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HomeMy WebLinkAbout8071127 Turtle Properties 825 Pacific St LRPage 1 of 12 Laboratory Report LIAL# 8071127 July 19, 2018 Turtle Properties Inc Joe Morgano 2 Fort Lane Re: 825 Pacific Street Mattituck Dear Joe Morgano, Enclosed please find the laboratory Analysis Report(s) for sample(s) received on July 11, 2018. Long Island Analytical laboratories analyzed the samples on July 17, 2018 for the following: Montauk, NY 11954 ANALYSIS SAMPLE ID CP-51 Table 3 Semi-Volatiles, CP-51 Table 3 VolatilesNorth Wall CP-51 Table 3 Semi-Volatiles, CP-51 Table 3 VolatilesSouth Wall CP-51 Table 3 Semi-Volatiles, CP-51 Table 3 VolatilesEast Wall CP-51 Table 3 Semi-Volatiles, CP-51 Table 3 VolatilesWest Wall CP-51 Table 3 Semi-Volatiles, CP-51 Table 3 VolatilesFloor Samples received at 3.6 C Long Island Analytical Laboratories, Inc.Michael Veraldi - Laboratory Director If you have any questions or require further information, please call at your convenience. Long Island Analytical Laboratories Inc. is a NELAP accredited laboratory. All reported results meet the requirements of the NELAP standards unless noted. Report shall not be reproduced except in full without the written approval of the laboratory. Results related only to items tested. Long Island Analytical Laboratories would like to thank you for the opportunity to be of service to you. Best Regards, Page 2 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-01 ELAP: #11693 Sample ID: North Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:35 % Solid:97.58 Volatiles Low Level Analysis Parameter LOQCAS No.Result Units Flag 1,2,4-Trimethylbenzene 95-63-6 <9.97 ug/kg dry9.97 1,3,5-Trimethylbenzene 108-67-8 <9.97 ug/kg dry9.97 4-Isopropyltoluene 99-87-6 <9.97 ug/kg dry9.97 Ethylbenzene 100-41-4 <9.97 ug/kg dry9.97 Isopropylbenzene (Cumene)98-82-8 <9.97 ug/kg dry9.97 m,p-Xylenes 108-38-3/106-42-3 <19.9 ug/kg dry19.9 Methyl-tert-Butyl Ether 1634-04-4 <9.97 ug/kg dry9.97 Naphthalene 91-20-3 <9.97 ug/kg dry9.97 n-Butylbenzene 104-51-8 <9.97 ug/kg dry9.97 n-Propylbenzene 103-65-1 <9.97 ug/kg dry9.97 o-Xylene 95-47-6 <9.97 ug/kg dry9.97 sec-Butylbenzene 135-98-8 <9.97 ug/kg dry9.97 tert-Butylbenzene 98-06-6 <9.97 ug/kg dry9.97 Toluene 108-88-3 <9.97 ug/kg dry9.97 Surrogate CAS No.% Recovery Rec. Limits Flag 1,2-Dichloroethane-d4 10706-07-0 104 71.6-131 4-Bromofluorobenzene 460-00-4 114 75.4-133 Dibromofluoromethane 1868-53-7 118 75.6-135 Toluene-d8 2037-26-5 98 79.9-123 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 76 1,4-Difluorobenzene 50-200540-36-3 98 Chlorobenzene-d5 50-2003114-55-4 101 Pentafluorobenzene 50-200363-72-4 92 Date Prepared: 07/16/2018 Date Analyzed: 07/16/2018 Analytical Method: EPA 8260 C Preparation Method: EPA 5035A-L Page 3 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-01 ELAP: #11693 Sample ID: North Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:35 % Solid:97.58 Semivolatile Analysis Parameter LOQCAS No.Result Units Flag Acenaphthene 83-32-9 <154 ug/kg dry 4.T154 Acenaphthylene 208-96-8 <154 ug/kg dry154 Anthracene 120-12-7 <154 ug/kg dry 4.T154 Benzo(a)anthracene 56-55-3 <154 ug/kg dry154 Benzo(a)pyrene 50-32-8 <154 ug/kg dry154 Benzo(b)fluoranthene 205-99-2 <307 ug/kg dry307 Benzo(g,h,i)perylene 191-24-2 <154 ug/kg dry154 Benzo(k)fluoranthene 207-08-9 <154 ug/kg dry154 Chrysene 218-01-9 <154 ug/kg dry154 Dibenzo(a,h)anthracene 53-70-3 <154 ug/kg dry 4.T154 Fluoranthene 206-44-0 <154 ug/kg dry154 Fluorene 86-73-7 <154 ug/kg dry154 Indeno(1,2,3-cd)pyrene 193-39-5 <154 ug/kg dry154 Phenanthrene 85-01-8 <154 ug/kg dry154 Pyrene 129-00-0 <154 ug/kg dry154 Surrogate CAS No.% Recovery Rec. Limits Flag 2-Fluorobiphenyl 321-60-8 36 32.6-96.2 Nitrobenzene-d5 4165-60-0 41 28.1-100 Terphenyl-d14 1718-51-0 41 32.6-110 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 129 Acenaphthene-d10 50-20015067-26-2 121 Chrysene-d12 50-2001719-03-5 119 Naphthalene-d8 50-2001146-65-2 123 Perylene-d12 50-2001520-96-3 120 Phenanthrene-d10 50-2001517-22-2 119 Date Prepared: 07/12/2018 Date Analyzed: 07/13/2018 Analytical Method: EPA 8270 D Preparation Method: EPA 3545 A Page 4 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-02 ELAP: #11693 Sample ID: South Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:39 % Solid:99.12 Volatiles Low Level Analysis Parameter LOQCAS No.Result Units Flag 1,2,4-Trimethylbenzene 95-63-6 <10.9 ug/kg dry10.9 1,3,5-Trimethylbenzene 108-67-8 <10.9 ug/kg dry10.9 4-Isopropyltoluene 99-87-6 <10.9 ug/kg dry10.9 Ethylbenzene 100-41-4 <10.9 ug/kg dry10.9 Isopropylbenzene (Cumene)98-82-8 <10.9 ug/kg dry10.9 m,p-Xylenes 108-38-3/106-42-3 <21.8 ug/kg dry21.8 Methyl-tert-Butyl Ether 1634-04-4 <10.9 ug/kg dry10.9 Naphthalene 91-20-3 <10.9 ug/kg dry10.9 n-Butylbenzene 104-51-8 <10.9 ug/kg dry10.9 n-Propylbenzene 103-65-1 <10.9 ug/kg dry10.9 o-Xylene 95-47-6 <10.9 ug/kg dry10.9 sec-Butylbenzene 135-98-8 <10.9 ug/kg dry10.9 tert-Butylbenzene 98-06-6 <10.9 ug/kg dry10.9 Toluene 108-88-3 <10.9 ug/kg dry10.9 Surrogate CAS No.% Recovery Rec. Limits Flag 1,2-Dichloroethane-d4 10706-07-0 106 71.6-131 4-Bromofluorobenzene 460-00-4 115 75.4-133 Dibromofluoromethane 1868-53-7 122 75.6-135 Toluene-d8 2037-26-5 99 79.9-123 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 68 1,4-Difluorobenzene 50-200540-36-3 89 Chlorobenzene-d5 50-2003114-55-4 92 Pentafluorobenzene 50-200363-72-4 82 Date Prepared: 07/16/2018 Date Analyzed: 07/16/2018 Analytical Method: EPA 8260 C Preparation Method: EPA 5035A-L Page 5 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-02 ELAP: #11693 Sample ID: South Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:39 % Solid:99.12 Semivolatile Analysis Parameter LOQCAS No.Result Units Flag Acenaphthene 83-32-9 <151 ug/kg dry151 Acenaphthylene 208-96-8 <151 ug/kg dry151 Anthracene 120-12-7 <151 ug/kg dry151 Benzo(a)anthracene 56-55-3 <151 ug/kg dry151 Benzo(a)pyrene 50-32-8 <151 ug/kg dry151 Benzo(b)fluoranthene 205-99-2 <303 ug/kg dry303 Benzo(g,h,i)perylene 191-24-2 <151 ug/kg dry151 Benzo(k)fluoranthene 207-08-9 <151 ug/kg dry151 Chrysene 218-01-9 <151 ug/kg dry151 Dibenzo(a,h)anthracene 53-70-3 <151 ug/kg dry151 Fluoranthene 206-44-0 <151 ug/kg dry151 Fluorene 86-73-7 <151 ug/kg dry151 Indeno(1,2,3-cd)pyrene 193-39-5 <151 ug/kg dry151 Phenanthrene 85-01-8 <151 ug/kg dry151 Pyrene 129-00-0 <151 ug/kg dry151 Surrogate CAS No.