Loading...
The URL can be used to link to this page
Your browser does not support the video tag.
Home
My WebLink
About
(4) Soil Analytics
ENVIROSCIENCE CONSULTANTS, INC. 2150 SMITHTOWN AVENUE, RONKONKOMA, NY 11779 (631) 580-3191 FAX 580-3195 www.envirohealth.org C Figure 1 Sample Locations Soil Sampling Strong’s Yacht Center Mattituck, NY Area of Embankment Sample 1 and Embankment Grab 1 Area of Embankment Sample 2 and Embankment Grab 2 Table 1 Soil Chemical Analytical Results Strongs Yacht Center September 18, 2020 Page 1 of 1 Sample Location Embankment 1 Grab (VOCs only) Embankment 2 Grab (VOCs only) Embankment 1 Embankment 2 NYSDEC Unrestricted Use SCO NYSDEC Residential Use SCO NYSDEC Protection of Groundwater SCO Barium NA NA 3.95 1.96 350 350 820 Chromium NA NA 1.31 1.34 30 36 NS Copper NA NA 1.40 1.50 50 270 1,720 Lead NA NA 0.50 0.48 63 400 450 Manganese NA NA 26.2 11.6 1,600 2,000 2,000 Nickel NA NA 0.56 0.82 30 140 130 Zinc NA NA 1.50 1.50 109 2,200 2,480 Notes: Only detected metals are summarized in this table. No VOC’s were detected in any of the samples. NS = Not specified NA = Not Analyzed SCO = Soil Cleanup Objective CG82052 - CG82055 Thursday, September 24, 2020 Sample ID#s: Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 SDG ID:GCG82052 Project ID:STRONGS YACHT CENTER Sincerely yours, Laboratory Director Phyllis Shiller If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. NELAC - #NY11301 CT Lab Registration #PH-0618 MA Lab Registration #M-CT007 ME Lab Registration #CT-007 NH Lab Registration #213693-A,B NJ Lab Registration #CT-003 NY Lab Registration #11301 PA Lab Registration #68-03530 RI Lab Registration #63 UT Lab Registration #CT00007 VT Lab Registration #VT11301 This laboratory is in compliance with the NELAC requirements of procedures used except where indicated. This report contains results for the parameters tested, under the sampling conditions described on the Chain Of Custody, as received by the laboratory. This report is incomplete unless all pages indicated in the pagination at the bottom of the page are included. A scanned version of the COC form accompanies the analytical report and is an exact duplicate of the original. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. 587 East Middle Turnpike, P.O. Box 370, Manchester, CT 06040 Telephone (860) 645-1102 Fax (860) 645-0823 Page 1 of 32 Sample Id Cross Reference September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 Client Id Lab Id Matrix Project ID:STRONGS YACHT CENTER EMBANKMENT 1 CG82052 SOIL EMBANKMENT 2 CG82053 SOIL EMBANKMENT GRAB 1 CG82054 SOIL EMBANKMENT GRAB 2 CG82055 SOIL Page 2 of 32 Sample Information Custody Information Matrix: Location Code: Rush Request: P.O.#: Collected by: Received by: Analyzed by: SOIL ENV-SCI 72 Hour 09/18/20 B see "By" below JF Laboratory Data EMBANKMENT 1 Phoenix ID:CG82052 09/21/20 10:25 15:14 Parameter Result RL/ PQL Units Date/Time By Reference FOR:Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 Analysis Report September 24, 2020 Date Time SDG ID:GCG82052 Client ID: Project ID:STRONGS YACHT CENTER Dilution 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. < 0.34Silver 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 0.67Arsenic 0.67 09/22/20 EK SW6010Dmg/Kg 1 3.95Barium 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 0.27Beryllium 0.27 09/22/20 EK SW6010Dmg/Kg 1 < 0.34Cadmium 0.34 09/22/20 EK SW6010Dmg/Kg 1 1.31Chromium 0.34 09/22/20 EK SW6010Dmg/Kg 1 1.4Copper 0.7 09/22/20 EK SW6010Dmg/kg 1 < 0.03Mercury 0.03 09/22/20 RS SW7471Bmg/Kg 2 26.2Manganese 0.34 09/22/20 EK SW6010Dmg/Kg 1 0.56Nickel 0.34 09/22/20 EK SW6010Dmg/Kg 1 0.50Lead 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 1.3Selenium 1.3 09/22/20 EK SW6010Dmg/Kg 1 1.31Trivalent Chromium 0.34 09/22/20 CALC 6010-7196mg/kg 1 1.5Zinc 0.7 09/22/20 EK SW6010Dmg/Kg 1 98Percent Solid 09/21/20 CJ SW846-%Solid% < 0.40Chromium, Hex. (SW3060 digestion)0.40 09/22/20 ARG SW7196Amg/Kg 1 4.64pH at 25C - Soil 1.00 09/21/20 20:48 AP SW846 9045DpH Units 11 -23.3Redox Potential 09/21/20 AP SM2580B-09mV 11 < 0.57Total Cyanide (SW9010C Distill.)0.57 09/23/20 EG SW9012Bmg/Kg 1 CompletedMercury Digestion 09/22/20 AW/VTSW7471B CompletedSoil Extraction for Herbicide 09/21/20 J/D SW3550C CompletedSoil Extraction for PCB 09/21/20 L/A/ESW3545A CompletedSoil Extraction for Pesticides 09/21/20 L/A/ESW3545A CompletedSoil Extraction for SVOA 09/21/20 R/E SW3546 CompletedTotal Metals Digest 09/21/20 B/AG SW3050B Chlorinated Herbicides ND2,4,5-T 130 09/22/20 JRB SW8151Aug/Kg 10 Ver 1 Page 3 of 32 EMBANKMENT 1 Phoenix I.D.:CG82052 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution ND2,4,5-TP (Silvex)130 09/22/20 JRB SW8151Aug/Kg 10 ND2,4-D 250 09/22/20 JRB SW8151Aug/Kg 10 ND2,4-DB 2500 09/22/20 JRB SW8151Aug/Kg 10 NDDalapon 130 09/22/20 JRB SW8151Aug/Kg 10 NDDicamba 130 09/22/20 JRB SW8151Aug/Kg 10 NDDichloroprop 250 09/22/20 JRB SW8151Aug/Kg 10 NDDinoseb 250 09/22/20 JRB SW8151Aug/Kg 10 QA/QC Surrogates 54% DCAA 09/22/20 JRB 30 - 150 %%10 42% DCAA (Confirmation)09/22/20 JRB 30 - 150 %%10 Polychlorinated Biphenyls NDPCB-1016 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1221 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1232 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1242 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1248 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1254 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1260 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1262 330 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1268 330 09/22/20 SC SW8082Aug/Kg 10 QA/QC Surrogates 133% DCBP 09/22/20 SC 30 - 150 %%10 122% DCBP (Confirmation)09/22/20 SC 30 - 150 %%10 101% TCMX 09/22/20 SC 30 - 150 %%10 97% TCMX (Confirmation)09/22/20 SC 30 - 150 %%10 Pesticides - Soil ND4,4' -DDD 2.0 09/22/20 CG SW8081Bug/Kg 2 ND4,4' -DDE 2.0 09/22/20 CG SW8081Bug/Kg 2 ND4,4' -DDT 2.0 09/22/20 CG SW8081Bug/Kg 2 NDa-BHC 6.6 09/22/20 CG SW8081Bug/Kg 2 NDa-Chlordane 3.3 09/22/20 CG SW8081Bug/Kg 2 NDAldrin 3.3 09/22/20 CG SW8081Bug/Kg 2 NDb-BHC 6.6 09/22/20 CG SW8081Bug/Kg 2 NDChlordane 33 09/22/20 CG SW8081Bug/Kg 2 NDd-BHC 6.6 09/22/20 CG SW8081Bug/Kg 2 NDDieldrin 3.3 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan I 6.6 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan II 6.6 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan sulfate 6.6 09/22/20 CG SW8081Bug/Kg 2 NDEndrin 6.6 09/22/20 CG SW8081Bug/Kg 2 NDEndrin aldehyde 6.6 09/22/20 CG SW8081Bug/Kg 2 NDEndrin ketone 6.6 09/22/20 CG SW8081Bug/Kg 2 NDg-BHC 1.3 09/22/20 CG SW8081Bug/Kg 2 NDg-Chlordane 3.3 09/22/20 CG SW8081Bug/Kg 2 NDHeptachlor 6.6 09/22/20 CG SW8081Bug/Kg 2 NDHeptachlor epoxide 6.6 09/22/20 CG SW8081Bug/Kg 2 NDMethoxychlor 33 09/22/20 CG SW8081Bug/Kg 2 NDToxaphene 130 09/22/20 CG SW8081Bug/Kg 2 Ver 1 Page 4 of 32 EMBANKMENT 1 Phoenix I.D.:CG82052 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution QA/QC Surrogates 76% DCBP 09/22/20 CG 30 - 150 %%2 82% DCBP (Confirmation)09/22/20 CG 30 - 150 %%2 73% TCMX 09/22/20 CG 30 - 150 %%2 78% TCMX (Confirmation)09/22/20 CG 30 - 150 %%2 Volatiles ND1,1,1,2-Tetrachloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1,1-Trichloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1,2,2-Tetrachloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1,2-Trichloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloropropene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichloropropane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trichlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trimethylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromo-3-chloropropane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromoethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2-Dichlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloropropane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,3,5-Trimethylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,3-Dichlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,3-Dichloropropane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND1,4-Dichlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND2,2-Dichloropropane 