 2.0 uo 1su uo •TCMx 71 % 07 00 1t0 00 08 3.0 uo 1su uo •TCMX(Corfinnm|un) 78 % 73 70 42 70 71 1A uo 1su uo O/VUC Batch 5463O4(ug/kg).UC Sample No: CG822O8(CG82052.CG82O53) 1.2.4.5,etrachmmvenzene wo 230 00 03 4.7 03 73 14.7 *o 1*u uo 1.2.4Tncxwmbonzono wo 230 ux 53 3.7 58 07 12.7 40 1*o zm 1.2'o|cmomueozene wo 180 43 39 8.8 51 59 14.5 40 1*o xo / 1.2'o|vhenymyuramne wo 230 81 72 11�8 70 92 27.2 40 1*o xo 1.3'oiomombenzene wo 230 38 30 8.0 49 55 11.5 40 1*o xo / 1.4'oiomombenzene wo 230 41 37 10.3 50 58 10.5 40 1*o xo / 2.4.5'T,iomompxono| wo 230 84 70 10.0 73 85 15.2 40 1*o xo 2.4.0'T,iomompxono| wo 130 82 70 15.8 71 85 17.9 xo 1uo xo 2.4'oiomomphono| wo 130 05 03 3.1 03 73 14.7 xo 1xo xo 2.4'oimetxy|p»ono| wo 230 71 08 2.9 05 75 14.3 xn 1xo xo 2.4'oinumphono| wo 230 00 54 20.0 57 03 10.0 30-130 uu 2.4'oinunxo|"one wo 130 93 81 13.8 75 87 14.8 uo 1uo uu 2.0'oinunxo|"ene wo 130 88 78 13.2 72 87 18.9 *o 14u uu 2'Cmomnavhma|one wo 230 73 00 10.1 07 80 17.7 *o 14u uu 2'Cx|omphono| wo 230 54 49 8.7 58 00 129 uo 1uo uu 2'Mmhymavmha|ene wo 230 01 57 0.8 00 09 14.0 40 14u uu 2'Mmhy|vhonv|(o'cmso; wo 230 58 54 7.1 58 72 18.8 40 14u uu 2'wnmani|ino wo 330 152 132 14A 110 129 15.9 40 wu uu / 2-wnmvxenv| wo 230 80 80 0.0 81 90 10.5 40 1*o uu 3&4Mmhy|vhono|(m&p-cmso) wo 230 03 58 8.3 04 75 15.8 xo 1m xo 3.3'-Dich|umbonzmmo wo 130 87 82 5.9 00 80 182 40 1wo m 3'Nnmanmno wo 330 84 75 1t3 57 72 23.3 40 1wo m 4.0'oinum-2+nemy|pmonol wo 230 78 07 15.2 03 08 9.1 xo 1m m 4-ommophyny|phenyl ether wo 230 80 82 4.8 70 87 13.5 40 1wo m 4-Cxlom-3'metxy|pxono| wo 230 80 70 5.1 71 82 14.4 xo 1m m 4-Cxlomunmno wo 230 74 71 4.1 53 02 15.7 40 1wo m 4-Cxlompxony|phenyl ether wo 230 80 73 10.4 73 84 14.0 40 1wo m 4-whmonmno wo 230 97 80 12.0 81 90 10.9 40 1wo m 4-wumpmeno| wo 230 97 88 8.0 88 105 17.0 30-130 uu xoynupmmyny wo 230 78 08 13.5 70 82 15.8 uo 1uu uu xoynupmmyleny wo 130 73 05 11.0 05 81 21.9 *o 1*u uu *cetopmunono wo 230 x/ 52 82 01 73 17.9 *o 1*u uu Aniline wo 330 43 41 4.8 40 45 11.8 40 1*u uu *omooene wo 230 80 74 7.8 70 86 20.5 *o 1*o uu oonz(a)anmmcene wo 230 90 82 8.3 88 103 15.7 *o 1*u uu Page n4o,32 QA/QC Data SDGiD.: GCG82052 Y6 � am LCS LCSo LCS MS MSD MS Rec nPD Parameter Blank nL m % nPD % % RPD Limits umnu aonziume wo 330 58 51 118 ^10 <10 NC *o 1*o uo M aonzo(a)pymno wo 130 93 84 102 82 102 21.7 40 1*o zm aonzo(u)8uoonmone wo 100 107 97 8.8 88 124 234 40 1*o xo aonzo(gm)very|ono wo 230 84 74 123 00 9/ 38.0 40 1*o xo , oonzo(Nnuoranmene wo 230 70 04 9.0 00 81 20.4 40 1*o xo Benzoic Acid wo 070 70 43 47.8 00 03 4.8 xo 1uo xo , oonzy|butyl phthalate wo 230 97 88 8.0 82 98 17.8 40 1*o xo ois(o'cmomethoxy)met»ano wo 230 58 50 3.5 50 03 11.8 40 1*o xo ois(o'cmomethyVo,xe, wo 130 41 30 13.0 43 52 18.9 40 1*o xo / ois(o'cmomisnpmpyVathy, wo 230 42 38 10.0 45 53 10.3 40 1*o xo / ois(o'atxymyxy;pxmalate wo 230 99 90 9.5 80 101 10.0 40-140 