% Recovery Rec. Limits Flag 2-Fluorobiphenyl 321-60-8 4.D3132.6-96.2 Nitrobenzene-d5 4165-60-0 35 28.1-100 Terphenyl-d14 1718-51-0 37 32.6-110 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 119 Acenaphthene-d10 50-20015067-26-2 115 Chrysene-d12 50-2001719-03-5 114 Naphthalene-d8 50-2001146-65-2 117 Perylene-d12 50-2001520-96-3 116 Phenanthrene-d10 50-2001517-22-2 114 Date Prepared: 07/12/2018 Date Analyzed: 07/13/2018 Analytical Method: EPA 8270 D Preparation Method: EPA 3545 A Page 6 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-03 ELAP: #11693 Sample ID: East Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:45 % Solid:95.09 Volatiles Low Level Analysis Parameter LOQCAS No.Result Units Flag 1,2,4-Trimethylbenzene 95-63-6 <10.1 ug/kg dry10.1 1,3,5-Trimethylbenzene 108-67-8 <10.1 ug/kg dry10.1 4-Isopropyltoluene 99-87-6 <10.1 ug/kg dry10.1 Ethylbenzene 100-41-4 <10.1 ug/kg dry10.1 Isopropylbenzene (Cumene)98-82-8 <10.1 ug/kg dry10.1 m,p-Xylenes 108-38-3/106-42-3 <20.2 ug/kg dry20.2 Methyl-tert-Butyl Ether 1634-04-4 <10.1 ug/kg dry10.1 Naphthalene 91-20-3 <10.1 ug/kg dry10.1 n-Butylbenzene 104-51-8 <10.1 ug/kg dry10.1 n-Propylbenzene 103-65-1 <10.1 ug/kg dry10.1 o-Xylene 95-47-6 <10.1 ug/kg dry10.1 sec-Butylbenzene 135-98-8 <10.1 ug/kg dry10.1 tert-Butylbenzene 98-06-6 <10.1 ug/kg dry10.1 Toluene 108-88-3 <10.1 ug/kg dry10.1 Surrogate CAS No.% Recovery Rec. Limits Flag 1,2-Dichloroethane-d4 10706-07-0 106 71.6-131 4-Bromofluorobenzene 460-00-4 116 75.4-133 Dibromofluoromethane 1868-53-7 125 75.6-135 Toluene-d8 2037-26-5 97 79.9-123 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 65 1,4-Difluorobenzene 50-200540-36-3 85 Chlorobenzene-d5 50-2003114-55-4 89 Pentafluorobenzene 50-200363-72-4 77 Date Prepared: 07/16/2018 Date Analyzed: 07/16/2018 Analytical Method: EPA 8260 C Preparation Method: EPA 5035A-L Page 7 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-03 ELAP: #11693 Sample ID: East Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:45 % Solid:95.09 Semivolatile Analysis Parameter LOQCAS No.Result Units Flag Acenaphthene 83-32-9 <158 ug/kg dry158 Acenaphthylene 208-96-8 <158 ug/kg dry158 Anthracene 120-12-7 <158 ug/kg dry158 Benzo(a)anthracene 56-55-3 <158 ug/kg dry158 Benzo(a)pyrene 50-32-8 <158 ug/kg dry158 Benzo(b)fluoranthene 205-99-2 <315 ug/kg dry315 Benzo(g,h,i)perylene 191-24-2 <158 ug/kg dry158 Benzo(k)fluoranthene 207-08-9 <158 ug/kg dry158 Chrysene 218-01-9 <158 ug/kg dry158 Dibenzo(a,h)anthracene 53-70-3 <158 ug/kg dry158 Fluoranthene 206-44-0 <158 ug/kg dry158 Fluorene 86-73-7 <158 ug/kg dry158 Indeno(1,2,3-cd)pyrene 193-39-5 <158 ug/kg dry158 Phenanthrene 85-01-8 <158 ug/kg dry158 Pyrene 129-00-0 <158 ug/kg dry158 Surrogate CAS No.