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND2-Chlorotoluene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND2-Hexanone 30 09/21/20 JLI SW8260Cug/Kg 1 ND2-Isopropyltoluene 6.0 09/21/20 JLI SW8260Cug/Kg 11 ND4-Chlorotoluene 6.0 09/21/20 JLI SW8260Cug/Kg 1 ND4-Methyl-2-pentanone 30 09/21/20 JLI SW8260Cug/Kg 1 NDAcetone 30 09/21/20 JLI SW8260Cug/Kg 1 NDAcrylonitrile 12 09/21/20 JLI SW8260Cug/Kg 1 NDBenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDBromobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDBromochloromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDBromodichloromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDBromoform 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDBromomethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDCarbon Disulfide 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDCarbon tetrachloride 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDChlorobenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDChloroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDChloroform 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDChloromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDcis-1,2-Dichloroethene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDcis-1,3-Dichloropropene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDDibromochloromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 Ver 1 Page 5 of 32 EMBANKMENT 1 Phoenix I.D.:CG82052 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDDibromomethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDDichlorodifluoromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDEthylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDHexachlorobutadiene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDIsopropylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDm&p-Xylene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDMethyl Ethyl Ketone 30 09/21/20 JLI SW8260Cug/Kg 1 NDMethyl t-butyl ether (MTBE)12 09/21/20 JLI SW8260Cug/Kg 1 NDMethylene chloride 12 09/21/20 JLI SW8260Cug/Kg 1 NDNaphthalene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDn-Butylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDn-Propylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDo-Xylene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDp-Isopropyltoluene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDsec-Butylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDStyrene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDtert-Butylbenzene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDTetrachloroethene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDTetrahydrofuran (THF)12 09/21/20 JLI SW8260Cug/Kg 1 NDToluene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDTotal Xylenes 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDtrans-1,2-Dichloroethene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDtrans-1,3-Dichloropropene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDtrans-1,4-dichloro-2-butene 12 09/21/20 JLI SW8260Cug/Kg 1 NDTrichloroethene 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDTrichlorofluoromethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDTrichlorotrifluoroethane 6.0 09/21/20 JLI SW8260Cug/Kg 1 NDVinyl chloride 6.0 09/21/20 JLI SW8260Cug/Kg 1 QA/QC Surrogates 99% 1,2-dichlorobenzene-d4 09/21/20 JLI 70 - 130 %%1 102% Bromofluorobenzene 09/21/20 JLI 70 - 130 %%1 96% Dibromofluoromethane 09/21/20 JLI 70 - 130 %%1 103% Toluene-d8 09/21/20 JLI 70 - 130 %%1 1,4-dioxane ND1,4-dioxane 90 09/21/20 JLI SW8260Cug/kg 1 Semivolatiles ND1,2,4,5-Tetrachlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2,4-Trichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2-Diphenylhydrazine 340 09/22/20 AW SW8270Dug/Kg 1 ND1,3-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,4-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4,5-Trichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4,6-Trichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dimethylphenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dinitrophenol 340 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dinitrotoluene 240 09/22/20 AW SW8270Dug/Kg 1 Ver 1 Page 6 of 32 EMBANKMENT 1 Phoenix I.D.:CG82052 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution ND2,6-Dinitrotoluene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Chloronaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Chlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Methylnaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Methylphenol (o-cresol)240 09/22/20 AW SW8270Dug/Kg 1 ND2-Nitroaniline 340 09/22/20 AW SW8270Dug/Kg 1 ND2-Nitrophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND3&4-Methylphenol (m&p-cresol)340 09/22/20 AW SW8270Dug/Kg 1 ND3,3'-Dichlorobenzidine 240 09/22/20 AW SW8270Dug/Kg 1 ND3-Nitroaniline 340 09/22/20 AW SW8270Dug/Kg 1 ND4,6-Dinitro-2-methylphenol 340 09/22/20 AW SW8270Dug/Kg 1 ND4-Bromophenyl phenyl ether 340 09/22/20 AW SW8270Dug/Kg 1 ND4-Chloro-3-methylphenol 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Chloroaniline 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Chlorophenyl phenyl ether 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Nitroaniline 540 09/22/20 AW SW8270Dug/Kg 1 ND4-Nitrophenol 240 09/22/20 AW SW8270Dug/Kg 1 NDAcenaphthene 240 09/22/20 AW SW8270Dug/Kg 1 NDAcenaphthylene 240 09/22/20 AW SW8270Dug/Kg 1 NDAcetophenone 240 09/22/20 AW SW8270Dug/Kg 1 NDAniline 340 09/22/20 AW SW8270Dug/Kg 1 NDAnthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenz(a)anthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzidine 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(a)pyrene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(b)fluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(ghi)perylene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(k)fluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzoic acid 670 09/22/20 AW SW8270Dug/Kg 1 NDBenzyl butyl phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroethoxy)methane 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroethyl)ether 340 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroisopropyl)ether 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-ethylhexyl)phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDCarbazole 340 09/22/20 AW SW8270Dug/Kg 1 NDChrysene 240 09/22/20 AW SW8270Dug/Kg 1 NDDibenz(a,h)anthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDDibenzofuran 240 09/22/20 AW SW8270Dug/Kg 1 NDDiethyl phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDDimethylphthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDDi-n-butylphthalate 340 09/22/20 AW SW8270Dug/Kg 1 NDDi-n-octylphthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDFluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDFluorene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorobutadiene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorocyclopentadiene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachloroethane 240 09/22/20 AW SW8270Dug/Kg 1 NDIndeno(1,2,3-cd)pyrene 240 09/22/20 AW SW8270Dug/Kg 1 Ver 1 Page 7 of 32 EMBANKMENT 1 Phoenix I.D.:CG82052 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDIsophorone 240 09/22/20 AW SW8270Dug/Kg 1 NDNaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 NDNitrobenzene 240 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodimethylamine 340 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodi-n-propylamine 240 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodiphenylamine 340 09/22/20 AW SW8270Dug/Kg 1 NDPentachloronitrobenzene 340 09/22/20 AW SW8270Dug/Kg 1 NDPentachlorophenol 340 09/22/20 AW SW8270Dug/Kg 1 NDPhenanthrene 240 09/22/20 AW SW8270Dug/Kg 1 NDPhenol 240 09/22/20 AW SW8270Dug/Kg 1 NDPyrene 240 09/22/20 AW SW8270Dug/Kg 1 NDPyridine 340 09/22/20 AW SW8270Dug/Kg 1 QA/QC Surrogates 95% 2,4,6-Tribromophenol 09/22/20 AW 30 - 130 %%1 72% 2-Fluorobiphenyl 09/22/20 AW 30 - 130 %%1 54% 2-Fluorophenol 09/22/20 AW 30 - 130 %%1 56% Nitrobenzene-d5 09/22/20 AW 30 - 130 %%1 58% Phenol-d5 09/22/20 AW 30 - 130 %%1 95% Terphenyl-d14 09/22/20 AW 30 - 130 %%1 CompletedField Extraction 09/18/20 SW5035A 1 Comments: Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine. The regulatory hold time for pH is immediately. This pH was performed in the laboratory and may be considered outside of hold- time. Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. Phyllis Shiller, Laboratory Director September 24, 2020 1 = This parameter is not certified by the primary accrediting authority (NY NELAC) for this matrix. NY NELAC does not offer certification for all parameters at this time. If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Reviewed and Released by: Rashmi Makol, Project Manager RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds. Ver 1 Page 8 of 32 Sample Information Custody Information Matrix: Location Code: Rush Request: P.O.#: Collected by: Received by: Analyzed by: SOIL ENV-SCI 72 Hour 09/18/20 B see "By" below JF Laboratory Data EMBANKMENT 2 Phoenix ID:CG82053 09/21/20 10:30 15:14 Parameter Result RL/ PQL Units Date/Time By Reference FOR:Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 Analysis Report September 24, 2020 Date Time SDG ID:GCG82052 Client ID: Project ID:STRONGS YACHT CENTER Dilution 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. < 0.34Silver 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 0.69Arsenic 0.69 09/22/20 EK SW6010Dmg/Kg 1 1.96Barium 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 0.27Beryllium 0.27 09/22/20 EK SW6010Dmg/Kg 1 < 0.34Cadmium 0.34 09/22/20 EK SW6010Dmg/Kg 1 1.34Chromium 0.34 09/22/20 EK SW6010Dmg/Kg 1 1.5Copper 0.7 09/22/20 EK SW6010Dmg/kg 1 < 0.03Mercury 0.03 09/22/20 RS SW7471Bmg/Kg 2 11.6Manganese 0.34 09/22/20 EK SW6010Dmg/Kg 1 0.82Nickel 0.34 09/22/20 EK SW6010Dmg/Kg 1 0.48Lead 0.34 09/22/20 EK SW6010Dmg/Kg 1 < 1.4Selenium 1.4 09/22/20 EK SW6010Dmg/Kg 1 1.34Trivalent Chromium 0.34 09/22/20 CALC 6010-7196mg/kg 1 1.5Zinc 0.7 09/22/20 EK SW6010Dmg/Kg 1 97Percent Solid 09/21/20 CJ SW846-%Solid% < 0.38Chromium, Hex. (SW3060 digestion)0.38 09/22/20 ARG SW7196Amg/Kg 1 4.73pH at 25C - Soil 1.00 09/21/20 20:48 AP SW846 9045DpH Units 11 81.9Redox Potential 09/21/20 AP SM2580B-09mV 11 < 0.43Total Cyanide (SW9010C Distill.)0.43 09/23/20 EG SW9012Bmg/Kg 1 CompletedMercury Digestion 09/22/20 AW/VTSW7471B CompletedSoil Extraction for Herbicide 09/21/20 J/D SW3550C CompletedSoil Extraction for PCB 09/21/20 L/A/ESW3545A CompletedSoil Extraction for Pesticides 09/21/20 L/A/ESW3545A CompletedSoil Extraction for SVOA 09/21/20 R/E SW3546 CompletedTotal Metals Digest 09/21/20 B/AG SW3050B Chlorinated Herbicides ND2,4,5-T 130 09/22/20 JRB SW8151Aug/Kg 10 Ver 1 Page 9 of 32 EMBANKMENT 2 Phoenix I.D.:CG82053 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution ND2,4,5-TP (Silvex)130 09/22/20 JRB SW8151Aug/Kg 10 ND2,4-D 260 09/22/20 JRB SW8151Aug/Kg 10 ND2,4-DB 2600 09/22/20 JRB SW8151Aug/Kg 10 NDDalapon 130 09/22/20 JRB SW8151Aug/Kg 10 NDDicamba 130 09/22/20 JRB SW8151Aug/Kg 10 NDDichloroprop 260 09/22/20 JRB SW8151Aug/Kg 10 NDDinoseb 260 09/22/20 JRB SW8151Aug/Kg 10 QA/QC Surrogates 53% DCAA 09/22/20 JRB 30 - 150 %%10 51% DCAA (Confirmation)09/22/20 JRB 30 - 150 %%10 Polychlorinated Biphenyls NDPCB-1016 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1221 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1232 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1242 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1248 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1254 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1260 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1262 340 09/22/20 SC SW8082Aug/Kg 10 NDPCB-1268 340 09/22/20 SC SW8082Aug/Kg 10 QA/QC Surrogates 93% DCBP 09/22/20 SC 30 - 150 %%10 98% DCBP (Confirmation)09/22/20 SC 30 - 150 %%10 82% TCMX 09/22/20 SC 30 - 150 %%10 87% TCMX (Confirmation)09/22/20 SC 30 - 150 %%10 Pesticides - Soil ND4,4' -DDD 2.0 09/22/20 CG SW8081Bug/Kg 2 ND4,4' -DDE 2.0 09/22/20 CG SW8081Bug/Kg 2 ND4,4' -DDT 2.0 09/22/20 CG SW8081Bug/Kg 2 NDa-BHC 6.7 09/22/20 CG SW8081Bug/Kg 2 NDa-Chlordane 3.4 09/22/20 CG SW8081Bug/Kg 2 NDAldrin 3.4 09/22/20 CG SW8081Bug/Kg 2 NDb-BHC 6.7 09/22/20 CG SW8081Bug/Kg 2 NDChlordane 34 09/22/20 CG SW8081Bug/Kg 2 NDd-BHC 6.7 09/22/20 CG SW8081Bug/Kg 2 NDDieldrin 3.4 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan I 6.7 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan II 6.7 09/22/20 CG SW8081Bug/Kg 2 NDEndosulfan sulfate 6.7 09/22/20 CG SW8081Bug/Kg 2 NDEndrin 6.7 09/22/20 CG SW8081Bug/Kg 2 NDEndrin aldehyde 6.7 09/22/20 CG SW8081Bug/Kg 2 NDEndrin ketone 6.7 09/22/20 CG SW8081Bug/Kg 2 NDg-BHC 1.3 09/22/20 CG SW8081Bug/Kg 2 NDg-Chlordane 3.4 09/22/20 CG SW8081Bug/Kg 2 NDHeptachlor 6.7 09/22/20 CG SW8081Bug/Kg 2 NDHeptachlor epoxide 6.7 09/22/20 CG SW8081Bug/Kg 2 NDMethoxychlor 34 09/22/20 CG SW8081Bug/Kg 2 NDToxaphene 130 09/22/20 CG SW8081Bug/Kg 2 Ver 1 Page 10 of 32 EMBANKMENT 2 Phoenix I.D.:CG82053 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution QA/QC Surrogates 79% DCBP 09/22/20 CG 30 - 150 %%2 64% DCBP (Confirmation)09/22/20 CG 30 - 150 %%2 77% TCMX 09/22/20 CG 30 - 150 %%2 73% TCMX (Confirmation)09/22/20 CG 30 - 150 %%2 Volatiles ND1,1,1,2-Tetrachloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,1-Trichloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2,2-Tetrachloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2-Trichloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloropropene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichloropropane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trichlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trimethylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromo-3-chloropropane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromoethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloropropane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,3,5-Trimethylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichloropropane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND1,4-Dichlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND2,2-Dichloropropane 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND2-Chlorotoluene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND2-Hexanone 28 09/22/20 JLI SW8260Cug/Kg 1 ND2-Isopropyltoluene 5.7 09/22/20 JLI SW8260Cug/Kg 11 ND4-Chlorotoluene 5.7 09/22/20 JLI SW8260Cug/Kg 1 ND4-Methyl-2-pentanone 28 09/22/20 JLI SW8260Cug/Kg 1 NDAcetone 28 09/22/20 JLI SW8260Cug/Kg 1 NDAcrylonitrile 11 09/22/20 JLI SW8260Cug/Kg 1 NDBenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDBromobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDBromochloromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDBromodichloromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDBromoform 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDBromomethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon Disulfide 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon tetrachloride 