uu Cu,buzn|o wo 230 82 75 8.9 07 81 18.9 40 14u uu Chryoeno wo 230 88 81 8.3 82 100 19.8 *o 14u uu omonz(a.h)anmmoene wo 130 90 81 10.5 75 99 27.0 40 14u uu omonzwfunon wo 230 79 08 15.0 08 80 10.2 *o 14u uu Diethyl phthalate wo 230 94 83 12A 77 90 15.0 *o 14u uu o|momy|vmxa|aoo wo 230 90 80 1t8 73 87 17.5 *o 14u uu o|-nbuty|phmvlate wo 070 91 89 12 75 90 18.2 *o 14u uu o|-nooty|pmxalate wo 230 108 90 1t8 83 97 15.0 *o 14u uu F|uomnmene wo 230 81 77 5.1 83 98 10.0 40 14n xo Hvnmne wo 230 83 72 142 72 86 17.7 40 14o xo *oxaomumoonzono wo 130 94 90 4.3 81 98 18.0 40 14o xo Hoxoomombumdiono wo 230 00 57 5.1 04 73 13.1 40 14o xo Hoxoomomnyn|nponmdiono wo 230 58 57 3.4 39 35 10.8 40 14o xo M Hoxoomomomono wo 130 40 42 9.1 55 03 13.0 40 14o xo |ndeno(1.2.3'od)pynene wo 230 87 78 10.8 00 93 34.0 40 14o xo , |sopxomno wo 130 01 57 0.8 57 04 11.0 40 14o xo mapmxu|ono wo 230 54 50 7.7 50 05 14.9 40 14o xo Nitrobenzene wo 130 00 54 10.5 03 75 17.4 40-1*0 uu m'witmsodimo/xy|umine wo 230 uo 18 14.0 20 30 14.3 40 1*u uu /'m m'witmsodi'n'pmpy|ammo wo 130 04 58 8.1 05 74 12.9 40 1*u uu m-mitmsumvhony|amino wo 130 88 77 13.3 72 84 154 40 1*u uu Pnnmomumnumuonzvnv wo 230 101 94 7.2 87 100 13.9 40 1*u uu Ponmomumvhonv| wo 230 87 81 7.1 74 90 18.5 uo 1uu uu Pxenvnmmno wo 130 79 74 0.5 78 89 13.2 *o 1*u uu Phenol wo 230 xx 51 7.5 nO 73 22.9 uo 1uu uu Pymne wo 230 80 70 5.1 78 99 225 uo 1uu uu Pyridine wo 230 19 17 11A 22 24 8.7 40 14n xo •2.4.0'Tnummvpoenv| 112 % 103 97 0.0 83 111 17.0 xo 1xo xo •2'F|uomuipxnny| 75 % 08 02 8.2 03 74 10.1 xo 1xo xo •o'nuompxono| 51 % 44 40 9.5 50 54 7.7 xo 1xo xo •wumhonzono'd5 05 % 58 53 10.7 02 72 14.9 xn 1xo xo •Phynn|'d5 01 % 54 50 7.7 50 00 10.4 xn 1xo xo •Tymoony|'d14 92 % 88 84 5.8 08 88 20.8 xn 1xo xo Comment: Additional 8270 criteria:20%of compounds can be outside of acceptance criteria as long as recovery isau least 1Ov6 (Acid surrogates acceptance range for aqueous samples: 15'11Ov6.for soils 3O'13Ov6) OAJOC Batch 546302(ug/kg).UC Sample No: CG81774(CG82O52.CG82O53. CG82O54.CG82O55) Volatiles - Soil (Low Level) 1.1.1.2'rmracmommxane wo 5.0 101 107 5.8 ro 1uo uo 1.1.1Tncxwmehano wo 5.0 86 93 7.8 70-130 uo 1.1.2.2-Teraohmmomane wo 3.0 93 101 82 70-130 uo Page 25 of 32 QA/QC Data SDGiD.: GCG82052 Y6 � am LCS LCSo LCS MS MSD MS Rec nPD Parameter Blank nL m % nPD % % RPD Limits umnu 1.1.2-T rich wmemane wo 5.0 95 102 71 70-130 uo 1.1-Dichmmothane wo 5.0 82 89 82 m 130 30 1.1+nchmmomeoe wo 5.0 78 82 5.0 /o 1xo xo 1.1'o|chmmvmvene wo 5.0 88 96 8.7 /o 1xo xo 1.o.3-T rich lombynzeny wo 5.0 88 95 0.5 /o 1xo xo 1.o.3-T rich lompmpono wo 5.0 82 88 8.2 /o 1xo xo 1.o.4-T rich lombynzyny wo 5.0 87 94 7.7 /o 1xo xo 1.o.4-T rim ethyl benzene wo 1.0 88 90 7.0 /o 1xo xo 1.2'oibmm*3-uhbmpmpune wo 5.0 111 120 7.8 /o 1xo xo 1.2'oibmmnomune wo 5.0 90 104 8.0 /o 1xo xo 1.2'oio»lombenzene wo 5.0 88 84 5.5 70-130 uo 1.2'oio»lomomune