% Recovery Rec. Limits Flag 2-Fluorobiphenyl 321-60-8 54 32.6-96.2 Nitrobenzene-d5 4165-60-0 57 28.1-100 Terphenyl-d14 1718-51-0 64 32.6-110 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 122 Acenaphthene-d10 50-20015067-26-2 118 Chrysene-d12 50-2001719-03-5 113 Naphthalene-d8 50-2001146-65-2 115 Perylene-d12 50-2001520-96-3 116 Phenanthrene-d10 50-2001517-22-2 115 Date Prepared: 07/12/2018 Date Analyzed: 07/13/2018 Analytical Method: EPA 8270 D Preparation Method: EPA 3545 A Page 8 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-04 ELAP: #11693 Sample ID: West Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:48 % Solid:96.77 Volatiles Low Level Analysis Parameter LOQCAS No.Result Units Flag 1,2,4-Trimethylbenzene 95-63-6 <10.3 ug/kg dry10.3 1,3,5-Trimethylbenzene 108-67-8 <10.3 ug/kg dry10.3 4-Isopropyltoluene 99-87-6 <10.3 ug/kg dry 4.N10.3 Ethylbenzene 100-41-4 <10.3 ug/kg dry 4.T10.3 Isopropylbenzene (Cumene)98-82-8 <10.3 ug/kg dry10.3 m,p-Xylenes 108-38-3/106-42-3 <20.6 ug/kg dry 4.T20.6 Methyl-tert-Butyl Ether 1634-04-4 <10.3 ug/kg dry 4.G, 4.T10.3 Naphthalene 91-20-3 <10.3 ug/kg dry 4.G, 4.N, 4.T10.3 n-Butylbenzene 104-51-8 <10.3 ug/kg dry 4.N10.3 n-Propylbenzene 103-65-1 <10.3 ug/kg dry10.3 o-Xylene 95-47-6 <10.3 ug/kg dry 4.T10.3 sec-Butylbenzene 135-98-8 <10.3 ug/kg dry10.3 tert-Butylbenzene 98-06-6 <10.3 ug/kg dry10.3 Toluene 108-88-3 <10.3 ug/kg dry 4.T10.3 Surrogate CAS No.% Recovery Rec. Limits Flag 1,2-Dichloroethane-d4 10706-07-0 104 71.6-131 4-Bromofluorobenzene 460-00-4 121 75.4-133 Dibromofluoromethane 1868-53-7 127 75.6-135 Toluene-d8 2037-26-5 97 79.9-123 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 69 1,4-Difluorobenzene 50-200540-36-3 96 Chlorobenzene-d5 50-2003114-55-4 99 Pentafluorobenzene 50-200363-72-4 93 Date Prepared: 07/17/2018 Date Analyzed: 07/17/2018 Analytical Method: EPA 8260 C Preparation Method: EPA 5035A-L Page 9 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-04 ELAP: #11693 Sample ID: West Wall Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:48 % Solid:96.77 Semivolatile Analysis Parameter LOQCAS No.Result Units Flag Acenaphthene 83-32-9 <155 ug/kg dry155 Acenaphthylene 208-96-8 <155 ug/kg dry155 Anthracene 120-12-7 <155 ug/kg dry155 Benzo(a)anthracene 56-55-3 <155 ug/kg dry155 Benzo(a)pyrene 50-32-8 <155 ug/kg dry155 Benzo(b)fluoranthene 205-99-2 <310 ug/kg dry310 Benzo(g,h,i)perylene 191-24-2 <155 ug/kg dry155 Benzo(k)fluoranthene 207-08-9 <155 ug/kg dry155 Chrysene 218-01-9 <155 ug/kg dry155 Dibenzo(a,h)anthracene 53-70-3 <155 ug/kg dry155 Fluoranthene 206-44-0 <155 ug/kg dry155 Fluorene 86-73-7 <155 ug/kg dry155 Indeno(1,2,3-cd)pyrene 193-39-5 <155 ug/kg dry155 Phenanthrene 85-01-8 <155 ug/kg dry155 Pyrene 129-00-0 <155 ug/kg dry155 Surrogate CAS No.% Recovery Rec. Limits Flag 2-Fluorobiphenyl 321-60-8 45 32.6-96.2 Nitrobenzene-d5 4165-60-0 51 28.1-100 Terphenyl-d14 1718-51-0 61 32.6-110 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 126 Acenaphthene-d10 50-20015067-26-2 122 Chrysene-d12 50-2001719-03-5 120 Naphthalene-d8 50-2001146-65-2 123 Perylene-d12 50-2001520-96-3 122 Phenanthrene-d10 50-2001517-22-2 120 Date Prepared: 07/12/2018 Date Analyzed: 07/13/2018 Analytical Method: EPA 8270 D Preparation Method: EPA 3545 A Page 10 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-05 