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DATA VALIDATION AND QUALIFICATION SUMMARY Laboratory Numbers:2151491 Sample ID Analyte(s) Qualifier Reason(s) VOCs All samples Acetone,bromomethane UB if Detected in the Trip blank and chloromethane detected and/or method blank MW-31), MW-51) and MW-8D 1,4-Dichlorobenzene J The %Rs were above the QC limits in the MS and/or MSD Metals All samples Silver UJ The %R was below QC limit in the spike sample General Chemistry All samples Hexavalent chromium MW-11),MW-1S,MW-4S and Cyanide J/UJ Analyzed outside the holding MW-5S time MW-4S Nitrate MW-3S,MW-5S,MW-6S, Phenolics MW-8S and MW-8D UB Detected in the method blank All samples Total kjeldahl nitrogen J,if The%R was above QC limits (T,N) detected in the MSD All samples except MW-1SHexavalent chromium MW-04D Cyanide J/LTJ The %Rs were below QC limits in the MS and/or MSD VALIDATION PERFORMED BY&DATE: Donna M.Brown 8/22/2016 VALIDATION PERFORMED BY SIGNATURE: Pages \\dbfsl\Jobs\HazWaste\3753(Southold Landfill)A1st 2016 GW Report\2151491 Jun_2016.doc 6/6