wo 5.0 80 93 7.8 70-130 uo 1.2'oio»lompmpune wo 5.0 87 84 7.7 70-130 uo 1.3.nTnm ethyl benzene wo to 89 95 0.5 70-130 uo 1.3'D|chmmuenzene wo 5.0 91 97 0.4 70-130 uo 1.3'D|chmmvmvane wo 5.0 91 98 7.4 70-130 uo 1/-D|chmmuenzene wo 5.0 89 04 55 70-130 uo 1,4-dwxane wo 100 85 96 112 70-130 uo 2.2'o|chmmvmvane wo 5.0 87 93 6.7 70-130 uo 2'Cxwmm|ueoe wo 5.0 91 97 0.4 /o 1xo zm 2'ooxanono wo 25 125 131 4.7 /o 1xo xo / 2'1sovmpykn|uene wo 5.0 99 105 5.8 /o 1xo xo 4-Cxlomm|uene wo 5.0 90 90 0.5 /o 1xo xo 4-Mymy1-2-pontanone wo 25 92 98 7.3 /o 1xo xo Acetone wo 10 130 142 4.3 /o 1xo xo / xorykmmile wo 5.0 88 95 7.7 /o 1xo xo Benzene wo 1.0 91 98 7.4 /o 1xo xo ommobonzono wo 5.0 91 90 5.3 /o 1xo xo ommoohlommomane wo 5.0 91 90 5.3 70-130 uo ommodicxlommethono wo 5.0 90 103 7.0 70-130 uo ommofonn wo 5.0 105 111 5.0 70-130 uo ammomethano wo 5.0 80 89 10J 70-130 uo Carbon Disulfide wo 5.0 77 82 0.3 70-130 uo Carbon tetrachloride wo 5.0 88 04 0.0 70-130 uo Chhmuenznnv wo 5.0 92 98 0.3 70-130 uo Chwmemanv wo 5.0 80 89 10J 70-130 uo Chloroform wo 5.0 84 92 8.1 70-130 uo Chwmmemanv wo 5.0 80 88 8.5 /0130 zm cis-1.2'D|m`lomomene wo 5.0 82 88 7.1 /o 1xo xo cis-1.3-o|u`lomvmpene wo 5.0 92 99 7.3 /o 1xo xo oibmmochlommymano wo 3.0 100 110 9.0 /o 1xo xo oibmmomethono wo 5.0 88 95 0.5 /o 1xo xo oiox|omdmuommomane wo 5.0 105 112 0.5 /o 1xo xo Ethy|bonzono wo 1.0 93 98 0.3 /o 1xo xo Hexeoxlombmediemo wo 5.0 84 98 4.2 /o 1xo xo mopmpy|bonzono wo 1.0 91 90 5.3 /o 1xo xo m&p'xy|ono wo 2.0 92 98 0.3 70-130 uo Methyl ethyl ketone wo 5.0 132 142 7.3 70-130 uo / Methyl t-uut/|ether(MTee) wo to 73 79 7.8 70-130 uo Methylene chloride wo 5.0 05 71 8.8 70-130 uo / Naphthalene wo 5.0 95 102 7.1 70-130 uo n-Buty|beozene wo 1�0 90 97 7.5 70-130 uo n-Pmpy|benzene wo 1�0 91 97 0.4 70-130 uo Page noo,32 QA/QC Data SDGiD.: GCG82052 Y6 � am LCS LCSo LCS MS MSD MS Rec nPD Parameter Blank nL m % nPD % % RPD Limits umnu o-Xylene wo M 95 101 0.1 m 1uo uo p-movmpynomene wo 1�0 93 99 0.3 /o 1xo zm sec-nmy|ueozene wo 1�0 98 105 0.8 /o 1xo xo Styrene wo 5.0 95 102 7.1 /0130 xo tert-omy|benzeno wo 1.0 92 97 5.3 /o 1xo xo netmoxlomoxyny wo 5.0 98 103 5.0 /o 1xo xo netmxydmfuran(THr) wo 5.0 80 80 7.2 /o 1xo xo Toluene wo 1.0 95 101 0.1 /o 1xo xo trano~1.2-Dxox|omohyny wo 5.0 78 84 7.4 /o 1xo xo trans~1.3-oicmnmpmp*no wo 5.0 93 100 7.3 /o 1xo xo trans~1.4-dinxlom-2'bmono wo 5.0 108 117 8.0 70-130 uo Tmumomyhene wo 5.0 92 98 7.3 70-130 uo Tmumnmnuommymano wo 5.0 80 88 9.5 70-130 uo Tncmou*mUvnmehano wo 5.0 78 82 5.0 70-130 uo Vinyl chloride wo 5.0 83 91 8.2 70-130 uo • 1.2u|un|omu*nzono-d4 87 % 99 99 0.0 70-130 uo •BmmuMuombonzono 104 % 104 103 1.0 70-130 uo •0umm"Uunmmethane 80 % 103 101 2.0 70-130 uo •Tmuoneu8 103 % 100 101 1.0 70-130 uo Comment: The Low Level MSxwSo are not reported for this batch. Additional 8260 criteria: 10%of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery isw0-10Ov6.u5'1OOv6for cmomsthen*HL and Tnomnmn"ommethano'*L. |=This parameter is outside laboratory LCS/LCSo specified recovery limits. m=This parameter i*outside laboratory MS/mSo specified recovery limits. ,=This parameter is outside laboratory Rro specified recovery limits. If there are any questions regarding this data, please call Phoenix Client Services at extension 200. RPD'Relative Percent Difference LCS' Laboratory Control Sample LCSD- Laboratory Control Sample Duplicate MS- Matrix Spike Phyllisi||er. Laboratory Director MS Oup- Matrix Spike Duplicate 7 Soptomber24. 2O2O NC No Criteria |ntf- Interference Page nro,3m Thursday,September 24,2020 Sample Criteria Exceedances Report Criteria: None GCG82052 - ENV-SCI State: NY RL Analysis SampNo Acode Phoenix Analyte Criteria Result RL Criteria Criteria Units ***No Data to Display*** Phoenix Laboratories does not assume responsibility for the data contained in this exceedance report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data(obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance. Page 28 of 32 t AG € PHOEVIX Mmmbl qt Environmental Laboratories, Inc. NY 11301 w 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Comments September 24, 2020 SDG I.D.: GCG82052 The following analysis comments are made regarding exceptions to criteria not already noted in the Analysis Report or QA/QC Report: Herbicide Narration AU-ECD12 09/22/20-1: CG82052,CG82053 The following Continuing Calibration compounds did not meet%deviation criteria: Samples:CG82052,CG82053 Preceding CC 922BO15-2,4,5-T(11)22%H(15%), Dalapon(1)27%H(15%), Dinoseb 17%H(15%) Succeeding CC 922BO27-None. PCB Narration AU-ECD8 09/22/20-1: CG82053 The following Continuing Calibration compounds did not meet%deviation criteria: Samples:CG82053 Preceding CC 922BO37-TCMX SURR 18%L(15%) Succeeding CC 922BO49-None. PEST Narration AU-ECD7 09/22/20-1: CG82052,CG82053 The following Continuing Calibration compounds did not meet%deviation criteria: Samples:CG82052,CG82053 Preceding CC 922AO31 -b-BHC 21%L(20%),Endrin 21%L(20%) Succeeding CC 922AO38-Endrin 22%L(20%) A low"W'standard was run after the samples to demonstrate capability to detect any compounds outside of the CC acceptance criteria. All reported samples were ND for the affected compounds. SVOA Narration CHEM07 09/21/20-2: CG82052,CG82053 For 8270 full list,the DDT breakdown and pentachlorophenol&benzidine peak tailing were evaluated in the DFTPP tune and were found to be in control. For 8270 BN list, benzidine peak tailing was evaluated in the DFTPP tune and was found to be in control. The following Initial Calibration compounds did not meet recommended response factors:2-Nitrophenol 0.073(0.1), Hexachlorobenzene 0.084 (0.1) The following Initial Calibration compounds did not meet minimum response factors: None. The following Continuing Calibration