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDChlorobenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDChloroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDChloroform 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDChloromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,2-Dichloroethene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,3-Dichloropropene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDDibromochloromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 Ver 1 Page 11 of 32 EMBANKMENT 2 Phoenix I.D.:CG82053 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDDibromomethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDDichlorodifluoromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDEthylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDHexachlorobutadiene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDIsopropylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDm&p-Xylene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl Ethyl Ketone 28 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl t-butyl ether (MTBE)11 09/22/20 JLI SW8260Cug/Kg 1 NDMethylene chloride 11 09/22/20 JLI SW8260Cug/Kg 1 NDNaphthalene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDn-Butylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDn-Propylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDo-Xylene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDp-Isopropyltoluene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDsec-Butylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDStyrene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDtert-Butylbenzene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDTetrachloroethene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDTetrahydrofuran (THF)11 09/22/20 JLI SW8260Cug/Kg 1 NDToluene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDTotal Xylenes 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,2-Dichloroethene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,3-Dichloropropene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,4-dichloro-2-butene 11 09/22/20 JLI SW8260Cug/Kg 1 NDTrichloroethene 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorofluoromethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorotrifluoroethane 5.7 09/22/20 JLI SW8260Cug/Kg 1 NDVinyl chloride 5.7 09/22/20 JLI SW8260Cug/Kg 1 QA/QC Surrogates 98% 1,2-dichlorobenzene-d4 09/22/20 JLI 70 - 130 %%1 102% Bromofluorobenzene 09/22/20 JLI 70 - 130 %%1 93% Dibromofluoromethane 09/22/20 JLI 70 - 130 %%1 103% Toluene-d8 09/22/20 JLI 70 - 130 %%1 1,4-dioxane ND1,4-dioxane 85 09/22/20 JLI SW8260Cug/kg 1 Semivolatiles ND1,2,4,5-Tetrachlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2,4-Trichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,2-Diphenylhydrazine 340 09/22/20 AW SW8270Dug/Kg 1 ND1,3-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND1,4-Dichlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4,5-Trichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4,6-Trichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dichlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dimethylphenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dinitrophenol 340 09/22/20 AW SW8270Dug/Kg 1 ND2,4-Dinitrotoluene 240 09/22/20 AW SW8270Dug/Kg 1 Ver 1 Page 12 of 32 EMBANKMENT 2 Phoenix I.D.:CG82053 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution ND2,6-Dinitrotoluene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Chloronaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Chlorophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Methylnaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 ND2-Methylphenol (o-cresol)240 09/22/20 AW SW8270Dug/Kg 1 ND2-Nitroaniline 340 09/22/20 AW SW8270Dug/Kg 1 ND2-Nitrophenol 240 09/22/20 AW SW8270Dug/Kg 1 ND3&4-Methylphenol (m&p-cresol)340 09/22/20 AW SW8270Dug/Kg 1 ND3,3'-Dichlorobenzidine 240 09/22/20 AW SW8270Dug/Kg 1 ND3-Nitroaniline 340 09/22/20 AW SW8270Dug/Kg 1 ND4,6-Dinitro-2-methylphenol 340 09/22/20 AW SW8270Dug/Kg 1 ND4-Bromophenyl phenyl ether 340 09/22/20 AW SW8270Dug/Kg 1 ND4-Chloro-3-methylphenol 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Chloroaniline 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Chlorophenyl phenyl ether 240 09/22/20 AW SW8270Dug/Kg 1 ND4-Nitroaniline 540 09/22/20 AW SW8270Dug/Kg 1 ND4-Nitrophenol 240 09/22/20 AW SW8270Dug/Kg 1 NDAcenaphthene 240 09/22/20 AW SW8270Dug/Kg 1 NDAcenaphthylene 240 09/22/20 AW SW8270Dug/Kg 1 NDAcetophenone 240 09/22/20 AW SW8270Dug/Kg 1 NDAniline 340 09/22/20 AW SW8270Dug/Kg 1 NDAnthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenz(a)anthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzidine 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(a)pyrene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(b)fluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(ghi)perylene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzo(k)fluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDBenzoic acid 670 09/22/20 AW SW8270Dug/Kg 1 NDBenzyl butyl phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroethoxy)methane 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroethyl)ether 340 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-chloroisopropyl)ether 240 09/22/20 AW SW8270Dug/Kg 1 NDBis(2-ethylhexyl)phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDCarbazole 340 09/22/20 AW SW8270Dug/Kg 1 NDChrysene 240 09/22/20 AW SW8270Dug/Kg 1 NDDibenz(a,h)anthracene 240 09/22/20 AW SW8270Dug/Kg 1 NDDibenzofuran 240 09/22/20 AW SW8270Dug/Kg 1 NDDiethyl phthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDDimethylphthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDDi-n-butylphthalate 340 09/22/20 AW SW8270Dug/Kg 1 NDDi-n-octylphthalate 240 09/22/20 AW SW8270Dug/Kg 1 NDFluoranthene 240 09/22/20 AW SW8270Dug/Kg 1 NDFluorene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorobenzene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorobutadiene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachlorocyclopentadiene 240 09/22/20 AW SW8270Dug/Kg 1 NDHexachloroethane 240 09/22/20 AW SW8270Dug/Kg 1 NDIndeno(1,2,3-cd)pyrene 240 09/22/20 AW SW8270Dug/Kg 1 Ver 1 Page 13 of 32 EMBANKMENT 2 Phoenix I.D.:CG82053 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDIsophorone 240 09/22/20 AW SW8270Dug/Kg 1 NDNaphthalene 240 09/22/20 AW SW8270Dug/Kg 1 NDNitrobenzene 240 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodimethylamine 340 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodi-n-propylamine 240 09/22/20 AW SW8270Dug/Kg 1 NDN-Nitrosodiphenylamine 340 09/22/20 AW SW8270Dug/Kg 1 NDPentachloronitrobenzene 340 09/22/20 AW SW8270Dug/Kg 1 NDPentachlorophenol 340 09/22/20 AW SW8270Dug/Kg 1 NDPhenanthrene 240 09/22/20 AW SW8270Dug/Kg 1 NDPhenol 240 09/22/20 AW SW8270Dug/Kg 1 NDPyrene 240 09/22/20 AW SW8270Dug/Kg 1 NDPyridine 340 09/22/20 AW SW8270Dug/Kg 1 QA/QC Surrogates 90% 2,4,6-Tribromophenol 09/22/20 AW 30 - 130 %%1 68% 2-Fluorobiphenyl 09/22/20 AW 30 - 130 %%1 52% 2-Fluorophenol 09/22/20 AW 30 - 130 %%1 55% Nitrobenzene-d5 09/22/20 AW 30 - 130 %%1 56% Phenol-d5 09/22/20 AW 30 - 130 %%1 90% Terphenyl-d14 09/22/20 AW 30 - 130 %%1 CompletedField Extraction 09/18/20 SW5035A 1 Comments: Per 1.4.6 of EPA method 8270D, 1,2-Diphenylhydrazine is unstable and readily converts to Azobenzene. Azobenzene is used for the calibration of 1,2-Diphenylhydrazine. The regulatory hold time for pH is immediately. This pH was performed in the laboratory and may be considered outside of hold- time. Hexavalent Chromium: This sample is in a reducing state. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. Phyllis Shiller, Laboratory Director September 24, 2020 1 = This parameter is not certified by the primary accrediting authority (NY NELAC) for this matrix. NY NELAC does not offer certification for all parameters at this time. If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Reviewed and Released by: Rashmi Makol, Project Manager RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds. Ver 1 Page 14 of 32 Sample Information Custody Information Matrix: Location Code: Rush Request: P.O.#: Collected by: Received by: Analyzed by: SOIL ENV-SCI 72 Hour 09/18/20 B see "By" below JF Laboratory Data EMBANKMENT GRAB 1 Phoenix ID:CG82054 09/21/20 10:35 15:14 Parameter Result RL/ PQL Units Date/Time By Reference FOR:Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 Analysis Report September 24, 2020 Date Time SDG ID:GCG82052 Client ID: Project ID:STRONGS YACHT CENTER Dilution 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. Volatiles ND1,1,1,2-Tetrachloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,1-Trichloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2,2-Tetrachloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2-Trichloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloropropene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichloropropane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trichlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trimethylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromo-3-chloropropane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromoethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloropropane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,3,5-Trimethylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichloropropane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND1,4-Dichlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND2,2-Dichloropropane 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND2-Chlorotoluene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND2-Hexanone 27 09/22/20 JLI SW8260Cug/Kg 1 ND2-Isopropyltoluene 5.4 09/22/20 JLI SW8260Cug/Kg 11 ND4-Chlorotoluene 5.4 09/22/20 JLI SW8260Cug/Kg 1 ND4-Methyl-2-pentanone 27 09/22/20 JLI SW8260Cug/Kg 1 Ver 1 Page 15 of 32 EMBANKMENT GRAB 1 Phoenix I.D.:CG82054 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDAcetone 27 09/22/20 JLI SW8260Cug/Kg 1 NDAcrylonitrile 11 09/22/20 JLI SW8260Cug/Kg 1 NDBenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDBromobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDBromochloromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDBromodichloromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDBromoform 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDBromomethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon Disulfide 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon tetrachloride 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDChlorobenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDChloroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDChloroform 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDChloromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,2-Dichloroethene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,3-Dichloropropene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDDibromochloromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDDibromomethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDDichlorodifluoromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDEthylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDHexachlorobutadiene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDIsopropylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDm&p-Xylene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl Ethyl Ketone 27 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl t-butyl ether (MTBE)11 09/22/20 JLI SW8260Cug/Kg 1 NDMethylene chloride 11 09/22/20 JLI SW8260Cug/Kg 1 NDNaphthalene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDn-Butylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDn-Propylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDo-Xylene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDp-Isopropyltoluene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDsec-Butylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDStyrene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDtert-Butylbenzene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDTetrachloroethene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDTetrahydrofuran (THF)11 09/22/20 JLI SW8260Cug/Kg 1 NDToluene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDTotal Xylenes 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,2-Dichloroethene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,3-Dichloropropene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,4-dichloro-2-butene 11 09/22/20 JLI SW8260Cug/Kg 1 NDTrichloroethene 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorofluoromethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorotrifluoroethane 5.4 09/22/20 JLI SW8260Cug/Kg 1 NDVinyl chloride 5.4 09/22/20 JLI SW8260Cug/Kg 1 QA/QC Surrogates 99% 1,2-dichlorobenzene-d4 09/22/20 JLI 70 - 130 %%1 102% Bromofluorobenzene 09/22/20 JLI 70 - 130 %%1 94% Dibromofluoromethane 09/22/20 JLI 70 - 130 %%1 Ver 1 Page 16 of 32 EMBANKMENT GRAB 1 Phoenix I.D.:CG82054 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution 104% Toluene-d8 09/22/20 JLI 70 - 130 %%1 1,4-dioxane ND1,4-dioxane 81 09/22/20 JLI SW8260Cug/kg 1 CompletedField Extraction 09/18/20 SW5035A 1 Comments: Results are reported on an ``as received`` basis, and are not corrected for dry weight. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. Phyllis Shiller, Laboratory Director September 24, 2020 1 = This parameter is not certified by the primary accrediting authority (NY NELAC) for this matrix. NY NELAC does not offer certification for all parameters at this time. If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Reviewed and Released by: Rashmi Makol, Project Manager RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds. Ver 1 Page 17 of 32 Sample Information Custody Information Matrix: Location Code: Rush Request: P.O.#: Collected by: Received by: Analyzed by: SOIL ENV-SCI 72 Hour 09/18/20 B see "By" below JF Laboratory Data EMBANKMENT GRAB 2 Phoenix ID:CG82055 09/21/20 10:40 15:14 Parameter Result RL/ PQL Units Date/Time By Reference FOR:Attn: Kathryn Loddengaard Enviroscience Consultants 2150 Smithtown Ave Ronkonkoma, NY 11779 Analysis Report September 24, 2020 Date Time SDG ID:GCG82052 Client ID: Project ID:STRONGS YACHT CENTER Dilution 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. Volatiles ND1,1,1,2-Tetrachloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,1-Trichloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2,2-Tetrachloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1,2-Trichloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloroethene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,1-Dichloropropene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,3-Trichloropropane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trichlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2,4-Trimethylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromo-3-chloropropane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dibromoethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,2-Dichloropropane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,3,5-Trimethylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,3-Dichloropropane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND1,4-Dichlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND2,2-Dichloropropane 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND2-Chlorotoluene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND2-Hexanone 