ELAP: #11693 Sample ID: Floor Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:56 % Solid:99.35 Volatiles Low Level Analysis Parameter LOQCAS No.Result Units Flag 1,2,4-Trimethylbenzene 95-63-6 <9.57 ug/kg dry9.57 1,3,5-Trimethylbenzene 108-67-8 <9.57 ug/kg dry9.57 4-Isopropyltoluene 99-87-6 <9.57 ug/kg dry 4.N9.57 Ethylbenzene 100-41-4 <9.57 ug/kg dry9.57 Isopropylbenzene (Cumene)98-82-8 <9.57 ug/kg dry9.57 m,p-Xylenes 108-38-3/106-42-3 <19.1 ug/kg dry19.1 Methyl-tert-Butyl Ether 1634-04-4 <9.57 ug/kg dry9.57 Naphthalene 91-20-3 <9.57 ug/kg dry 4.N9.57 n-Butylbenzene 104-51-8 <9.57 ug/kg dry 4.N9.57 n-Propylbenzene 103-65-1 <9.57 ug/kg dry9.57 o-Xylene 95-47-6 <9.57 ug/kg dry9.57 sec-Butylbenzene 135-98-8 <9.57 ug/kg dry9.57 tert-Butylbenzene 98-06-6 <9.57 ug/kg dry9.57 Toluene 108-88-3 <9.57 ug/kg dry9.57 Surrogate CAS No.% Recovery Rec. Limits Flag 1,2-Dichloroethane-d4 10706-07-0 111 71.6-131 4-Bromofluorobenzene 460-00-4 121 75.4-133 Dibromofluoromethane 1868-53-7 133 75.6-135 Toluene-d8 2037-26-5 97 79.9-123 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 69 1,4-Difluorobenzene 50-200540-36-3 91 Chlorobenzene-d5 50-2003114-55-4 96 Pentafluorobenzene 50-200363-72-4 87 Date Prepared: 07/17/2018 Date Analyzed: 07/17/2018 Analytical Method: EPA 8260 C Preparation Method: EPA 5035A-L Page 11 of 12 Client: Turtle Properties Inc Date (Time) Received: 07/11/2018 16:08 Matrix: Soil Laboratory ID: 8071127-05 ELAP: #11693 Sample ID: Floor Client ID: 825 Pacific Street Mattituck Date (Time) Collected: 07/11/2018 11:56 % Solid:99.35 Semivolatile Analysis Parameter LOQCAS No.Result Units Flag Acenaphthene 83-32-9 <151 ug/kg dry151 Acenaphthylene 208-96-8 <151 ug/kg dry151 Anthracene 120-12-7 <151 ug/kg dry151 Benzo(a)anthracene 56-55-3 <151 ug/kg dry151 Benzo(a)pyrene 50-32-8 <151 ug/kg dry151 Benzo(b)fluoranthene 205-99-2 <302 ug/kg dry302 Benzo(g,h,i)perylene 191-24-2 <151 ug/kg dry151 Benzo(k)fluoranthene 207-08-9 <151 ug/kg dry151 Chrysene 218-01-9 <151 ug/kg dry151 Dibenzo(a,h)anthracene 53-70-3 <151 ug/kg dry151 Fluoranthene 206-44-0 <151 ug/kg dry151 Fluorene 86-73-7 <151 ug/kg dry151 Indeno(1,2,3-cd)pyrene 193-39-5 <151 ug/kg dry151 Phenanthrene 85-01-8 <151 ug/kg dry151 Pyrene 129-00-0 <151 ug/kg dry151 Surrogate CAS No.% Recovery Rec. Limits Flag 2-Fluorobiphenyl 321-60-8 48 32.6-96.2 Nitrobenzene-d5 4165-60-0 53 28.1-100 Terphenyl-d14 1718-51-0 61 32.6-110 Internal Standard CAS No.FlagRec. Limits% Recovery 1,4-Dichlorobenzene-d4 50-2003855-82-1 125 Acenaphthene-d10 50-20015067-26-2 118 Chrysene-d12 50-2001719-03-5 113 Naphthalene-d8 50-2001146-65-2 119 Perylene-d12 50-2001520-96-3 115 Phenanthrene-d10 50-2001517-22-2 115 Date Prepared: 07/12/2018 Date Analyzed: 07/13/2018 Analytical Method: EPA 8270 D Preparation Method: EPA 3545 A Page 12 of 12 Data Qualifiers Key Reference: 4.D Surrogate recovery has failed low. 4.G Spike recovery out of range due to matrix interference. 4.N LCS recovery was below QC acceptance limit. 4.T Sample Matrix Spike/Spike Dup RPD is above acceptable range. Minimum Detection LimitMDL LOQ Limit of Quantitation