compounds did not meet recommended response factors:2-Nitrophenol 0.075(0.1), Hexachlorobenzene 0.089(0.1) The following Continuing Calibration compounds did not meet minimum response factors: None. Up to eight compounds can be outside of ICAL%RSD criteria and up to sixteen compounds can be outside of CCAL%Dev criteria if less than 40%. VOA Narration CHEM03 09/21/20-2: CG82052,CG82053,CG82054,CG82055 Page 29 of 32 PHOEVIX Mmmbl qt Environmental Laboratories, Inc. NY 11301 w 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 Analysis Comments September 24, 2020 SDG I.D.: GCG82052 The following Initial Calibration compounds did not meet RSD%criteria: 1,1,1,2-Tetrachloroethane 21%(20%), 1,2-Dibromo-3-chloropropane 26%(20%), Bromoform 34%(20%),Chloroethane 22%(20%), Dibromochloromethane 23%(20%),trans-1,4-dichloro-2-butene 35%(20%) The following Initial Calibration compounds did not meet maximum RSD%criteria: None. The following Initial Calibration compounds did not meet recommended response factors: 1,2-Dibromo-3-chloropropane 0.049(0.05), Bromoform 0.069(0.1),Tetrachloroethene 0.126(0.2) The following Initial Calibration compounds did not meet minimum response factors: 1,2-Dibromo-3-chloropropane 0.049(0.05) Up to eight compounds can be outside of ICAO%RSD criteria and up to sixteen compounds can be outside of CCAL%Dev criteria if less than 40%. Page 30 of 32 ig AC O,9 PHOENJX ,,';I� rya ', tF Environmental Laboratories, Inc. 'NY#11301 587 East Middle Turnpike,P.O.Box 370,Manchester,CT 06045 Tel.(860)645-1102 Fax(860)645-0823 NY Temperature Narration September 24, 2020 SDG I.D.: GCG82052 The samples in this delivery group were received at 2.0°C. (Note acceptance criteria for relevant matrices is above freezing up to 6°C) Page 31 of 32 S� SP ❑ O O A q� u /�1 4p Ga J m V m W rn , O00 OpSf let:, S'c'`"p ��P� tL 'S v `„ oS i y c iL ro o a O i 4 2 m ¢ aO1i Q a In o_ — Sc, o Y . 0 ► �s's !�4 f�0��d ❑ ❑ ❑ ❑ Elv �Jyf bf f°s�f s�y� a a = m aEi c d Sb oo� �sb o F a o U p U2y �O/ JJ°?b0 b�0 � O 2 O hi Ql �'Pr ��ti O N O -O zO c 00 v ou� cnmN ° vUiv vUi � cn a -c m E Py, aGi !i° O a. to rcu) m 'nN p ° t- a. LL LU a� 'PSG S+, O U Cl) M� M U CO O N ❑❑❑ fi o° J ~ 'o !° m M SrA M m V ':.� _m D m O 0 O O � U CD El O E °Q ZE Cl) mO U v o v Z10 ❑ ❑ El Ela UJ (D,D o v � � � W �� C 010 T �. T T fT6 N 6 tV0 N L O R D U O. W ca (N C) 0 LL Ix O sm+ Z co �Cy F❑❑❑^ULJ❑ '� G Ll El Z m o " aTL IL O uoi to �s . c� p cn O a � � oa .. so m � wui o Q CL ° °' a�i o .� � l �� r ~ N N = LU �C s- > � m o- a cs Q V o a> a G U c m }C K w Z z a a � � as kk ❑ ❑ ❑ ❑ Z v, E o cn p " � 0 Z a w `` E rd o 3-- Lij >. tip E Z a° f m CL O o o X n ' p E a w n C7 m o N C3� m ❑ ❑ ❑ o �f m cmi 1 m 7 El U) d u a Ci m C E C y N E 'O CC N L o Ve cmi m N o E Eli w } ' m Z u L m Oat a Q E � y ?y y W m N O xOWO ZQ a ° c rc u n u m N c E <( E .4 m U cncn 0it0 a — --------Page-32-a€