26 09/22/20 JLI SW8260Cug/Kg 1 ND2-Isopropyltoluene 5.1 09/22/20 JLI SW8260Cug/Kg 11 ND4-Chlorotoluene 5.1 09/22/20 JLI SW8260Cug/Kg 1 ND4-Methyl-2-pentanone 26 09/22/20 JLI SW8260Cug/Kg 1 Ver 1 Page 18 of 32 EMBANKMENT GRAB 2 Phoenix I.D.:CG82055 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution NDAcetone 26 09/22/20 JLI SW8260Cug/Kg 1 NDAcrylonitrile 10 09/22/20 JLI SW8260Cug/Kg 1 NDBenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDBromobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDBromochloromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDBromodichloromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDBromoform 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDBromomethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon Disulfide 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDCarbon tetrachloride 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDChlorobenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDChloroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDChloroform 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDChloromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,2-Dichloroethene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDcis-1,3-Dichloropropene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDDibromochloromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDDibromomethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDDichlorodifluoromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDEthylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDHexachlorobutadiene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDIsopropylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDm&p-Xylene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl Ethyl Ketone 26 09/22/20 JLI SW8260Cug/Kg 1 NDMethyl t-butyl ether (MTBE)10 09/22/20 JLI SW8260Cug/Kg 1 NDMethylene chloride 10 09/22/20 JLI SW8260Cug/Kg 1 NDNaphthalene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDn-Butylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDn-Propylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDo-Xylene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDp-Isopropyltoluene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDsec-Butylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDStyrene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDtert-Butylbenzene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDTetrachloroethene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDTetrahydrofuran (THF)10 09/22/20 JLI SW8260Cug/Kg 1 NDToluene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDTotal Xylenes 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,2-Dichloroethene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,3-Dichloropropene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDtrans-1,4-dichloro-2-butene 10 09/22/20 JLI SW8260Cug/Kg 1 NDTrichloroethene 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorofluoromethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDTrichlorotrifluoroethane 5.1 09/22/20 JLI SW8260Cug/Kg 1 NDVinyl chloride 5.1 09/22/20 JLI SW8260Cug/Kg 1 QA/QC Surrogates 98% 1,2-dichlorobenzene-d4 09/22/20 JLI 70 - 130 %%1 102% Bromofluorobenzene 09/22/20 JLI 70 - 130 %%1 95% Dibromofluoromethane 09/22/20 JLI 70 - 130 %%1 Ver 1 Page 19 of 32 EMBANKMENT GRAB 2 Phoenix I.D.:CG82055 Client ID: STRONGS YACHT CENTERProject ID: Parameter Result RL/ PQL Units Date/Time ByDilution 103% Toluene-d8 09/22/20 JLI 70 - 130 %%1 1,4-dioxane ND1,4-dioxane 77 09/22/20 JLI SW8260Cug/kg 1 CompletedField Extraction 09/18/20 SW5035A 1 Comments: Results are reported on an ``as received`` basis, and are not corrected for dry weight. All soils, solids and sludges are reported on a dry weight basis unless otherwise noted in the sample comments. Phyllis Shiller, Laboratory Director September 24, 2020 1 = This parameter is not certified by the primary accrediting authority (NY NELAC) for this matrix. NY NELAC does not offer certification for all parameters at this time. If you are the client above and have any questions concerning this testing, please do not hesitate to contact Phoenix Client Services at ext.200. The contents of this report cannot be discussed with anyone other than the client listed above without their written consent. Reviewed and Released by: Rashmi Makol, Project Manager RL/PQL=Reporting/Practical Quantitation Level (Equivalent to NELAC LOQ, Limit of Quantitation) ND=Not Detected at RL/PQL BRL=Below Reporting Level L=Biased Low QA/QC Surrogates: Surrogates are compounds (preceeded with a %) added by the lab to determine analysis efficiency. Surrogate results(%) listed in the report are not "detected" compounds. Ver 1 Page 20 of 32 QA/QC Data Parameter BlkBlank RL MS%MSD%MSRPD QA/QC Report September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 LCS%DupRPD LCSD%LCSRPD %RecLimits %RPDLimitsSampleResultDupResult QA/QC Batch 546359 (mg/kg), QC Sample No: CG82052 40X (CG82052, CG82053) Chromium, Hexavalent - Soil Chromium, Hexavalent BRL 102NC 85 - 115 30<0.40 <0.400.40 Chromium, Hexavalent (Ins)99.6110 85 - 115 30 Chromium, Hexavalent (Sol)10793.4 85 - 115 30 QA/QC Batch 546354 (mg/kg), QC Sample No: CG81780 2X (CG82052, CG82053) Mercury - Soil 87.9 91.0BRL 3.5112NC1110.9 70 - 130 300.04 0.040.03 Additional Mercury criteria: LCS acceptance range for waters is 80-120% and for soils is 70-130%. MS acceptance range is 75-125%. Comment: QA/QC Batch 546265 (mg/kg), QC Sample No: CG81773 (CG82052, CG82053) ICP Metals - Soil Arsenic 95.6BRL93.9NC 88.6 5.8 75 - 125 351.59 1.760.67 Barium 112BRL99.27.70 93.0 6.5 75 - 125 3549.7 53.70.33 Beryllium 97.4BRL104NC96.5 7.5 75 - 125 350.47 0.480.27 Cadmium 95.1BRL99.6NC 93.3 6.5 75 - 125 350.58 0.630.33 Chromium 96.8BRL96.54.50 90.3 6.6 75 - 125 3510.9 11.40.33 Copper 95.6BRL94.611.9 85.5 10.1 75 - 125 3524.4 27.50.67 Lead 96.0BRL90.918.1 85.9 5.7 75 - 125 3525.7 30.80.33 Manganese 95.2BRL97.14.90 90.3 7.3 75 - 125 352372490.33 Nickel 96.9BRL1048.10 97.4 6.6 75 - 125 359.02 9.780.33 Selenium 96.5BRL95.3NC 88.1 7.9 75 - 125 35<1.3 <1.51.3 Silver 95.0BRL83.1NC 78.1 6.2 75 - 125 35<0.32 <0.380.33 Zinc 97.6BRL95.212.0 90.4 5.2 75 - 125 3538.3 43.20.67 Additional Criteria: LCS acceptance range is 80-120% MS acceptance range 75-125%. Comment: Page 21 of 32 QA/QC Data Parameter BlkBlank RL MS%MSD%MSRPD QA/QC Report September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 LCS%DupRPD LCSD%LCSRPD %RecLimits %RPDLimitsSampleResultDupResult QA/QC Batch 546439 (mg/Kg), QC Sample No: CG82052 38.5X (CG82052, CG82053) Total Cyanide (SW9010C Distill.)112BRL97.0NC 80 - 120 30<0.57 <0.570.38 Additional: LCS acceptance range is 80-120% for soils MS acceptance range 75-125% for soils Comment: QA/QC Batch 546326 (PH), QC Sample No: CG81590 (CG82052, CG82053) pH at 25C - Soil 1000.40 85 - 115 208.23 8.20 Page 22 of 32 QA/QC Data Parameter BlkBlank RL MS%MSD%MSRPD QA/QC Report September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 LCS%LCSD%LCSRPD %RecLimits %RPDLimits QA/QC Batch 546246 (ug/Kg), QC Sample No: CG82052 10X (CG82052, CG82053) Chlorinated Herbicides - Soil 2,4,5-T 67 81ND 18.976805.1 40 - 140 30130 2,4,5-TP (Silvex)65 79ND 19.474751.3 40 - 140 30130 2,4-D 68 86ND 23.473775.3 40 - 140 30250 2,4-DB 59 80ND 30.267653.0 40 - 140 302500 Dalapon 52 54ND 3.869690.0 40 - 140 30130 Dicamba 78 81ND 3.888880.0 40 - 140 30130 Dichloroprop 60 82ND 31.073752.7 r40 - 140 30130 Dinoseb 88 91ND 3.41008121.0 40 - 140 30130 % DCAA (Surrogate Rec)47 5952 22.652567.4 30 - 150 30% % DCAA (Surrogate Rec) (Confirm 44 5552 22.249537.8 30 - 150 30% Additional criteria: LCS acceptance range is 40-140% MS acceptance range 30-150%. Comment: QA/QC Batch 546220 (ug/Kg), QC Sample No: CG82046 2X (CG82052, CG82053) Polychlorinated Biphenyls - Soil PCB-1016 66 73ND 10.173752.7 40 - 140 3033 PCB-1221 ND 40 - 140 3033 PCB-1232 ND 40 - 140 3033 PCB-1242 ND 40 - 140 3033 PCB-1248 ND 40 - 140 3033 PCB-1254 ND 40 - 140 3033 PCB-1260 78 86ND 9.8729022.2 40 - 140 3033 PCB-1262 ND 40 - 140 3033 PCB-1268 ND 40 - 140 3033 % DCBP (Surrogate Rec)76 8580 11.2748615.0 30 - 150 30% % DCBP (Surrogate Rec) (Confirm 81 8778 7.1748615.0 30 - 150 30% % TCMX (Surrogate Rec)68 7877 13.776805.1 30 - 150 30% % TCMX (Surrogate Rec) (Confirm 74 8176 9.074819.0 30 - 150 30% QA/QC Batch 546232 (ug/Kg), QC Sample No: CG82046 2X (CG82052, CG82053) Pesticides - Soil 4,4' -DDD 84 85ND 1.289828.2 40 - 140 301.7 4,4' -DDE 95 89ND 6.51179125.0 40 - 140 301.7 4,4' -DDT 74 75ND 1.377735.3 40 - 140 301.7 a-BHC 70 74ND 5.6746611.4 40 - 140 301.0 a-Chlordane 68 69ND 1.571667.3 40 - 140 303.3 Aldrin 71 71ND 0.072668.7 40 - 140 301.0 b-BHC 104 122ND 15.91091008.6 40 - 140 301.0 Chlordane 73 75ND 2.777726.7 40 - 140 3033 d-BHC 80 82ND 2.585788.6 40 - 140 303.3 Dieldrin 67 69ND 2.971658.8 40 - 140 301.0 Endosulfan I 61 68ND 10.955608.7 40 - 140 303.3 Page 23 of 32 QA/QC Data Parameter Blk Blank RL MS % MSD % MS RPD SDG I.D.:GCG82052 LCS % LCSD % LCS RPD %Rec Limits %RPD Limits Endosulfan II 73 75ND 2.777735.3 40 - 140 303.3 Endosulfan sulfate 90 97ND 7.590882.2 40 - 140 303.3 Endrin 68 69ND 1.572677.2 40 - 140 303.3 Endrin aldehyde 88 96ND 8.790864.5 40 - 140 303.3 Endrin ketone 82 87ND 5.91068719.7 40 - 140 303.3 g-BHC 73 81ND 10.475698.3 40 - 140 301.0 g-Chlordane 73 75ND 2.777726.7 40 - 140 303.3 Heptachlor 67 69ND 2.969639.1 40 - 140 303.3 Heptachlor epoxide 69 71ND 2.974688.5 40 - 140 303.3 Methoxychlor 104 108ND 3.889828.2 40 - 140 303.3 Toxaphene NA NAND NCNANANC 40 - 140 30130 % DCBP 72 7375 1.479746.5 30 - 150 30% % DCBP (Confirmation)76 7882 2.682793.7 30 - 150 30% % TCMX 66 6871 3.0676011.0 30 - 150 30% % TCMX (Confirmation)70 7178 1.473704.2 30 - 150 30% QA/QC Batch 546304 (ug/kg), QC Sample No: CG82209 (CG82052, CG82053) Semivolatiles - Soil 1,2,4,5-Tetrachlorobenzene 63 73ND 14.766634.7 40 - 140 30230 1,2,4-Trichlorobenzene 59 67ND 12.755533.7 40 - 140 30230 1,2-Dichlorobenzene 51 59ND 14.543399.8 l40 - 140 30180 1,2-Diphenylhydrazine 70 92ND 27.2817211.8 40 - 140 30230 1,3-Dichlorobenzene 49 55ND 11.539368.0 l40 - 140 30230 1,4-Dichlorobenzene 50 59ND 16.5413710.3 l40 - 140 30230 2,4,5-Trichlorophenol 73 85ND 15.2847610.0 40 - 140 30230 2,4,6-Trichlorophenol 71 85ND 17.9827015.8 30 - 130 30130 2,4-Dichlorophenol 63 73ND 14.765633.1 30 - 130 30130 2,4-Dimethylphenol 65 75ND 14.371692.9 30 - 130 30230 2,4-Dinitrophenol 57 63ND 10.0665420.0 30 - 130 30230 2,4-Dinitrotoluene 75 87ND 14.8938113.8 30 - 130 30130 2,6-Dinitrotoluene 72 87ND 18.9897813.2 40 - 140 30130 2-Chloronaphthalene 67 80ND 17.7736610.1 40 - 140 30230 2-Chlorophenol 58 66ND 12.954499.7 30 - 130 30230 2-Methylnaphthalene 60 69ND 14.061576.8 40 - 140 30230 2-Methylphenol (o-cresol)59 72ND 19.858547.1 40 - 140 30230 2-Nitroaniline 110 129ND 15.915213214.1 l40 - 140 30330 2-Nitrophenol 81 90ND 10.580800.0 40 - 140 30230 3&4-Methylphenol (m&p-cresol)64 75ND 15.863588.3 30 - 130 30230 3,3'-Dichlorobenzidine 66 80ND 19.287825.9 40 - 140 30130 3-Nitroaniline 57 72ND 23.3847511.3 40 - 140 30330 4,6-Dinitro-2-methylphenol 63 69ND 9.1786715.2 30 - 130 30230 4-Bromophenyl phenyl ether 76 87ND 13.586824.8 40 - 140 30230 4-Chloro-3-methylphenol 71 82ND 14.480765.1 30 - 130 30230 4-Chloroaniline 53 62ND 15.774714.1 40 - 140 30230 4-Chlorophenyl phenyl ether 73 84ND 14.0867316.4 40 - 140 30230 4-Nitroaniline 81 96ND 16.9978612.0 40 - 140 30230 4-Nitrophenol 88 105ND 17.697898.6 30 - 130 30230 Acenaphthene 70 82ND 15.8796913.5 30 - 130 30230 Acenaphthylene 65 81ND 21.9736511.6 40 - 140 30130 Acetophenone 61 73ND 17.957529.2 40 - 140 30230 Aniline 40 45ND 11.843414.8 40 - 140 30330 Anthracene 70 86ND 20.580747.8 40 - 140 30230 Benz(a)anthracene 88 103ND 15.790829.3 40 - 140 30230 Page 24 of 32 QA/QC Data Parameter Blk Blank RL MS % MSD % MS RPD SDG I.D.:GCG82052 LCS % LCSD % LCS RPD %Rec Limits %RPD Limits Benzidine <10 <10ND NC585112.8 m40 - 140 30330 Benzo(a)pyrene 82 102ND 21.7938410.2 40 - 140 30130 Benzo(b)fluoranthene 98 124ND 23.4107979.8 40 - 140 30160 Benzo(ghi)perylene 66 97ND 38.0847412.7 r40 - 140 30230 Benzo(k)fluoranthene 66 81ND 20.470649.0 40 - 140 30230 Benzoic Acid 60 63ND 4.9704347.8 r30 - 130 30670 Benzyl butyl phthalate 82 98ND 17.897898.6 40 - 140 30230 Bis(2-chloroethoxy)methane 56 63ND 11.858563.5 40 - 140 30230 Bis(2-chloroethyl)ether 43 52ND 18.9413613.0 l40 - 140 30130 Bis(2-chloroisopropyl)ether 45 53ND 16.3423810.0 l40 - 140 30230 Bis(2-ethylhexyl)phthalate 86 101ND 16.099909.5 40 - 140 30230 Carbazole 67 81ND 18.982758.9 40 - 140 30230 Chrysene 82 100ND 19.888818.3 40 - 140 30230 Dibenz(a,h)anthracene 75 99ND 27.6908110.5 40 - 140 30130 Dibenzofuran 68 80ND 16.2796815.0 40 - 140 30230 Diethyl phthalate 77 90ND 15.6948312.4 40 - 140 30230 Dimethylphthalate 73 87ND 17.5908011.8 40 - 140 30230 Di-n-butylphthalate 75 90ND 18.291892.2 40 - 140 30670 Di-n-octylphthalate 83 97ND 15.61089611.8 40 - 140 30230 Fluoranthene 83 98ND 16.681775.1 40 - 140 30230 Fluorene 72 86ND 17.7837214.2 40 - 140 30230 Hexachlorobenzene 81 98ND 19.094904.3 40 - 140 30130 Hexachlorobutadiene 64 73ND 13.160575.1 40 - 140 30230 Hexachlorocyclopentadiene 39 35ND 10.859573.4 m40 - 140 30230 Hexachloroethane 55 63ND 13.646429.1 40 - 140 30130 Indeno(1,2,3-cd)pyrene 66 93ND 34.0877810.9 r40 - 140 30230 Isophorone 57 64ND 11.661576.8 40 - 140 30130 Naphthalene 56 65ND 14.954507.7 40 - 140 30230 Nitrobenzene 63 75ND 17.4605410.5 40 - 140 30130 N-Nitrosodimethylamine 26 30ND 14.3221914.6 l,m40 - 140 30230 N-Nitrosodi-n-propylamine 65 74ND 12.964598.1 40 - 140 30130 N-Nitrosodiphenylamine 72 84ND 15.4887713.3 40 - 140 30130 Pentachloronitrobenzene 87 100ND 13.9101947.2 40 - 140 30230 Pentachlorophenol 74 90ND 19.587817.1 30 - 130 30230 Phenanthrene 78 89ND 13.279746.5 40 - 140 30130 Phenol 58 73ND 22.955517.5 30 - 130 30230 Pyrene 79 99ND 22.580765.1 30 - 130 30230 Pyridine 22 24ND 8.7191711.1 l,m40 - 140 30230 % 2,4,6-Tribromophenol 93 111112 17.6103976.0 30 - 130 30% % 2-Fluorobiphenyl 63 7475 16.168629.2 30 - 130 30% % 2-Fluorophenol 50 5451 7.744409.5 30 - 130 30% % Nitrobenzene-d5 62 7265 14.9595310.7 30 - 130 30% % Phenol-d5 56 6661 16.454507.7 30 - 130 30% % Terphenyl-d14 68 8992 26.889845.8 30 - 130 30% Additional 8270 criteria: 20% of compounds can be outside of acceptance criteria as long as recovery is at least 10%. (Acid surrogates acceptance range for aqueous samples: 15-110%, for soils 30-130%) Comment: QA/QC Batch 546392 (ug/kg), QC Sample No: CG81774 (CG82052, CG82053, CG82054, CG82055) Volatiles - Soil (Low Level) 1,1,1,2-Tetrachloroethane ND 101 107 5.8 70 - 130 305.0 1,1,1-Trichloroethane ND 86 93 7.8 70 - 130 305.0 1,1,2,2-Tetrachloroethane ND 93 101 8.2 70 - 130 303.0 Page 25 of 32 QA/QC Data Parameter Blk Blank RL MS % MSD % MS RPD SDG I.D.:GCG82052 LCS % LCSD % LCS RPD %Rec Limits %RPD Limits 1,1,2-Trichloroethane ND 95 102 7.1 70 - 130 305.0 1,1-Dichloroethane ND 82 89 8.2 70 - 130 305.0 1,1-Dichloroethene ND 78 82 5.0 70 - 130 305.0 1,1-Dichloropropene ND 88 96 8.7 70 - 130 305.0 1,2,3-Trichlorobenzene ND 89 95 6.5 70 - 130 305.0 1,2,3-Trichloropropane ND 82 89 8.2 70 - 130 305.0 1,2,4-Trichlorobenzene ND 87 94 7.7 70 - 130 305.0 1,2,4-Trimethylbenzene ND 89 96 7.6 70 - 130 301.0 1,2-Dibromo-3-chloropropane ND 111 120 7.8 70 - 130 305.0 1,2-Dibromoethane ND 96 104 8.0 70 - 130 305.0 1,2-Dichlorobenzene ND 89 94 5.5 70 - 130 305.0 1,2-Dichloroethane ND 86 93 7.8 70 - 130 305.0 1,2-Dichloropropane ND 87 94 7.7 70 - 130 305.0 1,3,5-Trimethylbenzene ND 89 95 6.5 70 - 130 301.0 1,3-Dichlorobenzene ND 91 97 6.4 70 - 130 305.0 1,3-Dichloropropane ND 91 98 7.4 70 - 130 305.0 1,4-Dichlorobenzene ND 89 94 5.5 70 - 130 305.0 1,4-dioxane ND 85 96 12.2 70 - 130 30100 2,2-Dichloropropane ND 87 93 6.7 70 - 130 305.0 2-Chlorotoluene ND 91 97 6.4 70 - 130 305.0 2-Hexanone ND 125 131 4.7 l70 - 130 3025 2-Isopropyltoluene ND 99 105 5.9 70 - 130 305.0 4-Chlorotoluene ND 90 96 6.5 70 - 130 305.0 4-Methyl-2-pentanone ND 92 99 7.3 70 - 130 3025 Acetone ND 136 142 4.3 l70 - 130 3010 Acrylonitrile ND 88 95 7.7 70 - 130 305.0 Benzene ND 91 98 7.4 70 - 130 301.0 Bromobenzene ND 91 96 5.3 70 - 130 305.0 Bromochloromethane ND 91 96 5.3 70 - 130 305.0 Bromodichloromethane ND 96 103 7.0 70 - 130 305.0 Bromoform ND 105 111 5.6 70 - 130 305.0 Bromomethane ND 80 89 10.7 70 - 130 305.0 Carbon Disulfide ND 77 82 6.3 70 - 130 305.0 Carbon tetrachloride ND 88 94 6.6 70 - 130 305.0 Chlorobenzene ND 92 98 6.3 70 - 130 305.0 Chloroethane ND 80 89 10.7 70 - 130 305.0 Chloroform ND 84 92 9.1 70 - 130 305.0 Chloromethane ND 80 88 9.5 70 - 130 305.0 cis-1,2-Dichloroethene ND 82 88 7.1 70 - 130 305.0 cis-1,3-Dichloropropene ND 92 99 7.3 70 - 130 305.0 Dibromochloromethane ND 106 116 9.0 70 - 130 303.0 Dibromomethane ND 89 95 6.5 70 - 130 305.0 Dichlorodifluoromethane ND 105 112 6.5 70 - 130 305.0 Ethylbenzene ND 93 99 6.3 70 - 130 301.0 Hexachlorobutadiene ND 94 98 4.2 70 - 130 305.0 Isopropylbenzene ND 91 96 5.3 70 - 130 301.0 m&p-Xylene ND 92 98 6.3 70 - 130 302.0 Methyl ethyl ketone ND 132 142 7.3 l70 - 130 305.0 Methyl t-butyl ether (MTBE)ND 73 79 7.9 70 - 130 301.0 Methylene chloride ND 65 71 8.8 l70 - 130 305.0 Naphthalene ND 95 102 7.1 70 - 130 305.0 n-Butylbenzene ND 90 97 7.5 70 - 130 301.0 n-Propylbenzene ND 91 97 6.4 70 - 130 301.0 Page 26 of 32 QA/QC Data Parameter Blk Blank RL MS % MSD % MS RPD SDG I.D.:GCG82052 LCS % LCSD % LCS RPD %Rec Limits %RPD Limits o-Xylene ND 95 101 6.1 70 - 130 302.0 p-Isopropyltoluene ND 93 99 6.3 70 - 130 301.0 sec-Butylbenzene ND 98 105 6.9 70 - 130 301.0 Styrene ND 95 102 7.1 70 - 130 305.0 tert-Butylbenzene ND 92 97 5.3 70 - 130 301.0 Tetrachloroethene ND 98 103 5.0 70 - 130 305.0 Tetrahydrofuran (THF)ND 80 86 7.2 70 - 130 305.0 Toluene ND 95 101 6.1 70 - 130 301.0 trans-1,2-Dichloroethene ND 78 84 7.4 70 - 130 305.0 trans-1,3-Dichloropropene ND 93 100 7.3 70 - 130 305.0 trans-1,4-dichloro-2-butene ND 108 117 8.0 70 - 130 305.0 Trichloroethene ND 92 99 7.3 70 - 130 305.0 Trichlorofluoromethane ND 80 88 9.5 70 - 130 305.0 Trichlorotrifluoroethane ND 78 82 5.0 70 - 130 305.0 Vinyl chloride ND 83 91 9.2 70 - 130 305.0 % 1,2-dichlorobenzene-d4 97 99 99 0.0 70 - 130 30% % Bromofluorobenzene 104 104 103 1.0 70 - 130 30% % Dibromofluoromethane 96 103 101 2.0 70 - 130 30% % Toluene-d8 103 100 101 1.0 70 - 130 30% The Low Level MS/MSD are not reported for this batch. Additional 8260 criteria: 10% of LCS/LCSD compounds can be outside of acceptance criteria as long as recovery is 40-160%, 25-160% for Chloroethane-HL and Trichlorofluoromethane-HL. Comment: l = This parameter is outside laboratory LCS/LCSD specified recovery limits. m = This parameter is outside laboratory MS/MSD specified recovery limits. r = This parameter is outside laboratory RPD specified recovery limits. MS - Matrix Spike Phyllis Shiller, Laboratory Director If there are any questions regarding this data, please call Phoenix Client Services at extension 200. September 24, 2020MS Dup - Matrix Spike Duplicate RPD - Relative Percent Difference LCS - Laboratory Control Sample LCSD - Laboratory Control Sample Duplicate NC - No Criteria Intf - Interference Page 27 of 32 Sample Criteria Exceedances ReportThursday, September 24, 2020 Acode Phoenix Analyte CriteriaResultRLSampNo Analysis UnitsCriteria GCG82052 - ENV-SCICriteria:None RL Criteria State:NY #Type!*** No Data to Display *** Phoenix Laboratories does not assume responsibility for the data contained in this exceedance report. It is provided as an additional tool to identify requested criteria exceedences. All efforts are made to ensure the accuracy of the data (obtained from appropriate agencies). A lack of exceedence information does not necessarily suggest conformance to the criteria. It is ultimately the site professional's responsibility to determine appropriate compliance. Page 28 of 32 Analysis Comments September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 The following analysis comments are made regarding exceptions to criteria not already noted in the Analysis Report or QA/QC Report: Herbicide Narration CG82052, CG82053AU-ECD12 09/22/20-1: The following Continuing Calibration compounds did not meet % deviation criteria: Samples: CG82052, CG82053 Preceding CC 922B015 - 2,4,5-T (11) 22%H (15%), Dalapon (1) 27%H (15%), Dinoseb 17%H (15%) Succeeding CC 922B027 - None. PCB Narration CG82053AU-ECD8 09/22/20-1: The following Continuing Calibration compounds did not meet % deviation criteria: Samples: CG82053 Preceding CC 922B037 - TCMX SURR 18%L (15%) Succeeding CC 922B049 - None. PEST Narration CG82052, CG82053AU-ECD7 09/22/20-1: The following Continuing Calibration compounds did not meet % deviation criteria: Samples: CG82052, CG82053 Preceding CC 922A031 - b-BHC 21%L (20%), Endrin 21%L (20%) Succeeding CC 922A038 - Endrin 22%L (20%) A low "1A" standard was run after the samples to demonstrate capability to detect any compounds outside of the CC acceptance criteria. All reported samples were ND for the affected compounds. SVOA Narration CG82052, CG82053CHEM07 09/21/20-2: For 8270 full list, the DDT breakdown and pentachlorophenol & benzidine peak tailing were evaluated in the DFTPP tune and were found to be in control. For 8270 BN list, benzidine peak tailing was evaluated in the DFTPP tune and was found to be in control. The following Initial Calibration compounds did not meet recommended response factors: 2-Nitrophenol 0.073 (0.1), Hexachlorobenzene 0.084 (0.1) The following Initial Calibration compounds did not meet minimum response factors: None. The following Continuing Calibration compounds did not meet recommended response factors: 2-Nitrophenol 0.075 (0.1), Hexachlorobenzene 0.089 (0.1) The following Continuing Calibration compounds did not meet minimum response factors: None. Up to eight compounds can be outside of ICAL %RSD criteria and up to sixteen compounds can be outside of CCAL %Dev criteria if less than 40%. VOA Narration CG82052, CG82053, CG82054, CG82055CHEM03 09/21/20-2: Page 29 of 32 Analysis Comments September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 The following Initial Calibration compounds did not meet RSD% criteria: 1,1,1,2-Tetrachloroethane 21% (20%), 1,2-Dibromo-3-chloropropane 26% (20%), Bromoform 34% (20%), Chloroethane 22% (20%), Dibromochloromethane 23% (20%), trans-1,4-dichloro-2-butene 35% (20%) The following Initial Calibration compounds did not meet maximum RSD% criteria: None. The following Initial Calibration compounds did not meet recommended response factors: 1,2-Dibromo-3-chloropropane 0.049 (0.05), Bromoform 0.069 (0.1), Tetrachloroethene 0.126 (0.2) The following Initial Calibration compounds did not meet minimum response factors: 1,2-Dibromo-3-chloropropane 0.049 (0.05) Up to eight compounds can be outside of ICAL %RSD criteria and up to sixteen compounds can be outside of CCAL %Dev criteria if less than 40%. Page 30 of 32 NY Temperature Narration September 24, 2020 587 East Middle Turnpike, P.O.Box 370, Manchester, CT 06045 Tel. (860) 645-1102 Fax (860) 645-0823 Environmental Laboratories, Inc. SDG I.D.:GCG82052 The samples in this delivery group were received at 2.0°C. (Note acceptance criteria for relevant matrices is above freezing up to 6°C) Page 31 of 32 Page 32 of 32